#------------------------------------------------------------------------------ #$Date: 2018-01-13 08:33:57 +0200 (Sat, 13 Jan 2018) $ #$Revision: 205185 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/54/86/1548677.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1548677 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.9241 _cell_length_b 9.7350 _cell_length_c 22.4440 _exptl_crystal_F_000 704.00 _reflns_d_resolution_high 0.7707 _cod_data_source_file tk4042Isup2.hkl _cod_data_source_block I _shelx_title ' x792cout_a.res in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 194.14 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 89.64 36.60 9.87 o 4 0 0 385.83 325.86 32.40 o 6 0 0 2004.38 2225.67 158.64 o 2 1 0 19336.87 20394.44 857.60 o 4 1 0 1481.71 1661.68 66.07 o 6 1 0 73.46 91.13 26.62 o 0 2 0 5248.36 5361.73 106.88 o 2 2 0 227.38 251.32 17.29 o 4 2 0 2304.35 2282.57 196.44 o 6 2 0 962.10 1102.26 111.30 o 2 3 0 13.13 38.50 8.67 o 4 3 0 1185.38 1168.91 77.25 o 6 3 0 0.17 -5.83 18.18 o 0 4 0 1710.69 1695.12 86.87 o 2 4 0 1937.97 2307.39 73.26 o 4 4 0 0.26 37.50 18.51 o 6 4 0 94.61 152.77 42.53 o 2 5 0 6123.92 6762.40 179.15 o 4 5 0 15.71 62.68 37.54 o 6 5 0 181.03 170.95 47.31 o 0 6 0 6405.13 6582.69 1083.36 o 2 6 0 54.52 75.14 14.83 o 4 6 0 961.86 942.36 109.65 o 6 6 0 351.16 329.73 78.52 o 2 7 0 2156.89 1957.18 119.59 o 4 7 0 213.10 220.64 40.99 o 6 7 0 29.35 32.97 31.37 o 0 8 0 6.06 9.18 13.79 o 2 8 0 329.74 347.84 45.76 o 4 8 0 123.70 121.46 58.51 o 2 9 0 1568.41 1612.61 193.82 o 4 9 0 303.51 275.72 58.82 o 0 10 0 241.07 222.32 72.03 o 2 10 0 2096.83 1863.75 180.04 o 4 10 0 187.16 220.17 55.57 o 2 11 0 53.70 65.62 22.86 o 0 12 0 569.54 522.04 92.01 o 2 12 0 279.36 349.53 94.02 o 1 1 1 27.15 50.92 3.44 o 2 1 1 5323.58 5643.65 147.42 o 3 1 1 344.16 362.28 14.71 o 4 1 1 378.68 410.06 18.88 o 5 1 1 44.35 38.86 8.72 o 6 1 1 584.99 592.40 35.77 o 7 1 1 200.82 258.79 41.37 o 0 2 1 78.44 123.43 14.78 o 1 2 1 252.87 294.17 30.98 o 2 2 1 909.88 967.62 27.02 o 3 2 1 551.82 561.77 20.86 o 4 2 1 1161.04 1205.91 38.65 o 5 2 1 231.79 262.90 30.20 o 6 2 1 423.51 539.29 38.41 o 7 2 1 27.53 11.69 13.97 o 1 3 1 4203.61 4742.37 163.91 o 2 3 1 20.24 32.44 5.95 o 3 3 1 691.92 741.55 34.23 o 4 3 1 134.66 144.53 13.63 o 5 3 1 2.47 8.14 9.45 o 6 3 1 10.51 8.19 11.18 o 7 3 1 55.80 