#------------------------------------------------------------------------------ #$Date: 2018-03-13 05:52:49 +0200 (Tue, 13 Mar 2018) $ #$Revision: 206914 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/54/90/1549063.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1549063 loop_ _publ_author_name 'Nievergelt, Philipp P.' 'Babor, Martin' 'Cejka, Jan' 'Spingler, Bernhard' _publ_section_title ; A high throughput screening method for the nano-crystallization of salts of organic cations ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/C8SC00783G _journal_year 2018 _chemical_formula_sum 'C19 H23 Cl I N5 O' _chemical_formula_weight 499.77 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2014/7 _audit_update_record ; 2017-11-15 deposited with the CCDC. 2018-03-06 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 109.8430(12) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.9279(2) _cell_length_b 12.54570(15) _cell_length_c 13.13900(15) _cell_measurement_reflns_used 9061 _cell_measurement_temperature 160(2) _cell_measurement_theta_max 34.060 _cell_measurement_theta_min 3.631 _cell_volume 2004.48(5) _computing_cell_refinement 'CrysAlis PRO (Rigaku, 2015)' _computing_data_collection 'CrysAlis PRO (Rigaku, 2015)' _computing_data_reduction 'CrysAlis PRO (Rigaku, 2015)' _computing_molecular_graphics 'ORTEP-3 (Farrugia, 1997)' _computing_publication_material 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SIR-97 (Altomare, 1999)' _diffrn_ambient_temperature 160(2) _diffrn_detector_area_resol_mean 10.3801 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'Agilent SuperNova dual radiation CCD' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator mirror _diffrn_radiation_source 'SuperNova (Mo) X-ray Source' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0340 _diffrn_reflns_av_unetI/netI 0.0389 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 27961 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 33.727 _diffrn_reflns_theta_min 3.248 _exptl_absorpt_coefficient_mu 1.750 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.64878 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43c (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.656 _exptl_crystal_description plate _exptl_crystal_F_000 1000 _exptl_crystal_recrystallization_method 'Vapour diffusion' _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.070 _exptl_crystal_size_min 0.040 _refine_diff_density_max 0.712 _refine_diff_density_min -0.452 _refine_diff_density_rms 0.095 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.025 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 244 _refine_ls_number_reflns 7970 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.025 _refine_ls_R_factor_all 0.0527 _refine_ls_R_factor_gt 0.0336 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0260P)^2^+0.5517P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0626 _refine_ls_wR_factor_ref 0.0684 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6177 _reflns_number_total 7970 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file c8sc00783g2.cif _cod_data_source_block PN220716_10444_A3_D3_Mo _cod_database_code 1549063 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.721 _shelx_estimated_absorpt_t_max 0.933 _shelx_res_file ; PN220716_10444_A3_D3_Mo.res created by SHELXL-2014/7 TITL PN220716_10444_A3_D3_MO_A.RES IN P2(1)/C CELL 0.71073 12.92790 12.54570 13.13900 90.00000 109.84300 90.00000 ZERR 4 0.00020 0.00015 0.00015 0.00000 0.00120 0.00000 LATT 1 SYMM -X, Y+ 0.50000, -Z+ 0.50000 SFAC C H CL I N O UNIT 76 92 4 4 20 4 LIST 4 ! automatically inserted. Change 6 to 4 for CHECKCIF!! TEMP -113 PLAN 30 HTAB FMAP 2 SHEL 100 0.64 L.S. 4 SIZE 0.04 0.07 0.20 BOND $H CONF ACTA REM COLOURLESS PLATE REM OLD TITL PN220716_10444_A3_D3_MO IN P21/C #14 REM SHELXT SOLUTION IN P2(1)/C REM R1 0.114, RWEAK 0.005, ALPHA 0.034, ORIENTATION AS INPUT REM FORMULA FOUND BY SHELXT: C19 N5 O2 CL26 REM REM REM WGHT 0.026000 0.551700 FVAR 0.34347 C1 1 0.981207 0.819483 0.802687 11.00000 0.01921 0.02889 = 0.02924 -0.00816 0.00897 -0.00216 C4 1 1.210434 0.657031 0.805942 11.00000 0.02493 0.02863 = 0.03240 -0.00469 0.01161 0.00022 AFIX 43 H4 2 1.245721 0.637967 0.755841 11.00000 -1.20000 AFIX 0 C5 1 1.248090 0.620292 0.908746 11.00000 0.02391 0.02229 = 0.03882 0.00049 0.00050 0.00096 AFIX 43 H5A 2 1.310755 0.575091 0.930836 11.00000 -1.20000 AFIX 0 C6 1 1.196016 0.647797 0.984370 11.00000 0.03371 0.03251 = 0.02258 0.00607 -0.00080 -0.01215 AFIX 43 H6 2 1.223062 0.619384 1.055574 11.00000 -1.20000 AFIX 0 C7 1 1.109383 0.713211 0.956481 11.00000 0.02727 0.03901 = 0.01958 -0.00421 0.00910 -0.01259 AFIX 43 H7A 2 1.075210 0.733069 1.007262 11.00000 -1.20000 AFIX 0 C9 1 1.116922 0.724768 0.774614 11.00000 0.02134 0.02372 = 0.01992 -0.00132 0.00724 -0.00271 C11 1 0.909525 0.894762 0.616682 11.00000 0.02234 0.02729 = 0.03850 0.00756 0.00156 -0.00119 AFIX 23 H11A 2 0.948582 0.917471 0.567272 11.00000 -1.20000 H11B 2 0.892852 0.959539 0.651281 11.00000 -1.20000 AFIX 0 C12 1 0.801439 0.841347 0.550267 11.00000 0.02171 0.02846 = 0.03258 0.00655 0.00205 -0.00179 AFIX 23 H12A 2 0.758119 0.890514 0.492602 11.00000 -1.20000 H12B 2 0.817177 0.776361 0.515339 11.00000 -1.20000 AFIX 0 C13 1 0.735428 0.811955 0.621286 11.00000 0.01853 0.02423 = 0.02756 0.00286 0.00028 -0.00153 AFIX 23 H13A 2 0.772552 0.751946 0.668523 11.00000 -1.20000 H13B 2 0.735508 0.873382 0.668611 11.00000 -1.20000 AFIX 0 C15 1 0.567703 0.739186 0.640903 11.00000 0.02158 0.02189 = 0.02059 -0.00012 0.00501 0.00107 AFIX 23 H15A 2 0.608497 0.675267 0.677483 11.00000 -1.20000 H15B 2 0.573514 0.794048 0.696736 11.00000 -1.20000 AFIX 0 C16 1 0.448956 0.710869 0.585350 11.00000 0.01959 0.02319 = 0.02410 -0.00403 0.00758 -0.00006 AFIX 23 H16A 2 0.417863 0.683035 0.639330 11.00000 -1.20000 H16B 2 0.407344 0.775739 0.552545 11.00000 -1.20000 AFIX 0 C18 1 0.486557 0.664909 0.422531 11.00000 0.02285 0.02496 = 0.02174 -0.00085 0.00800 -0.00588 AFIX 23 H18A 2 0.444427 0.725782 0.380558 11.00000 -1.20000 H18B 2 0.482666 0.605862 0.371376 11.00000 -1.20000 AFIX 0 C19 1 0.605722 0.697803 0.476305 11.00000 0.02217 0.02178 = 0.02434 -0.00182 0.00830 -0.00250 AFIX 23 H19A 2 0.649911 0.634402 0.509501 11.00000 -1.20000 H19B 2 0.634432 0.726036 0.420744 11.00000 -1.20000 AFIX 0 C20 1 0.334396 0.578605 0.461276 11.00000 0.01898 0.01491 = 0.02516 0.00068 0.00772 0.00033 C21 1 0.290593 0.544113 0.353596 11.00000 0.02047 0.01951 = 0.02384 0.00241 0.00693 -0.00119 AFIX 43 H21A 2 0.327113 0.560134 0.303734 11.00000 -1.20000 AFIX 0 C22 1 0.193380 0.486360 0.320688 11.00000 0.01981 0.01997 = 0.02777 0.00062 0.00334 0.00154 C23 1 0.134614 0.462814 0.387902 11.00000 0.01944 0.02322 = 0.04302 -0.00043 0.01065 -0.00248 AFIX 43 H23A 2 0.067449 0.424257 0.362573 11.00000 -1.20000 AFIX 0 C24 1 0.177902 0.497944 0.494385 11.00000 0.03029 0.02718 = 0.03982 0.00016 0.02018 -0.00336 AFIX 43 H24A 2 0.139521 0.483196 0.542947 11.00000 -1.20000 AFIX 0 C25 1 0.275811 0.553970 0.530959 11.00000 0.02982 0.02446 = 0.02967 -0.00139 0.01476 -0.00250 AFIX 43 H25A 2 0.303946 0.576178 0.604388 11.00000 -1.20000 AFIX 0 CL26 3 0.144551 0.439180 0.187856 11.00000 0.02881 0.03468 = 0.03071 -0.00382 0.00074 -0.00626 I31 4 0.516514 0.973724 0.341655 11.00000 0.02825 0.02237 = 0.02111 0.00102 0.00580 -0.00066 N2 5 0.982153 0.826168 0.700359 11.00000 0.02083 0.02840 = 0.02395 0.00044 0.00494 0.00019 N3 5 1.064336 0.768965 0.680555 11.00000 0.02225 0.03270 = 0.02431 -0.00003 0.00918 0.00216 N8 5 1.071038 0.751051 0.851790 11.00000 0.01702 0.02722 = 0.02110 -0.00176 0.00628 -0.00119 N14 5 0.618366 0.780743 0.561421 11.00000 0.01763 0.01560 = 0.02351 0.00337 0.00206 0.00043 AFIX 13 H14A 2 0.576985 0.845833 0.526080 11.00000 -1.20000 AFIX 0 N17 5 0.436509 0.630757 0.501226 11.00000 0.02093 0.01874 = 0.02121 -0.00230 0.00872 -0.00282 O10 6 0.920358 0.859174 0.845156 11.00000 0.02737 0.05372 = 0.04132 -0.01593 0.01451 0.00543 HKLF 4 REM PN220716_10444_A3_D3_MO_A.RES IN P2(1)/C REM R1 = 0.0336 for 6177 Fo > 4sig(Fo) and 0.0527 for all 7970 data REM 244 parameters refined using 0 restraints END WGHT 0.0261 0.5510 REM Instructions for potential hydrogen bonds EQIV $1 x, -y+3/2, z+1/2 HTAB C7 N3_$1 HTAB C12 I31 EQIV $2 -x+1, -y+2, -z+1 HTAB C15 I31_$2 HTAB C16 I31_$1 EQIV $3 -x+1, y-1/2, -z+1/2 HTAB C18 I31_$3 HTAB N14 I31 HTAB N14 I31_$2 REM Highest difference peak 0.712, deepest hole -0.452, 1-sigma level 0.095 Q1 1 0.9848 0.8114 0.8775 11.00000 0.05 0.71 Q2 1 0.4701 1.0151 0.3152 11.00000 0.05 0.69 Q3 1 0.4722 0.9433 0.2996 11.00000 0.05 0.64 Q4 1 0.5214 0.9306 0.3106 11.00000 0.05 0.60 Q5 1 1.0898 0.7270 0.8075 11.00000 0.05 0.57 Q6 1 1.0018 0.8132 0.6227 11.00000 0.05 0.56 Q7 1 1.2218 0.6511 0.9419 11.00000 0.05 0.54 Q8 1 0.7543 0.8824 0.7003 11.00000 0.05 0.53 Q9 1 0.1521 0.4722 0.4410 11.00000 0.05 0.52 Q10 1 0.4604 0.6442 0.4615 11.00000 0.05 0.52 Q11 1 1.1576 0.6784 0.7708 11.00000 0.05 0.51 Q12 1 0.2509 0.5088 0.3393 11.00000 0.05 0.49 Q13 1 0.5295 1.0156 0.3074 11.00000 0.05 0.49 Q14 1 0.4995 0.9447 0.3872 11.00000 0.05 0.49 Q15 1 0.1477 0.4983 0.3427 11.00000 0.05 0.46 Q16 1 0.4490 0.5243 0.4688 11.00000 0.05 0.44 Q17 1 1.0777 0.7590 0.9063 11.00000 0.05 0.42 Q18 1 0.9659 0.8111 0.7488 11.00000 0.05 0.42 Q19 1 1.0292 0.7746 0.8336 11.00000 0.05 0.40 Q20 1 0.5364 1.0069 0.4223 11.00000 0.05 0.40 Q21 1 1.0586 0.7258 0.8922 11.00000 0.05 0.40 Q22 1 0.8705 0.9278 0.7324 11.00000 0.05 0.39 Q23 1 0.3182 0.5472 0.4076 11.00000 0.05 0.39 Q24 1 0.9378 0.8572 0.7895 11.00000 0.05 0.38 Q25 1 1.1168 0.7660 0.8211 11.00000 0.05 0.38 Q26 1 0.5857 0.7512 0.5911 11.00000 0.05 0.38 Q27 1 0.2976 0.5617 0.4929 11.00000 0.05 0.37 Q28 1 1.0706 0.7165 0.7276 11.00000 0.05 0.36 Q29 1 0.0756 0.4721 0.1579 11.00000 0.05 0.36 Q30 1 1.0264 0.7905 0.7218 11.00000 0.05 0.35 ; _shelx_res_checksum 41085 _shelx_hkl_file ; 0 0 -2 94.50 2.86 0 0 -3 0.00 1.08 0 0 3 -0.40 1.08 0 0 3 -1.14 1.31 0 0 -3 -0.72 1.25 0 0 -4 2045.13 18.96 0 0 -4 2013.93 16.64 0 0 4 2021.77 18.09 0 0 -4 2035.73 18.49 0 0 4 2038.87 21.76 