#------------------------------------------------------------------------------ #$Date: 2019-06-26 10:49:47 +0300 (Wed, 26 Jun 2019) $ #$Revision: 216575 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/19/1551910.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1551910 loop_ _publ_author_name 'Lauren N. McHugh' 'Matthew J. McPherson' 'Laura J. McCormick' 'Samuel A. Morris' 'Paul S. Wheatley' 'Simon J. Teat' 'David McKay' 'Daniel M. Dawson' 'Charlotte E. F. Sansome' 'Sharon E. Ashbrook' 'Corinne A. Stone' 'Martin W. Smith' 'Russell E. Morris' _publ_section_title ; Hydrolytic stability in hemilabile metal-organic frameworks ; _journal_name_full 'Nature Chemistry' _journal_page_first 1096 _journal_page_last 1102 _journal_paper_doi 10.1038/s41557-018-0104-x _journal_volume 10 _journal_year 2018 _chemical_formula_sum 'C10 H8 Cu O5' _chemical_formula_weight 271.70 _space_group_crystal_system trigonal _space_group_IT_number 157 _space_group_name_Hall 'P 3 -2' _space_group_name_H-M_alt 'P 3 1 m' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary 'dual space' _atom_sites_solution_secondary difmap _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 18 _cell_length_a 33.028(3) _cell_length_b 33.028(3) _cell_length_c 5.2047(6) _cell_measurement_reflns_used 9920 _cell_measurement_temperature 300(2) _cell_measurement_theta_max 24.07 _cell_measurement_theta_min 2.80 _cell_volume 4916.9(8) _computing_cell_refinement 'SAINT V8.34A Bruker-AXS, Madison WI' _computing_data_collection 'Bruker APEX2 Bruker-AXS, Madison WI' _computing_data_reduction 'SAINT V8.34A Bruker-AXS, Madison WI' _computing_structure_refinement 'SHELXL-2016/4 (Sheldrick, 2016)' _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' _diffrn_ambient_temperature 300(2) _diffrn_detector_area_resol_mean 10.42 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker D8 with PHOTON 100 detector' _diffrn_measurement_method '\f and \w shutterless scans' _diffrn_radiation_type synchrotron _diffrn_radiation_wavelength 0.7749 _diffrn_reflns_av_R_equivalents 0.0955 _diffrn_reflns_av_unetI/netI 0.0637 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 34 _diffrn_reflns_limit_h_min -34 _diffrn_reflns_limit_k_max 34 _diffrn_reflns_limit_k_min -34 _diffrn_reflns_limit_l_max 5 _diffrn_reflns_limit_l_min -5 _diffrn_reflns_number 26548 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 24.079 _diffrn_reflns_theta_max 24.079 _diffrn_reflns_theta_min 2.329 _diffrn_source ; Advanced Light Source, station 11.3.1 ; _exptl_absorpt_coefficient_mu 2.529 _exptl_absorpt_correction_T_max 0.951 _exptl_absorpt_correction_T_min 0.579 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2014/5 - Bruker AXS, Madison WI' _exptl_crystal_colour blue _exptl_crystal_density_diffrn 1.652 _exptl_crystal_description plate _exptl_crystal_F_000 2466 _exptl_crystal_size_max 0.070 _exptl_crystal_size_mid 0.030 _exptl_crystal_size_min 0.020 _refine_diff_density_max 2.880 _refine_diff_density_min -4.101 _refine_diff_density_rms 0.322 _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack 0.55(12) _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.104 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 222 _refine_ls_number_reflns 4168 _refine_ls_number_restraints 76 _refine_ls_restrained_S_all 1.106 _refine_ls_R_factor_all 0.1685 _refine_ls_R_factor_gt 0.1515 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0001P)^2^+507.3451P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.3291 _refine_ls_wR_factor_ref 0.3410 _reflns_Friedel_coverage 0.987 _reflns_Friedel_fraction_full 0.999 _reflns_Friedel_fraction_max 0.999 _reflns_number_gt 3680 _reflns_number_total 4168 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file 41557_2018_104_MOESM3_ESM.cif _cod_data_source_block CuEtOipRTvac _cod_original_cell_volume 4917.0(10) _cod_database_code 1551910 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.843 _shelx_estimated_absorpt_t_max 0.951 _shelx_res_file ; TITL sad_a.res in P31m sad_a.res created by SHELXL-2016/4 at 17:56:52 on 01-Aug-2017 CELL 0.77490 33.0283 33.0283 5.2047 90.000 90.000 120.000 ZERR 18.00 0.0028 0.0028 0.0006 0.000 0.000 0.000 LATT -1 SYMM - Y, X - Y, Z SYMM - X + Y, - X, Z SYMM Y, X, Z SYMM X - Y, - Y, Z SYMM - X, - X + Y, Z SFAC C H O CU DISP H 0.00000 0.00000 0.67 DISP C 0.00399 0.00197 13.60 DISP O 0.01323 0.00737 40.17 DISP Cu 0.29127 1.48033 6565.59 UNIT 180 144 90 18 LIST 4 MERG 2 TWIN acta FLAT 0.05 c25 o12 o13 flat 0.05 o12 o13 c25 c31 FLAT 0.100 C15 C16 C17 c18 c19 c20 C21 FLAT 0.10 C27 C28 C29 c30 c31 c26 o16 c25 flat 0.1 c25 c31 o12 o13 SADI c25 o12 c25 o13 c32 o14 c32 o15 SIMU 0.02 0.04 c9 c10 c9 c8 c9 c11 sadi c23 c24 c13 c14 c6 c7 c33 c34 simu 0.02 0.04 o16 c33 c34 simu 0.02 0.04 c26 c31 c27 simu 0.005 0.01 c31 c25 o12 o13 Cu4 o9 o10 Cu3 c22 delu 0.005 0.01 c31 c25 o12 o13 Cu4 o9 o10 Cu3 c22 simu 0.01 0.02 c29 c30 c31 dfix 21.00 0.02 c25 c31 c27 c32 c8 c9 c15 c21 c1 c2 c22 c17_$5 dfix 31.00 0.02 c2 c3 c2 c4 c4 c5 c9 c10 c9 c11 c11 c12 dfix 31.00 0.02 c16 c17 c17 c18 c18 c19 c19 c20 c20 c21 c21 c16 dfix 31.00 0.02 c26 c27 c27 c28 c28 c29 c29 c30 c30 c31 c31 c26 FMAP 2 PLAN 20 size 0.07 0.03 0.02 ACTA BOND $H bind Cu1 o8_$1 eqiv $1 x, y, z-1 bind Cu2 o4_$2 eqiv $2 x, y, z+1 bind Cu3 O12_$2 bind Cu4 o10_$1 bind Cu2 o12_$3 eqiv $3 x-y+1, -y+2, z+1 bind Cu4 o10_$4 eqiv $4 x-y+1, -y+2, z-1 eqiv $5 -x+1, -x+y+1, z sadi o3 c6 o6 c13 o16 c33 o11 c23 L.S. 10 TEMP 27.00 WGHT 0.000100 507.345093 BASF 0.54851 FVAR 0.18294 1.51050 1.38506 C1 1 0.735199 0.822572 0.385216 11.00000 0.00164 C2 1 0.776665 0.817658 0.452022 11.00000 0.00219 C3 1 0.781389 0.781389 0.352841 10.50000 0.01480 AFIX 43 H3 2 0.761387 0.761388 0.227071 10.50000 -1.20000 AFIX 0 C4 1 0.804412 0.843791 0.659069 11.00000 0.01861 AFIX 43 H4 2 0.797703 0.865592 0.730387 11.00000 -1.20000 AFIX 0 C5 1 0.840538 0.840538 0.767729 10.50000 0.04540 PART -1 C6 1 0.873246 0.912374 0.962020 10.50000 0.02382 AFIX 23 H6A 2 0.873921 0.918856 1.144229 10.50000 -1.20000 H6B 2 0.846683 0.913166 0.888204 10.50000 -1.20000 AFIX 0 C7 1 0.918058 0.951095 0.838377 10.50000 0.14540 AFIX 33 H7A 2 0.920169 0.980798 0.867322 10.50000 -1.50000 H7B 2 0.944678 0.951223 0.913348 10.50000 -1.50000 H7C 2 0.917405 0.945525 0.656990 10.50000 -1.50000 AFIX 0 PART 0 C8 1 0.715455 0.913638 0.105190 11.00000 0.01777 C9 1 0.752219 0.959271 -0.007058 11.00000 0.00131 C10 1 0.758087 1.000000 0.095904 10.50000 0.00590 AFIX 43 H10 2 0.739327 1.000000 0.229154 10.50000 -1.20000 AFIX 0 C11 1 0.778570 0.959965 -0.214785 11.00000 0.01858 AFIX 43 H11 2 0.771067 0.931621 -0.291436 11.00000 -1.20000 AFIX 0 C12 1 0.815162 1.000000 -0.314710 10.50000 0.02692 PART -1 C13 1 0.840171 0.957261 -0.568755 10.50000 0.00717 AFIX 23 H13A 2 0.808658 0.934566 -0.621691 10.50000 -1.20000 H13B 2 0.848439 0.944539 -0.423054 10.50000 -1.20000 AFIX 0 C14 1 0.874379 0.966656 -0.791162 10.50000 0.13542 AFIX 33 H14A 2 0.873088 0.937990 -0.839683 10.50000 -1.50000 H14B 2 0.865871 0.978949 -0.935415 10.50000 -1.50000 H14C 2 0.905545 0.988896 -0.737310 10.50000 -1.50000 AFIX 0 PART 0 C15 1 0.617278 0.758036 0.577748 11.00000 0.00336 same 0.005 c16 > c21 same 0.005 c16 c21 < c20 C16 1 0.571073 0.674143 0.571616 11.00000 0.07224 AFIX 43 H16 2 0.588027 0.673260 0.431191 11.00000 -1.20000 AFIX 0 C17 1 0.534762 0.635141 0.689210 11.00000 0.06546 C18 1 0.509092 0.634802 0.899021 11.00000 0.06731 AFIX 43 H18 2 0.485861 0.606851 0.968889 11.00000 -1.20000 AFIX 0 C19 1 0.519029 0.677383 1.002088 11.00000 0.05547 C20 1 0.554446 0.718228 0.900895 11.00000 0.03576 AFIX 43 H20 2 0.561932 0.747150 0.969495 11.00000 -1.20000 AFIX 0 C21 1 0.578440 0.714631 0.693646 11.00000 0.04873 C22 1 0.472172 1.058541 0.678721 11.00000 0.06114 C23 1 0.495919 0.719974 1.291796 11.00000 0.05234 AFIX 23 H23A 2 0.490685 0.736851 1.155402 11.00000 -1.20000 H23B 2 0.526742 0.740153 1.363383 11.00000 -1.20000 AFIX 0 C24 1 0.458647 0.706512 1.501704 11.00000 0.07170 AFIX 33 H24A 2 0.460269 0.734281 1.570084 11.00000 -1.50000 H24B 2 0.428214 0.686774 1.429422 11.00000 -1.50000 H24C 2 0.464165 0.690066 1.636797 11.00000 -1.50000 AFIX 0 C25 1 0.518371 0.946132 0.382139 11.00000 0.04980 same 0.005 c26 > c31 same 