56.78 26.34 o 0 4 1 8467.47 8766.46 565.03 o 1 4 1 1290.59 1427.89 36.01 o 2 4 1 329.87 350.65 16.33 o 3 4 1 352.53 394.63 23.79 o 4 4 1 1267.81 1258.52 79.82 o 5 4 1 172.49 197.42 23.12 o 6 4 1 269.81 313.29 31.16 o 7 4 1 27.71 34.39 16.49 o 1 5 1 115.76 126.83 8.69 o 2 5 1 4448.59 4721.21 163.84 o 3 5 1 38.56 45.17 9.25 o 4 5 1 832.79 830.45 72.67 o 5 5 1 336.79 349.43 42.82 o 6 5 1 92.14 96.16 23.76 o 7 5 1 53.50 41.25 18.16 o 0 6 1 489.35 466.13 184.06 o 1 6 1 27.45 26.99 4.71 o 2 6 1 1031.74 1124.53 55.57 o 3 6 1 154.14 161.18 26.87 o 4 6 1 30.32 44.04 13.02 o 5 6 1 18.71 14.18 9.81 o 6 6 1 97.23 118.47 26.04 o 1 7 1 609.43 569.52 54.81 o 2 7 1 51.60 132.24 51.17 o 3 7 1 55.89 81.63 15.42 o 4 7 1 27.85 34.25 10.31 o 5 7 1 5.21 25.05 12.91 o 6 7 1 148.95 117.68 26.92 o 0 8 1 596.19 613.18 102.84 o 1 8 1 163.74 178.40 19.23 o 2 8 1 41.97 42.52 15.13 o 3 8 1 38.89 51.45 15.08 o 4 8 1 483.16 517.49 70.44 o 5 8 1 55.84 68.39 22.10 o 1 9 1 6.94 8.92 7.69 o 2 9 1 1.07 36.35 15.27 o 3 9 1 312.36 312.81 35.49 o 4 9 1 1.96 34.55 19.05 o 5 9 1 85.01 87.93 22.20 o 0 10 1 685.56 690.67 68.19 o 1 10 1 8.78 25.87 10.20 o 2 10 1 133.75 160.81 31.38 o 3 10 1 77.43 61.35 18.87 o 4 10 1 307.18 326.81 47.08 o 1 11 1 110.61 102.13 21.57 o 2 11 1 330.14 312.58 31.92 o 3 11 1 31.99 44.87 18.37 o 0 12 1 145.58 141.19 44.95 o 1 12 1 0.22 16.60 13.06 o 2 12 1 0.02 14.50 14.55 o 0 0 2 18.47 2.64 2.17 o 1 0 2 765.06 705.88 15.40 o 2 0 2 1569.65 1762.11 33.50 o 3 0 2 4267.67 4845.43 121.21 o 4 0 2 3149.06 3195.71 85.02 o 5 0 2 221.38 185.07 24.81 o 6 0 2 255.31 262.29 47.68 o 7 0 2 520.86 469.84 80.44 o 1 1 2 394.14 396.51 12.67 o 2 1 2 1437.89 1649.70 36.17 o 3 1 2 2718.05 2898.82 68.24 o 4 1 2 272.35 271.16 15.28 o 5 1 2 205.24 182.97 17.50 o 6 1 2 122.57 135.79 21.30 o 7 1 2 123.51 138.76 27.46 o 0 2 2 306.39 297.03 16.98 o 1 2 2 37689.20 38076.64 712.66 o 2 2 2 166.79 192.78 11.70 o 3 2 2 42.63 22.55 5.17 o 4 2 2 427.62 469.84 24.95 o 5 2 2 393.17 400.41 27.65 o 6 2 2 2.98 16.17 7.69 o 7 2 2 5.64 6.26 14.96 o 1 3 2 29585.08 30949.21 796.06 o 2 3 2 3066.60 3263.66 91.97 o 3 3 2 1195.26 1160.83 31.82 o 4 3 2 81.41 105.96 12.18 o 5 3 2 196.87 178.98 22.18 o 6 3 2 288.96 289.02 30.92 o 7 3 2 242.38 268.46 37.71 o 0 4 2 833.72 846.35 39.49 o 1 4 2 375.00 317.21 21.72 o 2 4 2 186.47 232.02 16.38 o 3 4 2 722.00 