#------------------------------------------------------------------------------ #$Date: 2018-03-14 09:26:22 +0200 (Wed, 14 Mar 2018) $ #$Revision: 206946 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/54/90/1549066.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1549066 loop_ _publ_author_name 'Chaurasia, Rahul' 'Bharti, Akhilesh' 'Butcher, Ray J.' 'Wikaira, Jan L.' 'Bharty, Manoj K.' _publ_section_title ; 4-Cyclohexyl-1-(2-methoxybenzoyl)thiosemicarbazide with an unknown solvent ; _journal_coeditor_code SU5423 _journal_issue 3 _journal_name_full IUCrData _journal_page_first x180383 _journal_paper_doi 10.1107/S2414314618003838 _journal_volume 3 _journal_year 2018 _chemical_formula_iupac 'C15 H21 N3 O2 S' _chemical_formula_moiety 'C15 H21 N3 O2 S' _chemical_formula_sum 'C15 H21 N3 O2 S' _chemical_formula_weight 307.41 _chemical_name_systematic ; 4-Cyclohexyl-1-(2-methoxybenzoyl)thiosemicarbazide ; _space_group_crystal_system orthorhombic _space_group_IT_number 56 _space_group_name_Hall '-P 2ab 2ac' _space_group_name_H-M_alt 'P c c n' _symmetry_space_group_name_Hall '-P 2ab 2ac' _symmetry_space_group_name_H-M 'P c c n' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 29.5823(10) _cell_length_b 15.1971(8) _cell_length_c 7.4303(2) _cell_measurement_reflns_used 5858 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 36.8740 _cell_measurement_theta_min 4.0570 _cell_volume 3340.4(2) _computing_cell_refinement ; CrysAlis PRO (Rigaku OD, 2015) ; _computing_data_collection ; CrysAlis PRO (Rigaku OD, 2015) ; _computing_data_reduction ; CrysAlis PRO (Rigaku OD, 2015) ; _computing_molecular_graphics ; SHELXTL (Sheldrick, 2008) ; _computing_publication_material ; SHELXTL (Sheldrick, 2008) ; _computing_structure_refinement ; SHELXL2014 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 10.6501 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.946 _diffrn_measurement_device_type ; Rigaku OD SuperNova, Dual, Cu at zero, Atlas ; _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0383 _diffrn_reflns_limit_h_max 32 _diffrn_reflns_limit_h_min -51 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_l_max 9 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_number 23969 _diffrn_reflns_theta_full 25.500 _diffrn_reflns_theta_max 37.948 _diffrn_reflns_theta_min 3.348 _exptl_absorpt_coefficient_mu 0.202 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.76644 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlis PRO; Rigaku OD, 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.223 _exptl_crystal_description block _exptl_crystal_F_000 1312 _exptl_crystal_size_max 0.35 _exptl_crystal_size_mid 0.31 _exptl_crystal_size_min 0.18 _refine_diff_density_max 0.566 _refine_diff_density_min -0.491 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.005 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 191 _refine_ls_number_reflns 8579 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.005 _refine_ls_R_factor_all 0.0810 _refine_ls_R_factor_gt 0.0512 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0573P)^2^+0.9308P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1222 _refine_ls_wR_factor_ref 0.1412 _reflns_number_gt 5943 _reflns_number_total 8579 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file su5423sup1.cif _cod_data_source_block I _cod_database_code 1549066 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_hkl_file ; -5 0 0 386.648 54.1194 1 5 0 0 312.031 45.8996 1 -6 0 0 79565.4 632.397 1 6 0 0 78590.0 613.315 1 -7 0 0 884.170 90.0489 1 7 0 0 369.259 58.6788 1 8 0 0 7155.03 217.695 1 -8 0 0 7383.65 232.978 1 -9 0 0 37.6675 52.4954 1 9 0 0 10.6858 19.7095 1 -10 0 0 41043.3 606.906 1 10 0 0 39416.8 561.517 1 -11 0 0 330.602 87.0249 1 11 0 0 169.567 49.7318 1 -12 0 0 4458.83 226.592 1 -13 0 0 289.762 97.0176 1 -14 0 0 48300.9 802.201 1 -15 0 0 238.405 103.606 1 -16 0 0 38419.7 767.686 1 -17 0 0 571.082 132.135 1 -18 0 0 16661.0 534.216 1 -19 0 0 354.005 120.319 1 -20 0 0 21719.9 648.987 1 -21 0 0 682.405 162.738 1 -22 0 0 53001.5 1074.77 1 -23 0 0 1025.78 221.215 1 -24 0 0 84492.4 1421.19 1 -25 0 0 782.887 199.640 1 -26 0 0 15138.8 635.133 1 -27 0 0 690.146 173.565 1 -28 0 0 17500.4 713.299 1 -29 0 0 779.055 215.745 1 -30 0 0 49636.9 1261.35 1 -31 0 0 689.126 200.921 1 -32 0 0 1688.20 250.282 1 -33 0 0 85.9538 87.5200 1 -34 0 0 9813.92 602.385 1 -35 0 0 155.847 105.958 1 -36 0 0 537.227 162.829 1 -37 0 0 99.0673 90.5736 1 -38 0 0 535.923 161.860 1 -39 0 0 187.617 108.998 1 -40 0 0 3002.41 367.188 1 -41 0 0 195.261 114.575 1 -42 0 0 2376.69 342.496 1 -43 0 0 302.273 152.273 1 -44 0 0 2882.17 392.307 1 -45 0 0 353.850 173.184 1 -46 0 0 6569.09 586.286 1 -47 0 0 244.261 96.6974 1 -48 0 0 1084.73 227.719 1 -49 0 0-71.2552 95.7524 1 -50 0 0 2906.46 385.344 1 -5 -1 0 135393. 838.282 1 5 -1 0 131477. 680.667 1 -6 1 0 19.0288 16.4282 1 6 -1 0 4.09895 20.7312 1 -7 1 0 156243. 895.212 1 7 -1 0 157638. 880.506 1 -7 -1 0 151746. 1027.87 1 -8 1 0-5.88158 16.7377 1 8 1 0-8.09575 19.5609 1 9 -1 0 4106.25 166.555 1 -9 1 0 4173.28 170.474 1 -9 -1 0 3946.68 195.470 1 9 1 0 4364.08 181.470 1 -10 -1 0 0.08400 25.7238 1 10 -1 0 0.49079 18.0499 1 -10 1 0-18.6835 24.7843 1 10 1 0-16.4667 21.7268 1 11 -1 0 6577.69 228.455 1 -11 -1 0 6556.04 266.067 1 -11 1 0 6716.49 246.917 1 -12 -1 0 20.4393 47.1166 1 -12 1 0 9.08470 38.6837 1 -13 -1 0 9958.61 358.585 1 -13 1 0 9980.68 328.039 1 -14 1 0 86.1892 56.5505 1 -14 -1 0 75.3313 70.1458 1 -15 -1 0 12575.2 431.753 1 -15 1 0 12474.0 403.364 1 -16 1 0 112.301 63.5268 1 -16 -1 0 30.6269 52.9653 1 -17 1 0 320.699 74.9181 1 -17 -1 0 229.922 68.3676 1 -18 1 0 28.5981 50.8995 1 -18 -1 0 65.1702 67.2512 1 -19 1 0 14330.0 491.848 1 -19 -1 0 14692.4 532.327 1 -20 -1 0 113.256 78.4558 1 -20 1 0 74.4493 65.1213 1 -21 1 0 72.3263 50.2997 1 -21 -1 0 71.2956 46.3516 1 -22 1 0-23.0596 59.7831 1 -22 -1 0 16.9297 79.2378 1 -23 -1 0 1986.11 223.737 1 -23 1 0 2102.05 215.593 1 -24 1 0 34.5830 73.2375 1 -24 -1 0-41.9809 87.1519 1 -25 1 0 1326.43 172.440 1 -25 -1 0 1376.88 194.775 1 -26 1 0 24.0736 51.7398 1 -26 -1 0-39.0288 78.8005 1 -27 -1 0 703.992 152.984 1 -27 1 0 789.626 146.160 1 -28 -1 0 46.7115 95.0240 1 -28 1 0-43.6860 77.0499 1 -29 1 0 1267.59 195.963 1 -29 -1 0 1535.76 237.222 1 -30 -1 0 214.141 138.833 1 -30 1 0 75.7670 95.3209 1 -31 -1 0 5741.34 455.817 1 -31 1 0 5315.89 410.317 1 -32 -1 0 94.8993 97.9329 1 -32 1 0 129.703 66.4072 1 -33 1 0 36.7044 67.2635 1 -33 -1 0 349.069 134.460 1 -34 -1 0-21.9310 93.9206 1 -34 1 0-83.0345 90.0830 1 -35 -1 0 57.1094 81.2150 1 -35 1 0 97.7425 82.5293 1 -36 -1 0-124.680 94.5707 1 -36 1 0-109.962 88.7237 1 -37 -1 0-151.582 103.660 1 -37 1 0 32.9056 62.1878 1 -38 1 0-145.607 98.4982 1 -38 -1 0-54.5190 71.9124 1 -39 -1 0 126.026 89.9710 1 -39 1 0 363.163 140.501 1 -40 1 0 152.551 120.025 1 -40 -1 0-7.04837 77.4639 1 -41 -1 0 3199.39 390.961 1 -41 1 0 3913.39 427.071 1 -42 1 0-109.207 126.574 1 -42 -1 0-88.5805 120.794 1 -43 1 0-126.604 102.661 1 -43 -1 0-18.3247 83.2026 1 -44 -1 0-75.8105 122.414 1 -44 1 0 14.4537 64.3750 1 -45 1 0 24.5218 93.3747 1 -45 -1 0-186.068 117.087 1 -46 1 0 163.644 99.2208 1 -46 -1 0-123.575 90.9933 1 -47 -1 0 39.9334 80.1551 1 -47 1 0 43.0102 75.9386 1 -48 1 0 51.9326 69.1418 1 -48 -1 0-82.0426 131.856 1 -49 -1 0 1161.54 258.586 1 -49 1 0 490.522 157.146 1 -50 -1 0-22.1038 90.1362 1 -51 -1 0 566.121 186.809 1 3 2 0-12.7623 13.8193 1 -4 2 0 215851. 726.184 1 4 -2 0 213117. 727.739 1 -4 -2 0 209495. 1046.27 1 -5 -2 0-11.3091 24.4757 1 -5 2 0 18.7304 11.2197 1 5 -2 0-4.02690 12.7098 1 -6 -2 0 91028.1 797.479 1 -6 2 0 90777.4 593.779 1 6 -2 0 92981.3 593.482 1 7 -2 0-20.5544 21.0048 1 -7 2 0-47.8005 22.8414 1 8 -2 0 378.755 45.7077 1 -8 -2 0 316.705 53.7015 1 -8 2 0 318.611 40.6396 1 9 -2 0 8.66139 13.4917 1 -9 2 0 4.57036 18.8518 1 -10 -2 0 53904.4 766.151 1 -10 2 0 53830.0 622.351 1 10 -2 0 56569.6 618.257 1 11 -2 0 51.5319 34.4460 1 -11 2 0-9.27542 23.4229 1 -12 -2 0 29090.0 619.920 1 -12 2 0 28868.3 508.838 1 12 -2 0 29887.1 489.752 1 -13 2 0 23.6095 32.2937 1 -13 -2 0 129.919 81.4948 1 -14 2 0 18993.9 462.808 1 -14 -2 0 19724.9 550.143 1 -15 -2 0 24.7027 57.6192 1 -15 2 0-24.4628 42.3461 1 -16 -2 0 5428.52 311.179 1 -16 2 0 5389.98 265.580 1 -17 2 0 65.2319 64.2070 1 -17 -2 0 371.653 134.086 1 -18 2 0 58801.3 951.292 1 -18 -2 0 59150.0 1078.16 1 -19 -2 0 457.787 162.935 1 -19 2 0 272.880 120.242 1 -20 -2 0 22419.9 698.184 1 -20 2 0 23225.5 626.061 1 -21 -2 0 51.2108 81.9306 1 -21 2 0 35.5571 66.9164 1 -22 2 0 9245.85 419.181 1 -22 -2 0 9219.88 475.257 1 -23 -2 0 129.592 93.2133 1 -23 2 0 34.6442 68.4686 1 -24 -2 0 18419.6 703.713 1 -24 2 0 18113.7 618.761 1 -25 -2 0 2.37153 66.0889 1 -25 2 0 55.5888 74.8564 1 -26 2 0 612.645 121.120 1 -26 -2 0 499.296 120.789 1 -27 -2 0 78.3845 76.9977 1 -27 2 0 27.5662 50.3159 1 -28 2 0 2317.85 244.182 1 -28 -2 0 1987.47 255.459 1 -29 2 0 109.514 86.5251 1 -29 -2 0 190.440 126.867 1 -30 2 0 16768.0 697.170 1 -30 -2 0 16833.1 769.014 1 -31 -2 0 166.385 114.789 1 -31 2 0 74.2739 86.3505 1 -32 -2 0 110.895 113.957 1 -32 2 0 29.9150 57.9058 1 -33 2 0 203.537 113.750 1 -33 -2 0 51.2904 90.2785 1 -34 -2 0 2492.23 331.963 1 -34 2 0 2523.55 293.988 1 -35 2 0 216.457 110.900 1 -35 -2 0-83.6257 84.8923 1 -36 -2 0 4586.67 452.711 1 -36 2 0 4765.32 415.816 1 -37 2 0-31.6150 61.1809 1 -37 -2 0 189.336 139.606 1 -38 -2 0 2487.48 350.920 1 -38 2 0 2266.51 313.133 1 -39 -2 0 47.8163 74.4595 1 -39 2 0 38.6372 106.956 1 -40 2 0 1720.73 278.168 1 -40 -2 0 1631.97 287.364 1 -41 -2 0 183.942 103.026 1 -41 2 0 113.871 78.8118 1 -42 -2 0 2966.54 396.531 1 -42 2 0 2973.07 369.417 1 -43 2 0 72.8330 90.4231 1 -43 -2 0-13.7919 77.4235 1 -44 -2 0 595.726 188.511 1 -44 2 0 513.861 166.575 1 -45 2 0 48.0489 66.9465 1 -45 -2 0 274.887 143.273 1 -46 2 0 8114.86 615.798 1 -46 -2 0 8729.45 702.089 1 -47 2 0 108.472 76.9758 1 -47 -2 0 47.4807 118.014 1 -48 2 0-84.6674 89.6353 1 -48 -2 0-204.137 161.254 1 -49 -2 0 319.879 165.276 1 -50 -2 0 1053.61 259.274 1 0 3 0 15.1536 10.8038 1 0 -3 0 22.9857 15.6354 1 -1 3 0 45858.5 348.451 1 1 3 0 47182.8 413.148 1 -1 -3 0 46121.5 433.654 1 1 -3 0 47414.8 545.215 2 1 -3 0 45129.8 369.373 1 -2 -3 0-10.8673 17.5776 1 2 -3 0 36.2959 26.7188 2 2 3 0 3.92414 14.9407 1 -2 3 0 3.68182 10.8465 1 -3 3 0 56949.0 368.912 1 3 -3 0 59259.1 648.365 2 -3 -3 0 54772.5 562.955 1 3 3 0 54802.5 523.875 1 4 3 0 13.4558 17.3334 1 -4 3 0-7.04601 11.5762 1 4 -3 0 12.6428 22.2215 2 -4 -3 0 36.9919 19.1037 1 5 3 0 25140.6 400.920 1 -5 3 0 25126.7 270.642 1 5 -3 0 25855.4 484.004 2 -5 -3 0 24518.3 420.029 1 5 -3 0 25895.5 281.655 1 6 -3 0 13.7260 13.6962 1 6 3 0-32.3855 26.3574 1 -6 -3 0-35.6941 26.4617 1 -6 3 0-9.52920 16.1171 1 6 -3 0 14.4350 24.6587 2 -7 -3 0 44620.2 642.020 1 -7 3 0 48733.2 448.416 1 7 -3 0 48453.8 459.367 1 7 3 0 47160.7 600.303 1 -8 -3 0 8.99083 49.2612 1 8 -3 0-0.87431 18.3680 1 -8 3 0 9.99526 16.7487 1 -9 -3 0 2799.02 179.145 1 9 -3 0 2920.95 136.095 1 -9 3 0 2946.22 130.172 1 -10 3 0-21.1918 30.0130 1 10 -3 0-17.3294 19.6252 1 -11 3 0 97332.8 845.841 1 11 -3 0 98992.7 858.425 1 -11 -3 0 100255. 1157.69 1 12 -3 0 34.7722 34.1045 1 -12 3 0-23.6131 30.8699 1 -13 3 0 14431.4 369.776 1 -13 -3 0 14459.7 471.636 1 13 -3 0 14307.0 345.678 1 -14 3 0-7.59675 44.7702 1 -14 -3 0 208.060 88.0885 1 -15 -3 0 1359.54 166.671 1 -15 3 0 1252.12 123.372 1 -16 3 0 123.603 67.9118 1 -16 -3 0 215.097 110.745 1 -17 3 0 24958.8 575.512 1 -17 -3 0 24642.9 699.314 1 -18 3 0 4.74156 56.5128 1 -18 -3 0 110.443 92.2687 1 -19 -3 0 4087.76 308.823 1 -19 3 0 4362.61 257.646 1 -20 3 0 159.633 80.2435 1 -20 -3 0 195.031 112.146 1 -21 3 0 1776.14 184.954 1 -21 -3 0 1423.25 204.901 1 -22 -3 0 203.113 143.418 1 -22 3 0 99.6551 93.5056 1 -23 -3 0 15297.3 647.089 1 -23 3 0 15463.9 548.346 1 -24 3 0 41.3711 72.8580 1 -24 -3 0 110.738 109.625 1 -25 3 0 7916.51 413.846 1 -25 -3 0 7342.67 469.262 1 -26 -3 0-88.1480 88.6352 1 -26 3 0-57.1417 53.5774 1 -27 -3 0 1658.78 238.331 1 -27 3 0 1612.88 197.798 1 -28 -3 0 24.3932 87.9495 1 -28 3 0-41.9768 68.3638 1 -29 3 0 113.512 71.8428 1 -29 -3 0 76.4751 97.9903 1 -30 3 0 40.2692 54.8856 1 -30 -3 0 85.4844 100.652 1 -31 3 0 1064.12 176.696 1 -31 -3 0 762.798 175.520 1 -32 3 0 35.5705 48.5196 1 -32 -3 0 32.4887 77.2587 1 -33 -3 0 1262.31 245.752 1 -33 3 0 1344.33 208.364 1 -34 -3 0 79.6083 102.440 1 -34 3 0 81.8866 104.404 1 -35 -3 0 7566.42 582.476 1 -35 3 0 8052.25 517.247 1 -36 -3 0 244.888 148.427 1 -36 3 0 12.8528 80.3507 1 -37 3 0 2377.12 298.261 1 -37 -3 0 2294.49 338.590 1 -38 3 0 42.9209 76.1413 1 -38 -3 0 72.6084 129.123 1 -39 -3 0 75.0047 82.8254 1 -39 3 0 16.4540 59.9283 1 -40 3 0 116.604 90.9967 1 -40 -3 0 65.0781 85.7229 1 -41 3 0 5748.13 491.251 1 -41 -3 0 4678.80 501.655 1 -42 -3 0 42.3077 123.486 1 -42 3 0 230.571 145.653 1 -43 -3 0 5322.55 546.242 1 -43 3 0 4752.81 449.676 1 -44 3 0-233.531 108.638 1 -44 -3 0 44.0444 126.141 1 -45 3 0 181.128 102.879 1 -45 -3 0 173.877 150.078 1 -46 3 0-12.2028 70.1741 1 -46 -3 0-62.8745 116.079 1 -47 -3 0 174.533 143.838 1 -48 -3 0 136.989 118.052 1 -49 -3 0 1035.29 247.666 1 -50 -3 0-233.621 134.338 1 0 -4 0 15261.9 260.454 1 0 4 0 15763.7 248.705 1 0 4 0 15625.2 372.941 2 1 -4 0 4.90689 20.8621 2 -1 4 0-0.49177 9.69340 1 1 -4 0 22.2094 15.3167 1 -1 -4 0 5.06048 21.1456 1 1 4 0 19.0786 20.5822 1 2 -4 0 228980. 