#------------------------------------------------------------------------------ #$Date: 2019-11-17 08:12:14 +0200 (Sun, 17 Nov 2019) $ #$Revision: 228818 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/54/90/1549062.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1549062 loop_ _publ_author_name 'Nievergelt, Philipp P.' 'Babor, Martin' '\2.0\s(I) _oxford_diffrn_Wilson_B_factor 2.25 _oxford_diffrn_Wilson_scale 0.11 _oxford_refine_ls_r_factor_ref 0.0356 _oxford_refine_ls_scale 3.04(3) _oxford_reflns_number_all 6622 _oxford_reflns_threshold_expression_ref I>-3.0\s(I) _iucr_refine_instructions_details ; # # Punched on 12/10/17 at 12:40:41 # #LIST 12 BLOCK SCALE X'S U'S CONT ENANTIO EQUIVALENCE PART(1001, OCC) CONTINUE PART(1002, OCC) WEIGHT -1 PART(1002, OCC) RIDE N ( 1,X'S) H ( 13,X'S) H ( 12,X'S) H ( 11,X'S) RIDE C ( 2,X'S) H ( 21,X'S) H ( 22,X'S) RIDE C ( 3,X'S) H ( 31,X'S) H ( 32,X'S) RIDE C ( 5,X'S) H ( 51,X'S) RIDE N ( 6,X'S) H ( 61,X'S) RIDE C ( 9,X'S) H ( 91,X'S) RIDE C ( 10,X'S) H ( 101,X'S) RIDE C ( 12,X'S) H ( 121,X'S) RIDE C ( 14,X'S) H ( 142,X'S) H ( 141,X'S) RIDE C ( 16,X'S) H ( 161,X'S) RIDE C ( 17,X'S) H ( 171,X'S) RIDE C ( 18,X'S) H ( 181,X'S) RIDE C ( 19,X'S) H ( 191,X'S) RIDE C ( 20,X'S) H ( 201,X'S) RIDE N ( 21,X'S) H ( 211,X'S) H ( 212,X'S) H ( 213,X'S) RIDE C ( 22,X'S) H ( 224,X'S) H ( 223,X'S) CONT H ( 222,X'S) H ( 221,X'S) RIDE C ( 23,X'S) H ( 231,X'S) H ( 232,X'S) RIDE C ( 25,X'S) H ( 251,X'S) RIDE N ( 26,X'S) H ( 261,X'S) RIDE C ( 29,X'S) H ( 291,X'S) RIDE C ( 30,X'S) H ( 301,X'S) RIDE C ( 32,X'S) H ( 321,X'S) RIDE C ( 34,X'S) H ( 342,X'S) H ( 341,X'S) RIDE C ( 36,X'S) H ( 361,X'S) RIDE C ( 37,X'S) H ( 371,X'S) RIDE C ( 38,X'S) H ( 381,X'S) RIDE C ( 39,X'S) H ( 391,X'S) RIDE C ( 40,X'S) H ( 401,X'S) RIDE N ( 121,X'S) H (1212,X'S) H (1213,X'S) H (1211,X'S) END # # Punched on 12/10/17 at 12:40:41 # #LIST 16 NO REM HREST START (DO NOT REMOVE THIS LINE) REM HREST END (DO NOT REMOVE THIS LINE) DISTANCE 1.250000 , 0.020000 = O(145) TO C(144) DISTANCE 1.250000 , 0.020000 = O(146) TO C(144) DISTANCE 1.250000 , 0.020000 = O(141) TO C(142) DISTANCE 1.250000 , 0.020000 = O(143) TO C(142) DISTANCE 1.520000 , 0.020000 = C(144) TO C(142) ANGLE 116.000000 , 2.000000 = O(145) TO C(144) TO C(142) ANGLE 116.000000 , 2.000000 = O(146) TO C(144) TO C(142) ANGLE 116.000000 , 2.000000 = O(141) TO C(142) TO C(144) ANGLE 116.000000 , 2.000000 = O(143) TO C(142) TO C(144) ANGLE 126.000000 , 2.000000 = O(146) TO C(144) TO O(145) ANGLE 126.000000 , 2.000000 = O(141) TO C(142) TO O(143) DISTANCE 1.510000 , 0.0050000 = C(22) TO N(121) U(IJ)'S 0.0, 0.0010000 = O(145) TO O(41) U(IJ)'S 0.0, 0.0010000 = O(146) TO O(41) U(IJ)'S 0.0, 0.0010000 = O(141) TO O(41) U(IJ)'S 0.0, 0.0010000 = O(143) TO O(41) U(IJ)'S 0.0, 0.0010000 = O(147) TO O(41) U(IJ)'S 0.0, 0.0010000 = O(148) TO O(41) U(IJ)'S 0.0, 0.0010000 = C(144) TO C(44) U(IJ)'S 0.0, 0.0010000 = C(142) TO C(44) U(IJ)'S 0.0, 0.010000 = N(121) TO N(21) END ; _cod_data_source_file c8sc00783g2.cif _cod_data_source_block I_CCDC11 _cod_depositor_comments 'Adding full bibliography for 1549042--1549063.cif.' _cod_original_sg_symbol_H-M 'P 1 21 1 ' _cod_database_code 1549062 _iucr_refine_reflections_details ; # An asterisk in column 34 indicates a format overflow # Data was input as F-squared 0 -11 0 -8.53 22.75 0 -11 1 1951.88 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14 4300.80 154.82 0 2 14 4491.39 159.22 0 2 14 4597.88 199.54 0 2 14 4247.67 154.99 0 2 -14 4022.19 154.89 0 2 -14 4084.90 194.49 0 2 -14 4121.43 154.61 0 2 14 4495.34 157.97 0 2 -15 15168.8 523.7 0 2 15 16185.8 527.0 0 2 -15 14783.5 522.4 0 2 15 16179.5 527.1 0 2 -15 15084.9 523.5 0 2 15 15354.8 523.2 0 2 15 16039.3 527.4 0 2 15 15756.4 523.8 0 2 15 16230.7 571.5 0 2 -15 15002.9 522.1 0 2 -15 16072.4 572.8 0 2 16 518.68 42.84 0 2 16 480.85 38.71 0 2 -16 648.20 75.66 0 2 -16 482.24 39.00 0 2 -16 446.04 36.41 0 2 -16 494.65 37.31 0 2 16 548.17 39.20 0 2 -16 538.91 38.98 0 2 16 475.25 73.54 0 2 16 565.66 45.87 0 2 16 500.25 47.25 0 2 17 361.96 41.90 0 2 -17 371.15 35.29 0 2 17 315.03 41.52 0 2 -17 354.73 32.63 0 2 -17 362.92 31.45 0 2 -17 351.93 64.20 0 2 17 458.71 69.71 0 2 17 388.19 36.24 0 2 17 346.01 44.53 0 2 17 320.80 34.70 0 2 -17 351.67 36.53 0 2 -18 1363.18 60.03 0 2 -18 1376.59 64.92 0 2 -18 1338.35 61.55 0 2 18 1358.17 103.89 0 2 18 1234.11 68.59 0 2 -18 1319.79 64.57 0 2 -18 1172.99 99.14 0 2 18 1398.42 63.49 0 2 18 1368.19 63.47 0 2 18 1379.33 68.49 0 2 -19 136.28 26.27 0 2 -19 168.66 51.16 0 2 -19 162.01 30.99 0 2 -19 133.92 31.25 0 2 19 169.05 28.36 0 2 -19 135.16 24.45 0 2 19 164.05 29.70 0 2 -20 96.79 28.03 0 2 20 104.41 25.37 0 2 -20 112.00 28.96 0 2 -20 124.60 22.40 0 2 20 102.02 33.75 0 2 20 73.52 26.51 0 2 21 23.80 21.47 0 2 -21 41.14 23.42 0 2 21 43.79 20.92 0 2 21 8.68 28.43 0 2 22 52.21 24.77 0 2 -22 65.26 19.50 0 2 22 51.72 16.84 0 2 23 123.26 20.27 0 2 -23 122.28 16.58 0 3 0 83.03 26.63 0 3 0 -2.93 31.87 0 3 1 564.08 47.23 0 3 -1 615.50 39.70 0 3 1 569.49 40.66 0 3 -1 625.96 46.10 0 3 -2 38417.9 1287.0 0 3 -2 38807.9 1291.5 0 3 2 38796.8 1289.2 0 3 -3 230.31 32.08 0 3 -3 230.14 38.10 0 3 3 287.50 35.68 0 3 4 10429.2 369.7 0 3 -4 10349.3 366.2 0 3 -4 11066.5 372.6 0 3 -5 7548.70 269.08 0 3 5 7407.90 256.14 0 3 5 7688.96 256.43 0 3 5 7676.63 256.14 0 3 -5 7777.74 275.11 0 3 5 7473.78 255.57 0 3 6 840.84 35.91 0 3 6 816.11 38.83 0 3 -6 849.09 60.69 0 3 6 850.54 38.88 0 3 6 826.09 37.51 0 3 -6 896.21 52.66 0 3 6 814.97 36.72 0 3 7 8652.67 295.02 0 3 7 8835.78 296.34 0 3 7 8684.34 295.14 0 3 -7 8825.24 319.83 0 3 7 8793.22 296.97 0 3 -7 8786.41 312.33 0 3 7 8789.44 297.10 0 3 8 2713.83 99.39 0 3 8 2658.14 101.11 0 3 -8 2908.64 127.69 0 3 8 2775.02 99.78 0 3 8 2785.13 100.74 0 3 -8 2699.49 117.30 0 3 9 9044.88 309.68 0 3 9 9131.71 308.47 0 3 -9 8780.41 328.65 0 3 9 9203.11 310.76 0 3 -9 9471.54 338.38 0 3 9 8869.06 335.20 0 3 9 9047.83 308.65 0 3 10 2059.40 82.99 0 3 10 2006.85 79.22 0 3 10 2144.25 81.22 0 3 -10 1920.08 107.78 0 3 10 2057.55 78.91 0 3 11 878.40 46.13 0 3 -11 901.36 44.15 0 3 -11 956.42 43.47 0 3 11 890.26 45.35 0 3 11 962.55 76.88 0 3 11 883.00 44.60 0 3 -11 856.01 44.23 0 3 11 942.56 45.25 0 3 11 928.90 46.17 0 3 -11 949.73 79.08 0 3 11 885.57 46.01 0 3 11 898.96 48.97 0 3 12 3071.98 115.14 0 3 12 3190.21 151.38 0 3 12 3228.24 116.55 0 3 -12 2953.71 113.88 0 3 12 3079.48 116.79 0 3 -12 3007.40 114.73 0 3 -12 2918.87 113.25 0 3 12 3194.97 116.45 0 3 12 3036.10 115.65 0 3 -12 3075.10 111.29 0 3 12 3062.92 115.61 0 3 -12 3245.26 152.98 0 3 12 3228.55 119.04 0 3 13 3492.43 128.42 0 3 13 3522.87 126.19 0 3 -13 3371.78 124.73 0 3 -13 3114.10 120.39 0 3 -13 2992.54 149.77 0 3 -13 3374.42 125.97 0 3 13 3449.58 130.75 0 3 13 3506.55 126.98 0 3 13 3283.04 127.65 0 3 13 3290.56 126.58 0 3 -13 3474.71 167.29 0 3 13 3717.06 168.74 0 3 13 3442.30 128.45 0 3 -13 3493.15 125.33 0 3 -14 668.43 63.26 0 3 14 587.05 44.93 0 3 14 595.68 46.48 0 3 14 607.85 42.57 0 3 -14 664.51 78.24 0 3 14 646.84 45.38 0 3 -14 640.82 40.80 0 3 14 710.62 77.77 0 3 14 690.01 45.38 0 3 -14 633.37 38.34 0 3 -14 654.52 41.01 0 3 14 621.74 42.84 0 3 14 609.62 40.94 0 3 15 360.07 35.15 0 3 -15 305.92 33.99 0 3 15 336.09 40.70 0 3 15 386.71 34.83 0 3 15 245.40 62.51 0 3 15 296.78 39.35 0 3 -15 297.92 31.69 0 3 -15 335.77 35.79 0 3 15 240.11 38.29 0 3 15 300.55 38.31 0 3 -15 298.21 64.91 0 3 16 472.81 73.06 0 3 16 547.58 45.86 0 3 -16 466.90 68.71 0 3 16 548.72 45.81 0 3 -16 506.77 39.37 0 3 16 503.75 40.11 0 3 16 475.09 45.86 0 3 16 481.81 43.45 0 3 16 507.09 40.24 0 3 -16 539.48 40.82 0 3 17 6746.65 248.20 0 3 17 7105.85 246.15 0 3 17 6998.72 249.57 0 3 -17 7169.55 245.88 0 3 17 7115.41 250.43 0 3 17 7154.01 291.46 0 3 17 6907.09 246.88 0 3 -17 6320.73 288.64 0 3 17 6817.44 247.66 0 3 -17 7195.75 246.25 0 3 18 320.72 35.77 0 3 -18 374.88 34.83 0 3 -18 353.98 33.20 0 3 -18 239.29 56.11 0 3 18 291.14 40.21 0 3 18 342.89 42.56 0 3 18 369.08 65.05 0 3 18 336.74 33.64 0 3 -18 297.57 37.27 0 3 18 290.86 39.02 0 3 19 2934.55 111.39 0 3 19 2775.67 116.18 0 3 19 3035.64 112.76 0 3 -19 2916.28 110.31 0 3 19 2985.80 115.33 0 3 -19 2871.19 110.59 0 3 -19 2962.54 113.54 0 3 -20 183.47 28.50 0 3 -20 188.38 30.63 0 3 20 180.58 26.39 0 3 20 182.69 26.91 0 3 -20 133.54 24.50 0 3 20 150.84 33.25 0 3 -20 156.77 24.94 0 3 -21 1423.98 58.36 0 3 21 1305.97 55.47 0 3 -21 1249.73 53.37 0 3 21 1425.35 60.92 0 3 21 1291.65 55.91 0 3 -22 86.39 20.35 0 3 22 79.66 22.94 0 3 22 70.59 15.50 0 3 23 53.25 16.81 0 3 -23 43.82 14.33 0 4 0 9811.35 339.19 0 4 0 10523.8 355.9 0 4 0 9984.61 360.51 0 4 0 10396.8 340.2 0 4 -1 7460.14 271.38 0 4 1 7444.21 249.60 0 4 -1 7159.35 248.54 0 4 1 7299.42 249.09 0 4 -1 7515.43 249.44 0 4 1 7466.42 266.33 0 4 -1 7450.34 264.73 0 4 2 5527.98 190.17 0 4 -2 5648.93 189.63 0 4 -2 5414.42 188.67 0 4 2 5468.63 188.90 0 4 -2 5857.40 213.16 0 4 2 5661.81 189.74 0 4 2 5446.81 206.85 0 4 -2 5398.21 203.97 0 4 3 3349.51 117.78 0 4 -3 3262.85 116.02 0 4 -3 3387.53 140.36 0 4 3 3278.00 135.88 0 4 3 3310.15 116.74 0 4 3 3193.55 117.46 0 4 -3 3602.21 133.73 0 4 -3 3439.51 117.17 0 4 3 3265.00 116.10 0 4 4 1161.81 49.12 0 4 -4 1220.66 48.71 0 4 -4 1212.20 47.54 0 4 4 1244.35 71.04 0 4 4 1124.97 47.17 0 4 -4 1174.96 71.72 0 4 -4 1180.78 64.45 0 4 4 1172.96 49.95 0 4 4 1145.69 49.55 0 4 5 1102.83 46.73 0 4 5 1092.24 47.91 0 4 5 1059.44 42.82 0 4 -5 1044.18 44.55 0 4 -5 1028.18 70.49 0 4 -5 1038.08 61.44 0 4 -5 1045.02 45.33 0 4 5 1048.11 44.98 0 4 5 1091.66 48.05 0 4 6 1765.75 67.98 0 4 -6 1551.80 64.72 0 4 -6 1642.26 92.86 0 4 6 1690.74 66.36 0 4 6 1698.74 63.95 0 4 6 1742.89 67.60 0 4 -6 1732.76 83.53 0 4 6 1682.40 67.84 0 4 6 1705.26 63.72 0 4 -7 8624.50 323.19 0 4 7 9245.29 306.20 0 4 7 9030.53 306.57 0 4 -7 8880.14 304.26 0 4 -7 8786.98 333.49 0 4 7 9102.68 303.89 0 4 7 8827.68 303.33 0 4 7 9200.48 305.63 0 4 7 8790.76 306.48 0 4 8 4862.90 172.35 0 4 8 4767.56 168.71 0 4 -8 4950.83 169.28 0 4 8 4887.48 168.37 0 4 -8 4842.30 190.06 0 4 8 4671.91 171.16 0 4 8 4844.24 170.87 0 4 -8 4792.42 201.70 0 4 9 4604.48 161.48 0 4 -9 4612.71 192.94 0 4 9 4574.11 159.68 0 4 9 4647.55 186.87 0 4 -9 4002.36 157.10 0 4 9 4436.16 157.12 0 4 -9 4405.26 156.82 0 4 9 4549.08 156.97 0 4 -9 4310.99 180.07 0 4 9 4443.56 158.29 0 4 9 4455.84 160.51 0 4 9 4484.83 157.93 0 4 -10 1008.16 80.00 0 4 10 1013.88 75.89 0 4 -10 979.16 44.13 0 4 10 939.64 46.97 0 4 10 905.77 45.67 0 4 10 896.89 49.66 0 4 10 939.84 47.65 0 4 -10 875.65 46.57 0 4 10 907.40 46.38 0 4 -10 827.39 63.71 0 4 10 1028.74 48.11 0 4 -10 987.13 42.90 0 4 10 943.97 50.26 0 4 11 2385.42 124.21 0 4 -11 2199.21 112.45 0 4 11 2397.62 91.34 0 4 11 2346.31 91.80 0 4 11 2280.09 93.31 0 4 -11 2227.98 125.41 0 4 11 2393.93 90.66 0 4 -11 2170.89 90.37 0 4 11 2344.07 94.99 0 4 11 2287.62 90.35 0 4 -11 2397.27 88.49 0 4 -11 2224.76 86.23 0 4 11 2278.16 91.30 0 4 -12 5764.98 205.81 0 4 12 6140.03 209.59 0 4 12 5906.98 209.44 0 4 12 6073.68 213.86 0 4 -12 5440.54 232.78 0 4 -12 5708.35 248.74 0 4 12 5745.00 209.04 0 4 12 5975.05 212.68 0 4 12 6337.38 209.97 0 4 12 6153.41 246.08 0 4 -12 5864.10 208.20 0 4 12 5969.96 209.96 0 4 12 5917.23 209.97 0 4 -12 5566.51 207.15 0 4 -13 3432.29 131.62 0 4 13 3478.94 168.58 0 4 13 3786.01 134.80 0 4 -13 3185.10 130.35 0 4 13 3677.48 133.16 0 4 -13 3350.58 127.69 0 4 13 3626.73 134.15 0 4 13 3603.22 134.43 0 4 13 3747.50 137.27 0 4 -13 3739.10 176.98 0 4 13 3549.71 133.38 0 4 -14 2215.44 85.88 0 4 -14 2108.78 81.81 0 4 14 2027.60 92.37 0 4 14 2148.07 86.75 0 4 14 2168.93 124.22 0 4 14 2068.09 88.64 0 4 -14 2049.01 86.44 0 4 14 2100.41 88.28 0 4 14 2016.43 88.22 0 4 -14 2013.86 86.31 0 4 14 1982.33 88.49 0 4 -14 1940.94 125.95 0 4 15 1627.70 73.67 0 4 15 1535.57 75.18 0 4 15 1745.90 76.69 0 4 15 1700.48 75.71 0 4 -15 1648.87 73.02 0 4 -15 1448.92 68.95 0 4 15 1712.27 75.94 0 4 -15 1634.20 66.90 0 4 -15 1632.25 114.36 0 4 -15 1688.28 72.77 0 4 -15 1679.36 74.84 0 4 15 1680.08 110.44 0 4 -15 1579.47 74.16 0 4 -16 1417.38 67.86 0 4 -16 1320.84 68.01 0 4 16 1462.88 68.26 0 4 -16 1355.07 66.87 0 4 -16 1332.96 66.55 0 4 16 1382.62 66.40 0 4 -16 1383.38 62.42 0 4 16 1539.60 71.55 0 4 16 1501.34 68.89 0 4 16 1464.63 69.81 0 4 16 1351.82 100.69 0 4 -16 1288.54 101.51 0 4 17 732.65 49.43 0 4 -17 839.11 47.51 0 4 -17 754.49 49.63 0 4 -17 752.60 46.95 0 4 -17 792.48 78.42 0 4 17 603.19 74.87 0 4 17 858.94 48.13 0 4 -17 775.82 47.89 0 4 17 792.12 52.13 0 4 17 749.55 50.78 0 4 17 783.11 49.88 0 4 18 68.11 28.80 0 4 -18 65.42 28.18 0 4 -18 64.71 31.65 0 4 18 68.66 35.09 0 4 18 21.26 31.86 0 4 18 40.59 30.96 0 4 -18 20.07 27.27 0 4 -18 33.84 31.48 0 4 -19 285.78 31.04 0 4 19 322.50 31.48 0 4 -19 265.44 30.36 0 4 19 258.10 36.52 0 4 19 286.58 33.57 0 4 -19 278.72 33.97 0 4 20 578.23 35.76 0 4 -20 690.28 36.71 0 4 20 580.29 40.53 0 4 -20 592.34 34.84 0 4 -21 92.58 19.58 0 4 21 92.28 24.77 0 4 21 118.37 19.59 0 4 -22 