683.76 39.20 o 4 4 2 547.37 561.91 33.24 o 5 4 2 300.89 416.96 33.77 o 6 4 2 59.66 71.29 18.86 o 7 4 2 0.08 7.47 15.40 o 1 5 2 32.51 36.81 4.72 o 2 5 2 115.10 174.06 24.65 o 3 5 2 808.37 741.11 60.50 o 4 5 2 25.89 28.27 8.92 o 5 5 2 570.10 595.32 60.07 o 6 5 2 30.18 38.63 15.83 o 7 5 2 173.27 152.13 45.72 o 0 6 2 1778.09 1748.55 136.88 o 1 6 2 163.66 158.12 11.18 o 2 6 2 1.51 17.60 11.60 o 3 6 2 159.10 182.49 23.03 o 4 6 2 499.84 471.56 52.57 o 5 6 2 54.52 61.31 15.75 o 6 6 2 491.62 635.09 51.43 o 1 7 2 124.87 143.04 13.37 o 2 7 2 150.70 204.82 25.69 o 3 7 2 413.60 528.54 62.31 o 4 7 2 228.67 274.21 41.38 o 5 7 2 9.31 8.16 10.91 o 6 7 2 25.84 20.52 17.64 o 0 8 2 199.29 194.22 34.08 o 1 8 2 23.34 28.25 10.10 o 2 8 2 98.41 102.28 16.17 o 3 8 2 665.54 670.95 43.97 o 4 8 2 187.33 190.62 34.09 o 5 8 2 1.15 11.82 16.01 o 1 9 2 55.63 66.79 14.02 o 2 9 2 507.61 511.17 36.66 o 3 9 2 305.18 342.13 53.99 o 4 9 2 7.05 13.02 11.63 o 5 9 2 9.46 24.12 14.18 o 0 10 2 824.93 795.65 67.41 o 1 10 2 613.70 564.31 39.93 o 2 10 2 16.60 11.45 9.31 o 3 10 2 17.46 19.07 11.22 o 4 10 2 6.04 15.36 14.84 o 1 11 2 282.03 331.99 33.75 o 2 11 2 2.16 9.63 11.08 o 3 11 2 0.03 -4.29 14.12 o 0 12 2 147.11 161.33 37.79 o 1 12 2 850.35 823.42 66.47 o 2 12 2 13.76 18.22 25.96 o 1 1 3 416.93 377.47 9.90 o 2 1 3 517.23 525.10 15.28 o 3 1 3 3778.80 3920.60 107.57 o 4 1 3 196.50 226.90 15.48 o 5 1 3 23.65 26.05 8.90 o 6 1 3 0.45 15.93 10.74 o 7 1 3 214.75 165.80 28.03 o 0 2 3 15498.07 15438.14 540.38 o 1 2 3 12411.62 12677.86 232.46 o 2 2 3 1074.10 1067.55 24.78 o 3 2 3 277.00 309.96 17.48 o 4 2 3 316.49 351.93 21.71 o 5 2 3 830.09 851.41 43.22 o 6 2 3 78.14 66.13 13.05 o 7 2 3 2.34 4.18 14.80 o 1 3 3 1534.86 1636.72 61.13 o 2 3 3 6.25 29.35 6.39 o 3 3 3 208.95 235.55 18.73 o 4 3 3 1091.93 1090.74 43.24 o 5 3 3 356.93 399.15 27.95 o 6 3 3 114.63 93.66 20.09 o 7 3 3 2.44 29.80 15.42 o 0 4 3 109.99 125.47 31.14 o 1 4 3 423.92 397.73 17.07 o 2 4 3 2319.52 2575.12 56.36 o 3 4 3 4.31 3.47 4.94 o 4 4 3 1556.13 1553.84 63.53 o 5 4 3 334.41 332.65 30.84 o 6 4 3 2.29 21.13 14.14 o 7 4 3 0.26 4.45 15.41 o 1 5 3 1.91 6.26 3.61 o 2 5 3 2379.34 2260.01 66.03 o 3 5 3 975.43 996.86 41.13 o 4 5 3 408.91 430.03 31.74 o 5 5 3 50.67 62.87 22.28 o 6 5 3 70.84 72.23 17.06 o 7 5 3 18.84 26.14 23.62 o 0 6 3 1726.67 1817.53 138.51 o 1 6 3 231.04 267.18 