0 0 4 2019.24 16.33 0 0 -5 0.23 1.12 0 0 -5 -1.20 1.62 0 0 -5 1.10 1.47 0 0 5 0.30 1.18 0 0 5 0.66 1.85 0 0 5 0.70 1.57 0 0 6 6254.77 46.14 0 0 -6 6074.24 40.30 0 0 6 6122.31 34.81 0 0 -6 6155.90 39.76 0 0 6 6067.72 38.25 0 0 -6 6195.27 35.10 0 0 7 0.51 1.30 0 0 -7 0.03 1.28 0 0 7 0.29 1.63 0 0 -7 0.37 1.66 0 0 -7 -0.95 1.71 0 0 7 0.78 1.99 0 0 -8 292.11 8.99 0 0 -8 299.62 10.25 0 0 8 289.51 8.90 0 0 -8 296.58 10.61 0 0 8 295.21 11.91 0 0 8 295.39 9.87 0 0 -9 2.61 2.48 0 0 9 -1.48 1.83 0 0 -9 -0.57 1.61 0 0 -9 0.12 2.21 0 0 -9 1.54 2.08 0 0 -10 452.89 15.09 0 0 -10 469.24 15.34 0 0 -10 454.87 12.52 0 0 -11 -0.86 2.27 0 0 -11 0.81 2.78 0 0 -11 1.01 1.92 0 0 -12 394.96 12.76 0 0 -12 398.67 15.76 0 0 -12 398.91 16.04 0 0 -13 0.98 2.20 0 0 -13 -2.16 2.85 0 0 -13 2.04 2.81 0 0 -14 3.67 3.29 0 0 -15 -0.82 3.52 0 0 -16 133.32 12.47 0 0 -16 137.73 12.03 0 0 -17 -2.24 4.27 0 0 -17 3.65 4.71 0 1 -2 94.54 3.44 0 1 -2 86.23 3.75 0 -1 2 92.26 3.75 0 1 -2 86.41 3.38 0 -1 2 85.97 3.22 0 1 -2 86.97 3.53 0 -1 2 88.69 3.49 0 -1 2 92.30 3.43 0 -1 -2 90.64 2.64 0 -1 -3 6622.87 26.75 0 -1 3 6758.39 32.94 0 -1 3 6571.42 34.35 0 1 -3 6513.15 31.64 0 -1 3 6503.42 30.50 0 -1 -3 6745.87 30.72 0 1 -3 6603.50 34.03 0 -1 -3 6727.96 23.23 0 1 -3 6560.85 35.08 0 1 -4 312.12 8.46 0 -1 -4 301.60 6.93 0 1 -4 304.43 7.72 0 1 -4 322.07 8.65 0 -1 -4 299.54 5.10 0 -1 -4 309.12 6.12 0 -1 4 305.33 8.35 0 -1 4 290.43 7.25 0 1 -5 264.41 7.83 0 -1 5 256.58 7.51 0 1 -5 248.80 8.33 0 -1 -5 266.90 5.64 0 1 5 270.23 5.87 0 -1 5 256.24 8.28 0 -1 -5 274.07 7.58 0 -1 -5 258.32 6.46 0 1 -5 267.79 8.57 0 1 -6 56.14 4.49 0 1 6 57.38 3.12 0 -1 -6 57.71 3.57 0 1 -6 64.06 4.88 0 -1 -6 66.07 4.26 0 1 -6 64.99 4.36 0 -1 -6 62.96 3.17 0 -1 6 54.86 4.48 0 -1 6 61.92 4.13 0 1 -7 263.98 8.94 0 -1 -7 269.10 6.96 0 -1 -7 263.66 8.98 0 1 7 256.56 6.93 0 -1 -7 250.51 7.77 0 1 -7 266.35 9.90 0 -1 7 254.70 9.46 0 -1 7 258.49 10.97 0 1 -7 264.86 9.93 0 -1 7 261.66 8.68 0 1 -8 129.88 7.45 0 1 -8 119.69 6.53 0 -1 -8 121.11 6.59 0 -1 -8 117.96 5.94 0 -1 -8 136.85 7.09 0 -1 8 121.35 6.36 0 -1 8 132.49 7.38 0 -1 8 125.93 8.45 0 1 8 131.93 5.39 0 -1 -8 124.94 5.24 0 1 -8 136.03 7.75 0 1 9 1144.58 16.68 0 -1 -9 1121.81 16.41 0 -1 -9 1125.39 21.41 0 -1 9 1109.71 21.71 0 1 -9 1127.64 23.00 0 -1 9 1079.70 25.21 0 -1 -9 1130.31 19.01 0 1 -9 1117.79 20.29 0 -1 -9 1137.37 21.16 0 -1 -10 1.08 1.56 0 -1 -10 -1.24 2.16 0 1 -10 -1.12 2.60 0 -1 -10 -1.78 2.40 0 -1 10 0.68 3.01 0 1 -10 0.57 1.96 0 -1 -10 1.28 1.90 0 -1 10 0.36 2.28 0 -1 -11 9.13 3.02 0 -1 -11 10.21 2.28 0 -1 -11 6.91 2.86 0 1 -11 2.60 2.73 0 1 -11 9.04 2.87 0 1 -11 7.62 3.19 0 -1 -12 1.11 2.71 0 -1 -12 3.17 1.97 0 1 -12 1.83 2.87 0 1 -12 6.76 2.91 0 -1 -12 -0.45 2.53 0 -1 -13 203.00 8.41 0 1 -13 186.27 9.90 0 1 -13 206.78 12.53 0 -1 -13 208.12 11.79 0 -1 -13 206.19 12.22 0 -1 -14 66.82 7.69 0 -1 -14 72.34 7.62 0 -1 -14 53.74 7.55 0 1 -14 70.18 6.71 0 1 -14 70.89 8.12 0 -1 -15 90.62 9.53 0 1 -15 85.89 9.22 0 -1 -15 111.24 10.38 0 1 -16 5.84 5.01 0 -1 -16 0.36 4.08 0 1 -16 -0.76 3.80 0 -1 -16 3.24 3.90 0 1 -17 11.26 4.94 0 1 -17 4.70 5.31 0 1 -18 16.52 6.01 0 1 -18 17.96 6.48 0 2 0 865.55 10.50 0 -2 0 850.56 9.65 0 -2 -1 98.67 2.94 0 2 -1 101.68 3.97 0 -2 -1 91.38 2.88 0 2 -1 97.21 3.71 0 2 1 93.05 2.88 0 -2 1 101.55 4.37 0 2 1 100.85 2.94 0 -2 -2 683.15 7.60 0 2 -2 726.77 10.92 0 -2 2 742.15 12.36 0 2 -2 719.41 11.32 0 2 2 716.75 7.25 0 2 -3 146.07 5.54 0 2 -3 152.53 6.36 0 -2 3 144.61 6.24 0 -2 3 146.42 5.65 0 -2 3 140.98 5.44 0 -2 -3 136.49 4.05 0 2 -3 138.55 5.60 0 -2 3 157.98 5.99 0 2 3 147.75 3.76 0 2 -4 1038.94 16.12 0 -2 4 1035.43 16.00 0 -2 4 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9.08 4.18 -4 9 -3 8.24 4.08 4 -9 3 8.22 4.38 -4 -9 -3 12.85 4.47 4 9 3 6.93 2.45 4 -9 4 -1.75 2.93 -4 -9 -4 2.11 3.24 4 -9 4 3.53 4.33 4 -9 4 2.61 3.98 4 9 4 -1.84 1.70 -4 9 -4 4.77 3.68 4 -9 5 12.65 5.15 4 -9 5 1.85 4.10 -4 9 -5 14.18 5.35 4 9 5 9.79 2.09 -4 -9 -5 13.10 4.44 4 -9 5 2.99 3.06 4 -9 6 186.74 12.67 4 -9 6 164.72 13.41 -4 9 -6 184.91 13.70 4 -9 6 186.78 14.32 -4 -9 -6 184.24 11.91 4 -9 7 8.90 5.34 4 -9 7 5.15 3.77 -4 -9 -7 0.75 3.19 -4 9 -7 6.33 4.05 4 -9 7 9.10 4.87 -4 9 -7 -0.43 3.65 -4 9 -8 423.00 19.83 4 -9 8 445.76 20.64 -4 -9 -8 446.06 18.90 4 -9 8 427.83 22.73 4 -9 8 422.60 22.44 -4 9 -8 471.31 22.43 4 -9 9 15.84 6.32 -4 -9 -9 2.12 4.03 -4 9 -9 4.60 5.03 4 -9 9 11.22 5.30 -4 9 -9 12.65 5.46 4 -9 9 9.24 6.01 -4 9 -10 11.53 5.34 4 -9 10 9.15 4.84 -4 9 -10 14.95 5.56 -4 9 -11 33.32 7.76 -4 9 -11 13.54 5.65 4 -9 11 18.13 6.96 -4 9 -12 84.49 11.13 -4 9 -12 106.26 12.44 4 -9 12 106.93 12.95 -4 9 -13 -3.05 5.93 -4 9 -13 1.07 5.03 -4 9 -14 57.03 10.53 -4 9 -14 61.24 10.15 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8.33 4 11 -16 27.25 10.92 4 11 -15 1.75 6.09 4 11 -15 18.31 7.63 -4 -11 15 15.83 8.42 -4 -11 14 122.63 14.88 4 11 -14 95.25 13.94 4 11 -14 114.13 13.65 -4 -11 13 14.79 6.89 4 11 -13 6.39 3.89 4 11 -13 20.97 9.23 4 11 -12 7.46 5.41 4 11 -12 -4.72 5.30 -4 -11 12 6.15 5.18 -4 -11 11 20.48 6.87 4 11 -11 26.56 6.92 4 11 -11 26.07 7.77 -4 -11 10 208.37 17.21 4 11 -10 206.84 17.16 4 11 -10 207.57 16.17 -4 -11 9 34.42 8.03 4 11 -9 35.55 7.25 4 11 -9 56.59 9.26 4 11 -8 305.46 18.13 4 11 -8 322.61 19.48 -4 -11 8 312.23 19.94 4 11 -7 12.08 5.52 4 11 -7 23.42 5.70 -4 11 7 16.89 4.79 4 -11 -7 18.06 3.73 -4 -11 7 11.76 5.91 4 -11 -6 6.03 2.92 -4 -11 6 7.28 5.03 -4 11 6 8.49 3.53 4 11 -6 16.24 5.39 4 11 -6 12.01 4.53 4 11 -5 6.77 3.71 4 -11 -5 2.94 2.65 4 11 -5 5.34 3.93 -4 -11 5 -0.95 4.53 -4 11 5 3.91 3.32 -4 11 5 5.77 1.32 -4 11 4 576.73 20.76 -4 -11 4 564.91 24.31 4 11 -4 573.26 22.09 4 -11 -4 578.81 14.51 4 11 -4 569.98 21.67 4 -11 -4 563.10 19.16 -4 11 4 556.03 11.91 -4 11 3 40.24 4.05 4 -11 -3 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11 -15 -6.70 6.65 5 11 -15 12.35 5.56 -5 -11 15 0.45 6.36 5 11 -14 89.86 12.27 5 11 -14 93.83 13.99 -5 -11 14 79.95 12.03 5 11 -13 17.73 6.81 5 11 -13 9.33 4.99 -5 -11 13 19.31 7.43 -5 -11 12 2.51 5.33 5 11 -12 -0.55 4.99 5 11 -12 -0.53 4.52 5 11 -11 8.36 5.55 -5 -11 11 16.18 6.98 5 11 -11 9.61 5.70 5 11 -10 265.41 17.96 -5 -11 10 261.54 19.53 5 11 -10 261.16 19.38 5 11 -9 45.57 8.34 5 11 -9 20.32 5.98 -5 -11 9 32.43 7.51 5 11 -8 151.26 13.07 5 11 -8 173.10 14.45 -5 -11 8 151.20 14.27 -5 -11 7 12.38 6.20 -5 11 7 8.72 4.30 5 11 -7 11.57 4.94 5 11 -7 14.97 5.97 -5 -11 6 130.41 13.30 5 11 -6 147.65 12.05 5 11 -6 141.19 12.20 5 -11 -6 124.96 8.66 -5 11 6 133.80 10.51 5 11 -5 32.52 6.66 -5 11 5 26.11 2.41 5 11 -5 31.99 6.47 -5 -11 5 31.18 7.25 -5 11 5 22.88 5.13 5 -11 -5 30.10 5.14 -5 -11 4 695.91 27.47 5 11 -4 627.82 22.93 5 11 -4 636.15 22.84 -5 11 4 654.52 13.89 5 -11 -4 624.33 20.70 -5 11 4 653.38 22.93 5 -11 -3 24.27 5.16 -5 11 3 24.28 3.65 -5 11 3 18.99 5.30 -5 -11 3 21.51 6.26 5 11 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12 -11 119.69 14.03 -5 -12 10 2.81 5.84 5 12 -10 0.83 4.94 5 12 -10 -0.79 5.21 -5 -12 9 0.34 5.64 5 12 -9 8.57 5.31 5 12 -9 3.99 4.35 5 12 -8 19.11 6.24 5 12 -8 25.98 6.88 -5 -12 8 22.10 7.86 -5 12 7 344.14 16.97 5 12 -7 324.55 19.17 5 12 -7 338.87 20.02 -5 -12 7 325.62 21.13 -5 12 6 173.47 12.47 5 12 -6 181.09 13.91 5 12 -6 161.71 13.25 5 -12 -6 187.54 11.10 -5 -12 6 170.71 15.25 -5 -12 5 201.25 16.16 -5 12 5 190.63 13.09 5 12 -5 189.09 14.03 5 12 -5 192.64 13.64 5 -12 -5 183.43 11.72 -5 12 4 2.68 2.06 5 -12 -4 6.07 3.92 5 12 -4 2.43 3.56 -5 12 4 1.20 4.17 -5 -12 4 8.13 5.25 5 12 -4 -2.40 3.74 -5 12 3 266.93 15.78 5 12 -3 283.82 15.94 5 12 -3 280.35 14.91 5 -12 -3 282.65 15.22 -5 -12 3 275.66 18.21 -5 12 3 296.42 10.96 5 -12 -2 215.73 11.67 -5 12 2 219.99 14.68 -5 -12 2 200.74 15.33 5 12 -2 198.64 13.17 5 12 -2 201.96 11.97 5 -12 -2 195.58 13.28 -5 12 2 193.25 9.71 5 -12 -1 602.40 20.34 5 12 -1 624.76 19.29 -5 12 1 579.31 23.70 5 12 -1 596.82 21.50 -5 -12 1 562.99 24.72 5 -12 -1 568.82 22.98 -5 12 1 617.49 18.09 -5 12 0 147.70 9.58 5 -12 0 168.16 11.66 5 12 0 156.49 10.79 -5 -12 0 166.97 13.83 -5 12 0 153.33 12.91 5 -12 0 162.27 13.12 5 12 1 17.90 4.36 5 -12 1 17.26 5.20 -5 12 -1 16.79 4.02 5 -12 1 16.60 4.90 -5 -12 -1 25.03 6.28 -5 12 -1 22.33 6.15 5 12 1 23.98 3.59 5 -12 2 8.58 5.34 5 -12 2 0.70 3.66 -5 12 -2 -1.74 2.86 -5 12 -2 7.71 4.55 5 12 2 4.59 3.45 -5 -12 -2 0.16 3.70 -5 12 -3 325.88 16.15 5 -12 3 294.91 17.72 5 -12 3 328.12 19.95 -5 12 -3 325.63 19.51 5 12 3 311.94 13.16 -5 -12 -3 323.36 18.02 5 -12 4 56.32 9.15 5 -12 4 53.44 8.66 -5 12 -4 52.39 7.30 5 12 4 54.45 5.67 -5 12 -4 44.83 8.46 -5 -12 -4 65.17 8.86 -5 -12 -5 433.98 20.11 -5 12 -5 456.92 20.64 5 -12 5 494.63 24.63 -5 12 -5 438.16 23.67 5 -12 5 443.08 24.11 5 -12 6 40.95 8.73 -5 12 -6 38.63 7.14 5 -12 6 38.87 8.32 -5 -12 -6 40.65 6.89 -5 12 -6 48.17 9.00 -5 12 -7 16.34 5.98 5 -12 7 18.05 7.20 -5 12 -7 23.01 7.47 -5 -12 -7 18.32 4.82 5 -12 7 22.83 7.49 -5 12 -8 -1.07 4.13 -5 12 -8 -2.93 4.96 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158.59 9.36 7 -9 1 148.48 12.14 -7 9 -1 149.64 10.41 -7 9 -2 605.53 24.27 7 -9 2 646.41 22.84 -7 -9 -2 626.01 25.15 7 9 2 599.97 16.84 7 -9 2 624.58 24.60 -7 9 -2 624.71 21.57 7 9 2 712.43 16.59 -7 9 -3 45.28 6.77 -7 -9 -3 41.85 7.59 7 -9 3 27.33 5.45 7 -9 3 35.54 7.00 -7 9 -3 33.16 6.91 7 9 3 36.39 4.46 -7 9 -4 27.43 6.07 7 -9 4 18.81 5.26 -7 9 -4 26.01 6.75 -7 -9 -4 18.47 5.81 7 9 4 14.98 2.89 7 -9 4 18.82 6.34 -7 9 -5 18.65 5.49 7 -9 5 19.85 5.64 -7 9 -5 14.72 5.90 -7 -9 -5 10.37 5.53 7 -9 6 259.99 16.66 -7 9 -6 237.84 16.77 -7 -9 -6 257.11 17.30 -7 9 -6 236.98 15.93 -7 9 -7 4.55 4.82 7 -9 7 -3.84 4.62 -7 9 -7 5.81 4.27 -7 -9 -7 5.27 4.88 7 -9 8 209.43 15.59 -7 -9 -8 180.14 15.07 -7 9 -8 200.66 16.09 -7 9 -8 202.16 16.15 -7 9 -9 1.44 4.90 7 -9 9 3.63 4.66 -7 9 -9 14.84 6.63 -7 -9 -9 -6.21 6.53 -7 9 -10 17.21 6.87 7 -9 10 17.52 5.75 -7 9 -10 8.07 5.43 -7 9 -11 32.48 8.15 7 -9 11 26.11 7.23 -7 9 -11 31.69 8.49 -7 9 -12 118.58 15.03 7 -9 12 130.40 13.94 -7 9 -12 119.56 13.47 -7 9 -13 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6.61 -7 -12 15 1.33 5.70 -7 -12 14 2.73 6.05 7 12 -14 6.74 5.79 7 12 -14 3.54 7.05 -7 -12 13 102.51 14.15 7 12 -13 106.65 