0.005 c26 c31 < c30 C26 1 0.551637 0.893238 0.312035 11.00000 0.07617 AFIX 43 H26 2 0.565858 0.906344 0.468151 11.00000 -1.20000 AFIX 0 C27 1 0.560748 0.858584 0.220547 11.00000 0.05806 C28 1 0.532041 0.836739 0.009198 11.00000 0.08381 AFIX 43 H28 2 0.534990 0.812704 -0.064703 11.00000 -1.20000 AFIX 0 C29 1 0.499784 0.846064 -0.105051 11.00000 0.07206 C30 1 0.499868 0.884777 -0.001898 11.00000 0.07196 AFIX 43 H30 2 0.480838 0.894062 -0.084106 11.00000 -1.20000 AFIX 0 C31 1 0.524855 0.911606 0.209533 11.00000 0.05820 C32 1 0.600726 0.851169 0.296905 11.00000 0.04945 C33 1 0.432315 0.820064 -0.358127 11.00000 0.10046 AFIX 23 H33A 2 0.439659 0.852214 -0.379243 11.00000 -1.20000 H33B 2 0.410086 0.805890 -0.218726 11.00000 -1.20000 AFIX 0 C34 1 0.413229 0.792172 -0.609498 11.00000 0.08921 AFIX 33 H34A 2 0.384999 0.791822 -0.657673 11.00000 -1.50000 H34B 2 0.436067 0.806635 -0.743271 11.00000 -1.50000 H34C 2 0.406737 0.760692 -0.584071 11.00000 -1.50000 AFIX 0 O1 3 0.714576 0.806995 0.155345 11.00000 0.03020 O2 3 0.727601 0.849289 0.506955 11.00000 0.01484 O3 3 0.866504 0.866504 0.930680 10.50000 0.03413 O4 3 0.697405 0.877433 -0.036286 11.00000 0.00395 O5 3 0.707238 0.914585 0.335168 11.00000 0.02031 O6 3 0.842117 1.000000 -0.496559 10.50000 0.02285 O7 3 0.623200 0.759098 0.350516 11.00000 0.01952 O8 3 0.636097 0.796462 0.724695 11.00000 0.02232 O9 3 0.464506 1.049408 0.434235 11.00000 0.05666 O10 3 0.496600 1.050517 0.777525 11.00000 0.06680 O11 3 0.493285 0.678377 1.190732 11.00000 0.06734 O12 3 0.501706 0.959075 0.205491 11.00000 0.04901 O13 3 0.527835 0.954203 0.612458 11.00000 0.03517 O14 3 0.607883 0.826264 0.146515 11.00000 0.02188 O15 3 0.619621 0.866797 0.508506 11.00000 0.02033 O16 3 0.473760 0.817411 -0.312453 11.00000 0.09600 CU1 4 0.658136 0.812824 0.126172 11.00000 0.01700 0.01601 = 0.08384 -0.01676 -0.00220 0.00839 CU2 4 0.675471 0.859353 0.553747 11.00000 0.02155 0.01584 = 0.04044 -0.01090 -0.00279 0.00964 CU3 4 0.513280 1.000000 0.705924 10.50000 0.01333 CU4 4 0.474974 1.000000 0.276968 10.50000 0.01824 HKLF 4 REM sad_a.res in P31m REM R1 = 0.1515 for 3680 Fo > 4sig(Fo) and 0.1685 for all 4168 data REM 222 parameters refined using 76 restraints END WGHT 0.0001 507.2336 REM Highest difference peak 2.880, deepest hole -4.101, 1-sigma level 0.322 Q1 1 0.4813 1.0209 0.2658 11.00000 0.05 2.88 Q2 1 0.5228 1.0209 0.6884 11.00000 0.05 2.56 Q3 1 0.4828 1.0000 0.4592 10.50000 0.05 2.00 Q4 1 0.4770 1.0275 0.8713 11.00000 0.05 1.94 Q5 1 0.4856 1.0712 0.4985 11.00000 0.05 1.68 Q6 1 0.4814 0.8637 0.1738 11.00000 0.05 1.61 Q7 1 0.4745 1.0568 0.2568 11.00000 0.05 1.58 Q8 1 0.4913 1.0265 1.0242 11.00000 0.05 1.55 Q9 1 0.9211 1.0000 1.0553 10.50000 0.05 1.48 Q10 1 0.5033 0.9706 0.0658 11.00000 0.05 1.46 Q11 1 0.5254 1.0000 0.2558 10.50000 0.05 1.46 Q12 1 0.3333 0.6667 -0.8870 10.33333 0.05 1.43 Q13 1 0.9487 0.9487 0.4327 10.50000 0.05 1.36 Q14 1 0.3569 0.6921 -0.1525 11.00000 0.05 1.32 Q15 1 0.8849 0.8849 0.7999 10.50000 0.05 1.27 Q16 1 0.6695 0.8302 0.4016 11.00000 0.05 1.27 Q17 1 0.3333 0.6667 -0.3821 10.33333 0.05 1.26 Q18 1 0.6690 0.7969 0.5837 11.00000 0.05 1.26 Q19 1 0.6550 0.8522 0.5892 11.00000 0.05 1.25 Q20 1 0.6688 0.8463 -0.0009 11.00000 0.05 1.25 ; _shelx_res_checksum 49883 _shelx_hkl_file ; 3 -3 0 7407.76 357.06 -3 0 0 7604.64 357.76 2 -4 0 9726.63 458.95 -2 -2 0 9473.65 458.75 4 -2 0 9999.00 461.35 -4 2 0 9477.75 460.75 4 -1 0 26.90 3.70 3 1 0 27.20 4.50 1 -4 0 26.60 4.50 -4 3 0 21.00 4.40 4 -1 0 28.00 4.10 -3 4 0 19.60 3.20 -3 4 0 23.70 3.90 -1 4 0 22.10 4.20 -4 1 0 27.40 3.80 4 -3 0 21.60 2.90 1 3 0 24.20 4.00 4 -3 0 29.10 4.40 1 3 0 31.50 4.70 -1 4 0 31.80 5.50 -3 -1 0 19.30 3.40 3 -4 0 23.90 4.60 4 0 0 3.90 4.10 -4 4 0 1.40 2.80 4 0 0 1.10 3.90 4 -4 0 0.90 4.50 -4 0 0 3.40 2.40 0 4 0 2.60 4.30 0 4 0 1.10 2.70 -5 3 0 140.69 8.80 5 -2 0 124.29 9.70 -3 5 0 131.29 8.30 2 -5 0 124.99 9.20 -3 5 0 126.99 9.30 5 -2 0 129.69 8.30 3 2 0 132.29 10.10 3 -5 0 118.99 9.80 2 3 0 131.99 8.30 5 -3 0 116.39 9.60 2 3 0 135.79 10.10 -5 2 0 151.28 8.40 5 -3 0 123.39 7.70 -2 5 0 131.79 9.50 -2 5 0 138.59 8.60 2 3 0 132.59 6.60 4 1 0 64.99 5.40 5 -1 0 61.49 8.20 5 -1 0 70.99 7.50 -4 5 0 72.79 6.70 4 1 0 66.39 8.80 -4 5 0 56.79 6.10 -5 4 0 65.29 6.90 1 -5 0 71.59 6.80 -4 -1 0 66.19 6.00 1 4 0 72.89 6.30 5 -4 0 68.49 4.90 -1 5 0 67.69 6.40 5 -4 0 58.59 8.30 1 4 0 69.69 8.70 -1 5 0 68.49 8.30 -5 1 0 79.59 5.90 4 -5 0 62.69 9.10 5 0 0 -1.20 5.50 -5 5 0 -5.20 4.00 5 0 0 8.70 5.40 5 -5 0 -0.20 6.60 0 5 0 -1.50 3.60 -5 0 0 5.20 3.50 0 5 0 -5.40 5.90 6 -3 0 6326.47 308.77 3 3 0 6156.68 304.87 3 -6 0 6408.56 304.97 -6 3 0 6584.04 309.27 -3 -3 0 6319.57 304.87 -6 4 0 61.69 7.70 -4 6 0 66.89 9.60 4 2 0 60.29 10.80 4 2 0 69.59 4.50 6 -2 0 83.89 9.90 -4 6 0 64.49 7.90 6 -2 0 59.89 7.90 2 -6 0 55.69 9.10 -2 6 0 60.59 7.50 2 4 0 77.99 7.50 2 4 0 87.69 9.10 -4 -2 0 66.29 7.40 6 -4 0 70.09 6.00 -2 6 0 79.19 7.90 6 -4 0 66.29 9.80 4 -6 0 80.29 8.80 -5 6 0 188.58 11.60 -1 -5 0 214.88 12.10 6 -1 0 199.58 13.60 -6 5 0 188.88 12.80 5 1 0 194.58 14.30 -5 6 0 197.38 12.70 5 1 0 215.18 11.50 6 -1 0 211.68 13.60 1 -6 0 179.68 12.80 6 -5 0 166.98 15.10 -1 6 0 193.38 12.20 1 5 0 208.18 12.10 5 -6 0 168.28 14.90 6 -5 0 195.38 10.40 -5 -1 0 200.98 11.90 -1 6 0 154.48 14.40 1 5 0 170.88 14.80 -6 1 0 201.88 11.70 -6 6 0 7242.58 356.26 0 -6 0 7385.06 353.46 6 -6 0 7697.13 357.36 0 6 0 7089.59 353.56 -6 0 0 7632.44 358.76 3 -7 0 6.60 8.90 -4 7 0 3.80 8.80 7 -3 0 21.70 9.20 4 3 0 -6.20 9.20 7 -3 0 9.50 5.50 -4 7 0 2.90 5.80 -7 4 0 7.70 6.20 7 -4 0 14.30 8.90 3 4 0 22.90 5.80 4 -7 0 0.70 9.20 7 -4 0 10.30 5.00 3 4 0 -3.60 9.10 -3 7 0 3.10 5.80 2 -7 0 730.63 40.30 7 -2 0 805.92 41.10 -5 7 0 865.51 39.80 7 -2 0 776.22 40.00 -5 7 0 837.72 39.80 5 2 0 840.22 41.40 5 2 0 726.43 38.10 -7 5 0 850.01 39.80 -5 -2 0 817.22 39.40 2 5 0 823.82 39.60 5 -7 0 741.83 41.60 7 -5 0 791.72 38.60 -2 7 0 795.72 39.60 2 5 0 772.02 41.70 -7 2 0 841.52 39.50 -2 7 0 741.93 40.70 1 -7 0 142.09 14.30 -6 7 0 198.58 12.20 7 -1 0 133.69 14.60 6 1 0 143.49 17.10 -6 7 0 142.49 13.20 -1 -6 0 148.49 12.70 -1 7 0 166.08 12.80 7 -6 0 186.38 9.80 1 6 0 181.58 12.90 -6 -1 0 178.08 12.60 7 -6 0 128.49 17.10 6 -7 0 133.19 17.80 0 7 0 1.70 6.60 -7 0 0 14.00 6.30 7 -7 0 -18.80 12.10 4 4 0 1372.66 64.69 4 4 0 1371.66 66.19 8 -4 0 1196.08 67.49 4 -8 0 1284.17 67.79 -4 8 0 1395.66 67.19 8 -4 0 1322.77 65.89 -8 4 0 1489.65 66.69 4 4 0 1423.96 68.39 -4 8 0 1449.65 66.59 -5 8 0 14.80 7.30 3 -8 0 10.30 11.20 5 3 0 1.40 11.80 5 3 0 27.20 4.10 8 -3 0 46.70 11.90 8 -3 0 25.10 7.50 -5 8 0 28.70 10.40 -8 5 0 30.60 8.10 5 -8 0 17.90 12.10 -3 8 0 2.80 10.50 8 -5 0 36.30 6.10 3 5 0 36.00 7.40 8 -5 0 29.70 11.90 -3 8 0 27.50 7.60 3 5 0 6.90 11.70 -5 -3 0 16.50 7.60 -6 8 0 74.79 8.80 8 -2 0 68.19 10.10 6 2 0 75.19 12.60 -8 6 0 82.29 9.60 2 -8 0 55.99 11.20 2 6 0 55.59 13.20 -2 8 0 59.69 12.40 8 -6 0 79.69 7.90 8 -6 0 88.79 12.90 6 -8 0 79.19 13.90 -6 -2 0 66.99 10.30 -2 8 0 54.19 11.90 2 6 0 83.39 12.30 1 -8 0 398.76 24.60 -7 8 0 435.36 24.50 -7 8 0 463.15 23.00 7 1 0 411.46 27.10 7 1 0 483.65 23.10 -1 -7 0 405.56 23.60 8 -1 0 431.96 25.90 -8 7 0 424.06 24.30 1 7 0 373.46 27.30 1 7 0 442.46 23.90 -8 1 0 460.65 23.30 8 -7 0 453.85 21.40 8 -7 0 371.06 28.00 -1 8 0 433.06 23.90 -1 8 0 343.67 27.30 -7 -1 0 455.95 23.70 8 0 0 5.90 10.50 8 -8 0 11.40 12.30 0 8 0 25.80 7.30 9 -4 0 436.86 27.90 4 -9 0 405.16 28.00 -9 5 0 495.25 25.60 -5 9 0 443.76 27.10 9 -4 0 439.96 24.50 -5 9 0 495.45 25.90 5 4 0 443.46 29.20 5 4 0 431.06 21.90 9 -5 0 398.36 27.30 4 5 0 496.55 22.10 -4 9 0 410.76 27.90 -9 4 0 511.45 25.40 5 -9 0 425.16 28.50 4 5 0 448.56 28.30 -4 9 0 477.25 25.70 9 -5 0 450.85 24.10 4 5 0 500.15 25.00 -6 9 0 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468.95 28.60 -8 10 0 546.95 27.60 -10 8 0 546.65 27.90 8 2 0 499.75 29.60 2 8 0 513.35 27.30 10 -8 0 538.45 25.20 -10 2 0 486.65 26.20 10 -8 0 416.16 29.50 -2 10 0 456.15 29.10 8 -10 0 447.66 30.20 2 8 0 486.15 29.90 -8 -2 0 508.55 26.90 -2 10 0 510.35 27.20 1 -10 0 -12.20 8.60 10 -1 0 -2.40 9.00 -9 10 0 10.30 6.60 -10 9 0 -7.10 6.90 -9 10 0 -11.50 6.70 10 -1 0 13.00 10.30 9 1 0 12.10 7.20 9 1 0 -2.50 10.00 10 -9 0 4.70 3.60 -9 -1 0 4.30 6.00 -10 1 0 12.80 6.00 1 9 0 -7.20 10.10 9 -10 