21.37 o 2 6 3 2211.27 2281.64 63.58 o 3 6 3 14.83 18.70 10.98 o 4 6 3 0.34 18.78 12.03 o 5 6 3 28.74 38.14 14.32 o 6 6 3 15.84 18.68 18.22 o 1 7 3 461.83 457.57 27.43 o 2 7 3 1178.41 1213.26 56.86 o 3 7 3 3404.91 3732.18 168.31 o 4 7 3 619.74 665.94 59.71 o 5 7 3 39.31 25.12 13.73 o 6 7 3 41.44 37.55 12.67 o 0 8 3 213.84 217.26 28.31 o 1 8 3 2075.02 2083.80 95.09 o 2 8 3 339.38 351.23 30.80 o 3 8 3 3.76 9.82 9.19 o 4 8 3 0.49 14.17 12.22 o 5 8 3 501.91 566.93 60.38 o 1 9 3 209.30 222.84 24.74 o 2 9 3 88.50 85.95 16.30 o 3 9 3 57.01 47.68 17.93 o 4 9 3 29.15 14.36 12.34 o 5 9 3 6.46 26.35 11.83 o 0 10 3 74.38 90.95 31.33 o 1 10 3 52.66 58.63 15.21 o 2 10 3 16.36 12.03 10.36 o 3 10 3 9.14 28.61 14.16 o 4 10 3 163.66 175.93 35.38 o 1 11 3 21.47 27.38 10.44 o 2 11 3 264.58 325.13 43.28 o 3 11 3 122.18 131.93 31.06 o 0 12 3 14.70 12.96 18.22 o 1 12 3 21.22 21.71 13.53 o 2 12 3 8.23 9.74 16.98 o 0 0 4 32780.75 29620.29 1292.48 o 1 0 4 1933.06 1926.78 47.06 o 2 0 4 41.02 50.44 9.25 o 3 0 4 2440.47 2582.86 82.76 o 4 0 4 268.34 270.92 19.48 o 5 0 4 472.93 523.05 39.67 o 6 0 4 10.62 2.35 12.34 o 7 0 4 9.95 3.96 29.03 o 1 1 4 20.60 28.44 3.21 o 2 1 4 335.54 326.03 12.93 o 3 1 4 1200.13 1298.85 33.68 o 4 1 4 110.50 107.14 12.31 o 5 1 4 209.16 237.49 20.62 o 6 1 4 33.58 40.10 12.65 o 7 1 4 3.43 18.15 14.53 o 0 2 4 97.31 83.05 8.80 o 1 2 4 65.40 57.40 5.48 o 2 2 4 466.31 401.39 17.64 o 3 2 4 95.89 91.05 9.55 o 4 2 4 1110.46 1111.65 38.41 o 5 2 4 288.72 290.19 26.31 o 6 2 4 90.33 53.83 13.46 o 7 2 4 14.28 7.68 15.16 o 1 3 4 196.78 149.08 8.46 o 2 3 4 4993.93 5278.39 89.56 o 3 3 4 4240.90 4343.82 148.91 o 4 3 4 288.80 290.23 20.71 o 5 3 4 47.26 29.32 10.26 o 6 3 4 1.29 4.62 11.03 o 7 3 4 560.93 644.67 50.94 o 0 4 4 7341.29 7444.18 262.26 o 1 4 4 1326.59 1313.39 33.03 o 2 4 4 2022.05 2180.82 42.46 o 3 4 4 2.86 7.37 6.54 o 4 4 4 5.18 18.04 8.16 o 5 4 4 1001.55 1080.71 375.69 o 6 4 4 238.43 253.11 32.71 o 7 4 4 80.24 152.64 32.17 o 1 5 4 1082.55 1153.68 39.04 o 2 5 4 417.47 479.94 25.07 o 3 5 4 66.07 83.97 13.72 o 4 5 4 109.72 63.79 22.71 o 5 5 4 193.23 217.51 29.00 o 6 5 4 0.04 22.00 13.58 o 0 6 4 797.49 884.82 85.79 o 1 6 4 1314.87 1255.27 49.61 o 2 6 4 1502.82 1526.00 46.19 o 3 6 4 785.90 838.33 65.90 o 4 6 4 102.09 79.13 13.65 o 5 6 4 788.68 919.66 80.42 o 6 6 4 0.59 4.87 10.91 o 1 7 4 1046.26 