60.85 11.79 0 4 22 52.50 12.26 0 4 22 59.30 19.01 0 5 0 -45.20 42.52 0 5 0 -1.40 19.71 0 5 0 10.35 18.12 0 5 0 15.19 16.16 0 5 0 2.27 33.43 0 5 1 537.65 50.24 0 5 -1 567.97 29.47 0 5 1 526.42 31.85 0 5 -1 501.59 56.92 0 5 1 621.98 33.35 0 5 -1 603.83 31.42 0 5 1 632.88 30.59 0 5 -1 521.83 47.72 0 5 1 564.81 28.40 0 5 -1 617.51 32.99 0 5 -2 7838.10 269.05 0 5 2 7964.50 270.98 0 5 -2 7942.98 270.98 0 5 2 7817.97 268.85 0 5 2 8180.24 270.47 0 5 2 8186.05 271.92 0 5 2 7670.47 292.04 0 5 -2 7920.16 270.09 0 5 -2 7790.39 299.28 0 5 -2 8080.55 290.11 0 5 -3 8765.84 312.07 0 5 3 8857.38 291.31 0 5 3 8829.09 293.33 0 5 -3 8339.84 290.46 0 5 3 8696.78 293.67 0 5 3 8605.78 292.23 0 5 -3 8499.08 291.47 0 5 -3 8676.39 292.58 0 5 -3 8154.98 320.08 0 5 3 8163.01 315.18 0 5 4 332.47 27.68 0 5 -4 350.69 26.04 0 5 4 308.97 48.57 0 5 4 297.74 29.16 0 5 -4 300.27 39.60 0 5 4 297.99 24.02 0 5 -4 317.59 24.23 0 5 -4 287.77 51.60 0 5 4 321.20 26.95 0 5 -5 952.15 71.16 0 5 -5 806.24 39.75 0 5 -5 776.25 37.48 0 5 5 785.23 41.34 0 5 5 824.36 39.11 0 5 5 767.79 42.94 0 5 -5 870.48 56.75 0 5 5 755.74 42.46 0 5 -6 2911.85 104.99 0 5 6 2913.14 107.82 0 5 6 2830.55 105.04 0 5 -6 3030.58 138.48 0 5 6 2835.69 107.72 0 5 6 2829.70 106.62 0 5 -6 2811.18 124.16 0 5 6 2871.82 102.25 0 5 6 2759.53 105.48 0 5 -6 2741.26 103.83 0 5 6 2795.75 105.94 0 5 -6 2839.06 103.35 0 5 -7 3225.33 117.96 0 5 -7 2997.39 117.83 0 5 -7 3125.74 117.52 0 5 7 3109.42 119.36 0 5 -7 3490.19 141.30 0 5 -7 3363.27 117.37 0 5 7 3361.27 119.52 0 5 7 3434.95 121.09 0 5 7 3073.60 119.71 0 5 7 3337.10 122.44 0 5 7 3237.56 122.07 0 5 7 3366.90 117.12 0 5 -7 3546.18 155.80 0 5 -7 3419.38 118.74 0 5 -7 3033.20 117.85 0 5 8 1611.00 68.94 0 5 8 1610.86 69.85 0 5 8 1480.38 66.41 0 5 -8 1525.79 63.29 0 5 8 1652.25 67.12 0 5 8 1590.81 66.55 0 5 -8 1559.39 83.93 0 5 -8 1530.76 62.12 0 5 -8 1497.84 95.44 0 5 -8 1492.57 63.93 0 5 8 1631.77 70.21 0 5 8 1577.66 63.43 0 5 -8 1514.46 61.86 0 5 -8 1448.82 64.64 0 5 -8 1471.13 63.76 0 5 -8 1589.46 64.26 0 5 8 1458.55 65.89 0 5 9 545.97 36.95 0 5 -9 523.88 66.82 0 5 9 518.92 31.80 0 5 -9 473.44 29.63 0 5 9 543.09 62.49 0 5 9 398.16 38.29 0 5 9 489.72 36.45 0 5 -9 563.27 34.66 0 5 9 540.14 37.36 0 5 -9 524.85 50.33 0 5 -9 493.71 33.93 0 5 9 551.87 37.22 0 5 9 480.40 40.12 0 5 -9 572.30 34.59 0 5 -9 548.67 33.78 0 5 -9 522.07 35.71 0 5 -9 487.95 32.13 0 5 9 525.00 33.06 0 5 9 433.20 38.95 0 5 10 1610.80 69.53 0 5 -10 1535.94 64.08 0 5 10 1671.15 99.62 0 5 10 1492.19 70.33 0 5 -10 1642.18 106.48 0 5 10 1633.80 68.88 0 5 -10 1587.90 65.97 0 5 -10 1535.50 62.87 0 5 -10 1512.56 68.10 0 5 -10 1514.41 67.31 0 5 -10 1516.91 66.80 0 5 10 1571.41 72.85 0 5 10 1527.25 73.46 0 5 10 1511.73 65.28 0 5 10 1556.93 65.96 0 5 -10 1507.15 65.15 0 5 10 1577.63 69.62 0 5 -11 668.61 38.85 0 5 -11 695.30 42.23 0 5 -11 642.78 42.15 0 5 11 743.59 44.46 0 5 11 624.13 41.61 0 5 11 711.33 69.01 0 5 -11 681.84 40.67 0 5 -11 654.08 40.15 0 5 11 684.80 41.25 0 5 -11 697.89 78.61 0 5 11 698.29 45.09 0 5 11 682.69 49.77 0 5 11 736.13 46.63 0 5 -11 676.30 42.73 0 5 11 680.07 50.95 0 5 -12 16.83 25.42 0 5 12 33.87 30.67 0 5 12 -16.89 37.14 0 5 12 -37.88 50.95 0 5 12 26.58 33.23 0 5 -12 45.67 20.92 0 5 -12 14.20 28.45 0 5 12 10.75 26.39 0 5 -12 18.87 23.94 0 5 12 16.82 27.42 0 5 12 -6.18 28.91 0 5 -12 15.36 52.23 0 5 -12 29.93 27.65 0 5 -12 23.63 27.86 0 5 -13 660.12 78.65 0 5 -13 682.89 46.80 0 5 -13 601.59 39.42 0 5 13 706.23 48.03 0 5 -13 697.06 38.09 0 5 13 596.18 52.43 0 5 13 649.80 43.20 0 5 -13 675.52 44.57 0 5 13 637.46 43.75 0 5 13 632.36 49.58 0 5 13 732.93 46.25 0 5 13 536.15 69.16 0 5 -13 665.39 41.06 0 5 14 5902.30 222.01 0 5 14 5964.32 220.58 0 5 14 6526.95 223.03 0 5 -14 6326.99 222.63 0 5 -14 6265.72 218.68 0 5 14 6380.98 223.76 0 5 -14 6156.78 218.15 0 5 -14 5991.14 220.10 0 5 -14 6044.06 221.68 0 5 14 6498.47 226.73 0 5 14 6536.71 224.02 0 5 14 6396.17 261.14 0 5 -14 5918.79 266.43 0 5 15 1247.81 65.63 0 5 15 1496.22 71.47 0 5 -15 1437.97 61.54 0 5 15 1486.32 70.46 0 5 -15 1449.18 68.27 0 5 -15 1411.01 67.28 0 5 15 1356.77 66.97 0 5 -15 1415.27 67.52 0 5 15 1365.31 71.52 0 5 -15 1472.63 106.26 0 5 15 1500.61 68.69 0 5 16 259.82 33.98 0 5 -16 344.54 35.59 0 5 16 305.69 35.37 0 5 16 253.04 37.92 0 5 16 267.42 40.36 0 5 16 236.38 35.00 0 5 -16 337.85 61.23 0 5 -16 283.35 27.16 0 5 -16 330.97 37.65 0 5 -16 303.16 35.06 0 5 17 2312.55 95.18 0 5 -17 2211.39 84.78 0 5 17 2163.98 93.05 0 5 -17 2371.29 92.57 0 5 17 2341.88 94.40 0 5 17 2371.46 92.90 0 5 -17 2347.92 92.85 0 5 -17 2356.98 92.74 0 5 17 1988.71 91.54 0 5 -18 633.41 39.56 0 5 -18 585.12 38.63 0 5 18 606.07 43.78 0 5 18 570.85 40.21 0 5 -18 548.93 40.89 0 5 -18 631.49 40.13 0 5 -19 51.87 25.31 0 5 19 23.76 29.58 0 5 -19 29.24 27.23 0 5 -19 54.54 24.27 0 5 19 37.49 23.14 0 5 -19 43.67 24.49 0 5 20 424.68 27.33 0 5 20 392.66 32.52 0 5 -20 416.84 29.84 0 5 -20 410.08 28.45 0 5 -20 350.61 27.12 0 5 21 1728.36 63.92 0 5 -21 1725.89 61.61 0 5 -21 1779.67 63.25 0 6 0 568.54 36.15 0 6 0 570.76 54.49 0 6 0 534.85 31.89 0 6 0 560.06 31.74 0 6 0 567.80 36.52 0 6 0 620.17 32.66 0 6 0 550.68 34.07 0 6 -1 426.51 27.29 0 6 -1 415.59 28.32 0 6 1 362.20 29.54 0 6 1 420.19 28.69 0 6 1 435.62 32.37 0 6 -1 409.85 29.31 0 6 1 431.73 49.13 0 6 -1 358.71 45.88 0 6 1 466.23 28.07 0 6 1 410.32 27.98 0 6 -1 416.21 28.35 0 6 1 388.90 30.19 0 6 -1 395.33 31.25 0 6 -2 2632.36 95.24 0 6 -2 2470.13 115.64 0 6 2 2667.34 95.66 0 6 -2 2653.92 93.95 0 6 2 2378.35 92.28 0 6 2 2554.63 96.31 0 6 -2 2427.38 92.80 0 6 -2 2286.05 91.96 0 6 2 2579.46 93.46 0 6 -2 2563.17 91.90 0 6 2 2428.99 120.10 0 6 -2 2411.32 92.53 0 6 -2 2550.29 128.60 0 6 2 2282.72 94.33 0 6 -2 2383.76 91.95 0 6 3 10031.1 332.8 0 6 -3 9653.67 333.53 0 6 3 9296.05 335.53 0 6 -3 9552.83 333.53 0 6 -3 10241.6 372.9 0 6 -3 10229.0 334.1 0 6 3 10122.9 336.0 0 6 -3 9837.10 333.88 0 6 3 10088.9 334.4 0 6 3 9795.73 332.81 0 6 3 8940.52 334.60 0 6 -3 10486.9 335.6 0 6 -3 9784.09 358.15 0 6 3 9909.41 336.43 0 6 3 9282.90 362.13 0 6 -4 2348.74 89.39 0 6 4 2389.57 90.00 0 6 4 2333.80 94.50 0 6 -4 2435.98 91.30 0 6 4 2394.58 94.09 0 6 -4 2406.18 127.14 0 6 4 2268.53 92.76 0 6 -4 2347.19 90.59 0 6 4 2333.78 93.52 0 6 4 2497.62 89.49 0 6 4 2298.97 91.54 0 6 -4 2491.49 91.28 0 6 -4 2320.26 90.66 0 6 -4 2248.34 111.29 0 6 -4 2433.14 90.38 0 6 -4 2540.83 92.71 0 6 5 21.33 24.73 0 6 -5 45.97 32.24 0 6 -5 52.51 19.57 0 6 -5 74.11 21.73 0 6 -5 29.02 20.61 0 6 5 36.00 24.81 0 6 -5 78.41 22.06 0 6 -5 12.21 21.67 0 6 -5 61.33 22.44 0 6 5 35.41 23.19 0 6 5 70.10 27.27 0 6 -5 70.89 21.25 0 6 5 44.81 28.03 0 6 5 22.66 20.37 0 6 -5 36.95 46.34 0 6 -6 712.38 38.74 0 6 -6 620.43 36.54 0 6 6 633.07 42.70 0 6 6 662.95 40.72 0 6 -6 553.72 36.40 0 6 -6 801.36 74.74 0 6 -6 711.98 36.31 0 6 -6 624.18 37.21 0 6 -6 587.24 37.58 0 6 6 676.08 38.91 0 6 -6 591.82 36.25 0 6 -6 657.37 55.76 0 6 6 662.21 43.75 0 6 6 612.99 40.18 0 6 -7 3503.18 131.78 0 6 -7 3722.83 130.78 0 6 -7 3560.80 132.03 0 6 7 3609.98 136.24 0 6 7 3737.18 133.35 0 6 -7 3791.58 175.25 0 6 7 3513.32 134.63 0 6 7 3421.10 137.05 0 6 -7 3597.92 131.42 0 6 7 3664.43 137.35 0 6 -7 3653.49 132.74 0 6 -7 3621.00 132.87 0 6 -7 3783.87 133.16 0 6 -7 3447.46 132.12 0 6 -8 838.31 44.02 0 6 -8 806.60 80.03 0 6 8 747.68 51.56 0 6 -8 747.38 41.04 0 6 -8 755.03 43.73 0 6 8 781.75 48.96 0 6 -8 765.65 44.78 0 6 8 783.66 51.77 0 6 8 901.98 46.58 0 6 -8 807.71 44.90 0 6 -8 802.82 44.08 0 6 8 847.20 48.04 0 6 9 1538.78 70.93 0 6 -9 1638.50 68.97 0 6 -9 1545.10 66.13 0 6 9 1536.60 75.19 0 6 9 1523.98 76.28 0 6 -9 1585.44 70.47 0 6 -9 1572.35 68.00 0 6 9 1489.62 75.96 0 6 -9 1612.29 66.87 0 6 -9 1642.15 109.56 0 6 -9 1671.40 69.29 0 6 9 1612.39 72.13 0 6 -9 1616.77 69.97 0 6 -10 261.89 31.88 0 6 10 223.18 35.91 0 6 -10 256.31 28.75 0 6 -10 236.97 31.81 0 6 10 285.33 29.71 0 6 10 252.95 43.00 0 6 -10 270.21 29.87 0 6 -10 232.52 28.80 0 6 10 235.53 40.32 0 6 10 236.02 35.72 0 6 10 249.55 35.43 0 6 -10 196.72 32.11 0 6 -10 210.27 25.73 0 6 -10 242.11 60.09 0 6 -10 222.51 32.86 0 6 -11 146.02 27.70 0 6 -11 146.37 23.77 0 6 -11 152.95 33.31 0 6 -11 143.40 27.80 0 6 11 122.04 34.27 0 6 -11 48.03 53.79 0 6 -11 170.67 31.30 0 6 11 135.16 38.30 0 6 11 90.03 40.68 0 6 -11 141.33 26.27 0 6 11 123.14 26.31 0 6 -11 160.34 29.66 0 6 11 124.82 33.81 0 6 11 140.22 34.95 0 6 -11 136.71 29.33 0 6 12 7600.15 274.79 0 6 12 8197.63 279.36 0 6 -12 8050.90 277.67 0 6 12 7810.99 281.42 0 6 -12 7767.13 274.44 0 6 -12 7673.68 274.91 0 6 -12 8127.46 275.37 0 6 -12 8044.20 277.38 0 6 -12 7993.74 274.22 0 6 12 7546.92 279.52 0 6 -12 7997.90 326.20 0 6 -12 8034.70 277.23 0 6 12 8184.11 279.46 0 6 -13 69.99 30.10 0 6 -13 64.26 25.16 0 6 -13 38.44 51.80 0 6 13 83.59 38.12 0 6 13 72.36 33.80 0 6 -13 52.72 31.93 0 6 -13 46.10 33.80 0 6 -13 66.22 27.78 0 6 -13 86.25 32.16 0 6 13 30.23 25.66 0 6 13 50.21 32.07 0 6 -13 77.23 24.28 0 6 -13 29.99 28.16 0 6 14 132.29 36.54 0 6 14 164.06 36.90 0 6 -14 170.44 24.67 0 6 -14 150.99 55.29 0 6 -14 181.73 35.56 0 6 14 143.55 28.89 0 6 -14 159.45 32.33 0 6 -14 165.93 28.37 0 6 -14 201.78 32.08 0 6 -14 172.10 30.70 0 6 14 217.61 36.42 0 6 -15 209.86 36.54 0 6 15 222.69 30.62 0 6 15 244.56 36.22 0 6 15 297.49 40.42 0 6 -15 245.52 31.15 0 6 -15 261.58 29.28 0 6 -15 186.62 33.07 0 6 16 1166.85 57.14 0 6 -16 1107.71 53.99 0 6 -16 1156.38 58.65 0 6 -16 1127.42 55.05 0 6 16 1217.41 60.93 0 6 -16 1078.85 50.23 0 6 16 935.48 52.68 0 6 17 138.89 33.43 0 6 -17 202.71 30.78 0 6 -17 158.93 29.95 0 6 -17 197.80 28.95 0 6 17 210.49 29.74 0 6 -17 193.77 21.66 0 6 -18 12.05 23.20 0 6 18 0.85 23.65 0 6 18 27.55 27.87 0 6 -18 36.28 25.58 0 6 -18 18.08 24.04 0 6 19 557.58 33.87 0 6 -19 540.04 31.23 0 6 19 480.30 30.43 0 6 -19 513.61 31.19 0 6 -20 175.41 17.58 0 6 20 205.79 21.49 0 6 -20 194.30 18.94 0 6 -20 159.92 19.46 0 6 20 174.24 17.03 0 7 0 19.37 28.53 0 7 0 19.68 24.38 0 7 0 1.81 20.36 0 7 0 15.93 21.16 0 7 0 10.47 35.61 0 7 0 26.16 22.75 0 7 0 -4.61 21.79 0 7 -1 782.00 43.79 0 7 1 656.78 65.26 0 7 -1 790.62 40.46 0 7 -1 784.59 40.26 0 7 1 773.51 41.09 0 7 -1 779.83 43.09 0 7 -1 762.51 41.12 0 7 1 731.16 42.16 0 7 1 786.32 47.43 0 7 -1 791.07 64.20 0 7 -1 796.94 46.52 0 7 1 825.53 45.72 0 7 1 810.81 41.81 0 7 -1 774.66 42.41 0 7 1 809.99 47.62 0 7 -2 684.95 39.75 0 7 -2 780.50 39.52 0 7 2 704.82 44.45 0 7 -2 722.33 41.35 0 7 2 732.91 37.71 0 7 -2 753.40 45.07 0 7 2 659.36 40.98 0 7 2 713.73 46.16 0 7 2 739.68 40.20 0 7 -2 702.84 41.70 0 7 2 547.66 61.49 0 7 -2 715.17 40.81 0 7 -2 672.49 61.14 0 7 2 681.69 46.53 0 7 -3 788.21 44.29 0 7 -3 918.83 49.05 0 7 3 835.28 49.53 0 7 3 769.76 49.51 0 7 -3 875.28 45.47 0 7 3 860.22 46.83 0 7 -3 884.80 45.28 0 7 -3 836.46 45.01 0 7 -3 831.41 81.50 0 7 -3 864.02 43.73 0 7 3 844.21 51.68 0 7 3 853.08 43.39 0 7 -4 300.24 29.67 0 7 4 332.40 37.42 0 7 -4 395.13 31.09 0 7 -4 314.10 34.91 0 7 4 321.14 35.61 0 7 4 325.96 29.13 0 7 4 297.49 32.84 0 7 -4 335.07 63.89 0 7 4 342.22 39.67 0 7 -4 327.16 30.68 0 7 -4 367.14 32.52 0 7 5 2408.67 95.98 0 7 -5 2484.70 97.12 0 7 5 2364.34 100.37 0 7 5 2381.18 102.05 0 7 -5 2623.41 97.86 0 7 -5 2414.34 96.88 0 7 5 2472.30 103.69 0 7 -5 2547.93 95.81 0 7 -5 2587.63 140.29 0 7 5 2561.83 99.74 0 7 -5 2578.29 99.23 0 7 5 2534.19 94.92 0 7 -5 2448.97 95.28 0 7 -5 2505.22 97.70 0 7 6 3295.12 129.42 0 7 6 3377.08 124.01 0 7 -6 3035.65 164.47 0 7 -6 3367.60 124.35 0 7 -6 3267.01 123.05 0 7 6 3261.65 128.13 0 7 6 3163.85 127.03 0 7 -6 3388.46 124.82 0 7 -6 3330.64 124.84 0 7 6 3233.75 127.00 0 7 -6 3365.74 125.26 0 7 6 3365.54 130.73 0 7 -7 61.48 24.40 0 7 -7 51.57 28.02 0 7 7 58.42 27.36 0 7 -7 67.18 54.14 0 7 -7 46.69 26.50 0 7 -7 14.72 25.86 0 7 7 48.89 36.62 0 7 7 45.51 36.56 0 7 7 102.65 33.90 0 7 -7 51.15 25.89 0 7 7 43.75 32.63 0 7 -7 34.83 24.02 0 7 -8 1401.71 65.87 0 7 8 1410.33 69.27 0 7 -8 1389.83 63.30 0 7 8 1339.43 65.12 0 7 -8 1558.84 107.70 0 7 8 1458.22 74.38 0 7 8 1440.17 69.52 0 7 -8 1330.96 62.46 0 7 -8 1408.59 65.11 0 7 -8 1370.21 63.67 0 7 -8 1450.55 64.74 0 7 -8 1461.19 65.27 0 7 8 1462.62 73.51 0 7 -9 339.09 34.55 0 7 9 239.43 38.22 0 7 -9 258.95 31.73 0 7 -9 372.47 63.02 0 7 9 226.37 43.18 0 7 -9 253.08 33.44 0 7 9 317.89 39.38 0 7 9 238.24 34.04 0 7 -9 251.92 34.41 0 7 -9 235.01 30.22 0 7 -9 295.68 33.95 0 7 -9 233.19 30.83 0 7 -10 387.07 38.68 0 7 10 437.98 48.79 0 7 10 374.08 43.81 0 7 -10 433.93 38.54 0 7 -10 460.70 37.97 0 7 10 433.92 44.29 0 7 -10 501.81 36.06 0 7 10 367.60 39.01 0 7 -10 447.52 35.92 0 7 -10 506.13 72.14 0 7 -10 418.44 32.55 0 7 -11 200.72 31.61 0 7 -11 164.10 30.72 0 7 11 169.32 36.99 0 7 -11 193.75 27.30 0 7 -11 227.65 27.49 0 7 -11 188.61 27.79 0 7 -11 176.18 26.02 0 7 11 126.71 32.09 0 7 11 208.26 38.86 0 7 -11 158.14 34.33 0 7 -11 212.44 57.56 0 7 -11 166.54 30.98 0 7 11 163.63 38.64 0 7 -12 4594.40 165.20 0 7 12 4553.34 168.24 0 7 -12 4323.05 161.00 0 7 -12 4472.11 164.69 0 7 12 4474.87 165.97 0 7 -12 4481.98 209.40 