0 3.80 11.50 -1 10 0 5.10 6.70 -1 10 0 -11.30 10.40 1 9 0 2.40 6.60 10 -9 0 -3.40 11.70 10 0 0 8.50 8.80 -10 10 0 4.80 6.00 10 0 0 -0.20 9.60 -10 10 0 -5.40 6.90 0 10 0 -7.60 10.50 -10 0 0 7.50 5.90 0 10 0 6.70 6.80 10 -10 0 9.30 12.10 11 -5 0 247.98 15.70 11 -5 0 244.98 20.40 6 5 0 230.78 21.60 5 -11 0 228.78 20.30 -6 11 0 243.98 18.60 -6 11 0 248.68 17.30 -11 6 0 259.77 17.10 -5 11 0 231.88 19.30 -11 5 0 263.57 17.50 5 6 0 267.47 16.00 5 6 0 231.28 21.40 6 -11 0 219.58 21.10 5 6 0 251.07 12.50 11 -6 0 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194.98 14.70 2 9 0 171.28 19.40 11 -1 0 7.30 10.20 -10 11 0 12.40 7.00 10 1 0 3.60 10.30 1 -11 0 -6.70 8.70 11 -1 0 7.40 9.00 -10 11 0 -3.30 6.80 10 1 0 13.10 7.20 1 10 0 9.00 6.70 -11 1 0 14.90 6.20 -1 11 0 6.00 6.80 11 -10 0 9.90 11.80 1 10 0 -3.90 10.70 -10 -1 0 8.90 6.10 -1 11 0 -0.50 10.40 10 -11 0 1.40 11.60 0 -11 0 -8.70 8.10 11 0 0 1.80 9.50 -11 11 0 3.60 5.90 -11 11 0 -6.60 7.20 11 0 0 4.70 8.80 0 11 0 -0.80 7.20 11 -11 0 6.10 11.60 -11 0 0 13.20 6.30 0 11 0 -12.30 10.30 12 -6 0 922.71 50.19 12 -6 0 990.10 47.60 6 6 0 947.81 50.39 -12 6 0 1003.60 48.40 6 6 0 991.50 45.80 6 -12 0 920.91 50.19 -6 12 0 984.40 48.30 6 6 0 911.21 47.80 -6 12 0 987.10 49.10 5 -12 0 -1.70 11.10 -12 7 0 5.30 7.60 7 5 0 7.00 11.20 12 -5 0 27.70 12.10 12 -5 0 8.10 7.00 -7 12 0 17.40 9.40 -7 12 0 10.80 7.40 -7 -5 0 10.50 7.30 -5 12 0 7.80 7.00 12 -7 0 17.20 11.60 12 -7 0 10.60 5.70 5 7 0 18.50 6.90 5 7 0 10.20 10.90 -12 5 0 24.50 7.80 -5 12 0 13.10 10.10 7 -12 0 13.60 12.20 12 -4 0 40.20 11.90 12 -4 0 31.80 7.70 -8 12 0 29.70 7.50 -12 8 0 25.70 8.00 8 4 0 27.20 4.00 8 4 0 18.60 10.90 4 -12 0 24.70 11.10 -8 12 0 21.00 9.70 12 -8 0 34.40 5.60 4 8 0 34.00 7.50 -4 12 0 27.40 7.50 12 -8 0 32.80 11.80 4 8 0 15.50 11.50 -4 12 0 22.90 10.30 8 -12 0 29.30 12.60 -8 -4 0 23.90 6.80 3 -12 0 1051.49 54.69 -9 12 0 1093.59 54.09 12 -3 0 1086.29 53.99 -3 -9 0 1174.18 53.09 9 3 0 1033.40 51.79 -9 12 0 1167.68 54.09 12 -3 0 1068.09 54.89 9 3 0 1128.29 55.59 -12 9 0 1171.88 54.09 -9 -3 0 1106.89 53.49 9 -12 0 1048.30 56.19 3 9 0 1062.19 53.69 -3 12 0 1093.79 55.29 -12 3 0 1012.60 53.19 3 9 0 1092.19 55.89 -3 12 0 1092.39 53.99 12 -9 0 1101.79 52.29 12 -9 0 915.31 55.19 2 -12 0 -9.60 9.70 10 2 0 3.60 10.70 -12 10 0 -10.00 7.00 10 2 0 8.50 5.50 -10 12 0 -10.10 8.40 12 -2 0 14.20 10.80 -10 12 0 -0.10 6.90 -2 -10 0 -6.70 6.90 12 -2 0 -5.40 8.60 -2 12 0 7.10 7.30 12 -10 0 5.80 4.10 -10 -2 0 10.20 6.60 -2 12 0 3.10 10.60 2 10 0 -0.90 10.80 2 10 0 2.40 7.20 12 -10 0 9.40 11.70 10 -12 0 3.20 12.60 12 -1 0 76.39 11.40 11 1 0 63.49 10.60 -12 11 0 68.29 9.50 -11 12 0 80.09 8.80 12 -1 0 87.49 11.70 -11 12 0 58.79 12.20 11 1 0 71.39 12.10 1 -12 0 64.39 11.10 12 -11 0 76.89 14.00 1 11 0 76.49 13.10 -11 -1 0 81.99 10.70 -12 1 0 76.49 10.30 -1 12 0 81.89 12.90 -12 12 0 295.87 19.00 -12 12 0 308.87 16.70 0 -12 0 252.57 19.10 12 0 0 271.27 23.50 12 0 0 286.87 18.50 12 -12 0 244.38 22.70 0 12 0 268.17 22.00 -12 0 0 288.97 17.50 0 12 0 278.67 18.50 13 -6 0 426.96 24.40 -7 13 0 446.96 26.30 13 -6 0 406.66 27.80 -13 7 0 458.95 25.20 -7 13 0 462.45 25.40 6 -13 0 429.66 27.50 7 6 0 460.85 28.40 7 -13 0 420.16 28.00 6 7 0 438.16 28.30 13 -7 0 401.86 28.10 6 7 0 449.16 24.40 -13 6 0 449.66 25.50 -6 13 0 470.15 25.30 13 -7 0 424.96 23.60 -6 13 0 452.15 26.80 -8 13 0 418.66 23.50 13 -5 0 357.76 26.60 8 5 0 409.56 26.50 -13 8 0 401.96 23.40 13 -5 0 381.06 22.60 -8 13 0 421.16 24.00 5 -13 0 360.66 25.60 13 -8 0 381.66 20.80 5 8 0 340.37 25.80 13 -8 0 373.66 26.50 5 8 0 395.36 23.00 -5 13 0 394.46 23.00 -5 13 0 398.26 24.80 -8 -5 0 397.16 22.40 8 -13 0 360.26 26.20 -13 5 0 392.36 23.30 -13 9 0 61.39 13.20 13 -4 0 91.99 15.90 4 -13 0 98.79 13.00 -9 13 0 84.09 11.90 -9 13 0 83.09 14.10 9 4 0 70.49 5.80 13 -4 0 75.39 12.20 9 -13 0 80.29 14.50 13 -9 0 86.99 8.70 -13 4 0 102.69 11.80 13 -9 0 94.29 13.70 -4 13 0 101.79 15.90 -9 -4 0 87.19 11.00 -4 13 0 78.59 13.60 4 9 0 74.69 15.40 4 9 0 88.09 13.70 -10 13 0 112.59 12.30 10 3 0 98.09 7.80 -3 -10 0 119.49 11.10 13 -3 0 117.59 16.80 -10 13 0 103.59 13.10 10 3 0 109.49 20.40 3 -13 0 95.69 16.10 13 -3 0 104.79 13.60 -13 10 0 93.79 13.80 3 10 0 110.39 14.00 -3 13 0 97.59 16.80 -3 13 0 94.79 16.00 13 -10 0 106.09 14.70 -13 3 0 137.09 12.10 3 10 0 112.89 14.30 13 -10 0 104.59 8.40 -10 -3 0 108.59 12.10 2 -13 0 27.60 10.60 11 2 0 32.70 6.30 -13 11 0 25.10 8.30 11 2 0 34.10 11.80 -11 13 0 28.30 7.90 -2 -11 0 17.50 8.00 13 -2 0 31.70 17.90 13 -2 0 33.00 10.60 -11 13 0 30.70 9.20 -2 13 0 30.60 7.80 13 -11 0 34.40 4.70 -13 2 0 51.59 9.30 13 -11 0 24.00 13.60 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38.90 12.40 -14 9 0 28.10 9.60 14 -5 0 23.20 7.90 -9 14 0 23.20 8.70 9 5 0 32.60 11.80 14 -9 0 32.40 5.90 -5 14 0 27.00 7.80 5 9 0 26.60 7.50 -9 -5 0 17.20 6.90 14 -9 0 36.30 12.80 -5 14 0 37.80 11.30 -14 5 0 47.00 9.00 9 -14 0 30.90 13.20 14 -4 0 267.67 21.00 -14 10 0 258.47 18.60 14 -4 0 260.97 18.00 10 4 0 250.37 21.10 -4 -10 0 286.17 15.90 -10 14 0 239.58 18.70 -10 14 0 268.37 18.10 4 -14 0 232.28 20.50 10 4 0 234.88 13.10 -4 14 0 266.87 20.70 -4 14 0 261.37 18.40 14 -10 0 259.57 14.80 4 10 0 242.68 17.20 -10 -4 0 248.88 17.00 10 -14 0 240.78 23.70 -14 4 0 245.58 18.90 14 -3 0 7.60 8.50 -11 14 0 -1.70 7.00 14 -3 0 7.00 11.40 11 3 0 7.30 11.20 -11 14 0 -11.80 9.80 -3 -11 0 11.50 7.30 3 -14 0 2.80 10.60 11 3 0 7.60 4.30 -11 -3 0 5.90 6.70 11 -14 0 10.20 12.90 14 -11 0 14.20 12.50 -14 3 0 15.00 7.50 3 11 0 8.30 7.30 -3 14 0 1.20 7.10 -3 14 0 4.20 11.00 3 11 0 -2.00 13.60 14 -11 0 2.20 4.20 2 -14 0 13.10 10.60 12 2 0 23.10 11.50 -2 -12 0 7.50 8.20 -14 12 0 9.60 8.40 -12 14 0 18.50 7.90 14 -2 0 28.50 12.20 14 -2 0 30.60 9.90 12 2 0 22.00 6.40 -12 14 0 17.00 9.40 2 12 0 18.60 7.90 14 -12 0 19.50 4.40 2 12 0 20.60 12.40 -2 14 0 25.90 12.30 12 -14 0 35.10 14.30 14 -12 0 26.30 13.50 -12 -2 0 29.90 7.50 -2 14 0 32.10 8.00 14 -1 0 92.39 15.00 13 1 0 108.09 13.90 1 -14 0 90.79 15.00 -13 14 0 87.19 12.80 -14 13 0 76.59 13.60 14 -1 0 98.59 15.50 -1 -13 0 108.99 12.00 13 1 0 83.59 11.80 -13 14 0 84.59 13.90 1 13 0 95.79 12.80 1 13 0 122.49 15.30 -14 1 0 125.29 11.90 13 -14 0 86.99 16.00 -1 14 0 138.29 15.40 -13 -1 0 100.39 12.40 14 -13 0 115.19 15.90 -1 14 0 105.39 13.10 -14 14 0 4.40 7.60 14 0 0 -2.30 9.20 14 0 0 4.80 10.90 0 -14 0 -5.30 9.60 -14 14 0 -10.20 8.00 0 14 0 -5.70 12.30 -14 0 0 9.50 7.20 0 14 0 0.00 7.80 14 -14 0 7.90 13.80 -8 15 0 1076.09 52.79 -15 8 0 987.30 53.49 15 -7 0 1042.90 51.99 15 -7 0 943.51 54.39 7 -15 0 1024.00 57.29 8 7 0 1098.39 54.89 -8 15 0 1086.69 53.29 -7 15 0 1119.09 52.99 15 -8 0 1014.60 51.59 -15 7 0 1067.49 53.09 -7 15 0 1094.59 53.29 7 8 0 1026.70 52.19 7 8 0 1107.99 55.49 15 -8 0 998.50 54.59 8 -15 0 1008.60 55.09 15 -6 0 73.39 11.80 9 6 0 73.49 13.30 -15 9 0 75.19 10.70 -9 15 0 115.59 14.90 6 -15 0 69.89 15.80 15 -6 0 76.49 13.90 -9 15 0 76.19 12.70 6 9 0 91.39 14.40 6 9 0 92.79 11.90 -6 15 0 89.89 12.50 -6 15 0 64.99 13.60 9 -15 0 85.09 15.20 -9 -6 0 66.09 12.00 15 -9 0 75.69 9.60 -15 6 0 79.49 13.60 5 -15 0 653.13 38.20 -10 15 0 719.43 36.30 -15 10 0 696.63 36.40 15 -5 0 605.94 37.70 15 -5 0 666.53 36.00 10 5 0 729.63 38.80 -10 15 0 688.23 36.40 -5 -10 0 765.22 34.50 5 10 0 671.53 35.90 5 10 0 693.53 39.50 15 -10 0 678.13 34.20 -5 15 0 708.23 36.70 -15 5 0 677.53 36.10 -5 15 0 683.13 38.00 10 -15 0 668.73 39.90 -10 -5 0 693.83 35.80 15 -10 0 584.24 38.40 -15 11 0 620.14 33.40 -11 15 0 636.64 33.00 4 -15 0 598.34 34.70 11 4 0 588.84 29.50 15 -4 0 602.44 35.20 -4 -11 0 656.53 31.70 11 4 0 627.34 35.70 -11 15 0 582.74 33.30 15 -11 0 547.65 36.40 4 11 0 603.74 32.70 11 -15 0 564.14 37.30 -4 15 0 619.64 35.00 4 11 0 634.14 36.40 15 -11 0 592.84 30.50 -15 4 0 594.24 32.30 -11 -4 0 615.04 32.30 -4 15 0 648.74 33.50 12 3 0 96.99 8.30 -12 15 0 124.29 13.30 -12 15 0 100.29 13.50 12 3 0 114.59 18.10 -3 -12 0 98.89 12.60 15 -3 0 89.69 13.70 -15 12 0 75.79 14.30 3 -15 0 116.59 14.40 15 -3 0 128.59 15.70 3 12 0 122.29 15.70 12 -15 0 133.89 17.20 -12 -3 0 108.39 12.80 3 12 0 111.99 13.10 15 -12 0 99.09 8.70 -15 3 0 124.39 12.20 15 -12 0 105.39 16.00 -3 15 0 113.79 18.70 -3 15 0 108.69 13.60 -13 15 0 62.39 11.20 15 -2 0 78.09 12.00 -15 13 0 63.69 10.30 -13 15 0 59.39 9.90 13 2 0 76.49 13.30 15 -2 0 69.79 13.70 2 -15 0 61.69 12.80 13 2 0 71.09 8.00 -2 -13 0 55.49 10.40 13 -15 0 86.69 16.70 15 -13 0 71.19 15.60 -2 15 0 75.49 14.10 -15 2 0 91.59 11.80 -13 -2 0 54.89 8.90 2 13 0 68.09 12.60 2 13 0 81.69 14.50 -2 15 0 72.39 10.40 -1 -14 0 144.49 16.30 14 1 0 177.78 20.10 -15 14 0 201.18 13.60 -14 15 0 148.69 15.60 -14 15 0 164.08 16.40 14 1 0 166.08 14.10 1 -15 0 156.78 17.60 15 -1 0 191.68 18.90 -15 14 0 146.29 16.10 15 -1 0 175.98 17.60 -14 -1 0 168.28 15.30 -1 15 0 177.68 16.00 -1 15 0 174.28 21.00 14 -15 0 180.78 22.70 -15 1 0 178.28 15.00 1 14 0 169.78 15.50 15 -14 0 129.79 22.30 1 14 0 167.58 21.40 15 0 0 358.06 25.90 -15 15 0 374.96 21.50 15 0 0 343.37 22.90 0 -15 0 374.06 24.20 -15 15 0 331.27 22.80 -15 0 0 354.86 22.10 0 15 0 384.26 27.60 -16 8 0 1870.21 89.39 8 -16 0 1758.22 90.99 16 -8 0 1808.32 88.39 8 8 0 1766.52 90.79 -8 16 0 1880.21 89.69 -8 16 0 1878.01 89.49 -9 16 0 13.60 8.50 16 -7 0 25.60 13.90 7 -16 0 22.40 13.80 16 -7 0 23.90 7.90 -9 16 0 43.50 11.40 -16 9 0 13.30 8.80 9 7 0 15.40 12.30 16 -9 0 14.20 6.70 -9 -7 0 13.30 8.20 16 -9 0 26.20 14.00 9 -16 0 11.80 14.10 7 9 0 25.40 7.50 7 9 0 18.80 13.40 -16 7 0 16.60 9.20 -7 16 0 17.50 8.20 -7 16 0 29.70 11.60 -10 16 0 27.10 8.80 -16 10 0 15.90 9.30 16 -6 0 41.90 13.20 -10 16 0 44.60 11.00 16 -6 0 28.00 8.60 6 -16 0 27.50 13.70 10 6 0 24.00 12.90 -10 -6 0 18.40 8.00 6 10 0 27.00 8.50 10 -16 0 29.10 14.60 16 -10 0 38.50 14.10 16 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16.00 16 -13 0 14.70 14.40 -3 16 0 6.20 13.10 3 13 0 12.30 9.00 3 13 0 -3.90 13.20 16 -13 0 2.70 4.60 -14 16 0 6.10 9.00 2 -16 0 11.10 12.20 16 -2 0 13.70 10.70 16 -2 0 17.60 12.80 14 2 0 11.80 19.70 -14 16 0 0.40 10.70 14 2 0 12.60 6.90 -2 -14 0 7.80 10.00 -16 14 0 -4.80 9.10 -14 -2 0 19.40 8.00 16 -14 0 32.40 26.80 -2 16 0 15.40 10.70 2 14 0 13.40 10.10 14 -16 0 21.10 17.00 -2 16 0 34.30 13.90 2 14 0 22.30 14.10 -16 2 0 29.80 7.90 1 -16 0 110.69 17.70 16 -1 0 142.59 18.70 -15 16 0 112.89 15.20 -1 -15 0 118.09 16.40 -16 15 0 148.49 13.10 -16 15 0 104.29 15.30 16 -1 0 136.99 16.70 15 1 0 116.99 18.90 15 1 0 125.39 13.50 -15 16 0 122.49 15.10 -15 -1 0 138.69 15.70 1 15 0 122.59 21.50 16 -15 0 141.79 18.90 -16 1 0 161.68 14.60 15 -16 0 155.08 19.60 1 15 0 152.48 16.30 -1 16 0 130.69 20.70 -1 16 0 137.69 15.60 -16 16 0 12.40 9.20 16 0 0 23.50 12.40 0 -16 0 8.80 11.70 16 0 0 18.30 10.40 -16 16 0 4.50 17.70 0 16 0 17.90 9.20 0 16 0 19.00 14.70 -16 0 0 19.30 10.20 16 -16 0 20.10 16.10 9 8 0 744.93 41.10 17 -8 0 716.03 37.60 -9 17 0 769.02 39.80 17 -8 0 662.93 41.50 8 -17 0 702.53 42.10 -17 9 0 721.33 39.10 -9 17 0 742.03 38.90 -17 8 0 752.52 38.90 17 -9 0 678.93 41.90 8 9 0 737.33 41.50 17 -9 0 676.53 37.00 -8 17 0 748.93 39.70 -8 17 0 752.62 39.20 9 -17 0 658.23 41.40 -9 -8 0 780.72 38.70 10 7 0 34.60 15.30 7 -17 0 38.60 15.00 -17 10 0 20.80 10.00 -10 17 0 37.50 9.40 17 -7 0 36.80 16.70 -17 7 0 37.50 10.00 7 10 0 54.69 14.80 17 -10 0 42.40 7.30 17 -10 0 48.70 15.50 -10 -7 0 39.60 9.20 7 10 0 63.29 12.00 -7 17 0 34.80 9.70 10 -17 0 42.60 15.60 -7 17 0 50.99 13.20 17 -6 0 268.27 20.00 -11 17 0 294.87 21.40 17 -6 0 242.78 24.20 6 -17 0 261.97 25.40 -11 17 0 339.57 22.20 -6 -11 0 350.66 18.00 -17 11 0 285.77 21.20 6 11 0 302.57 27.50 17 -11 0 282.17 17.50 -6 17 0 318.17 23.10 17 -11 0 253.27 25.50 6 11 0 302.77 26.40 -6 17 0 304.27 24.20 -11 -6 0 296.67 19.60 -17 6 0 305.27 21.40 11 -17 0 296.77 27.90 -5 -12 0 352.06 20.20 5 -17 0 313.07 26.10 17 -5 0 336.07 26.90 17 -5 0 347.77 22.40 -17 12 0 296.27 22.80 -12 17 0 350.36 23.10 12 5 0 363.36 28.90 -12 17 0 348.77 22.10 -12 -5 0 345.27 22.10 5 12 0 290.97 24.80 17 -12 0 324.67 28.50 -17 5 0 347.07 22.20 5 12 0 306.47 27.60 -5 17 0 367.96 26.30 17 -12 0 330.57 18.80 -4 -13 0 588.74 29.80 17 -4 0 545.35 31.40 -17 13 0 530.95 31.30 13 4 0 564.84 34.00 17 -4 0 559.74 34.10 -13 17 0 555.34 31.30 -13 17 0 491.35 31.10 4 -17 0 557.94 34.10 13 -17 0 492.65 36.80 -4 17 0 553.44 31.00 -4 17 0 593.84 34.00 4 13 0 557.74 35.40 17 -13 0 483.75 37.10 -13 -4 0 586.44 36.10 4 13 0 539.75 30.60 17 -13 0 499.15 27.50 -17 4 0 526.35 29.80 -14 17 0 369.36 26.80 17 -3 0 437.46 29.10 14 3 0 444.66 28.90 -3 -14 0 421.06 25.00 17 -3 0 396.96 26.00 14 3 0 398.56 21.50 -14 17 0 448.66 31.00 -17 14 0 415.76 26.40 -3 17 0 430.66 25.70 17 -14 0 370.96 30.40 -3 17 0 456.95 29.60 3 14 0 439.46 25.30 14 -17 0 412.66 32.70 17 -14 0 366.76 21.40 -17 3 0 417.16 24.80 3 14 0 439.76 30.60 -14 -3 0 422.56 32.60 15 2 0 50.49 8.10 15 2 0 50.79 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18 0 87.09 13.90 10 8 0 45.70 14.70 -18 10 0 53.19 11.20 18 -8 0 65.79 15.90 18 -8 0 57.49 9.50 8 -18 0 43.80 16.00 -10 18 0 48.20 11.60 18 -10 0 73.39 17.00 -8 18 0 78.29 14.70 -8 18 0 55.59 10.50 8 10 0 46.30 15.20 18 -10 0 57.29 8.60 -10 -8 0 39.50 10.00 -18 8 0 60.09 11.40 10 -18 0 77.39 19.20 11 7 0 152.28 21.00 7 -18 0 155.38 19.30 18 -7 0 158.48 15.30 -11 18 0 129.19 18.00 18 -7 0 134.09 20.10 18 -11 0 169.48 24.00 7 11 0 143.19 14.70 -7 18 0 160.38 20.60 -11 -7 0 136.99 15.30 7 11 0 152.68 21.50 -7 18 0 149.69 16.40 -18 7 0 146.19 16.40 18 -11 0 147.29 12.60 11 -18 0 139.49 24.00 -12 18 0 602.64 31.50 18 -6 0 531.35 34.80 12 6 0 534.25 33.90 6 -18 0 498.35 34.60 -6 -12 0 579.54 28.50 18 -6 0 517.25 30.30 -12 18 0 549.74 31.20 -18 12 0 518.55 31.40 6 12 0 491.45 30.20 18 -12 0 531.65 27.90 12 -18 0 516.85 36.90 -6 18 0 522.55 31.40 -18 6 0 533.45 30.60 -6 18 0 537.65 33.40 18 -12 0 550.74 35.80 -12 -6 0 515.45 30.10 13 5 0 75.29 15.40 5 -18 0 91.69 16.80 -18 13 0 71.19 12.80 -13 18 0 113.29 16.50 18 -5 0 84.29 15.20 18 -5 0 94.89 16.50 -13 18 0 68.59 14.20 13 -18 0 82.59 18.50 -5 18 0 89.89 14.90 5 13 0 85.89 14.20 -5 18 0 104.79 16.10 18 -13 0 78.39 9.40 -18 5 0 134.99 23.10 -13 -5 0 78.29 14.10 18 -13 0 91.89 20.20 18 -4 0 198.28 18.60 -14 18 0 170.28 19.00 18 -4 0 200.38 23.80 14 4 0 194.88 21.70 -4 -14 0 163.18 16.60 14 4 0 181.48 11.30 -14 18 0 181.78 17.40 4 -18 0 192.38 23.50 4 14 0 202.58 17.40 4 14 0 211.98 27.20 -4 18 0 213.38 22.70 18 -14 0 187.98 12.60 -14 -4 0 210.18 17.10 -18 4 0 220.18 17.60 18 -14 0 224.98 26.70 -4 18 0 206.28 18.00 14 -18 0 178.68 27.60 18 -3 0 791.92 43.90 3 -18 0 794.92 45.00 -3 -15 0 742.93 41.80 15 3 0 758.92 39.10 15 3 0 822.22 45.00 -15 18 0 844.72 42.70 -15 18 0 735.03 42.90 -18 15 0 815.22 42.80 18 -3 0 843.32 44.90 15 -18 0 749.82 47.90 -15 -3 0 793.12 42.10 3 15 0 886.91 47.60 -18 3 0 758.42 41.80 3 15 0 833.52 42.90 18 -15 0 772.72 47.60 -3 18 0 796.22 46.60 -3 18 0 836.62 43.30 -16 18 0 0.30 9.70 -18 16 0 -16.30 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19 -8 0 156.38 18.40 8 -19 0 179.68 20.80 11 8 0 114.29 21.20 -11 19 0 107.29 16.00 -19 11 0 125.69 20.20 -8 19 0 122.29 16.30 8 11 0 158.38 15.40 11 -19 0 168.98 21.30 19 -11 0 156.28 20.50 19 -11 0 118.99 12.60 8 11 0 120.69 21.30 -11 -8 0 129.89 15.60 -8 19 0 179.28 21.80 -19 8 0 119.09 19.10 -19 12 0 137.69 19.30 19 -7 0 146.19 16.10 12 7 0 143.39 21.90 7 -19 0 132.19 19.40 19 -7 0 134.69 21.80 -12 19 0 145.49 16.80 -7 19 0 179.88 21.60 -7 19 0 149.88 17.20 -19 7 0 149.79 18.00 19 -12 0 190.98 26.80 -12 -7 0 154.48 15.90 7 12 0 168.68 15.60 7 12 0 145.89 22.50 19 -12 0 146.19 12.70 12 -19 0 170.78 21.40 13 6 0 57.49 15.90 -13 19 0 52.69 11.10 19 -6 0 58.49 16.70 19 -6 0 65.09 11.50 -19 13 0 38.00 11.40 6 -19 0 53.49 16.50 -13 -6 0 54.59 10.30 -6 19 0 43.70 11.00 -19 6 0 60.69 11.60 6 13 0 47.30 16.60 6 13 0 49.30 10.40 19 -13 0 75.99 18.20 -6 19 0 85.69 16.10 19 -13 0 51.09 7.40 13 -19 0 43.30 18.40 -5 -14 0 18.50 9.40 14 5 0 -2.70 14.40 19 -5 0 20.80 17.70 -14 19 0 31.10 11.70 5 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16.20 20 -14 0 10.30 18.40 6 14 0 2.10 9.70 -6 20 0 2.60 10.50 -20 6 0 18.80 11.30 -14 -6 0 2.90 9.30 20 -14 0 -0.80 6.10 6 14 0 -1.80 16.50 14 -20 0 8.70 18.90 -15 20 0 -4.20 10.10 20 -5 0 -19.10 18.70 20 -5 0 3.90 11.40 15 5 0 -5.30 15.10 -15 20 0 24.20 12.20 5 -20 0 -21.70 16.10 -5 20 0 17.90 20.10 5 15 0 2.50 10.30 20 -15 0 0.60 5.90 -15 -5 0 4.00 10.00 -5 20 0 -4.10 10.50 15 -20 0 5.40 19.80 5 15 0 -7.60 16.70 20 -15 0 24.30 18.90 -20 16 0 99.59 15.30 -16 20 0 129.99 19.70 4 -20 0 162.08 20.30 20 -4 0 110.79 19.00 -16 20 0 97.29 17.80 20 -4 