13.82 7 12 -13 105.41 14.34 7 12 -12 20.79 7.92 -7 -12 12 3.27 5.62 7 12 -12 16.49 7.21 7 12 -11 101.40 12.79 -7 -12 11 80.82 12.58 7 12 -11 98.46 13.05 7 12 -10 -3.93 5.91 7 12 -10 -4.32 5.09 -7 -12 10 -1.14 5.93 -7 -12 9 49.60 10.40 7 12 -9 46.95 9.07 7 12 -9 56.73 9.48 -7 -12 8 15.97 6.72 7 12 -8 17.32 5.95 7 12 -8 23.26 6.91 -7 -12 7 575.91 28.46 7 12 -7 484.92 23.25 7 12 -7 538.63 25.06 -7 12 7 535.51 23.07 -7 -12 6 14.76 6.77 -7 12 6 18.04 5.59 7 12 -6 7.46 4.74 7 12 -6 7.46 4.72 -7 12 5 133.49 12.32 -7 -12 5 145.46 14.35 7 12 -5 131.10 11.72 7 12 -5 144.51 12.31 -7 12 4 7.96 4.74 7 12 -4 15.92 5.45 7 12 -4 19.16 5.04 -7 -12 4 14.41 6.19 -7 12 4 11.16 3.01 7 -12 -3 51.18 6.92 -7 -12 3 56.52 9.31 -7 12 3 53.06 8.32 7 12 -3 43.91 7.30 7 12 -3 50.03 6.81 7 -12 -3 44.65 6.90 -7 12 3 50.26 5.56 7 -12 -2 225.86 13.71 7 12 -2 223.43 13.97 7 -12 -2 217.53 14.54 7 12 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183.80 10.75 8 6 -7 879.35 26.28 8 6 -7 813.47 26.05 -8 6 7 889.54 17.09 8 6 -6 151.87 10.88 -8 6 6 152.40 7.81 8 6 -6 163.65 11.43 -8 6 5 240.40 10.16 8 6 -5 229.52 12.92 8 6 -5 214.08 11.93 -8 6 4 12.27 4.64 8 6 -4 10.51 3.40 -8 6 4 12.60 3.46 8 6 -4 14.91 4.20 -8 -6 3 389.03 19.04 -8 6 3 375.07 13.82 8 6 -3 370.10 15.08 -8 6 3 365.92 16.73 -8 -6 2 632.01 24.13 -8 6 2 616.82 21.65 -8 6 2 640.24 18.60 8 6 -2 612.56 18.59 -8 6 1 601.13 21.60 -8 -6 1 583.88 23.13 -8 6 1 578.30 18.57 8 6 -1 572.94 17.33 -8 -6 0 147.61 12.18 -8 6 0 136.38 10.78 -8 6 0 149.05 10.15 8 6 0 130.59 8.22 -8 -6 -1 39.92 6.49 -8 6 -1 63.19 7.95 -8 6 -1 58.91 6.79 -8 6 -2 78.01 8.78 -8 -6 -2 68.65 8.81 -8 6 -2 76.72 8.12 -8 6 -3 71.53 8.67 -8 -6 -3 66.03 8.82 -8 6 -3 86.04 8.80 -8 6 -4 582.55 22.96 -8 -6 -4 565.96 24.04 -8 6 -4 578.50 22.36 -8 6 -5 245.63 15.35 -8 -6 -5 258.41 16.69 -8 6 -5 250.26 15.49 -8 6 -6 14.86 5.73 -8 6 -6 15.88 5.28 -8 -6 -6 15.16 6.27 -8 6 -7 -2.69 3.96 8 -6 7 3.58 4.24 -8 6 -7 1.76 4.36 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8 -7 -11 153.23 10.19 8 7 -10 1007.06 32.55 -8 -7 10 1033.69 32.46 8 7 -10 1061.05 34.11 8 -7 -10 1060.10 25.86 8 -7 -9 3.41 1.88 8 7 -9 4.68 4.64 -8 -7 9 6.17 4.70 8 7 -9 2.38 3.77 8 7 -8 434.80 19.81 8 7 -8 431.88 20.42 -8 7 7 128.03 6.16 8 7 -7 136.79 11.23 8 7 -7 133.89 11.33 -8 7 6 360.71 11.39 8 7 -6 374.76 17.49 -8 7 5 280.22 15.29 -8 7 5 302.11 11.19 8 7 -5 282.56 14.69 -8 7 4 633.87 22.48 -8 7 4 643.03 16.99 8 7 -4 618.17 20.58 -8 -7 3 18.20 5.42 -8 7 3 20.49 3.95 8 7 -3 17.59 4.08 -8 7 3 18.62 5.47 -8 -7 2 98.45 10.66 -8 7 2 121.51 10.46 -8 7 2 126.86 8.84 8 7 -2 113.48 8.46 -8 -7 1 100.41 10.55 -8 7 1 88.96 9.20 -8 7 1 90.97 7.72 8 7 -1 108.55 7.91 -8 -7 0 184.92 13.88 -8 7 0 197.03 13.33 -8 7 0 186.63 11.36 8 7 0 184.87 9.67 -8 7 -1 128.87 11.23 -8 -7 -1 117.18 11.23 -8 7 -1 112.21 9.30 -8 7 -2 273.39 16.00 -8 -7 -2 289.81 17.37 -8 7 -2 284.75 14.96 -8 7 -3 59.89 7.61 -8 -7 -3 64.54 8.93 -8 7 -3 59.48 8.38 -8 7 -4 0.72 4.16 -8 7 -4 1.44 3.84 -8 -7 -4 3.90 4.34 -8 7 -5 40.26 7.28 8 -7 5 21.86 5.35 -8 -7 -5 21.39 6.48 -8 7 -5 37.58 7.37 8 -7 6 178.24 13.42 -8 7 -6 156.37 13.20 -8 -7 -6 155.22 13.51 -8 7 -6 154.10 13.15 8 -7 7 164.06 13.33 -8 7 -7 162.27 13.87 -8 -7 -7 181.78 15.18 -8 7 -7 181.97 14.86 8 -7 8 136.89 12.62 -8 7 -8 132.66 12.87 -8 -7 -8 159.32 14.77 -8 7 -8 135.77 13.45 -8 7 -9 19.32 6.50 8 -7 9 24.79 6.98 -8 7 -9 19.75 6.58 -8 -7 -9 22.12 6.75 -8 7 -10 63.51 10.71 8 -7 10 46.39 8.27 -8 7 -10 50.79 8.84 -8 -7 -10 54.01 9.45 8 -7 11 1.01 4.76 -8 7 -11 4.91 5.64 -8 -7 -11 1.95 6.03 -8 7 -11 18.76 7.67 8 -7 12 147.68 14.31 -8 7 -12 127.75 13.61 -8 7 -12 136.87 15.77 8 -7 13 26.75 6.85 -8 7 -13 3.37 6.41 8 -7 14 17.26 7.13 8 8 -19 42.48 9.84 8 8 -18 25.40 7.14 8 8 -18 13.95 7.07 8 8 -17 57.32 10.27 8 8 -17 44.17 10.26 -8 -8 17 40.85 9.25 -8 -8 16 34.95 8.40 8 8 -16 35.02 8.48 8 8 -16 25.99 8.47 -8 -8 15 4.80 4.72 8 8 -15 0.35 5.07 8 8 -15 4.11 6.37 -8 -8 14 16.47 6.32 8 8 -14 2.12 4.66 8 8 -14 4.95 5.10 8 8 -13 176.48 15.21 8 8 -13 203.29 17.54 -8 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60.68 11.33 8 9 -13 27.70 7.66 8 9 -13 35.07 8.98 -8 -9 13 41.15 9.16 -8 -9 12 -1.07 4.57 8 9 -12 -2.24 5.00 8 9 -12 5.06 4.77 -8 -9 11 8.03 5.39 8 9 -11 1.00 4.58 8 9 -11 -0.70 4.72 -8 -9 10 417.59 23.16 8 9 -10 423.11 21.57 8 9 -10 392.99 22.18 -8 -9 9 20.22 7.13 8 9 -9 10.96 5.15 8 9 -9 3.72 4.47 -8 -9 8 73.00 10.06 8 -9 -8 57.08 4.99 8 9 -8 61.37 8.48 8 9 -8 73.90 9.95 8 -9 -7 26.17 4.14 -8 -9 7 31.93 7.51 8 9 -7 24.72 5.99 8 9 -7 49.14 7.34 8 -9 -6 227.80 10.83 -8 9 6 219.64 14.27 -8 9 6 223.88 8.46 8 9 -6 223.17 14.44 8 -9 -5 10.66 3.46 -8 9 5 15.64 5.09 -8 9 5 16.60 3.19 8 9 -5 25.42 5.40 8 -9 -4 507.44 17.51 -8 9 4 500.58 21.25 -8 9 4 517.09 15.53 8 9 -4 527.13 20.14 8 -9 -3 86.89 7.93 -8 9 3 76.76 9.37 -8 9 3 75.99 6.60 8 9 -3 66.56 7.41 8 -9 -2 61.10 7.01 -8 9 2 50.13 7.90 8 9 -2 55.59 6.59 -8 9 2 55.78 6.27 8 -9 -1 31.97 5.85 -8 9 1 37.44 7.04 8 9 -1 41.70 5.26 -8 9 1 38.30 5.58 8 -9 0 584.65 21.50 -8 -9 0 594.35 25.61 -8 9 0 588.59 24.22 -8 9 0 567.43 20.21 8 9 0 614.96 18.06 8 -9 1 144.12 11.44 -8 9 -1 135.79 12.35 8 9 1 139.64 9.10 -8 9 -1 170.42 11.72 -8 -9 -1 141.53 13.22 8 -9 2 383.03 18.47 -8 -9 -2 411.39 21.71 -8 9 -2 394.47 20.51 8 9 2 370.50 13.82 -8 9 -2 391.03 18.20 -8 9 -3 6.84 3.56 8 -9 3 7.67 4.67 -8 9 -3 11.00 4.98 -8 -9 -3 6.95 5.05 8 9 3 -0.42 2.23 -8 9 -4 -4.74 4.41 8 -9 4 0.48 3.75 -8 9 -4 1.35 4.42 -8 -9 -4 -2.61 5.28 8 9 4 -0.78 2.09 -8 9 -5 64.77 9.35 8 -9 5 60.21 8.54 -8 -9 -5 56.65 9.29 -8 9 -5 60.10 9.13 8 -9 6 328.13 19.03 -8 -9 -6 307.72 19.79 -8 9 -6 336.36 20.32 -8 9 -6 311.13 18.92 -8 9 -7 8.43 5.52 8 -9 7 8.77 5.35 -8 9 -7 12.60 5.48 -8 -9 -7 5.89 5.20 8 -9 8 146.55 13.85 -8 9 -8 148.74 14.29 -8 -9 -8 172.48 15.78 -8 9 -8 180.46 15.99 -8 9 -9 5.39 5.21 8 -9 9 -3.38 5.04 -8 9 -9 3.66 5.24 -8 -9 -9 -3.67 5.21 -8 9 -10 16.23 7.11 8 -9 10 12.56 6.76 -8 9 -10 15.18 6.73 -8 9 -11 1.65 6.26 8 -9 11 19.99 7.16 -8 9 -11 13.72 6.04 8 -9 12 110.86 13.44 -8 9 -12 101.28 13.03 -8 9 -12 96.43 14.06 8 10 -17 81.49 13.16 8 10 -17 82.05 14.21 -8 -10 17 92.48 13.48 8 10 -16 6.07 6.12 8 10 -16 4.65 6.77 -8 -10 16 0.50 5.82 -8 -10 15 3.57 5.80 8 10 -15 2.62 5.04 8 10 -15 2.40 5.38 -8 -10 14 21.07 7.27 8 10 -14 21.66 7.64 8 10 -14 23.37 7.87 8 10 -13 141.16 14.52 -8 -10 13 97.16 13.20 8 10 -13 113.78 14.10 8 10 -12 30.62 8.14 8 10 -12 43.56 9.14 -8 -10 12 21.88 7.22 -8 -10 11 47.59 9.32 8 10 -11 45.74 8.91 8 10 -11 38.16 8.84 8 10 -10 -2.99 4.33 -8 -10 10 8.48 6.29 8 10 -10 6.96 4.97 8 10 -9 30.70 7.43 8 10 -9 38.48 7.73 -8 -10 9 24.78 7.82 -8 -10 8 36.72 8.12 8 10 -8 43.76 7.33 8 10 -8 44.28 7.96 8 -10 -7 277.67 11.60 8 10 -7 288.31 17.18 8 10 -7 300.63 17.98 -8 -10 7 290.35 19.02 8 -10 -6 12.94 3.43 -8 10 6 13.60 5.31 -8 -10 6 15.15 6.42 8 10 -6 9.65 4.26 8 10 -6 16.11 5.52 8 -10 -5 127.61 9.09 -8 10 5 132.18 11.46 -8 10 5 127.47 7.47 8 10 -5 109.15 10.30 8 10 -5 140.45 11.28 8 -10 -4 2.86 3.26 -8 10 4 -0.31 4.16 8 10 -4 2.40 3.51 -8 10 4 1.95 2.32 8 10 -4 2.17 3.23 8 -10 -3 412.44 16.96 -8 10 3 400.43 19.94 8 10 -3 413.94 18.25 -8 10 3 425.13 15.13 8 10 -3 400.50 17.23 8 -10 -2 9.65 4.28 -8 10 2 17.29 5.85 8 10 -2 8.50 3.90 8 10 -2 13.22 4.13 -8 10 2 7.38 3.26 8 -10 -1 562.25 20.96 -8 10 1 571.10 24.47 8 10 -1 523.16 19.27 -8 10 1 567.59 19.53 8 10 -1 558.70 18.42 -8 10 0 6.37 3.60 8 -10 0 5.14 3.69 -8 10 0 7.13 4.89 8 10 0 5.37 3.64 8 10 0 13.83 3.95 -8 10 -1 69.46 8.02 8 -10 1 57.44 7.84 -8 10 -1 48.34 8.15 -8 -10 -1 74.13 10.24 8 10 1 66.53 6.77 8 10 1 68.03 6.09 -8 10 -2 1.43 3.57 8 -10 2 5.68 4.28 -8 10 -2 4.71 4.45 8 10 2 11.12 3.51 -8 -10 -2 12.01 5.70 8 -10 3 394.81 19.80 -8 -10 -3 398.17 22.12 -8 10 -3 390.38 21.59 8 10 3 393.76 13.66 -8 10 -3 405.08 19.50 -8 10 -4 4.75 4.05 8 -10 4 -3.44 4.51 -8 -10 -4 -2.25 4.71 -8 10 -4 3.66 4.92 8 -10 5 305.57 18.43 -8 -10 -5 276.76 19.00 -8 10 -5 265.73 18.57 -8 10 -5 285.10 17.86 -8 10 -6 19.30 6.20 8 -10 6 14.59 5.38 -8 10 -6 14.83 5.97 -8 -10 -6 26.15 7.54 -8 10 -7 23.85 6.95 8 -10 7 38.81 8.08 -8 10 -7 19.30 6.25 -8 -10 -7 22.31 6.83 -8 10 -8 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125.55 14.21 -9 8 -9 136.01 15.19 9 -8 10 -1.44 5.84 -9 8 -10 -5.06 6.20 -9 -8 -10 3.14 6.22 -9 8 -10 -3.72 5.79 9 -8 11 73.38 10.94 -9 8 -11 65.22 10.81 -9 8 -11 72.43 12.19 9 -8 12 11.66 7.11 9 9 -18 9.16 6.82 9 9 -17 -15.02 6.58 9 9 -17 11.99 6.88 -9 -9 17 -2.79 5.32 -9 -9 16 132.56 14.80 9 9 -16 145.37 15.43 9 9 -16 129.05 16.21 -9 -9 15 -3.24 5.27 9 9 -15 1.57 5.13 9 9 -15 1.82 5.52 9 9 -14 81.77 11.48 -9 -9 14 91.36 12.88 9 9 -14 82.47 13.18 -9 -9 13 23.89 7.56 9 9 -13 11.94 4.51 9 9 -13 25.06 8.05 -9 -9 12 5.49 5.46 9 9 -12 0.85 4.60 9 9 -12 6.61 5.43 9 9 -11 3.41 4.32 9 9 -11 -3.60 5.43 -9 -9 11 -0.58 4.73 -9 -9 10 238.56 18.18 9 9 -10 243.92 16.61 9 9 -10 259.82 18.46 9 -9 -9 92.06 6.15 -9 -9 9 110.56 12.63 9 9 -9 105.72 11.98 9 -9 -8 303.17 11.85 9 9 -8 298.12 18.38 -9 -9 8 313.85 19.51 9 -9 -7 14.02 3.54 9 9 -7 20.79 6.35 9 -9 -6 90.66 7.56 -9 9 6 94.36 6.71 9 9 -6 101.99 10.26 9 -9 -5 5.64 3.43 -9 9 5 7.39 5.03 -9 9 5 2.67 2.86 9 9 -5 0.79 3.05 9 -9 -4 377.48 16.23 -9 9 4 336.99 18.60 -9 9 4 351.45 14.16 9 9 -4 354.33 17.00 9 -9 -3 0.05 3.24 -9 9 3 3.02 4.75 -9 9 3 3.54 3.01 9 9 -3 -2.23 3.18 9 -9 -2 128.37 10.33 -9 9 2 113.54 11.43 -9 9 2 145.84 10.30 9 9 -2 134.31 10.11 9 -9 -1 79.59 8.81 -9 -9 1 78.30 10.29 -9 9 1 82.15 9.91 -9 9 1 78.17 8.03 9 9 -1 78.51 7.37 9 -9 0 265.62 15.54 -9 -9 0 298.12 19.34 -9 9 0 265.94 17.25 -9 9 0 252.40 14.19 9 9 0 281.85 12.92 9 9 1 7.84 3.39 9 -9 1 -0.12 3.64 -9 -9 -1 -4.36 5.26 -9 9 -1 3.90 5.00 -9 9 -1 4.63 4.53 9 -9 2 276.18 16.77 -9 -9 -2 266.54 18.59 -9 9 -2 275.59 18.03 -9 9 -2 284.44 16.45 9 -9 3 12.20 5.73 -9 9 -3 6.43 4.96 -9 -9 -3 5.48 4.68 9 9 3 3.19 2.43 -9 9 -3 13.42 5.51 9 -9 4 10.31 5.33 -9 9 -4 1.17 5.40 -9 -9 -4 17.24 6.87 -9 9 -4 -3.14 4.81 -9 9 -5 7.33 4.64 9 -9 5 8.89 5.21 -9 9 -5 28.47 7.62 -9 -9 -5 16.12 6.84 9 -9 6 326.34 19.87 -9 -9 -6 292.05 20.64 -9 9 -6 348.01 21.52 -9 9 -6 277.21 27.05 -9 9 -7 16.89 6.58 9 -9 7 18.88 7.05 -9 9 -7 22.07 