1382.33 2 -2 4 0 224520. 832.457 1 2 4 0 225704. 1079.21 1 3 4 0-4.86579 17.1136 1 3 -4 0 21.7235 25.8268 2 -3 -4 0 0.29104 22.2989 1 -3 4 0 14.9014 9.66086 1 -4 4 0 184309. 762.755 1 4 -4 0 192258. 1342.48 2 -4 -4 0 187829. 1194.50 1 4 4 0 188384. 1095.25 1 5 4 0-17.8777 19.4776 1 -5 4 0 0.35041 11.7621 1 5 -4 0-29.5746 24.7682 2 -5 -4 0 19.2521 28.7374 1 -6 4 0 6873.92 155.220 1 -6 -4 0 6476.04 248.407 1 6 4 0 7296.15 235.653 1 6 -4 0 6694.02 158.541 1 -7 4 0-0.64846 12.9898 1 7 -4 0 1.84325 13.9012 1 -7 -4 0-10.7874 29.2577 1 8 -4 0 24483.3 347.799 1 -8 4 0 24106.2 331.673 1 -8 -4 0 23249.1 517.524 1 -9 4 0 14.2157 16.7914 1 9 -4 0-16.6766 23.8068 1 -10 4 0 3541.46 147.497 1 -10 -4 0 3626.60 222.071 1 10 -4 0 3683.00 153.845 1 -11 4 0-12.7655 22.6441 1 11 -4 0 6.67961 18.7540 1 -11 -4 0 4.65646 52.2156 1 12 -4 0 2996.73 149.400 1 -12 -4 0 2667.02 211.823 1 -12 4 0 2746.92 147.256 1 13 -4 0-29.5294 34.0910 1 -13 4 0 15.3807 30.8686 1 -14 -4 0 43066.3 881.223 1 -14 4 0 43915.5 639.411 1 14 -4 0 44804.4 624.885 1 -15 -4 0 153.536 100.378 1 -15 4 0 17.4036 32.2511 1 -16 4 0 1042.47 111.770 1 -16 -4 0 1257.96 168.716 1 -17 4 0-19.8466 35.5862 1 -17 -4 0-31.3449 62.3738 1 -18 -4 0 664.886 129.291 1 -18 4 0 608.882 92.1276 1 -19 -4 0 2.33738 54.5860 1 -19 4 0-18.0114 40.9707 1 -20 -4 0 186.696 110.623 1 -20 4 0 124.662 55.3034 1 -21 4 0 0.70857 55.1861 1 -21 -4 0 343.374 147.538 1 -22 4 0 11744.8 453.811 1 -22 -4 0 11959.2 578.225 1 -23 4 0 47.5376 75.1403 1 -23 -4 0 309.981 172.589 1 -24 -4 0 26325.7 887.762 1 -24 4 0 25054.5 695.025 1 -25 -4 0 89.4695 103.169 1 -25 4 0-23.2355 47.3113 1 -26 4 0 149.907 62.2296 1 -26 -4 0 106.773 84.6491 1 -27 -4 0-93.2731 102.812 1 -27 4 0 34.4950 53.8114 1 -28 -4 0 1668.75 252.360 1 -28 4 0 1804.97 208.201 1 -29 4 0-58.6913 86.1974 1 -29 -4 0-53.6596 82.2629 1 -30 -4 0 2959.34 346.213 1 -30 4 0 2922.86 281.314 1 -31 -4 0-91.0555 81.1568 1 -31 4 0 65.8842 84.4783 1 -32 -4 0 649.113 169.368 1 -32 4 0 642.429 135.649 1 -33 4 0-28.0888 49.0935 1 -33 -4 0 55.3951 93.8295 1 -34 4 0 171.488 89.4627 1 -34 -4 0 79.2755 141.709 1 -35 4 0 122.225 90.4248 1 -35 -4 0 121.456 110.066 1 -36 4 0 567.802 153.066 1 -36 -4 0 525.015 197.018 1 -37 4 0-24.4440 74.2738 1 -37 -4 0 16.5974 77.7781 1 -38 -4 0 1505.23 271.929 1 -38 4 0 2009.38 280.146 1 -39 4 0-125.472 94.0100 1 -39 -4 0 78.1708 74.5514 1 -40 -4 0-73.9644 142.162 1 -40 4 0 150.733 101.362 1 -41 -4 0 23.9310 84.1902 1 -41 4 0 104.433 106.380 1 -42 4 0 439.334 146.440 1 -42 -4 0 272.485 117.470 1 -43 -4 0-71.6770 109.655 1 -43 4 0 68.5241 86.8759 1 -44 -4 0-39.7746 110.540 1 -44 4 0-0.43964 87.8262 1 -45 -4 0 185.163 143.070 1 -46 -4 0 3700.93 472.343 1 -47 -4 0 85.0633 87.6805 1 -48 -4 0 248.309 169.182 1 -49 -4 0 47.1473 131.785 1 0 -5 0 233.529 44.5720 1 0 5 0 263.073 71.5077 2 0 5 0 138.470 33.6524 1 -1 5 0 2689.09 182.276 2 1 -5 0 2733.99 122.246 1 1 5 0 2842.83 124.083 1 1 5 0 2762.50 181.790 2 -1 5 0 2946.72 113.910 1 1 -5 0 2731.78 167.957 2 -1 -5 0 2907.74 135.613 1 -2 -5 0 17.5077 19.3900 1 -2 5 0-4.52984 11.1318 1 -2 5 0-3.64710 37.1157 2 2 5 0 35.3001 23.1686 1 3 5 0 24987.7 400.130 1 -3 5 0 24279.8 564.699 2 -3 5 0 24866.9 304.427 1 -3 -5 0 23557.0 437.779 1 -4 5 0-14.9717 12.7682 1 4 5 0 4.84740 20.3360 1 -4 -5 0-10.4539 28.5414 1 -5 5 0 43449.5 410.911 1 5 5 0 44978.5 581.644 1 -5 -5 0 41816.8 642.624 1 -6 -5 0-24.7172 39.1412 1 -6 5 0 27.2698 14.9028 1 -7 -5 0 34087.0 636.519 1 -7 5 0 32890.6 364.907 1 -8 5 0-24.7427 21.6035 1 8 -5 0 32.4765 21.4726 1 -8 -5 0-27.6279 34.4554 1 9 -5 0 10065.1 236.129 1 -9 5 0 10668.9 225.020 1 -9 -5 0 10688.8 380.599 1 10 -5 0 120.579 35.0562 1 -10 5 0 102.623 34.2429 1 -11 5 0 130221. 910.095 1 11 -5 0 132156. 942.319 1 -11 -5 0 123916. 1429.43 1 12 -5 0 34.0480 27.4294 1 -12 5 0 14.4392 27.4673 1 -13 5 0 122342. 973.906 1 -13 -5 0 121988. 1486.12 1 13 -5 0 125278. 985.959 1 -14 5 0 39.7365 37.8853 1 14 -5 0-27.0135 26.5229 1 -15 5 0 2908.08 165.877 1 -15 -5 0 3048.82 256.169 1 -16 -5 0 19.5058 54.3921 1 -16 5 0 0.82052 23.6729 1 -17 -5 0 1418.84 186.788 1 -17 5 0 1168.97 115.809 1 -18 5 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1 -5 6 0-14.0283 18.8240 1 -5 -6 0-25.0580 35.8063 1 -6 6 0 21684.0 308.105 1 -6 -6 0 21202.3 508.046 1 -7 6 0-4.91186 17.8767 1 -7 -6 0-3.81304 42.2395 1 -8 6 0 748.687 59.5974 1 -8 -6 0 782.620 105.698 1 -9 6 0-13.8659 22.0292 1 -9 -6 0 67.1339 59.3659 1 -10 6 0 3935.38 143.789 1 10 -6 0 3935.93 153.832 1 -10 -6 0 3850.48 248.893 1 -11 6 0-19.3164 24.4597 1 -11 -6 0 14.6231 60.1311 1 11 -6 0 39.1389 26.6802 1 12 -6 0 8915.02 248.850 1 -12 -6 0 8414.08 395.783 1 -12 6 0 8643.78 238.327 1 -13 6 0-1.04310 24.8257 1 -13 -6 0 37.1515 77.8892 1 13 -6 0 26.9023 21.0796 1 -14 6 0 4404.03 186.348 1 -14 -6 0 4154.25 303.828 1 14 -6 0 3887.75 177.462 1 15 -6 0-10.5060 22.0540 1 -15 6 0 0.15615 20.7347 1 -16 -6 0 18536.3 657.627 1 -16 6 0 18136.8 412.387 1 -17 6 0 14.9976 30.2786 1 -17 -6 0 156.471 124.961 1 -18 6 0 11574.2 366.836 1 -18 -6 0 11575.3 552.401 1 -19 -6 0 230.577 151.503 1 -19 6 0 71.3402 51.7609 1 -20 6 0 29999.8 627.213 1 -20 -6 0 30724.4 932.717 1 -21 6 0 85.1568 58.4861 1 -21 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169.243 1 -41 -6 0-188.534 147.359 1 -42 -6 0-199.982 196.446 1 -43 -6 0-166.257 148.511 1 -44 -6 0 358.033 187.331 1 -45 -6 0-68.6111 143.349 1 -46 -6 0-6.41945 113.837 1 -47 -6 0-283.722 185.498 1 -48 -6 0 923.368 251.271 1 0 7 0 419.200 60.9513 1 0 -7 0 521.807 81.5382 1 1 7 0 39776.5 524.120 1 -1 -7 0 37791.9 594.997 1 -1 7 0 41206.8 499.255 1 -2 -7 0 29.2292 35.7005 1 -2 7 0 12.9325 20.1774 1 2 7 0 2.64056 21.9357 1 -3 -7 0 15741.0 417.018 1 -3 7 0 16213.9 291.717 1 -4 7 0 3.52782 14.6692 1 -4 -7 0 18.6574 36.8663 1 -5 -7 0 462.141 83.9028 1 -5 7 0 389.240 50.3714 1 -5 7 0 456.237 46.3507 1 -6 -7 0-34.3722 37.0840 1 -6 7 0-17.2854 19.2645 1 -7 7 0 214.763 37.8562 1 -7 7 0 277.718 44.1918 1 -7 -7 0 230.340 77.3347 1 -8 7 0 23.4384 16.7703 1 -8 -7 0 3.98638 39.3743 1 -9 -7 0 755.718 118.900 1 -9 7 0 663.926 57.8186 1 -10 7 0-8.58564 21.7640 1 -10 -7 0 257.249 116.258 1 -11 -7 0 62450.4 1078.64 1 -11 7 0 60956.0 582.352 1 -12 -7 0 76.0532 112.939 1 -12 7 0 16.5987 22.7603 1 -13 -7 0 33966.0 842.554 1 -13 7 0 33252.1 469.985 1 13 -7 0 33220.3 490.677 1 14 -7 0 358.364 55.9118 1 -14 7 0 263.525 51.1733 1 -14 -7 0 472.990 138.881 1 -15 7 0 12069.6 308.551 1 15 -7 0 12059.6 311.253 1 -15 -7 0 12083.7 540.272 1 -16 7 0 20.7796 24.6404 1 16 -7 0-22.0853 22.9959 1 -17 -7 0 13440.6 598.947 1 -17 7 0 13173.0 355.239 1 -18 -7 0 142.639 118.644 1 -18 7 0 30.7691 37.3427 1 -19 -7 0 10912.9 570.229 1 -19 7 0 9188.69 324.466 1 -20 7 0 28.5068 38.7557 1 -20 -7 0 56.2307 98.4221 1 -21 -7 0 2654.97 292.039 1 -21 7 0 2775.06 192.466 1 -22 7 0 5.76262 42.5752 1 -22 -7 0 71.8971 85.3523 1 -23 -7 0 104.936 111.215 1 -23 7 0 78.6704 54.3347 1 -24 7 0-74.2209 39.0590 1 -24 -7 0 106.946 145.652 1 -25 -7 0 17243.4 801.324 1 -25 7 0 16655.0 531.911 1 -26 -7 0 95.3829 115.298 1 -26 7 0 60.6558 56.8057 1 -27 -7 0 1320.80 233.253 1 -27 7 0 1163.04 149.700 1 -28 7 0 37.9703 43.3021 1 -28 -7 0 65.5652 125.294 1 -29 7 0 7504.98 397.309 1 -29 -7 0 7530.08 573.296 1 -30 -7 0 211.913 148.058 1 -30 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15352.4 272.516 1 -6 8 0 15551.1 303.461 1 -7 8 0 20.1519 17.0605 1 -7 -8 0 50.9539 46.8850 1 -7 8 0 8.95523 15.3014 1 -8 8 0 16643.4 295.108 1 -8 8 0 17881.0 299.016 1 -8 -8 0 17410.7 547.845 1 -9 -8 0-26.2761 54.0477 1 -9 8 0 16.6374 14.4181 1 -10 8 0 2483.22 112.704 1 -10 -8 0 2768.28 234.615 1 -11 8 0-2.26515 15.1360 1 -11 -8 0 20.1718 51.8595 1 -12 8 0 1140.10 78.8350 1 -12 -8 0 1057.71 150.820 1 -13 8 0 1.43615 15.3800 1 -13 -8 0-61.6204 75.2805 1 -14 -8 0 13884.3 580.008 1 -14 8 0 14319.3 307.202 1 -15 8 0 0.40473 20.6203 1 -15 -8 0 130.830 116.361 1 -16 8 0 20739.8 405.249 1 -16 -8 0 20965.8 739.518 1 17 -8 0 10.5932 23.8492 1 -17 8 0 12.5136 31.3652 1 -18 8 0 3937.14 193.018 1 -18 -8 0 4536.90 370.009 1 -19 -8 0 3.98423 83.8133 1 -19 8 0 46.6844 42.8904 1 -20 -8 0 813.047 174.630 1 -20 8 0 784.163 96.4207 1 -21 8 0 46.6463 49.3676 1 -21 -8 0 377.940 177.659 1 -22 8 0 25955.7 572.350 1 -22 -8 0 25166.7 945.851 1 -23 -8 0 715.825 244.579 1 -23 8 0 161.801 77.6991 1 -24 -8 0 42007.0 1253.74 1 -24 8 0 41745.0 777.736 1 -25 8 0 94.2681 61.7342 1 -25 -8 0 698.299 225.462 1 -26 -8 0-21.4911 85.4466 1 -26 8 0 78.3880 55.2494 1 -27 -8 0 53.5105 106.471 1 -27 8 0 48.0841 57.9294 1 -28 -8 0 7165.45 558.129 1 -28 8 0 6993.62 368.406 1 -29 -8 0 561.246 213.625 1 -29 8 0 77.9531 78.5599 1 -30 -8 0 20042.5 960.330 1 -30 8 0 19431.0 638.480 1 -31 -8 0 204.158 164.385 1 -31 8 0 61.3158 53.9386 1 -32 8 0 247.547 87.2770 1 -32 -8 0 92.1764 81.5004 1 -33 8 0 111.593 56.0233 1 -33 -8 0-12.4052 99.8283 1 -34 -8 0 995.812 249.940 1 -35 -8 0-55.9889 115.362 1 -36 -8 0 589.030 204.604 1 -37 -8 0 418.032 167.952 1 -38 -8 0 275.931 151.899 1 -39 -8 0-94.0031 94.1602 1 -40 -8 0-154.075 163.441 1 -41 -8 0-146.350 136.893 1 -42 -8 0-58.5010 155.067 1 -43 -8 0 74.7913 84.5938 1 -44 -8 0 209.396 151.323 1 -45 -8 0-49.9052 97.5193 1 -46 -8 0 269.987 132.818 1 -47 -8 0-169.072 158.415 1 0 -9 0 21.6896 29.7675 1 -1 9 0 436.226 57.0785 1 -1 -9 0 409.010 73.5330 1 -2 9 0 23.2745 21.2145 1 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36.4122 1 -19 9 0 43440.1 634.506 1 -19 -9 0 43333.8 1172.18 1 -20 -9 0 412.725 180.867 1 -20 9 0 7.28568 35.3759 1 -21 9 0 4340.99 219.072 1 -21 -9 0 4216.92 390.235 1 -22 9 0 32.6766 38.7353 1 -22 -9 0 132.205 122.537 1 -23 -9 0 1362.68 238.128 1 -23 9 0 1787.95 153.342 1 -24 9 0 109.243 68.0484 1 -24 -9 0 564.197 249.746 1 -25 9 0 54055.5 869.184 1 -25 -9 0 50625.8 1440.84 1 -26 9 0 38.8881 52.5104 1 -26 -9 0 477.957 208.287 1 -27 -9 0 880.288 219.607 1 -27 9 0 1014.55 129.942 1 -28 9 0-14.0953 33.1122 1 -28 -9 0 237.031 128.607 1 -29 9 0 668.821 118.695 1 -29 -9 0 658.411 202.175 1 -30 -9 0-7.05880 149.025 1 -30 9 0 10.8665 36.0631 1 -31 -9 0 970.621 222.360 1 -32 -9 0 21.0348 125.675 1 -33 -9 0 6323.11 586.352 1 -34 -9 0 158.508 141.477 1 -35 -9 0 3223.97 427.683 1 -36 -9 0-175.251 155.108 1 -37 -9 0 375.188 141.794 1 -38 -9 0 129.159 155.056 1 -39 -9 0 1669.06 314.917 1 -40 -9 0-80.7375 157.921 1 -41 -9 0 848.145 247.254 1 -42 -9 0-71.0751 94.6201 1 -43 -9 0 988.401 269.204 1 -44 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37605.5 427.502 1 -10 -10 0 39887.8 934.466 1 -11 10 0 10.4354 13.5580 1 -11 10 0-5.50943 13.5443 1 -11 -10 0 21.6098 60.6918 1 -12 10 0 2534.44 113.414 1 -12 10 0 2625.40 114.598 1 -12 -10 0 2647.67 257.949 1 -13 10 0 14.7263 18.6788 1 -13 -10 0-30.3786 77.3306 1 -13 10 0 24.9085 21.0659 1 -14 10 0 42077.7 481.789 1 -14 -10 0 42383.3 1073.02 1 -15 -10 0 195.364 148.049 1 -15 10 0 9.11702 18.4123 1 -16 -10 0 18066.6 726.705 1 -16 10 0 16866.8 323.657 1 -17 10 0 29.7532 27.2739 1 -17 -10 0 131.201 102.352 1 -18 -10 0 4564.57 381.819 1 -18 10 0 4983.52 189.692 1 -19 -10 0-28.8153 92.2115 1 -19 10 0-7.94448 19.1223 1 -20 10 0 365.158 58.4850 1 -20 -10 0 421.646 126.275 1 -21 10 0 16.8918 33.4497 1 -21 -10 0 95.0304 122.435 1 -22 10 0 15219.3 389.706 1 -22 -10 0 14474.1 740.853 1 -23 -10 0 377.475 186.647 1 -23 10 0 63.2056 47.8441 1 -24 10 0 8378.51 314.471 1 -24 -10 0 8653.87 601.969 1 -25 10 0-26.4320 28.7919 1 -25 -10 0 371.457 183.523 1 -26 -10 0 1625.81 270.198 1 -26 10 0 1806.24 155.248 1 -27 -10 0-5.83954 81.1004 1 -28 -10 0 91.8368 101.934 1 -29 -10 0-112.620 116.272 1 -30 -10 0 3448.95 419.542 1 -31 -10 0 4.55409 94.1899 1 -32 -10 0 2601.44 376.839 1 -33 -10 0 41.6949 89.6422 1 -34 -10 0 3376.93 442.195 1 -35 -10 0-64.1460 106.916 1 -36 -10 0 1893.71 358.458 1 -37 -10 0 83.6747 118.541 1 -38 -10 0 787.001 216.380 1 -39 -10 0-96.1998 130.332 1 -40 -10 0 788.815 217.751 1 -41 -10 0-111.829 130.516 1 -42 -10 0 1091.87 257.832 1 -43 -10 0-116.288 169.510 1 -44 -10 0 1331.06 317.995 1 -45 -10 0-158.213 190.199 1 0 11 0-34.2586 91.4206 2 1 11 0 181.745 77.2448 2 -1 -11 0 279.806 67.4666 1 2 11 0-40.8304 82.6058 2 -2 11 0 44.9061 66.7462 2 -2 -11 0-13.7337 47.4964 1 -3 -11 0 219.900 67.8948 1 -3 11 0 225.953 42.4157 1 -3 11 0 284.015 103.058 2 3 11 0 374.040 120.295 2 4 11 0 29.1370 76.0925 2 -4 11 0 134.868 131.140 2 -4 -11 0 57.8615 42.6132 1 -4 11 0 41.7012 24.8851 1 -5 11 0 38818.4 484.025 1 -5 -11 0 38013.9 835.576 1 5 11 0 37650.5 1047.83 2 -5 11 0 38354.1 1119.60 2 -6 11 0 46.3810 93.7336 2 6 11 0 187.259 112.195 2 -6 -11 0 53.5107 53.0847 1 -6 11 0-34.7084 28.9026 1 -6 11 0 27.1400 28.2243 1 -7 11 0 6113.91 212.048 1 -7 -11 0 6197.41 357.377 1 -7 11 0 5825.11 466.543 2 -7 11 0 