996.31 47.18 o 2 7 4 7.30 5.23 6.02 o 3 7 4 116.98 161.81 25.20 o 4 7 4 29.90 20.25 10.46 o 5 7 4 0.30 24.08 11.70 o 6 7 4 0.05 23.71 16.29 o 0 8 4 485.57 492.44 42.15 o 1 8 4 0.88 22.34 9.44 o 2 8 4 513.53 509.34 35.11 o 3 8 4 25.66 18.19 10.65 o 4 8 4 205.55 221.68 35.31 o 5 8 4 89.26 67.51 20.50 o 1 9 4 679.03 667.70 40.30 o 2 9 4 0.15 2.29 11.49 o 3 9 4 6.60 11.13 11.57 o 4 9 4 76.87 89.65 23.28 o 5 9 4 18.15 27.26 14.55 o 0 10 4 0.20 3.97 12.38 o 1 10 4 71.35 83.78 15.07 o 2 10 4 355.87 368.45 41.43 o 3 10 4 43.89 28.07 12.38 o 4 10 4 49.80 64.42 18.35 o 1 11 4 18.98 26.33 8.32 o 2 11 4 25.45 17.37 15.92 o 3 11 4 0.19 16.42 14.59 o 0 12 4 31.45 36.49 19.20 o 1 12 4 84.13 76.21 17.50 o 2 12 4 0.52 -3.09 16.89 o 1 1 5 90.31 103.11 7.31 o 2 1 5 192.90 193.72 10.16 o 3 1 5 3670.03 3903.10 60.53 o 4 1 5 101.97 120.90 11.75 o 5 1 5 1178.18 1234.93 50.20 o 6 1 5 17.13 8.42 10.60 o 7 1 5 117.95 106.71 27.18 o 0 2 5 449.66 442.05 19.69 o 1 2 5 2989.61 2997.67 55.83 o 2 2 5 334.39 329.77 14.80 o 3 2 5 313.75 243.91 14.11 o 4 2 5 91.84 110.62 11.90 o 5 2 5 1481.00 1553.95 69.87 o 6 2 5 0.01 6.78 10.48 o 7 2 5 68.02 50.75 19.74 o 1 3 5 4496.11 4601.37 80.81 o 2 3 5 22.00 17.27 3.74 o 3 3 5 111.55 107.51 16.64 o 4 3 5 9.83 8.77 5.97 o 5 3 5 4.29 5.93 7.31 o 6 3 5 95.77 71.57 14.81 o 7 3 5 13.18 36.31 20.01 o 0 4 5 122.88 131.60 13.16 o 1 4 5 2541.99 2398.31 53.12 o 2 4 5 3518.24 3899.24 88.59 o 3 4 5 10.87 9.23 3.83 o 4 4 5 676.70 675.62 40.57 o 5 4 5 449.13 298.68 88.09 o 6 4 5 238.56 168.69 59.74 o 7 4 5 76.68 111.78 29.52 o 1 5 5 887.73 816.35 29.43 o 2 5 5 1707.61 1753.05 49.12 o 3 5 5 3366.41 3426.52 103.38 o 4 5 5 420.12 218.70 101.40 o 5 5 5 366.08 402.03 41.09 o 6 5 5 80.01 72.55 17.66 o 0 6 5 2786.49 2955.56 131.79 o 1 6 5 21.05 29.03 8.02 o 2 6 5 358.31 387.76 22.82 o 3 6 5 920.39 111.17 430.46 o 4 6 5 68.44 42.03 10.51 o 5 6 5 14.19 20.81 13.00 o 6 6 5 169.27 188.18 30.02 o 1 7 5 110.01 92.63 12.09 o 2 7 5 220.54 232.41 17.75 o 3 7 5 2260.26 2392.97 95.93 o 4 7 5 269.94 267.41 26.56 o 5 7 5 117.78 135.00 26.31 o 6 7 5 80.53 75.91 16.06 o 0 8 5 500.91 512.97 45.30 o 1 8 5 875.93 837.90 52.73 o 2 8 5 37.07 25.35 8.43 o 3 8 5 729.46 697.41 48.89 o 4 8 5 3.50 5.13 10.33 o 5 8 5 553.70 604.09 65.06 o 1 9 5 312.05 298.23 27.75 o 2 9 5 351.51 405.81 31.40 o 3 9 5 74.80 64.78 16.94 o 4 9 5 