7.13 -9 -9 -7 16.68 7.15 9 -9 8 83.06 10.97 -9 9 -8 70.79 11.01 -9 -9 -8 67.44 11.06 -9 9 -8 62.46 10.54 9 -9 9 -2.66 4.47 -9 9 -9 -0.26 5.38 -9 -9 -9 -8.25 7.02 -9 9 -9 1.67 5.35 9 -9 10 47.25 9.53 -9 9 -10 45.04 9.55 -9 9 -10 42.74 10.02 9 -9 11 -9.94 6.43 -9 9 -11 -9.54 7.69 -9 9 -11 -4.97 6.04 9 10 -17 45.84 10.00 -9 -10 17 38.43 9.75 -9 -10 16 18.08 8.63 9 10 -16 12.34 7.25 9 10 -16 15.36 5.70 -9 -10 15 1.20 5.64 9 10 -15 6.34 6.79 9 10 -15 7.10 6.72 9 10 -14 -5.73 5.90 -9 -10 14 0.71 6.08 9 10 -14 3.33 5.16 9 10 -13 192.83 17.07 9 10 -13 191.41 17.99 -9 -10 13 180.26 17.54 -9 -10 12 -2.72 6.03 9 10 -12 6.51 5.95 9 10 -12 12.51 7.41 -9 -10 11 145.79 15.05 9 10 -11 130.08 13.47 9 10 -11 169.29 16.09 9 10 -10 -0.60 4.64 9 10 -10 -4.33 4.96 -9 -10 10 2.08 5.45 -9 -10 9 125.70 13.37 9 10 -9 163.65 14.26 9 10 -9 131.66 13.15 9 -10 -8 56.11 5.89 -9 -10 8 52.04 9.47 9 10 -8 56.68 8.42 9 10 -8 49.11 8.29 -9 -10 7 246.56 17.94 9 -10 -7 241.23 11.73 9 10 -7 260.86 16.60 9 10 -7 251.48 16.57 9 -10 -6 11.20 3.54 -9 10 6 11.61 4.85 9 10 -6 25.74 6.71 9 10 -6 15.72 5.30 9 -10 -5 80.20 7.76 -9 10 5 77.21 9.48 -9 10 5 71.49 6.25 9 10 -5 76.38 9.16 9 10 -5 83.38 9.04 9 -10 -4 0.63 3.02 -9 10 4 1.56 4.42 -9 10 4 0.53 2.67 9 10 -4 4.73 3.81 9 -10 -3 169.49 11.64 -9 10 3 195.16 14.87 -9 10 3 174.43 10.74 9 10 -3 179.26 12.02 9 -10 -2 39.24 6.35 -9 10 2 26.78 6.78 9 10 -2 38.61 6.31 -9 10 2 33.46 5.55 9 10 -2 47.92 6.59 9 -10 -1 134.40 11.21 -9 10 1 116.65 12.21 9 10 -1 121.01 9.91 -9 10 1 113.49 9.62 9 10 -1 119.89 9.13 9 -10 0 2.94 4.12 -9 -10 0 10.98 6.44 -9 10 0 5.87 4.43 9 10 0 7.96 3.45 -9 10 0 2.62 3.95 9 10 0 8.45 3.39 9 10 1 16.24 3.92 9 -10 1 9.64 4.64 -9 -10 -1 10.68 5.86 -9 10 -1 4.40 5.06 9 10 1 6.34 3.26 -9 10 -1 9.03 4.29 9 -10 2 -0.05 4.11 -9 -10 -2 6.07 4.63 -9 10 -2 10.04 5.78 9 10 2 5.47 2.87 -9 10 -2 12.52 4.47 9 -10 3 156.45 13.30 -9 -10 -3 179.18 16.04 -9 10 -3 150.46 14.41 9 10 3 167.81 9.51 -9 10 -3 155.58 12.91 -9 10 -4 39.65 7.60 9 -10 4 40.76 7.83 -9 -10 -4 28.02 7.84 -9 10 -4 32.12 8.54 9 -10 5 235.22 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3 189.06 11.56 10 6 -3 188.40 11.89 -10 6 2 275.17 16.53 -10 -6 2 254.88 17.33 -10 6 2 247.46 13.77 10 6 -2 259.84 13.44 -10 6 1 447.34 20.79 -10 -6 1 417.62 21.78 -10 6 1 412.05 18.02 10 6 -1 426.43 16.68 -10 6 0 369.49 19.18 -10 -6 0 350.11 19.98 -10 6 0 369.85 17.69 10 6 0 357.47 15.19 -10 -6 -1 78.36 10.23 -10 6 -1 82.99 9.64 -10 6 -1 81.88 9.04 -10 6 -2 15.24 5.56 -10 -6 -2 9.66 4.89 -10 6 -2 22.80 5.89 -10 6 -3 245.32 16.21 -10 -6 -3 226.01 17.21 -10 6 -3 235.75 15.85 -10 6 -4 144.18 12.70 -10 -6 -4 136.90 13.66 -10 6 -4 111.08 11.97 -10 6 -5 65.93 9.22 -10 -6 -5 76.40 10.69 -10 6 -5 74.63 10.49 -10 6 -6 27.31 7.03 -10 -6 -6 32.39 8.46 -10 6 -6 34.68 8.06 -10 6 -7 111.00 12.15 -10 -6 -7 77.57 11.51 -10 6 -7 101.80 12.86 10 -6 8 -6.82 5.09 -10 6 -8 3.18 4.19 -10 -6 -8 -2.70 5.19 -10 6 -8 -4.75 5.89 10 -6 9 139.45 13.46 -10 -6 -9 125.06 14.74 -10 6 -9 144.31 15.75 -10 6 -9 117.80 12.61 10 -6 10 11.38 5.36 -10 6 -10 30.76 8.12 -10 -6 -10 19.99 7.09 -10 6 -10 22.66 8.73 10 -6 11 11.11 5.79 -10 -6 -11 26.08 8.66 -10 6 -11 0.26 5.90 10 -6 12 -9.26 6.48 -10 -6 -12 -24.98 8.35 10 7 -19 -2.11 5.31 10 7 -18 -6.56 7.20 10 7 -18 -0.03 6.46 10 7 -17 -4.02 5.93 10 7 -17 13.38 7.75 -10 -7 16 63.46 10.65 10 7 -16 66.92 10.60 10 7 -16 72.84 12.45 10 7 -15 -3.73 5.84 10 7 -15 -8.73 6.03 10 7 -15 9.18 7.35 -10 -7 15 2.28 4.54 10 7 -14 107.80 13.73 10 7 -14 147.64 14.28 10 7 -14 131.89 14.77 10 -7 -14 112.42 10.33 -10 -7 14 114.95 13.15 10 -7 -13 8.20 4.18 10 7 -13 6.37 5.62 -10 -7 13 12.13 6.27 10 7 -13 -2.10 5.52 10 -7 -12 45.56 6.72 -10 -7 12 39.66 8.40 10 7 -12 47.72 9.24 10 7 -12 48.26 9.07 10 -7 -11 43.53 6.53 -10 -7 11 52.92 8.72 10 7 -11 34.78 6.76 10 7 -11 48.90 8.55 -10 -7 10 334.33 19.84 10 7 -10 353.28 20.11 10 7 -10 339.46 20.28 10 7 -9 26.96 5.86 10 7 -9 28.48 6.80 -10 7 8 88.81 6.63 10 7 -8 83.49 9.80 10 7 -8 82.92 9.76 10 7 -7 0.07 3.83 -10 7 7 0.38 2.95 10 7 -7 1.82 4.09 10 7 -6 123.22 10.59 -10 7 6 112.70 8.32 10 7 -6 130.57 11.11 -10 7 5 192.37 11.10 10 7 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7.09 -10 8 -10 -5.55 6.13 10 -8 11 28.57 7.89 -10 8 -11 13.17 6.68 -10 -9 17 -4.11 5.23 10 9 -17 1.38 7.00 10 9 -17 10.64 6.47 -10 -9 16 49.10 10.45 10 9 -16 64.41 11.58 10 9 -16 47.27 10.36 10 9 -15 -11.10 7.14 -10 -9 15 -0.02 5.03 10 9 -15 12.99 7.86 -10 -9 14 64.76 11.06 10 9 -14 64.74 10.66 10 9 -14 78.99 12.45 -10 -9 13 2.69 5.94 10 9 -13 -4.95 5.15 10 9 -13 3.33 6.19 10 9 -12 84.95 11.38 -10 -9 12 86.75 12.55 10 9 -12 82.31 11.53 -10 -9 11 1.27 5.98 10 9 -11 7.32 5.31 10 9 -11 11.88 6.23 -10 -9 10 141.43 14.25 10 9 -10 166.40 15.07 10 -9 -9 32.91 4.49 -10 -9 9 30.99 8.55 10 9 -9 28.01 7.20 10 -9 -8 44.87 5.42 10 9 -8 27.21 6.84 10 -9 -7 9.84 3.69 10 9 -7 2.51 3.81 10 -9 -6 210.58 12.09 -10 9 6 205.35 10.74 10 9 -6 206.55 14.35 -10 9 5 3.56 5.13 -10 9 5 0.91 3.21 10 9 -5 -0.13 3.44 -10 9 4 349.78 19.85 -10 9 4 327.92 14.68 10 9 -4 337.68 16.98 -10 9 3 6.55 5.40 -10 9 3 10.06 4.04 10 9 -3 8.86 3.61 -10 -9 2 2.31 4.88 -10 9 2 -3.00 4.74 -10 9 2 1.22 3.36 10 9 -2 -0.44 3.00 -10 9 1 12.64 5.95 -10 -9 1 1.99 5.80 -10 9 1 7.34 4.10 10 9 -1 7.37 3.31 -10 -9 0 184.48 16.17 -10 9 0 206.62 15.98 -10 9 0 171.57 12.83 10 9 0 182.42 11.11 10 9 1 29.02 5.11 10 -9 1 6.88 4.62 -10 9 -1 24.69 7.34 -10 -9 -1 23.72 6.79 -10 9 -1 20.20 6.12 10 -9 2 341.52 19.29 -10 -9 -2 328.13 21.71 -10 9 -2 291.67 19.13 -10 9 -2 287.06 17.52 10 -9 3 33.47 7.09 -10 9 -3 34.85 8.65 -10 -9 -3 21.77 7.34 -10 9 -3 22.72 6.40 10 -9 4 6.80 4.70 -10 9 -4 11.15 6.83 -10 -9 -4 4.08 5.28 -10 9 -4 5.45 5.15 10 -9 5 3.60 4.71 -10 9 -5 1.91 5.66 -10 -9 -5 -1.26 5.22 -10 9 -5 1.28 4.65 10 -9 6 188.49 15.64 -10 9 -6 184.89 16.60 -10 -9 -6 188.86 17.89 -10 9 -6 187.82 16.63 10 -9 7 9.99 5.47 -10 9 -7 2.03 5.70 -10 -9 -7 2.71 6.13 -10 9 -7 3.78 5.62 10 -9 8 93.34 12.08 -10 9 -8 89.23 12.85 -10 -9 -8 80.29 12.70 -10 9 -8 83.49 12.29 10 -9 9 0.14 4.67 -10 9 -9 6.44 5.67 -10 -9 -9 -2.55 7.04 -10 9 -9 -2.76 5.38 10 -9 10 10.44 5.96 -10 9 -10 -0.06 6.49 -10 9 -10 -3.88 6.47 -10 9 -11 -0.42 4.72 -10 -10 17 40.55 9.15 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-1.11 3.03 10 -10 -1 411.65 19.85 -10 10 1 459.00 23.89 -10 10 1 412.89 18.98 10 10 -1 448.77 17.69 10 -10 0 1.50 4.00 -10 -10 0 4.37 5.50 -10 10 0 -1.36 5.03 -10 10 0 2.45 3.60 10 10 0 -2.13 3.09 10 10 1 -1.89 3.48 10 -10 1 -0.74 4.08 -10 -10 -1 9.52 6.11 -10 10 -1 2.88 5.37 10 10 1 -2.24 3.66 -10 10 -1 8.45 4.61 10 -10 2 23.07 6.39 -10 10 -2 21.99 7.59 -10 -10 -2 38.04 8.83 10 10 2 18.87 4.38 -10 10 -2 33.38 7.19 10 -10 3 114.03 12.28 -10 10 -3 103.05 12.56 -10 -10 -3 88.69 12.28 -10 10 -3 89.44 10.49 10 -10 4 6.61 5.67 -10 -10 -4 2.12 5.27 -10 10 -4 -5.19 5.40 10 -10 5 82.20 11.32 -10 10 -5 96.19 12.77 -10 -10 -5 99.61 13.73 -10 10 -5 86.04 11.20 10 -10 6 11.07 5.12 -10 10 -6 17.41 6.97 -10 -10 -6 3.98 5.86 -10 10 -6 7.61 5.07 10 -10 7 7.47 5.58 -10 10 -7 3.12 5.23 -10 -10 -7 -6.33 6.94 10 -10 8 2.63 5.04 -10 10 -8 0.33 6.16 -10 -10 -8 -3.52 6.42 -10 10 -8 11.05 6.52 10 -10 9 68.03 10.96 -10 10 -9 74.43 11.68 -10 10 -9 85.54 12.90 10 -10 10 0.80 4.89 -10 10 -10 4.69 5.91 -10 -11 17 25.57 10.29 -10 -11 16 62.93 11.83 -10 -11 15 -2.26 5.19 10 11 -15 -1.90 6.21 10 11 -15 -2.88 6.07 10 11 -14 57.14 10.84 -10 -11 14 61.25 11.42 10 11 -14 83.64 13.12 -10 -11 13 -3.53 6.35 10 11 -13 -1.00 5.04 10 11 -13 3.01 5.80 -10 -11 12 26.82 8.34 10 11 -12 34.30 8.60 10 11 -12 47.58 10.33 10 11 -11 8.89 5.91 -10 -11 11 10.96 6.11 10 11 -11 23.50 7.69 -10 -11 10 173.66 17.19 10 11 -10 156.13 15.15 10 11 -10 180.32 16.32 -10 -11 9 9.71 6.20 10 11 -9 10.09 6.49 10 11 -9 6.17 6.04 -10 -11 8 68.17 11.37 10 11 -8 65.44 10.23 10 11 -8 62.11 9.51 10 -11 -7 -4.46 3.57 -10 -11 7 8.49 5.76 10 11 -7 -0.73 5.34 10 11 -7 -1.52 5.03 10 -11 -6 238.36 13.24 10 11 -6 265.97 17.60 10 11 -6 254.00 16.71 10 -11 -5 12.81 3.90 -10 11 5 12.16 6.20 10 11 -5 15.35 5.55 10 11 -5 16.30 5.30 10 -11 -4 285.39 15.65 -10 11 4 267.88 18.39 -10 11 4 277.09 13.74 10 11 -4 259.69 16.55 10 11 -4 271.89 16.01 10 -11 -3 2.79 3.94 -10 11 3 -0.81 5.36 10 11 -3 3.40 4.48 -10 11 3 7.47 3.93 10 11 -3 7.05 3.70 10 -11 -2 13.74 5.61 -10 11 2 13.33 6.21 10 11 -2 9.89 4.01 -10 11 2 16.12 5.13 10 11 -2 12.39 4.40 10 -11 -1 16.39 5.47 -10 11 1 5.94 5.25 10 11 -1 6.80 3.97 -10 11 1 6.52 4.68 10 11 -1 8.32 3.77 10 -11 0 408.82 20.86 -10 11 0 430.57 24.05 10 11 0 402.40 18.09 -10 11 0 403.24 19.69 10 11 0 445.89 17.31 10 -11 1 19.77 6.38 -10 -11 -1 25.38 8.85 -10 11 -1 16.98 7.12 10 11 1 22.49 4.85 -10 11 -1 20.99 5.98 10 -11 2 178.40 14.91 -10 -11 -2 174.80 16.97 -10 11 -2 179.05 16.91 -10 11 -2 163.63 13.61 10 -11 3 0.48 4.59 -10 11 -3 1.77 5.50 -10 -11 -3 6.34 5.65 -10 11 -3 4.02 4.85 10 -11 4 14.92 5.84 -10 -11 -4 1.16 5.72 -10 11 -4 16.81 7.37 -10 11 -4 7.25 5.00 10 -11 5 5.99 5.44 -10 11 -5 -0.48 6.43 -10 -11 -5 10.15 7.17 -10 11 -5 0.48 5.33 10 -11 6 84.10 11.66 -10 11 -6 81.53 12.36 -10 -11 -6 102.14 14.08 -10 11 -6 70.88 11.11 10 -11 7 -11.96 7.15 -10 11 -7 -10.57 7.10 -10 -11 -7 -3.06 7.16 -10 11 -7 8.71 6.27 10 -11 8 63.80 11.06 -10 11 -8 44.93 10.47 -10 11 -8 61.35 11.05 10 -11 9 36.41 9.28 -10 11 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2.60 5.69 -11 -11 14 61.90 11.77 11 11 -14 62.74 12.27 11 11 -14 71.72 12.68 -11 -11 13 1.82 5.84 11 11 -13 -3.19 5.93 11 11 -13 -4.36 6.08 11 11 -12 50.04 9.55 -11 -11 12 57.99 11.28 11 11 -12 61.68 10.88 11 11 -11 12.14 7.17 11 11 -11 2.82 5.07 -11 -11 11 -7.78 7.84 -11 -11 10 37.73 8.77 11 11 -10 41.23 8.76 11 11 -10 46.27 9.01 -11 -11 9 11.82 6.17 11 11 -9 22.38 7.78 11 11 -9 13.39 5.71 -11 -11 8 18.33 8.18 11 11 -8 17.62 7.25 11 11 -8 16.43 6.38 11 -11 -7 4.09 3.29 -11 -11 7 8.14 6.60 11 11 -7 -1.83 4.06 11 11 -7 1.44 4.66 11 -11 -6 54.55 7.31 11 11 -6 69.83 10.17 11 11 -6 59.17 8.94 11 -11 -5 22.68 5.61 -11 11 5 38.53 8.12 11 11 -5 45.55 7.64 11 11 -5 35.90 7.11 11 -11 -4 164.71 12.71 -11 11 4 144.01 13.95 -11 11 4 148.41 11.08 11 11 -4 181.59 14.30 11 11 -4 