4840.97 167.487 1 -8 11 0-2.43020 16.7146 1 -8 11 0-5.08951 13.1780 1 -8 -11 0 40.3057 50.5972 1 -9 11 0 4695.54 164.249 1 -9 11 0 4626.99 145.631 1 -9 -11 0 4556.41 319.486 1 -10 11 0 7.50708 16.9561 1 -10 11 0 0.38140 11.7662 1 -11 -11 0 422.139 114.168 1 -11 11 0 427.768 44.2366 1 -11 11 0 518.375 52.1072 1 -12 -11 0-1.53139 64.9434 1 -12 11 0-2.60405 16.9055 1 -12 11 0-8.81849 9.35320 1 -13 11 0 2521.85 106.854 1 -13 11 0 2637.10 102.416 1 -13 -11 0 2690.19 272.133 1 -14 11 0 24.7795 12.8726 1 -14 -11 0 24.2043 84.6347 1 -14 11 0 18.1710 17.5535 1 -15 -11 0 13337.2 634.490 1 -15 11 0 13270.0 246.806 1 -15 11 0 12692.7 241.343 1 -16 11 0 11.2714 13.9332 1 -16 -11 0 10.5024 78.1046 1 -17 -11 0 1374.63 221.922 1 -17 11 0 1206.65 80.6691 1 -18 -11 0-9.74286 65.8162 1 -18 11 0-9.59317 13.5538 1 -19 -11 0 1406.41 228.326 1 -19 11 0 1499.12 97.3097 1 -20 11 0 40.3849 27.2563 1 -20 -11 0 145.437 152.795 1 -21 -11 0 34100.7 1151.68 1 -21 11 0 32883.3 498.993 1 -22 -11 0 157.159 142.743 1 -22 11 0 45.1447 36.3525 1 -23 -11 0 255.749 117.994 1 -24 -11 0-23.7887 107.636 1 -25 -11 0 1914.59 300.642 1 -26 -11 0-131.180 90.6585 1 -27 -11 0 4042.83 442.632 1 -28 -11 0-123.409 132.071 1 -29 -11 0-47.4224 101.586 1 -30 -11 0 16.0919 107.422 1 -31 -11 0 1628.60 305.406 1 -32 -11 0 51.2942 111.260 1 -33 -11 0 3620.82 464.080 1 -34 -11 0-73.8206 100.860 1 -35 -11 0 2142.71 348.928 1 -36 -11 0 142.685 124.741 1 -37 -11 0 193.816 116.113 1 -38 -11 0 55.1151 128.773 1 -39 -11 0 69.4867 161.445 1 -40 -11 0 111.904 150.411 1 -41 -11 0 64.8217 113.566 1 -42 -11 0-251.074 169.062 1 -43 -11 0 1162.67 304.677 1 -44 -11 0 287.140 233.711 1 0 12 0 5242.96 422.445 2 1 12 0-21.1481 66.7427 2 -1 12 0-19.0961 68.3543 2 2 12 0 2165.82 271.964 2 -2 -12 0 2245.79 195.998 1 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1 13 0 5221.99 437.007 2 -1 13 0 5827.74 469.671 2 -2 13 0-42.8871 80.4616 2 2 13 0-38.2173 88.7145 2 -3 -13 0 575.385 107.346 1 -3 13 0 581.273 170.039 2 3 13 0 915.544 192.101 2 -4 13 0 101.964 107.123 2 -4 -13 0-30.9626 51.5569 1 4 13 0-65.0984 81.3132 2 5 13 0 10451.7 617.511 2 -5 13 0 12036.1 693.410 2 -5 -13 0 11008.2 488.807 1 6 13 0 113.120 169.085 2 -6 13 0-19.0516 175.902 2 -6 -13 0-42.4434 64.3029 1 -6 13 0-14.4650 22.9517 1 -7 13 0 2894.69 124.643 1 -7 13 0 3010.61 163.079 1 7 13 0 2896.92 346.540 2 -7 13 0 2980.31 363.657 2 -7 -13 0 3060.79 273.781 1 -8 13 0-25.8702 89.6207 2 8 13 0-3.87679 73.0555 2 -8 13 0 21.5271 24.2090 1 -8 -13 0-10.3803 55.6886 1 -9 -13 0 1437.31 193.656 1 -9 13 0 1505.66 94.2407 1 -9 13 0 1395.88 254.781 2 9 13 0 1576.62 242.131 2 -10 -13 0 33.0325 55.3081 1 -10 13 0-23.1959 19.9870 1 -11 13 0 7817.71 163.293 1 -11 -13 0 7905.75 470.780 1 -12 -13 0 27.4704 70.3731 1 -12 13 0-3.30890 7.39805 1 -13 -13 0 378.222 131.065 1 -14 -13 0-105.902 100.037 1 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0-48.7454 59.3166 1 -4 14 0 43.6223 78.8563 2 -5 14 0 71.4469 99.5444 2 -5 -14 0-31.8372 54.8565 1 5 14 0 55.9502 117.276 2 -6 -14 0 3244.32 274.694 1 6 14 0 2581.68 319.644 2 -6 14 0 3164.04 180.090 1 -6 14 0 3247.02 395.513 2 -7 14 0 297.659 59.1088 1 -7 14 0 1132.69 277.135 2 7 14 0 836.913 203.634 2 -7 -14 0 319.624 111.418 1 -8 -14 0 21019.4 736.400 1 -8 14 0 21944.9 1025.01 2 8 14 0 19632.5 865.562 2 -8 14 0 18605.8 368.629 1 -9 14 0-28.0225 111.939 2 -9 14 0 0.11346 12.2735 1 9 14 0-39.5172 83.6380 2 -9 -14 0 78.7038 76.5572 1 -10 -14 0 3031.21 293.805 1 10 14 0 2431.47 316.615 2 -11 -14 0-4.60770 57.2773 1 11 14 0-155.550 119.406 2 -12 -14 0 34.5658 76.7174 1 -13 -14 0-9.95621 57.8414 1 -14 -14 0 2178.57 278.706 1 -15 -14 0-126.327 88.1280 1 -16 -14 0 5447.35 437.576 1 -17 -14 0-5.47564 71.9627 1 -18 -14 0 350.178 106.773 1 -19 -14 0-113.569 91.7652 1 -20 -14 0-76.1232 107.018 1 -21 -14 0-173.321 139.906 1 -22 -14 0-57.7089 106.515 1 -23 -14 0-151.832 131.832 1 -24 -14 0 3522.22 412.913 1 -25 -14 0-90.5576 116.325 1 -26 -14 0 3073.41 401.405 1 -27 -14 0 119.153 140.072 1 -28 -14 0 2632.96 386.330 1 -29 -14 0-72.3065 108.199 1 -30 -14 0 1186.75 278.716 1 -31 -14 0-22.3483 126.704 1 -32 -14 0 64.4377 138.419 1 -33 -14 0 57.8609 107.788 1 -34 -14 0 315.588 124.911 1 -35 -14 0 546.610 234.300 1 -36 -14 0 190.452 156.706 1 -37 -14 0 314.444 193.369 1 -38 -14 0 4279.57 548.362 1 -39 -14 0 116.384 142.412 1 -40 -14 0 1312.91 313.151 1 -41 -14 0-51.9811 97.8345 1 0 15 0 5.09858 82.5868 2 1 15 0 1542.89 276.215 2 -1 15 0 1794.60 291.633 2 -2 15 0 15.9119 104.685 2 2 15 0-34.0016 94.9905 2 -3 15 0 6232.34 545.752 2 3 15 0 6328.49 519.941 2 -4 15 0 237.964 222.039 2 4 15 0-122.631 110.138 2 -5 15 0 28745.0 585.372 1 -5 15 0 27133.6 1150.81 2 5 15 0 26456.2 1053.75 2 6 15 0 167.183 106.360 2 -6 15 0 3.73596 154.143 2 -6 -15 0 62.8354 66.7492 1 -6 15 0 25.4269 31.9775 1 7 15 0 75.8789 123.680 2 -7 15 0 41.3136 28.1809 1 -7 15 0 72.6102 192.016 2 -7 -15 0-43.0157 47.4346 1 -8 15 0 5.26128 151.741 2 8 15 0 2.13036 97.8536 2 -8 -15 0-16.8722 61.6161 1 9 15 0 1149.83 226.534 2 -9 -15 0 1305.15 193.424 1 10 15 0 207.650 171.824 2 -10 -15 0 153.651 99.4721 1 11 15 0 19210.0 898.167 2 -11 -15 0 20266.9 788.181 1 12 15 0 20.2246 110.884 2 -12 -15 0 172.723 147.322 1 13 15 0 2001.47 296.643 2 -13 -15 0 2261.35 283.108 1 -14 -15 0 92.5314 96.9342 1 -15 -15 0 727.319 170.693 1 -16 -15 0 10.8911 68.6657 1 -17 -15 0 181.212 107.509 1 -18 -15 0-46.9622 93.4673 1 -19 -15 0 116.429 87.2258 1 -20 -15 0 305.475 122.573 1 -21 -15 0 3077.20 363.361 1 -22 -15 0 116.388 126.518 1 -23 -15 0 727.971 208.215 1 -24 -15 0-92.6039 130.761 1 -25 -15 0 195.168 112.960 1 -26 -15 0 119.334 160.920 1 -27 -15 0 11.2793 141.397 1 -28 -15 0 7.61431 113.267 1 -29 -15 0-93.4821 80.8678 1 -30 -15 0 33.6698 97.9277 1 -31 -15 0 2948.17 422.382 1 -32 -15 0 254.445 177.689 1 -33 -15 0 255.371 122.088 1 -34 -15 0 265.873 182.748 1 -35 -15 0 6878.19 672.318 1 -36 -15 0 166.319 151.957 1 -37 -15 0 515.307 215.319 1 -38 -15 0 122.997 139.447 1 -39 -15 0 1504.24 335.971 1 0 16 0 669.950 208.038 2 -1 16 0-89.8975 131.534 2 1 16 0 59.6410 88.9940 2 -2 16 0 184.981 149.927 2 2 16 0 232.433 131.595 2 -3 16 0 215.746 120.079 2 3 16 0 80.1714 97.9333 2 -4 16 0 6170.19 565.083 2 4 16 0 5543.18 502.450 2 5 16 0-184.732 132.163 2 -5 16 0 63.7268 167.019 2 6 16 0 2394.31 336.158 2 -6 16 0 2403.92 374.435 2 -7 16 0-182.848 165.562 2 -7 -16 0-85.5155 81.5918 1 7 16 0 0.77318 85.2700 2 -8 16 0 2971.83 410.116 2 8 16 0 2836.72 359.495 2 -8 -16 0 2479.19 262.801 1 9 16 0-41.5979 181.151 2 -9 -16 0 10.7861 65.5241 1 10 16 0 12973.3 765.513 2 -10 -16 0 13858.1 654.333 1 -11 -16 0 104.734 85.9063 1 11 16 0 8.15929 145.648 2 12 16 0-57.1644 100.668 2 -12 -16 0-72.5946 100.275 1 -13 -16 0-76.2344 89.8399 1 13 16 0-167.766 159.266 2 -14 -16 0 2306.94 295.384 1 14 16 0 2342.40 336.614 2 15 16 0-127.749 119.518 2 -15 -16 0 35.2016 78.3739 1 -16 -16 0 86.6011 72.4823 1 -17 -16 0 59.4260 96.5126 1 -18 -16 0 1384.01 240.583 1 -19 -16 0 80.5121 93.7088 1 -20 -16 0 244.583 95.4072 1 -21 -16 0 56.9191 73.2203 1 -22 -16 0 496.091 156.638 1 -23 -16 0-110.927 117.960 1 -24 -16 0 301.064 139.875 1 -25 -16 0 158.003 101.337 1 -26 -16 0 4615.69 495.577 1 -27 -16 0 156.849 131.873 1 -28 -16 0 252.938 154.175 1 -29 -16 0 195.272 142.457 1 -30 -16 0 140.194 120.455 1 -31 -16 0-51.1933 96.5881 1 -32 -16 0-11.5381 120.392 1 -33 -16 0 1.87941 125.800 1 -34 -16 0 2393.53 410.818 1 -35 -16 0 243.236 181.968 1 -36 -16 0 314.469 159.610 1 -37 -16 0 197.062 125.436 1 -38 -16 0 1200.15 300.808 1 0 17 0 598.053 211.582 2 1 17 0 2225.16 337.920 2 -1 17 0 2195.30 342.616 2 2 17 0 6.40796 96.1535 2 -2 17 0 50.8789 94.6856 2 3 17 0 943.208 223.317 2 -3 17 0 639.071 202.254 2 -4 17 0 63.2516 138.268 2 4 17 0-44.6975 110.401 2 -5 17 0 2712.66 412.803 2 5 17 0 2632.36 361.282 2 6 17 0 29.5250 116.858 2 -6 17 0 56.3479 149.094 2 7 17 0 2793.72 372.728 2 -7 17 0 2683.74 410.957 2 -8 17 0 83.9708 141.590 2 8 17 0-112.117 100.118 2 9 17 0 949.515 241.757 2 -9 -17 0 692.830 150.528 1 10 17 0 362.323 354.690 2 -10 -17 0 156.739 105.269 1 -11 -17 0 28149.3 962.836 1 11 17 0 25829.6 1117.50 2 12 17 0 133.564 199.910 2 -12 -17 0 63.4910 114.339 1 13 17 0 1005.88 235.557 2 -13 -17 0 1312.15 236.512 1 -14 -17 0-43.5059 71.3383 1 14 17 0 101.292 147.956 2 -15 -17 0 3029.67 346.286 1 15 17 0 2458.33 353.426 2 -16 -17 0-64.1863 117.656 1 16 17 0-13.3856 94.3050 2 -17 -17 0 442.338 149.728 1 17 17 0 520.559 177.247 2 -18 -17 0 99.4558 111.291 1 18 17 0-173.409 139.635 2 -19 -17 0 1785.25 291.849 1 -20 -17 0 2.13845 91.6296 1 -21 -17 0 1760.67 302.837 1 -22 -17 0-130.441 144.968 1 -23 -17 0 2301.99 342.753 1 -24 -17 0-158.730 136.218 1 -25 -17 0 4379.75 486.979 1 -26 -17 0-103.526 104.203 1 -27 -17 0 11.8932 142.995 1 -28 -17 0 186.206 120.923 1 -29 -17 0 2064.62 362.915 1 -30 -17 0 44.1113 107.087 1 -31 -17 0 1325.70 303.657 1 -32 -17 0 70.2956 93.6040 1 -33 -17 0 1431.87 324.377 1 -34 -17 0 29.5419 116.838 1 -35 -17 0 5603.62 623.579 1 -36 -17 0 295.090 180.948 1 -37 -17 0 319.786 175.073 1 0 18 0 766.153 222.988 2 -1 18 0-13.9204 104.622 2 1 18 0-139.163 146.851 2 -2 18 0 124.555 134.065 2 2 18 0 145.228 122.380 2 3 18 0-161.284 124.742 2 -3 18 0-23.4545 102.380 2 4 18 0 834.897 226.035 2 -4 18 0 900.439 245.616 2 -5 18 0 114.292 151.010 2 5 18 0 158.474 129.438 2 -6 18 0 38.2387 127.425 2 6 18 0 240.393 173.963 2 -7 18 0-37.9779 116.360 2 7 18 0 99.1049 87.3690 2 8 18 0 1587.57 280.921 2 9 18 0 237.440 150.467 2 10 18 0 12.7849 81.5870 2 11 18 0 66.8918 115.765 2 -11 -18 0 4.33856 74.7426 1 -12 -18 0 2187.69 282.276 1 12 18 0 1417.81 281.113 2 -13 -18 0 63.1385 66.8194 1 13 18 0 45.9987 95.2498 2 -14 -18 0-35.1651 71.6711 1 14 18 0-134.787 140.000 2 -15 -18 0 30.5116 102.792 1 15 18 0-175.741 149.312 2 -16 -18 0 1261.87 237.061 1 16 18 0 1006.19 223.895 2 -17 -18 0-26.6711 65.9500 1 17 18 0 29.2112 79.9976 2 18 18 0 220.178 136.191 2 -18 -18 0 141.883 90.6917 1 19 18 0-144.780 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21 2 4321.92 582.779 2 3 21 -2 669.355 249.397 2 -3 21 2 1044.76 376.461 2 3 21 2 831.488 296.510 2 4 21 2 1390.41 339.747 2 4 21 -2 1155.55 259.195 2 -4 21 2 1375.48 345.109 2 5 21 -2 196.459 166.407 2 -5 21 2 270.562 188.606 2 5 21 2 229.644 203.164 2 6 21 2-179.758 162.850 2 6 21 -2-133.091 156.181 2 -6 21 2 77.3248 122.700 2 7 21 2-20.2888 117.330 2 -7 21 2 172.137 130.836 2 7 21 -2 346.077 160.103 2 8 21 -2 512.150 213.068 2 8 21 2 405.681 175.702 2 9 21 2-36.3246 109.052 2 9 21 -2-53.7525 92.2938 2 10 21 -2 204.270 141.324 2 10 21 2-41.3587 143.090 2 11 21 2-43.2055 122.586 2 11 21 -2-135.616 116.039 2 12 21 2 146.386 133.177 2 12 21 -2 41.8666 99.7744 2 13 21 -2 605.121 206.536 2 13 21 2 533.813 214.426 2 14 21 2 1301.48 313.632 2 14 21 -2 1186.40 281.066 2 15 21 2 891.602 286.805 2 15 21 -2 703.923 249.424 2 16 21 -2 1109.80 251.200 2 16 21 2 1025.14 282.126 2 17 21 2 699.481 259.794 2 17 21 -2 331.872 152.068 2 18 21 -2-15.5824 109.799 2 18 21 2 742.879 234.968 2 19 21 2 253.384 160.952 2 19 21 -2 176.255 151.815 2 20 21 2 625.862 211.323 2 20 21 -2 1469.77 285.066 2 21 21 -2 813.614 223.299 2 21 21 2 748.791 254.013 2 22 21 2 232.541 171.897 2 22 21 -2 52.3966 85.6846 2 23 21 2 364.315 171.544 2 23 21 -2 86.0389 77.5595 2 24 21 2 252.995 171.992 2 24 21 -2 100.056 85.2732 2 -24 -21 -2 207.429 94.2251 1 25 21 2-65.2285 106.681 2 25 21 -2 75.3858 85.3183 2 -25 -21 -2-60.1867 80.0381 1 26 21 2-39.9562 92.0825 2 -26 -21 -2-208.723 120.329 1 26 21 -2 76.2228 82.9308 2 -27 -21 -2-4.08929 61.0983 1 27 21 -2 124.684 105.538 2 28 21 -2 122.647 97.5030 2 -28 -21 -2-33.7524 72.7146 1 -29 -21 -2 800.109 188.956 1 0 22 -2 3004.20 447.665 2 0 22 2 3580.60 522.273 2 1 22 -2 399.683 215.961 2 1 22 2 604.484 344.494 2 -1 22 2 731.810 329.346 2 2 22 -2 5287.98 581.031 2 -2 22 2 5248.74 628.067 2 2 22 2 6099.14 663.379 2 -3 22 2 360.642 226.921 2 3 22 -2 530.542 209.077 2 3 22 2 834.206 317.802 2 4 22 2 1908.12 380.177 2 4 22 -2 1477.27 311.248 2 -4 22 2 1571.94 355.176 2 -5 22 2 116.585 225.042 2 5 22 2 119.587 181.139 2 5 22 -2 67.9163 105.842 2 6 22 -2 716.480 211.392 2 6 22 2 430.727 184.711 2 -6 22 2 382.928 230.217 2 7 22 -2 102.241 104.387 2 -7 22 2-36.0043 128.782 2 7 22 2-54.3943 135.823 2 8 22 2 416.543 171.159 2 8 22 -2 551.481 172.577 2 9 22 2 74.4701 112.169 2 9 22 -2 25.6291 89.5359 2 10 22 2-94.8874 110.632 2 10 22 -2 88.1433 117.444 2 11 22 -2 449.642 176.377 2 11 22 2 302.687 178.890 2 12 22 2 195.092 144.009 2 12 22 -2-193.923 138.598 2 13 22 2 477.420 199.381 2 13 22 -2 83.5692 78.3302 2 14 22 -2 127.999 111.584 2 14 22 2 155.135 229.188 2 15 22 2 1280.87 319.573 2 15 22 -2 606.365 199.716 2 16 22 2 110.966 102.044 2 16 22 -2 322.672 172.086 2 17 22 -2 267.018 144.354 2 17 22 2 532.147 222.693 2 18 22 -2 83.9806 69.7075 2 18 22 2 359.161 196.071 2 19 22 2-36.5604 119.481 2 19 22 -2-277.323 147.881 2 20 22 -2 88.3677 70.9615 2 20 22 2 172.128 176.638 2 21 22 -2 21.9934 103.190 2 21 22 2 110.869 99.3546 2 22 22 2-94.9205 154.986 2 22 