185.15 172.33 28.82 o 5 9 5 13.78 15.67 16.00 o 0 10 5 121.63 134.62 23.40 o 1 10 5 98.58 95.28 17.45 o 2 10 5 325.45 286.91 32.58 o 3 10 5 14.43 21.47 9.93 o 4 10 5 108.17 80.24 18.98 o 1 11 5 10.90 11.98 8.42 o 2 11 5 4.82 21.13 9.01 o 3 11 5 31.06 44.09 16.07 o 0 12 5 46.19 37.42 21.51 o 1 12 5 82.98 80.19 16.81 o 0 0 6 1370.97 1378.07 111.68 o 1 0 6 13086.91 12995.91 403.40 o 2 0 6 1649.47 1589.62 33.39 o 3 0 6 118.87 128.00 13.27 o 4 0 6 376.63 372.34 27.28 o 5 0 6 662.19 696.49 52.31 o 6 0 6 12.91 16.64 14.32 o 7 0 6 71.73 42.39 25.26 o 1 1 6 1217.87 1095.83 28.82 o 2 1 6 261.54 288.28 12.75 o 3 1 6 1162.40 1081.48 30.45 o 4 1 6 100.55 94.47 11.34 o 5 1 6 980.16 1021.78 49.41 o 6 1 6 28.58 14.99 10.39 o 7 1 6 29.48 39.88 20.26 o 0 2 6 48.70 56.47 7.77 o 1 2 6 1.01 -0.71 3.33 o 2 2 6 0.69 1.85 3.41 o 3 2 6 759.26 814.02 24.12 o 4 2 6 50.10 51.63 9.22 o 5 2 6 378.78 379.40 26.31 o 6 2 6 282.81 249.30 30.56 o 7 2 6 24.93 22.15 16.06 o 1 3 6 2240.97 2319.84 51.52 o 2 3 6 990.37 1013.66 22.89 o 3 3 6 2897.14 3167.19 88.72 o 4 3 6 110.41 133.35 29.16 o 5 3 6 3.59 14.43 9.32 o 6 3 6 1.85 8.44 11.80 o 7 3 6 424.09 429.06 40.30 o 0 4 6 617.59 518.62 29.37 o 1 4 6 3896.21 3972.34 98.22 o 2 4 6 0.10 -1.02 3.77 o 3 4 6 293.12 295.40 18.56 o 4 4 6 78.93 72.13 14.12 o 5 4 6 242.72 149.03 33.97 o 6 4 6 39.99 26.17 11.77 o 7 4 6 10.42 -2.04 14.22 o 1 5 6 79.48 71.67 7.79 o 2 5 6 6.00 8.32 5.66 o 3 5 6 1282.29 1283.54 54.05 o 4 5 6 80.60 61.27 14.90 o 5 5 6 68.10 25.17 12.47 o 6 5 6 21.77 14.09 15.03 o 0 6 6 453.08 433.70 48.09 o 1 6 6 4013.21 4135.30 117.83 o 2 6 6 4.58 5.12 6.11 o 3 6 6 131.54 65.38 19.29 o 4 6 6 35.79 33.84 9.64 o 5 6 6 593.65 642.28 64.43 o 6 6 6 274.53 293.74 35.47 o 1 7 6 132.37 124.56 13.30 o 2 7 6 22.26 21.46 6.97 o 3 7 6 466.61 452.06 50.13 o 4 7 6 62.55 57.81 14.46 o 5 7 6 47.14 33.73 14.11 o 6 7 6 20.28 22.01 18.20 o 0 8 6 342.63 400.16 38.28 o 1 8 6 681.18 686.26 43.49 o 2 8 6 29.31 35.99 8.56 o 3 8 6 144.92 117.16 19.74 o 4 8 6 155.74 147.86 20.32 o 5 8 6 57.77 41.65 21.26 o 1 9 6 355.13 330.27 24.78 o 2 9 6 42.11 34.63 12.98 o 3 9 6 1530.62 1461.73 70.64 o 4 9 6 8.80 6.93 11.66 o 5 9 6 22.60 15.68 19.12 o 0 10 6 514.82 488.44 63.03 o 1 10 6 90.81 86.35 15.21 o 2 10 6 139.16 127.58 21.22 o 3 10 6 1.42 4.99 13.79 o 4 10 6 2.61 11.48 10.77 o 1 11 6 4.73 8.41 7.51 o 2 11 