166.05 12.89 11 -11 -3 17.61 5.78 -11 11 3 14.69 7.29 11 11 -3 23.88 6.24 -11 11 3 10.84 4.14 11 11 -3 24.13 6.01 11 -11 -2 -3.97 4.48 -11 11 2 7.06 6.28 11 11 -2 -1.43 3.65 -11 11 2 1.25 3.72 11 11 -2 -0.51 3.02 11 -11 -1 7.06 5.30 -11 11 1 8.69 7.23 11 11 -1 -4.49 3.77 -11 11 1 2.16 4.25 11 11 -1 3.23 4.15 11 -11 0 282.62 18.30 -11 11 0 273.00 20.12 11 11 0 295.72 16.07 -11 11 0 248.01 16.66 11 -11 1 16.72 6.24 -11 -11 -1 19.29 8.17 -11 11 -1 30.31 8.82 11 11 1 21.43 5.14 -11 11 -1 17.73 6.49 11 -11 2 85.14 11.08 -11 -11 -2 105.88 14.06 -11 11 -2 108.42 13.97 -11 11 -2 79.96 10.93 11 -11 3 25.47 7.19 -11 11 -3 29.39 8.68 -11 -11 -3 18.19 8.26 -11 11 -3 23.97 7.92 11 -11 4 40.27 8.76 -11 11 -4 35.63 8.96 -11 -11 -4 57.49 11.93 -11 11 -4 35.90 8.65 11 -11 5 11.87 6.41 -11 11 -5 -6.48 5.94 -11 -11 -5 3.30 6.13 -11 11 -5 2.85 5.52 11 -11 6 216.94 18.45 -11 -11 -6 212.47 20.34 -11 11 -6 185.88 18.37 -11 11 -6 200.42 18.31 -11 11 -7 4.80 5.99 -11 -11 -7 8.01 6.06 -11 11 -7 -4.32 5.44 -11 11 -8 40.21 10.66 -11 11 -8 17.92 8.16 -11 -12 15 4.09 6.32 11 12 -14 14.99 6.33 11 12 -14 31.76 10.54 -11 -12 14 7.75 6.31 -11 -12 13 78.42 14.27 11 12 -13 79.35 12.53 11 12 -13 79.92 12.92 -11 -12 12 -2.42 7.29 11 12 -12 13.76 8.06 11 12 -12 0.48 5.27 11 12 -11 10.43 7.32 -11 -12 11 4.56 7.31 11 12 -11 -0.66 5.51 -11 -12 10 13.35 5.70 11 12 -10 14.03 5.74 11 12 -10 13.87 6.73 -11 -12 9 5.61 6.43 11 12 -9 1.28 4.76 11 12 -9 4.75 4.87 -11 -12 8 -0.24 5.75 11 12 -8 -0.35 4.53 11 12 -8 2.52 5.41 11 12 -7 56.86 9.57 -11 -12 7 60.15 10.81 11 12 -7 46.82 8.57 11 -12 -6 11.32 4.31 11 12 -6 13.67 5.92 -11 -12 6 1.71 5.03 11 12 -6 11.98 6.04 11 -12 -5 -2.65 3.50 -11 12 5 4.69 5.64 11 12 -5 -1.20 4.86 11 12 -5 -0.95 4.09 11 -12 -4 5.24 3.93 -11 12 4 17.31 7.35 11 12 -4 6.43 5.30 11 12 -4 8.37 4.54 11 -12 -3 42.42 7.78 -11 12 3 38.47 8.86 11 12 -3 47.89 8.03 11 12 -3 32.00 6.49 11 -12 -2 18.73 6.36 -11 12 2 25.77 8.21 11 12 -2 16.73 5.29 -11 12 2 36.06 7.10 11 12 -2 26.07 5.22 11 -12 -1 66.46 9.46 -11 12 1 75.52 11.85 11 12 -1 66.98 8.83 -11 12 1 53.31 8.19 11 -12 0 12.42 5.41 -11 12 0 16.20 7.13 11 12 0 3.19 3.61 -11 12 0 5.70 4.94 -11 12 -1 -1.76 5.81 -11 12 -1 0.67 4.91 11 -12 2 1.77 5.12 -11 12 -2 1.72 7.20 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9.08 12 5 -9 77.02 9.73 12 -5 -8 35.35 6.45 -12 5 8 30.28 5.69 12 5 -8 31.87 7.16 12 5 -8 30.53 6.35 -12 5 7 -1.22 3.50 12 5 -7 1.83 4.40 12 5 -7 7.09 4.24 -12 -5 6 97.03 11.58 -12 5 6 100.63 9.46 12 5 -6 104.89 9.67 12 5 -6 114.48 10.69 -12 -5 5 189.18 16.15 12 5 -5 161.66 11.36 -12 5 5 167.86 12.09 12 5 -5 173.93 12.58 12 5 -4 105.46 8.97 -12 -5 4 107.07 12.35 -12 5 4 105.04 10.00 12 5 -4 105.30 9.86 -12 -5 3 56.44 9.85 -12 5 3 85.65 9.50 12 5 -3 60.75 6.68 12 5 -3 77.44 8.72 12 5 -2 27.28 5.33 -12 -5 2 28.74 7.34 12 5 -2 23.42 4.29 -12 5 2 17.98 5.53 -12 -5 1 117.83 12.90 -12 5 1 134.73 12.20 12 5 -1 127.02 10.48 -12 -5 0 380.21 22.74 -12 5 0 408.36 21.13 -12 -5 -1 179.43 15.99 -12 5 -1 161.75 14.21 -12 -5 -2 98.04 12.22 -12 5 -2 113.68 12.40 -12 5 -3 -0.27 4.74 -12 -5 -3 -2.95 6.26 -12 5 -3 1.10 5.20 -12 -5 -4 22.22 7.13 -12 5 -4 26.56 7.61 -12 5 -4 39.54 8.47 -12 -5 -5 45.70 9.66 -12 5 -5 63.93 10.46 -12 5 -5 45.97 9.31 -12 5 -6 28.87 7.60 -12 -5 -6 20.74 7.42 -12 5 -6 35.43 8.51 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156.52 13.32 12 6 -7 207.47 14.60 -12 6 7 233.27 13.69 12 6 -7 233.55 15.43 12 6 -6 35.71 6.82 -12 6 6 46.44 7.15 12 6 -6 44.11 7.69 -12 -6 5 6.61 5.89 12 6 -5 -3.56 3.29 -12 6 5 -0.85 3.71 12 6 -5 2.60 4.01 -12 -6 4 8.08 6.60 12 6 -4 5.01 3.19 -12 6 4 9.89 4.81 12 6 -4 2.68 3.85 12 6 -3 349.09 15.04 -12 -6 3 378.23 23.00 -12 6 3 326.27 17.41 12 6 -3 336.39 17.01 -12 -6 2 71.05 10.64 -12 6 2 82.34 9.74 12 6 -2 82.43 8.69 -12 -6 1 170.51 15.85 -12 6 1 178.66 13.91 12 6 -1 176.77 12.18 -12 -6 0 6.52 5.69 -12 6 0 6.69 4.72 -12 6 -1 40.73 7.89 -12 -6 -1 23.58 6.86 -12 6 -1 30.29 6.77 -12 6 -2 20.93 6.41 -12 -6 -2 6.54 5.21 -12 6 -2 13.90 4.93 -12 6 -3 288.03 19.47 -12 -6 -3 294.38 21.21 -12 6 -3 268.26 19.00 -12 6 -4 17.42 6.79 -12 -6 -4 14.68 6.85 -12 6 -4 7.33 5.32 -12 6 -5 156.87 15.19 -12 -6 -5 148.83 16.05 -12 6 -5 177.50 16.78 -12 6 -6 5.68 5.19 -12 -6 -6 13.82 7.92 -12 6 -6 7.37 6.30 -12 6 -7 15.02 6.89 -12 -6 -7 1.93 5.83 -12 6 -7 4.88 6.27 12 -6 8 58.20 9.73 -12 6 -8 56.02 10.12 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242.29 20.18 -12 8 -3 223.13 18.06 -12 8 -4 6.05 5.44 -12 -8 -4 4.76 5.96 -12 8 -4 21.59 7.54 12 -8 5 38.79 8.28 -12 8 -5 36.73 9.21 -12 -8 -5 43.89 10.12 -12 8 -5 22.19 7.18 12 -8 6 -12.53 6.28 -12 8 -6 -1.98 5.61 -12 -8 -6 -0.67 5.77 -12 8 -6 -1.60 5.70 12 -8 7 52.97 9.90 -12 8 -7 66.65 10.98 -12 -8 -7 57.33 11.47 -12 8 -7 60.64 11.11 12 -8 8 -3.80 5.92 -12 8 -8 -1.45 5.32 -12 -8 -8 -7.43 6.88 -12 8 -8 -6.46 6.21 12 -8 9 127.63 14.81 -12 8 -9 90.64 13.27 -12 -8 -9 67.21 12.33 -12 -9 17 2.85 5.06 12 9 -16 73.84 12.19 12 9 -16 72.12 12.54 -12 -9 16 60.85 10.80 -12 -9 15 7.84 7.21 12 9 -15 5.63 6.47 12 9 -15 5.23 6.88 -12 -9 14 37.76 9.63 12 9 -14 37.40 9.29 12 9 -14 44.93 9.93 12 9 -13 5.92 6.44 12 9 -13 4.91 5.47 -12 -9 13 -4.56 6.92 -12 -9 12 45.24 10.05 12 9 -12 46.72 10.13 -12 -9 11 49.04 10.49 12 9 -11 40.67 8.55 -12 -9 10 125.17 14.37 12 9 -10 112.54 12.88 12 9 -9 19.46 5.71 12 9 -8 42.69 8.12 12 9 -7 6.29 4.97 -12 9 6 60.98 7.22 12 9 -6 72.24 9.35 -12 9 5 -0.14 3.63 12 9 -5 2.36 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13 -4 -18 54.48 8.97 13 4 -17 13.00 6.94 13 4 -17 5.78 6.77 13 -4 -17 1.59 4.61 13 4 -16 7.18 6.68 13 4 -16 -4.21 5.37 13 -4 -16 10.72 5.85 -13 -4 15 40.97 8.12 13 4 -15 37.64 9.23 13 4 -15 22.57 7.73 13 -4 -15 35.67 7.49 13 4 -14 100.80 12.63 -13 -4 14 126.10 12.51 13 4 -14 107.32 13.16 13 -4 -14 109.53 11.86 13 4 -13 57.10 9.76 13 4 -13 60.49 10.05 13 -4 -13 59.08 9.03 13 4 -12 126.57 13.29 13 4 -12 102.91 12.07 13 -4 -12 124.50 12.00 13 -4 -11 38.83 7.25 13 4 -11 28.10 6.94 13 4 -11 24.45 6.48 13 -4 -10 2.64 4.20 13 4 -10 0.62 4.22 13 4 -10 -0.74 5.59 13 -4 -9 31.87 6.80 -13 4 9 33.25 6.55 13 4 -9 26.85 6.22 13 4 -9 37.27 7.91 -13 4 8 141.46 11.89 13 4 -8 128.75 11.48 13 4 -8 140.87 12.64 13 -4 -8 126.51 11.63 13 -4 -7 35.84 6.98 -13 -4 7 39.73 8.56 -13 4 7 34.43 7.15 13 4 -7 33.29 6.36 13 4 -7 23.23 6.28 -13 -4 6 159.19 15.17 -13 4 6 201.35 14.07 13 4 -6 180.59 12.60 13 4 -6 203.55 14.47 -13 -4 5 36.57 8.72 -13 4 5 12.86 4.86 13 4 -5 17.81 5.04 13 4 -5 28.98 6.48 -13 -4 4 24.40 7.69 -13 4 4 19.14 5.91 13 4 -4 22.67 4.71 13 4 -4 22.16 5.62 13 4 -3 8.60 4.17 -13 -4 3 12.75 6.29 13 4 -3 4.35 3.34 -13 4 3 6.87 4.41 -13 -4 2 488.30 25.78 13 4 -2 503.57 16.64 -13 4 2 472.39 22.62 13 4 -2 478.08 20.92 13 4 -1 23.43 3.93 -13 -4 1 27.53 7.53 -13 4 1 27.83 7.16 -13 -4 0 12.32 6.22 -13 4 0 10.08 5.72 -13 -4 -1 69.69 10.97 -13 4 -1 70.05 10.42 -13 -4 -2 98.34 13.12 -13 4 -2 89.76 12.19 -13 -4 -3 37.21 9.42 -13 4 -3 45.33 9.51 -13 -4 -4 84.12 12.29 -13 4 -4 90.27 12.40 -13 -4 -5 5.70 5.73 -13 4 -5 1.85 6.00 -13 -4 -6 12.44 6.69 -13 4 -6 3.30 6.70 -13 -4 -7 84.83 12.96 -13 4 -7 98.17 14.55 -13 -4 -8 59.65 11.74 -13 4 -8 49.86 10.88 -13 -4 -9 44.55 10.89 -13 4 -9 38.07 10.60 13 -4 10 -4.63 6.35 -13 -4 -10 8.66 6.46 13 5 -18 6.47 6.69 13 5 -17 12.67 6.11 13 5 -17 14.16 6.97 13 -5 -17 13.03 5.92 13 5 -16 200.17 18.54 13 5 -16 194.48 18.53 13 -5 -16 206.58 16.41 -13 -5 15 99.62 12.06 13 5 -15 111.81 14.07 13 5 -15 96.30 12.99 13 -5 -15 103.81 11.84 13 -5 -14 17.10 5.98 13 5 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9.36 -13 -5 -1 151.59 15.66 -13 5 -1 172.75 15.36 -13 -5 -2 7.23 5.85 -13 5 -2 15.92 6.78 -13 -5 -3 -3.99 6.04 -13 5 -3 6.46 5.41 -13 -5 -4 131.82 15.09 -13 5 -4 113.31 13.64 -13 -5 -5 49.19 10.89 -13 5 -5 59.33 10.99 -13 -5 -6 43.76 10.12 -13 5 -6 10.78 7.27 -13 -5 -7 18.30 7.72 -13 5 -7 13.36 6.42 -13 -5 -8 -10.19 8.28 -13 5 -8 17.18 9.18 13 -5 9 2.65 5.63 -13 -5 -9 -2.20 6.20 -13 5 -9 2.39 6.66 13 6 -18 15.23 7.31 13 6 -17 19.16 8.55 13 6 -17 -3.98 6.31 13 -6 -16 33.15 7.73 -13 -6 16 24.76 7.13 13 6 -16 44.90 10.52 13 6 -16 31.27 8.27 13 -6 -15 27.02 7.02 13 6 -15 23.56 8.45 13 6 -15 31.70 10.00 -13 -6 15 13.39 5.44 13 -6 -14 5.78 5.17 13 6 -14 17.76 7.13 -13 -6 14 15.44 5.47 13 6 -14 23.38 8.20 13 -6 -13 100.14 11.23 13 6 -13 117.17 13.97 -13 -6 13 95.56 12.12 13 6 -13 110.39 13.10 13 -6 -12 13.38 5.92 13 6 -12 11.77 5.53 13 6 -12 9.34 6.02 13 -6 -11 4.70 4.56 13 6 -11 3.26 4.72 13 6 -11 6.26 4.79 13 6 -10 28.84 7.36 13 6 -10 19.53 6.36 -13 6 9 29.43 5.52 13 6 -9 21.29 6.17 13 6 -9 20.92 6.29 -13 6 8 166.92 12.52 13 6 -8 160.26 13.75 13 6 -8 176.32 14.62 -13 6 7 281.13 16.05 13 6 -7 258.81 16.43 13 6 -7 240.37 16.30 -13 -6 6 11.63 7.26 13 6 -6 6.76 3.85 -13 6 6 11.71 5.06 13 6 -6 15.13 5.79 -13 -6 5 6.68 6.44 13 6 -5 4.58 3.96 -13 6 5 5.79 4.61 13 6 -5 13.62 4.86 -13 -6 4 40.36 9.47 13 6 -4 32.12 5.77 -13 6 4 17.32 4.66 13 6 -4 33.17 6.50 -13 -6 3 94.00 12.44 -13 6 3 108.47 11.35 13 6 -3 112.17 10.39 -13 -6 2 140.85 15.14 -13 6 2 143.25 12.85 13 6 -2 152.67 12.06 13 6 -1 55.30 7.72 -13 -6 1 72.85 11.41 -13 6 1 57.09 8.53 -13 -6 0 64.40 11.26 -13 6 0 54.84 8.89 -13 -6 -1 14.75 7.65 -13 6 -1 9.92 6.69 -13 -6 -2 55.47 10.47 -13 6 -2 53.98 9.57 -13 -6 -3 112.07 14.09 -13 6 -3 133.33 14.79 -13 -6 -4 81.82 12.73 -13 6 -4 60.46 10.83 -13 -6 -5 -4.70 5.56 -13 6 -5 2.11 6.25 -13 -6 -6 21.84 7.58 -13 6 -6 27.54 8.27 -13 -6 -7 19.78 8.19 -13 6 -7 40.71 10.79 13 -6 8 10.04 5.48 -13 -6 -8 -8.88 7.72 -13 6 -8 -0.72 6.44 13 -6 9 49.27 9.69 -13 -6 -9 42.12 10.01 13 7 -17 5.95 6.75 13 7 -17 4.61 6.99 13 7 -17 -0.18 6.78 -13 -7 16 56.27 9.92 13 7 -16 75.66 13.33 13 7 -16 82.17 13.43 13 -7 -15 6.99 5.47 13 7 -15 7.11 7.13 -13 -7 15 2.43 5.23 13 7 -15 11.15 6.78 13 -7 -14 34.80 6.96 -13 -7 14 50.93 10.45 13 7 -14 31.32 9.04 13 7 -14 34.41 8.85 -13 -7 13 20.53 7.81 13 7 -13 8.77 6.38 13 7 -13 12.97 6.94 13 7 -12 5.39 6.75 -13 -7 12 3.27 5.88 13 7 -12 1.00 4.89 13 7 -11 8.90 5.41 13 7 -11 16.28 6.50 13 7 -10 176.48 15.52 13 7 -10 215.79 16.97 13 7 -9 69.63 9.84 13 7 -9 73.87 9.80 -13 7 8 -0.94 3.87 13 7 -8 -1.02 4.60 13 7 -8 5.84 5.25 13 7 -7 29.16 7.05 -13 7 7 33.49 6.32 13 7 -7 42.03 7.64 13 7 -6 106.28 10.82 -13 7 6 106.82 10.20 13 7 -6 112.06 11.51 -13 -7 5 132.49 15.10 -13 7 5 121.26 11.15 13 7 -5 121.92 11.49 -13 -7 4 121.56 14.80 -13 7 4 113.58 11.22 13 7 -4 127.64 11.57 -13 -7 3 4.32 5.32 -13 7 3 11.62 5.09 13 7 -3 10.03 4.54 13 7 -2 36.56 6.58 -13 -7 2 48.21 10.93 -13 7 2 43.94 7.83 13 7 -1 23.72 5.48 -13 -7 1 42.34 9.99 -13 7 1 37.65 7.64 -13 -7 0 208.82 18.76 -13 7 0 221.72 16.94 -13 -7 -1 106.21 13.82 -13 7 -1 107.83 12.23 -13 7 -2 46.08 9.04 -13 -7 -2 28.26 9.65 -13 7 -2 24.49 8.11 -13 7 -3 10.28 5.31 -13 -7 -3 8.10 6.98 -13 7 -3 15.88 7.43 -13 7 -4 30.81 8.37 -13 -7 -4 19.54 7.63 -13 7 -4 31.71 8.73 -13 7 -5 17.61 8.04 -13 -7 -5 25.04 8.92 -13 7 -5 25.77 8.93 -13 7 -6 163.82 16.66 -13 -7 -6 141.62 17.15 -13 7 -6 184.65 18.93 13 -7 7 29.76 8.25 -13 7 -7 33.95 8.48 -13 -7 -7 43.50 10.08 -13 7 -7 43.84 10.22 13 -7 8 1.76 5.12 -13 -7 -8 3.35 7.32 -13 7 -8 7.29 7.45 -13 -7 -9 19.99 9.14 -13 -8 16 -5.45 5.29 13 8 -16 9.67 7.58 13 8 -16 0.91 5.69 -13 -8 15 13.23 6.97 13 8 -15 15.58 8.05 -13 -8 14 -0.71 5.05 13 8 -14 -7.11 6.54 13 8 -13 140.86 15.60 -13 -8 13 166.69 16.73 13 8 -13 179.39 17.13 13 8 -12 36.54 8.69 -13 -8 12 35.44 9.22 13 8 -12 33.27 8.38 13 8 -11 3.24 4.91 13 8 -11 -1.33 4.87 13 8 -10 43.47 8.55 13 8 -10 39.45 8.47 13 8 -9 73.94 10.44 13 8 -8 32.67 7.08 -13 8 7 84.64 8.92 13 8 -7 66.36 9.50 -13 8 6 6.94 3.63 13 8 -6 3.05 4.39 -13 8 5 16.62 5.57 13 8 -5 20.52 5.89 -13 -8 4 38.52 9.24 -13 8 4 35.50 6.99 13 8 -4 39.95 7.00 -13 -8 3 201.71 18.74 -13 8 3 174.46 13.66 13 8 -3 195.67 13.89 13 8 -2 61.76 7.97 -13 -8 2 65.43 11.50 -13 8 2 57.58 8.86 -13 -8 1 120.66 15.04 -13 8 1 97.35 12.08 13 8 -1 100.31 9.95 -13 8 0 9.33 6.70 -13 -8 0 22.14 8.96 -13 8 0 4.92 5.26 -13 8 -1 46.31 9.53 -13 -8 -1 36.12 10.34 -13 8 -1 29.07 7.40 -13 8 -2 4.03 5.41 -13 -8 -2 20.67 8.55 -13 8 -2 12.49 6.61 -13 8 -3 79.59 11.96 -13 -8 -3 83.96 13.12 -13 8 -3 94.54 12.84 -13 8 -4 4.87 6.06 -13 -8 -4 -11.16 8.88 -13 8 -4 0.97 5.80 13 -8 5 32.84 8.57 -13 8 -5 50.63 10.60 -13 -8 -5 24.25 8.60 -13 8 -5 28.65 8.39 13 -8 6 28.43 7.93 -13 8 -6 11.46 7.32 -13 -8 -6 7.81 6.40 -13 8 -6 7.96 5.62 13 -8 7 17.32 7.39 -13 8 -7 5.47 6.76 -13 -8 -7 -5.18 7.63 -13 8 -7 -11.85 8.72 -13 8 -8 -0.19 5.33 -13 -8 -8 -25.56 9.13 -13 -9 16 69.93 13.13 -13 -9 15 12.26 6.60 13 9 -15 19.63 8.05 13 9 -15 14.65 7.97 13 9 -14 23.52 7.79 -13 -9 14 12.68 7.17 13 9 -14 22.91 8.21 -13 -9 13 -3.97 5.78 13 9 -13 3.18 5.02 -13 -9 12 147.49 15.92 13 9 -12 163.76 16.40 -13 -9 11 6.04 6.37 13 9 -11 3.27 5.12 13 9 -10 154.06 15.15 13 9 -9 7.82 5.49 13 9 -8 0.72 4.06 13 9 -7 17.69 6.07 13 9 -6 285.00 18.22 -13 9 5 41.01 7.36 13 9 -5 34.05 7.00 -13 9 4 82.52 9.87 13 9 -4 67.73 8.96 -13 -9 3 7.87 7.41 -13 9 3 -0.37 3.95 13 9 -3 2.20 4.12 13 9 -2 20.61 5.26 -13 -9 2 22.75 8.51 -13 9 2 8.12 5.09 13 9 -1 10.14 4.16 -13 9 1 2.89 5.93 -13 -9 1 20.86 7.98 -13 9 1 13.79 6.15 -13 9 0 180.87 17.17 -13 -9 0 145.20 16.78 -13 9 0 144.56 14.09 -13 9 -1 9.43 6.32 -13 -9 -1 -1.72 5.81 -13 9 -1 5.74 5.72 -13 9 -2 26.37 7.68 -13 -9 -2 31.68 8.79 -13 9 -2 16.00 6.91 13 -9 3 3.31 5.02 -13 9 -3 12.89 7.04 -13 -9 -3 1.62 6.65 -13 9 -3 2.82 5.92 13 -9 4 6.94 4.79 -13 9 -4 10.77 6.44 -13 -9 -4 -0.50 7.36 -13 9 -4 13.96 6.45 13 -9 5 2.21 5.43 -13 9 -5 -3.82 5.92 -13 -9 -5 3.28 6.57 -13 9 -5 -5.33 6.77 13 -9 6 130.54 15.03 -13 9 -6 136.10 15.98 -13 -9 -6 137.03 17.76 -13 9 -6 100.56 14.76 13 -9 7 -0.45 6.19 -13 9 -7 0.69 6.08 -13 -9 -7 0.27 5.91 -13 9 -7 -5.21 7.00 -13 9 -8 5.47 6.38 -13 -9 -8 -14.45 8.39 -13 -10 16 3.92 5.35 -13 -10 15 46.71 10.19 13 10 -15 37.70 8.68 13 10 -15 34.52 9.57 -13 -10 14 7.54 6.13 13 10 -14 -8.00 7.40 13 10 -14 9.94 6.68 13 10 -13 45.61 9.59 13 10 -13 47.02 10.82 -13 -10 13 45.23 10.41 -13 -10 12 4.02 5.55 13 10 -12 3.13 5.40 13 10 -12 0.18 5.11 -13 -10 11 16.43 7.47 13 10 -11 11.42 6.46 -13 -10 10 1.44 6.66 13 10 -10 3.65 4.97 13 10 -9 77.55 10.93 13 -10 -8 -3.18 4.27 13 10 -8 3.11 4.97 13 -10 -7 256.39 15.65 13 10 -7 241.77 17.48 13 10 -6 -1.33 4.34 13 10 -5 6.25 5.25 -13 10 4 -2.93 3.99 13 10 -4 -0.31 3.82 -13 10 3 209.19 15.09 13 10 -3 216.26 14.94 13 10 -2 0.87 3.48 -13 10 2 1.03 5.71 -13 -10 2 5.28 6.95 -13 10 2 2.41 4.59 13 -10 -1 148.27 14.15 -13 -10 1 168.11 18.41 -13 10 1 156.00 16.35 -13 10 1 135.09 13.30 13 10 -1 156.48 12.36 13 -10 0 -1.85 5.67 -13 10 0 3.98 6.18 -13 -10 0 1.05 6.53 -13 10 0 9.29 6.50 13 -10 1 18.94 7.96 -13 10 -1 27.92 8.64 -13 -10 -1 21.46 9.01 -13 10 -1 22.14 7.70 13 -10 2 44.53 8.98 -13 10 -2 56.46 11.44 -13 -10 -2 30.58 8.70 -13 10 -2 62.26 10.93 13 -10 3 206.98 17.88 -13 10 -3 210.53 19.63 -13 -10 -3 244.16 22.55 -13 10 -3 202.48 18.26 13 -10 4 19.14 8.35 -13 10 -4 13.19 7.28 -13 -10 -4 14.00 8.27 -13 10 -4 12.61 7.03 13 -10 5 24.33 8.08 -13 10 -5 12.54 7.73 -13 -10 -5 21.30 8.69 -13 10 -5 32.54 9.10 13 -10 6 21.56 7.44 -13 10 -6 25.74 8.79 -13 -10 -6 29.26 10.38 -13 10 -6 51.09 11.01 -13 10 -7 11.57 7.40 -13 -10 -7 -0.31 9.10 -13 -11 15 1.58 6.69 -13 -11 14 19.44 7.98 13 11 -14 14.42 7.53 13 11 -13 9.89 8.25 -13 -11 13 19.20 8.49 13 11 -13 4.91 6.68 -13 -11 12 -1.62 7.36 13 11 -12 22.66 8.47 13 11 -12 30.63 9.63 13 11 -11 2.83 5.81 -13 -11 11 3.79 6.32 13 11 -11 -2.03 4.82 -13 -11 10 101.31 14.10 13 11 -10 117.54 13.96 13 11 -10 136.52 14.91 13 11 -9 12.94 6.33 13 11 -9 -3.68 5.38 -13 -11 9 -1.45 5.64 13 11 -8 16.79 6.53 13 -11 -7 0.49 4.61 13 11 -7 -2.57 5.39 13 -11 -6 105.49 10.85 13 11 -6 98.65 11.15 13 -11 -5 5.57 5.18 13 11 -5 0.02 4.41 13 -11 -4 90.28 10.76 13 11 -4 91.08 10.68 13 -11 -3 10.21 5.76 -13 11 3 -1.48 4.86 13 11 -3 -3.18 4.10 13 11 -2 11.48 4.94 13 -11 -2 10.78 6.44 -13 11 2 6.55 8.11 -13 11 2 12.35 5.78 13 -11 -1 1.02 5.47 -13 11 1 -0.03 5.76 -13 11 1 7.58 6.36 13 -11 0 175.40 15.87 -13 -11 0 181.67 19.32 -13 11 0 203.68 19.24 -13 11 0 169.23 15.56 13 -11 1 -3.18 5.89 -13 11 -1 2.96 6.51 -13 -11 -1 -4.05 7.49 -13 11 -1 -8.92 6.34 13 -11 2 52.29 10.13 -13 11 -2 46.41 10.44 -13 -11 -2 68.99 13.82 -13 11 -2 26.80 7.85 13 -11 3 2.44 5.64 -13 11 -3 -11.60 7.37 -13 -11 -3 6.28 8.11 -13 11 -3 2.64 6.24 13 -11 4 16.91 8.16 -13 11 -4 19.86 7.97 -13 -11 -4 17.63 9.23 -13 11 -4 10.31 6.83 13 -11 5 2.09 5.45 -13 11 -5 -7.39 6.72 -13 -11 -5 1.98 6.85 -13 11 -5 3.06 5.68 -13 -11 -6 57.09 12.77 -13 -12 13 61.33 13.11 13 12 -13 82.51 13.53 13 12 -12 -7.52 7.46 -13 -12 12 -0.55 6.67 13 12 -12 0.11 6.44 -13 -12 11 9.64 5.36 13 12 -11 -0.75 5.72 13 12 -11 5.31 5.26 13 12 -10 5.22 7.90 -13 -12 10 -4.39 6.41 13 12 -10 -2.54 5.32 -13 -12 9 103.81 15.11 13 12 -9 123.47 14.81 13 12 -9 91.16 12.14 13 12 -8 13.80 6.74 -13 -12 8 10.36 7.23 13 12 -8 6.27 4.58 13 12 -7 109.64 13.33 13 12 -7 107.65 12.18 13 -12 -6 3.84 4.05 13 12 -6 10.07 5.28 13 12 -6 8.11 5.26 13 -12 -5 1.53 4.48 13 12 -5 -0.89 4.75 13 12 -5 -1.07 4.05 13 -12 -4 3.17 4.19 13 12 -4 -10.76 5.77 13 12 -4 5.80 3.86 13 -12 -3 119.94 13.00 -13 12 3 119.35 15.44 13 12 -3 106.54 11.94 13 -12 -2 29.71 7.83 -13 12 2 33.11 9.97 13 12 -2 39.55 7.96 13 -12 -1 50.06 9.37 -13 12 1 101.65 14.37 -13 12 1 69.73 10.51 13 -12 0 17.25 7.19 -13 12 0 11.64 7.83 -13 12 0 -1.65 4.75 13 -12 1 19.24 6.57 -13 12 -1 9.37 6.76 -13 12 -1 8.25 6.74 13 -12 2 9.65 7.00 -13 -12 -2 9.95 8.56 -13 12 -2 -9.44 7.49 -13 12 -2 -0.35 6.48 13 -12 3 76.22 12.22 -13 -12 -3 50.33 12.40 -13 12 -3 62.17 12.58 -13 12 -3 55.36 10.04 -13 12 -4 0.84 6.59 -13 -12 -4 10.08 10.70 -13 12 -4 -2.20 5.52 -13 -12 -5 16.10 8.50 13 13 -12 15.51 7.33 13 13 -11 41.23 10.60 13 13 -11 58.62 10.87 -13 -13 11 40.21 10.60 -13 -13 10 33.02 10.16 13 13 -10 17.99 8.04 13 13 -10 16.56 7.02 13 13 -9 25.06 7.46 -13 -13 9 19.99 8.84 13 13 -9 22.38 7.18 -13 -13 8 -3.06 6.91 13 13 -8 12.78 6.67 13 13 -8 0.99 5.40 -13 -13 7 16.17 7.90 13 13 -7 1.64 5.62 13 13 -7 5.67 4.92 13 13 -6 63.44 11.50 -13 -13 6 71.24 12.18 13 13 -6 62.75 9.25 13 -13 -5 43.53 8.15 13 13 -5 33.43 7.72 13 13 -5 51.52 8.43 13 -13 -4 72.62 10.12 13 13 -4 73.81 10.87 13 -13 -3 9.95 6.47 -13 13 3 -7.85 7.74 13 13 -3 -0.25 5.16 13 -13 -2 43.31 8.61 -13 13 2 48.82 10.83 13 -13 -1 11.64 6.77 -13 13 1 17.69 8.58 13 -13 0 77.52 11.61 -13 13 0 76.87 12.95 13 -13 1 19.68 8.02 -13 13 -1 -1.08 6.34 -13 13 -1 11.27 7.14 13 -13 2 45.75 9.73 -13 13 -2 30.32 9.13 -13 13 -2 34.58 8.84 -13 13 -3 22.91 8.67 -13 13 -4 8.77 6.67 13 14 -11 3.17 5.43 13 14 -10 -4.07 4.88 13 14 -9 38.42 10.42 13 14 -9 34.35 8.27 -13 -14 8 70.34 14.01 13 14 -8 86.64 13.42 13 14 -8 59.93 10.38 13 14 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7.02 -14 -6 16 6.77 6.47 14 6 -16 -3.63 6.70 14 -6 -15 23.01 7.14 -14 -6 15 23.00 7.97 14 6 -15 7.96 5.56 14 6 -15 18.20 7.32 14 -6 -14 16.89 5.95 -14 -6 14 28.78 8.01 14 6 -14 44.31 10.00 14 6 -14 43.38 9.24 14 -6 -13 72.31 9.91 14 6 -13 74.53 11.56 -14 -6 13 83.17 12.00 14 6 -13 55.67 9.43 14 -6 -12 7.02 4.97 14 6 -12 8.16 5.24 14 6 -12 14.96 6.38 14 6 -11 3.46 5.72 14 6 -11 0.55 5.05 14 6 -10 -0.92 5.46 14 6 -10 4.34 4.96 14 6 -9 75.54 10.19 14 6 -9 56.14 9.18 -14 6 8 56.15 8.15 14 6 -8 61.64 9.33 14 6 -8 69.90 10.28 -14 6 7 211.14 15.01 14 6 -7 237.03 16.05 14 6 -7 213.92 16.01 -14 -6 6 22.14 7.45 14 6 -6 9.57 4.12 -14 6 6 12.02 4.86 14 6 -6 11.40 5.41 -14 -6 5 18.00 7.26 14 6 -5 14.86 4.86 -14 6 5 5.12 4.29 14 6 -5 14.07 5.39 -14 -6 4 73.87 11.99 14 6 -4 58.52 7.29 -14 6 4 61.85 9.08 14 6 -4 71.05 9.38 14 6 -3 52.47 7.76 -14 -6 3 66.21 11.42 -14 6 3 56.04 9.06 14 6 -2 5.53 4.10 -14 -6 2 2.35 5.76 -14 6 2 -3.32 4.69 -14 -6 1 101.34 13.94 -14 6 1 90.19 11.72 -14 -6 0 7.70 6.02 -14 6 0 12.83 5.84 -14 -6 -1 10.84 7.72 -14 6 -1 7.35 6.47 -14 -6 -2 17.00 7.44 -14 6 -2 11.27 6.96 -14 -6 -3 85.44 13.13 -14 6 -3 110.13 14.30 -14 -6 -4 30.03 9.06 -14 6 -4 26.56 9.59 -14 -6 -5 26.35 9.76 -14 6 -5 19.03 7.62 -14 -6 -6 30.52 9.39 -14 6 -6 5.83 6.39 -14 -6 -7 20.38 7.33 -14 6 -7 43.23 10.71 -14 -6 -8 -10.59 8.31 14 7 -16 37.57 9.52 -14 -7 16 56.15 10.58 14 7 -16 41.15 10.59 14 7 -15 16.82 8.19 14 7 -15 10.93 6.89 -14 -7 15 19.24 6.70 14 7 -14 7.71 6.12 -14 -7 14 -8.73 7.24 14 7 -14 3.29 5.26 14 7 -13 3.58 5.53 14 7 -13 