0 7 12 4451.26 169.97 0 7 -12 4877.88 164.99 0 7 -12 4377.27 161.82 0 7 12 4659.86 168.06 0 7 -12 4740.46 165.44 0 7 -12 4577.07 162.70 0 7 -12 4140.29 158.92 0 7 -13 1629.95 69.64 0 7 -13 1450.30 66.47 0 7 13 1698.45 74.43 0 7 13 1601.80 73.00 0 7 13 1419.27 71.31 0 7 -13 1619.79 71.53 0 7 -13 1569.88 66.38 0 7 -13 1456.12 69.75 0 7 -13 1549.09 70.52 0 7 -13 1490.60 65.21 0 7 -14 1223.58 58.78 0 7 -14 1283.21 58.86 0 7 14 1275.55 65.67 0 7 -14 1275.47 56.52 0 7 14 1346.07 63.99 0 7 -14 1365.23 63.48 0 7 -14 1361.51 59.26 0 7 -14 1388.51 62.42 0 7 -15 473.57 38.80 0 7 -15 417.25 27.88 0 7 -15 463.87 34.36 0 7 15 419.22 39.92 0 7 -15 481.06 33.09 0 7 -15 498.92 32.64 0 7 15 533.30 38.90 0 7 -15 472.34 37.09 0 7 -16 2236.29 87.31 0 7 -16 2214.16 83.49 0 7 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28.88 0 8 3 107.18 34.54 0 8 -3 104.28 25.19 0 8 3 151.31 28.50 0 8 3 90.12 35.78 0 8 -3 117.51 29.02 0 8 -3 145.09 27.52 0 8 4 1398.15 72.54 0 8 -4 1609.67 66.24 0 8 4 1465.16 63.71 0 8 -4 1537.27 67.48 0 8 4 1388.81 66.83 0 8 4 1294.00 70.24 0 8 -4 1481.59 64.34 0 8 4 1393.04 71.09 0 8 -4 1356.87 63.28 0 8 -4 1361.79 68.29 0 8 5 709.47 54.07 0 8 5 759.74 51.42 0 8 -5 849.45 48.72 0 8 5 776.15 48.20 0 8 -5 848.06 47.07 0 8 5 828.38 53.93 0 8 -5 797.64 47.15 0 8 -5 794.29 49.08 0 8 5 831.85 43.60 0 8 -6 9210.86 315.73 0 8 6 8568.74 316.75 0 8 6 8982.32 319.62 0 8 6 9119.55 312.70 0 8 -6 9481.24 316.43 0 8 6 8946.70 321.06 0 8 -6 9640.20 316.68 0 8 6 9236.17 320.17 0 8 -6 8859.23 313.59 0 8 -6 8999.20 316.65 0 8 -6 9563.15 317.32 0 8 7 477.42 41.28 0 8 7 501.70 47.10 0 8 -7 476.31 39.13 0 8 7 501.22 48.70 0 8 -7 570.10 39.24 0 8 -7 536.52 40.66 0 8 -7 481.77 70.28 0 8 -7 552.76 36.90 0 8 7 433.73 44.20 0 8 -7 443.58 37.02 0 8 -8 89.01 27.09 0 8 -8 53.49 28.35 0 8 -8 54.71 24.60 0 8 -8 32.00 27.31 0 8 8 31.02 25.73 0 8 8 -1.45 36.58 0 8 -8 56.47 27.68 0 8 -8 23.97 31.15 0 8 -8 5.36 48.48 0 8 8 -7.97 31.62 0 8 -9 1166.65 55.42 0 8 -9 1230.44 59.23 0 8 9 1013.66 54.95 0 8 -9 1255.31 59.39 0 8 -9 1156.30 90.95 0 8 -9 1180.88 55.69 0 8 9 1099.84 64.19 0 8 -9 1211.28 59.76 0 8 -9 1146.79 56.32 0 8 -9 1111.72 54.65 0 8 9 1086.19 60.79 0 8 -10 182.13 30.64 0 8 10 189.30 35.85 0 8 -10 198.45 31.53 0 8 -10 195.53 30.14 0 8 -10 205.98 27.73 0 8 10 221.79 30.17 0 8 -10 160.93 31.51 0 8 -10 193.40 33.20 0 8 -11 3537.09 127.26 0 8 11 3153.07 130.83 0 8 -11 3341.74 124.22 0 8 -11 3695.51 127.37 0 8 -11 3440.42 128.05 0 8 -11 3560.77 127.43 0 8 11 3009.58 126.58 0 8 -12 64.13 20.73 0 8 12 52.12 24.63 0 8 -12 69.46 28.16 0 8 -12 78.23 25.34 0 8 -12 65.24 29.76 0 8 12 81.77 33.79 0 8 -13 252.79 27.58 0 8 -13 340.73 31.54 0 8 -13 339.63 30.92 0 8 13 329.19 35.54 0 8 -13 376.93 32.93 0 8 -14 47.59 24.07 0 8 -14 -9.88 23.25 0 8 -14 32.71 23.52 0 8 14 6.78 26.41 0 8 -14 52.25 16.16 0 8 -14 18.17 18.47 0 8 -15 1090.22 47.10 0 8 -15 1037.33 45.10 0 8 -15 1071.26 47.29 0 8 15 1106.12 48.85 0 8 16 109.09 22.05 0 8 -16 109.14 20.71 0 8 -16 132.54 20.81 0 8 -16 113.73 17.16 0 8 17 276.53 19.31 0 8 -17 274.74 20.25 0 9 0 26.70 28.28 0 9 0 11.33 28.02 0 9 0 28.01 24.05 0 9 0 -12.01 33.26 0 9 1 1388.27 69.82 0 9 -1 1409.12 64.52 0 9 -1 1539.16 67.45 0 9 -1 1391.23 60.81 0 9 1 1513.75 66.18 0 9 -1 1397.46 68.67 0 9 -1 1422.75 64.40 0 9 1 1286.13 65.81 0 9 1 1479.24 62.95 0 9 -2 712.96 39.36 0 9 -2 662.93 45.57 0 9 -2 716.13 39.81 0 9 2 586.12 44.94 0 9 2 777.53 40.63 0 9 -2 656.29 45.94 0 9 2 619.74 49.10 0 9 -2 738.12 44.76 0 9 2 710.74 43.80 0 9 -3 1619.93 67.50 0 9 3 1414.06 71.13 0 9 -3 1569.40 65.87 0 9 3 1390.43 73.63 0 9 -3 1590.99 71.58 0 9 -3 1569.01 70.44 0 9 -3 1568.36 70.74 0 9 3 1629.94 68.32 0 9 -4 60.18 28.87 0 9 -4 3.35 29.86 0 9 -4 54.66 26.86 0 9 4 35.78 35.62 0 9 -4 21.86 24.53 0 9 4 24.42 31.28 0 9 4 17.48 22.09 0 9 5 442.00 43.08 0 9 5 457.03 45.73 0 9 5 490.12 37.55 0 9 -5 497.56 35.83 0 9 -5 515.33 38.62 0 9 -5 549.51 38.39 0 9 5 545.76 33.94 0 9 -5 491.44 40.12 0 9 6 1360.65 70.30 0 9 -6 1465.33 64.80 0 9 -6 1527.11 66.51 0 9 6 1491.52 61.26 0 9 -6 1517.13 67.81 0 9 -6 1507.10 68.88 0 9 6 1424.34 66.48 0 9 6 1472.90 73.22 0 9 -6 1510.97 66.73 0 9 -7 1313.94 61.51 0 9 -7 1247.92 57.48 0 9 7 1156.39 63.11 0 9 -7 1202.20 57.62 0 9 -7 1317.62 59.22 0 9 7 1097.27 58.88 0 9 -7 1304.27 59.63 0 9 -8 -3.00 27.80 0 9 8 27.58 31.73 0 9 -8 18.50 27.36 0 9 -8 8.81 24.53 0 9 8 9.92 26.17 0 9 8 8.67 33.05 0 9 9 122.76 28.27 0 9 -9 138.62 26.81 0 9 -9 81.15 24.77 0 9 -9 146.74 30.59 0 9 -10 624.63 37.29 0 9 -10 728.91 40.12 0 9 -10 644.71 39.56 0 9 -10 691.88 40.66 0 9 -11 11.61 23.52 0 9 -11 41.93 19.20 0 9 -11 42.73 19.78 0 9 -11 31.15 23.79 0 9 -11 38.16 25.51 0 9 -12 69.91 21.87 0 9 12 59.65 26.31 0 9 -12 22.55 19.62 0 9 -12 50.82 19.26 0 9 -13 149.34 21.80 0 9 -13 112.78 14.74 0 9 -13 135.66 18.72 0 9 -13 114.47 18.98 0 9 -14 143.65 16.33 0 9 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1987.92 77.55 -1 6 0 1728.90 76.15 1 6 0 1940.61 74.74 1 6 0 2039.65 76.28 -1 6 0 1848.47 74.96 1 6 0 1964.08 74.98 -1 6 0 1977.87 74.93 1 6 1 5469.88 190.48 -1 6 -1 5476.52 187.11 1 6 1 5248.92 219.07 -1 6 -1 5497.58 188.66 1 6 1 5463.48 189.08 -1 6 -1 5376.62 187.71 1 6 1 5336.82 189.64 -1 6 -1 5421.68 187.88 1 6 1 5306.74 187.22 1 6 1 5300.69 187.40 1 6 1 5412.25 187.17 -1 6 -1 5151.02 186.34 1 6 2 1373.62 88.13 1 6 2 1338.95 57.36 -1 6 -2 1322.19 57.80 -1 6 -2 1432.80 58.85 1 6 2 1366.39 56.61 1 6 2 1385.67 61.31 -1 6 -2 1335.54 57.51 1 6 2 1419.08 58.08 -1 6 -2 1479.39 91.62 -1 6 -2 1387.27 57.95 1 6 2 1378.05 62.06 1 6 2 1335.78 59.58 1 6 3 1744.17 69.36 1 6 3 1737.74 71.19 -1 6 -3 1775.43 100.15 -1 6 -3 1682.86 69.45 1 6 3 1735.93 68.32 -1 6 -3 1686.26 68.80 -1 6 -3 1697.25 68.26 1 6 3 1749.16 73.24 1 6 3 1647.45 71.38 1 6 3 1565.56 98.09 1 6 3 1804.47 74.03 -1 6 -3 1718.24 69.50 1 6 3 1541.48 71.76 -1 6 -3 1809.44 69.75 1 6 3 1813.30 67.50 1 6 4 2808.95 108.92 -1 6 -4 2759.96 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1153.42 48.01 1 7 -18 1165.78 47.44 1 7 -18 1063.55 47.92 -1 7 18 1105.86 49.66 -1 7 18 1261.30 50.12 1 7 -18 1145.38 48.76 1 7 -17 51.56 22.62 -1 7 17 120.87 25.56 1 7 -17 92.87 21.05 1 7 -17 61.49 21.53 1 7 -17 80.70 23.47 1 7 -17 68.42 16.47 -1 7 17 62.00 25.84 1 7 -16 796.17 44.43 1 7 -16 818.68 42.80 1 7 -16 795.28 39.65 -1 7 16 913.49 47.54 1 7 -16 799.31 41.77 1 7 -16 900.90 46.60 1 7 -15 370.56 30.57 -1 7 15 510.19 41.00 1 7 -15 478.51 38.21 1 7 -15 443.05 31.40 1 7 -15 390.62 33.08 1 7 -15 461.51 33.54 1 7 -14 205.62 27.48 1 7 -14 180.32 26.97 1 7 -14 223.18 28.80 -1 7 14 222.77 36.35 1 7 -14 179.40 28.97 1 7 -14 195.34 32.72 1 7 -14 164.20 23.21 1 7 -14 162.15 33.66 1 7 -13 687.41 41.57 1 7 -13 637.95 43.58 1 7 -13 600.46 39.40 -1 7 13 602.75 47.64 1 7 -13 632.18 37.54 1 7 -13 597.51 44.27 1 7 -13 636.17 40.94 1 7 -12 199.90 34.08 1 7 -12 268.58 29.29 -1 7 12 231.02 39.03 -1 7 12 281.53 39.63 1 7 -12 324.15 61.07 1 7 -12 156.48 32.13 1 7 -12 210.93 35.60 1 7 -12 188.70 32.98 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3806.46 149.73 1 7 -5 4183.12 146.02 -1 7 4 840.62 51.48 1 7 -4 996.50 48.17 -1 7 4 995.65 49.46 1 7 -4 905.84 74.28 1 7 -4 979.16 50.80 1 7 -4 801.87 82.94 1 7 -4 1015.60 49.85 1 7 -4 987.79 54.43 1 7 -4 1004.49 51.62 -1 7 4 912.42 53.42 1 7 -4 1035.70 50.27 1 7 -4 996.98 49.77 -1 7 4 994.52 47.07 -1 7 4 974.88 55.26 1 7 -3 1926.16 120.91 1 7 -3 1920.07 76.13 1 7 -3 1664.57 104.44 -1 7 3 1850.35 80.68 1 7 -3 1832.71 76.65 -1 7 3 1896.45 75.02 1 7 -3 1841.02 77.61 1 7 -3 1930.23 76.86 1 7 -3 1922.86 81.08 -1 7 3 1763.43 79.94 -1 7 3 1760.75 77.88 1 7 -3 1894.99 76.87 -1 7 2 4033.09 148.34 1 7 -2 4545.97 154.05 -1 7 2 4477.13 152.74 1 7 -2 3790.39 150.06 1 7 -2 3920.76 150.38 -1 7 2 3704.78 152.25 1 7 -2 3993.12 149.46 1 7 -2 4210.18 151.02 1 7 -2 4424.55 186.60 -1 7 2 4441.97 154.63 -1 7 2 4117.44 150.60 1 7 -2 4540.68 155.30 1 7 -2 4550.79 151.83 1 7 -1 4070.32 185.61 -1 7 1 4236.17 154.79 1 7 -1 4266.32 155.09 -1 7 1 4258.61 152.97 -1 7 1 4285.24 152.67 -1 7 1 3971.91 154.88 -1 7 1 4121.29 151.28 1 7 -1 4231.44 151.41 1 7 -1 4318.76 152.60 1 7 -1 4261.00 156.71 1 7 -1 4278.76 153.15 1 7 -1 4312.02 153.35 -1 7 0 45.47 27.60 -1 7 0 67.95 23.61 -1 7 0 67.26 24.26 1 7 0 49.16 22.77 1 7 0 11.96 45.73 1 7 0 89.16 20.56 1 7 0 84.26 24.70 -1 7 0 87.56 23.03 1 7 0 62.47 31.58 1 7 0 58.04 21.53 1 7 0 58.40 26.38 1 7 0 23.79 28.58 1 7 1 1077.68 56.01 1 7 1 1037.64 53.51 1 7 1 1050.85 58.65 1 7 1 1119.65 84.45 -1 7 -1 1109.79 54.68 1 7 1 1069.77 52.26 -1 7 -1 1126.37 52.19 1 7 1 1156.92 51.32 1 7 1 1078.25 49.81 -1 7 -1 1118.58 52.55 -1 7 -1 1117.20 50.26 1 7 2 466.89 32.57 -1 7 -2 501.17 35.79 1 7 2 488.52 61.99 1 7 2 452.49 41.96 -1 7 -2 489.02 33.46 -1 7 -2 513.39 34.96 1 7 2 498.55 31.36 1 7 2 496.77 40.64 1 7 2 491.64 34.61 1 7 2 484.93 38.05 -1 7 -2 459.32 35.04 1 7 3 256.42 57.76 -1 7 -3 408.90 32.81 1 7 3 414.86 40.37 1 7 3 430.27 28.67 1 7 3 373.58 36.50 -1 7 -3 385.54 32.50 -1 7 -3 376.97 29.27 1 7 3 345.75 38.93 -1 7 -3 413.62 33.18 1 7 3 369.27 31.69 -1 7 -3 367.73 32.38 1 7 3 402.82 31.00 1 7 4 140.81 35.33 1 7 4 203.90 35.19 -1 7 -4 180.79 24.67 -1 7 -4 285.35 56.22 1 7 4 168.43 28.14 -1 7 -4 157.52 25.75 1 7 4 194.46 33.38 -1 7 -4 197.21 29.43 -1 7 -4 241.65 28.25 1 7 4 214.45 25.61 1 7 5 55.77 26.37 1 7 5 89.62 34.91 -1 7 -5 89.34 22.79 -1 7 -5 115.92 26.45 -1 7 -5 69.42 51.80 1 7 5 82.88 32.42 -1 7 -5 87.90 25.68 1 7 5 76.56 35.88 -1 7 -5 120.59 28.13 1 7 5 95.30 22.89 -1 7 -5 75.16 27.70 1 7 5 64.54 29.47 1 7 6 1100.32 59.86 1 7 6 1104.07 58.21 1 7 6 1150.50 62.77 -1 7 -6 1268.11 56.31 -1 7 -6 1112.26 90.36 -1 7 -6 1245.36 58.60 -1 7 -6 1153.15 56.38 -1 7 -6 1205.39 55.12 1 7 6 1051.45 63.23 1 7 6 1179.84 66.41 -1 7 -6 1356.10 59.53 -1 7 -6 1228.28 58.60 1 7 6 1252.75 61.76 1 7 6 1219.23 53.71 -1 7 -7 1322.92 94.89 1 7 7 1234.79 63.67 -1 7 -7 1160.79 56.40 1 7 7 1176.55 60.28 -1 7 -7 1268.40 59.39 -1 7 -7 1231.89 57.24 1 7 7 1151.87 63.42 -1 7 -7 1233.24 60.27 1 7 7 1303.35 64.00 1 7 7 1138.11 66.99 -1 7 -7 1218.10 58.53 1 7 8 384.41 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1324.20 55.25 2 7 -17 1276.75 53.06 2 7 -16 194.29 26.33 -2 7 16 175.11 28.21 2 7 -16 232.71 26.24 2 7 -16 230.79 22.34 2 7 -16 166.92 25.75 2 7 -16 206.49 29.64 -2 7 16 217.58 32.03 2 7 -16 220.26 24.91 -2 7 15 1342.56 61.61 -2 7 15 1348.28 63.31 2 7 -15 1394.52 60.49 2 7 -15 1233.08 58.33 2 7 -15 1305.56 56.64 2 7 -15 1267.76 58.26 2 7 -15 1354.98 58.92 2 7 -15 1400.24 62.28 2 7 -14 6073.09 217.94 2 7 -14 6272.35 218.37 2 7 -14 6248.15 218.29 2 7 -14 6338.83 216.00 2 7 -14 5792.74 212.47 2 7 -14 5972.24 215.86 -2 7 14 6464.51 219.98 2 7 -14 6424.69 219.45 -2 7 14 6453.97 221.14 -2 7 13 20.33 32.54 2 7 -13 60.51 30.63 2 7 -13 40.30 29.22 2 7 -13 66.04 31.98 2 7 -13 33.27 28.94 2 7 -13 69.40 25.12 2 7 -13 60.62 25.58 2 7 -13 41.33 27.83 2 7 -13 35.54 21.30 -2 7 13 25.92 33.16 2 7 -12 1798.67 120.78 2 7 -12 1976.39 79.65 2 7 -12 1771.61 80.57 2 7 -12 2008.53 82.56 -2 7 12 1864.35 82.64 2 7 -12 1853.65 79.15 2 7 -12 1935.04 76.32 2 7 -12 1824.74 81.81 -2 7 12 1973.54 85.32 -2 7 11 3791.05 144.88 2 7 -11 3686.14 142.61 2 7 -11 3991.69 145.57 2 7 -11 3980.83 142.83 2 7 -11 3930.62 192.05 2 7 -11 3797.51 141.79 2 7 -11 3883.56 140.08 2 7 -11 3796.63 143.52 2 7 -11 3683.22 136.90 -2 7 11 3966.98 146.73 -2 7 10 1691.10 81.07 2 7 -10 1901.20 80.76 2 7 -10 1742.00 78.45 2 7 -10 1758.39 77.33 2 7 -10 1983.39 124.86 2 7 -10 1885.90 75.52 2 7 -10 1861.96 76.08 2 7 -10 1603.96 77.98 2 7 -10 1838.89 72.87 -2 7 10 1787.26 80.68 2 7 -9 377.85 39.23 2 7 -9 381.07 66.80 2 7 -9 330.74 35.80 2 7 -9 317.38 55.74 2 7 -9 263.35 33.50 -2 7 9 338.84 39.14 2 7 -9 337.36 32.18 2 7 -9 270.44 34.92 2 7 -9 301.57 29.70 2 7 -9 338.07 34.90 -2 7 9 317.55 38.30 2 7 -9 346.82 31.68 2 7 -8 794.63 47.33 2 7 -8 787.34 49.47 2 7 -8 652.26 69.38 2 7 -8 792.87 83.85 2 7 -8 755.45 45.13 2 7 -8 762.61 44.82 2 7 -8 696.76 43.39 2 7 -8 718.16 42.73 2 7 -8 688.52 39.69 -2 7 8 680.90 48.69 -2 7 8 629.51 44.04 -2 7 8 648.33 47.10 2 7 -7 620.89 67.28 2 7 -7 767.89 47.93 2 7 -7 649.78 81.73 2 7 -7 716.59 45.89 2 7 -7 702.22 42.86 2 7 -7 672.99 42.95 -2 7 7 616.70 45.81 2 7 -7 713.96 41.07 2 7 -7 759.55 45.71 -2 7 7 651.15 46.98 2 7 -7 650.90 41.92 2 7 -6 79.37 22.74 2 7 -6 61.79 25.57 2 7 -6 70.71 31.19 2 7 -6 45.14 43.18 2 7 -6 81.23 32.63 2 7 -6 37.87 26.89 2 7 -6 94.44 28.16 -2 7 6 68.02 29.70 2 7 -6 81.03 59.44 -2 7 6 69.64 31.00 2 7 -6 97.02 26.82 -2 7 6 58.53 34.04 -2 7 5 2699.91 111.95 -2 7 5 2774.13 110.97 2 7 -5 2873.74 113.20 2 7 -5 2863.51 107.00 2 7 -5 2846.67 144.67 2 7 -5 2622.31 151.52 2 7 -5 2956.58 110.01 2 7 -5 2965.47 111.69 2 7 -5 2891.80 109.28 2 7 -5 2802.40 109.25 -2 7 5 2715.99 111.14 2 7 -5 2811.68 107.97 2 7 -4 81.40 23.14 -2 7 4 98.84 32.05 2 7 -4 94.28 31.82 2 7 -4 109.63 25.08 2 7 -4 120.82 33.23 -2 7 4 81.20 31.85 2 7 -4 75.40 47.87 2 7 -4 