6 28.92 40.06 14.89 o 3 11 6 2.92 0.83 13.79 o 0 12 6 51.11 51.14 20.34 o 1 12 6 15.79 15.39 13.64 o 1 1 7 7483.40 7727.61 173.38 o 2 1 7 57.13 73.38 7.24 o 3 1 7 889.53 804.91 23.78 o 4 1 7 1.89 3.91 6.65 o 5 1 7 594.77 634.76 34.87 o 6 1 7 293.16 288.56 27.84 o 7 1 7 260.28 223.79 31.57 o 0 2 7 3.50 11.09 6.60 o 1 2 7 776.04 746.03 16.22 o 2 2 7 1069.04 1031.66 24.08 o 3 2 7 86.74 86.07 10.44 o 4 2 7 1653.04 1724.62 52.80 o 5 2 7 723.73 726.65 52.26 o 6 2 7 32.32 34.06 12.73 o 7 2 7 43.65 30.70 15.25 o 1 3 7 2955.47 3154.76 69.89 o 2 3 7 40.32 41.39 7.06 o 3 3 7 2.21 4.59 5.51 o 4 3 7 1175.88 1210.55 41.32 o 5 3 7 647.72 575.92 30.19 o 6 3 7 221.20 169.66 34.15 o 7 3 7 0.24 0.35 13.35 o 0 4 7 11.11 12.40 5.17 o 1 4 7 2720.80 2774.59 64.21 o 2 4 7 21.56 16.50 4.82 o 3 4 7 475.56 486.74 23.53 o 4 4 7 1794.36 1889.34 70.68 o 5 4 7 437.23 478.70 31.10 o 6 4 7 6.67 17.36 9.66 o 7 4 7 5.65 10.21 16.43 o 1 5 7 1320.30 1230.11 35.73 o 2 5 7 1537.22 1508.46 31.28 o 3 5 7 444.19 427.27 28.66 o 4 5 7 180.60 132.41 28.36 o 5 5 7 109.32 85.56 29.93 o 6 5 7 317.38 321.13 37.46 o 0 6 7 1102.77 1018.68 70.87 o 1 6 7 640.71 559.46 33.82 o 2 6 7 269.24 269.13 17.74 o 3 6 7 0.81 9.59 7.16 o 4 6 7 197.70 145.77 31.39 o 5 6 7 32.27 33.78 16.52 o 6 6 7 19.28 38.62 19.84 o 1 7 7 495.15 474.18 26.12 o 2 7 7 473.18 441.08 25.75 o 3 7 7 658.13 622.30 48.55 o 4 7 7 81.18 76.09 13.61 o 5 7 7 3.98 9.75 12.36 o 6 7 7 7.91 27.07 16.04 o 0 8 7 31.86 21.01 13.75 o 1 8 7 116.79 110.62 13.17 o 2 8 7 19.29 14.26 7.39 o 3 8 7 30.32 38.37 11.23 o 4 8 7 14.92 8.46 10.54 o 5 8 7 164.27 147.89 31.57 o 1 9 7 190.29 186.67 19.67 o 2 9 7 58.10 40.49 9.89 o 3 9 7 357.95 357.83 38.63 o 4 9 7 12.72 17.09 11.54 o 5 9 7 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8.52 o 2 9 8 150.20 157.50 16.95 o 3 9 8 341.10 351.13 34.69 o 4 9 8 219.04 198.41 33.82 o 0 10 8 2.89 7.90 10.11 o 1 10 8 222.46 228.43 24.73 o 2 10 8 53.74 58.27 13.03 o 3 10 8 133.68 156.64 26.41 o 4 10 8 358.87 319.55 61.65 o 1 11 8 3.06 5.58 11.19 o 2 11 8 104.12 135.80 26.06 o 3 11 8 37.95 23.52 16.02 o 0 12 8 298.19 352.81 78.21 o 1 12 8 37.53 13.32 23.84 o 1 1 9 2063.48 2054.36 37.17 o 2 1 9 6758.93 7276.67 127.65 o 3 1 9 315.29 325.64 16.80 o 4 1 9 2119.15 2197.51 60.62 o 5 1 9 1469.52 1541.79 52.83 o 6 1 9 2.69 3.74 11.73 o 7 1 9 37.19 19.24 14.98 o 0 2 