0.03 4.86 -14 -7 13 -1.43 6.93 14 7 -12 50.55 10.34 14 7 -12 52.84 10.01 14 7 -11 3.59 5.78 14 7 -11 1.82 5.25 14 7 -10 200.55 16.83 14 7 -10 235.15 18.15 14 7 -9 10.99 5.04 14 7 -9 9.83 5.59 14 7 -8 1.90 4.77 14 7 -8 -4.44 5.27 14 7 -7 5.82 4.66 -14 7 7 12.12 5.58 14 7 -7 2.86 4.04 14 7 -6 161.18 12.96 -14 7 6 160.78 13.26 14 7 -6 182.23 14.77 -14 -7 5 48.36 10.23 -14 7 5 58.65 8.67 14 7 -5 51.48 8.40 -14 -7 4 318.02 23.39 -14 7 4 277.60 17.81 14 7 -4 311.14 18.35 14 7 -3 18.49 5.72 -14 -7 3 10.74 6.50 -14 7 3 15.28 5.62 14 7 -2 1.41 3.67 -14 -7 2 -0.97 6.16 -14 7 2 -1.15 4.55 -14 -7 1 34.58 10.04 -14 7 1 25.23 6.97 -14 -7 0 203.07 19.43 -14 7 0 214.46 17.42 -14 -7 -1 23.63 8.64 -14 7 -1 39.38 9.43 -14 -7 -2 39.76 9.61 -14 7 -2 59.40 10.78 -14 -7 -3 -0.70 7.24 -14 7 -3 17.17 8.52 -14 -7 -4 2.35 6.23 -14 7 -4 41.86 10.76 -14 -7 -5 63.66 12.09 -14 7 -5 82.01 13.66 -14 -7 -6 47.58 11.13 -14 7 -6 67.93 13.11 14 -7 7 6.27 6.71 -14 -7 -7 -5.67 8.66 -14 -8 16 -10.02 5.84 -14 -8 15 57.63 10.43 14 8 -15 57.91 11.12 -14 -8 14 5.11 5.03 14 8 -14 11.16 8.52 14 8 -13 171.93 17.21 -14 -8 13 163.27 17.00 14 8 -13 150.44 16.15 -14 -8 12 5.13 5.76 14 8 -12 -0.53 5.89 14 8 -12 -5.80 6.33 14 8 -11 -2.84 6.49 14 8 -11 -2.80 5.96 14 8 -10 6.55 4.89 14 8 -10 9.58 6.20 14 8 -9 213.68 17.16 14 8 -8 3.28 5.13 14 8 -7 47.34 7.88 -14 8 6 19.21 5.78 14 8 -6 12.99 5.58 -14 8 5 1.00 4.58 14 8 -5 7.76 5.15 -14 -8 4 0.68 5.92 -14 8 4 -0.96 4.41 14 8 -4 -0.52 4.10 -14 -8 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7.58 6.08 -14 -10 1 -4.09 6.85 -14 10 1 4.28 5.51 14 -10 0 111.55 13.33 -14 -10 0 141.52 17.80 -14 10 0 107.63 13.72 14 -10 1 3.46 5.77 -14 10 -1 15.97 8.01 -14 -10 -1 14.14 8.63 -14 10 -1 8.51 6.03 14 -10 2 7.07 6.43 -14 10 -2 9.07 7.32 -14 -10 -2 0.10 7.47 -14 10 -2 6.66 6.63 14 -10 3 146.94 15.85 -14 10 -3 162.02 17.81 -14 -10 -3 137.60 17.99 -14 10 -3 147.13 16.51 14 -10 4 3.58 5.34 -14 10 -4 15.40 7.79 -14 -10 -4 -2.91 6.84 -14 10 -5 5.76 6.64 -14 -10 -5 18.85 9.86 -14 10 -5 11.40 7.43 -14 -10 -6 22.26 10.68 14 11 -13 10.64 6.89 -14 -11 13 21.48 8.05 -14 -11 12 16.40 7.21 14 11 -12 36.26 9.06 14 11 -12 27.06 8.53 -14 -11 11 46.52 10.75 14 11 -11 46.83 10.03 14 11 -11 27.16 7.48 -14 -11 10 51.05 10.87 14 11 -10 21.05 9.44 14 11 -10 39.70 9.53 -14 -11 9 2.83 5.95 14 11 -9 3.44 5.47 14 11 -8 -3.45 4.76 14 -11 -7 4.53 4.77 14 11 -7 9.80 5.58 14 -11 -6 100.53 11.09 14 11 -6 82.44 10.50 14 -11 -5 11.15 5.96 14 11 -5 20.84 7.21 14 -11 -4 40.05 7.81 14 11 -4 35.94 7.46 14 -11 -3 15.58 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15 3 -7 99.83 11.56 15 3 -6 18.09 5.72 -15 -3 6 14.47 6.90 -15 3 6 11.90 6.37 15 3 -6 25.13 6.00 -15 -3 5 352.37 23.59 -15 3 5 312.37 19.72 15 3 -5 329.45 16.68 15 3 -5 302.53 18.67 15 3 -4 27.91 6.61 -15 -3 4 41.57 10.12 -15 3 4 24.20 7.09 15 3 -4 35.11 5.89 -15 -3 3 3.96 5.74 -15 3 3 17.90 7.14 15 3 -3 9.70 3.57 -15 -3 2 5.70 6.27 -15 3 2 4.17 5.01 -15 -3 1 102.84 13.70 -15 3 1 92.62 12.55 -15 -3 0 67.79 10.70 -15 3 0 95.13 13.09 -15 -3 -1 200.84 18.97 -15 3 -1 237.63 19.73 -15 -3 -2 23.74 8.73 -15 3 -2 -3.74 6.29 -15 -3 -3 -15.98 8.41 -15 3 -3 2.19 6.82 -15 -3 -4 36.87 9.80 -15 3 -4 57.06 11.39 -15 -3 -5 151.07 18.24 -15 3 -5 153.09 17.76 -15 -3 -6 78.98 14.21 -15 3 -6 62.38 12.47 -15 -3 -7 55.05 11.77 15 4 -17 16.33 8.37 15 4 -17 9.96 5.71 15 -4 -17 7.42 4.39 15 -4 -16 2.04 4.78 15 4 -16 6.81 6.43 15 4 -16 6.43 5.92 15 -4 -15 -1.50 5.71 -15 -4 15 14.96 7.13 15 4 -15 7.45 5.24 15 4 -15 -7.73 7.47 15 -4 -14 27.73 8.01 15 4 -14 20.41 7.27 15 4 -14 17.01 6.67 15 -4 -13 5.22 4.92 15 4 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33.19 5.92 -15 5 4 30.50 7.54 15 5 -3 27.73 6.34 -15 -5 3 3.68 5.90 -15 5 3 9.10 5.52 -15 -5 2 64.17 11.61 -15 5 2 68.16 10.28 -15 -5 1 52.21 11.31 -15 5 1 65.07 10.98 -15 -5 0 69.12 12.22 -15 5 0 87.90 12.41 -15 -5 -1 31.66 9.56 -15 5 -1 23.80 8.33 -15 -5 -2 22.65 8.24 -15 5 -2 37.29 10.02 -15 -5 -3 34.51 9.46 -15 5 -3 43.55 10.08 -15 -5 -4 41.30 10.55 -15 5 -4 15.15 7.96 -15 -5 -5 -12.30 9.03 -15 5 -5 5.10 6.73 -15 -5 -6 40.46 9.87 -15 5 -6 18.84 10.02 15 -6 -16 7.97 4.46 15 6 -16 -2.30 5.97 15 6 -16 -0.15 5.84 15 -6 -15 29.42 7.54 15 6 -15 52.34 11.61 -15 -6 15 57.51 9.97 15 6 -15 37.05 8.96 15 -6 -14 20.72 7.55 15 6 -14 29.11 7.45 -15 -6 14 30.85 9.40 15 6 -14 35.79 8.91 15 6 -13 43.84 9.17 15 6 -13 74.65 11.54 15 6 -12 36.63 8.82 15 6 -12 38.75 9.21 15 6 -11 0.39 5.00 15 6 -11 5.01 5.66 15 6 -10 -2.78 4.65 15 6 -10 -7.78 6.68 15 6 -9 74.51 10.69 15 6 -9 80.44 11.17 -15 6 8 122.60 12.74 15 6 -8 131.53 12.94 15 6 -8 122.62 13.04 15 6 -7 113.11 11.69 -15 6 7 106.17 11.44 15 6 -7 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3 2 3.45 6.73 -18 -3 1 12.66 8.37 -18 3 1 21.06 8.55 -18 -3 0 14.92 9.26 -18 3 0 2.78 6.69 -18 -3 -1 15.75 8.18 -18 3 -1 24.82 9.92 18 -4 -14 42.23 9.23 18 4 -14 29.27 7.60 18 4 -13 2.07 5.60 18 4 -13 24.35 8.64 18 4 -12 6.62 5.16 18 4 -12 2.17 5.62 18 4 -11 13.64 6.81 18 4 -11 8.10 6.35 18 4 -10 18.78 7.01 18 4 -10 2.67 5.14 18 4 -9 0.89 5.49 18 4 -9 5.18 5.43 18 4 -8 64.62 11.30 -18 -4 8 43.30 10.56 -18 4 8 49.02 10.46 18 4 -8 33.79 7.62 18 4 -7 1.39 4.98 -18 -4 7 -7.77 8.51 -18 4 7 14.95 7.87 18 4 -6 -2.50 4.96 -18 4 6 -3.25 5.57 -18 -4 5 7.50 6.74 -18 4 5 36.03 9.64 -18 -4 4 30.30 8.35 -18 4 4 68.51 12.37 -18 -4 3 30.94 10.25 -18 4 3 33.95 10.05 -18 -4 2 24.02 9.21 -18 4 2 11.47 6.26 -18 -4 1 10.79 8.46 -18 4 1 23.89 8.95 -18 -4 0 -9.20 9.07 -18 4 0 8.36 6.78 -18 4 -1 61.98 13.29 18 5 -13 18.72 7.70 18 5 -12 36.55 8.84 18 5 -12 48.85 9.85 18 5 -11 12.48 6.54 18 5 -11 9.13 6.08 18 5 -10 0.32 5.13 18 5 -10 4.33 5.72 18 5 -9 5.36 6.06 18 5 -9 -5.24 4.62 18 5 -8 32.17 8.86 18 5 -7 34.18 8.25 -18 -5 7 19.93 11.69 -18 5 7 24.90 7.61 18 5 -6 50.94 9.65 -18 -5 6 34.94 10.43 -18 5 6 73.18 11.92 -18 -5 5 23.16 8.89 -18 5 5 19.18 8.33 -18 -5 4 7.73 7.52 -18 5 4 12.40 6.53 -18 -5 3 -11.72 8.38 -18 5 3 -3.92 7.32 -18 -5 2 54.40 13.16 -18 5 2 49.75 10.64 -18 -5 1 25.82 11.08 -18 5 1 15.79 8.22 -18 -5 0 156.50 19.16 -18 5 0 124.00 16.58 -18 5 -1 44.11 10.93 18 6 -13 -8.39 6.57 18 6 -12 4.47 6.88 18 6 -12 1.49 5.07 18 6 -11 3.37 5.96 18 6 -11 13.24 6.85 18 6 -10 16.37 6.58 18 6 -10 30.23 8.41 18 6 -9 35.13 7.25 18 6 -9 20.40 7.25 18 6 -8 4.73 5.50 18 6 -7 -4.16 5.46 18 6 -6 -5.18 4.93 -18 -6 6 -6.49 9.35 -18 6 6 -0.08 6.29 18 6 -5 50.99 9.25 -18 -6 5 69.86 13.14 -18 6 5 54.69 10.57 -18 -6 4 15.22 7.82 -18 6 4 17.96 8.04 -18 -6 3 46.89 12.14 -18 6 3 57.56 11.45 -18 -6 2 12.81 9.26 -18 6 2 11.51 7.83 -18 -6 1 -13.77 8.33 -18 6 1 -4.60 6.77 -18 6 0 10.69 6.73 18 7 -12 68.09 12.02 18 7 -11 22.38 6.04 18 7 -11 32.52 8.41 18 7 -10 45.22 9.16 18 7 -10 41.24 9.39 18 7 -9 8.46 5.43 18 7 -8 2.78 5.30 18 7 -7 1.12 4.83 18 7 -6 42.67 9.71 18 7 -5 12.72 6.22 -18 -7 5 25.35 9.59 -18 7 5 22.48 8.53 -18 -7 4 10.10 9.50 -18 7 4 -3.57 6.17 -18 -7 3 14.81 11.08 -18 7 3 16.87 8.48 -18 -7 2 -7.22 9.39 -18 7 2 16.16 8.75 -18 7 1 -12.08 7.62 -18 7 0 5.37 7.55 18 8 -10 7.54 6.88 18 8 -9 40.21 9.90 18 8 -8 15.35 7.30 18 8 -7 66.40 11.23 18 8 -6 13.18 7.60 18 8 -5 7.20 6.55 -18 8 3 41.19 10.17 -18 8 2 -15.54 7.84 -18 8 1 -2.07 6.69 18 9 -9 42.95 9.22 18 9 -8 46.83 9.45 18 9 -7 15.27 7.14 18 9 -6 39.29 7.72 18 9 -5 21.10 6.37 18 10 -7 11.18 6.11 18 10 -6 7.91 5.14 19 0 -12 11.87 6.88 19 0 -11 7.95 5.05 19 0 -10 26.92 7.75 -19 0 9 4.47 6.20 -19 0 8 26.79 9.29 -19 0 7 5.86 7.33 -19 0 6 2.66 6.49 -19 0 5 5.55 7.38 -19 0 4 37.67 10.38 -19 0 3 4.28 7.57 -19 0 2 28.55 11.87 -19 0 1 16.19 9.52 19 1 -13 20.56 6.70 19 1 -12 -0.03 6.16 19 -1 -12 4.69 5.89 19 1 -12 1.01 4.78 19 1 -11 67.01 11.92 19 -1 -11 49.59 10.22 19 1 -11 48.41 9.25 19 1 -10 -8.67 7.56 19 1 -9 14.49 6.22 -19 -1 9 2.75 6.73 -19 1 9 6.55 5.86 -19 -1 8 4.68 6.05 -19 1 8 10.32 5.92 -19 -1 7 39.73 11.09 -19 1 7 39.61 9.56 -19 -1 6 -10.56 7.22 -19 1 6 10.14 8.73 -19 -1 5 38.29 10.02 -19 1 5 18.39 7.77 -19 -1 4 4.80 8.13 -19 1 4 27.81 10.23 -19 -1 3 17.74 9.40 -19 1 3 3.04 7.41 -19 -1 2 18.32 9.93 -19 1 2 3.07 6.99 -19 -1 1 70.59 13.82 -19 1 1 62.42 13.07 19 2 -13 2.52 4.92 19 2 -12 4.33 5.68 19 -2 -12 4.02 5.25 19 2 -12 20.16 7.63 19 2 -11 3.77 5.71 19 2 -11 7.46 6.53 19 2 -10 32.12 8.24 -19 2 10 22.01 8.80 19 2 -10 20.19 7.35 19 2 -9 -1.31 5.59 -19 -2 9 12.73 8.21 -19 2 9 3.15 6.68 19 2 -9 2.17 4.09 19 2 -8 23.94 7.42 -19 -2 8 36.35 9.24 -19 2 8 11.60 6.00 -19 -2 7 -6.24 7.69 -19 2 7 7.72 5.87 -19 -2 6 0.63 7.44 -19 2 6 -6.05 5.76 -19 -2 5 12.73 7.82 -19 2 5 -1.66 5.94 -19 -2 4 34.37 10.74 -19 2 4 25.24 9.49 -19 -2 3 10.29 8.38 -19 2 3 11.70 8.11 -19 -2 2 53.69 12.23 -19 2 2 27.60 9.46 -19 2 1 1.74 7.15 19 3 -13 15.98 7.40 19 3 -12 13.50 6.86 19 3 -11 12.94 5.99 19 3 -11 18.59 6.39 19 3 -10 10.63 5.88 19 3 -10 3.69 4.13 19 3 -9 5.60 5.11 19 3 -9 2.85 4.70 19 3 -8 -4.73 6.86 -19 -3 8 -0.33 6.79 -19 3 8 -9.78 6.68 19 3 -7 28.01 8.24 -19 -3 7 36.00 10.47 -19 3 7 36.23 9.54 -19 -3 6 8.37 6.57 -19 3 6 23.29 9.75 -19 -3 5 21.22 7.40 -19 3 5 20.15 8.73 -19 -3 4 3.31 6.49 -19 3 4 -7.03 6.53 -19 -3 3 19.23 9.14 -19 3 3 4.89 6.70 -19 -3 2 14.74 9.09 -19 3 2 14.75 8.90 -19 3 1 11.99 8.87 19 4 -13 -7.34 6.25 19 4 -12 -19.42 7.04 19 4 -11 -4.21 5.73 19 4 -11 -0.06 6.81 19 4 -10 76.53 12.43 19 4 -10 67.94 10.64 19 4 -9 35.12 8.41 19 4 -8 30.80 9.12 -19 -4 8 31.27 10.71 -19 4 8 13.86 7.20 19 4 -7 23.94 7.49 -19 -4 7 19.76 8.68 -19 4 7 17.91 7.62 -19 -4 6 -1.16 8.48 -19 4 6 -15.54 7.48 -19 -4 5 2.32 7.40 -19 4 5 -1.03 6.71 -19 -4 4 29.39 9.47 -19 4 4 49.06 11.16 -19 -4 3 15.69 9.16 -19 4 3 29.36 9.96 -19 4 2 15.76 8.03 -19 4 1 5.99 9.75 19 5 -12 31.30 8.19 19 5 -11 21.63 7.82 19 5 -10 14.56 6.01 19 5 -9 21.14 8.23 19 5 -8 -1.62 5.77 19 5 -7 10.45 6.06 -19 -5 7 13.60 8.90 -19 -5 6 24.49 9.74 -19 5 6 25.55 8.00 -19 -5 5 26.72 9.53 -19 5 5 51.65 12.01 -19 -5 4 -4.34 8.77 -19 5 4 23.60 9.28 -19 5 3 -3.09 6.22 -19 5 2 14.69 8.90 19 6 -9 66.51 11.26 19 6 -8 42.20 10.06 19 6 -7 -8.14 7.35 19 6 -6 3.11 5.82 -19 6 5 -1.28 5.90 -19 6 4 21.95 9.05 -19 6 3 19.84 9.05 -19 6 2 24.41 10.61 19 7 -8 10.15 7.60 19 7 -7 4.50 6.18 19 7 -6 36.11 8.40 -19 7 3 -2.88 6.49 19 8 -6 -4.30 6.30 -20 0 9 1.82 6.34 -20 0 8 54.51 11.22 -20 0 7 6.41 8.17 -20 0 6 31.14 10.00 -20 0 5 2.97 6.32 20 1 -11 18.76 6.78 20 1 -10 -2.05 4.55 -20 -1 9 -7.68 8.09 -20 1 9 -4.67 6.66 -20 -1 8 0.07 7.08 -20 1 8 -5.58 6.63 -20 -1 7 73.75 13.27 -20 1 7 17.12 6.29 -20 -1 6 -4.20 7.59 -20 1 6 9.57 9.33 -20 -1 5 49.75 11.46 -20 1 5 47.63 11.59 -20 1 4 11.70 9.94 20 2 -11 3.61 4.32 -20 2 9 25.38 9.17 -20 -2 8 41.20 12.93 -20 2 8 32.39 9.93 -20 -2 7 5.52 7.24 -20 2 7 -5.70 7.48 -20 -2 6 -21.32 9.42 -20 2 6 6.46 7.18 -20 2 5 4.84 8.55 -20 2 4 19.34 10.24 -20 3 8 13.42 7.78 -20 3 7 38.12 10.62 -20 3 6 15.62 8.84 -20 3 5 22.58 10.03 -20 3 4 12.50 9.66 -20 4 7 27.13 8.84 -20 4 6 0.71 5.68 -20 4 5 18.37 9.76 TITL PN220716_10444_A3_D3_Mo in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 0.71073 12.927789 12.546574 13.138196 90.0000 109.8422 90.0000 ZERR 9.00 0.000270 0.000173 0.000223 0.0000 0.0022 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O UNIT 99.00 90.00 9.00 9.