67.87 56.51 2 7 -4 68.84 26.26 -2 7 4 63.33 27.13 2 7 -4 57.99 27.07 2 7 -4 81.59 27.52 2 7 -4 65.75 27.48 -2 7 4 103.45 24.00 2 7 -3 67.05 27.00 2 7 -3 78.90 23.68 2 7 -3 68.11 32.33 2 7 -3 75.08 50.20 -2 7 3 104.14 29.99 2 7 -3 76.36 26.14 2 7 -3 59.61 25.08 -2 7 3 70.70 23.42 -2 7 3 72.58 28.95 2 7 -3 93.89 30.72 2 7 -2 237.79 27.45 -2 7 2 191.76 29.74 2 7 -2 163.37 54.58 2 7 -2 220.85 36.30 2 7 -2 272.14 34.33 -2 7 2 173.22 24.39 2 7 -2 201.21 27.89 2 7 -2 206.26 27.71 -2 7 2 189.25 30.63 2 7 -2 212.55 30.79 -2 7 2 180.23 26.06 2 7 -1 5850.22 205.09 -2 7 1 5506.04 201.77 2 7 -1 5608.97 205.49 2 7 -1 5999.22 203.56 2 7 -1 5578.62 240.99 -2 7 1 5250.16 202.30 2 7 -1 5679.97 200.82 -2 7 1 5871.06 200.42 2 7 -1 5744.62 201.55 2 7 -1 5604.60 200.09 -2 7 1 5941.10 202.37 2 7 -1 5736.21 201.77 2 7 0 1079.89 87.68 2 7 0 1093.82 59.45 -2 7 0 1063.01 52.58 2 7 0 1031.34 55.03 2 7 0 978.99 56.67 -2 7 0 1094.88 51.80 2 7 0 1143.28 50.94 2 7 0 1133.55 52.58 -2 7 0 1142.15 54.15 2 7 0 1087.97 52.21 2 7 0 1010.04 51.21 -2 7 -1 117.51 27.08 2 7 1 138.71 26.54 2 7 1 130.52 30.87 2 7 1 140.31 34.74 2 7 1 122.71 51.93 -2 7 -1 107.25 26.35 -2 7 -1 126.19 26.41 2 7 1 141.91 26.26 -2 7 -1 148.55 24.93 2 7 1 109.53 25.80 2 7 1 133.70 34.42 2 7 2 1012.75 50.24 -2 7 -2 868.69 46.95 -2 7 -2 941.83 50.77 -2 7 -2 950.49 49.52 2 7 2 1000.94 47.86 2 7 2 862.50 53.90 2 7 2 1018.84 48.48 2 7 2 924.04 53.58 2 7 2 1102.40 88.88 2 7 3 3910.82 194.16 2 7 3 4502.78 155.66 2 7 3 4528.36 158.35 -2 7 -3 4338.77 155.33 2 7 3 4238.55 152.67 -2 7 -3 4093.03 155.36 2 7 3 4317.79 154.29 -2 7 -3 3984.31 153.59 2 7 3 4237.65 158.99 2 7 3 4179.89 151.70 2 7 4 705.15 39.25 2 7 4 710.09 43.99 -2 7 -4 716.30 43.70 -2 7 -4 759.53 44.37 2 7 4 688.53 37.97 2 7 4 530.51 72.12 -2 7 -4 798.24 45.27 2 7 4 674.34 46.46 2 7 4 716.11 40.33 2 7 4 677.63 49.90 2 7 4 654.78 45.67 2 7 5 1557.21 70.04 -2 7 -5 1511.27 69.20 -2 7 -5 1546.22 69.34 2 7 5 1541.76 75.11 2 7 5 1573.74 72.06 2 7 5 1544.70 73.78 2 7 5 1628.31 65.82 2 7 5 1474.31 65.01 -2 7 -5 1500.85 65.00 2 7 6 73.66 31.38 2 7 6 44.79 35.97 -2 7 -6 48.84 25.29 2 7 6 88.28 35.35 -2 7 -6 34.31 43.48 2 7 6 97.77 24.13 2 7 6 112.18 24.20 -2 7 -6 66.33 29.13 -2 7 -6 90.67 29.45 -2 7 -6 55.06 27.71 2 7 6 83.86 32.89 2 7 6 92.60 38.86 -2 7 -7 4103.85 147.59 2 7 7 4140.41 151.44 -2 7 -7 4067.64 147.46 2 7 7 4168.31 154.90 2 7 7 3951.16 153.35 -2 7 -7 4152.43 150.09 2 7 7 3983.07 147.15 -2 7 -7 4270.61 150.72 2 7 7 3897.84 150.90 2 7 7 4067.06 145.12 2 7 7 3663.15 154.33 2 7 7 3855.91 149.78 2 7 8 1022.30 51.49 2 7 8 1003.95 60.47 -2 7 -8 1059.50 52.76 2 7 8 994.50 56.60 2 7 8 996.30 61.27 2 7 8 938.39 57.37 -2 7 -8 1066.67 53.21 -2 7 -8 1110.85 55.54 2 7 8 999.78 56.45 -2 7 -8 1066.07 55.18 2 7 9 4546.04 163.94 2 7 9 4565.60 168.08 -2 7 -9 4530.27 165.06 2 7 9 4501.81 167.09 -2 7 -9 4681.80 166.73 -2 7 -9 4276.73 166.13 -2 7 -9 4658.38 164.90 -2 7 -9 4356.18 164.90 2 7 9 4512.21 166.82 2 7 9 4530.46 170.22 2 7 9 4450.22 170.07 2 7 10 179.66 58.77 -2 7 -10 123.36 29.35 2 7 10 116.71 28.55 -2 7 -10 136.71 30.04 2 7 10 146.95 32.17 -2 7 -10 120.07 29.19 -2 7 -10 147.27 32.61 2 7 10 114.99 35.09 2 7 10 111.01 34.92 2 7 10 109.00 39.21 2 7 11 196.52 36.54 2 7 11 244.35 36.94 2 7 11 203.37 30.87 2 7 11 182.22 41.11 2 7 11 237.34 32.87 2 7 11 222.82 40.89 -2 7 -11 237.04 32.78 -2 7 -11 260.56 33.38 -2 7 -11 216.62 29.05 -2 7 -11 204.39 34.78 2 7 12 -3.59 30.58 -2 7 -12 15.68 30.52 -2 7 -12 -21.01 26.76 -2 7 -12 -4.36 31.08 -2 7 -12 51.15 30.01 2 7 12 -5.35 31.79 2 7 12 28.43 27.74 2 7 12 5.67 34.61 2 7 12 -1.08 25.18 2 7 13 758.51 44.86 2 7 13 705.49 49.45 -2 7 -13 818.31 48.57 -2 7 -13 891.71 47.69 2 7 13 884.74 49.50 -2 7 -13 851.97 45.71 -2 7 -13 924.27 48.30 2 7 13 888.15 46.38 2 7 13 710.99 52.93 -2 7 -14 421.53 28.41 -2 7 -14 401.88 35.57 -2 7 -14 421.64 30.65 -2 7 -14 420.29 33.00 2 7 14 364.42 36.88 -2 7 -14 368.00 30.52 -2 7 -14 435.42 36.65 2 7 14 384.83 31.54 2 7 14 383.30 31.72 2 7 14 433.03 37.00 2 7 15 187.98 28.89 -2 7 -15 161.25 20.74 -2 7 -15 129.75 20.04 -2 7 -15 160.36 29.04 -2 7 -15 146.28 27.44 -2 7 -15 151.55 24.99 2 7 15 110.79 22.45 2 7 15 153.82 22.95 2 7 15 120.49 27.42 2 7 16 522.62 33.74 -2 7 -16 541.67 33.46 2 7 16 438.32 30.23 -2 7 -16 552.77 30.53 -2 7 -16 528.64 34.52 2 7 16 522.46 27.76 -2 7 -17 225.82 23.37 -2 7 -17 164.70 17.00 -2 7 -17 212.87 22.96 -2 7 -18 194.11 18.97 -2 7 -18 210.35 19.08 2 8 -17 71.14 11.59 2 8 -17 83.18 15.52 2 8 -17 64.47 14.29 -2 8 17 52.97 17.67 2 8 -16 499.38 28.04 2 8 -16 493.56 25.22 2 8 -16 521.92 29.35 -2 8 16 485.38 31.02 2 8 -16 468.27 25.78 2 8 -15 402.35 25.21 2 8 -15 401.26 25.97 2 8 -15 423.68 29.45 2 8 -15 396.07 26.18 2 8 -15 456.91 30.19 -2 8 15 438.61 32.16 2 8 -14 546.10 35.58 2 8 -14 626.93 36.27 2 8 -14 594.64 34.14 2 8 -14 528.91 28.25 -2 8 14 581.88 39.07 2 8 -14 481.11 32.28 2 8 -14 587.52 32.12 2 8 -13 595.54 38.96 2 8 -13 626.27 37.43 2 8 -13 568.62 32.99 2 8 -13 634.91 39.33 2 8 -13 620.17 37.10 -2 8 13 613.56 43.59 2 8 -13 634.85 34.37 2 8 -12 5315.07 182.84 2 8 -12 4992.12 182.64 2 8 -12 4987.87 179.65 2 8 -12 4884.59 181.66 -2 8 12 5225.75 185.51 2 8 -12 5393.86 182.51 2 8 -11 484.77 38.04 2 8 -11 570.98 40.14 2 8 -11 513.92 40.19 2 8 -11 506.51 34.66 2 8 -11 488.85 30.20 -2 8 11 488.07 43.98 2 8 -11 545.58 39.11 2 8 -11 505.64 35.04 2 8 -10 479.17 37.42 2 8 -10 471.15 39.72 2 8 -10 410.81 34.10 2 8 -10 420.94 35.57 2 8 -10 408.02 30.73 -2 8 10 385.43 41.56 2 8 -10 460.31 35.40 2 8 -10 525.17 40.56 2 8 -9 99.56 30.60 2 8 -9 110.86 52.65 2 8 -9 103.32 31.87 2 8 -9 161.50 30.06 2 8 -9 109.12 28.66 2 8 -9 123.19 29.31 2 8 -9 113.53 24.51 2 8 -9 168.91 31.78 -2 8 9 136.16 36.05 2 8 -9 127.13 28.64 2 8 -8 624.36 41.27 2 8 -8 655.53 41.93 2 8 -8 651.23 77.31 2 8 -8 616.78 43.70 2 8 -8 568.13 37.92 2 8 -8 653.02 45.61 2 8 -8 604.02 41.56 2 8 -8 632.61 43.27 2 8 -8 568.77 39.37 -2 8 8 604.41 46.69 2 8 -7 284.40 29.53 -2 8 7 279.42 38.02 2 8 -7 324.46 68.14 2 8 -7 357.69 37.16 2 8 -7 304.83 32.42 2 8 -7 341.31 34.72 2 8 -7 368.06 35.93 2 8 -7 293.53 31.12 2 8 -7 291.11 31.14 2 8 -7 291.36 38.06 2 8 -6 444.21 35.66 2 8 -6 409.78 58.60 2 8 -6 428.67 41.91 2 8 -6 448.69 38.03 -2 8 6 423.05 41.39 2 8 -6 392.46 33.73 2 8 -6 501.22 39.79 2 8 -6 413.91 36.57 2 8 -6 442.55 38.52 2 8 -5 641.27 40.60 2 8 -5 519.40 63.71 2 8 -5 608.16 42.48 2 8 -5 681.62 44.54 2 8 -5 659.47 47.57 2 8 -5 688.75 45.06 2 8 -5 681.24 43.58 -2 8 5 652.05 38.50 -2 8 5 572.81 42.36 -2 8 5 503.59 45.79 2 8 -5 714.46 41.03 -2 8 4 77.75 24.74 2 8 -4 83.31 34.46 2 8 -4 92.70 44.95 -2 8 4 46.10 32.98 2 8 -4 76.59 28.95 2 8 -4 129.42 28.44 2 8 -4 98.13 32.29 2 8 -4 68.65 29.88 -2 8 4 95.50 31.95 2 8 -4 83.15 31.25 2 8 -4 101.54 29.28 2 8 -3 1239.61 91.98 2 8 -3 1320.77 64.19 2 8 -3 1229.03 60.96 2 8 -3 1183.71 58.10 2 8 -3 1176.93 58.97 -2 8 3 1162.06 61.25 2 8 -3 1373.66 60.40 -2 8 3 1111.75 57.14 -2 8 3 1207.10 62.11 2 8 -3 1448.21 66.41 2 8 -2 2629.06 104.94 2 8 -2 2477.04 96.45 -2 8 2 2378.89 100.30 2 8 -2 2502.97 136.46 2 8 -2 2468.37 100.59 -2 8 2 2426.17 95.93 2 8 -2 2527.36 98.09 2 8 -2 2495.85 99.85 -2 8 2 2584.27 99.30 2 8 -2 2613.21 100.05 2 8 -2 2452.67 99.67 2 8 -2 2578.08 103.04 2 8 -1 1317.14 55.50 2 8 -1 1310.54 65.43 -2 8 1 1144.51 58.09 2 8 -1 1047.43 88.15 2 8 -1 1200.32 62.26 2 8 -1 1159.44 57.25 2 8 -1 1186.40 59.40 -2 8 1 1133.26 55.27 2 8 -1 1044.41 53.90 2 8 -1 1215.97 58.38 -2 8 1 1124.15 58.25 2 8 -1 1174.66 56.91 2 8 0 2174.16 84.81 -2 8 0 2060.33 87.74 2 8 0 2069.84 124.68 2 8 0 2231.78 93.89 2 8 0 2169.15 86.29 2 8 0 2090.79 89.17 -2 8 0 2184.21 87.13 2 8 0 2138.30 87.07 -2 8 0 2192.35 88.72 2 8 0 2304.04 88.74 2 8 0 1952.50 91.32 2 8 1 427.32 64.30 2 8 1 451.49 35.74 -2 8 -1 498.17 34.56 2 8 1 361.86 42.75 -2 8 -1 422.96 36.13 2 8 1 501.98 36.31 2 8 1 455.98 45.70 -2 8 -1 466.59 39.00 2 8 1 515.06 37.96 2 8 1 485.00 41.32 2 8 2 775.43 45.58 2 8 2 848.18 55.18 -2 8 -2 755.28 45.04 -2 8 -2 850.38 49.37 2 8 2 933.66 45.06 2 8 2 804.03 54.07 -2 8 -2 882.18 49.66 2 8 2 879.13 48.32 2 8 2 797.42 78.52 2 8 2 751.20 50.22 2 8 3 360.26 45.22 2 8 3 418.56 36.70 2 8 3 378.89 67.31 -2 8 -3 416.64 35.30 2 8 3 360.18 43.89 -2 8 -3 446.20 38.88 2 8 3 478.93 32.52 2 8 3 400.89 40.70 -2 8 -3 429.73 40.35 2 8 3 438.51 36.12 2 8 4 4598.18 175.38 2 8 4 4856.20 181.04 -2 8 -4 4909.05 175.13 -2 8 -4 4795.74 176.74 2 8 4 4799.56 179.11 2 8 4 5038.70 172.42 -2 8 -4 4765.76 177.87 2 8 4 4983.57 174.46 2 8 5 52.55 28.65 2 8 5 82.48 23.85 2 8 5 55.64 37.55 -2 8 -5 73.11 32.82 -2 8 -5 71.58 29.73 2 8 5 31.48 33.96 2 8 6 1884.90 85.81 -2 8 -6 2272.06 89.17 -2 8 -6 2003.17 82.28 2 8 6 2154.34 90.69 2 8 6 2095.58 81.95 -2 8 -6 2139.18 85.79 2 8 6 1854.43 91.55 2 8 7 549.74 49.35 2 8 7 624.52 43.96 -2 8 -7 711.29 44.46 -2 8 -7 659.53 40.34 -2 8 -7 628.35 44.39 -2 8 -7 682.42 45.71 2 8 7 620.21 37.01 2 8 7 637.84 51.61 2 8 7 707.65 50.79 2 8 8 1582.19 76.42 2 8 8 1588.62 73.00 -2 8 -8 1634.87 68.25 2 8 8 1573.31 72.17 -2 8 -8 1646.66 71.85 -2 8 -8 1464.00 70.50 2 8 8 1520.80 76.74 2 8 8 1485.95 74.36 2 8 9 1728.54 78.14 -2 8 -9 1761.83 74.72 -2 8 -9 1960.49 78.41 -2 8 -9 1666.45 72.73 -2 8 -9 1802.77 77.26 2 8 9 1908.51 78.83 2 8 9 1651.58 82.80 2 8 9 1782.41 82.31 -2 8 -10 408.74 34.06 2 8 10 394.45 36.62 2 8 10 339.10 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6868.58 230.29 3 3 4 23858.0 789.4 3 3 4 23768.8 789.4 3 3 4 24239.0 789.5 3 3 4 23499.0 788.4 3 3 4 23700.0 812.9 -3 3 -4 22285.9 798.1 3 3 4 24103.2 789.5 3 3 4 23767.7 789.1 3 3 5 305.77 24.84 3 3 5 362.82 25.88 3 3 5 332.70 24.19 3 3 5 275.28 46.31 -3 3 -5 321.17 33.63 3 3 5 309.74 24.77 3 3 5 285.65 24.56 3 3 5 330.63 24.70 3 3 6 4433.69 150.93 3 3 6 4454.94 150.99 -3 3 -6 4111.30 163.54 3 3 6 4166.25 149.64 3 3 6 3851.12 174.61 3 3 6 4218.81 151.07 3 3 6 4204.29 150.26 3 3 6 4333.03 151.09 3 3 7 507.57 33.01 3 3 7 503.91 32.47 3 3 7 512.37 31.88 3 3 7 483.80 30.08 -3 3 -7 546.90 43.53 3 3 7 455.51 31.53 3 3 7 458.53 31.00 3 3 8 5405.79 198.46 3 3 8 5885.27 200.18 3 3 8 5858.91 200.73 -3 3 -8 5783.71 199.00 3 3 8 5545.16 199.82 -3 3 -8 5937.88 199.57 -3 3 -8 5549.56 217.80 -3 3 -8 5799.32 199.02 -3 3 -8 5642.20 199.17 -3 3 -8 5658.67 200.11 -3 3 -8 5509.75 199.98 3 3 8 5678.09 200.65 3 3 8 5971.27 200.32 3 3 9 123.21 26.21 3 3 9 205.51 27.28 -3 3 -9 158.88 24.10 3 3 9 138.50 27.00 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4 2 658.29 34.06 3 4 2 621.08 34.90 3 4 2 640.16 35.11 3 4 3 60273.0 1970.7 3 4 3 61180.3 1970.4 3 4 3 59211.1 1970.5 3 4 3 59712.2 1971.1 3 4 3 57090.9 1970.6 3 4 3 60228.9 1971.0 3 4 4 10396.6 349.3 3 4 4 9623.41 376.81 3 4 4 10156.9 348.6 3 4 4 10175.5 348.6 3 4 4 10595.5 348.6 3 4 4 10294.0 349.0 3 4 4 10319.3 349.4 3 4 5 7220.82 251.77 3 4 5 7281.35 251.35 3 4 5 7101.41 281.90 3 4 5 7240.06 251.75 3 4 5 7546.58 252.44 3 4 5 7402.94 252.58 3 4 6 1153.66 50.68 3 4 6 1144.22 51.64 3 4 6 1010.16 50.23 3 4 6 1173.68 51.87 3 4 6 1025.77 77.43 -3 4 -6 1057.52 49.40 3 4 6 1171.56 51.97 -3 4 -6 1076.65 50.06 -3 4 -6 1056.31 49.58 3 4 7 1856.80 71.89 3 4 7 1813.38 71.33 3 4 7 1629.54 70.66 -3 4 -7 1702.15 69.22 -3 4 -7 1721.98 69.68 -3 4 -7 1666.75 70.08 -3 4 -7 1714.86 70.95 -3 4 -7 1523.98 70.04 3 4 7 1782.48 71.96 3 4 7 1802.68 72.12 -3 4 -8 1067.22 50.56 3 4 8 1171.00 54.14 3 4 8 1216.79 54.18 3 4 8 1098.21 53.41 -3 4 -8 1228.02 53.21 -3 4 -8 1086.78 53.17 -3 4 -8 1091.71 53.47 -3 4 -8 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27.45 -3 6 -14 138.41 30.89 -3 6 -14 151.31 33.42 -3 6 -14 225.63 26.35 -3 6 -14 90.08 27.26 -3 6 -15 1838.94 76.23 3 6 15 1810.15 78.58 -3 6 -15 1914.31 81.00 -3 6 -15 1979.11 76.42 -3 6 -15 1975.13 77.69 -3 6 -15 2219.98 83.29 3 6 15 2066.44 79.09 3 6 15 1853.15 80.99 -3 6 -16 451.50 29.82 3 6 16 407.91 32.61 3 6 16 466.91 34.59 -3 6 -16 526.52 35.82 -3 6 -16 449.29 26.77 3 6 16 478.79 32.23 -3 6 -16 445.10 29.73 -3 6 -16 546.34 35.93 3 6 17 67.01 21.19 -3 6 -17 77.93 17.97 3 6 17 66.08 20.42 -3 6 -17 76.08 24.04 -3 6 -17 59.84 22.33 -3 6 -17 91.95 18.99 -3 6 -17 45.43 15.02 3 6 17 90.38 20.90 -3 6 -18 60.30 15.36 -3 6 -18 84.88 13.48 -3 6 -18 108.53 19.92 3 6 18 83.51 16.14 -3 6 -19 117.19 13.00 3 7 -18 101.68 16.62 3 7 -18 72.92 11.89 3 7 -18 94.37 17.16 -3 7 18 94.64 19.72 3 7 -17 893.36 39.57 3 7 -17 818.66 37.48 3 7 -17 847.97 39.45 3 7 -17 921.32 41.49 -3 7 17 916.99 42.52 3 7 -16 862.68 40.07 3 7 -16 760.28 40.08 3 7 -16 682.84 37.28 3 7 -16 744.81 39.15 3 7 -16 801.67 35.25 3 7 -16 717.35 38.73 3 7 -16 747.21 40.66 -3 7 16 823.23 43.34 3 7 -15 1339.48 59.07 3 7 -15 1341.72 58.18 3 7 -15 1382.05 56.60 3 7 -15 1319.60 58.58 3 7 -15 1390.52 61.42 3 7 -15 1386.21 61.02 -3 7 15 1428.18 63.75 3 7 -14 243.86 29.18 3 7 -14 209.45 29.39 -3 7 14 263.46 31.45 3 7 -14 201.35 31.29 3 7 -14 238.48 27.28 -3 7 14 283.44 35.07 3 7 -14 164.97 26.15 3 7 -13 339.30 35.06 3 7 -13 326.66 33.23 -3 7 13 319.14 