0 132.59 19.60 16 4 0 152.38 19.50 -16 -4 0 145.39 16.70 -4 20 0 137.49 18.50 -20 4 0 144.79 16.70 4 16 0 161.18 21.70 -4 20 0 155.68 25.20 16 -20 0 124.49 23.40 4 16 0 143.19 18.60 20 -16 0 152.58 23.30 17 3 0 293.87 26.80 20 -3 0 289.97 26.70 -20 17 0 261.57 23.70 17 3 0 303.77 17.80 -17 20 0 276.67 24.10 20 -3 0 299.47 25.00 3 -20 0 319.07 28.50 3 17 0 297.07 30.70 20 -17 0 329.57 34.50 -3 20 0 313.97 24.00 -20 3 0 313.77 22.60 -3 20 0 329.67 30.60 17 -20 0 334.97 34.70 -17 -3 0 317.67 22.60 3 17 0 318.77 23.10 -20 18 0 55.19 11.00 20 -2 0 29.90 15.80 18 2 0 19.10 15.70 18 2 0 33.30 8.60 -18 20 0 27.30 12.00 20 -2 0 30.30 14.10 2 -20 0 45.50 17.20 -18 -2 0 43.60 11.70 2 18 0 29.90 19.10 2 18 0 39.40 12.10 18 -20 0 42.70 22.30 -2 20 0 35.90 12.50 20 -18 0 69.89 22.20 -2 20 0 46.40 19.50 19 1 0 220.28 24.30 1 -20 0 201.38 25.10 19 1 0 218.68 18.30 -19 20 0 196.18 22.40 20 -1 0 222.18 22.50 -20 19 0 206.58 20.50 20 -1 0 205.78 24.00 -20 19 0 173.58 22.00 -1 20 0 224.78 30.90 20 -19 0 244.88 32.30 1 19 0 224.98 21.30 1 19 0 232.38 29.20 19 -20 0 259.17 34.60 -1 20 0 235.58 22.50 -19 -1 0 229.38 20.20 -20 1 0 225.38 19.00 20 0 0 4.30 12.20 0 -20 0 -19.60 16.20 -20 20 0 -7.40 12.40 -20 20 0 -22.00 14.20 20 0 0 -8.80 14.20 0 20 0 4.20 12.00 -20 0 0 23.90 11.10 20 -20 0 23.70 24.00 0 20 0 2.20 20.40 10 -21 0 948.81 55.19 11 10 0 943.81 53.39 -11 21 0 1040.90 52.19 -11 21 0 972.00 50.59 21 -10 0 876.61 48.50 -21 11 0 920.81 50.19 21 -11 0 880.51 53.89 21 -11 0 928.81 48.50 -11 -10 0 984.10 50.49 -21 10 0 968.00 50.89 -10 21 0 967.50 50.79 -10 21 0 1026.40 52.29 10 11 0 945.11 53.39 11 -21 0 951.60 55.69 21 -9 0 199.48 25.30 21 -9 0 202.28 17.70 12 9 0 184.58 25.10 -12 21 0 198.28 20.10 9 -21 0 179.28 28.60 -21 12 0 190.38 21.60 -12 -9 0 213.08 19.90 -21 9 0 181.48 20.90 -9 21 0 253.37 25.00 21 -12 0 227.98 28.50 9 12 0 203.68 25.30 12 -21 0 229.28 30.60 21 -12 0 205.28 16.30 -9 21 0 203.08 20.30 21 -8 0 158.98 26.70 13 8 0 173.38 24.80 8 -21 0 176.68 27.50 -21 13 0 175.38 20.60 -13 21 0 193.38 19.50 21 -8 0 201.98 22.50 21 -13 0 241.38 29.70 -8 21 0 258.87 24.90 8 13 0 204.08 25.30 -8 21 0 199.88 20.30 -21 8 0 190.88 21.40 -13 -8 0 193.08 18.80 8 13 0 227.48 18.70 13 -21 0 199.78 28.70 21 -7 0 59.19 18.30 21 -7 0 66.99 12.60 7 -21 0 64.09 19.40 -21 14 0 32.20 12.90 -7 -14 0 37.10 10.10 -14 21 0 46.50 12.30 14 7 0 48.40 17.60 -7 21 0 98.39 18.40 -14 -7 0 62.49 11.70 21 -14 0 59.29 10.50 -21 7 0 69.79 13.10 21 -14 0 88.69 21.40 7 14 0 62.19 18.50 -7 21 0 63.29 12.60 7 14 0 87.39 15.50 14 -21 0 72.19 21.70 -15 21 0 654.13 38.60 -21 15 0 660.23 38.60 -6 -15 0 599.84 35.60 21 -6 0 692.93 38.20 6 -21 0 707.93 43.20 15 6 0 678.53 41.20 21 -6 0 687.03 42.50 -21 6 0 657.33 38.40 21 -15 0 695.63 45.10 -6 21 0 680.23 39.00 -15 -6 0 667.63 37.20 6 15 0 694.73 38.20 15 -21 0 636.44 45.70 6 15 0 672.93 43.80 21 -15 0 657.43 34.10 -6 21 0 644.64 47.20 -16 21 0 490.65 30.90 16 5 0 483.35 34.50 -21 16 0 443.56 31.70 -16 21 0 567.34 31.80 21 -5 0 463.85 36.20 21 -5 0 495.05 31.50 5 16 0 533.75 30.70 21 -16 0 503.85 40.10 -21 5 0 473.35 30.60 -5 21 0 517.75 32.20 -5 21 0 533.65 36.20 16 -21 0 501.25 40.80 21 -16 0 449.76 26.10 -16 -5 0 508.55 30.10 5 16 0 520.75 37.70 4 -21 0 66.79 19.30 -17 21 0 79.59 14.40 17 4 0 55.19 17.30 21 -4 0 50.59 14.00 -17 21 0 47.00 12.80 -21 17 0 35.70 13.30 -17 -4 0 56.69 12.10 4 17 0 68.39 20.40 -4 21 0 90.69 20.60 17 -21 0 69.79 23.10 21 -17 0 101.09 23.60 4 17 0 50.59 12.20 -4 21 0 58.59 12.70 -21 18 0 120.79 21.30 3 -21 0 174.28 26.70 21 -3 0 140.09 21.90 18 3 0 174.38 24.10 -21 18 0 209.98 17.40 21 -3 0 157.28 23.30 -18 21 0 148.89 20.20 18 3 0 160.68 12.80 21 -18 0 216.68 34.10 -21 3 0 208.78 19.90 3 18 0 175.08 20.60 -3 21 0 176.68 29.40 -3 21 0 174.38 21.00 3 18 0 155.98 28.90 18 -21 0 179.28 26.80 -18 -3 0 197.78 20.00 -19 21 0 7.90 12.30 21 -2 0 15.60 16.10 21 -2 0 10.40 14.10 2 -21 0 13.40 17.90 19 2 0 12.10 8.20 19 2 0 11.90 16.00 -21 19 0 -13.00 12.70 -21 19 0 16.10 12.10 2 19 0 13.80 20.80 19 -21 0 55.89 22.90 -19 -2 0 25.50 11.70 2 19 0 28.50 12.50 -2 21 0 24.40 12.50 21 -19 0 69.09 24.10 -2 21 0 22.80 21.40 1 -21 0 100.69 19.70 20 1 0 105.29 13.30 21 -1 0 85.29 17.30 20 1 0 79.19 17.70 -20 21 0 73.69 15.20 -21 20 0 85.69 15.40 -1 -20 0 84.29 18.20 21 -1 0 96.49 16.20 -20 -1 0 117.69 18.10 1 20 0 97.49 19.00 -1 21 0 103.69 20.50 20 -21 0 118.59 25.80 21 -20 0 120.39 26.30 1 20 0 98.29 23.30 -1 21 0 109.89 23.80 -21 21 0 2234.98 101.79 0 -21 0 2085.19 102.89 21 0 0 2063.49 100.39 21 0 0 2020.90 102.69 -21 21 0 2008.50 101.79 -21 0 0 1823.82 100.49 21 -21 0 2035.20 107.09 0 21 0 2135.09 104.89 0 21 0 2033.20 101.79 22 -11 0 485.05 35.90 11 -22 0 497.15 39.00 -11 22 0 509.65 31.10 -11 -11 0 459.85 30.30 11 11 0 457.95 35.20 22 -11 0 533.15 28.70 -22 11 0 471.85 30.90 12 10 0 6.30 17.20 10 -22 0 31.30 20.50 22 -10 0 30.30 17.80 -12 22 0 2.70 11.70 -22 12 0 -10.00 12.50 22 -10 0 18.30 10.00 -12 -10 0 2.30 11.10 -10 22 0 7.60 11.80 -22 10 0 2.60 12.40 -10 22 0 34.80 17.30 10 12 0 14.40 17.40 22 -12 0 10.50 9.10 22 -12 0 35.50 19.40 12 -22 0 18.10 21.00 13 9 0 14.90 17.30 -13 22 0 21.30 12.10 9 -22 0 30.50 20.60 22 -9 0 25.00 12.20 -22 13 0 -3.80 12.80 9 13 0 4.30 17.30 -13 -9 0 22.00 11.20 13 -22 0 26.60 21.40 22 -13 0 41.60 20.50 -22 9 0 19.60 13.60 -9 22 0 48.60 17.80 22 -13 0 29.90 8.80 -9 22 0 16.50 11.80 22 -8 0 90.99 13.50 8 -22 0 80.09 21.60 14 8 0 79.49 19.10 -22 14 0 66.59 14.40 22 -8 0 87.59 20.30 -14 22 0 79.69 14.00 14 -22 0 118.79 23.70 22 -14 0 126.69 23.00 8 14 0 108.39 17.40 8 14 0 89.09 19.90 -8 22 0 138.79 24.60 -14 -8 0 96.39 17.80 -22 8 0 82.49 14.60 22 -14 0 79.39 11.90 -8 22 0 73.49 13.90 7 -22 0 162.28 23.50 15 7 0 141.89 26.30 -15 22 0 135.59 20.30 -22 15 0 102.59 21.90 22 -7 0 154.58 20.10 22 -7 0 163.68 23.10 -7 -15 0 145.59 14.00 22 -15 0 130.99 15.00 -15 -7 0 156.28 18.80 7 15 0 158.38 22.10 -7 22 0 144.89 21.00 7 15 0 187.18 18.70 15 -22 0 170.58 25.20 -7 22 0 172.38 38.40 -22 7 0 164.28 19.80 22 -15 0 170.88 29.60 6 -22 0 49.50 20.50 16 6 0 63.99 17.50 22 -6 0 59.19 14.00 -16 22 0 43.20 13.00 -22 16 0 27.10 13.70 22 -6 0 43.60 19.80 -22 6 0 77.39 14.40 16 -22 0 83.99 23.90 22 -16 0 99.59 23.40 22 -16 0 62.89 10.20 6 16 0 58.09 12.90 -16 -6 0 55.59 12.80 -6 22 0 60.29 13.60 -6 22 0 103.49 21.20 6 16 0 40.90 19.60 22 -5 0 139.69 21.90 -17 22 0 136.29 19.00 22 -5 0 153.38 20.80 17 5 0 159.88 21.40 -22 17 0 123.99 17.10 5 -22 0 149.69 23.10 -5 22 0 161.68 27.70 5 17 0 163.08 24.60 -5 22 0 129.89 20.20 5 17 0 148.49 19.90 17 -22 0 157.08 26.60 22 -17 0 206.88 33.70 -22 5 0 145.59 20.50 -17 -5 0 153.38 19.10 18 4 0 22.70 17.30 22 -4 0 19.60 13.90 22 -4 0 26.40 17.80 -18 22 0 6.60 12.30 4 -22 0 14.30 20.10 18 4 0 26.30 6.60 -4 22 0 22.70 13.60 4 18 0 23.10 21.20 -22 4 0 41.90 12.10 22 -18 0 59.39 24.00 4 18 0 32.60 12.20 -18 -4 0 25.60 11.20 18 -22 0 56.29 24.00 -4 22 0 55.79 21.60 -22 19 0 46.10 12.20 22 -3 0 18.20 14.60 -19 22 0 -10.80 13.70 -19 22 0 -2.00 13.10 19 3 0 18.70 17.00 19 3 0 22.00 8.20 -22 3 0 40.40 12.10 -19 -3 0 31.00 12.30 3 19 0 27.40 12.40 22 -19 0 61.19 24.60 -3 22 0 29.50 23.00 19 -22 0 69.59 24.60 -3 22 0 25.70 13.10 3 19 0 13.00 21.60 -22 20 0 280.77 23.30 20 2 0 281.87 28.70 20 2 0 253.87 18.10 22 -2 0 270.37 25.70 2 -22 0 254.17 31.20 -22 20 0 235.48 25.50 22 -2 0 260.87 26.70 -20 22 0 232.28 25.30 20 -22 0 351.16 37.00 22 -20 0 369.56 39.30 -2 22 0 278.97 24.40 -2 22 0 294.67 34.50 -22 2 0 289.67 23.10 2 20 0 292.97 33.20 -20 -2 0 310.07 23.60 2 20 0 286.37 24.00 -22 21 0 458.75 33.10 -21 22 0 458.45 33.10 22 -1 0 459.65 33.70 21 1 0 469.45 33.90 21 1 0 465.25 28.90 1 -22 0 514.55 37.30 22 -1 0 476.25 32.10 -1 -21 0 457.15 35.30 -22 21 0 479.15 32.40 1 21 0 520.05 39.90 21 -22 0 551.34 43.60 22 -21 0 553.44 45.70 -22 1 0 483.95 31.70 -1 22 0 541.35 41.80 -1 22 0 500.75 32.60 1 21 0 507.45 33.40 -21 -1 0 490.85 31.50 0 -22 0 89.69 19.90 22 0 0 80.69 15.30 22 0 0 65.29 17.70 -22 22 0 53.79 15.00 22 -22 0 141.39 28.90 0 22 0 67.89 14.90 0 22 0 84.79 25.20 -22 0 0 110.79 19.90 -12 23 0 22.50 12.70 -11 -12 0 19.30 12.70 -23 12 0 2.80 13.70 23 -11 0 35.30 19.10 12 11 0 25.70 18.30 11 -23 0 66.69 22.80 23 -12 0 39.70 19.20 11 12 0 14.70 18.20 -12 -11 0 22.30 12.60 -11 23 