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 8658 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp C1 C 0.98121(16) 0.81948(16) 0.80269(16) 0.0256(4) Uani 1 1 d . . C4 C 1.21043(17) 0.65703(16) 0.80594(16) 0.0282(4) Uani 1 1 d . . H4 H 1.2457 0.6380 0.7558 0.034 Uiso 1 1 calc R U C5 C 1.24809(18) 0.62029(15) 0.90875(17) 0.0309(4) Uani 1 1 d . . H5A H 1.3108 0.5751 0.9308 0.037 Uiso 1 1 calc R U C6 C 1.19602(19) 0.64780(16) 0.98437(16) 0.0323(5) Uani 1 1 d . . H6 H 1.2231 0.6194 1.0556 0.039 Uiso 1 1 calc R U C7 C 1.10938(17) 0.71321(16) 0.95648(14) 0.0283(4) Uani 1 1 d . . H7A H 1.0752 0.7331 1.0073 0.034 Uiso 1 1 calc R U C9 C 1.11692(16) 0.72477(14) 0.77461(14) 0.0216(3) Uani 1 1 d . . C11 C 0.90953(17) 0.89476(16) 0.61668(17) 0.0316(4) Uani 1 1 d . . H11A H 0.9486 0.9175 0.5673 0.038 Uiso 1 1 calc R U H11B H 0.8929 0.9595 0.6513 0.038 Uiso 1 1 calc R U C12 C 0.80144(17) 0.84135(16) 0.55027(16) 0.0294(4) Uani 1 1 d . . H12A H 0.7581 0.8905 0.4926 0.035 Uiso 1 1 calc R U H12B H 0.8172 0.7764 0.5153 0.035 Uiso 1 1 calc R U C13 C 0.73543(16) 0.81196(15) 0.62129(15) 0.0254(4) Uani 1 1 d . . H13A H 0.7726 0.7519 0.6685 0.030 Uiso 1 1 calc R U H13B H 0.7355 0.8734 0.6686 0.030 Uiso 1 1 calc R U C15 C 0.56770(15) 0.73919(14) 0.64090(14) 0.0219(3) Uani 1 1 d . . H15A H 0.6085 0.6753 0.6775 0.026 Uiso 1 1 calc R U H15B H 0.5735 0.7940 0.6967 0.026 Uiso 1 1 calc R U C16 C 0.44896(15) 0.71087(14) 0.58535(14) 0.0223(3) Uani 1 1 d . . H16A H 0.4179 0.6830 0.6393 0.027 Uiso 1 1 calc R U H16B H 0.4073 0.7757 0.5525 0.027 Uiso 1 1 calc R U C18 C 0.48656(16) 0.66491(15) 0.42253(14) 0.0231(4) Uani 1 1 d . . H18A H 0.4444 0.7258 0.3806 0.028 Uiso 1 1 calc R U H18B H 0.4827 0.6059 0.3714 0.028 Uiso 1 1 calc R U C19 C 0.60572(16) 0.69780(14) 0.47631(14) 0.0227(4) Uani 1 1 d . . H19A H 0.6499 0.6344 0.5095 0.027 Uiso 1 1 calc R U H19B H 0.6344 0.7260 0.4207 0.027 Uiso 1 1 calc R U C20 C 0.33440(15) 0.57861(13) 0.46128(14) 0.0196(3) Uani 1 1 d . . C21 C 0.29059(15) 0.54411(13) 0.35360(14) 0.0214(3) Uani 1 1 d . . H21A H 0.3271 0.5601 0.3037 0.026 Uiso 1 1 calc R U C22 C 0.19338(16) 0.48636(14) 0.32069(15) 0.0237(4) Uani 1 1 d . . C23 C 0.13461(17) 0.46281(15) 0.38790(18) 0.0285(4) Uani 1 1 d . . H23A H 0.0674 0.4243 0.3626 0.034 Uiso 1 1 calc R U C24 C 0.17790(18) 0.49794(16) 0.49438(18) 0.0303(4) Uani 1 1 d . . H24A H 0.1395 0.4832 0.5429 0.036 Uiso 1 1 calc R U C25 C 0.27581(17) 0.55397(15) 0.53096(16) 0.0268(4) Uani 1 1 d . . H25A H 0.3039 0.5762 0.6044 0.032 Uiso 1 1 calc R U Cl26 Cl 0.14455(4) 0.43918(4) 0.18786(4) 0.03379(11) Uani 1 1 d . . I31 I 0.51651(2) 0.97372(2) 0.34165(2) 0.02457(4) Uani 1 1 d . . N2 N 0.98215(14) 0.82617(13) 0.70036(13) 0.0251(3) Uani 1 1 d . . N3 N 1.06434(14) 0.76897(13) 0.68056(12) 0.0261(3) Uani 1 1 d . . N8 N 1.07104(13) 0.75105(12) 0.85179(12) 0.0218(3) Uani 1 1 d . . N14 N 0.61837(12) 0.78074(11) 0.56142(12) 0.0202(3) Uani 1 1 d . . H14A H 0.5770 0.8458 0.5261 0.024 Uiso 1 1 calc R U N17 N 0.43651(13) 0.63076(11) 0.50123(11) 0.0199(3) Uani 1 1 d . . O10 O 0.92036(13) 0.85917(14) 0.84516(12) 0.0401(4) Uani 1 1 d . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0192(9) 0.0289(9) 0.0292(9) -0.0082(8) 0.0090(8) -0.0022(7) C4 0.0249(10) 0.0286(9) 0.0324(9) -0.0047(8) 0.0116(8) 0.0002(7) C5 0.0239(11) 0.0223(8) 0.0388(10) 0.0005(8) 0.0005(9) 0.0010(7) C6 0.0337(12) 0.0325(10) 0.0226(8) 0.0061(8) -0.0008(8) -0.0122(9) C7 0.0273(11) 0.0390(11) 0.0196(8) -0.0042(8) 0.0091(8) -0.0126(8) C9 0.0213(9) 0.0237(8) 0.0199(8) -0.0013(7) 0.0072(7) -0.0027(7) C11 0.0223(11) 0.0273(9) 0.0385(10) 0.0076(8) 0.0016(9) -0.0012(7) C12 0.0217(10) 0.0285(9) 0.0326(10) 0.0065(8) 0.0021(8) -0.0018(7) C13 0.0185(9) 0.0242(8) 0.0276(9) 0.0029(7) 0.0003(7) -0.0015(7) C15 0.0216(9) 0.0219(8) 0.0206(8) -0.0001(7) 0.0050(7) 0.0011(6) C16 0.0196(9) 0.0232(8) 0.0241(8) -0.0040(7) 0.0076(7) -0.0001(7) C18 0.0228(10) 0.0250(8) 0.0217(8) -0.0008(7) 0.0080(7) -0.0059(7) C19 0.0222(10) 0.0218(8) 0.0243(8) -0.0018(7) 0.0083(7) -0.0025(7) C20 0.0190(9) 0.0149(7) 0.0252(8) 0.0007(6) 0.0077(7) 0.0003(6) C21 0.0205(9) 0.0195(8) 0.0238(8) 0.0024(6) 0.0069(7) -0.0012(6) C22 0.0198(9) 0.0200(8) 0.0278(9) 0.0006(7) 0.0033(7) 0.0015(6) C23 0.0194(10) 0.0232(9) 0.0430(11) -0.0004(8) 0.0106(8) -0.0025(7) C24 0.0303(11) 0.0272(9) 0.0398(11) 0.0002(8) 0.0202(9) -0.0034(8) C25 0.0298(11) 0.0245(8) 0.0297(9) -0.0014(7) 0.0148(8) -0.0025(7) Cl26 0.0288(3) 0.0347(2) 0.0307(2) -0.0038(2) 0.0007(2) -0.0063(2) I31 0.02825(7) 0.02237(6) 0.02111(6) 0.00102(4) 0.00580(5) -0.00066(5) N2 0.0208(8) 0.0284(8) 0.0240(7) 0.0004(6) 0.0049(6) 0.0002(6) N3 0.0222(9) 0.0327(8) 0.0243(7) 0.0000(6) 0.0092(7) 0.0022(6) N8 0.0170(8) 0.0272(7) 0.0211(7) -0.0018(6) 0.0063(6) -0.0012(6) N14 0.0176(8) 0.0156(6) 0.0235(7) 0.0034(5) 0.0021(6) 0.0004(5) N17 0.0209(8) 0.0187(6) 0.0212(7) -0.0023(6) 0.0087(6) -0.0028(5) O10 0.0274(9) 0.0537(10) 0.0413(8) -0.0159(8) 0.0145(7) 0.0054(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle O10 C1 N2 131.1(2) O10 C1 N8 126.85(19) N2 C1 N8 102.04(16) C5 C4 C9 118.44(19) C5 C4 H4 120.8 C9 C4 H4 120.8 C4 C5 C6 121.4(2) C4 C5 H5A 119.3 C6 C5 H5A 119.3 C7 C6 C5 120.68(18) C7 C6 H6 119.7 C5 C6 H6 119.7 C6 C7 N8 118.00(19) C6 C7 H7A 121.0 N8 C7 H7A 121.0 N3 C9 N8 112.13(17) N3 C9 C4 130.02(18) N8 C9 C4 117.84(16) N2 C11 C12 113.66(16) N2 C11 H11A 108.8 C12 C11 H11A 108.8 N2 C11 H11B 108.8 C12 C11 H11B 108.8 H11A C11 H11B 107.7 C13 C12 C11 110.71(17) C13 C12 H12A 109.5 C11 C12 H12A 109.5 C13 C12 H12B 109.5 C11 C12 H12B 109.5 H12A C12 H12B 108.1 N14 C13 C12 114.90(15) N14 C13 H13A 108.5 C12 C13 H13A 108.5 N14 C13 H13B 108.5 C12 C13 H13B 108.5 H13A C13 H13B 107.5 C16 C15 N14 111.06(14) C16 C15 H15A 109.4 N14 C15 H15A 109.4 C16 C15 H15B 109.4 N14 C15 H15B 109.4 H15A C15 H15B 108.0 N17 C16 C15 111.23(15) N17 C16 H16A 109.4 C15 C16 H16A 109.4 N17 C16 H16B 109.4 C15 C16 H16B 109.4 H16A C16 H16B 108.0 N17 C18 C19 111.99(14) N17 C18 H18A 109.2 C19 C18 H18A 109.2 N17 C18 H18B 109.2 C19 C18 H18B 109.2 H18A C18 H18B 107.9 N14 C19 C18 111.92(15) N14 C19 H19A 109.2 C18 C19 H19A 109.2 N14 C19 H19B 109.2 C18 C19 H19B 109.2 H19A C19 H19B 107.9 C21 C20 N17 121.80(16) C21 C20 C25 117.83(17) N17 C20 C25 120.28(16) C22 C21 C20 119.26(17) C22 C21 H21A 120.4 C20 C21 H21A 120.4 C23 C22 C21 123.41(18) C23 C22 Cl26 118.49(15) C21 C22 Cl26 118.09(15) C22 C23 C24 117.11(18) C22 C23 H23A 121.4 C24 C23 H23A 121.4 C25 C24 C23 121.25(19) C25 C24 H24A 119.4 C23 C24 H24A 119.4 C24 C25 C20 121.12(18) C24 C25 H25A 119.4 C20 C25 H25A 119.4 C1 N2 N3 115.05(16) C1 N2 C11 124.43(18) N3 N2 C11 120.32(16) C9 N3 N2 103.18(15) C9 N8 C7 123.59(17) C9 N8 C1 107.59(15) C7 N8 C1 128.81(17) C19 N14 C13 114.09(15) C19 N14 C15 108.40(13) C13 N14 C15 109.04(14) C19 N14 H14A 108.4 C13 N14 H14A 108.4 C15 N14 H14A 108.4 C20 N17 C18 117.30(14) C20 N17 C16 116.79(15) C18 N17 C16 111.88(14) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance C1 O10 1.215(2) C1 N2 1.351(2) C1 N8 1.412(3) C4 C5 1.352(3) C4 C9 1.420(3) C4 H4 0.9500 C5 C6 1.419(3) C5 H5A 0.9500 C6 C7 1.335(3) C6 H6 0.9500 C7 N8 1.379(2) C7 H7A 0.9500 C9 N3 1.314(2) C9 N8 1.377(2) C11 N2 1.459(2) C11 C12 1.528(3) C11 H11A 0.9900 C11 H11B 0.9900 C12 C13 1.508(3) C12 H12A 0.9900 C12 H12B 0.9900 C13 N14 1.501(2) C13 H13A 0.9900 C13 H13B 0.9900 C15 C16 1.502(3) C15 N14 1.502(2) C15 H15A 0.9900 C15 H15B 0.9900 C16 N17 1.462(2) C16 H16A 0.9900 C16 H16B 0.9900 C18 N17 1.458(2) C18 C19 1.518(3) C18 H18A 0.9900 C18 H18B 0.9900 C19 N14 1.495(2) C19 H19A 0.9900 C19 H19B 0.9900 C20 C21 1.402(2) C20 N17 1.406(2) C20 C25 1.406(3) C21 C22 1.387(3) C21 H21A 0.9500 C22 C23 1.378(3) C22 Cl26 1.7455(19) C23 C24 1.390(3) C23 H23A 0.9500 C24 C25 1.384(3) C24 H24A 0.9500 C25 H25A 0.9500 N2 N3 1.378(2) N14 H14A 1.0000 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C9 C4 C5 C6 0.2(3) C4 C5 C6 C7 -1.6(3) C5 C6 C7 N8 1.4(3) C5 C4 C9 N3 -178.9(2) C5 C4 C9 N8 1.3(3) N2 C11 C12 C13 62.3(2) C11 C12 C13 N14 167.50(15) N14 C15 C16 N17 58.45(19) N17 C18 C19 N14 -54.2(2) N17 C20 C21 C22 175.39(16) C25 C20 C21 C22 -1.0(3) C20 C21 C22 C23 1.8(3) C20 C21 C22 Cl26 -177.00(13) C21 C22 C23 C24 -1.3(3) Cl26 C22 C23 C24 177.54(15) C22 C23 C24 C25 -0.1(3) C23 C24 C25 C20 0.8(3) C21 C20 C25 C24 -0.3(3) N17 C20 C25 C24 -176.71(18) O10 C1 N2 N3 -179.6(2) N8 C1 N2 N3 -0.3(2) O10 C1 N2 C11 5.5(3) N8 C1 N2 C11 -175.22(17) C12 C11 N2 C1 -89.9(2) C12 C11 N2 N3 95.5(2) N8 C9 N3 N2 0.4(2) C4 C9 N3 N2 -179.38(19) C1 N2 N3 C9 0.0(2) C11 N2 N3 C9 175.08(16) N3 C9 N8 C7 178.59(17) C4 C9 N8 C7 -1.6(3) N3 C9 N8 C1 -0.7(2) C4 C9 N8 C1 179.17(17) C6 C7 N8 C9 0.2(3) C6 C7 N8 C1 179.31(19) O10 C1 N8 C9 179.9(2) N2 C1 N8 C9 0.6(2) O10 C1 N8 C7 0.7(3) N2 C1 N8 C7 -178.62(18) C18 C19 N14 C13 176.93(14) C18 C19 N14 C15 55.24(18) C12 C13 N14 C19 50.8(2) C12 C13 N14 C15 172.16(16) C16 C15 N14 C19 -57.50(18) C16 C15 N14 C13 177.76(14) C21 C20 N17 C18 10.7(2) C25 C20 N17 C18 -173.01(16) C21 C20 N17 C16 147.63(16) C25 C20 N17 C16 -36.1(2) C19 C18 N17 C20 -167.61(15) C19 C18 N17 C16 53.5(2) C15 C16 N17 C20 165.06(14) C15 C16 N17 C18 -55.78(19)