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433.818 1 7 8 -4 6821.30 279.199 2 -7 8 4 6484.13 435.467 2 7 -8 -4 6208.20 203.203 1 -7 -8 -4 7260.70 373.108 1 7 -8 -4 6608.24 217.905 1 -8 8 -4 12.3874 81.5880 1 8 -8 -4 58.3491 22.2724 1 -8 8 4-30.0113 65.6355 2 8 8 -4 93.5098 42.9984 2 -8 -8 -4 12.5568 57.8354 1 8 -8 -4 74.6180 25.3903 1 -9 8 -4 1637.56 217.390 1 9 -8 -4 1706.11 103.281 1 -9 -8 -4 1866.33 207.357 1 -9 8 4 1722.41 238.921 2 9 8 -4 1747.81 147.443 2 9 -8 -4 1722.77 95.3223 1 10 -8 -4 3112.44 134.456 1 10 8 -4 2874.46 195.758 2 -10 -8 -4 2642.37 253.816 1 10 -8 -4 2475.84 111.493 1 -10 8 -4 2944.29 286.178 1 11 -8 -4 1271.11 83.7078 1 -11 8 -4 1222.01 186.675 1 -11 -8 -4 1245.32 175.812 1 11 -8 -4 1216.26 73.7769 1 12 -8 -4 45.5658 15.4037 1 -12 8 -4 27.0385 68.9792 1 -12 -8 -4 95.2141 90.9417 1 12 -8 -4 109.427 26.1544 1 13 -8 -4 2626.03 102.405 1 13 -8 -4 2699.76 118.311 1 -13 -8 -4 2828.65 271.046 1 -13 8 -4 2657.94 267.383 1 -14 8 -4 300.081 105.013 1 14 -8 -4 344.001 36.5139 1 14 -8 -4 372.842 47.4735 1 -14 -8 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4 11 4 88.2271 88.4888 2 -4 11 -4 317.215 111.985 1 -5 11 -4 2991.54 311.506 1 5 -11 -4 2842.05 111.815 1 -5 -11 -4 3041.86 229.392 1 -5 11 4 3278.48 365.843 2 5 11 4 2827.64 334.573 2 -6 11 -4 62.3038 90.0392 1 6 11 4 218.625 96.6906 2 -6 11 4 224.855 130.565 2 -6 -11 -4 106.949 53.5303 1 -7 -11 -4 11.4460 43.2679 1 7 11 4-81.4583 116.396 2 -7 11 4-11.7281 78.4371 2 -7 11 -4 69.2960 90.8436 1 -8 -11 -4 5212.81 332.175 1 -8 11 4 4903.16 466.699 2 -8 11 -4 4442.07 381.693 1 -9 11 -4 3698.77 334.827 1 -9 -11 -4 4076.14 300.925 1 -9 11 4 3656.60 394.380 2 9 11 -4 3963.75 275.878 2 -10 -11 -4 107.009 67.7387 1 10 11 -4 126.193 58.1694 2 -10 11 4 19.7161 94.5716 2 -10 11 -4 162.690 85.3201 1 -11 -11 -4 701.071 141.246 1 11 11 -4 585.056 113.049 2 -11 11 -4 681.444 143.105 1 -12 -11 -4 3717.76 319.973 1 12 11 -4 3380.10 264.308 2 -12 11 -4 3472.06 326.850 1 13 11 -4 212.541 75.9188 2 -13 11 -4 307.326 117.327 1 -13 -11 -4 390.749 126.979 1 -14 11 -4 7097.34 459.962 1 -14 -11 -4 8289.32 490.679 1 14 11 -4 7173.62 393.904 2 -15 -11 -4 1588.95 218.255 1 -15 11 -4 1323.60 198.891 1 -16 -11 -4 197.360 100.211 1 -16 11 -4 252.183 81.9257 1 -17 -11 -4 518.585 151.343 1 -17 11 -4 487.556 126.143 1 -18 11 -4 1743.02 236.452 1 -18 -11 -4 1873.45 253.839 1 -19 11 -4 1876.70 244.928 1 -19 -11 -4 2351.82 293.391 1 -20 11 -4 488.119 128.732 1 -20 -11 -4 496.968 154.770 1 -21 11 -4 189.313 98.9031 1 -21 -11 -4 40.5071 89.9897 1 -22 11 -4 2.28880 53.2892 1 -22 -11 -4-7.46495 102.602 1 -23 11 -4 39.4499 68.4149 1 -23 -11 -4-158.062 128.699 1 -23 -11 4 38.4265 94.4834 1 -24 11 -4 348.897 82.3597 1 -24 -11 -4 436.769 145.055 1 -24 -11 4 690.979 217.112 1 -25 -11 -4 2811.31 354.725 1 -25 -11 4 2683.61 395.586 1 -25 11 -4 2995.72 312.806 1 -26 11 -4 873.332 175.449 1 -26 -11 -4 1352.90 266.445 1 -26 -11 4 1174.78 283.399 1 -27 -11 -4 482.057 165.316 1 -27 -11 4 854.934 249.442 1 -27 11 -4 745.068 166.751 1 -28 11 -4 2175.10 271.544 1 -28 -11 -4 2310.81 336.089 1 -28 -11 4 2020.87 347.642 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894.549 211.192 2 -5 13 -4 774.698 169.187 1 -6 -13 -4 1887.75 191.342 1 6 13 4 1661.13 276.189 2 -6 13 -4 1814.29 249.707 1 -6 13 4 1711.23 287.273 2 6 13 -4 1835.14 221.251 2 -7 -13 -4 51.0152 45.2105 1 -7 13 4-3.25861 118.819 2 7 13 4 70.8501 98.5401 2 7 13 -4 65.6970 48.2773 2 -7 13 -4 154.987 114.406 1 -8 -13 -4 194.313 65.3054 1 8 13 4 186.664 111.814 2 -8 13 -4 268.383 110.222 1 8 13 -4 224.563 97.1426 2 -8 13 4 252.700 133.220 2 9 13 -4-57.8678 58.2691 2 -9 13 -4-55.9638 65.5896 1 -9 -13 -4 22.3196 53.8966 1 9 13 4-215.490 157.964 2 -9 13 4-36.2535 94.4749 2 -10 -13 -4 126.621 63.4153 1 10 13 -4 129.792 61.7958 2 -10 13 -4 216.850 100.063 1 11 13 -4 593.473 121.058 2 -11 -13 -4 557.875 126.472 1 -11 13 -4 433.391 119.620 1 -11 13 4 326.309 158.862 2 12 13 -4-111.817 85.5537 2 -12 -13 -4-39.0012 74.1949 1 -12 13 -4-52.0456 76.2191 1 13 13 -4 193.893 71.0618 2 -13 13 -4 138.565 72.9020 1 -13 -13 -4 48.2214 52.2340 1 -14 13 -4 389.995 120.860 1 -14 -13 -4 423.285 114.935 1 14 13 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437.717 187.089 1 -31 -13 4-190.051 203.413 1 -32 -13 -4 791.349 218.034 1 -32 -13 4 678.498 208.812 1 -33 -13 -4 420.018 149.652 1 -33 -13 4 431.598 163.439 1 -34 -13 -4-57.9115 99.7348 1 -34 -13 4-3.46167 117.485 1 -35 -13 -4-213.345 162.667 1 -35 -13 4-12.0771 148.009 1 -36 -13 -4 273.445 144.046 1 -36 -13 4-64.1964 138.522 1 -37 -13 -4 198.356 157.402 1 -37 -13 4-26.9142 100.356 1 -38 -13 -4 317.557 153.579 1 -38 -13 4 99.5265 94.2160 1 -39 -13 -4 93.9926 99.1526 1 0 14 4 893.504 216.006 2 0 -14 -4 863.940 96.4164 1 -1 14 4 7942.10 627.741 2 1 14 4 8622.66 643.452 2 1 14 -4 7895.81 493.110 2 1 -14 -4 8322.07 259.437 1 -1 -14 -4 8521.62 316.327 1 2 14 4 1099.65 245.223 2 2 14 -4 1130.44 193.775 2 -2 14 4 791.123 216.669 2 -2 -14 -4 982.560 125.770 1 3 14 4 8226.11 631.195 2 -3 14 4 9648.29 682.781 2 3 14 -4 9101.29 516.595 2 -3 14 -4 8351.84 551.225 1 -3 -14 -4 8376.56 363.299 1 -4 -14 -4 448.786 96.3549 1 -4 14 -4 119.635 88.1047 1 -4 14 4 393.865 186.111 2 4 14 -4 193.900 108.341 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598.700 141.011 1 12 14 -4 750.936 153.701 2 -13 14 -4 197.279 83.2246 1 13 14 -4 336.993 104.148 2 -14 14 -4-28.8625 54.2570 1 -14 -14 -4 66.1056 75.9422 1 14 14 -4-77.5505 82.1479 2 -15 -14 -4 6243.13 443.244 1 -15 14 -4 5797.29 432.184 1 15 14 -4 5275.58 398.445 2 -16 -14 -4 3019.95 329.238 1 16 14 -4 2747.24 296.771 2 -16 14 -4 2782.00 297.029 1 -17 -14 -4 4218.75 396.303 1 -17 14 -4 3852.64 347.610 1 17 14 -4 3717.49 342.894 2 -18 -14 -4 3408.06 358.279 1 -18 14 -4 2747.85 298.695 1 18 14 -4 2659.23 284.449 2 -19 -14 -4 2502.65 313.709 1 -19 14 -4 2446.64 276.482 1 19 14 -4 2521.24 288.638 2 -20 -14 -4 134.882 117.596 1 -20 14 -4 188.949 101.861 1 20 14 -4 330.497 111.222 2 -21 14 -4 6799.98 456.268 1 -21 -14 -4 6751.09 528.237 1 -22 -14 -4 484.429 168.854 1 -22 14 -4 151.399 89.9973 1 -23 14 -4 211.318 68.0894 1 -23 -14 -4 232.756 123.541 1 -24 -14 -4 127.572 95.0260 1 -25 -14 -4 2151.45 321.132 1 -26 -14 -4 2321.86 338.943 1 -27 -14 -4 1532.84 283.071 1 -28 -14 -4 667.110 227.238 1 -29 -14 -4 3514.47 437.508 1 -30 -14 -4 518.715 206.680 1 -31 -14 -4-21.1405 91.4488 1 -32 -14 -4 325.755 196.461 1 -33 -14 -4 249.374 173.752 1 -34 -14 -4-50.3748 113.518 1 -35 -14 -4 572.495 202.006 1 -36 -14 -4 36.2786 79.7891 1 -37 -14 -4 21.9763 114.750 1 -38 -14 -4-92.2043 108.393 1 0 15 4 4982.89 512.736 2 -1 15 4 80.6391 130.590 2 1 15 4 126.183 122.278 2 1 15 -4 57.0922 63.5351 2 -2 -15 -4 9.49920 35.1119 1 -2 15 4 81.0635 104.540 2 2 15 -4-110.895 93.9339 2 3 15 -4 2196.41 265.983 2 3 15 4 1882.53 324.479 2 -3 15 4 2245.89 351.529 2 -3 -15 -4 2044.41 174.905 1 -3 15 -4 2198.77 286.572 1 -4 15 -4 1218.32 232.366 1 4 15 4 1058.72 252.683 2 4 15 -4 895.986 168.485 2 -4 15 4 1389.21 284.295 2 -4 -15 -4 1213.47 142.240 1 -5 -15 -4 10.7905 37.0456 1 5 15 4-94.9568 120.379 2 -5 15 -4-44.8966 77.5753 1 -5 15 4-95.3459 133.818 2 5 15 -4 2.04710 56.8873 2 6 15 4 5835.25 550.279 2 6 15 -4 6156.15 430.395 2 -6 15 4 5056.36 533.594 2 -6 15 -4 6012.76 454.730 1 -6 -15 -4 5668.07 334.089 1 -7 -15 -4 99.1659 64.4919 1 7 15 -4 194.081 97.2415 2 -7 15 4 158.024 138.092 2 -7 15 -4 221.037 105.860 1 7 15 4 118.832 153.724 2 -8 15 -4 3006.59 316.448 1 8 15 -4 2995.41 302.843 2 -8 15 4 2859.13 418.597 2 8 15 4 2406.74 353.791 2 -8 -15 -4 3073.73 266.865 1 -9 15 -4 76.5076 75.1134 1 -9 -15 -4 13.1724 56.2351 1 9 15 -4 83.8942 78.9959 2 9 15 4 9.00099 93.4725 2 -9 15 4-162.358 103.924 2 -10 -15 -4 2154.55 237.390 1 -10 15 -4 1933.38 266.719 1 10 15 4 2184.38 391.392 2 10 15 -4 1988.45 253.552 2 -10 15 4 1771.04 351.187 2 -11 -15 -4 4943.15 368.221 1 11 15 4 4633.99 505.722 2 -11 15 -4 4953.83 402.222 1 11 15 -4 4642.05 380.602 2 -12 -15 -4 6428.25 429.447 1 12 15 4 6722.01 618.808 2 12 15 -4 6710.80 458.316 2 -12 15 -4 6527.35 464.753 1 -13 -15 -4 1124.59 196.654 1 -13 15 -4 1027.37 184.157 1 13 15 4 684.595 228.479 2 13 15 -4 922.240 173.011 2 -14 15 -4 145.733 71.7103 1 -14 -15 -4 250.078 113.962 1 14 15 -4 89.8086 52.4200 2 -15 -15 -4 887.311 177.974 1 15 15 -4 775.127 155.115 2 -15 15 -4 447.194 123.274 1 -16 -15 -4 341.996 108.519 1 16 15 -4 312.820 112.307 2 -16 15 -4 569.014 143.014 1 -17 -15 -4-126.797 111.233 1 -17 15 -4-22.4976 75.7090 1 17 15 -4-33.8264 73.5965 2 -18 -15 -4-85.6861 96.9613 1 -18 15 -4-45.0531 59.7139 1 18 15 -4 8.11423 52.4292 2 -19 -15 -4 15.3830 75.0614 1 19 15 -4 218.129 90.2381 2 -19 15 -4 166.128 95.0957 1 20 15 -4-52.0039 55.9436 2 -20 -15 -4-13.3563 79.4480 1 -20 15 -4 2.03920 44.4253 1 -21 -15 -4 740.416 184.543 1 21 15 -4 841.771 171.183 2 -22 -15 -4-94.5991 78.9128 1 22 15 -4-45.9379 64.1599 2 -23 -15 -4 423.185 150.716 1 23 15 -4 632.157 157.080 2 -24 -15 -4-16.6010 95.3612 1 -25 -15 -4-26.5314 71.8314 1 -26 -15 -4 1624.85 305.617 1 -27 -15 -4 619.924 222.595 1 -28 -15 -4 1232.55 286.654 1 -29 -15 -4 410.720 181.634 1 -30 -15 -4 1242.19 271.130 1 -31 -15 -4 134.416 141.020 1 -32 -15 -4 681.961 218.226 1 -33 -15 -4-74.7345 111.338 1 -34 -15 -4-11.8901 97.3293 1 -35 -15 -4 93.6647 113.774 1 -36 -15 -4 104.195 103.178 1 -37 -15 -4 262.372 84.9404 1 0 16 4 33.1499 107.623 2 1 16 4 63.0680 121.030 2 -1 16 4 102.748 93.6620 2 -2 16 4 2024.96 344.016 2 2 16 -4 2528.38 310.686 2 -2 16 -4 2328.20 301.941 1 2 16 4 2106.39 351.180 2 -3 16 -4 841.826 189.942 1 -3 16 4 526.648 202.586 2 3 16 4 870.452 232.709 2 3 16 -4 809.251 183.005 2 4 16 4 4778.04 518.248 2 -4 16 4 4342.97 513.732 2 4 16 -4 4505.11 410.774 2 -4 16 -4 4422.25 412.646 1 -5 16 4 4150.68 487.352 2 5 16 -4 4316.75 390.490 2 5 16 4 3991.85 480.807 2 -5 16 -4 4369.31 403.155 1 -5 -16 -4 4291.19 276.541 1 -6 -16 -4 255.617 74.6292 1 6 16 4 188.987 98.0710 2 6 16 -4 83.5046 50.4828 2 -6 16 4 238.570 135.418 2 -6 16 -4 306.230 127.994 1 -7 -16 -4 441.542 100.456 1 -7 16 -4 196.143 105.723 1 7 16 4 267.619 131.360 2 7 16 -4 415.490 132.385 2 -7 16 4 191.930 131.761 2 -8 -16 -4 485.299 109.432 1 -8 16 -4 498.316 134.946 1 8 16 4 345.848 154.193 2 8 16 -4 315.951 104.293 2 -8 16 4 289.550 153.654 2 9 16 -4 1600.70 237.594 2 9 16 4 967.001 255.731 2 -9 16 4 1644.46 341.324 2 -9 -16 -4 1619.24 199.741 1 -9 16 -4 1434.09 232.072 1 10 16 4 1260.66 286.939 2 -10 -16 -4 1273.56 183.960 1 -10 16 4 839.938 251.610 2 10 16 -4 883.296 167.665 2 -10 16 -4 1246.71 204.750 1 -11 -16 -4 416.756 112.127 1 11 16 4 400.179 198.999 2 -11 16 -4 256.409 94.6267 1 11 16 -4 279.082 88.7772 2 12 16 4 175.118 121.768 2 -12 -16 -4 285.874 98.4694 1 12 16 -4 221.198 81.0750 2 -12 16 -4 322.127 107.200 1 -13 -16 -4 11.5204 51.6987 1 -13 16 -4 126.471 71.5070 1 13 16 4-100.332 117.983 2 13 16 -4 121.439 61.2881 2 -14 16 -4 1285.76 201.930 1 -14 -16 -4 1389.25 209.966 1 14 16 4 1303.20 286.479 2 14 16 -4 1160.59 199.105 2 -15 -16 -4 583.572 153.000 1 15 16 4 749.205 236.932 2 15 16 -4 636.037 153.180 2 -15 16 -4 295.593 92.8477 1 -16 -16 -4-1.99595 70.9711 1 16 16 4-10.1570 109.432 2 16 16 -4 71.5537 60.7031 2 -16 16 -4-53.9116 75.6837 1 -17 -16 -4 582.044 162.302 1 17 16 -4 386.356 110.350 2 -18 -16 -4-128.088 112.630 1 18 16 -4 82.4656 64.7267 2 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329.855 1 -28 -8 -5 2743.54 373.572 1 -29 -8 -5 836.169 221.123 1 -29 8 -5 734.905 185.071 1 -30 -8 -5 1804.29 306.953 1 -30 8 -5 1790.00 278.379 1 -31 -8 -5 232.731 138.640 1 -31 8 -5 228.022 117.807 1 -32 -8 -5 2168.23 350.047 1 -32 8 -5 1870.41 287.882 1 -33 -8 -5 400.223 196.028 1 -33 8 -5 28.7015 89.1149 1 -34 -8 -5 414.917 156.192 1 -34 8 -5 564.757 153.656 1 -35 -8 -5 112.271 130.520 1 -35 8 -5 134.150 113.151 1 -36 -8 -5 5065.30 546.938 1 -36 8 -5 4839.71 458.685 1 -37 8 -5 1641.76 278.804 1 -37 -8 -5 1613.96 320.082 1 -38 -8 -5 49.9573 98.6783 1 -38 8 -5 227.590 126.624 1 -39 -8 -5 611.653 199.162 1 -39 8 -5 601.889 167.119 1 -40 -8 -5 1488.39 322.218 1 -40 8 -5 1345.94 249.346 1 -41 -8 -5 1390.93 334.786 1 -41 8 -5 750.294 200.684 1 -42 -8 -5 2046.50 364.425 1 0 9 5-9.78113 65.7670 2 0 -9 -5 57.4778 59.3940 1 1 9 5 18283.6 762.639 2 -1 9 5 18280.7 763.546 2 -1 -9 -5 19240.0 569.957 1 1 -9 -5 18821.3 539.067 1 2 9 5 9800.73 560.960 2 -2 9 -5 10234.1 609.615 1 -2 9 5 9539.33 552.506 2 -2 -9 -5 9929.32 421.637 1 2 -9 -5 10709.9 390.332 1 3 -9 -5 78.7936 40.3958 1 -3 9 -5 113.869 128.612 1 3 9 5-23.8726 91.5767 2 -3 9 5 126.676 88.7896 2 -3 -9 -5 141.952 75.5184 1 -4 9 5 2153.87 272.348 2 -4 -9 -5 2351.74 225.864 1 -4 9 -5 1955.94 278.406 1 4 -9 -5 2063.12 161.529 1 4 9 5 2377.12 280.650 2 5 9 5 27003.9 958.018 2 -5 9 5 26624.2 932.118 2 -5 -9 -5 28717.6 776.641 1 -5 9 -5 26905.1 973.394 1 5 -9 -5 28205.9 561.693 1 -6 -9 -5 1736.02 206.255 1 -6 9 5 1131.88 198.956 2 6 -9 -5 1615.19 136.018 1 -6 9 -5 1303.37 246.834 1 7 9 -5 17869.7 420.259 2 -7 9 -5 18310.4 818.830 1 -7 -9 -5 18418.7 