0 29.80 12.90 12 -23 0 58.89 23.10 23 -12 0 33.30 10.30 -23 11 0 18.40 13.20 -23 13 0 277.17 26.90 -13 23 0 340.57 25.90 23 -10 0 284.17 33.30 10 -23 0 372.06 35.30 13 10 0 308.57 30.50 23 -10 0 348.67 23.50 13 -23 0 335.77 36.90 -23 10 0 316.67 26.50 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41.60 12.70 -17 23 0 95.19 19.70 23 -6 0 126.29 20.50 23 -6 0 80.59 21.50 17 6 0 117.19 20.40 6 -23 0 103.59 23.10 -6 23 0 180.28 24.60 -23 6 0 129.99 21.50 -6 23 0 114.39 21.50 17 -23 0 146.69 27.00 -17 -6 0 139.29 18.60 23 -17 0 90.29 12.00 6 17 0 129.49 19.30 6 17 0 137.19 23.50 5 -23 0 -9.70 20.50 23 -5 0 -21.60 18.10 -18 23 0 -9.90 12.70 23 -5 0 3.70 13.60 18 5 0 -3.10 16.70 5 18 0 -0.40 20.20 -5 23 0 2.80 12.50 -23 5 0 24.00 13.30 -5 23 0 51.39 22.20 -18 -5 0 17.20 12.00 23 -18 0 27.70 24.30 5 18 0 9.40 12.60 18 -23 0 40.00 24.90 23 -4 0 733.43 42.50 -19 23 0 804.82 41.00 23 -4 0 678.83 43.80 -19 23 0 708.53 41.50 19 4 0 704.43 45.20 -23 19 0 691.23 42.70 4 -23 0 700.73 46.70 -23 4 0 642.74 39.90 -4 23 0 730.03 42.40 -4 23 0 797.82 51.39 23 -19 0 778.52 51.99 19 -23 0 676.43 49.70 -19 -4 0 739.63 40.80 4 19 0 694.33 42.60 4 19 0 739.73 48.10 20 3 0 339.97 30.20 -23 20 0 368.76 24.90 20 3 0 342.47 20.10 23 -3 0 327.77 28.80 -20 23 0 370.66 27.20 -20 23 0 307.67 27.60 3 -23 0 336.07 34.00 -23 20 0 288.07 28.30 23 -3 0 342.57 33.60 20 -23 0 399.26 39.70 -3 23 0 363.36 28.10 -23 3 0 341.37 26.60 3 20 0 353.66 28.20 -20 -3 0 376.16 26.30 -3 23 0 393.26 36.50 23 -20 0 438.86 39.30 3 20 0 348.37 36.30 23 -2 0 41.20 16.40 23 -2 0 41.60 18.50 2 -23 0 44.40 25.80 -21 23 0 33.40 14.40 21 2 0 39.30 9.90 -23 21 0 24.00 14.70 21 2 0 44.30 17.50 -23 21 0 34.40 15.40 2 21 0 50.99 14.00 -2 23 0 64.79 25.20 2 21 0 46.70 24.20 23 -21 0 105.39 28.20 -2 23 0 54.49 14.40 21 -23 0 99.69 29.10 23 -1 0 59.99 16.20 23 -1 0 65.59 17.30 22 1 0 46.10 17.60 22 1 0 60.79 12.40 -23 22 0 20.10 16.90 -22 23 0 38.40 15.50 -1 -22 0 80.89 19.10 1 -23 0 79.69 23.90 23 -22 0 145.49 29.30 -1 23 0 69.39 15.30 -1 23 0 106.99 26.80 1 22 0 72.49 15.00 -22 -1 0 71.29 14.60 1 22 0 62.19 25.70 -23 1 0 69.99 15.40 22 -23 0 120.49 29.40 -23 23 0 20.30 15.20 23 0 0 45.10 17.30 23 0 0 52.29 15.80 0 -23 0 50.19 20.40 0 23 0 43.10 15.10 -23 0 0 58.59 14.60 23 -23 0 120.89 29.70 0 23 0 64.69 26.10 24 -12 0 481.15 28.00 -24 12 0 427.56 32.10 12 -24 0 485.95 40.80 -12 -12 0 480.85 30.70 -12 24 0 468.15 32.10 12 12 0 452.25 37.20 24 -12 0 414.56 36.40 -24 13 0 119.49 17.10 -13 24 0 118.59 20.10 11 -24 0 140.79 25.40 13 11 0 122.79 21.70 24 -11 0 130.99 23.20 -11 -13 0 104.19 21.40 24 -11 0 112.39 17.00 24 -13 0 123.79 22.50 24 -13 0 122.59 15.60 13 -24 0 163.68 26.00 11 13 0 125.59 21.70 -11 24 0 144.39 20.80 -13 -11 0 119.59 19.40 -24 11 0 113.69 22.10 24 -10 0 236.08 32.40 10 -24 0 320.67 34.60 14 10 0 244.78 31.10 -24 14 0 237.08 26.20 -14 24 0 286.27 25.90 24 -10 0 292.07 22.80 14 -24 0 320.57 37.10 -10 24 0 279.67 24.90 10 14 0 270.57 30.40 24 -14 0 325.47 33.80 24 -14 0 310.87 20.60 -14 -10 0 271.17 24.40 -24 10 0 273.57 26.80 -24 15 0 238.58 25.20 24 -9 0 298.77 23.20 -15 24 0 278.47 24.50 24 -9 0 250.67 32.20 9 -24 0 248.28 34.50 15 9 0 271.47 31.00 -24 9 0 278.97 26.70 9 15 0 247.48 30.60 24 -15 0 317.87 34.30 15 -24 0 306.67 37.70 24 -15 0 308.57 19.50 -15 -9 0 284.47 24.30 -9 24 0 277.37 26.00 -16 24 0 28.70 13.40 8 -24 0 24.90 22.30 24 -8 0 28.10 13.00 24 -8 0 -23.10 20.90 -24 16 0 4.30 14.90 16 8 0 26.00 18.90 24 -16 0 36.70 9.20 -8 24 0 34.00 14.00 24 -16 0 85.29 24.30 8 16 0 22.20 20.30 -24 8 0 25.80 15.00 -8 24 0 75.79 22.10 -16 -8 0 24.00 12.60 8 16 0 43.90 12.50 16 -24 0 55.09 25.30 7 -24 0 13.40 21.80 -17 24 0 2.80 13.20 24 -7 0 -30.60 24.10 24 -7 0 26.00 13.90 17 7 0 17.80 18.40 7 17 0 31.20 20.80 17 -24 0 44.50 25.40 -7 24 0 66.49 22.90 -17 -7 0 31.10 13.30 -7 24 0 18.00 13.80 24 -17 0 63.89 24.30 24 -17 0 23.20 8.70 -24 7 0 26.90 14.50 7 17 0 33.10 12.50 -18 24 0 218.38 23.90 18 6 0 242.48 28.40 -6 -18 0 204.88 20.10 6 -24 0 214.18 37.30 24 -6 0 244.58 27.00 24 -6 0 235.28 24.00 -6 24 0 255.77 25.10 24 -18 0 343.37 38.20 -18 -6 0 265.87 23.40 6 18 0 244.68 32.70 -24 6 0 259.17 25.50 18 -24 0 261.47 38.80 6 18 0 258.67 23.70 -6 24 0 297.87 34.30 5 -24 0 116.39 24.20 24 -5 0 122.59 22.00 19 5 0 94.59 20.90 -19 24 0 91.19 16.20 24 -5 0 137.39 22.60 -5 24 0 143.79 32.90 -19 -5 0 131.19 20.70 5 19 0 142.49 20.30 5 19 0 120.59 24.00 19 -24 0 149.09 28.40 24 -19 0 163.08 28.40 -5 24 0 117.39 22.90 -24 5 0 137.79 20.10 -20 24 0 106.89 22.30 4 -24 0 137.99 24.50 24 -4 0 121.39 18.60 -24 20 0 157.08 18.70 24 -4 0 125.39 22.20 20 4 0 120.69 21.30 20 -24 0 190.48 30.70 -4 24 0 133.29 22.50 -24 4 0 147.29 22.40 -20 -4 0 135.79 21.90 -4 24 0 201.18 27.90 4 20 0 123.49 25.60 4 20 0 130.19 20.70 24 -3 0 161.58 24.20 3 -24 0 176.18 25.10 -21 24 0 132.59 23.30 -24 21 0 159.08 21.80 24 -3 0 162.68 26.20 21 3 0 142.69 12.90 -24 21 0 151.18 19.00 21 3 0 144.19 25.20 3 21 0 209.28 28.80 21 -24 0 233.38 37.50 24 -21 0 272.47 39.60 3 21 0 151.78 21.70 -21 -3 0 189.38 20.70 -24 3 0 209.48 21.90 -3 24 0 211.98 34.70 -3 24 0 161.38 24.50 2 -24 0 24.40 21.00 -24 22 0 -0.70 16.30 22 2 0 13.70 17.20 -24 22 0 -4.00 14.20 22 2 0 20.90 11.30 24 -2 0 23.10 16.60 -22 24 0 8.90 14.60 -2 24 0 71.09 26.70 24 -22 0 74.69 27.70 -22 -2 0 55.99 13.80 2 22 0 29.70 14.70 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21.80 -25 11 0 215.28 25.00 -11 25 0 257.17 25.00 -14 -11 0 257.27 23.20 14 -25 0 302.27 37.40 11 14 0 260.47 30.30 25 -14 0 260.67 32.00 -25 15 0 0.60 14.80 10 -25 0 55.19 24.00 25 -10 0 -2.30 21.20 25 -10 0 31.00 16.20 15 10 0 24.40 19.40 -15 25 0 10.10 13.70 15 -25 0 49.80 25.90 25 -15 0 33.60 10.00 -10 25 0 18.20 14.20 -15 -10 0 23.10 13.80 -25 10 0 12.90 15.90 10 15 0 5.40 19.40 25 -15 0 78.09 22.80 25 -9 0 17.80 13.60 9 -25 0 -0.50 23.10 16 9 0 7.20 18.80 -16 25 0 7.00 13.70 -9 25 0 63.39 23.80 25 -16 0 3.90 8.70 25 -16 0 57.49 23.90 -16 -9 0 16.20 13.00 -9 25 0 0.10 14.10 -25 9 0 -7.90 15.40 16 -25 0 44.20 26.20 9 16 0 5.30 20.60 8 -25 0 322.47 36.50 -17 25 0 320.47 28.10 25 -8 0 363.26 26.70 17 8 0 336.87 33.50 -25 17 0 282.97 28.70 -25 8 0 342.97 28.80 -8 25 0 453.75 35.90 25 -17 0 410.66 39.20 8 17 0 356.16 34.10 -8 25 0 360.26 29.80 17 -25 0 358.16 38.90 8 17 0 375.36 27.90 -17 -8 0 348.37 26.80 25 -17 0 356.26 22.00 -25 18 0 178.38 25.80 25 -7 0 185.98 27.90 7 -25 0 221.48 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82.19 28.30 -1 25 0 54.39 25.70 -24 -1 0 37.70 14.90 -1 25 0 22.20 15.30 25 0 0 -21.40 12.10 25 0 0 8.60 16.10 -25 25 0 -6.00 13.70 0 -25 0 0.90 19.20 25 -25 0 67.99 28.50 0 25 0 37.40 24.70 -25 0 0 26.90 14.90 0 25 0 13.40 13.50 26 -13 0 202.08 33.80 -26 13 0 191.18 25.60 -13 -13 0 209.38 24.90 13 13 0 188.58 29.60 26 -13 0 249.48 20.60 -13 26 0 221.38 24.00 13 -26 0 279.97 37.40 -14 26 0 41.40 15.10 -26 14 0 38.40 16.10 14 12 0 40.40 19.90 12 -26 0 92.39 25.80 26 -12 0 61.29 13.40 26 -12 0 -4.30 22.10 -12 -14 0 30.90 14.30 12 14 0 48.60 21.60 -26 12 0 37.80 15.90 26 -14 0 55.59 22.30 -12 26 0 45.70 15.40 26 -14 0 64.89 12.10 14 -26 0 96.19 26.60 -14 -12 0 50.29 14.50 -26 15 0 62.99 16.70 -15 26 0 55.89 15.30 11 -26 0 114.89 26.30 15 11 0 73.29 20.70 26 -11 0 13.30 22.10 -11 -15 0 77.79 16.90 26 -11 0 94.49 14.40 26 -15 0 86.49 14.90 11 15 0 84.59 22.40 -11 26 0 74.79 15.70 -15 -11 0 79.09 16.00 26 -15 0 85.39 23.00 -26 11 0 51.29 16.70 15 -26 0 99.19 27.50 26 -10 0 307.27 24.70 -26 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252.27 25.50 -27 9 0 221.38 26.00 18 -27 0 296.27 39.80 27 -18 0 275.37 35.00 -9 27 0 254.57 26.00 9 18 0 258.97 33.90 -19 27 0 1.20 13.70 19 8 0 10.70 18.30 8 -27 0 8.00 22.90 27 -8 0 18.00 14.90 -27 8 0 3.10 15.60 19 -27 0 53.29 28.30 -8 27 0 7.60 14.70 -19 -8 0 6.00 13.50 8 19 0 19.60 13.70 27 -19 0 27.60 24.50 27 -19 0 -7.10 8.90 8 19 0 5.90 21.40 7 -27 0 -1.10 22.50 27 -7 0 4.10 13.80 20 7 0 4.30 17.70 -20 27 0 4.20 14.00 20 -27 0 66.09 29.50 27 -20 0 47.80 24.70 -27 7 0 5.40 17.50 7 20 0 23.20 14.50 7 20 0 27.80 22.40 -20 -7 0 23.30 15.00 -7 27 0 11.70 14.80 -27 21 0 141.99 20.60 27 -6 0 184.58 24.40 -21 27 0 160.68 22.40 27 -6 0 203.88 23.50 6 -27 0 197.48 27.60 21 6 0 187.08 26.20 -6 27 0 184.18 24.20 21 -27 0 