35.61 3 7 -13 375.70 33.51 3 7 -13 370.79 32.02 3 7 -13 352.12 26.39 3 7 -13 340.80 37.29 3 7 -13 283.54 28.82 -3 7 13 331.42 38.48 3 7 -13 354.52 35.33 3 7 -12 4748.63 177.03 3 7 -12 5062.75 178.76 3 7 -12 4981.11 180.95 3 7 -12 5104.93 178.65 3 7 -12 4865.91 178.93 3 7 -12 5144.92 177.60 3 7 -12 5004.57 174.43 3 7 -12 4832.50 178.79 -3 7 12 4928.84 181.10 -3 7 12 4804.41 178.32 3 7 -11 2019.42 80.42 3 7 -11 2008.70 83.20 -3 7 11 1717.29 79.49 3 7 -11 1926.48 113.09 3 7 -11 1841.78 118.27 3 7 -11 1872.53 80.86 3 7 -11 1835.53 78.40 3 7 -11 1915.17 79.57 3 7 -11 1864.40 76.05 3 7 -11 1687.42 80.13 -3 7 11 1850.59 82.23 3 7 -11 1937.48 81.64 3 7 -10 1864.96 75.90 3 7 -10 1879.54 78.32 3 7 -10 1869.34 81.90 3 7 -10 1910.68 114.23 3 7 -10 1821.18 79.02 3 7 -10 1767.22 75.37 3 7 -10 1966.63 122.87 3 7 -10 1870.21 80.28 3 7 -10 1702.43 71.53 -3 7 10 1831.84 81.30 3 7 -9 726.14 50.03 3 7 -9 654.96 72.91 3 7 -9 689.96 80.76 3 7 -9 663.27 40.89 3 7 -9 689.96 44.51 3 7 -9 707.80 43.09 3 7 -9 713.72 38.82 -3 7 9 736.50 49.15 3 7 -9 671.35 47.48 3 7 -8 1119.23 54.93 3 7 -8 1119.88 58.08 3 7 -8 1107.31 91.38 3 7 -8 1101.90 95.35 3 7 -8 1127.56 61.75 3 7 -8 1175.05 58.02 3 7 -8 1141.11 56.00 -3 7 8 1097.52 59.70 3 7 -8 1120.44 52.73 3 7 -8 1139.10 60.56 3 7 -7 2792.84 147.76 3 7 -7 2654.08 151.86 3 7 -7 2750.33 107.50 3 7 -7 2851.21 112.82 3 7 -7 2741.59 108.06 3 7 -7 2794.43 108.11 -3 7 7 2693.29 109.95 3 7 -7 2772.85 105.85 3 7 -7 2866.29 111.89 3 7 -7 2830.60 109.96 3 7 -6 961.51 49.10 3 7 -6 1034.41 57.49 3 7 -6 893.32 85.45 3 7 -6 923.08 89.90 3 7 -6 937.45 52.57 3 7 -6 866.11 50.01 3 7 -6 943.47 52.08 -3 7 6 847.92 51.92 3 7 -6 971.93 48.76 3 7 -6 968.94 54.90 3 7 -6 900.69 52.51 3 7 -5 423.16 34.39 3 7 -5 420.54 42.10 3 7 -5 340.84 60.17 3 7 -5 410.20 68.44 3 7 -5 457.27 37.17 3 7 -5 395.50 40.71 3 7 -5 405.70 37.52 -3 7 5 392.30 37.42 3 7 -5 399.24 33.61 3 7 -5 417.88 37.47 3 7 -4 22.55 24.95 3 7 -4 93.48 53.57 3 7 -4 23.98 32.42 3 7 -4 68.49 25.96 3 7 -4 14.33 26.67 3 7 -4 37.15 28.11 -3 7 4 49.24 29.11 -3 7 4 43.07 22.91 3 7 -4 75.95 33.35 3 7 -4 56.82 30.54 3 7 -3 1124.80 56.02 3 7 -3 1072.71 61.12 3 7 -3 1088.69 59.09 3 7 -3 1121.87 90.14 3 7 -3 1285.43 57.42 3 7 -3 1231.72 56.88 -3 7 3 1206.14 55.71 -3 7 3 1058.11 56.35 3 7 -3 1204.53 56.29 3 7 -3 1103.72 53.42 3 7 -2 8184.21 316.56 3 7 -2 8338.26 273.71 3 7 -2 7719.25 269.86 3 7 -2 7381.99 267.27 3 7 -2 8065.62 269.70 3 7 -2 7834.83 269.10 -3 7 2 7822.52 269.08 -3 7 2 6972.72 268.49 3 7 -2 8063.20 272.14 3 7 -1 1773.11 75.67 3 7 -1 1919.76 78.76 3 7 -1 1855.98 117.57 -3 7 1 1822.53 76.58 3 7 -1 1856.95 79.52 3 7 -1 1785.14 76.67 -3 7 1 1826.42 78.93 3 7 -1 1790.99 77.62 3 7 -1 2051.85 84.17 3 7 -1 2176.23 83.43 3 7 0 2137.32 82.96 3 7 0 2176.38 127.48 -3 7 0 2047.12 83.62 3 7 0 1956.57 88.41 3 7 0 2044.19 84.36 3 7 0 2016.23 87.48 3 7 0 2057.33 81.77 3 7 0 2006.65 85.34 -3 7 0 2035.05 85.10 3 7 0 2067.99 84.44 3 7 1 100.20 35.99 3 7 1 69.18 54.62 3 7 1 102.05 29.03 -3 7 -1 105.07 29.20 -3 7 -1 117.49 27.00 -3 7 -1 107.60 24.91 3 7 1 101.88 27.26 3 7 1 129.57 24.14 3 7 1 137.93 34.15 3 7 1 97.18 25.28 3 7 1 93.79 34.55 3 7 1 81.44 26.08 3 7 2 132.31 34.77 3 7 2 152.85 30.61 3 7 2 125.30 25.73 3 7 2 106.42 35.20 -3 7 -2 156.36 29.20 -3 7 -2 132.29 25.90 3 7 2 129.83 26.58 3 7 2 174.51 61.50 -3 7 -2 144.27 31.76 3 7 2 150.78 38.68 3 7 2 142.41 28.98 3 7 3 2258.00 91.16 3 7 3 2334.25 94.97 3 7 3 2419.36 99.02 -3 7 -3 2342.43 92.13 -3 7 -3 2300.30 93.93 3 7 3 2272.25 90.57 3 7 3 2183.98 132.59 -3 7 -3 2238.84 94.64 3 7 3 2327.14 92.30 3 7 3 2500.09 98.15 3 7 4 840.74 46.37 3 7 4 848.95 54.78 3 7 4 947.00 56.24 3 7 4 781.75 85.17 -3 7 -4 950.04 50.41 3 7 4 875.46 52.03 -3 7 -4 933.36 51.82 3 7 4 863.64 44.94 -3 7 -4 880.80 50.60 3 7 4 936.00 48.47 3 7 5 852.65 47.20 3 7 5 822.77 52.84 3 7 5 807.74 84.41 -3 7 -5 879.47 49.06 3 7 5 933.49 51.63 -3 7 -5 854.44 51.39 3 7 5 894.11 44.19 3 7 5 811.11 45.62 3 7 5 904.53 56.96 3 7 6 1336.30 67.33 3 7 6 1251.29 65.53 -3 7 -6 1352.71 62.88 -3 7 -6 1269.98 63.88 3 7 6 1222.03 60.40 3 7 6 1267.34 58.18 3 7 6 1408.00 69.12 3 7 7 4809.09 171.71 3 7 7 4446.80 168.93 3 7 7 4762.30 175.85 -3 7 -7 4710.69 169.41 -3 7 -7 5081.25 173.66 -3 7 -7 5046.84 173.97 -3 7 -7 4565.73 169.67 3 7 7 4700.23 175.15 -3 7 -7 4803.62 173.86 3 7 7 4630.92 176.87 3 7 7 4706.29 168.24 3 7 7 4621.02 176.53 3 7 8 3559.30 136.38 3 7 8 3462.25 132.17 3 7 8 3411.00 130.16 3 7 8 3411.51 135.96 -3 7 -8 3601.49 130.62 -3 7 -8 3765.67 134.38 -3 7 -8 3507.54 131.64 -3 7 -8 3574.12 133.30 3 7 8 3377.56 131.81 3 7 8 3647.53 128.08 3 7 8 3466.14 137.53 3 7 8 3290.02 137.61 -3 7 -9 1437.44 64.89 3 7 9 1538.91 68.19 3 7 9 1474.18 65.33 3 7 9 1462.26 72.14 -3 7 -9 1665.70 70.66 -3 7 -9 1403.97 67.01 -3 7 -9 1511.30 69.94 3 7 9 1492.62 67.42 3 7 9 1473.84 74.45 3 7 10 1694.14 77.24 3 7 10 1636.10 72.61 3 7 10 1576.55 69.75 3 7 10 1671.89 113.36 -3 7 -10 1683.52 71.72 -3 7 -10 1812.63 75.46 -3 7 -10 1638.76 74.52 -3 7 -10 1704.27 72.28 3 7 10 1686.57 71.32 3 7 10 1571.92 72.16 3 7 10 1544.02 77.83 -3 7 -11 544.63 39.74 3 7 11 550.73 45.96 3 7 11 555.46 40.31 3 7 11 563.57 37.26 3 7 11 492.69 45.32 -3 7 -11 568.41 40.16 -3 7 -11 626.99 42.40 3 7 11 578.36 36.72 3 7 11 611.90 41.36 3 7 12 -5.11 28.76 3 7 12 42.68 23.41 -3 7 -12 -3.17 28.05 -3 7 -12 31.13 26.43 3 7 12 21.20 28.19 3 7 12 34.53 26.03 -3 7 -12 12.58 30.14 -3 7 -12 18.19 25.63 3 7 13 84.82 32.48 3 7 13 74.76 30.35 3 7 13 116.27 26.75 3 7 13 73.02 23.28 -3 7 -13 156.70 27.23 -3 7 -13 147.89 28.44 -3 7 -13 114.78 25.99 -3 7 -13 134.52 29.46 -3 7 -13 110.46 28.39 3 7 13 109.17 26.03 3 7 14 137.67 25.27 3 7 14 119.04 22.64 3 7 14 163.29 29.22 -3 7 -14 178.54 26.35 -3 7 -14 195.17 24.02 -3 7 -14 188.52 27.62 -3 7 -14 183.60 27.40 3 7 15 178.53 26.71 -3 7 -15 257.46 24.93 -3 7 -15 273.99 22.13 -3 7 -15 241.29 26.16 -3 7 -15 295.93 27.72 3 7 15 218.09 25.10 -3 7 -16 163.15 21.31 -3 7 -16 153.33 19.41 -3 7 -16 202.96 23.27 -3 7 -16 123.07 18.17 -3 7 -17 230.71 20.18 -3 7 -17 174.93 14.96 3 8 -17 354.39 17.72 -3 8 17 354.04 21.58 3 8 -16 451.20 22.73 3 8 -16 436.83 23.18 3 8 -16 414.06 21.12 3 8 -16 447.73 25.69 -3 8 16 398.63 26.89 3 8 -15 150.94 18.35 3 8 -15 104.48 20.54 3 8 -15 82.20 18.65 3 8 -15 69.08 18.75 3 8 -15 95.25 20.81 3 8 -15 104.41 17.64 -3 8 15 118.89 23.63 3 8 -14 219.51 21.83 3 8 -14 158.60 24.55 3 8 -14 171.40 23.51 3 8 -14 183.60 23.75 3 8 -14 172.56 25.27 3 8 -14 168.22 21.91 -3 8 14 153.48 26.82 3 8 -13 584.99 35.43 3 8 -13 505.28 33.84 3 8 -13 517.93 29.11 3 8 -13 540.46 35.14 3 8 -13 545.57 35.25 -3 8 13 520.89 37.60 3 8 -13 506.82 31.73 3 8 -13 524.26 34.09 3 8 -12 158.92 28.73 3 8 -12 187.01 28.48 3 8 -12 220.17 29.46 3 8 -12 224.49 29.65 3 8 -12 177.22 23.14 3 8 -12 182.24 28.00 3 8 -12 165.80 24.99 -3 8 12 190.64 32.42 3 8 -11 191.45 24.02 3 8 -11 187.54 27.14 3 8 -11 203.52 29.00 3 8 -11 234.30 31.37 3 8 -11 217.42 31.02 3 8 -11 197.14 26.02 -3 8 11 211.46 33.37 3 8 -10 1782.81 76.74 3 8 -10 1850.95 76.39 3 8 -10 1873.55 79.36 3 8 -10 1825.99 74.60 3 8 -10 1869.16 74.73 3 8 -10 1774.17 75.77 3 8 -10 1765.66 70.97 -3 8 10 1842.14 79.64 3 8 -9 54.85 25.36 3 8 -9 64.82 28.38 3 8 -9 40.16 31.06 3 8 -9 39.21 27.09 3 8 -9 33.77 26.32 3 8 -9 71.68 29.94 -3 8 9 30.39 30.83 3 8 -9 61.86 22.65 3 8 -9 32.03 28.72 3 8 -8 902.05 47.31 3 8 -8 839.55 52.28 3 8 -8 860.46 49.22 3 8 -8 867.79 49.62 3 8 -8 854.51 47.45 3 8 -8 756.20 45.19 3 8 -8 852.93 43.56 -3 8 8 828.62 50.31 3 8 -8 763.28 48.94 3 8 -8 871.08 47.58 3 8 -7 541.18 44.91 3 8 -7 517.07 64.80 3 8 -7 595.73 42.64 3 8 -7 674.97 41.54 3 8 -7 625.05 41.79 3 8 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312.97 60.16 4 6 -5 405.89 63.63 4 6 -5 370.65 38.56 4 6 -5 354.16 31.93 4 6 -5 345.58 31.04 4 6 -5 308.16 38.40 4 6 -4 1829.50 80.82 4 6 -4 2043.07 82.59 4 6 -4 1851.50 118.47 4 6 -4 1841.12 77.29 4 6 -4 1853.46 82.62 4 6 -4 1955.35 82.87 4 6 -3 238.48 33.12 4 6 -3 226.70 33.72 4 6 -3 274.71 60.29 4 6 -3 240.25 30.43 -4 6 3 222.55 26.68 4 6 -3 264.93 29.24 4 6 -3 281.67 35.66 4 6 -2 118.86 31.87 4 6 -2 115.57 31.03 4 6 -2 95.41 52.78 -4 6 2 135.30 26.23 4 6 -2 121.91 32.23 4 6 -2 117.15 25.54 4 6 -1 126.03 29.03 4 6 -1 218.11 32.10 4 6 -1 138.70 32.84 4 6 -1 146.78 58.62 -4 6 1 139.56 25.97 -4 6 1 182.96 27.34 4 6 -1 140.76 32.76 4 6 0 6795.71 234.09 4 6 0 6784.90 232.35 4 6 0 6898.10 235.43 4 6 0 6527.20 274.96 -4 6 0 6111.32 229.75 4 6 0 6974.85 236.22 -4 6 0 6591.02 232.08 -4 6 0 6409.64 233.53 4 6 0 7073.21 235.53 4 6 0 6489.10 232.52 4 6 0 6778.74 235.81 4 6 1 2391.19 95.99 4 6 1 2446.01 94.50 4 6 1 2457.14 97.94 -4 6 -1 2317.05 93.34 -4 6 -1 2400.51 95.02 4 6 1 2375.62 97.54 -4 6 -1 2435.21 97.07 4 6 1 2472.31 95.47 4 6 1 2444.38 98.56 4 6 1 2418.12 98.07 4 6 2 1634.95 71.11 4 6 2 1592.79 69.34 4 6 2 1626.90 72.21 -4 6 -2 1595.15 69.93 -4 6 -2 1620.01 71.02 -4 6 -2 1659.32 72.30 4 6 2 1599.37 72.51 4 6 2 1646.82 69.91 4 6 2 1651.77 74.06 4 6 3 2056.21 85.21 4 6 3 1996.56 83.36 4 6 3 2000.02 82.27 4 6 3 2095.97 85.66 -4 6 -3 1954.29 82.57 -4 6 -3 1993.33 84.29 -4 6 -3 1956.09 84.47 4 6 3 2053.91 83.42 4 6 3 2142.57 87.63 4 6 4 12254.3 416.9 4 6 4 12145.6 415.8 4 6 4 12179.6 414.3 4 6 4 12388.8 416.4 -4 6 -4 11827.0 414.7 -4 6 -4 12600.8 416.4 -4 6 -4 11746.1 416.4 4 6 4 12314.0 414.8 4 6 4 12097.5 417.5 4 6 5 1769.06 81.42 4 6 5 1821.75 79.40 4 6 5 1872.87 78.75 4 6 5 1826.03 80.70 4 6 5 1647.60 113.56 4 6 5 1887.93 82.70 -4 6 -5 1968.72 79.83 -4 6 -5 1963.41 80.93 -4 6 -5 1880.47 76.74 -4 6 -5 1714.62 79.55 4 6 5 1851.58 77.25 4 6 6 11111.8 376.1 4 6 6 11074.6 374.3 4 6 6 10970.1 373.1 4 6 6 10702.7 374.0 -4 6 -6 10842.3 373.7 -4 6 -6 10883.4 374.9 -4 6 -6 10522.8 371.6 4 6 6 10725.0 376.2 4 6 6 10899.4 371.5 4 6 6 11169.9 376.0 4 6 7 492.72 45.20 4 6 7 496.92 41.50 4 6 7 523.04 45.27 4 6 7 541.93 41.70 4 6 7 485.01 40.62 -4 6 -7 505.70 41.85 -4 6 -7 541.58 43.06 -4 6 -7 499.52 37.40 -4 6 -7 454.39 41.51 4 6 7 529.32 35.65 4 6 7 485.01 44.39 4 6 8 866.45 51.42 4 6 8 799.74 48.30 4 6 8 790.45 48.41 -4 6 -8 890.62 45.76 -4 6 -8 835.63 51.08 -4 6 -8 810.36 49.56 4 6 8 845.99 53.25 4 6 8 842.94 54.48 4 6 8 841.49 44.02 4 6 8 784.18 44.21 4 6 8 707.91 51.21 4 6 9 1380.42 63.58 4 6 9 1599.62 68.88 4 6 9 1536.61 69.51 -4 6 -9 1536.29 66.45 -4 6 -9 1432.85 70.25 -4 6 -9 1303.96 70.09 -4 6 -9 1575.52 70.20 4 6 9 1470.29 62.31 4 6 9 1365.00 70.19 4 6 9 1644.48 74.06 4 6 10 392.33 40.78 4 6 10 401.54 38.89 -4 6 -10 391.83 34.44 -4 6 -10 380.99 39.37 4 6 10 425.58 33.72 -4 6 -10 422.11 39.11 -4 6 -10 389.90 39.14 4 6 10 386.03 40.00 4 6 10 439.71 43.11 4 6 11 623.31 46.58 4 6 11 679.35 45.05 4 6 11 763.09 86.68 -4 6 -11 637.01 42.39 -4 6 -11 693.51 47.36 -4 6 -11 665.36 45.37 -4 6 -11 732.42 46.13 4 6 11 709.66 40.52 4 6 11 680.55 46.15 4 6 11 608.85 47.93 4 6 12 387.53 37.27 4 6 12 364.95 37.07 -4 6 -12 390.57 35.38 -4 6 -12 421.86 36.78 -4 6 -12 360.34 35.71 -4 6 -12 445.68 39.32 4 6 12 426.17 32.54 4 6 12 429.92 40.02 4 6 13 49.46 29.61 4 6 13 39.67 26.39 -4 6 -13 82.51 27.70 -4 6 -13 21.03 27.31 4 6 13 19.05 29.16 -4 6 -13 50.00 31.49 -4 6 -13 26.01 26.97 4 6 13 75.67 23.19 4 6 13 65.71 28.16 4 6 14 339.08 35.75 4 6 14 407.07 34.21 -4 6 -14 412.84 33.65 -4 6 -14 479.07 33.59 4 6 14 386.15 34.74 -4 6 -14 422.47 34.00 -4 6 -14 450.10 36.25 4 6 14 346.41 27.71 4 6 15 269.81 28.66 -4 6 -15 346.46 28.62 4 6 15 184.95 28.76 4 6 15 236.41 27.89 -4 6 -15 310.87 29.14 -4 6 -15 301.86 26.14 -4 6 -15 280.51 26.12 -4 6 -15 343.30 30.18 -4 6 -16 137.67 20.11 4 6 16 104.55 21.90 4 6 16 138.88 21.63 -4 6 -16 113.64 17.49 -4 6 -16 146.29 25.24 -4 6 -17 115.54 15.10 -4 6 -17 98.44 16.65 -4 6 -17 96.61 20.40 -4 6 -18 1976.79 69.53 -4 6 -18 1941.69 71.26 4 7 -18 698.18 29.84 4 7 -18 677.30 29.29 -4 7 18 706.72 30.46 4 7 -17 437.20 22.02 4 7 -17 582.71 28.03 4 7 -17 495.74 27.29 4 7 -17 614.89 29.45 -4 7 17 528.79 28.98 4 7 -16 58.61 19.54 4 7 -16 22.94 18.07 4 7 -16 45.60 14.90 4 7 -16 30.58 19.02 4 7 -16 26.35 21.68 4 7 -16 53.41 13.19 -4 7 16 34.51 20.71 4 7 -16 14.70 16.86 4 7 -15 84.56 21.23 4 7 -15 96.02 23.33 4 7 -15 111.16 23.53 4 7 -15 119.83 20.22 4 7 -15 98.73 22.19 4 7 -15 109.42 24.92 4 7 -15 102.83 19.09 -4 7 15 88.05 25.35 4 7 -15 90.75 19.69 4 7 -14 -2.07 23.82 4 7 -14 45.14 20.97 4 7 -14 19.34 26.92 4 7 -14 28.76 20.80 -4 7 14 -2.85 25.14 4 7 -14 -6.93 20.62 4 7 -14 1.91 23.16 4 7 -13 13.94 19.66 4 7 -13 53.84 27.23 4 7 -13 31.72 23.43 4 7 -13 19.61 23.13 4 7 -13 -21.16 29.07 4 7 -13 38.65 16.46 4 7 -13 25.06 22.23 -4 7 13 4.16 27.36 4 7 -13 64.45 26.65 4 7 -12 669.94 40.67 4 7 -12 800.67 44.78 4 7 -12 763.98 43.18 4 7 -12 781.44 43.38 4 7 -12 744.37 37.73 4 7 -12 788.67 46.60 4 7 -12 773.29 46.15 -4 7 12 682.41 45.73 4 7 -12 749.21 46.03 4 7 -12 716.70 43.55 4 7 -11 299.47 30.67 4 7 -11 306.43 36.01 4 7 -11 238.18 35.91 4 7 -11 326.24 34.43 4 7 -11 395.45 33.72 4 7 -11 318.35 27.99 -4 7 