650.971 1 -7 9 5 18235.9 790.988 2 7 -9 -5 18517.7 433.851 1 -8 9 -5 3669.52 373.604 1 -8 9 5 3743.20 364.690 2 8 9 -5 3306.36 181.895 2 -8 -9 -5 3658.75 293.229 1 8 -9 -5 3694.71 188.331 1 9 -9 -5 251.349 48.8208 1 9 9 -5 301.418 56.4784 2 -9 9 5 400.722 133.364 2 -9 -9 -5 273.095 93.4082 1 -9 9 -5 166.576 74.1323 1 10 -9 -5 274.741 51.4466 1 10 9 -5 295.135 56.1269 2 -10 -9 -5 163.869 83.4324 1 -10 9 -5 322.657 112.797 1 11 -9 -5 635.020 69.1498 1 11 9 -5 670.617 85.4197 2 -11 9 -5 583.219 146.202 1 -11 -9 -5 875.196 162.207 1 12 -9 -5 911.064 78.1363 1 -12 9 -5 975.367 188.998 1 -12 -9 -5 734.218 148.176 1 12 9 -5 1042.12 113.563 2 13 -9 -5 1847.45 105.078 1 -13 9 -5 1957.72 264.224 1 13 9 -5 1608.34 145.420 2 -13 -9 -5 2238.37 262.197 1 14 -9 -5 518.351 57.7372 1 -14 9 -5 551.771 161.720 1 14 9 -5 502.107 83.7095 2 -14 -9 -5 550.013 128.271 1 -15 -9 -5 2556.31 285.578 1 -15 9 -5 2401.34 294.685 1 -16 -9 -5 632.780 161.482 1 -16 9 -5 538.445 157.405 1 -17 9 -5 10661.4 621.075 1 -17 -9 -5 10167.0 588.169 1 -18 -9 -5 1838.25 264.400 1 -18 9 -5 1917.85 263.622 1 -19 -9 -5-33.9861 69.1942 1 -19 9 -5-5.84145 69.4165 1 -20 -9 -5 637.913 161.190 1 -20 9 -5 738.081 162.044 1 -21 9 -5 569.458 150.716 1 -21 -9 -5 495.704 144.820 1 -22 -9 -5 835.157 193.644 1 -22 9 -5 772.412 170.047 1 -23 9 -5 231.101 106.749 1 -23 -9 -5 74.0536 99.4708 1 -24 9 -5 1549.18 242.957 1 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60.2035 91.0528 2 -1 -10 -5 158.024 68.0596 1 1 -10 -5 157.535 59.9692 1 2 10 5 14273.6 713.411 2 -2 10 5 13676.9 704.556 2 -2 10 -5 13589.6 718.552 1 2 -10 -5 14819.8 434.486 1 -2 -10 -5 14807.0 499.260 1 3 10 5 488.701 126.598 2 -3 10 -5 354.111 155.309 1 -3 10 5 358.136 133.660 2 -3 -10 -5 528.531 110.999 1 3 -10 -5 453.908 77.8847 1 -4 10 5 1099.27 200.858 2 4 10 5 1010.34 198.733 2 -4 -10 -5 1504.58 174.567 1 4 -10 -5 1247.57 117.826 1 -4 10 -5 1328.61 223.772 1 -5 10 -5 122.327 87.4079 1 5 10 5 137.630 101.956 2 -5 10 5 118.700 71.6470 2 -5 -10 -5 177.860 68.9622 1 5 -10 -5 134.810 38.6691 1 6 10 5 450.481 145.707 2 -6 10 5 320.157 116.270 2 -6 -10 -5 623.368 133.413 1 6 -10 -5 400.928 61.9323 1 -6 10 -5 291.124 100.658 1 -7 10 -5 830.733 190.940 1 7 10 5 811.074 188.803 2 -7 10 5 927.091 198.903 2 7 10 -5 810.865 102.531 2 -7 -10 -5 1001.62 154.796 1 7 -10 -5 810.118 81.2007 1 -8 10 -5 8161.25 542.297 1 -8 -10 -5 9024.15 456.396 1 -8 10 5 7859.91 556.566 2 8 -10 -5 8032.11 232.578 1 8 10 -5 7913.10 318.507 2 -9 10 -5 3384.28 354.081 1 9 10 -5 3413.21 211.433 2 -9 10 5 3225.16 362.396 2 9 -10 -5 3318.46 137.621 1 -9 -10 -5 3837.03 313.829 1 10 10 -5 628.607 89.8475 2 10 -10 -5 519.685 49.1624 1 -10 -10 -5 490.956 118.507 1 -10 10 5 534.312 157.349 2 -10 10 -5 573.188 157.863 1 11 10 -5 3766.85 228.719 2 -11 -10 -5 3899.02 324.965 1 -11 10 -5 3669.94 363.013 1 -12 10 -5-48.6054 94.3705 1 12 10 -5-0.13661 31.9341 2 -12 -10 -5 15.3908 58.6184 1 -13 10 -5 1664.92 244.546 1 -13 -10 -5 2075.47 255.964 1 -14 10 -5 2425.27 296.373 1 -14 -10 -5 2824.26 294.136 1 -15 10 -5 141.115 114.646 1 -15 -10 -5 24.7713 80.3990 1 -16 -10 -5 1985.69 268.708 1 -16 10 -5 1887.82 273.056 1 -17 -10 -5 256.752 130.602 1 -17 10 -5 9.34542 74.6794 1 -18 -10 -5 957.919 188.291 1 -18 10 -5 1097.97 205.330 1 -19 -10 -5 382.270 128.911 1 -19 10 -5 312.730 98.8124 1 -20 10 -5 567.918 155.930 1 -20 -10 -5 375.308 137.320 1 -21 10 -5 2997.01 339.549 1 -21 -10 -5 2801.60 350.166 1 -22 10 -5 1852.93 263.834 1 -22 -10 -5 1892.76 289.984 1 -23 10 -5 565.917 157.914 1 -23 -10 -5 362.741 156.212 1 -24 10 -5-30.0443 99.0054 1 -24 -10 -5-64.0382 105.721 1 -25 10 -5 520.692 135.620 1 -25 -10 -5 324.147 140.761 1 -26 10 -5 1081.17 210.772 1 -26 -10 -5 1013.64 200.611 1 -27 10 -5 877.751 197.234 1 -27 -10 -5 563.732 176.443 1 -28 -10 -5 3286.41 403.253 1 -28 10 -5 3029.99 344.270 1 -29 -10 -5 301.925 174.653 1 -29 10 -5 73.7762 116.977 1 -30 -10 -5 1401.58 277.944 1 -30 10 -5 1150.58 220.500 1 -31 -10 -5 69.9659 136.268 1 -31 10 -5 128.028 112.301 1 -32 -10 -5 2197.70 353.501 1 -32 10 -5 1756.14 267.694 1 -33 -10 -5 227.736 113.303 1 -33 10 -5 72.8598 67.9908 1 -34 -10 -5 136.852 147.963 1 -34 10 -5-138.945 105.728 1 -35 -10 -5 536.010 206.313 1 -35 10 -5 686.069 179.796 1 -36 -10 -5 1021.89 279.892 1 -36 10 -5 755.330 190.829 1 -37 -10 -5-57.2911 144.230 1 -38 -10 -5 213.241 141.161 1 -39 -10 -5-85.5268 115.709 1 -40 -10 -5 591.928 224.356 1 0 11 5-71.5440 115.182 2 0 -11 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334.586 2 -3 13 5 2095.46 317.714 2 4 13 5 63.6085 89.6495 2 -4 -13 -5 196.547 69.8163 1 -4 13 5 222.370 131.395 2 -4 13 -5 280.260 126.963 1 -5 -13 -5 1915.35 192.375 1 -5 13 -5 2181.65 299.190 1 5 13 5 1313.30 247.294 2 -5 13 5 1979.80 316.631 2 -6 -13 -5 799.339 135.055 1 6 13 5 928.919 225.645 2 -6 13 5 1159.35 240.490 2 6 13 -5 657.693 123.892 2 -6 13 -5 756.420 187.306 1 -7 -13 -5 6021.97 362.773 1 -7 13 -5 5917.28 479.432 1 7 13 5 5289.71 501.139 2 7 13 -5 6005.99 354.352 2 -7 13 5 5485.38 522.493 2 -8 13 5 4437.42 491.162 2 -8 -13 -5 4609.96 327.412 1 8 13 -5 4359.72 303.301 2 -8 13 -5 4759.83 421.773 1 8 13 5 4287.55 460.821 2 -9 13 -5 697.192 172.014 1 9 13 5 602.028 187.166 2 -9 -13 -5 749.484 141.916 1 9 13 -5 687.404 127.873 2 -9 13 5 669.546 220.176 2 10 13 5 878.222 219.410 2 -10 -13 -5 893.428 166.452 1 10 13 -5 790.829 132.106 2 -10 13 5 758.798 212.611 2 -10 13 -5 585.273 132.993 1 11 13 5 173.978 98.0894 2 -11 -13 -5 419.376 116.006 1 11 13 -5 426.662 92.2167 2 -11 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2830.10 393.614 2 -4 15 -5 122.598 104.148 1 4 15 5 161.687 130.208 2 -4 15 5-115.956 126.826 2 -5 -15 -5 2134.04 200.855 1 -5 15 -5 1781.86 272.501 1 -5 15 5 1909.02 334.877 2 5 15 5 2259.43 363.164 2 -6 -15 -5 2314.76 219.143 1 6 15 5 2211.09 350.350 2 6 15 -5 1855.67 228.941 2 -6 15 5 2217.48 369.065 2 -6 15 -5 2207.63 305.042 1 -7 -15 -5 1611.14 185.262 1 7 15 5 1082.25 247.178 2 -7 15 -5 1405.52 255.038 1 7 15 -5 1659.80 215.798 2 -7 15 5 1187.39 283.100 2 -8 15 -5 321.336 135.940 1 -8 -15 -5 293.974 95.5014 1 8 15 5-97.7331 144.622 2 -8 15 5 245.926 145.954 2 -9 -15 -5 1248.87 181.784 1 9 15 5 1005.97 240.558 2 -9 15 5 880.467 233.963 2 -9 15 -5 1047.36 217.761 1 -10 -15 -5 67.9299 51.2551 1 10 15 5-203.130 166.234 2 -10 15 5-76.1791 144.283 2 -10 15 -5-132.441 113.985 1 -11 -15 -5 492.545 123.650 1 11 15 5 344.935 132.755 2 -11 15 -5 407.136 119.117 1 -12 -15 -5 214.297 88.5201 1 -12 15 -5-45.6932 76.6274 1 12 15 5 31.9742 117.263 2 -13 15 -5 298.140 113.060 1 -13 -15 -5 568.353 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344.121 2 -8 -13 -7 1895.80 231.841 1 -8 13 7 1843.89 303.855 2 -8 13 -7 1590.44 284.990 1 8 13 7 1666.30 288.382 2 9 13 7-52.8993 111.857 2 -9 -13 -7-49.9609 56.1450 1 -9 13 -7-60.0627 97.6766 1 10 13 7-42.9936 87.5253 2 -10 -13 -7-14.2927 53.9102 1 -10 13 -7 48.6441 86.5207 1 11 13 7 48.7152 110.050 2 -11 13 -7 17.9349 79.8075 1 -11 -13 -7 98.9050 89.3333 1 -12 -13 -7 4124.38 374.307 1 12 13 7 3396.69 423.799 2 -12 13 -7 4470.99 467.370 1 -13 -13 -7 3059.81 346.950 1 13 13 7 2964.67 411.529 2 -13 13 -7 3408.76 413.793 1 -14 13 -7 436.230 183.415 1 14 13 7 282.966 162.714 2 -14 -13 -7 477.415 144.055 1 -15 13 -7 343.416 152.386 1 15 13 7 69.7073 80.8511 2 -15 -13 -7 398.048 145.282 1 16 13 7 271.381 141.848 2 -16 -13 -7 272.081 119.876 1 -16 13 -7 36.2268 71.8235 1 -17 -13 -7 5.84622 70.1688 1 -17 13 -7 94.7161 71.2906 1 -18 -13 -7 1768.24 280.509 1 -18 13 -7 1545.93 282.326 1 -19 13 -7 825.286 210.827 1 -19 -13 -7 775.905 195.449 1 -20 -13 -7 600.120 185.902 1 -20 13 -7 190.476 122.938 1 -21 -13 -7 208.233 129.905 1 -21 13 -7 178.535 127.631 1 -22 -13 -7-149.412 135.719 1 -22 13 -7 30.7658 107.649 1 -23 -13 -7 2787.63 376.382 1 -23 13 -7 2414.77 346.847 1 -24 13 -7-75.3292 67.8000 1 -24 -13 -7 47.2267 85.7825 1 -25 13 -7-123.896 73.4586 1 -25 -13 -7-39.4356 90.4949 1 -26 13 -7 240.143 93.3780 1 -26 -13 -7 299.817 124.661 1 -27 13 -7 1217.59 241.707 1 -27 -13 -7 940.630 226.446 1 -28 13 -7 1941.29 301.596 1 -28 -13 -7 1270.39 264.272 1 -29 13 -7 86.3304 71.8941 1 -29 -13 -7 456.829 181.014 1 -30 13 -7 207.877 114.203 1 -30 -13 -7 149.105 126.100 1 -31 -13 -7 127.600 99.7587 1 -32 -13 -7 2798.22 397.372 1 -33 -13 -7 1201.38 269.202 1 0 14 7 47.0649 127.944 2 0 14 -7 78.4963 92.2321 1 1 14 -7 1460.52 306.123 1 -1 14 -7 1886.93 331.847 1 1 14 7 1624.41 294.343 2 -1 14 7 1353.05 275.632 2 -2 14 -7 86.2567 116.636 1 2 14 7 88.8151 81.3442 2 2 14 -7 70.6934 120.917 1 -2 14 7 133.027 103.938 2 3 14 -7 88.9546 128.106 1 3 14 7-8.30691 113.559 2 -3 14 7-20.0786 74.9030 2 -3 14 -7 14.3142 95.0408 1 4 14 7 305.940 120.518 2 -4 14 7 518.196 159.586 2 -4 14 -7 410.714 136.229 1 4 14 -7 365.488 145.198 1 -5 14 -7 420.464 167.029 1 5 14 7 486.025 173.079 2 -5 14 7 192.032 119.129 2 -6 14 -7-51.6898 108.084 1 6 14 7 103.526 86.2726 2 -6 14 7-101.126 103.102 2 -7 14 -7 435.358 167.160 1 7 14 7 391.746 146.830 2 -7 14 7 695.241 221.311 2 8 14 7 126.052 140.093 2 -8 -14 -7 109.756 78.7448 1 -8 14 7 16.9706 127.067 2 -8 14 -7-168.273 142.430 1 9 14 7 1089.51 236.701 2 -9 -14 -7 1468.34 210.185 1 -9 14 -7 1578.58 285.784 1 10 14 7-113.515 125.141 2 -10 -14 -7 25.0436 53.0858 1 -10 14 -7-143.588 145.094 1 -11 14 -7 99.0859 98.6459 1 11 14 7-41.0095 118.942 2 -11 -14 -7 189.315 104.174 1 -12 14 -7 157.690 110.206 1 12 14 7 627.867 196.866 2 -12 -14 -7 502.656 133.001 1 -13 -14 -7 3732.82 358.736 1 13 14 7 3560.66 454.196 2 -13 14 -7 3606.03 422.417 1 -14 14 -7-94.1805 133.319 1 14 14 7 2.16278 160.920 2 -14 -14 -7 47.7009 88.1748 1 -15 -14 -7 2997.61 338.659 1 15 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1530.80 309.213 1 -8 9 -9 1958.78 349.858 1 8 9 9 1926.80 262.791 2 -9 9 -9 1985.85 355.474 1 9 9 9 1469.90 220.131 2 9 9 -9 2209.91 391.177 1 -9 -9 -9 1704.38 266.591 1 10 9 -9 2163.81 396.780 1 -10 9 -9 2242.85 366.547 1 10 9 9 1380.46 226.423 2 -10 -9 -9 1822.85 273.752 1 -11 9 -9 2822.37 413.928 1 11 9 9 2379.25 306.593 2 11 9 -9 3048.41 465.905 1 -11 -9 -9 2731.28 353.966 1 12 9 9 5313.81 462.721 2 -12 9 -9 6483.43 624.982 1 -12 -9 -9 5902.79 510.082 1 12 9 -9 5295.56 565.363 1 13 9 9-35.6856 85.1532 2 -13 -9 -9-18.6045 78.5874 1 -13 9 -9-2.78977 100.407 1 14 9 9 38.4066 65.6907 2 -14 -9 -9 213.076 105.578 1 -14 9 -9 250.823 126.019 1 15 9 9 218.087 115.637 2 -15 -9 -9 280.786 113.808 1 -15 9 -9 149.326 91.0243 1 16 9 9 750.834 181.007 2 -16 9 -9 752.598 214.920 1 -16 -9 -9 639.078 193.918 1 17 9 9 733.689 191.389 2 -17 9 -9 882.763 236.221 1 -17 -9 -9 1000.20 226.375 1 -18 9 -9 566.182 193.447 1 -18 -9 -9 328.500 115.029 1 -19 9 -9-250.039 169.766 1 -19 -9 -9 114.415 99.4239 1 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-7 -11 883.362 189.236 1 -4 7 -11 1095.47 284.596 1 4 7 -11 1320.93 283.323 1 5 7 -11 236.351 157.280 1 -5 -7 -11 455.253 145.367 1 -5 7 -11 608.029 230.422 1 6 7 -11 999.098 281.514 1 -6 7 -11 750.970 239.213 1 -6 -7 -11 344.242 123.548 1 -7 7 -11 2011.84 369.989 1 -7 -7 -11 1422.98 256.495 1 7 7 -11 1824.95 357.573 1 -8 7 -11 167.126 128.951 1 -8 -7 -11-127.782 115.815 1 8 7 -11 198.126 154.545 1 -9 -7 -11-47.7968 97.3042 1 9 7 -11-149.905 100.121 1 -9 7 -11 18.8457 155.439 1 -10 -7 -11 387.592 144.184 1 10 7 -11 361.357 165.822 1 -10 7 -11 177.028 128.482 1 -11 -7 -11 421.647 167.382 1 11 7 -11 617.848 210.478 1 -11 7 -11 745.913 242.408 1 -12 -7 -11 3122.51 391.136 1 -12 7 -11 3757.50 502.266 1 12 7 -11 2997.51 438.109 1 -13 -7 -11 212.034 135.162 1 -13 7 -11 333.519 206.246 1 13 7 -11 441.343 201.278 1 14 7 -11 1660.14 319.905 1 -14 7 -11 1785.29 341.232 1 -14 -7 -11 1871.80 308.128 1 15 7 -11 852.857 228.381 1 -15 7 -11 909.817 247.890 1 -15 -7 -11 1495.91 284.244 1 16 7 -11 26.0543 83.2250 1 -16 7 -11 47.4818 122.625 1 -16 -7 -11-74.7073 92.2775 1 17 7 -11 206.862 146.101 1 -17 7 -11 34.0868 110.447 1 -17 -7 -11-78.2429 95.9833 1 -18 7 -11-17.1118 92.8660 1 18 7 -11 226.738 152.894 1 -18 -7 -11-111.389 106.278 1 19 7 -11-0.62580 92.5863 1 -19 -7 -11 87.6352 86.3971 1 -20 -7 -11-1.78902 92.9863 1 0 8 -11-132.193 164.357 1 -1 8 -11 26.8924 138.205 1 1 8 -11 30.1890 100.537 1 -2 8 -11 177.548 176.978 1 2 8 -11-193.049 163.103 1 -3 -8 -11 2133.47 290.481 1 -3 8 -11 2522.55 408.476 1 3 8 -11 2297.50 389.862 1 4 8 -11 481.022 227.428 1 -4 -8 -11 158.350 99.4610 1 -4 8 -11 399.986 186.854 1 -5 -8 -11 74.4095 72.7277 1 5 8 -11 109.176 116.443 1 -5 8 -11 185.237 142.119 1 -6 -8 -11-156.338 93.5178 1 -6 8 -11 97.9266 121.591 1 6 8 -11 185.994 165.053 1 -7 -8 -11 225.912 98.7518 1 -7 8 -11 535.101 186.298 1 7 8 -11 272.657 145.632 1 -8 -8 -11 462.279 144.107 1 -8 8 -11 474.333 199.648 1 8 8 -11 794.475 237.245 1 -9 -8 -11 1094.00 229.936 1 9 8 -11 1196.87 298.976 1 -9 8 -11 1349.62 300.915 1 10 8 -11 2873.83 436.109 1 -10 -8 -11 3111.14 371.160 1 -10 8 -11 2406.00 407.069 1 11 8 -11 875.428 253.957 1 -11 8 -11 1083.15 293.568 1 -11 -8 -11 1032.10 230.240 1 -12 8 -11 7488.20 714.514 1 12 8 -11 6888.56 