231.98 40.20 -27 6 0 183.18 23.80 6 21 0 202.98 32.60 6 21 0 187.58 22.60 -21 -6 0 202.98 22.50 27 -21 0 273.87 36.70 -27 22 0 161.28 20.90 22 5 0 111.29 20.00 27 -5 0 109.79 18.30 5 -27 0 117.19 25.20 -22 27 0 110.59 17.10 -5 27 0 136.99 23.00 5 22 0 129.19 21.10 -27 5 0 132.29 21.80 -22 -5 0 136.69 24.20 5 22 0 189.58 26.80 22 -27 0 165.58 31.70 27 -4 0 -32.40 19.00 27 -4 0 3.90 14.80 4 -27 0 -10.50 21.10 -27 23 0 -12.30 16.20 -27 23 0 -21.30 13.80 23 4 0 1.60 16.10 -23 27 0 -1.90 13.20 -23 -4 0 24.00 13.50 -4 27 0 -0.70 13.60 -4 27 0 64.59 26.20 4 23 0 13.50 13.50 27 -23 0 71.59 26.30 23 -27 0 42.70 27.60 4 23 0 28.10 22.90 -27 4 0 27.30 14.10 -27 24 0 58.59 16.40 3 -27 0 86.89 22.70 27 -3 0 72.89 16.80 -24 27 0 60.09 15.70 24 3 0 68.99 17.90 27 -3 0 64.39 19.70 -27 24 0 44.80 19.50 -24 -3 0 65.09 16.30 24 -27 0 109.39 29.50 -27 3 0 100.19 18.80 3 24 0 122.39 25.20 -3 27 0 59.79 15.30 3 24 0 64.69 15.30 27 -24 0 141.09 27.70 27 -2 0 46.20 18.40 -27 25 0 59.99 15.40 27 -2 0 76.29 17.20 25 2 0 68.99 16.80 -2 -25 0 98.49 20.30 -25 27 0 67.89 15.40 2 -27 0 62.99 21.60 -27 2 0 71.79 17.40 27 -25 0 124.39 27.80 -25 -2 0 99.09 19.40 -2 27 0 61.09 15.80 25 -27 0 127.59 29.10 2 25 0 60.19 14.90 -27 26 0 106.49 17.20 -26 27 0 93.89 17.00 -1 -26 0 118.99 21.40 1 -27 0 96.79 22.60 27 -1 0 109.89 17.90 26 1 0 111.19 18.60 -1 27 0 86.29 16.10 26 -27 0 174.68 30.60 27 -26 0 165.08 29.40 -27 1 0 75.09 18.70 1 26 0 100.59 21.10 -26 -1 0 82.99 18.50 0 -27 0 245.18 32.00 -27 27 0 281.77 26.80 27 0 0 309.87 27.90 -27 0 0 313.57 26.20 27 -27 0 374.06 40.40 0 27 0 275.17 27.00 -28 14 0 152.48 24.70 28 -14 0 146.09 25.60 28 -14 0 220.48 20.90 14 14 0 232.88 30.70 -14 -14 0 184.58 23.40 14 -28 0 218.88 34.80 -14 28 0 211.68 25.50 -13 -15 0 64.09 15.60 13 -28 0 60.99 26.30 28 -13 0 54.29 13.80 15 13 0 60.19 20.30 -28 15 0 24.10 20.50 -15 28 0 35.70 15.10 13 15 0 56.19 20.60 28 -15 0 13.20 21.70 15 -28 0 63.09 26.80 -13 28 0 55.29 15.60 -15 -13 0 38.10 15.50 -28 13 0 39.50 16.60 28 -15 0 70.99 13.30 -28 16 0 112.79 18.30 16 12 0 138.09 22.90 12 -28 0 169.28 28.30 -12 -16 0 98.29 18.00 -16 28 0 105.79 22.20 28 -12 0 135.79 20.30 28 -16 0 138.79 16.90 -12 28 0 116.59 22.20 16 -28 0 153.18 28.70 28 -16 0 101.69 24.30 -28 12 0 78.89 19.60 12 16 0 129.49 23.60 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15 0 296.97 31.70 29 -15 0 312.37 23.00 -14 29 0 268.67 27.60 29 -15 0 227.48 33.10 -29 14 0 232.38 28.70 -15 -14 0 303.77 25.90 15 -29 0 315.27 38.60 29 -13 0 241.78 28.70 -29 16 0 169.68 36.20 29 -13 0 238.78 22.00 16 13 0 247.88 28.50 13 -29 0 238.88 36.10 -16 29 0 234.18 23.90 -13 -16 0 184.28 27.20 -29 13 0 187.28 25.30 16 -29 0 287.67 38.00 29 -16 0 209.18 27.30 -13 29 0 216.38 25.40 29 -16 0 240.68 20.40 13 16 0 244.88 29.10 -16 -13 0 226.48 24.30 17 12 0 -1.50 18.10 -12 -17 0 -23.30 13.60 29 -12 0 -3.30 12.40 -17 29 0 8.10 13.50 12 -29 0 12.80 23.80 -17 -12 0 -2.40 14.50 -12 29 0 -5.90 14.20 29 -17 0 -4.30 21.00 12 17 0 -1.90 19.30 29 -17 0 -2.90 11.80 -29 12 0 -17.60 16.00 17 -29 0 18.30 26.50 11 -29 0 30.30 23.80 18 11 0 -2.50 17.40 29 -11 0 1.80 12.70 -29 18 0 -29.10 16.80 -18 29 0 -8.90 13.00 -11 29 0 -2.50 14.10 29 -18 0 -5.40 19.70 -18 -11 0 3.50 14.00 -29 11 0 -20.60 14.50 11 18 0 -0.60 19.00 29 -18 0 -8.70 9.30 18 -29 0 1.60 26.30 29 -10 0 131.39 19.70 -29 19 0 90.49 18.50 19 10 0 126.79 20.50 -19 29 0 114.99 20.60 10 -29 0 153.88 26.80 19 -29 0 144.99 30.20 29 -19 0 142.29 24.00 10 19 0 116.19 23.00 -19 -10 0 135.59 21.30 29 -19 0 103.39 14.00 -10 29 0 129.49 21.70 -29 10 0 89.49 21.60 29 -9 0 233.78 23.30 -29 20 0 169.78 26.10 -20 29 0 219.38 24.10 20 9 0 214.58 26.20 9 -29 0 219.38 34.10 -20 -9 0 205.28 25.30 20 -29 0 287.97 37.70 29 -20 0 195.28 31.90 -9 29 0 233.78 24.50 -29 9 0 165.58 28.00 9 20 0 246.28 29.20 8 -29 0 113.09 24.50 -21 29 0 87.09 15.60 29 -8 0 98.99 17.30 21 8 0 97.99 19.10 -29 8 0 94.49 17.10 29 -21 0 86.59 23.70 8 21 0 109.09 19.50 -8 29 0 102.69 21.10 -21 -8 0 109.59 20.90 8 21 0 104.89 23.00 21 -29 0 157.98 30.40 22 7 0 10.00 15.70 7 -29 0 4.20 21.60 29 -7 0 16.70 14.00 -22 29 0 3.50 13.10 -22 -7 0 11.00 14.40 7 22 0 36.70 21.10 29 -22 0 59.79 23.50 7 22 0 14.10 12.40 -29 7 0 20.40 15.00 -7 29 0 13.00 14.30 22 -29 0 40.80 27.60 6 -29 0 96.79 23.80 -29 23 0 70.89 19.00 23 6 0 111.79 19.00 29 -6 0 114.69 20.00 -29 23 0 137.89 23.90 -23 29 0 94.69 15.90 29 -23 0 125.69 25.10 6 23 0 73.09 16.90 -29 6 0 116.39 20.60 -23 -6 0 76.99 17.10 -6 29 0 81.89 16.60 -29 24 0 4.40 14.10 29 -5 0 20.80 14.50 24 5 0 8.70 15.70 5 -29 0 6.00 21.50 29 -5 0 -11.20 17.90 -24 29 0 15.80 13.60 24 -29 0 54.59 27.80 5 24 0 42.70 22.50 -24 -5 0 26.30 14.10 5 24 0 20.20 14.50 -29 5 0 20.40 15.80 -5 29 0 12.00 13.70 29 -24 0 55.39 24.10 29 -4 0 191.18 23.40 -25 29 0 199.48 23.60 -29 25 0 182.38 24.50 4 -29 0 223.28 27.40 25 4 0 174.58 25.30 -4 -25 0 174.78 31.10 4 25 0 174.48 23.70 -29 4 0 178.28 24.60 -4 29 0 190.88 24.50 25 -29 0 282.67 39.70 29 -25 0 267.37 35.70 4 25 0 249.08 32.20 -25 -4 0 142.29 23.90 -26 29 0 119.09 20.20 29 -3 0 110.79 18.20 26 3 0 106.09 18.70 29 -3 0 95.09 20.80 3 -29 0 100.79 24.40 -3 -26 0 127.19 23.30 -29 26 0 104.89 21.40 3 26 0 117.19 21.20 -26 -3 0 132.19 21.30 -3 29 0 86.19 18.40 -29 3 0 80.29 18.60 29 -26 0 136.79 27.90 26 -29 0 199.18 46.00 -2 -27 0 14.20 21.40 -27 29 0 42.00 15.40 27 2 0 37.70 17.00 29 -2 0 32.40 15.90 -29 27 0 26.00 15.30 2 -29 0 -6.00 22.20 -2 29 0 17.90 16.00 27 -29 0 95.39 32.80 -29 2 0 38.80 16.90 2 27 0 25.30 15.50 -27 -2 0 42.40 15.80 1 -29 0 -24.00 23.30 -29 28 0 26.60 15.50 -1 -28 0 -22.90 22.70 29 -1 0 28.10 16.60 -28 29 0 31.40 15.10 29 -28 0 86.09 27.80 28 -29 0 77.09 28.00 -29 1 0 30.10 17.00 -1 29 0 27.60 14.70 1 28 0 25.60 15.40 -28 -1 0 45.30 15.40 29 0 0 10.20 17.90 -29 29 0 -3.00 15.20 0 29 0 3.30 14.10 29 -29 0 33.00 26.70 15 -30 0 315.67 37.30 30 -15 0 281.37 31.40 -15 -15 0 227.88 24.30 15 15 0 230.58 27.70 -30 15 0 171.28 28.50 30 -15 0 263.87 22.00 -15 30 0 226.98 24.10 -16 30 0 98.29 20.60 30 -14 0 114.79 24.50 16 14 0 104.89 20.40 14 -30 0 133.19 27.20 -14 -16 0 86.39 16.20 30 -14 0 118.29 17.70 -30 16 0 106.29 18.60 16 -30 0 154.58 28.60 30 -16 0 112.69 17.10 14 16 0 102.49 20.70 30 -16 0 139.29 24.20 -16 -14 0 85.29 17.40 -30 14 0 106.99 17.50 -14 30 0 105.69 20.90 30 -13 0 117.99 24.70 30 -13 0 177.48 20.10 -17 30 0 149.88 21.60 17 13 0 151.28 26.50 13 -30 0 193.28 28.50 -30 17 0 112.69 20.90 13 17 0 188.68 27.90 30 -17 0 144.69 17.20 -17 -13 0 169.98 22.20 -13 30 0 148.79 22.00 30 -17 0 154.98 25.00 17 -30 0 211.18 36.60 30 -12 0 120.59 19.10 18 12 0 130.79 21.90 -12 -18 0 73.19 17.80 30 -12 0 75.69 23.70 12 -30 0 155.28 27.10 -30 18 0 132.79 20.00 -18 30 0 102.69 20.00 30 -18 0 91.89 14.90 30 -18 0 119.49 23.90 18 -30 0 152.68 29.50 -18 -12 0 123.99 20.20 -30 12 0 103.49 18.10 -12 30 0 106.19 21.10 12 18 0 118.29 21.70 11 -30 0 70.49 23.90 -30 19 0 4.20 16.10 30 -11 0 39.80 14.30 19 11 0 53.39 18.60 -19 30 0 31.10 13.50 11 19 0 47.50 20.10 30 -19 0 21.60 9.90 30 -19 0 15.00 20.40 -11 30 0 32.20 13.90 19 -30 0 62.79 27.60 -30 11 0 23.70 15.50 -19 -11 0 27.50 15.00 -20 30 0 6.60 13.10 30 -10 0 14.90 13.20 -30 20 0 -14.90 14.40 10 -30 0 15.80 22.60 20 10 0 1.00 16.20 20 -30 0 54.99 27.60 -10 30 0 8.20 13.90 30 -20 0 12.20 19.80 -30 10 0 -1.70 18.20 -20 -10 0 2.80 14.70 10 20 0 -0.10 19.50 9 -30 0 17.00 22.50 -30 21 0 -12.90 15.90 -21 30 0 12.60 13.50 30 -9 0 23.60 14.90 21 9 0 -6.00 15.90 9 21 0 8.50 20.10 30 -21 0 15.40 20.90 -30 9 0 -7.40 18.30 21 -30 0 48.10 28.20 -21 -9 0 16.90 14.00 -9 30 0 3.30 13.70 -22 30 0 11.30 13.20 22 8 0 5.50 16.20 8 -30 0 -3.60 21.30 30 -8 0 14.10 14.10 -30 22 0 -11.40 15.20 -30 8 0 -2.50 17.90 30 -22 0 -6.00 21.30 8 22 0 15.10 12.90 -8 30 0 10.50 14.30 22 -30 0 48.10 27.50 8 22 0 28.10 20.70 -22 -8 0 11.80 13.90 7 -30 0 89.39 24.50 30 -7 0 102.59 16.80 -23 30 0 94.39 15.70 -30 23 0 64.49 17.40 23 7 0 102.19 18.40 -30 7 0 62.09 19.30 7 23 0 60.99 16.30 30 -23 0 115.39 24.20 -7 30 0 71.49 16.40 7 23 0 135.19 24.40 -23 -7 0 70.39 17.70 23 -30 0 132.69 29.60 -30 24 0 95.19 17.90 30 -6 0 40.30 22.60 24 6 0 103.39 19.00 6 -30 0 107.19 25.20 -24 30 0 90.19 16.30 30 -6 0 104.59 17.10 6 24 0 154.38 25.40 -30 6 0 66.69 19.20 24 -30 0 