9 13709.99 14006.53 475.35 o 1 2 9 2258.68 2514.79 53.35 o 2 2 9 4.80 5.55 3.01 o 3 2 9 40.83 40.00 7.70 o 4 2 9 140.13 128.98 12.40 o 5 2 9 0.36 2.94 9.43 o 6 2 9 590.74 614.78 34.70 o 7 2 9 32.76 20.44 14.92 o 1 3 9 193.78 207.74 11.55 o 2 3 9 95.99 105.15 8.05 o 3 3 9 443.50 465.51 21.73 o 4 3 9 221.15 226.21 18.82 o 5 3 9 182.28 181.94 19.69 o 6 3 9 39.91 40.41 15.51 o 7 3 9 48.46 46.15 19.43 o 0 4 9 5306.41 5266.78 198.21 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30.52 o 3 1 21 2.07 9.70 6.50 o 4 1 21 45.13 50.07 11.66 o 5 1 21 84.00 87.88 19.47 o 0 2 21 56.78 79.75 30.97 o 1 2 21 96.09 96.29 12.81 o 2 2 21 1026.25 1133.20 192.88 o 3 2 21 24.60 31.58 9.60 o 4 2 21 721.93 773.74 43.12 o 5 2 21 43.86 50.99 18.34 o 1 3 21 24.03 27.95 8.66 o 2 3 21 148.25 89.07 15.06 o 3 3 21 1.61 9.72 11.25 o 4 3 21 60.27 48.19 16.23 o 5 3 21 40.12 43.89 20.81 o 0 4 21 142.64 166.42 28.92 o 1 4 21 2.24 2.64 8.01 o 2 4 21 214.03 189.58 32.66 o 3 4 21 81.27 53.44 13.08 o 4 4 21 539.94 660.24 48.29 o 1 5 21 33.37 35.18 10.91 o 2 5 21 590.30 678.60 35.28 o 3 5 21 7.81 17.93 12.09 o 4 5 21 182.06 217.65 31.37 o 0 6 21 0.41 6.90 11.69 o 1 6 21 110.80 92.05 16.56 o 2 6 21 10.26 19.66 13.75 o 3 6 21 42.97 19.29 13.71 o 1 7 21 0.11 0.14 11.64 o 2 7 21 248.71 217.91 26.93 o 3 7 21 178.38 148.77 26.92 o 0 8 21 711.95 881.52 88.03 o 1 8 21 3.74 11.91 12.05 o 2 8 21 11.39 -1.00 14.55 o 0 0 22 453.47 560.50 61.06 o 1 0 22 1689.66 1813.69 79.40 o 2 0 22 55.35 25.95 14.05 o 3 0 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18.82 o 2 1 26 1.08 -11.69 13.13 o 3 1 26 24.14 24.31 18.49 o 0 2 26 24.07 38.27 22.12 o 1 2 26 190.56 211.22 27.35 o 2 2 26 43.30 20.21 13.14 o 3 2 26 3.94 9.68 15.81 o 1 3 26 532.10 684.28 46.16 o 2 3 26 8.14 -0.91 15.49 o 0 4 26 5.13 5.72 19.08 o 1 4 26 342.53 306.24 45.87 o 2 4 26 14.10 16.89 15.35 o 1 5 26 105.75 119.61 25.14 o 1 1 27 158.52 235.69 28.50 o 2 1 27 27.13 25.92 15.05 o 0 2 27 6.98 21.28 21.23 o 1 2 27 129.52 169.97 25.91 o 2 2 27 6.89 24.91 17.34 o 1 3 27 8.32 4.28 13.52 o 2 3 27 8.91 19.70 16.84 o 0 4 27 1.09 8.87 21.07 o 1 4 27 79.59 71.17 20.00 o 0 0 28 713.92 961.59 126.50 o 1 0 28 69.19 93.43 29.63 o 2 0 28 8.92 26.85 33.36 o 1 1 28 3.05 13.76 15.63 o 2 1 28 77.10 60.57 26.49 o 0 2 28 148.54 194.04 38.49 o 1 2 28 1.79 9.54 14.68 o 1 3 28 3.62 10.72 19.27 o