664.298 1 -12 -8 -11 6859.88 559.603 1 13 8 -11 317.932 190.382 1 -13 8 -11 0.67886 148.877 1 -13 -8 -11 159.524 119.868 1 14 8 -11 42.6774 153.802 1 -14 8 -11 58.2610 111.173 1 -14 -8 -11 12.2426 82.5938 1 15 8 -11 211.090 122.547 1 -15 8 -11 720.240 237.596 1 -15 -8 -11 547.158 154.850 1 16 8 -11 926.685 253.826 1 -16 8 -11 1148.43 305.197 1 -16 -8 -11 958.275 221.914 1 17 8 -11 1088.46 275.196 1 -17 -8 -11 1543.06 263.749 1 -18 -8 -11 275.069 143.576 1 -19 -8 -11 46.9091 86.3635 1 0 9 -11-30.7935 125.269 1 -1 9 -11 707.201 226.788 1 1 9 -11 599.267 211.104 1 -2 9 -11 192.460 145.828 1 2 9 -11 179.141 140.458 1 -3 9 -11 1131.17 276.198 1 3 9 -11 1022.46 276.104 1 4 9 -11 1656.76 325.688 1 -4 9 -11 1542.45 327.721 1 5 9 -11 89.7871 149.093 1 -5 9 -11 159.017 135.304 1 -6 9 -11 2874.84 442.809 1 6 9 -11 2231.56 391.097 1 -7 9 -11-85.7919 139.493 1 7 9 -11-66.4829 90.5684 1 -8 9 -11-16.8189 118.580 1 8 9 -11 14.3841 121.618 1 -8 -9 -11 105.998 103.985 1 -9 9 -11-156.222 155.671 1 9 9 -11 244.489 155.923 1 -9 -9 -11 156.141 102.160 1 10 9 -11 316.668 194.770 1 -10 -9 -11 288.823 139.642 1 -10 9 -11 79.2317 146.678 1 11 9 -11 660.508 218.844 1 -11 9 -11 451.584 182.057 1 -11 -9 -11 348.347 129.592 1 -12 9 -11-56.2638 92.5199 1 -12 -9 -11 86.5502 68.7025 1 12 9 -11 1.95726 90.7406 1 13 9 -11 1024.57 261.900 1 -13 9 -11 1226.46 282.319 1 -13 -9 -11 898.799 200.702 1 14 9 -11 126.577 129.944 1 -14 9 -11 371.557 177.550 1 -14 -9 -11-170.532 100.439 1 -15 -9 -11 13.3231 92.4922 1 -16 -9 -11-30.4033 72.0999 1 -17 -9 -11-288.351 130.497 1 -18 -9 -11 352.708 158.632 1 -19 -9 -11-128.888 103.487 1 0 10 -11 155.659 158.244 1 -1 10 -11 775.534 248.846 1 1 10 -11 275.703 158.527 1 -2 10 -11 408.746 220.763 1 2 10 -11 165.507 173.199 1 3 10 -11 2629.15 430.525 1 -3 10 -11 2719.09 437.517 1 4 10 -11 322.571 180.259 1 -4 10 -11 268.599 124.437 1 5 10 -11-147.477 154.132 1 -5 10 -11-94.6241 126.031 1 -6 10 -11 951.158 268.372 1 6 10 -11 978.037 262.931 1 -7 10 -11 777.721 243.820 1 7 10 -11 704.560 228.590 1 -8 10 -11 1468.75 326.396 1 8 10 -11 1427.89 305.316 1 -9 10 -11 982.039 263.434 1 9 10 -11 1304.55 287.582 1 10 10 -11-181.241 98.1270 1 -10 10 -11 118.407 146.016 1 11 10 -11 285.858 146.008 1 -11 10 -11 112.987 118.884 1 -12 10 -11 203.926 143.275 1 -14 -10 -11 188.635 96.8094 1 -15 -10 -11 177.193 115.245 1 -16 -10 -11 477.094 152.289 1 -17 -10 -11 570.628 167.922 1 0 11 -11 111.521 140.779 1 -1 11 -11 2341.73 400.922 1 1 11 -11 1951.46 372.750 1 -2 11 -11 353.720 189.192 1 2 11 -11-126.002 93.0671 1 3 11 -11 1710.24 346.494 1 -3 11 -11 1878.74 361.066 1 4 11 -11 121.628 156.135 1 -4 11 -11-182.527 153.278 1 5 11 -11-10.4733 126.525 1 -5 11 -11-112.775 166.786 1 -6 11 -11 689.808 214.185 1 6 11 -11 1156.30 300.055 1 -7 11 -11 133.420 104.786 1 7 11 -11-14.5395 117.188 1 -8 11 -11 272.588 113.466 1 0 0 -12 349.464 174.150 1 -1 0 -12 1275.94 266.713 1 1 0 -12 1308.61 280.483 1 -2 0 -12-95.1516 89.4583 1 2 0 -12 39.3764 97.6347 1 3 0 -12 439.658 165.542 1 -3 0 -12 332.964 154.975 1 4 0 -12 1365.35 276.481 1 -4 0 -12 1400.78 297.539 1 5 0 -12 2225.33 340.816 1 -5 0 -12 2831.75 401.959 1 6 0 -12 407.721 170.938 1 -6 0 -12 538.814 193.687 1 7 0 -12 2680.41 367.409 1 -7 0 -12 3129.02 424.632 1 8 0 -12-69.2798 106.256 1 -8 0 -12 116.404 122.779 1 9 0 -12 1990.34 317.992 1 -9 0 -12 1682.98 315.692 1 10 0 -12 419.371 173.493 1 -10 0 -12 706.590 227.916 1 11 0 -12 659.458 181.184 1 -11 0 -12 693.896 219.047 1 -12 0 -12 27.1392 79.8841 1 12 0 -12-32.7988 76.9348 1 -13 0 -12 134.420 152.941 1 13 0 -12 224.417 139.902 1 14 0 -12 205.905 140.177 1 15 0 -12 2770.63 348.152 1 16 0 -12 524.043 170.347 1 17 0 -12-154.262 120.733 1 0 -1 -12 258.990 103.264 1 0 1 -12 244.102 131.597 1 1 1 -12-69.6286 110.427 1 -1 -1 -12-163.660 132.181 1 1 -1 -12-65.8731 99.1907 1 -1 1 -12-82.7518 129.844 1 2 1 -12-70.8479 114.651 1 -2 -1 -12-4.58907 88.4429 1 -2 1 -12-310.566 191.759 1 2 -1 -12-32.9942 106.385 1 3 1 -12-65.3296 95.0401 1 -3 -1 -12-0.57997 90.3680 1 -3 1 -12 100.193 90.2663 1 3 -1 -12 141.348 129.007 1 4 1 -12-147.461 97.9699 1 -4 -1 -12-51.3338 75.0821 1 -4 1 -12 12.7136 91.8252 1 4 -1 -12 81.0009 107.784 1 5 -1 -12 2085.93 319.772 1 5 1 -12 1767.52 301.877 1 -5 -1 -12 2240.25 353.905 1 -5 1 -12 2293.08 374.595 1 6 -1 -12 216.261 126.748 1 6 1 -12 135.745 107.770 1 -6 -1 -12 197.256 122.059 1 -6 1 -12 292.356 175.555 1 7 -1 -12 296.133 147.312 1 7 1 -12 178.764 107.424 1 -7 -1 -12 407.653 170.312 1 -7 1 -12 392.715 187.514 1 8 -1 -12 132.432 95.2581 1 8 1 -12-120.927 161.110 1 -8 -1 -12-37.6440 102.919 1 9 -1 -12-61.2303 110.899 1 9 1 -12-154.773 94.8232 1 -9 -1 -12 16.2706 84.5847 1 -9 1 -12-19.3742 100.506 1 10 -1 -12 210.059 113.878 1 -10 -1 -12 560.472 179.021 1 10 1 -12 496.690 172.009 1 -10 1 -12 555.010 196.288 1 11 -1 -12 12.7764 94.3206 1 -11 -1 -12 391.235 169.152 1 -11 1 -12 49.6007 92.8606 1 11 1 -12 289.028 133.301 1 12 -1 -12 205.585 133.309 1 -12 -1 -12 320.060 139.122 1 -12 1 -12 38.4762 78.7781 1 12 1 -12 405.874 151.485 1 -13 -1 -12 354.637 129.376 1 13 -1 -12 243.176 87.9475 1 13 1 -12 432.631 172.842 1 14 -1 -12 144.165 118.274 1 14 1 -12 224.274 103.029 1 15 -1 -12 447.523 140.395 1 15 1 -12 257.272 112.784 1 16 1 -12 101.457 108.675 1 17 1 -12 568.131 156.022 1 18 1 -12 500.127 164.881 1 0 2 -12 877.760 229.744 1 0 -2 -12 578.282 186.934 1 1 2 -12-111.800 114.499 1 -1 -2 -12 267.148 118.727 1 1 -2 -12 212.542 100.318 1 -1 2 -12 229.392 125.135 1 2 2 -12-142.425 147.815 1 -2 -2 -12 126.448 70.6213 1 2 -2 -12-29.3116 93.8610 1 -2 2 -12 44.9446 87.1086 1 3 2 -12 621.353 185.403 1 -3 -2 -12 567.097 181.152 1 3 -2 -12 579.724 182.300 1 -3 2 -12 545.158 214.684 1 4 2 -12 219.643 75.1757 1 -4 -2 -12 463.677 162.637 1 -4 2 -12 537.072 185.375 1 4 -2 -12 290.121 131.907 1 5 2 -12 1960.62 340.027 1 -5 -2 -12 2594.29 382.009 1 -5 2 -12 2530.52 404.804 1 5 -2 -12 2228.87 328.595 1 -6 -2 -12 3220.77 423.717 1 6 2 -12 2408.88 372.901 1 -6 2 -12 2748.90 419.423 1 6 -2 -12 2325.10 329.511 1 7 2 -12-229.772 124.162 1 -7 -2 -12 51.6454 117.026 1 -7 2 -12 304.176 175.331 1 7 -2 -12 118.622 106.543 1 8 -2 -12 962.702 205.518 1 -8 -2 -12 489.357 177.595 1 8 2 -12 820.165 217.992 1 -8 2 -12 870.843 207.580 1 9 -2 -12 33.2997 65.2024 1 -9 -2 -12 62.5924 62.8856 1 9 2 -12-1.74031 112.422 1 -9 2 -12 132.185 131.927 1 10 -2 -12 412.802 151.989 1 -10 -2 -12 354.723 122.265 1 10 2 -12 506.845 168.092 1 -10 2 -12 535.114 195.948 1 -11 -2 -12 3704.17 460.407 1 11 -2 -12 2932.36 347.588 1 11 2 -12 3362.82 420.153 1 12 -2 -12 310.846 139.415 1 -12 -2 -12 229.147 178.463 1 -12 2 -12 237.329 187.933 1 12 2 -12 314.818 141.531 1 -13 -2 -12 1413.60 285.952 1 13 2 -12 898.679 228.839 1 14 2 -12 60.6362 86.8415 1 15 2 -12 395.463 149.177 1 16 2 -12 831.560 209.220 1 0 3 -12-4.91720 111.813 1 0 -3 -12-118.997 146.568 1 -1 3 -12 150.723 91.1129 1 1 3 -12-256.427 155.964 1 -1 -3 -12-217.685 148.652 1 1 -3 -12 13.4492 68.1993 1 -2 3 -12 362.015 156.658 1 2 3 -12 164.126 93.6334 1 -2 -3 -12 321.638 133.073 1 2 -3 -12 122.928 76.9823 1 3 3 -12 353.909 164.849 1 -3 -3 -12 119.187 118.856 1 3 -3 -12 185.607 110.357 1 -3 3 -12-120.037 126.728 1 4 3 -12 404.205 161.859 1 -4 -3 -12 691.170 199.019 1 4 -3 -12 504.214 152.608 1 -4 3 -12 834.687 235.516 1 -5 -3 -12 3366.28 416.426 1 5 -3 -12 3706.13 403.894 1 -5 3 -12 3709.93 480.383 1 5 3 -12 3828.56 476.726 1 -6 -3 -12 41.1230 104.072 1 6 3 -12 66.7591 118.749 1 -6 3 -12 291.642 207.220 1 6 -3 -12 239.130 124.981 1 -7 -3 -12 1292.26 249.649 1 7 3 -12 1110.50 252.394 1 -7 3 -12 1334.28 298.170 1 7 -3 -12 901.715 201.183 1 -8 -3 -12-74.5910 113.953 1 8 3 -12-14.9718 88.0404 1 -8 3 -12-63.7583 139.184 1 8 -3 -12 55.6449 73.4301 1 -9 -3 -12 205.635 70.7872 1 9 3 -12 309.843 170.757 1 -9 3 -12 382.157 182.772 1 9 -3 -12 454.041 156.016 1 -10 -3 -12 579.554 194.517 1 -10 3 -12 559.185 216.783 1 10 3 -12 621.986 190.347 1 -11 -3 -12 29.7428 128.479 1 -11 3 -12 313.256 185.100 1 11 3 -12 177.136 117.295 1 -12 -3 -12 486.509 190.186 1 12 3 -12 766.907 231.100 1 -13 -3 -12 1810.70 321.116 1 13 3 -12 1525.70 291.065 1 14 3 -12 109.646 95.8516 1 15 3 -12 886.014 214.803 1 0 4 -12-235.012 152.019 1 0 -4 -12-135.861 114.381 1 -1 4 -12-139.500 136.056 1 1 4 -12-278.166 161.713 1 -1 -4 -12 110.810 89.7957 1 1 -4 -12 91.9277 70.7741 1 -2 4 -12 622.489 207.703 1 2 4 -12 421.894 178.944 1 -2 -4 -12 241.052 134.295 1 2 -4 -12 439.436 157.234 1 -3 4 -12 110.060 120.738 1 3 4 -12 174.989 97.1454 1 -3 -4 -12 129.858 117.116 1 3 -4 -12-68.7905 100.831 1 4 4 -12 301.415 157.445 1 -4 -4 -12 379.500 121.855 1 4 -4 -12 384.036 129.113 1 -4 4 -12 347.170 159.003 1 -5 -4 -12 57.3479 68.1139 1 5 4 -12 149.525 152.068 1 5 -4 -12 56.5794 92.8150 1 -5 4 -12 136.210 130.047 1 -6 -4 -12 897.350 216.019 1 6 4 -12 1185.05 265.838 1 6 -4 -12 1155.85 215.937 1 -6 4 -12 1257.40 281.140 1 -7 -4 -12 244.059 124.959 1 7 4 -12 406.648 151.851 1 -7 4 -12 730.954 245.113 1 -8 -4 -12 799.501 212.078 1 8 4 -12 1009.51 243.906 1 -8 4 -12 952.222 262.680 1 -9 -4 -12 116.135 96.3663 1 -9 4 -12 96.2073 115.083 1 9 4 -12 254.384 155.379 1 -10 -4 -12 229.945 131.208 1 10 4 -12 68.4399 101.734 1 -11 -4 -12 1372.75 268.682 1 11 4 -12 1311.89 277.054 1 -12 -4 -12 474.590 176.243 1 12 4 -12 296.097 161.375 1 -13 -4 -12 126.931 75.0240 1 13 4 -12 518.426 183.631 1 0 5 -12 272.387 139.816 1 0 -5 -12 122.739 60.2663 1 -1 5 -12-200.685 162.593 1 1 5 -12-64.8987 115.294 1 -1 -5 -12-201.117 139.388 1 1 -5 -12-40.2307 72.3805 1 -2 5 -12 109.519 114.835 1 -2 -5 -12 23.7514 64.4204 1 2 -5 -12 5.46133 67.8278 1 -3 5 -12-149.191 131.264 1 -3 -5 -12 27.6382 77.8765 1 3 5 -12-268.461 174.706 1 -4 5 -12 753.193 244.097 1 -4 -5 -12 337.500 119.605 1 4 5 -12 506.155 197.928 1 -5 -5 -12 709.603 178.135 1 5 5 -12 1100.29 263.936 1 -5 5 -12 1422.77 305.678 1 -6 -5 -12 886.055 210.065 1 6 5 -12 1326.38 298.721 1 -6 5 -12 1446.83 306.255 1 -7 -5 -12 238.858 119.945 1 -7 5 -12 76.1343 106.152 1 -8 -5 -12 619.028 184.858 1 8 5 -12 667.053 210.610 1 -9 -5 -12 448.985 154.434 1 9 5 -12 329.919 141.523 1 -10 -5 -12 183.054 119.887 1 10 5 -12 71.8101 114.105 1 -11 -5 -12 520.550 166.245 1 -12 -5 -12 211.177 139.427 1 -13 -5 -12-83.0741 71.1541 1 0 6 -12 385.243 177.963 1 -1 6 -12-188.959 160.643 1 1 6 -12-281.100 174.475 1 -2 6 -12-69.8063 174.659 1 -2 -6 -12 32.8994 63.0702 1 -3 6 -12 165.609 118.373 1 -3 -6 -12 115.127 74.4372 1 3 6 -12 422.458 178.724 1 -4 6 -12 2323.11 389.097 1 -4 -6 -12 1837.86 277.411 1 4 6 -12 2023.87 348.804 1 -5 -6 -12 1127.02 225.396 1 5 6 -12 1500.03 308.827 1 -6 -6 -12 651.366 190.211 1 6 6 -12 536.065 193.375 1 -7 -6 -12 2737.26 350.857 1 -8 -6 -12 1470.66 266.208 1 -9 -6 -12 1415.94 258.771 1 -10 -6 -12 486.444 154.774 1 -11 -6 -12 505.798 164.512 1 -12 -6 -12 109.059 94.8540 1 -6 -7 -12 1723.80 269.221 1 -7 -7 -12 324.530 141.744 1 -8 -7 -12 656.000 178.741 1 -9 -7 -12 462.435 177.218 1 -10 -7 -12-44.0714 87.6824 1 -11 -7 -12 108.925 91.4389 1 0 0 0 0.00 0.00 0 TITL RCH5 in Pccn REM Pccn (#56, found as Pnaa in -cba setting) CELL 0.71073 29.582312 15.197111 7.430342 90.0000 90.0000 90.0000 ZERR 7.00 0.001004 0.000823 0.000226 0.0000 0.0000 0.0000 LATT 1 SYMM -x+1/2,-y+1/2, z SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y,-z+1/2 SFAC C H N O S Mn UNIT 91.00 98.00 35.00 56.00 7.00 7.00 TREF HKLF 4 END ; _shelx_hkl_checksum 74963 _shelx_res_file ; shelx.res created by SHELXL-2014/7 TITL shelxt_a.res in Pccn REM Old TITL RCH5 in Pccn REM SHELXT solution in Pccn REM R1 0.200, Rweak 0.084, Alpha 0.025, Orientation as input REM Formula found by SHELXT: C15 N4 O2 S CELL 0.71073 29.5823 15.1971 7.4303 90.000 90.000 90.000 ZERR 8.000 0.0010 0.0008 0.0002 0.000 0.000 0.000 LATT 1 SYMM 1/2-X, 1/2-Y, Z SYMM -X, 1/2+Y, 1/2-Z SYMM 1/2+X, -Y, 1/2-Z SFAC C H N O S UNIT120 168 24 16 8 temp -173.15 L.S. 5 0 21 acta 51 conf BOND $H htab HTAB N1 O2 EQIV $1 -x+1, -y+1, -z+1 HTAB N2 O1_$1 HTAB N3 O1_$1 ABIN WGHT 0.057300 0.930800 FVAR 2.90514 S1 5 0.350053 0.459409 0.307356 11.00000 0.01858 0.04279 = 0.02381 -0.01162 -0.00243 0.00557 O1 4 0.519098 0.448653 0.301654 11.00000 0.01774 0.03079 = 0.01583 -0.00508 -0.00209 0.00553 N1 3 0.445763 0.420493 0.256024 11.00000 0.01819 0.02091 = 0.01446 -0.00391 0.00158 0.00349 AFIX 43 H1A 2 0.424536 0.396897 0.188529 11.00000 -1.20000 AFIX 0 N2 3 0.435105 0.457965 0.419709 11.00000 0.01747 0.02867 = 0.01291 -0.00340 -0.00026 0.00787 AFIX 43 H2A 2 0.455494 0.462208 0.505512 11.00000 -1.20000 AFIX 0 N3 3 0.388378 0.540632 0.588550 11.00000 0.01600 0.03667 = 0.01717 -0.00803 -0.00093 0.00887 AFIX 43 H3B 2 0.413357 0.555712 0.644990 11.00000 -1.20000 AFIX 0 C1 1 0.498674 0.385673 0.019095 11.00000 0.01912 0.01494 = 0.01256 -0.00046 0.00031 0.00430 O2 4 0.423176 0.344493 -0.042844 11.00000 0.01830 0.02732 = 0.02305 -0.00787 -0.00183 0.00180 C2 1 0.467035 0.347586 -0.098658 11.00000 0.02128 0.01534 = 0.01651 -0.00186 -0.00030 0.00349 C3 1 0.480831 0.314720 -0.264645 11.00000 0.02927 0.01900 = 0.01737 -0.00528 