11 335.08 34.82 4 7 -11 275.13 32.56 4 7 -10 174.80 28.25 4 7 -10 132.24 32.06 4 7 -10 181.51 35.86 4 7 -10 130.30 51.24 4 7 -10 99.13 49.94 4 7 -10 198.22 31.26 4 7 -10 171.99 27.22 4 7 -10 185.84 33.19 -4 7 10 141.19 31.23 4 7 -10 183.62 21.16 4 7 -10 188.97 33.90 4 7 -9 209.19 33.44 4 7 -9 155.84 28.32 4 7 -9 188.94 36.65 4 7 -9 273.58 56.13 4 7 -9 127.01 52.86 4 7 -9 191.25 31.24 4 7 -9 198.87 27.59 -4 7 9 156.94 30.96 4 7 -9 173.47 23.63 4 7 -9 188.55 35.19 4 7 -8 262.23 37.41 4 7 -8 355.66 63.15 4 7 -8 260.43 58.43 4 7 -8 197.79 32.79 4 7 -8 295.38 31.44 4 7 -8 206.35 29.38 -4 7 8 230.21 33.09 4 7 -8 232.10 26.71 4 7 -8 322.38 35.69 4 7 -7 1143.83 57.56 4 7 -7 1061.56 90.16 4 7 -7 1318.31 98.42 4 7 -7 992.44 58.59 4 7 -7 1217.95 57.24 4 7 -7 1217.83 59.26 -4 7 7 1112.15 56.89 4 7 -7 1077.37 53.58 4 7 -7 1181.48 62.56 4 7 -7 1202.40 60.76 4 7 -6 1315.54 66.79 4 7 -6 1257.45 99.19 4 7 -6 1443.45 65.28 4 7 -6 1318.24 63.88 4 7 -6 1463.81 64.91 -4 7 6 1388.66 63.39 4 7 -6 1361.75 61.47 4 7 -6 1343.92 68.55 4 7 -5 1656.05 74.13 4 7 -5 1725.68 114.78 4 7 -5 1702.62 77.93 4 7 -5 1755.36 73.55 -4 7 5 1581.23 71.57 4 7 -5 1676.63 71.62 4 7 -5 1689.10 78.85 4 7 -4 1096.92 57.91 4 7 -4 1095.90 60.26 4 7 -4 1076.88 90.80 4 7 -4 1193.74 60.52 4 7 -4 1182.54 57.28 -4 7 4 1030.20 52.49 4 7 -4 1065.89 53.57 4 7 -4 1086.36 61.49 4 7 -3 567.53 43.13 4 7 -3 447.61 39.06 4 7 -3 543.54 45.89 4 7 -3 634.12 73.86 4 7 -3 675.40 41.43 -4 7 3 551.17 38.58 4 7 -3 687.52 41.27 4 7 -3 565.03 48.49 4 7 -3 529.51 45.36 4 7 -2 493.65 39.46 4 7 -2 410.65 35.79 4 7 -2 492.37 42.85 4 7 -2 413.51 66.96 4 7 -2 560.87 38.80 -4 7 2 422.55 37.86 4 7 -2 566.23 44.52 4 7 -2 494.42 44.79 4 7 -1 191.87 33.00 -4 7 1 204.23 32.07 4 7 -1 186.92 36.98 4 7 -1 175.83 35.30 4 7 -1 215.09 31.07 4 7 -1 177.88 57.49 -4 7 1 172.68 28.45 4 7 -1 204.58 31.49 4 7 0 17038.1 569.7 4 7 0 17288.8 567.9 4 7 0 16794.1 570.8 4 7 0 15830.4 613.6 -4 7 0 16340.2 567.2 4 7 0 16803.9 567.7 -4 7 0 17035.0 569.3 4 7 0 16956.9 567.9 4 7 0 16504.7 570.8 4 7 1 289.36 38.29 4 7 1 310.12 39.72 4 7 1 295.99 30.34 4 7 1 291.35 34.38 4 7 1 312.48 39.13 4 7 1 272.21 62.56 -4 7 -1 304.37 29.97 4 7 1 334.07 33.50 -4 7 -1 254.35 32.28 -4 7 -1 306.62 35.63 4 7 1 311.39 33.25 4 7 2 467.94 38.65 4 7 2 470.65 34.84 4 7 2 528.86 42.76 4 7 2 322.04 62.35 4 7 2 535.32 42.36 -4 7 -2 517.40 37.13 -4 7 -2 489.20 40.45 4 7 2 454.79 37.24 -4 7 -2 421.19 39.38 4 7 2 472.02 36.66 4 7 2 493.68 44.71 4 7 2 533.24 45.19 4 7 3 9503.48 329.35 4 7 3 9238.17 326.56 4 7 3 9717.45 331.93 4 7 3 8980.01 376.10 4 7 3 10144.1 333.4 -4 7 -3 9586.00 328.74 -4 7 -3 9476.55 330.63 4 7 3 9500.86 327.95 -4 7 -3 8976.79 330.98 4 7 3 9541.92 329.03 4 7 3 9768.20 332.79 4 7 3 9897.51 331.92 4 7 4 5128.54 183.51 4 7 4 4932.95 180.05 4 7 4 4914.55 178.15 4 7 4 5105.51 182.91 -4 7 -4 5205.23 181.05 -4 7 -4 4968.30 182.54 4 7 4 5023.81 178.15 -4 7 -4 4650.22 182.34 4 7 4 4930.56 178.99 4 7 4 5129.10 184.35 4 7 4 4899.48 184.15 4 7 5 387.56 37.89 4 7 5 446.04 41.33 4 7 5 478.06 34.06 4 7 5 424.37 40.91 -4 7 -5 502.05 41.46 -4 7 -5 384.23 40.87 4 7 5 471.69 33.82 -4 7 -5 437.54 41.79 4 7 5 430.08 34.98 4 7 5 488.94 44.28 4 7 6 1153.58 63.10 4 7 6 1176.88 59.29 4 7 6 1123.05 56.85 4 7 6 1149.33 60.99 -4 7 -6 1289.02 61.82 -4 7 -6 1281.71 61.54 4 7 6 1289.64 54.48 4 7 6 1156.21 55.26 4 7 6 1139.50 63.96 4 7 7 1816.41 81.49 4 7 7 1818.89 78.08 4 7 7 1807.51 75.71 4 7 7 1742.58 78.85 -4 7 -7 1762.86 79.30 -4 7 -7 2045.21 80.49 -4 7 -7 1683.84 74.00 4 7 7 1577.53 80.97 4 7 7 1874.61 73.51 4 7 8 93.96 26.82 4 7 8 141.69 35.19 4 7 8 88.84 30.16 4 7 8 80.11 22.35 4 7 8 77.97 30.85 -4 7 -8 125.08 27.82 -4 7 -8 89.10 34.53 -4 7 -8 88.21 32.63 4 7 8 64.92 33.26 4 7 9 1487.99 72.41 4 7 9 1426.71 69.26 4 7 9 1488.63 66.78 -4 7 -9 1515.18 64.42 -4 7 -9 1733.14 71.80 -4 7 -9 1491.12 66.08 4 7 9 1455.41 71.78 4 7 9 1485.22 73.34 4 7 10 192.09 35.75 4 7 10 199.65 28.97 -4 7 -10 203.22 26.75 4 7 10 199.98 34.34 -4 7 -10 198.29 29.75 -4 7 -10 188.89 33.21 -4 7 -10 175.63 31.52 4 7 10 213.75 32.26 4 7 10 179.71 33.04 4 7 11 156.76 34.13 4 7 11 158.92 32.85 4 7 11 180.27 30.08 4 7 11 154.29 26.44 -4 7 -11 237.40 33.27 -4 7 -11 194.37 25.13 -4 7 -11 148.16 29.94 4 7 12 780.52 48.34 4 7 12 840.16 44.12 -4 7 -12 836.41 43.32 -4 7 -12 893.38 46.84 4 7 12 874.60 46.52 4 7 12 817.45 48.48 -4 7 -13 92.27 22.14 4 7 13 103.80 25.90 4 7 13 114.50 24.27 4 7 13 82.80 21.04 -4 7 -13 131.09 24.67 -4 7 -13 123.43 25.18 -4 7 -13 103.99 26.61 4 7 14 99.23 21.57 4 7 14 117.65 19.85 -4 7 -14 171.58 22.08 -4 7 -14 160.44 21.78 -4 7 -14 168.33 24.21 -4 7 -14 142.80 23.02 -4 7 -15 1330.55 49.21 4 7 15 1030.38 49.03 -4 7 -15 1100.61 46.64 -4 7 -15 1234.75 48.42 -4 7 -15 1222.74 49.80 -4 7 -16 170.58 18.27 -4 7 -16 189.75 16.07 4 8 -16 439.25 21.77 -4 8 16 456.94 23.32 4 8 -15 356.19 20.79 4 8 -15 372.51 20.55 4 8 -15 377.20 22.11 4 8 -15 391.41 24.08 -4 8 15 368.98 24.01 4 8 -14 463.30 27.92 4 8 -14 429.49 27.81 4 8 -14 445.88 26.45 4 8 -14 457.68 25.73 4 8 -14 447.71 28.38 -4 8 14 431.45 29.07 4 8 -14 403.00 25.99 4 8 -13 498.16 31.80 4 8 -13 486.05 31.66 4 8 -13 471.38 30.09 4 8 -13 493.97 29.57 4 8 -13 430.25 23.77 4 8 -13 501.32 31.80 -4 8 13 463.48 31.89 4 8 -13 473.59 29.68 4 8 -12 2002.95 76.81 4 8 -12 1990.23 78.50 4 8 -12 1915.15 75.90 4 8 -12 1872.63 74.67 4 8 -12 1937.83 72.26 4 8 -12 1937.49 75.82 4 8 -12 1881.59 74.56 -4 8 12 1852.97 76.57 4 8 -12 1928.31 76.53 4 8 -11 4364.90 154.80 4 8 -11 4331.02 156.90 4 8 -11 4325.42 154.54 4 8 -11 4354.76 154.31 4 8 -11 4501.98 152.16 4 8 -11 4300.70 154.19 -4 8 11 4135.24 154.39 4 8 -11 4172.15 155.16 4 8 -11 4271.36 153.84 4 8 -10 235.46 29.76 4 8 -10 186.02 31.28 4 8 -10 197.41 29.85 4 8 -10 212.32 28.97 4 8 -10 224.51 26.39 -4 8 10 179.45 29.23 4 8 -10 187.12 20.61 4 8 -10 170.98 28.18 4 8 -10 234.70 27.64 4 8 -9 695.81 43.23 4 8 -9 588.49 40.68 4 8 -9 657.66 43.46 4 8 -9 699.17 39.18 4 8 -9 562.65 38.92 4 8 -9 640.82 36.80 4 8 -9 677.33 34.83 -4 8 9 622.94 40.54 4 8 -9 705.23 42.40 4 8 -9 645.92 40.25 4 8 -8 1578.49 71.59 4 8 -8 1473.89 65.10 4 8 -8 1607.26 68.32 4 8 -8 1543.87 67.02 -4 8 8 1488.16 67.15 4 8 -8 1531.11 63.75 4 8 -8 1641.05 71.33 4 8 -8 1497.32 67.59 4 8 -7 1644.06 72.79 4 8 -7 1895.45 76.63 4 8 -7 1761.33 74.68 4 8 -7 1845.04 76.45 -4 8 7 1655.01 74.55 4 8 -7 1786.65 72.68 4 8 -7 1820.29 78.75 4 8 -6 500.72 36.10 4 8 -6 493.69 42.84 4 8 -6 505.52 40.42 4 8 -6 505.62 39.42 -4 8 6 502.07 36.66 4 8 -6 504.14 36.76 4 8 -6 492.49 40.37 4 8 -5 1653.29 74.58 4 8 -5 1560.97 67.21 4 8 -5 1432.81 102.05 4 8 -5 1545.42 72.10 4 8 -5 1622.84 69.46 4 8 -5 1686.37 71.93 4 8 -5 1631.71 69.39 4 8 -5 1637.10 73.52 4 8 -4 66.48 30.16 4 8 -4 79.94 24.16 4 8 -4 86.87 46.91 4 8 -4 67.90 30.02 4 8 -4 80.45 26.87 4 8 -4 79.86 30.90 4 8 -4 89.70 30.02 -4 8 4 38.74 22.97 4 8 -4 82.40 28.72 4 8 -4 49.93 34.29 4 8 -3 12.93 27.04 4 8 -3 4.99 22.47 4 8 -3 45.47 30.61 4 8 -3 28.22 27.23 4 8 -3 20.59 32.25 4 8 -3 46.54 47.41 4 8 -3 15.94 30.10 4 8 -3 6.71 29.48 4 8 -3 23.45 28.01 -4 8 3 27.14 23.15 4 8 -3 -10.82 33.87 4 8 -2 163.98 30.41 4 8 -2 154.77 26.12 4 8 -2 174.96 33.67 4 8 -2 164.08 36.13 4 8 -2 156.42 35.19 4 8 -2 187.61 54.62 -4 8 2 134.23 28.50 4 8 -2 172.58 32.18 4 8 -2 144.07 28.89 4 8 -1 489.89 41.94 4 8 -1 462.64 37.45 4 8 -1 375.13 31.97 4 8 -1 421.06 42.44 4 8 -1 476.72 67.19 4 8 -1 490.59 42.18 -4 8 1 403.46 33.15 4 8 -1 485.82 34.62 4 8 -1 431.87 37.65 -4 8 1 460.87 38.27 4 8 -1 410.92 35.98 4 8 0 2207.75 87.77 4 8 0 2235.59 91.02 4 8 0 2187.83 94.37 4 8 0 1915.85 125.63 -4 8 0 2088.35 87.90 4 8 0 2233.84 87.00 4 8 0 2249.89 88.97 -4 8 0 2200.07 90.57 4 8 0 2388.68 90.93 4 8 0 2161.53 94.34 4 8 0 2298.42 94.70 4 8 1 2153.78 86.75 4 8 1 2071.21 82.44 4 8 1 2169.29 89.48 4 8 1 2127.92 124.91 -4 8 -1 1979.21 84.49 4 8 1 1872.60 79.74 4 8 1 2045.87 83.76 -4 8 -1 2052.23 86.85 4 8 1 1942.18 84.22 4 8 1 2195.02 89.30 4 8 2 700.77 48.12 4 8 2 767.18 43.81 4 8 2 837.39 52.42 4 8 2 837.85 81.95 -4 8 -2 772.77 43.15 -4 8 -2 828.22 48.40 4 8 2 843.63 45.35 -4 8 -2 788.13 50.70 4 8 2 961.48 48.63 4 8 2 810.94 51.49 4 8 3 572.91 43.79 4 8 3 620.42 47.32 4 8 3 645.03 40.20 4 8 3 663.87 46.63 4 8 3 642.61 74.83 -4 8 -3 631.64 40.94 -4 8 -3 698.83 44.29 4 8 3 698.27 40.06 -4 8 -3 632.85 46.29 4 8 3 679.77 42.76 4 8 4 2809.68 115.39 4 8 4 2626.94 110.89 4 8 4 2952.21 115.14 -4 8 -4 3081.82 112.97 -4 8 -4 3000.63 114.61 4 8 4 3049.46 109.75 -4 8 -4 2822.08 115.72 4 8 4 3251.83 112.84 4 8 4 2814.37 116.88 4 8 4 2879.87 116.74 4 8 5 290.56 38.86 4 8 5 271.64 30.84 4 8 5 268.67 36.58 4 8 5 308.44 36.41 -4 8 -5 384.75 35.56 -4 8 -5 352.00 37.64 4 8 5 357.96 27.61 4 8 5 355.09 30.81 -4 8 -5 300.49 37.01 4 8 5 299.78 40.31 4 8 6 77.21 24.40 4 8 6 61.50 25.42 4 8 6 87.63 30.63 4 8 6 118.33 33.86 4 8 6 79.54 30.82 -4 8 -6 69.44 30.94 -4 8 -6 80.37 29.80 4 8 6 40.73 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45.73 4 9 -11 1351.02 52.34 4 9 -11 1299.57 53.67 4 9 -11 1327.97 52.71 4 9 -11 1260.77 50.04 4 9 -11 1173.72 51.46 4 9 -10 22.08 18.82 4 9 -10 39.91 20.14 4 9 -10 41.83 17.75 4 9 -10 39.17 20.71 4 9 -10 42.20 19.38 4 9 -9 1599.83 62.93 4 9 -9 1552.09 65.68 4 9 -9 1734.32 64.00 4 9 -9 1594.16 62.54 4 9 -9 1528.78 59.21 4 9 -9 1505.04 64.11 4 9 -9 1432.45 61.22 4 9 -8 909.04 43.67 4 9 -8 876.93 46.81 4 9 -8 911.36 45.63 4 9 -8 982.79 45.09 4 9 -8 961.48 44.79 4 9 -8 906.80 41.50 4 9 -8 896.29 45.65 4 9 -8 903.25 43.46 4 9 -7 50.39 22.68 4 9 -7 56.99 20.97 4 9 -7 29.58 24.64 4 9 -7 42.93 23.98 4 9 -7 64.12 24.48 4 9 -7 96.42 24.36 4 9 -7 51.18 19.93 4 9 -7 27.94 24.48 4 9 -6 526.11 33.15 4 9 -6 519.83 38.70 4 9 -6 611.39 38.02 4 9 -6 585.34 36.25 4 9 -6 609.76 37.24 4 9 -6 536.13 33.35 4 9 -6 573.14 37.76 4 9 -5 711.89 38.53 4 9 -5 740.31 43.10 4 9 -5 846.07 42.51 4 9 -5 765.87 42.56 4 9 -5 809.38 41.54 4 9 -5 722.50 44.46 4 9 -5 719.10 41.60 4 9 -4 735.70 42.09 4 9 -4 969.42 48.10 4 9 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1594.63 61.46 -10 -3 -3 227.18 22.34 -10 -3 -3 202.64 21.31 -10 -3 -3 250.25 20.93 -10 -3 -3 204.17 22.10 -10 -3 -3 184.85 18.90 -10 -3 -3 242.17 20.36 -10 -3 -4 1101.10 46.10 -10 -3 -4 1128.38 45.68 -10 -3 -4 1046.19 43.59 -10 -3 -4 1095.37 45.54 -10 -3 -4 1041.76 43.72 -10 -3 -5 401.94 24.60 -10 -3 -5 403.93 23.95 -10 -3 -5 386.67 19.94 -10 -3 -5 379.67 23.25 -10 -3 -5 375.19 20.74 -10 -3 -6 410.23 23.42 -10 -3 -6 401.65 22.57 -10 -3 -6 411.15 20.97 -10 -3 -7 286.87 18.41 -10 -3 -7 294.07 17.71 -10 -3 -7 265.93 15.34 -10 -2 12 12.85 11.21 -10 -2 12 4.57 11.12 -10 -2 12 16.88 9.59 -10 -2 11 3.65 13.41 -10 -2 11 12.74 14.50 -10 -2 11 8.83 12.40 -10 -2 10 166.77 16.24 -10 -2 10 197.46 20.12 -10 -2 10 217.14 18.14 -10 -2 10 217.45 19.64 -10 -2 9 304.05 22.37 -10 -2 9 288.98 22.15 -10 -2 9 298.69 23.75 -10 -2 9 306.59 21.82 -10 -2 8 948.41 41.58 -10 -2 8 904.16 41.23 -10 -2 8 954.11 42.96 -10 -2 8 939.94 41.47 -10 -2 8 893.93 39.92 -10 -2 7 921.37 41.21 -10 -2 7 844.20 41.16 -10 -2 7 861.25 42.52 -10 -2 7 920.97 41.55 -10 -2 7 862.47 39.69 -10 -2 6 787.45 38.47 -10 -2 6 738.23 39.17 -10 -2 6 746.33 39.97 -10 -2 6 831.84 38.66 -10 -2 6 771.78 37.13 -10 -2 5 769.15 38.55 -10 -2 5 707.15 34.86 -10 -2 5 828.95 40.53 -10 -2 5 784.48 40.49 -10 -2 5 746.14 39.09 -10 -2 5 762.57 37.08 -10 -2 4 552.91 33.43 -10 -2 4 512.09 29.67 -10 -2 4 534.69 34.39 -10 -2 4 541.81 34.35 -10 -2 4 558.09 33.64 -10 -2 4 509.72 30.47 -10 -2 3 747.67 39.08 -10 -2 3 737.29 36.50 -10 -2 3 761.46 40.64 -10 -2 3 769.85 40.88 -10 -2 3 727.63 39.43 -10 -2 3 717.27 36.97 -10 -2 2 629.69 36.03 -10 -2 2 603.73 33.33 -10 -2 2 625.69 37.42 -10 -2 2 634.89 37.97 -10 -2 2 650.49 36.77 -10 -2 2 615.18 33.68 -10 -2 1 2138.36 82.04 -10 -2 1 2223.21 81.13 -10 -2 1 2143.52 83.08 -10 -2 1 1995.32 79.03 -10 -2 0 1581.55 65.58 -10 -2 0 1640.67 64.64 -10 -2 0 1657.50 67.43 -10 -2 0 1565.76 62.89 -10 -2 -1 1597.88 67.20 -10 -2 -1 1687.91 66.81 -10 -2 -1 1681.28 68.22 -10 -2 -1 1700.54 64.40 -10 -2 -2 1941.09 75.44 -10 -2 -2 1875.73 74.32 -10 -2 -2 1969.00 75.82 -10 -2 -3 37.56 20.21 -10 -2 -3 30.84 18.54 -10 -2 -3 45.89 20.28 -10 -2 -4 1680.47 66.97 -10 -2 -4 1737.49 66.60 -10 -2 -4 1676.68 66.05 -10 -2 -5 574.37 31.54 -10 -2 -5 626.03 30.96 -10 -2 -5 505.62 28.69 -10 -2 -5 553.23 31.57 -10 -2 -6 1957.28 70.74 -10 -2 -6 1975.38 70.94 -10 -2 -6 1811.68 68.21 -10 -2 -6 1759.07 69.45 -10 -2 -6 1938.52 71.01 -10 -2 -7 373.27 22.22 -10 -2 -7 405.24 22.09 -10 -2 -7 285.71 16.62 -10 -2 -7 334.75 20.02 -10 -2 -7 337.86 22.17 -10 -2 -8 857.34 35.84 -10 -2 -8 953.25 36.40 -10 -2 -8 877.05 35.95 -10 -1 12 38.96 11.19 -10 -1 11 363.34 22.11 -10 -1 11 399.86 21.66 -10 -1 10 46.31 14.96 -10 -1 10 47.36 17.14 -10 -1 9 127.89 18.12 -10 -1 9 120.78 16.85 -10 -1 9 114.14 19.45 -10 -1 9 144.90 17.64 -10 -1 8 1.27 17.71 -10 -1 8 -16.45 17.12 -10 -1 8 25.60 18.92 -10 -1 8 5.24 17.19 -10 -1 7 702.58 34.76 -10 -1 7 663.35 35.00 -10 -1 7 677.86 36.11 -10 -1 7 663.20 34.95 -10 -1 6 227.28 23.50 -10 -1 6 255.04 25.07 -10 -1 6 240.69 26.22 -10 -1 6 249.93 24.56 -10 -1 5 159.44 22.80 -10 -1 5 150.63 24.16 -10 -1 5 109.12 24.64 -10 -1 5 115.82 22.30 -10 -1 4 45.95 20.69 -10 -1 4 17.79 23.36 -10 -1 4 22.77 23.24 -10 -1 4 32.34 21.37 -10 -1 3 1123.37 50.97 -10 -1 3 1185.01 48.56 -10 -1 3 1193.52 54.38 -10 -1 3 1146.08 53.65 -10 -1 3 1194.53 53.35 -10 -1 2 187.80 24.06 -10 -1 2 181.46 20.28 -10 -1 2 190.23 27.33 -10 -1 2 153.07 26.70 -10 -1 2 193.18 25.83 -10 -1 1 737.59 38.80 -10 -1 1 747.24 36.17 -10 -1 1 738.23 41.72 -10 -1 1 714.23 40.50 -10 -1 0 885.21 42.10 -10 -1 0 846.94 39.68 -10 -1 0 796.48 44.12 -10 -1 0 828.78 43.85 -10 -1 -1 1441.80 60.82 -10 -1 -1 1461.48 59.34 -10 -1 -1 1506.93 62.98 -10 -1 -2 1290.98 55.09 -10 -1 -2 1288.31 53.72 -10 -1 -2 1277.43 57.16 -10 -1 -3 710.36 38.28 -10 -1 -3 756.33 36.94 -10 -1 -3 766.13 39.85 -10 -1 -3 708.79 40.63 -10 -1 -4 1064.95 46.28 -10 -1 -4 986.84 45.02 -10 -1 -4 1055.87 47.39 -10 -1 -4 1039.70 48.42 -10 -1 -5 271.98 23.05 -10 -1 -5 268.40 22.18 -10 -1 -5 286.88 24.07 -10 -1 -5 289.90 21.08 -10 -1 -5 324.12 26.64 -10 -1 -6 2234.73 80.32 -10 -1 -6 2221.08 80.49 -10 -1 -6 2187.46 80.35 -10 -1 -6 2100.10 78.57 -10 -1 -6 2108.77 81.31 -10 -1 -7 223.94 19.24 -10 -1 -7 219.71 19.62 -10 -1 -7 260.32 18.87 -10 -1 -7 226.78 18.03 -10 -1 -8 40.92 12.68 -10 -1 -8 52.81 13.58 -10 -1 -8 47.44 10.54 -10 -1 -8 68.83 11.72 -10 0 9 179.54 16.93 -10 0 9 173.22 18.48 -10 0 8 416.18 24.98 -10 0 8 440.26 27.27 -10 0 8 439.24 25.40 -10 0 7 3170.83 112.96 -10 0 7 3203.33 114.22 -10 0 7 3256.11 114.76 -10 0 7 3099.04 113.76 -10 0 6 5.68 17.01 -10 0 6 0.76 18.74 -10 0 6 -4.55 18.73 -10 0 6 2.20 17.58 -10 0 5 980.85 43.14 -10 0 5 987.49 46.16 -10 0 5 1005.88 46.17 -10 0 5 960.25 45.75 -10 0 4 297.54 24.21 -10 0 4 295.11 28.07 -10 0 4 289.44 27.45 -10 0 4 270.07 26.62 -10 0 3 6.99 17.57 -10 0 3 -6.32 22.11 -10 0 3 6.94 21.97 -10 0 3 1.73 21.55 -10 0 2 171.70 20.96 -10 0 2 217.19 28.24 -10 0 2 147.23 24.96 -10 0 1 250.27 23.50 -10 0 1 247.58 28.06 -10 0 1 229.77 27.33 -10 0 0 31.24 19.21 -10 0 0 13.13 24.53 -10 0 0 -9.89 22.53 -10 0 -1 60.03 18.92 -10 0 -1 45.30 24.91 -10 0 -1 54.36 24.17 -10 0 -2 279.06 23.36 -10 0 -2 288.48 21.92 -10 0 -2 270.02 28.99 -10 0 -2 271.05 28.36 -10 0 -3 1543.26 61.11 -10 0 -3 1584.10 60.66 -10 0 -3 1509.68 64.76 -10 0 -4 3003.20 105.90 -10 0 -4 2809.22 105.45 -10 0 -4 3080.25 109.48 -10 0 -5 966.55 41.93 -10 0 -5 961.20 41.64 -10 0 -5 1014.68 45.83 -10 0 -5 1053.72 46.64 -10 0 -6 1157.73 47.57 -10 0 -6 1190.12 48.87 -10 0 -7 689.59 30.72 -10 0 -7 684.17 32.84 -10 0 -7 687.12 34.08 -10 0 -8 21.52 11.07 -10 0 -8 36.06 12.97 -10 0 -8 11.80 14.93 -10 0 -9 244.85 13.57 -10 0 -9 246.95 17.24 10 1 -7 611.19 31.55 10 1 -6 239.31 20.74 -10 1 6 228.23 21.60 -10 1 6 223.82 21.36 -10 1 6 234.54 20.79 10 1 -5 97.70 18.53 -10 1 5 81.31 19.89 -10 1 5 103.79 19.16 -10 1 5 101.40 18.71 10 1 -4 33.66 17.29 -10 1 4 15.05 19.87 -10 1 4 20.37 18.78 -10 1 4 5.20 18.48 -10 1 3 1182.28 51.48 -10 1 3 1108.68 49.57 -10 1 2 169.34 24.80 -10 1 2 161.32 23.59 -10 1 1 783.26 40.27 -10 1 1 658.73 37.63 -10 1 0 779.83 41.68 -10 1 0 765.76 39.61 -10 1 -1 1440.90 62.81 -10 1 -1 1484.76 61.50 -10 1 -2 1320.42 57.73 -10 1 -2 1300.73 56.33 -10 1 -3 774.13 41.34 -10 1 -3 798.03 40.41 -10 1 -4 1068.17 48.32 -10 1 -4 977.89 46.39 -10 1 -5 284.77 24.95 -10 1 -6 2167.07 81.07 -10 1 -7 242.15 20.27 -10 1 -7 249.28 20.86 -10 1 -8 56.09 13.78 -10 1 -8 46.10 14.22 10 2 -8 865.17 39.28 10 2 -7 802.95 38.06 10 2 -6 679.55 34.55 10 2 -5 781.80 38.08 10 2 -4 535.66 31.05 -10 2 4 512.62 29.57 10 2 -3 725.64 35.90 -10 2 3 708.68 35.76 -10 2 3 687.64 34.38 10 2 -2 580.66 32.60 -10 2 2 653.56 34.19 10 2 -1 1924.91 75.90 -10 2 1 2026.09 78.02 -10 2 1 2053.85 75.43 -10 2 0 1645.97 63.88 -10 2 0 1585.88 60.81 10 2 1 1686.60 64.06 -10 2 -1 1631.77 66.98 -10 2 -1 1622.15 64.24 10 2 2 1918.63 72.86 -10 2 -2 2037.25 76.94 -10 2 -2 1923.76 73.80 -10 2 -3 22.69 21.25 -10 2 -3 42.88 18.05 -10 2 -4 1708.44 66.65 -10 2 -4 1633.80 64.28 -10 2 -5 558.19 31.39 -10 2 -5 516.58 28.34 -10 2 -6 1963.09 71.30 -10 2 -6 1796.41 69.15 -10 2 -7 328.94 20.23 -10 2 -8 797.38 32.32 10 3 -7 49.80 17.50 10 3 -6 10.21 17.66 10 3 -6 27.22 11.39 10 3 -5 37.14 17.51 10 3 -4 398.18 25.98 10 3 -4 299.74 19.17 10 3 -3 645.00 32.56 10 3 -3 558.23 28.43 10 3 -2 587.04 31.02 -10 3 2 538.81 28.19 -10 3 1 215.35 20.74 10 3 -1 183.30 21.82 10 3 0 333.73 25.02 -10 3 0 326.48 24.15 10 3 1 134.40 19.70 -10 3 -1 155.60 19.99 10 3 2 1425.38 57.70 -10 3 -2 1522.00 59.34 -10 3 -3 199.68 21.35 -10 3 -4 1130.53 47.36 -10 3 -5 369.92 24.21 -10 3 -6 406.40 24.02 -10 3 -7 284.60 17.34 10 3 7 193.96 15.81 10 4 -8 369.67 18.82 10 4 -5 358.45 23.29 10 4 -5 369.94 19.53 10 4 -4 1.26 16.35 10 4 -4 4.03 13.45 10 4 -3 3.83 15.73 10 4 -3 2.51 15.31 10 4 -3 6.25 11.86 10 4 -2 0.64 15.61 10 4 -2 24.48 14.13 10 4 -1 706.22 32.20 10 4 -1 561.72 29.30 10 4 0 143.71 18.65 10 4 0 138.33 17.79 -10 4 -1 149.34 15.19 10 4 1 136.91 17.98 -10 4 -2 425.33 22.96 10 4 2 455.33 25.20 -10 4 -3 177.24 16.80 -10 4 -4 197.91 16.18 10 4 4 228.58 17.26 -10 4 -5 178.05 14.85 10 4 5 188.68 15.40 10 5 -6 201.96 14.29 10 5 -5 1298.06 48.59 10 5 -4 631.21 26.07 10 5 -3 486.91 22.70 10 5 -2 47.41 13.00 10 5 -2 51.75 9.79 10 5 -1 138.76 14.56 10 5 -1 110.18 11.93 10 5 0 33.64 11.23 10 5 1 226.40 17.47 10 5 1 266.10 16.10 -11 -2 5 66.59 11.23 -11 -2 5 94.70 13.19 -11 -2 5 85.82 12.72 -11 -2 5 107.52 12.00 -11 -2 4 126.46 12.39 -11 -2 4 132.77 14.39 -11 -2 4 129.20 15.00 -11 -2 4 146.33 13.48 -11 -2 3 50.97 11.07 -11 -2 3 69.51 13.23 -11 -2 3 51.44 13.01 -11 -2 3 80.61 12.51 -11 -2 2 20.79 11.08 -11 -2 2 18.15 13.13 -11 -2 2 23.97 12.73 -11 -2 2 39.70 12.74 -11 -2 1 526.53 24.49 -11 -2 1 552.22 25.52 -11 -2 0 48.98 10.66 -11 -2 0 54.73 13.44 -11 -1 6 1452.55 54.20 -11 -1 6 1501.10 54.74 -11 -1 6 1537.31 54.52 -11 -1 5 500.58 23.40 -11 -1 5 458.57 23.48 -11 -1 5 459.71 22.91 -11 -1 4 228.99 18.46 -11 -1 4 242.96 18.32 -11 -1 4 254.03 16.94 -11 -1 3 92.65 15.09 -11 -1 3 89.15 15.46 -11 -1 3 116.51 14.69 -11 -1 2 565.27 27.97 -11 -1 2 576.66 28.04 -11 -1 2 569.03 27.41 -11 -1 1 1732.18 64.99 -11 -1 1 1692.67 64.33 -11 -1 1 1808.83 64.55 -11 -1 0 131.87 15.98 -11 -1 0 105.96 15.15 -11 -1 0 130.23 14.74 -11 -1 -1 1780.10 65.41 -11 -1 -1 1800.68 65.57 -11 -1 -2 67.58 13.83 -11 -1 -2 86.83 13.02 -11 0 6 202.40 12.19 -11 0 5 9.43 10.49 -11 0 5 10.15 10.56 -11 0 5 6.77 10.07 -11 0 4 -3.05 12.67 -11 0 4 0.39 11.64 -11 0 4 0.81 11.63 -11 0 3 -0.47 13.13 -11 0 3 3.82 12.62 -11 0 3 -4.80 11.58 -11 0 2 113.20 15.59 -11 0 2 101.94 15.23 -11 0 2 148.80 15.57 -11 0 1 425.41 23.58 -11 0 1 412.49 22.99 -11 0 1 386.87 22.56 -11 0 0 93.07 15.62 -11 0 0 94.21 14.71 -11 0 0 102.59 14.67 -11 0 -1 166.76 16.68 -11 0 -1 156.81 15.79 -11 0 -1 155.16 15.95 -11 0 -2 7.74 12.60 -11 0 -2 13.05 11.47 -11 0 -2 0.86 12.15 -11 1 3 94.28 13.38 -11 1 3 102.97 11.04 -11 1 2 555.58 26.55 -11 1 2 557.88 24.88 -11 1 1 1599.87 60.66 -11 1 1 1660.49 59.46 -11 1 0 108.76 14.52 -11 1 0 116.88 11.33 -11 1 0 98.30 13.32 -11 1 -1 1675.18 60.26 -11 1 -1 1551.12 57.85 -11 1 -1 1673.32 59.16 -11 1 -2 79.99 13.21 -11 1 -2 59.80 9.91 -11 1 -2 55.38 11.63 -11 2 1 445.81 20.55 -11 2 0 41.93 10.40 ; loop_ _symmetry_equiv_pos_as_xyz x,y,z -x,y+1/2,-z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_occupancy _atom_site_adp_type _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N1 N -0.32343(16) 0.3385(2) 0.60159(8) 0.0341 1.0000 Uani . . . . . C2 C -0.32627(19) 0.2499(2) 0.66476(9) 0.0322 1.0000 Uani . . . . . C3 C -0.19053(18) 0.1490(2) 0.67420(9) 0.0258 1.0000 Uani . . . . . C4 C -0.04690(17) 0.23005(19) 0.67948(8) 0.0222 1.0000 Uani . . . . . C5 C 0.04607(17) 0.2501(2) 0.62889(8) 0.0241 1.0000 Uani . . . . . N6 N 0.16188(16) 0.33923(18) 0.65150(7) 0.0248 1.0000 Uani . . . . . C7 C 0.14416(17) 0.3798(2) 0.71837(8) 0.0223 1.0000 Uani . . . . . C8 C 0.01460(17) 0.3116(2) 0.73792(8) 0.0206 1.0000 Uani . . . . . C9 C 0.22964(18) 0.4703(2) 0.76320(9) 0.0270 1.0000 Uani . . . . . C10 C 0.18530(19) 0.4891(2) 0.82831(9) 0.0275 1.0000 Uani . . . . . C11 C 0.05911(18) 0.41778(19) 0.84976(8) 0.0231 1.0000 Uani . . . . . C12 C -0.02846(16) 0.3303(2) 0.80515(8) 0.0215 1.0000 Uani . . . . . O13 O 0.03361(14) 0.44284(17) 0.91722(6) 0.0289 1.0000 Uani . . . . . C14 C -0.07420(17) 0.3519(2) 0.94552(8) 0.0239 1.0000 Uani . . . . . C15 C -0.08089(17) 0.3932(2) 1.01974(8) 0.0236 1.0000 Uani . . . . . C16 C -0.16646(19) 0.5110(2) 1.03694(9) 0.0277 1.0000 Uani . . . . . C17 C -0.1697(2) 0.5510(2) 1.10548(10) 0.0336 1.0000 Uani . . . . . C18 C -0.0899(2) 0.4731(3) 1.15699(10) 0.0367 1.0000 Uani . . . . . C19 C -0.0093(2) 0.3542(3) 1.14061(10) 0.0369 1.0000 Uani . . . . . C20 C -0.0041(2) 0.3144(2) 1.07193(9) 0.0308 1.0000 Uani . . . . . N21 N 0.16049(18) 0.88099(19) 0.57327(8) 0.0284 0.8828(14) Uani . U P 1 1 C22 C 0.1679(2) 0.8979(2) 0.65055(10) 0.0342 1.0000 Uani D . . . . C23 C 0.31070(18) 0.9719(2) 0.67756(9) 0.0262 1.0000 Uani . . . . . C24 C 0.44748(17) 0.87925(19) 0.67981(8) 0.0227 1.0000 Uani . . . . . C25 C 0.53892(19) 0.8552(2) 0.62813(9) 0.0274 1.0000 Uani . . . . . N26 N 0.64869(16) 0.7601(2) 0.64982(8) 0.0304 1.0000 Uani . . . . . C27 C 0.63075(18) 0.7202(2) 0.71656(9) 0.0251 1.0000 Uani . . . . . C28 C 0.50586(17) 0.79346(19) 0.73736(8) 0.0210 1.0000 Uani . . . . . C29 C 0.71424(18) 0.6269(2) 0.76136(9) 0.0296 1.0000 Uani . . . . . C30 C 0.67250(19) 0.6119(2) 0.82710(8) 0.0281 1.0000 Uani . . . . . C31 C 0.54977(18) 0.68791(19) 0.84922(8) 0.0233 1.0000 Uani . . . . . C32 C 0.46520(17) 0.77809(19) 0.80507(8) 0.0214 1.0000 Uani . . . . . O33 O 0.52581(14) 0.66322(17) 0.91697(6) 0.0296 1.0000 Uani . . . . . C34 C 0.42126(18) 0.7565(2) 0.94624(8) 0.0244 1.0000 Uani . . . . . C35 C 0.41460(17) 0.7117(2) 1.02003(8) 0.0233 1.0000 Uani . . . . . C36 C 0.4913(2) 0.7884(2) 1.07309(9) 0.0297 1.0000 Uani . . . . . C37 C 0.4858(2) 0.7462(3) 1.14129(10) 0.0363 1.0000 Uani . . . . . C38 C 0.4043(2) 0.6263(2) 1.15632(9) 0.0327 1.0000 Uani . . . . . C39 C 0.3261(2) 0.5507(2) 1.10374(10) 0.0323 1.0000 Uani . . . . . C40 C 0.33007(18) 0.5941(2) 1.03605(9) 0.0274 1.0000 Uani . . . . . O41 O 0.39560(17) 0.63325(19) 0.50109(8) 0.0390 0.8828(14) Uani . U P 1 1 C42 C 0.3364(2) 0.5289(2) 0.52846(9) 0.0238 0.8828(14) Uani . . P 1 1 O43 O 0.39729(14) 0.44623(18) 0.57295(7) 0.0302 0.8828(14) Uani . . P 1 1 C44 C 0.1711(3) 0.4985(3) 0.50473(13) 0.0245 0.8828(14) Uani . U P 1 1 O45 O 0.08199(15) 0.59855(18) 0.51529(8) 0.0339 0.8828(14) Uani . . P 1 1 O46 O 0.14065(15) 0.38059(18) 0.47767(8) 0.0313 0.8828(14) Uani . . P 1 1 O47 O 0.09788(15) 1.07117(18) 0.37856(8) 0.0330 0.8828(14) Uani . . P 1 1 O48 O 0.29951(18) 1.1164(2) 0.51036(9) 0.0360 0.8828(14) Uani . . P 1 1 N121 N 0.1771(13) 0.7709(9) 0.6029(5) 0.0282 0.1172(14) Uani D U P 1 2 O141 O 0.3620(12) 1.2306(12) 0.5206(6) 0.0391 0.1172(14) Uani D U P 1 2 C142 C 0.3324(14) 1.1117(15) 0.4946(9) 0.0245 0.1172(14) Uani D U P 1 2 O143 O 0.4174(12) 1.0153(12) 0.4833(6) 0.0392 0.1172(14) Uani D U P 1 2 C144 C 0.1667(12) 1.0825(13) 0.4711(6) 0.0246 0.1172(14) Uani D U P 1 2 O145 O 0.1014(12) 1.1649(13) 0.4256(6) 0.0388 0.1172(14) Uani D U P 1 2 O146 O 0.1055(13) 0.9788(13) 0.4993(6) 0.0394 0.1172(14) Uani D U P 1 2 O148 O 0.203(2) 0.503(2) 0.4935(10) 0.0393 0.1172(14) Uani . U P 1 2 O147 O 0.4018(13) 0.5374(13) 0.6211(6) 0.0391 0.1172(14) Uani . U P 1 2 H161 H -0.2210 0.5617 1.0018 0.0331 1.0000 Uiso R . . . . H171 H -0.2264 0.6342 1.1164 0.0399 1.0000 Uiso R . . . . H181 H -0.0889 0.5028 1.2041 0.0435 1.0000 Uiso R . . . . H191 H 0.0480 0.3026 1.1764 0.0452 1.0000 Uiso R . . . . H201 H 0.0543 0.2372 1.0612 0.0379 1.0000 Uiso R . . . . H142 H -0.0413 0.2529 0.9406 0.0299 1.0000 Uiso R . . . . H141 H -0.1708 0.3665 0.9199 0.0286 1.0000 Uiso R . . . . H13 H -0.3298 0.2589 0.5658 0.0426 1.0000 Uiso R . . . . H12 H -0.2413 0.4038 0.6026 0.0514 1.0000 Uiso R . . . . H11 H -0.4101 0.3931 0.5918 0.0507 1.0000 Uiso R . . . . H21 H -0.3296 0.3152 0.7053 0.0401 1.0000 Uiso R . . . . H22 H -0.4140 0.1932 0.6599 0.0381 1.0000 Uiso R . . . . H31 H -0.1971 0.0923 0.7166 0.0296 1.0000 Uiso R . . . . H32 H -0.1932 0.0845 0.6336 0.0306 1.0000 Uiso R . . . . H51 H 0.0369 0.2088 0.5853 0.0288 1.0000 Uiso R . . . . H61 H 0.2293 0.3683 0.6281 0.0315 1.0000 Uiso R . . . . H101 H 0.2425 0.5471 0.8605 0.0323 1.0000 Uiso R . . . . H91 H 0.3172 0.5160 0.7508 0.0321 1.0000 Uiso R . . . . H121 H -0.1104 0.2837 0.8183 0.0260 1.0000 Uiso R . . . . H301 H 0.7275 0.5455 0.8590 0.0340 1.0000 Uiso R . . . . H291 H 0.7977 0.5755 0.7467 0.0354 1.0000 Uiso R . . . . H261 H 0.7207 0.7285 0.6246 0.0373 1.0000 Uiso R . . . . H251 H 0.5353 0.8912 0.5812 0.0328 1.0000 Uiso R . . . . H231 H 0.2948 1.0026 0.7249 0.0303 1.0000 Uiso