0.00014 0.00181 AFIX 43 H3A 2 0.459377 0.288720 -0.343535 11.00000 -1.20000 AFIX 0 C4 1 0.525827 0.319928 -0.314754 11.00000 0.03387 0.02038 = 0.01646 -0.00359 0.00664 0.00319 AFIX 43 H4A 2 0.535111 0.297019 -0.427826 11.00000 -1.20000 AFIX 0 C5 1 0.557402 0.358138 -0.201900 11.00000 0.02369 0.02081 = 0.01942 0.00039 0.00656 0.00359 AFIX 43 H5A 2 0.588229 0.361828 -0.236920 11.00000 -1.20000 AFIX 0 C6 1 0.543449 0.390942 -0.037134 11.00000 0.02002 0.01707 = 0.01605 0.00054 0.00154 0.00360 AFIX 43 H6A 2 0.565080 0.417824 0.039727 11.00000 -1.20000 AFIX 0 C7 1 0.390003 0.305951 -0.158493 11.00000 0.02383 0.03149 = 0.03627 -0.01239 -0.00710 0.00250 AFIX 137 H7A 2 0.360139 0.310462 -0.102156 11.00000 -1.50000 H7B 2 0.397380 0.243860 -0.178630 11.00000 -1.50000 H7C 2 0.389753 0.337115 -0.273958 11.00000 -1.50000 AFIX 0 C8 1 0.488673 0.420569 0.201682 11.00000 0.01813 0.01747 = 0.01291 -0.00003 0.00045 0.00543 C9 1 0.392276 0.488214 0.445228 11.00000 0.01766 0.02555 = 0.01523 -0.00061 0.00095 0.00625 C10 1 0.345755 0.574774 0.658554 11.00000 0.01709 0.02966 = 0.01537 -0.00309 0.00116 0.00822 AFIX 13 H10A 2 0.324002 0.580649 0.556240 11.00000 -1.20000 AFIX 0 C11 1 0.353949 0.665594 0.738032 11.00000 0.01840 0.02836 = 0.02144 -0.00270 -0.00160 0.00649 AFIX 23 H11A 2 0.364761 0.705817 0.642474 11.00000 -1.20000 H11B 2 0.377699 0.661832 0.831585 11.00000 -1.20000 AFIX 0 C12 1 0.310696 0.702422 0.820770 11.00000 0.02152 0.02920 = 0.02134 -0.00476 -0.00244 0.00984 AFIX 23 H12A 2 0.317307 0.759681 0.878602 11.00000 -1.20000 H12B 2 0.288143 0.712619 0.724568 11.00000 -1.20000 AFIX 0 C13 1 0.291116 0.639749 0.959636 11.00000 0.02979 0.03573 = 0.02077 -0.00399 0.00646 0.01307 AFIX 23 H13A 2 0.312424 0.634074 1.061718 11.00000 -1.20000 H13B 2 0.262393 0.664077 1.006540 11.00000 -1.20000 AFIX 0 C14 1 0.282479 0.549546 0.878586 11.00000 0.02742 0.03508 = 0.02581 -0.00111 0.01020 0.00489 AFIX 23 H14A 2 0.258942 0.554233 0.784356 11.00000 -1.20000 H14B 2 0.271232 0.509220 0.973162 11.00000 -1.20000 AFIX 0 C15 1 0.325590 0.512168 0.796828 11.00000 0.02749 0.02801 = 0.02136 -0.00126 0.00494 0.00799 AFIX 23 H15A 2 0.347939 0.501410 0.893529 11.00000 -1.20000 H15B 2 0.318795 0.455116 0.738479 11.00000 -1.20000 AFIX 0 HKLF 4 REM shelxt_a.res in Pccn REM R1 = 0.0512 for 5943 Fo > 4sig(Fo) and 0.0810 for all 8579 data REM 191 parameters refined using 0 restraints END WGHT 0.0549 0.9274 REM Instructions for potential hydrogen bonds HTAB N1 O2 HTAB N2 O1_$1 HTAB N3 O1_$1 REM Highest difference peak 0.566, deepest hole -0.491, 1-sigma level 0.062 Q1 1 0.4824 0.3696 -0.0327 11.00000 0.05 0.57 Q2 1 0.5529 0.3732 -0.1161 11.00000 0.05 0.55 Q3 1 0.4706 0.3251 -0.1828 11.00000 0.05 0.50 Q4 1 0.4948 0.4047 0.1139 11.00000 0.05 0.49 Q5 1 0.4577 0.4884 0.4637 11.00000 0.05 0.47 Q6 1 0.3857 0.5111 0.5276 11.00000 0.05 0.45 Q7 1 0.3349 0.5463 0.7161 11.00000 0.05 0.40 Q8 1 0.5229 0.3815 0.0062 11.00000 0.05 0.39 Q9 1 0.3061 0.5383 0.8465 11.00000 0.05 0.36 Q10 1 0.3787 0.4759 0.3675 11.00000 0.05 0.36 Q11 1 0.5381 0.3475 -0.2522 11.00000 0.05 0.36 Q12 1 0.4697 0.4168 0.2535 11.00000 0.05 0.34 Q13 1 0.4997 0.4467 0.2540 11.00000 0.05 0.33 Q14 1 0.4151 0.4783 0.4414 11.00000 0.05 0.33 Q15 1 0.3522 0.6183 0.7078 11.00000 0.05 0.33 Q16 1 0.5055 0.3182 -0.2662 11.00000 0.05 0.31 Q17 1 0.4497 0.3428 -0.0562 11.00000 0.05 0.31 Q18 1 0.5009 0.3001 -0.2984 11.00000 0.05 0.30 Q19 1 0.5048 0.4230 0.2514 11.00000 0.05 0.30 Q20 1 0.2993 0.5191 0.8143 11.00000 0.05 0.29 ; _shelx_res_checksum 94470 _shelx_fab_file ; 6 0 0 -71.17 0.00 8 0 0 34.56 0.00 10 0 0 -8.02 0.00 12 0 0 -7.44 0.00 14 0 0 14.11 0.00 16 0 0 -14.80 0.00 18 0 0 11.84 0.00 20 0 0 -7.31 0.00 22 0 0 3.26 0.00 24 0 0 -1.12 0.00 26 0 0 1.05 0.00 28 0 0 -2.18 0.00 30 0 0 3.31 0.00 32 0 0 -3.73 0.00 34 0 0 3.27 0.00 36 0 0 -2.07 0.00 38 0 0 0.49 0.00 40 0 0 0.96 0.00 42 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0.00 5 0 10 0.68 0.00 6 0 10 0.23 0.00 7 0 10 -0.59 0.00 8 0 10 0.15 0.00 9 0 10 0.47 0.00 10 0 10 -0.46 0.00 11 0 10 -0.28 0.00 12 0 10 0.57 0.00 13 0 10 0.09 0.00 14 0 10 -0.50 0.00 15 0 10 -0.02 0.00 16 0 10 0.35 0.00 17 0 10 0.16 0.00 18 0 10 -0.24 0.00 19 0 10 -0.38 0.00 20 0 10 0.14 0.00 21 0 10 0.47 0.00 22 0 10 0.01 0.00 23 0 10 -0.26 0.00 24 0 10 -0.19 0.00 25 0 10 -0.19 0.00 26 0 10 0.29 0.00 27 0 10 0.60 0.00 28 0 10 -0.22 0.00 29 0 10 -0.73 0.00 0 1 10 0.63 0.00 1 1 10 0.57 0.00 2 1 10 -0.59 0.00 3 1 10 -0.52 0.00 4 1 10 0.52 0.00 5 1 10 0.35 0.00 6 1 10 -0.45 0.00 7 1 10 -0.04 0.00 8 1 10 0.37 0.00 9 1 10 -0.29 0.00 10 1 10 -0.25 0.00 11 1 10 0.47 0.00 12 1 10 0.08 0.00 13 1 10 -0.44 0.00 14 1 10 0.04 0.00 15 1 10 0.30 0.00 16 1 10 -0.01 0.00 17 1 10 -0.18 0.00 18 1 10 -0.17 0.00 19 1 10 0.12 0.00 20 1 10 0.34 0.00 21 1 10 -0.04 0.00 22 1 10 -0.28 0.00 23 1 10 -0.09 0.00 24 1 10 -0.05 0.00 25 1 10 0.22 0.00 26 1 10 0.47 0.00 27 1 10 -0.23 0.00 28 1 10 -0.73 0.00 29 1 10 0.11 0.00 0 2 10 0.41 0.00 1 2 10 -0.09 0.00 2 2 10 -0.40 0.00 3 2 10 0.06 0.00 4 2 10 0.34 0.00 5 2 10 -0.03 0.00 6 2 10 -0.16 0.00 7 2 10 0.02 0.00 8 2 10 -0.09 0.00 9 2 10 0.01 0.00 10 2 10 0.26 0.00 11 2 10 -0.09 0.00 12 2 10 -0.24 0.00 13 2 10 0.19 0.00 14 2 10 0.06 0.00 15 2 10 -0.21 0.00 16 2 10 0.09 0.00 17 2 10 0.11 0.00 18 2 10 -0.11 0.00 19 2 10 0.04 0.00 20 2 10 0.06 0.00 21 2 10 -0.10 0.00 22 2 10 -0.05 0.00 23 2 10 -0.06 0.00 24 2 10 0.11 0.00 25 2 10 0.38 0.00 26 2 10 -0.15 0.00 27 2 10 -0.67 0.00 28 2 10 0.09 0.00 29 2 10 0.74 0.00 30 2 10 0.04 0.00 0 3 10 0.46 0.00 1 3 10 -0.28 0.00 2 3 10 -0.44 0.00 3 3 10 0.27 0.00 4 3 10 0.39 0.00 5 3 10 -0.19 0.00 6 3 10 -0.32 0.00 7 3 10 0.03 0.00 8 3 10 0.29 0.00 9 3 10 0.09 0.00 10 3 10 -0.31 0.00 11 3 10 -0.04 0.00 12 3 10 0.36 0.00 13 3 10 -0.20 0.00 14 3 10 -0.37 0.00 15 3 10 0.45 0.00 16 3 10 0.29 0.00 17 3 10 -0.52 0.00 18 3 10 -0.15 0.00 19 3 10 0.39 0.00 20 3 10 0.03 0.00 21 3 10 -0.20 0.00 22 3 10 -0.05 0.00 23 3 10 0.10 0.00 24 3 10 0.22 0.00 25 3 10 -0.08 0.00 26 3 10 -0.47 0.00 27 3 10 0.06 0.00 28 3 10 0.63 0.00 0 4 10 -0.26 0.00 1 4 10 -0.83 0.00 2 4 10 0.26 0.00 3 4 10 0.68 0.00 4 4 10 -0.22 0.00 5 4 10 -0.49 0.00 6 4 10 0.11 0.00 7 4 10 0.37 0.00 8 4 10 -0.01 0.00 9 4 10 -0.39 0.00 10 4 10 0.07 0.00 11 4 10 0.47 0.00 12 4 10 -0.36 0.00 13 4 10 -0.51 0.00 14 4 10 0.73 0.00 15 4 10 0.42 0.00 16 4 10 -0.94 0.00 17 4 10 -0.24 0.00 18 4 10 0.84 0.00 19 4 10 0.04 0.00 20 4 10 -0.54 0.00 21 4 10 0.07 0.00 22 4 10 0.26 0.00 23 4 10 -0.04 0.00 24 4 10 -0.11 0.00 25 4 10 -0.12 0.00 26 4 10 0.07 0.00 27 4 10 0.31 0.00 28 4 10 -0.01 0.00 0 5 10 -1.08 0.00 1 5 10 0.28 0.00 2 5 10 0.93 0.00 3 5 10 -0.26 0.00 4 5 10 -0.58 0.00 5 5 10 0.18 0.00 6 5 10 0.30 0.00 7 5 10 -0.09 0.00 8 5 10 -0.27 0.00 9 5 10 0.11 0.00 10 5 10 0.43 0.00 11 5 10 -0.38 0.00 12 5 10 -0.60 0.00 13 5 10 0.82 0.00 14 5 10 0.60 0.00 15 5 10 -1.17 0.00 16 5 10 -0.41 0.00 17 5 10 1.21 0.00 18 5 10 0.12 0.00 19 5 10 -0.92 0.00 20 5 10 0.12 0.00 21 5 10 0.51 0.00 22 5 10 -0.22 0.00 23 5 10 -0.23 0.00 24 5 10 0.17 0.00 25 5 10 0.12 0.00 26 5 10 -0.03 0.00 27 5 10 -0.09 0.00 0 6 10 0.20 0.00 1 6 10 1.17 0.00 2 6 10 -0.20 0.00 3 6 10 -0.79 0.00 4 6 10 0.19 0.00 5 6 10 0.33 0.00 6 6 10 -0.15 0.00 7 6 10 -0.13 0.00 8 6 10 0.17 0.00 9 6 10 0.28 0.00 10 6 10 -0.37 0.00 11 6 10 -0.57 0.00 12 6 10 0.77 0.00 13 6 10 0.75 0.00 14 6 10 -1.17 0.00 15 6 10 -0.67 0.00 16 6 10 1.33 0.00 17 6 10 0.41 0.00 18 6 10 -1.13 0.00 19 6 10 -0.14 0.00 20 6 10 0.70 0.00 21 6 10 -0.05 0.00 22 6 10 -0.31 0.00 23 6 10 0.12 0.00 24 6 10 0.13 0.00 25 6 10 -0.10 0.00 26 6 10 -0.12 0.00 27 6 10 0.03 0.00 0 7 10 1.29 0.00 1 7 10 0.05 0.00 2 7 10 -1.07 0.00 3 7 10 0.02 0.00 4 7 10 0.57 0.00 5 7 10 -0.11 0.00 6 7 10 -0.18 0.00 7 7 10 0.23 0.00 8 7 10 0.15 0.00 9 7 10 -0.41 0.00 10 7 10 -0.40 0.00 11 7 10 0.70 0.00 12 7 10 0.67 0.00 13 7 10 -1.02 0.00 14 7 10 -0.77 0.00 15 7 10 1.19 0.00 16 7 10 0.70 0.00 17 7 10 -1.05 0.00 18 7 10 -0.58 0.00 19 7 10 0.66 0.00 20 7 10 0.46 0.00 21 7 10 -0.23 0.00 22 7 10 -0.36 0.00 23 7 10 -0.01 0.00 24 7 10 0.25 0.00 25 7 10 0.00 0.00 26 7 10 -0.14 0.00 0 8 10 0.38 0.00 1 8 10 -1.11 0.00 2 8 10 -0.30 0.00 3 8 10 0.79 0.00 4 8 10 0.08 0.00 5 8 10 -0.39 0.00 6 8 10 0.19 0.00 7 8 10 0.17 0.00 8 8 10 -0.45 0.00 9 8 10 -0.19 0.00 10 8 10 0.69 0.00 11 8 10 0.34 0.00 12 8 10 -0.86 0.00 13 8 10 -0.49 0.00 14 8 10 0.90 0.00 15 8 10 0.61 0.00 16 8 10 -0.73 0.00 17 8 10 -0.76 0.00 18 8 10 0.36 0.00 19 8 10 0.92 0.00 20 8 10 0.05 0.00 21 8 10 -0.99 0.00 22 8 10 -0.30 0.00 23 8 10 0.87 0.00 24 8 10 0.30 0.00 25 8 10 -0.59 0.00 26 8 10 -0.10 0.00 0 9 10 -0.74 0.00 1 9 10 -0.50 0.00 2 9 10 0.65 0.00 3 9 10 0.28 0.00 4 9 10 -0.44 0.00 5 9 10 0.09 0.00 6 9 10 0.23 0.00 7 9 10 -0.46 0.00 8 9 10 -0.06 0.00 9 9 10 0.71 0.00 10 9 10 -0.05 0.00 11 9 10 -0.77 0.00 12 9 10 0.08 0.00 13 9 10 0.64 0.00 14 9 10 0.05 0.00 15 9 10 -0.33 0.00 16 9 10 -0.41 0.00 17 9 10 -0.07 0.00 18 9 10 0.91 0.00 19 9 10 0.44 0.00 20 9 10 -1.31 0.00 21 9 10 -0.66 0.00 22 9 10 1.37 0.00 23 9 10 0.64 0.00 24 9 10 -1.06 0.00 25 9 10 -0.41 0.00 0 10 10 -0.36 0.00 1 10 10 0.18 0.00 2 10 10 0.24 0.00 3 10 10 -0.19 0.00 4 10 10 0.06 0.00 5 10 10 0.16 0.00 6 10 10 -0.44 0.00 7 10 10 0.00 0.00 8 10 10 0.73 0.00 9 10 10 -0.27 0.00 10 10 10 -0.77 0.00 11 10 10 0.55 0.00 12 10 10 0.52 0.00 13 10 10 -0.61 0.00 14 10 10 -0.07 0.00 15 10 10 0.28 0.00 16 10 10 -0.42 0.00 17 10 10 0.38 0.00 18 10 10 0.79 0.00 19 10 10 -1.08 0.00 20 10 10 -0.96 0.00 21 10 10 1.44 0.00 22 10 10 0.89 0.00 23 10 10 -1.30 0.00 24 10 10 -0.64 0.00 0 11 10 -0.21 0.00 1 11 10 -0.08 0.00 2 11 10 0.15 0.00 3 11 10 0.23 0.00 4 11 10 -0.03 0.00 5 11 10 -0.49 0.00 6 11 10 0.04 0.00 7 11 10 0.73 0.00 8 11 10 -0.29 0.00 9 11 10 -0.79 0.00 10 11 10 0.69 0.00 11 11 10 0.54 0.00 12 11 10 -0.95 0.00 13 11 10 -0.04 0.00 14 11 10 0.81 0.00 15 11 10 -0.53 0.00 16 11 10 -0.24 0.00 17 11 10 0.94 0.00 18 11 10 -0.51 0.00 19 11 10 -1.07 0.00 20 11 10 1.07 0.00 21 11 10 0.95 0.00 22 11 10 -1.16 0.00 23 11 10 -0.67 0.00 0 12 10 -0.47 0.00 1 12 10 0.18 0.00 2 12 10 0.49 0.00 3 12 10 -0.08 0.00 4 12 10 -0.58 0.00 5 12 10 0.03 0.00 6 12 10 0.70 0.00 7 12 10 -0.18 0.00 8 12 10 -0.77 0.00 9 12 10 0.52 0.00 10 12 10 0.62 0.00 11 12 10 -0.85 0.00 12 12 10 -0.20 0.00 13 12 10 0.89 0.00 14 12 10 -0.36 0.00 15 12 10 -0.55 0.00 16 12 10 0.80 0.00 17 12 10 -0.04 0.00 18 12 10 -0.96 0.00 19 12 10 0.56 0.00 20 12 10 0.83 0.00 21 12 10 -0.77 0.00 22 12 10 -0.55 0.00 0 13 10 -0.16 0.00 1 13 10 0.61 0.00 2 13 10 0.17 0.00 3 13 10 -0.59 0.00 4 13 10 -0.14 0.00 5 13 10 0.60 0.00 6 13 10 0.00 0.00 7 13 10 -0.64 0.00 8 13 10 0.27 0.00 9 13 10 0.61 0.00 10 13 10 -0.54 0.00 11 13 10 -0.38 0.00 12 13 10 0.62 0.00 13 13 10 -0.03 0.00 14 13 10 -0.45 0.00 15 13 10 0.44 0.00 16 13 10 0.11 0.00 17 13 10 -0.65 0.00 0 14 10 0.45 0.00 1 14 10 0.53 0.00 2 14 10 -0.42 0.00 3 14 10 -0.41 0.00 4 14 10 0.38 0.00 5 14 10 0.19 0.00 6 14 10 -0.40 0.00 7 14 10 0.08 0.00 8 14 10 0.45 0.00 9 14 10 -0.29 0.00 10 14 10 -0.43 0.00 11 14 10 0.34 0.00 12 14 10 0.24 0.00 13 14 10 -0.23 0.00 14 14 10 0.05 0.00 0 15 10 0.66 0.00 1 15 10 -0.15 0.00 2 15 10 -0.56 0.00 3 15 10 0.12 0.00 4 15 10 0.30 0.00 5 15 10 -0.12 0.00 6 15 10 -0.01 0.00 7 15 10 0.20 0.00 8 15 10 -0.19 0.00 1 1 11 0.04 0.00 2 1 11 0.02 0.00 3 1 11 -0.13 0.00 4 1 11 -0.04 0.00 5 1 11 0.19 0.00 6 1 11 0.03 0.00 7 1 11 -0.22 0.00 8 1 11 0.00 0.00 9 1 11 0.23 0.00 10 1 11 -0.04 0.00 11 1 11 -0.20 0.00 12 1 11 0.05 0.00 13 1 11 0.11 0.00 14 1 11 -0.01 0.00 15 1 11 0.02 0.00 16 1 11 -0.05 0.00 17 1 11 -0.15 0.00 18 1 11 0.09 0.00 19 1 11 0.22 0.00 20 1 11 -0.10 0.00 21 1 11 -0.18 0.00 22 1 11 0.09 0.00 23 1 11 0.06 0.00 24 1 11 -0.11 0.00 1 2 11 0.03 0.00 2 2 11 -0.20 0.00 3 2 11 -0.09 0.00 4 2 11 0.37 0.00 5 2 11 0.13 0.00 6 2 11 -0.48 0.00 7 2 11 -0.12 0.00 8 2 11 0.52 0.00 9 2 11 0.07 0.00 10 2 11 -0.47 0.00 11 2 11 -0.02 0.00 12 2 11 0.32 0.00 13 2 11 0.03 0.00 14 2 11 -0.06 0.00 15 2 11 -0.09 0.00 16 2 11 -0.24 0.00 17 2 11 0.16 0.00 18 2 11 0.44 0.00 19 2 11 -0.17 0.00 20 2 11 -0.46 0.00 21 2 11 0.14 0.00 22 2 11 0.29 0.00 23 2 11 -0.11 0.00 24 2 11 -0.04 0.00 25 2 11 0.13 0.00 1 3 11 -0.16 0.00 2 3 11 -0.10 0.00 3 3 11 0.46 0.00 4 3 11 0.21 0.00 5 3 11 -0.68 0.00 6 3 11 -0.30 0.00 7 3 11 0.78 0.00 8 3 11 0.31 0.00 9 3 11 -0.74 0.00 10 3 11 -0.26 0.00 11 3 11 0.53 0.00 12 3 11 0.20 0.00 13 3 11 -0.15 0.00 14 3 11 -0.19 0.00 15 3 11 -0.31 0.00 16 3 11 0.23 0.00 17 3 11 0.69 0.00 18 3 11 -0.24 0.00 19 3 11 -0.84 0.00 20 3 11 0.19 0.00 21 3 11 0.68 0.00 22 3 11 -0.10 0.00 23 3 11 -0.34 0.00 24 3 11 0.04 0.00 25 3 11 0.00 0.00 1 4 11 -0.07 0.00 2 4 11 0.37 0.00 3 4 11 0.23 0.00 4 4 11 -0.68 0.00 5 4 11 -0.40 0.00 6 4 11 0.86 0.00 7 4 11 0.52 0.00 8 4 11 -0.86 0.00 9 4 11 -0.53 0.00 10 4 11 0.63 0.00 11 4 11 0.44 0.00 12 4 11 -0.17 0.00 13 4 11 -0.35 0.00 14 4 11 -0.42 0.00 15 4 11 0.31 0.00 16 4 11 0.96 0.00 17 4 11 -0.30 0.00 18 4 11 -1.25 0.00 19 4 11 0.26 0.00 20 4 11 1.17 0.00 21 4 11 -0.15 0.00 22 4 11 -0.79 0.00 23 4 11 0.03 0.00 24 4 11 0.31 0.00 1 5 11 0.17 0.00 2 5 11 0.17 0.00 3 5 11 -0.47 0.00 4 5 11 -0.37 0.00 5 5 11 0.69 0.00 6 5 11 0.57 0.00 7 5 11 -0.74 0.00 8 5 11 -0.67 0.00 9 5 11 0.55 0.00 10 5 11 0.62 0.00 11 5 11 -0.10 0.00 12 5 11 -0.48 0.00 13 5 11 -0.54 0.00 14 5 11 0.35 0.00 15 5 11 1.17 0.00 16 5 11 -0.29 0.00 17 5 11 -1.58 0.00 18 5 11 0.28 0.00 19 5 11 1.61 0.00 20 5 11 -0.23 0.00 21 5 11 -1.25 0.00 22 5 11 0.14 0.00 1 6 11 0.08 0.00 2 6 11 -0.22 0.00 3 6 11 -0.26 0.00 4 6 11 0.41 0.00 5 6 11 0.45 0.00 6 6 11 -0.51 0.00 7 6 11 -0.60 0.00 8 6 11 0.41 0.00 9 6 11 0.62 0.00 10 6 11 -0.05 0.00 11 6 11 -0.51 0.00 12 6 11 -0.53 0.00 13 6 11 0.34 0.00 14 6 11 1.16 0.00 15 6 11 -0.22 0.00 16 6 11 -1.63 0.00 17 6 11 0.19 0.00 18 6 11 1.75 0.00 19 6 11 -0.21 0.00 20 6 11 -1.49 0.00 21 6 11 0.22 0.00 1 7 11 -0.06 0.00 2 7 11 -0.13 0.00 3 7 11 0.19 0.00 4 7 11 0.26 0.00 5 7 11 -0.30 0.00 6 7 11 -0.37 0.00 7 7 11 0.31 0.00 8 7 11 0.43 0.00 9 7 11 -0.12 0.00 10 7 11 -0.40 0.00 11 7 11 -0.28 0.00 12 7 11 0.29 0.00 13 7 11 0.80 0.00 14 7 11 -0.16 0.00 15 7 11 -1.24 0.00 16 7 11 0.08 0.00 17 7 11 1.43 0.00 18 7 11 -0.09 0.00 19 7 11 -1.31 0.00 20 7 11 0.15 0.00 1 8 11 -0.04 0.00 2 8 11 0.06 0.00 3 8 11 0.09 0.00 4 8 11 -0.16 0.00 5 8 11 -0.12 0.00 6 8 11 0.26 0.00 7 8 11 0.15 0.00 8 8 11 -0.27 0.00 9 8 11 -0.19 0.00 10 8 11 0.11 0.00 11 8 11 0.20 0.00 12 8 11 0.20 0.00 13 8 11 -0.16 0.00 14 8 11 -0.53 0.00 15 8 11 0.08 0.00 16 8 11 0.73 0.00 17 8 11 -0.01 0.00 18 8 11 -0.73 0.00 19 8 11 0.02 0.00 1 9 11 0.00 0.00 2 9 11 -0.01 0.00 3 9 11 -0.03 0.00 4 9 11 0.06 0.00 5 9 11 0.14 0.00 6 9 11 -0.10 0.00 7 9 11 -0.29 0.00 8 9 11 0.07 0.00 9 9 11 0.36 0.00 10 9 11 0.04 0.00 11 9 11 -0.30 0.00 12 9 11 -0.15 0.00 13 9 11 0.16 0.00 14 9 11 0.17 0.00 15 9 11 -0.02 0.00 16 9 11 -0.09 0.00 17 9 11 -0.04 0.00 18 9 11 -0.01 0.00 19 9 11 0.01 0.00 1 10 11 -0.03 0.00 2 10 11 0.08 0.00 3 10 11 0.11 0.00 4 10 11 -0.06 0.00 5 10 11 -0.22 0.00 6 10 11 -0.08 0.00 7 10 11 0.26 0.00 8 10 11 0.28 0.00 9 10 11 -0.16 0.00 10 10 11 -0.43 0.00 11 10 11 -0.05 0.00 12 10 11 0.48 0.00 14 10 11 -0.45 0.00 15 10 11 -0.23 0.00 16 10 11 0.40 0.00 17 10 11 0.10 0.00 1 11 11 0.10 0.00 2 11 11 0.06 0.00 3 11 11 -0.23 0.00 4 11 11 -0.17 0.00 5 11 11 0.21 0.00 6 11 11 0.28 0.00 7 11 11 -0.04 0.00 8 11 11 -0.28 0.00 0 0 12 0.13 0.00 1 0 12 0.31 0.00 2 0 12 -0.20 0.00 3 0 12 -0.18 0.00 4 0 12 0.36 0.00 5 0 12 0.04 0.00 6 0 12 -0.50 0.00 7 0 12 -0.05 0.00 8 0 12 0.52 0.00 9 0 12 0.33 0.00 10 0 12 -0.39 0.00 11 0 12 -0.87 0.00 12 0 12 0.20 0.00 13 0 12 1.46 0.00 14 0 12 -0.06 0.00 15 0 12 -1.79 0.00 16 0 12 0.02 0.00 17 0 12 1.69 0.00 0 1 12 0.30 0.00 1 1 12 -0.18 0.00 2 1 12 -0.23 0.00 3 1 12 0.25 0.00 4 1 12 0.08 0.00 5 1 12 -0.34 0.00 6 1 12 0.01 0.00 7 1 12 0.37 0.00 8 1 12 0.12 0.00 9 1 12 -0.30 0.00 10 1 12 -0.54 0.00 11 1 12 0.16 0.00 12 1 12 1.12 0.00 13 1 12 -0.03 0.00 14 1 12 -1.58 0.00 15 1 12 -0.01 0.00 16 1 12 1.68 0.00 17 1 12 -0.01 0.00 18 1 12 -1.35 0.00 0 2 12 -0.24 0.00 1 2 12 -0.18 0.00 2 2 12 0.21 0.00 3 2 12 0.09 0.00 4 2 12 -0.14 0.00 5 2 12 0.03 0.00 6 2 12 0.05 0.00 7 2 12 -0.04 0.00 8 2 12 0.03 0.00 9 2 12 -0.20 0.00 10 2 12 -0.10 0.00 11 2 12 0.66 0.00 12 2 12 0.14 0.00 13 2 12 -1.14 0.00 14 2 12 -0.12 0.00 15 2 12 1.37 0.00 16 2 12 0.07 0.00 0 3 12 -0.04 0.00 1 3 12 0.15 0.00 2 3 12 0.01 0.00 3 3 12 -0.01 0.00 4 3 12 0.06 0.00 5 3 12 -0.18 0.00 6 3 12 -0.12 0.00 7 3 12 0.33 0.00 8 3 12 0.07 0.00 9 3 12 -0.39 0.00 10 3 12 0.18 0.00 11 3 12 0.35 0.00 12 3 12 -0.56 0.00 13 3 12 -0.25 0.00 14 3 12 0.85 0.00 15 3 12 0.15 0.00 0 4 12 -0.08 0.00 1 4 12 -0.14 0.00 2 4 12 0.15 0.00 3 4 12 0.12 0.00 4 4 12 -0.28 0.00 5 4 12 -0.13 0.00 6 4 12 0.41 0.00 7 4 12 0.17 0.00 8 4 12 -0.44 0.00 9 4 12 -0.14 0.00 10 4 12 0.39 0.00 11 4 12 -0.02 0.00 12 4 12 -0.28 0.00 13 4 12 0.26 0.00 0 5 12 -0.29 0.00 1 5 12 0.43 0.00 2 5 12 0.22 0.00 3 5 12 -0.40 0.00 4 5 12 -0.10 0.00 5 5 12 0.33 0.00 6 5 12 0.08 0.00 7 5 12 -0.24 0.00 8 5 12 -0.17 0.00 9 5 12 0.14 0.00 10 5 12 0.24 0.00 11 5 12 -0.07 0.00 12 5 12 -0.19 0.00 13 5 12 0.04 0.00 0 6 12 0.68 0.00 1 6 12 0.27 0.00 2 6 12 -0.58 0.00 3 6 12 -0.08 0.00 4 6 12 0.30 0.00 5 6 12 -0.09 0.00 6 6 12 0.02 0.00 7 6 12 0.06 0.00 8 6 12 -0.25 0.00 9 6 12 0.14 0.00 10 6 12 0.33 0.00 11 6 12 -0.30 0.00 12 6 12 -0.25 0.00 6 7 12 0.29 0.00 7 7 12 -0.50 0.00 8 7 12 -0.15 0.00 9 7 12 0.65 0.00 10 7 12 -0.10 0.00 11 7 12 -0.56 0.00 2 0 0 -142.77 0.00 4 0 0 111.10 0.00 1 1 0 -137.18 0.00 3 1 0 116.24 0.00 0 2 0 -101.01 0.00 2 2 0 92.87 0.00 1 1 1 0.43 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 21116) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.250 0.250 -0.053 193 75 ' ' 2 0.750 0.750 -0.018 193 75 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 2 0 0 1.377 4 0 0 2.754 1 1 0 1.506 3 1 0 2.462 0 2 0 2.681 2 2 0 3.014 1 1 1 3.128 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL shelxt_a.res in Pccn CELL 29.5823 15.1971 7.4303 90.00 90.00 90.00 SPGR Pccn # Solvent Accessible Volume = 385 # Electrons Found in S.A.V. = 149 # Note: Atoms in Void as Cxxx and Qxxx all others C101 0.225 0.174 0.053 ! 5.20 eA-3 C102 0.207 0.206 0.156 ! 5.17 eA-3 C103 0.223 0.168 0.176 ! 4.27 eA-3 C104 0.781 0.688 0.070 ! 3.49 eA-3 C105 0.736 0.669 0.098 ! 3.08 eA-3 C106 0.294 0.198 0.052 ! 3.01 eA-3 C107 0.257 0.185 0.178 ! 2.77 eA-3 C108 0.750 0.745 0.187 ! 2.61 eA-3 C109 0.765 0.702 0.144 ! 2.50 eA-3 C110 0.277 0.170 0.058 ! 2.32 eA-3 C111 0.764 0.776 0.839 ! 1.33 eA-3 C112 0.261 0.213 0.041 ! 1.29 eA-3 Q113 0.049 0.625 0.627 ! 0.64 eA-3 Q114 0.521 0.637 0.025 ! 0.63 eA-3 Q115 0.045 0.020 0.440 ! 0.62 eA-3 Q116 0.387 0.511 0.524 ! 0.58 eA-3 Q117 0.338 0.951 0.222 ! 0.54 eA-3 Q118 0.306 0.953 0.352 ! 0.53 eA-3 Q119 0.959 0.327 0.256 ! 0.51 eA-3 ) ; _shelx_fab_checksum 53809 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y+1/2, z' '-x, y+1/2, -z+1/2' 'x+1/2, -y, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z' 'x, -y-1/2, z-1/2' '-x-1/2, y, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy S S1 0.35005(2) 0.45941(2) 0.30736(4) 0.02840(8) Uani d 1 O O1 0.51910(3) 0.44865(6) 0.30165(10) 0.02145(16) Uani d 1 N N1 0.44576(3) 0.42049(6) 0.25602(12) 0.01785(16) Uani d 1 H H1A 0.4245 0.3969 0.1885 0.021 Uiso calc 1 N N2 0.43510(3) 0.45797(6) 0.41971(12) 0.01968(17) Uani d 1 H H2A 0.4555 0.4622 0.5055 0.024 Uiso calc 1 N N3 0.38838(3) 0.54063(7) 0.58855(13) 0.02328(19) Uani d 1 H H3B 0.4134 0.5557 0.6450 0.028 Uiso calc 1 C C1 0.49867(3) 0.38567(6) 0.01910(13) 0.01554(16) Uani d 1 O O2 0.42318(3) 0.34449(6) -0.04284(11) 0.02289(16) Uani d 1 C C2 0.46703(4) 0.34759(7) -0.09866(13) 0.01771(18) Uani d 1 C C3 0.48083(4) 0.31472(7) -0.26464(15) 0.0219(2) Uani d 1 H H3A 0.4594 0.2887 -0.3435 0.026 Uiso calc 1 C C4 0.52583(4) 0.31993(7) -0.31475(14) 0.0236(2) Uani d 1 H H4A 0.5351 0.2970 -0.4278 0.028 Uiso calc 1 C C5 0.55740(4) 0.35814(7) -0.20190(14) 0.0213(2) Uani d 1 H H5A 0.5882 0.3618 -0.2369 0.026 Uiso calc 1 C C6 0.54345(4) 0.39094(7) -0.03713(13) 0.01772(18) Uani d 1 H H6A 0.5651 0.4178 0.0397 0.021 Uiso calc 1 C C7 0.39000(4) 0.30595(9) -0.15849(19) 0.0305(3) Uani d 1 H H7A 0.3601 0.3105 -0.1022 0.046 Uiso calc 1 H H7B 0.3974 0.2439 -0.1786 0.046 Uiso calc 1 H H7C 0.3898 0.3371 -0.2740 0.046 Uiso calc 1 C C8 0.48867(4) 0.42057(7) 0.20168(13) 0.01617(17) Uani d 1 C C9 0.39228(4) 0.48821(8) 0.44523(13) 0.01948(19) Uani d 1 C C10 0.34575(4) 0.57477(8) 0.65855(14) 0.0207(2) Uani d 1 H H10A 0.3240 0.5806 0.5562 0.025 Uiso calc 1 C C11 0.35395(4) 0.66559(8) 0.73803(16) 0.0227(2) Uani d 1 H H11A 0.3648 0.7058 0.6425 0.027 Uiso calc 1 H H11B 0.3777 0.6618 0.8316 0.027 Uiso calc 1 C C12 0.31070(4) 0.70242(8) 0.82077(15) 0.0240(2) Uani d 1 H H12A 0.3173 0.7597 0.8786 0.029 Uiso calc 1 H H12B 0.2881 0.7126 0.7246 0.029 Uiso calc 1 C C13 0.29112(5) 0.63975(9) 0.95964(16) 0.0288(3) Uani d 1 H H13A 0.3124 0.6341 1.0617 0.035 Uiso calc 1 H H13B 0.2624 0.6641 1.0065 0.035 Uiso calc 1 C C14 0.28248(5) 0.54955(9) 0.87859(18) 0.0294(3) Uani d 1 H H14A 0.2589 0.5542 0.7844 0.035 Uiso calc 1 H H14B 0.2712 0.5092 0.9732 0.035 Uiso calc 1 C C15 0.32559(4) 0.51217(8) 0.79683(16) 0.0256(2) Uani d 1 H H15A 0.3479 0.5014 0.8935 0.031 Uiso calc 1 H H15B 0.3188 0.4551 0.7385 0.031 Uiso calc 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 S1 0.01858(12) 0.04279(19) 0.02381(13) 0.00557(12) -0.00243(10) -0.01162(12) O1 0.0177(3) 0.0308(4) 0.0158(3) 0.0055(3) -0.0021(3) -0.0051(3) N1 0.0182(4) 0.0209(4) 0.0145(3) 0.0035(3) 0.0016(3) -0.0039(3) N2 0.0175(4) 0.0287(5) 0.0129(3) 0.0079(3) -0.0003(3) -0.0034(3) N3 0.0160(4) 0.0367(5) 0.0172(4) 0.0089(4) -0.0009(3) -0.0080(3) C1 0.0191(4) 0.0149(4) 0.0126(3) 0.0043(3) 0.0003(3) -0.0005(3) O2 0.0183(3) 0.0273(4) 0.0230(4) 0.0018(3) -0.0018(3) -0.0079(3) C2 0.0213(4) 0.0153(4) 0.0165(4) 0.0035(3) -0.0003(4) -0.0019(3) C3 0.0293(5) 0.0190(4) 0.0174(4) 0.0018(4) 0.0001(4) -0.0053(3) C4 0.0339(6) 0.0204(5) 0.0165(4) 0.0032(4) 0.0066(4) -0.0036(3) C5 0.0237(5) 0.0208(5) 0.0194(4) 0.0036(4) 0.0066(4) 0.0004(4) C6 0.0200(4) 0.0171(4) 0.0161(4) 0.0036(3) 0.0015(3) 0.0005(3) C7 0.0238(5) 0.0315(6) 0.0363(6) 0.0025(5) -0.0071(5) -0.0124(5) C8 0.0181(4) 0.0175(4) 0.0129(3) 0.0054(3) 0.0004(3) 0.0000(3) C9 0.0177(4) 0.0256(5) 0.0152(4) 0.0062(4) 0.0010(3) -0.0006(3) C10 0.0171(4) 0.0297(5) 0.0154(4) 0.0082(4) 0.0012(3) -0.0031(4) C11 0.0184(4) 0.0284(5) 0.0214(4) 0.0065(4) -0.0016(4) -0.0027(4) C12 0.0215(5) 0.0292(5) 0.0213(4) 0.0098(4) -0.0024(4) -0.0048(4) C13 0.0298(6) 0.0357(6) 0.0208(5) 0.0131(5) 0.0065(4) -0.0040(4) C14 0.0274(5) 0.0351(6) 0.0258(5) 0.0049(5) 0.0102(5) -0.0011(5) C15 0.0275(5) 0.0280(5) 0.0214(5) 0.0080(5) 0.0049(4) -0.0013(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C8 N1 N2 118.99(9) C8 N1 H1A 120.5 N2 N1 H1A 120.5 C9 N2 N1 118.36(9) C9 N2 H2A 120.8 N1 N2 H2A 120.8 C9 N3 C10 124.83(10) C9 N3 H3B 117.6 C10 N3 H3B 117.6 C6 C1 C2 118.08(9) C6 C1 C8 116.30(9) C2 C1 C8 125.62(9) C2 O2 C7 118.99(9) O2 C2 C3 122.44(10) O2 C2 C1 117.30(9) C3 C2 C1 120.26(10) C4 C3 C2 119.98(10) C4 C3 H3A 120.0 C2 C3 H3A 120.0 C5 C4 C3 120.68(10) C5 C4 H4A 119.7 C3 C4 H4A 119.7 C4 C5 C6 119.07(11) C4 C5 H5A 120.5 C6 C5 H5A 120.5 C5 C6 C1 121.91(10) C5 C6 H6A 119.0 C1 C6 H6A 119.0 O2 C7 H7A 109.5 O2 C7 H7B 109.5 H7A C7 H7B 109.5 O2 C7 H7C 109.5 H7A C7 H7C 109.5 H7B C7 H7C 109.5 O1 C8 N1 120.62(9) O1 C8 C1 121.60(9) N1 C8 C1 117.78(9) N3 C9 N2 113.15(9) N3 C9 S1 125.44(8) N2 C9 S1 121.41(8) N3 C10 C11 108.87(9) N3 C10 C15 110.91(9) C11 C10 C15 111.57(9) N3 C10 H10A 108.5 C11 C10 H10A 108.5 C15 C10 H10A 108.5 C10 C11 C12 110.84(10) C10 C11 H11A 109.5 C12 C11 H11A 109.5 C10 C11 H11B 109.5 C12 C11 H11B 109.5 H11A C11 H11B 108.1 C13 C12 C11 111.31(10) C13 C12 H12A 109.4 C11 C12 H12A 109.4 C13 C12 H12B 109.4 C11 C12 H12B 109.4 H12A C12 H12B 108.0 C14 C13 C12 111.14(10) C14 C13 H13A 109.4 C12 C13 H13A 109.4 C14 C13 H13B 109.4 C12 C13 H13B 109.4 H13A C13 H13B 108.0 C13 C14 C15 110.73(11) C13 C14 H14A 109.5 C15 C14 H14A 109.5 C13 C14 H14B 109.5 C15 C14 H14B 109.5 H14A C14 H14B 108.1 C10 C15 C14 111.37(10) C10 C15 H15A 109.4 C14 C15 H15A 109.4 C10 C15 H15B 109.4 C14 C15 H15B 109.4 H15A C15 H15B 108.0 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance S1 C9 1.6737(11) O1 C8 1.2426(13) N1 C8 1.3321(13) N1 N2 1.3795(12) N1 H1A 0.8800 N2 C9 1.3611(13) N2 H2A 0.8800 N3 C9 1.3349(14) N3 C10 1.4593(14) N3 H3B 0.8800 C1 C6 1.3912(15) C1 C2 1.4059(14) C1 C8 1.4864(13) O2 C2 1.3629(13) O2 C7 1.4299(14) C2 C3 1.3918(14) C3 C4 1.3845(17) C3 H3A 0.9500 C4 C5 1.3830(17) C4 H4A 0.9500 C5 C6 1.3848(14) C5 H5A 0.9500 C6 H6A 0.9500 C7 H7A 0.9800 C7 H7B 0.9800 C7 H7C 0.9800 C10 C11 1.5207(17) C10 C15 1.5221(17) C10 H10A 1.0000 C11 C12 1.5259(15) C11 H11A 0.9900 C11 H11B 0.9900 C12 C13 1.5190(18) C12 H12A 0.9900 C12 H12B 0.9900 C13 C14 1.5189(19) C13 H13A 0.9900 C13 H13B 0.9900 C14 C15 1.5225(17) C14 H14A 0.9900 C14 H14B 0.9900 C15 H15A 0.9900 C15 H15B 0.9900 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA N1 H1A O2 . 0.88 1.90 2.5907(12) 135 N2 H2A O1 5_666 0.88 2.11 2.8523(12) 142 N3 H3B O1 5_666 0.88 2.04 2.8607(12) 155 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C8 N1 N2 C9 155.21(10) C7 O2 C2 C3 0.13(16) C7 O2 C2 C1 -179.76(10) C6 C1 C2 O2 -178.77(9) C8 C1 C2 O2 1.90(15) C6 C1 C2 C3 1.33(15) C8 C1 C2 C3 -178.00(10) O2 C2 C3 C4 179.74(10) C1 C2 C3 C4 -0.37(16) C2 C3 C4 C5 -0.45(17) C3 C4 C5 C6 0.27(17) C4 C5 C6 C1 0.76(16) C2 C1 C6 C5 -1.54(15) C8 C1 C6 C5 177.85(9) N2 N1 C8 O1 4.70(15) N2 N1 C8 C1 -175.62(9) C6 C1 C8 O1 -3.58(14) C2 C1 C8 O1 175.77(10) C6 C1 C8 N1 176.75(9) C2 C1 C8 N1 -3.91(15) C10 N3 C9 N2 -173.24(11) C10 N3 C9 S1 6.15(17) N1 N2 C9 N3 -165.32(10) N1 N2 C9 S1 15.26(14) C9 N3 C10 C11 -147.21(11) C9 N3 C10 C15 89.66(13) N3 C10 C11 C12 -177.45(9) C15 C10 C11 C12 -54.71(12) C10 C11 C12 C13 55.32(13) C11 C12 C13 C14 -56.40(14) C12 C13 C14 C15 56.28(14) N3 C10 C15 C14 176.78(10) C11 C10 C15 C14 55.22(13) C13 C14 C15 C10 -55.65(14) _cod_database_fobs_code 1549066