R . . . . H232 H 0.3239 1.0596 0.6492 0.0306 1.0000 Uiso R . . . . H321 H 0.3821 0.8328 0.8196 0.0255 1.0000 Uiso R . . . . H361 H 0.5442 0.8733 1.0631 0.0362 1.0000 Uiso R . . . . H371 H 0.5377 0.8001 1.1776 0.0438 1.0000 Uiso R . . . . H381 H 0.4028 0.5955 1.2020 0.0388 1.0000 Uiso R . . . . H391 H 0.2720 0.4689 1.1144 0.0398 1.0000 Uiso R . . . . H401 H 0.2750 0.5426 0.9993 0.0333 1.0000 Uiso R . . . . H342 H 0.4556 0.8578 0.9442 0.0278 1.0000 Uiso R . . . . H341 H 0.3200 0.7463 0.9190 0.0296 1.0000 Uiso R . . . . H224 H 0.0809 0.9544 0.6610 0.0396 0.8828(14) Uiso R . P 1 1 H223 H 0.1609 0.8084 0.6731 0.0374 0.8828(14) Uiso R . P 1 1 H222 H 0.1239 0.8602 0.6905 0.0409 0.1172(14) Uiso R . P 1 2 H221 H 0.1009 0.9689 0.6277 0.0411 0.1172(14) Uiso R . P 1 2 H1212 H 0.1044 0.7087 0.6098 0.0460 0.1172(14) Uiso R . P 1 2 H1213 H 0.2655 0.7278 0.6115 0.0458 0.1172(14) Uiso R . P 1 2 H1211 H 0.1664 0.8003 0.5592 0.0459 0.1172(14) Uiso R . P 1 2 H211 H 0.0630 0.8688 0.5578 0.0436 0.8828(14) Uiso R . P 1 1 H212 H 0.1973 0.9585 0.5526 0.0438 0.8828(14) Uiso R . P 1 1 H213 H 0.2131 0.8053 0.5619 0.0426 0.8828(14) Uiso R . P 1 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 N1 0.0247(7) 0.0402(9) 0.0369(8) 0.0001(7) 0.0001(6) 0.0009(6) C2 0.0224(8) 0.0422(10) 0.0326(9) 0.0043(8) 0.0052(6) -0.0028(7) C3 0.0259(8) 0.0276(8) 0.0240(8) -0.0025(6) 0.0028(6) -0.0040(6) C4 0.0199(7) 0.0235(8) 0.0229(7) 0.0013(6) 0.0005(6) 0.0010(6) C5 0.0236(7) 0.0255(8) 0.0232(7) -0.0004(6) 0.0018(6) 0.0031(6) N6 0.0232(6) 0.0297(7) 0.0222(7) 0.0012(6) 0.0059(5) -0.0011(6) C7 0.0216(7) 0.0248(8) 0.0206(7) 0.0037(6) 0.0029(6) 0.0003(6) C8 0.0191(7) 0.0201(7) 0.0224(7) 0.0006(6) 0.0005(6) 0.0013(6) C9 0.0217(7) 0.0292(8) 0.0301(8) 0.0012(7) 0.0029(6) -0.0075(6) C10 0.0268(8) 0.0276(8) 0.0279(8) -0.0009(7) 0.0011(6) -0.0077(6) C11 0.0261(8) 0.0220(8) 0.0215(8) 0.0004(6) 0.0036(6) -0.0012(6) C12 0.0184(7) 0.0233(8) 0.0230(7) 0.0024(6) 0.0025(6) -0.0016(6) O13 0.0327(6) 0.0327(6) 0.0222(6) -0.0042(5) 0.0068(5) -0.0125(5) C14 0.0232(7) 0.0240(8) 0.0250(8) 0.0009(6) 0.0047(6) -0.0031(6) C15 0.0214(7) 0.0239(8) 0.0262(8) -0.0015(7) 0.0058(6) -0.0040(6) C16 0.0262(8) 0.0247(8) 0.0331(9) 0.0005(7) 0.0071(6) -0.0026(6) C17 0.0344(9) 0.0290(9) 0.0397(10) -0.0082(8) 0.0160(8) -0.0067(7) C18 0.0351(9) 0.0493(12) 0.0271(8) -0.0084(9) 0.0095(7) -0.0154(9) C19 0.0330(9) 0.0510(12) 0.0265(9) 0.0041(8) 0.0017(7) -0.0025(9) C20 0.0284(9) 0.0342(9) 0.0303(9) 0.0013(8) 0.0057(7) 0.0021(7) N21 0.0283(7) 0.0238(7) 0.0316(8) 0.0010(6) -0.0060(6) 0.0006(6) C22 0.0243(8) 0.0379(10) 0.0405(10) -0.0031(8) 0.0040(7) 0.0027(7) C23 0.0252(8) 0.0265(8) 0.0265(8) 0.0010(6) 0.0006(6) 0.0058(6) C24 0.0228(7) 0.0228(8) 0.0223(7) 0.0014(6) 0.0013(6) 0.0002(6) C25 0.0281(8) 0.0336(9) 0.0207(7) 0.0022(7) 0.0029(6) 0.0051(7) N26 0.0277(7) 0.0399(8) 0.0244(7) 0.0010(6) 0.0072(5) 0.0102(6) C27 0.0238(7) 0.0276(8) 0.0241(8) -0.0003(6) 0.0034(6) 0.0032(6) C28 0.0189(7) 0.0205(8) 0.0235(7) -0.0026(6) 0.0012(6) 0.0010(6) C29 0.0265(8) 0.0326(9) 0.0301(8) -0.0021(7) 0.0053(6) 0.0111(7) C30 0.0294(8) 0.0287(8) 0.0260(8) 0.0035(7) 0.0021(6) 0.0112(7) C31 0.0241(8) 0.0238(8) 0.0224(8) 0.0002(6) 0.0040(6) 0.0019(6) C32 0.0209(7) 0.0195(7) 0.0243(8) -0.0002(6) 0.0039(6) 0.0021(6) O33 0.0337(6) 0.0310(6) 0.0254(6) 0.0049(5) 0.0087(5) 0.0131(5) C34 0.0259(8) 0.0240(8) 0.0239(8) 0.0005(6) 0.0053(6) 0.0058(6) C35 0.0210(7) 0.0243(8) 0.0249(8) -0.0002(6) 0.0045(6) 0.0046(6) C36 0.0282(9) 0.0315(9) 0.0296(9) -0.0034(7) 0.0034(7) -0.0052(7) C37 0.0346(9) 0.0473(12) 0.0268(9) -0.0050(8) 0.0005(7) 0.0010(8) C38 0.0326(9) 0.0414(10) 0.0254(8) 0.0067(8) 0.0102(7) 0.0112(8) C39 0.0328(9) 0.0284(9) 0.0373(9) 0.0070(8) 0.0117(7) 0.0044(7) C40 0.0265(8) 0.0259(8) 0.0303(8) -0.0025(7) 0.0054(6) 0.0013(6) O41 0.0364(7) 0.0417(8) 0.0374(7) 0.0140(6) -0.0047(5) -0.0148(6) C42 0.0252(8) 0.0241(8) 0.0224(8) -0.0014(6) 0.0044(6) 0.0003(6) O43 0.0182(6) 0.0360(7) 0.0362(7) 0.0098(6) 0.0014(5) 0.0028(5) C44 0.0238(12) 0.0259(9) 0.0241(10) 0.0075(8) 0.0041(7) 0.0040(9) O45 0.0302(7) 0.0363(8) 0.0362(7) 0.0065(6) 0.0086(5) 0.0148(6) O46 0.0258(6) 0.0296(7) 0.0374(7) -0.0017(6) -0.0031(5) 0.0006(5) O47 0.0268(6) 0.0351(7) 0.0383(7) -0.0064(6) 0.0086(5) -0.0085(6) O48 0.0304(8) 0.0342(8) 0.0442(11) 0.0061(7) 0.0079(6) 0.0017(7) N121 0.023(5) 0.038(6) 0.024(5) 0.001(5) 0.006(4) -0.004(4) O141 0.0366(12) 0.0419(12) 0.0370(12) 0.0138(11) -0.0054(11) -0.0145(11) C142 0.0243(15) 0.0256(13) 0.0240(14) 0.0073(12) 0.0042(12) 0.0044(13) O143 0.0365(12) 0.0420(12) 0.0376(12) 0.0139(11) -0.0044(11) -0.0139(11) C144 0.0237(15) 0.0262(13) 0.0241(14) 0.0074(12) 0.0038(12) 0.0037(13) O145 0.0361(12) 0.0420(12) 0.0369(12) 0.0136(11) -0.0043(11) -0.0137(11) O146 0.0372(12) 0.0421(12) 0.0375(12) 0.0141(11) -0.0048(11) -0.0146(11) O148 0.0368(12) 0.0418(12) 0.0378(12) 0.0141(11) -0.0042(11) -0.0145(12) O147 0.0363(12) 0.0419(12) 0.0376(12) 0.0133(11) -0.0043(11) -0.0149(11) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source C 0.0181 0.0091 2.3100 20.8439 1.0200 10.2075 1.5886 0.5687 0.8650 51.6512 0.2156 'International Tables Vol C 4.2.6.8 and 6.1.1.4' H 0.0000 0.0000 0.4930 10.5109 0.3229 26.1257 0.1402 3.1424 0.0408 57.7998 0.0030 'International Tables Vol C 4.2.6.8 and 6.1.1.4' N 0.0311 0.0180 12.2126 0.0057 3.1322 9.8933 2.0125 28.9975 1.1663 0.5826 -11.5290 'International Tables Vol C 4.2.6.8 and 6.1.1.4' O 0.0492 0.0322 3.0485 13.2771 2.2868 5.7011 1.5463 0.3239 0.8670 32.9089 0.2508 'International Tables Vol C 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_publ_flag C2 N1 H13 99.1 no C2 N1 H12 114.2 no H13 N1 H12 118.2 no C2 N1 H11 113.1 no H13 N1 H11 105.4 no H12 N1 H11 106.7 no N1 C2 C3 111.34(14) yes N1 C2 H21 108.7 no C3 C2 H21 111.0 no N1 C2 H22 107.9 no C3 C2 H22 108.4 no H21 C2 H22 109.3 no C2 C3 C4 111.86(14) yes C2 C3 H31 108.5 no C4 C3 H31 109.4 no C2 C3 H32 108.3 no C4 C3 H32 108.5 no H31 C3 H32 110.2 no C3 C4 C5 127.26(15) yes C3 C4 C8 126.13(14) yes C5 C4 C8 106.47(14) yes C4 C5 N6 110.47(15) yes C4 C5 H51 126.6 no N6 C5 H51 122.9 no C5 N6 C7 108.50(13) yes C5 N6 H61 126.0 no C7 N6 H61 125.4 no N6 C7 C8 107.63(14) yes N6 C7 C9 130.68(15) yes C8 C7 C9 121.70(14) yes C4 C8 C7 106.93(13) yes C4 C8 C12 133.04(14) yes C7 C8 C12 120.02(14) yes C7 C9 C10 117.64(15) yes C7 C9 H91 122.4 no C10 C9 H91 119.9 no C9 C10 C11 121.57(15) yes C9 C10 H101 119.8 no C11 C10 H101 118.5 no C10 C11 C12 121.21(15) yes C10 C11 O13 114.43(14) yes C12 C11 O13 124.36(14) yes C8 C12 C11 117.79(14) yes C8 C12 H121 120.0 no C11 C12 H121 122.2 no C11 O13 C14 116.48(12) yes O13 C14 C15 107.92(13) yes O13 C14 H142 107.3 no C15 C14 H142 112.1 no O13 C14 H141 108.9 no C15 C14 H141 110.2 no H142 C14 H141 110.2 no C14 C15 C16 120.23(15) yes C14 C15 C20 120.57(15) yes C16 C15 C20 119.19(16) yes C15 C16 C17 120.13(17) yes C15 C16 H161 119.0 no C17 C16 H161 120.9 no C16 C17 C18 120.02(18) yes C16 C17 H171 119.2 no C18 C17 H171 120.8 no C17 C18 C19 120.17(18) yes C17 C18 H181 120.1 no C19 C18 H181 119.7 no C18 C19 C20 120.11(18) yes C18 C19 H191 119.7 no C20 C19 H191 120.1 no C19 C20 C15 120.32(18) yes C19 C20 H201 119.6 no C15 C20 H201 120.0 no C22 N21 H211 107.2 no C22 N21 H212 112.2 no H211 N21 H212 109.6 no C22 N21 H213 110.8 no H211 N21 H213 109.8 no H212 N21 H213 107.2 no N21 C22 C23 110.62(15) yes N21 C22 H224 107.5 no C23 C22 H224 110.7 no N21 C22 H223 111.8 no C23 C22 H223 109.4 no H224 C22 H223 106.7 no C23 C22 N121 118.6(5) yes C23 C22 H222 106.5 no N121 C22 H222 105.0 no C23 C22 H221 108.6 no N121 C22 H221 108.5 no H222 C22 H221 109.3 no C22 C23 C24 114.67(15) yes C22 C23 H231 105.3 no C24 C23 H231 109.2 no C22 C23 H232 108.8 no C24 C23 H232 110.3 no H231 C23 H232 108.3 no C23 C24 C25 128.09(15) yes C23 C24 C28 125.62(15) yes C25 C24 C28 106.27(14) yes C24 C25 N26 110.13(15) yes C24 C25 H251 131.5 no N26 C25 H251 118.4 no C25 N26 C27 108.83(14) yes C25 N26 H261 125.6 no C27 N26 H261 125.6 no N26 C27 C28 107.96(14) yes N26 C27 C29 130.79(15) yes C28 C27 C29 121.24(15) yes C24 C28 C27 106.81(14) yes C24 C28 C32 132.81(15) yes C27 C28 C32 120.32(14) yes C27 C29 C30 117.79(15) yes C27 C29 H291 121.0 no C30 C29 H291 121.2 no C29 C30 C31 121.50(15) yes C29 C30 H301 119.3 no C31 C30 H301 119.2 no C30 C31 C32 121.11(15) yes C30 C31 O33 113.93(14) yes C32 C31 O33 124.96(14) yes C28 C32 C31 117.99(14) yes C28 C32 H321 119.7 no C31 C32 H321 122.3 no C31 O33 C34 116.50(12) yes O33 C34 C35 107.30(13) yes O33 C34 H342 109.9 no C35 C34 H342 109.9 no O33 C34 H341 109.0 no C35 C34 H341 111.0 no H342 C34 H341 109.6 no C34 C35 C36 120.55(15) yes C34 C35 C40 120.43(15) yes C36 C35 C40 119.02(16) yes C35 C36 C37 120.44(17) yes C35 C36 H361 119.9 no C37 C36 H361 119.6 no C36 C37 C38 119.85(17) yes C36 C37 H371 120.1 no C38 C37 H371 120.1 no C37 C38 C39 119.92(17) yes C37 C38 H381 120.3 no C39 C38 H381 119.8 no C38 C39 C40 120.12(17) yes C38 C39 H391 119.3 no C40 C39 H391 120.6 no C35 C40 C39 120.61(16) yes C35 C40 H401 118.9 no C39 C40 H401 120.5 no O41 C42 O43 126.79(17) yes O41 C42 C44 116.88(17) yes O43 C42 C44 116.33(17) yes C42 C44 O45 115.2(2) yes C42 C44 O46 117.36(19) yes O45 C44 O46 127.4(2) yes C22 N121 H1212 109.3 no C22 N121 H1213 109.5 no H1212 N121 H1213 109.4 no C22 N121 H1211 109.8 no H1212 N121 H1211 109.2 no H1213 N121 H1211 109.5 no O141 C142 O143 128.5(11) yes O141 C142 C144 116.4(10) yes O143 C142 C144 115.1(10) yes C142 C144 O145 118.1(9) yes C142 C144 O146 117.1(10) yes O145 C144 O146 124.9(9) yes loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_publ_flag N1 C2 1.485(2) yes N1 H13 1.016 no N1 H12 0.957 no N1 H11 0.936 no C2 C3 1.540(2) yes C2 H21 1.001 no C2 H22 0.948 no C3 C4 1.494(2) yes C3 H31 0.988 no C3 H32 0.993 no C4 C5 1.365(2) yes C4 C8 1.437(2) yes C5 N6 1.374(2) yes C5 H51 0.929 no N6 C7 1.381(2) yes N6 H61 0.838 no C7 C8 1.412(2) yes C7 C9 1.394(2) yes C8 C12 1.412(2) yes C9 C10 1.377(2) yes C9 H91 0.947 no C10 C11 1.413(2) yes C10 H101 0.944 no C11 C12 1.384(2) yes C11 O13 1.376(2) yes C12 H121 0.913 no O13 C14 1.4371(19) yes C14 C15 1.504(2) yes C14 H142 0.977 no C14 H141 0.972 no C15 C16 1.400(2) yes C15 C20 1.386(2) yes C16 C17 1.390(3) yes C16 H161 0.934 no C17 C18 1.385(3) yes C17 H171 0.963 no C18 C19 1.378(3) yes C18 H181 0.958 no C19 C20 1.394(3) yes C19 H191 0.958 no C20 H201 0.927 no N21 C22 1.510(2) yes N21 H211 0.909 no N21 H212 0.905 no N21 H213 0.889 no C22 C23 1.511(2) yes C22 H224 0.981 no C22 H223 0.948 no C22 C23 1.511(2) yes C22 N121 1.512(5) yes C22 H222 0.972 no C22 H221 0.976 no C23 C24 1.502(2) yes C23 H231 0.989 no C23 H232 1.000 no C24 C25 1.378(2) yes C24 C28 1.437(2) yes C25 N26 1.365(2) yes C25 H251 0.973 no N26 C27 1.377(2) yes N26 H261 0.899 no C27 C28 1.408(2) yes C27 C29 1.401(2) yes C28 C32 1.410(2) yes C29 C30 1.376(2) yes C29 H291 0.957 no C30 C31 1.414(2) yes C30 H301 0.978 no C31 C32 1.381(2) yes C31 O33 1.377(2) yes C32 H321 0.969 no O33 C34 1.4386(19) yes C34 C35 1.505(2) yes C34 H342 0.995 no C34 H341 1.016 no C35 C36 1.387(2) yes C35 C40 1.387(2) yes C36 C37 1.392(3) yes C36 H361 0.954 no C37 C38 1.383(3) yes C37 H371 0.954 no C38 C39 1.382(3) yes C38 H381 0.936 no C39 C40 1.384(3) yes C39 H391 0.939 no C40 H401 0.962 no O41 C42 1.252(2) yes C42 O43 1.248(2) yes C42 C44 1.544(3) yes C44 O45 1.260(3) yes C44 O46 1.238(3) yes N121 H1212 0.894 no N121 H1213 0.894 no N121 H1211 0.890 no O141 C142 1.237(14) yes C142 O143 1.214(14) yes C142 C144 1.545(13) yes C144 O145 1.276(12) yes C144 O146 1.263(13) yes loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_angle_DHA _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_publ_flag N1 H13 O41 2_546 164 1.02 1.81 2.801(3) yes N1 H12 O47 2_546 165 0.96 2.04 2.972(3) yes N1 H12 C144 2_546 135 0.96 2.34 3.090(3) yes N1 H12 O146 2_546 126 0.96 2.53 3.186(3) yes N1 H11 O43 1_455 163 0.94 1.81 2.718(3) yes N1 H11 O147 1_455 154 0.94 2.28 3.144(3) yes C3 H32 O148 2_546 160 0.99 2.59 3.534(3) yes C5 H51 O45 2_546 158 0.93 2.38 3.259(3) yes N6 H61 O43 . 178 0.84 2.07 2.906(3) yes N6 H61 O147 . 144 0.84 2.23 2.945(3) yes N26 H261 O47 2_646 144 0.90 2.20 2.976(3) yes N26 H261 C142 2_646 123 0.90 2.57 3.156(3) yes N26 H261 C144 2_646 156 0.90 2.59 3.434(3) yes N26 H261 O145 2_646 175 0.90 2.04 2.938(3) yes C25 H251 O143 . 153 0.97 2.39 3.290(3) yes N121 H1212 O47 2_546 173 0.89 2.26 3.146(3) yes N121 H1212 O145 2_546 140 0.89 1.96 2.705(3) yes N121 H1213 O147 . 151 0.89 2.16 2.971(3) yes N21 H1211 O45 . 156 0.80 2.17 2.926(3) yes N121 H1211 O146 . 142 0.89 2.08 2.830(3) yes N21 H211 O46 2_556 169 0.91 1.90 2.800(3) yes N21 H211 O145 2_546 129 0.91 2.45 3.103(3) yes N21 H212 O48 . 173 0.91 1.96 2.859(3) yes N21 H212 C142 . 166 0.91 2.25 3.134(3) yes N21 H212 O143 . 137 0.91 2.56 3.280(3) yes N21 H212 C144 . 143 0.91 1.96 2.742(3) yes N121 H213 O146 . 123 0.95 2.20 2.830(3) yes