193.38 33.00 30 -24 0 117.89 25.90 -6 30 0 87.09 16.60 -24 -6 0 120.69 20.90 6 24 0 105.29 17.70 5 -30 0 -18.90 21.90 25 5 0 3.90 18.50 30 -5 0 3.40 14.30 -30 25 0 -7.90 14.70 -25 30 0 1.00 13.50 -30 5 0 -5.10 18.10 30 -25 0 32.60 24.40 -25 -5 0 8.20 14.90 5 25 0 45.40 23.30 -26 30 0 12.60 13.70 -30 26 0 -1.60 15.30 4 -30 0 -28.90 22.00 30 -4 0 10.00 14.80 -4 30 0 -0.90 14.20 4 26 0 12.20 14.50 4 26 0 56.59 24.40 26 -30 0 41.40 28.60 -26 -4 0 11.90 15.90 -30 4 0 22.80 18.40 27 3 0 10.90 16.50 30 -3 0 2.60 15.20 3 -30 0 -15.40 22.50 -27 30 0 15.00 14.40 -30 27 0 3.70 14.80 -30 3 0 21.00 17.10 -27 -3 0 18.90 14.90 30 -27 0 51.19 25.20 3 27 0 4.70 14.70 27 -30 0 66.89 28.00 3 27 0 72.09 25.60 -3 30 0 14.10 14.60 2 -30 0 -34.50 22.80 -30 28 0 0.00 15.30 28 2 0 12.30 16.00 28 -30 0 31.40 27.20 -2 30 0 7.90 14.40 2 28 0 10.30 16.00 30 -28 0 31.50 25.70 2 28 0 66.39 26.30 1 -30 0 115.89 26.90 30 -1 0 148.09 24.40 29 1 0 129.39 23.40 29 -30 0 204.88 35.30 30 -29 0 156.28 29.20 1 29 0 128.49 23.50 -29 -1 0 128.89 20.90 -1 30 0 128.39 23.60 -30 30 0 137.29 25.80 30 0 0 115.99 20.00 0 -30 0 71.49 27.40 -30 0 0 93.49 21.20 30 -30 0 156.08 28.70 0 30 0 71.59 18.30 31 -15 0 -1.20 12.40 -16 31 0 -9.00 12.90 -15 -16 0 -2.80 13.30 31 -15 0 0.70 21.70 16 15 0 10.80 17.30 -31 16 0 -5.60 16.80 15 -31 0 23.90 25.10 16 -31 0 20.20 25.80 15 16 0 6.10 17.40 -15 31 0 -8.10 13.20 31 -16 0 -8.70 11.50 -31 15 0 -15.20 14.10 31 -16 0 9.50 21.10 -16 -15 0 -3.70 13.70 31 -14 0 97.49 24.00 -14 -17 0 110.99 22.20 14 -31 0 183.78 29.30 17 14 0 149.29 26.40 31 -14 0 137.29 18.40 -31 17 0 113.69 19.00 -17 31 0 127.19 21.00 31 -17 0 110.99 17.20 -14 31 0 106.69 21.70 -31 14 0 86.99 20.10 31 -17 0 142.59 24.90 -17 -14 0 77.69 17.20 17 -31 0 158.68 29.70 14 17 0 136.49 21.50 31 -13 0 262.47 24.30 -31 18 0 231.48 28.50 13 -31 0 294.97 37.70 18 13 0 257.67 29.20 -18 31 0 260.57 24.10 -13 -18 0 213.68 26.20 31 -13 0 203.48 28.50 31 -18 0 254.77 21.20 -13 31 0 248.98 26.00 31 -18 0 250.57 32.20 -18 -13 0 235.08 23.80 13 18 0 242.18 28.50 18 -31 0 284.57 38.60 19 12 0 238.48 27.10 -12 -19 0 187.48 26.70 31 -12 0 185.58 27.70 31 -12 0 255.77 22.60 12 -31 0 262.87 36.50 -31 19 0 193.18 27.30 -19 31 0 231.68 23.50 19 -31 0 297.57 39.20 -31 12 0 250.77 25.40 -19 -12 0 212.18 25.50 31 -19 0 256.27 32.70 12 19 0 268.87 30.10 -12 31 0 223.08 25.90 31 -19 0 238.08 19.00 20 11 0 40.00 18.30 11 -31 0 49.90 24.20 -20 31 0 22.80 13.30 -31 20 0 13.40 15.30 31 -11 0 29.00 14.00 -11 31 0 14.00 14.20 31 -20 0 33.20 21.50 -20 -11 0 24.00 15.20 11 20 0 32.90 19.30 20 -31 0 59.59 27.50 -31 11 0 0.80 15.80 -21 31 0 109.99 21.50 10 -31 0 131.09 26.40 21 10 0 121.99 20.80 31 -10 0 107.69 17.50 -31 21 0 75.19 18.90 21 -31 0 137.29 30.90 10 21 0 125.29 22.50 -10 31 0 115.29 22.80 31 -21 0 109.59 23.60 -31 10 0 86.69 21.20 -21 -10 0 114.99 20.70 31 -9 0 20.50 14.00 22 9 0 3.30 22.30 9 -31 0 17.40 23.50 -31 22 0 -4.00 15.00 -22 31 0 10.20 13.70 -22 -9 0 11.00 14.70 -31 9 0 2.70 18.30 9 22 0 20.10 19.90 -9 31 0 12.30 14.70 31 -22 0 19.20 21.20 22 -31 0 34.90 28.10 31 -8 0 120.39 20.80 8 -31 0 109.79 25.70 -31 23 0 81.89 18.70 -23 31 0 120.19 19.90 -23 -8 0 75.79 18.60 8 23 0 146.39 24.70 31 -23 0 101.69 24.40 -31 8 0 88.39 21.00 23 -31 0 163.18 44.40 -31 24 0 83.79 18.20 -24 31 0 110.69 20.90 24 7 0 87.59 19.20 31 -7 0 102.19 18.40 7 -31 0 128.59 26.50 -7 31 0 91.69 25.00 24 -31 0 106.59 34.30 -24 -7 0 107.59 21.90 -31 7 0 83.19 20.90 31 -24 0 85.99 24.50 7 24 0 95.99 17.70 -25 31 0 51.39 14.80 31 -6 0 68.99 16.90 6 -31 0 53.99 24.60 -31 25 0 54.29 17.10 25 6 0 70.89 18.00 -25 -6 0 50.19 17.60 25 -31 0 113.89 29.90 -6 31 0 43.20 16.10 6 25 0 48.40 14.60 -31 6 0 79.49 20.20 31 -5 0 42.80 16.30 26 5 0 59.69 17.60 5 -31 0 19.20 24.10 -26 31 0 48.00 15.60 -31 26 0 37.20 19.60 31 -26 0 61.99 24.90 -31 5 0 39.10 19.10 5 26 0 109.89 25.80 5 26 0 48.10 15.90 -5 31 0 37.00 16.50 26 -31 0 80.69 29.50 -31 27 0 36.10 15.80 31 -4 0 40.60 16.30 27 4 0 34.40 16.90 4 -31 0 40.20 25.30 -4 31 0 21.10 16.10 4 27 0 105.39 26.70 31 -27 0 58.99 25.20 4 27 0 38.70 15.70 27 -31 0 110.69 29.90 31 -3 0 97.39 19.90 28 3 0 90.39 18.50 -28 31 0 67.89 17.80 3 -31 0 54.19 26.00 -3 31 0 62.19 16.60 3 28 0 59.59 16.20 28 -31 0 142.19 31.00 31 -28 0 102.39 27.00 -31 29 0 215.58 27.90 -29 31 0 201.48 24.60 2 -31 0 172.18 29.90 29 2 0 187.48 25.90 31 -2 0 202.68 25.30 -2 31 0 181.88 25.30 -29 -2 0 164.98 25.80 -31 2 0 125.59 24.90 31 -29 0 266.47 37.00 2 29 0 155.58 27.20 29 -31 0 266.17 36.80 -16 32 0 67.59 15.80 -16 -16 0 82.49 16.90 32 -16 0 95.09 24.30 16 -32 0 139.39 29.10 -32 16 0 101.89 17.90 16 16 0 87.69 20.40 32 -16 0 83.59 15.10 -15 -17 0 33.80 16.00 -17 32 0 31.40 14.60 32 -15 0 31.00 22.70 32 -15 0 29.00 13.20 15 -32 0 56.09 27.30 -32 17 0 21.80 17.40 17 15 0 60.39 21.20 -15 32 0 24.80 14.30 -32 15 0 25.40 18.00 32 -17 0 28.20 12.60 15 17 0 24.10 18.40 32 -17 0 59.19 22.90 -17 -15 0 44.00 16.20 17 -32 0 54.69 27.70 32 -14 0 -38.50 20.90 14 -32 0 64.99 26.40 -14 -18 0 18.80 17.90 -18 32 0 22.50 13.80 -32 18 0 12.00 17.40 32 -14 0 25.60 13.40 32 -18 0 14.70 11.40 14 18 0 33.00 19.20 18 -32 0 45.70 27.50 -18 -14 0 11.30 14.60 32 -18 0 44.90 22.20 -14 32 0 19.10 14.40 -19 32 0 33.90 14.20 13 -32 0 35.90 25.60 -32 19 0 38.00 17.20 32 -13 0 -12.00 21.70 32 -13 0 37.60 14.30 32 -19 0 24.70 12.50 -19 -13 0 25.00 14.90 -13 32 0 31.90 15.10 13 19 0 39.80 19.50 19 -32 0 67.39 27.90 32 -19 0 63.59 22.90 -32 13 0 4.30 17.70 -20 32 0 23.20 13.70 20 12 0 31.70 25.10 12 -32 0 34.60 25.80 32 -12 0 19.80 14.00 32 -12 0 -31.20 20.60 -32 20 0 -5.40 17.70 -32 12 0 14.40 16.80 32 -20 0 48.00 23.00 12 20 0 33.20 19.10 20 -32 0 36.60 27.70 -20 -12 0 10.80 15.40 -32 21 0 42.70 17.90 21 11 0 48.90 18.20 32 -11 0 52.19 16.90 32 -11 0 -5.30 21.00 -21 32 0 27.80 14.10 11 -32 0 59.59 25.80 -32 11 0 42.40 16.20 32 -21 0 52.79 23.50 11 21 0 49.40 20.40 21 -32 0 70.19 38.60 -32 22 0 31.30 17.50 -22 32 0 35.10 14.80 10 -32 0 27.40 24.80 32 -10 0 32.30 15.10 22 10 0 22.30 17.10 32 -22 0 70.99 23.80 10 22 0 47.10 21.10 -10 32 0 34.10 15.40 -32 10 0 34.80 19.60 22 -32 0 57.89 43.60 23 9 0 9.80 16.90 -23 32 0 8.00 14.20 -32 23 0 -9.50 17.40 9 -32 0 3.30 24.20 32 -9 0 8.60 15.80 -9 32 0 6.90 15.00 9 23 0 52.99 21.90 -32 9 0 -5.00 18.30 23 -32 0 35.30 28.20 32 -23 0 -2.70 22.20 32 -8 0 7.80 14.70 -32 24 0 -4.90 15.90 8 -32 0 14.90 24.60 24 8 0 8.40 16.70 -24 32 0 0.20 20.60 8 24 0 13.60 15.20 -24 -8 0 13.40 17.10 24 -32 0 50.39 29.50 -8 32 0 -13.60 14.70 -32 8 0 9.80 18.70 8 24 0 33.10 22.30 32 -7 0 3.40 14.70 25 7 0 3.60 15.70 7 -32 0 -15.10 23.90 -32 25 0 -7.00 16.00 -32 7 0 -6.90 19.10 7 25 0 4.60 13.60 -25 -7 0 8.40 16.00 -7 32 0 3.40 14.80 25 -32 0 31.60 29.00 32 -25 0 -10.80 21.70 6 -32 0 46.80 25.70 32 -6 0 66.89 17.40 -32 26 0 52.09 23.00 26 6 0 58.89 18.20 -26 32 0 56.29 16.00 -6 32 0 57.79 16.80 32 -26 0 65.79 24.00 -26 -6 0 63.49 18.10 26 -32 0 91.99 29.70 6 26 0 122.49 26.10 6 26 0 68.49 16.90 5 -32 0 261.87 38.00 27 5 0 340.27 29.70 -27 32 0 352.26 28.40 32 -5 0 319.07 36.50 5 27 0 263.07 31.60 -5 32 0 314.37 30.00 27 -32 0 425.96 43.60 32 -27 0 334.57 37.30 -33 17 0 186.08 24.10 33 -16 0 177.18 27.90 33 -16 0 200.78 22.30 17 16 0 170.68 28.10 -16 -17 0 174.78 24.30 16 -33 0 242.48 37.80 17 -33 0 226.88 33.40 -17 -16 0 157.38 25.20 16 17 0 194.38 28.30 33 -17 0 188.98 32.00 -33 16 0 163.08 27.60 33 -17 0 198.68 19.50 -16 33 0 173.08 28.40 33 -15 0 18.00 13.40 -15 -18 0 18.00 16.10 33 -15 0 -25.70 22.00 -33 18 0 11.10 18.10 15 -33 0 46.70 26.50 18 15 0 31.40 18.60 -18 -15 0 19.80 15.40 -15 33 0 29.30 15.30 33 -18 0 47.60 23.30 33 -18 0 18.80 15.10 18 -33 0 26.70 27.70 -33 15 0 7.60 18.00 15 18 0 40.70 19.40 14 -33 0 29.50 26.30 33 -14 0 -14.20 22.00 19 14 0 39.60 18.20 -14 -19 0 25.20 16.50 -33 19 0 16.20 19.40 33 -14 0 36.60 14.80 33 -19 0 49.70 23.40 -33 14 0 9.20 17.40 -14 33 0 33.30 15.30 -19 -14 0 18.60 15.40 14 19 0 54.49 28.20 19 -33 0 44.40 34.60 33 -13 0 -15.00 21.90 -33 20 0 -5.00 16.90 -20 33 0 2.80 19.30 33 -13 0 -3.90 13.70 20 13 0 11.70 17.60 13 -33 0 24.50 26.00 -13 -20 0 -4.10 14.80 33 -20 0 25.90 23.20 -20 -13 0 1.90 15.20 20 -33 0 37.00 41.40 -33 13 0 -2.60 17.60 -13 33 0 2.70 14.00 33 -12 0 31.90 22.60 21 12 0 61.89 18.70 -12 -21 0 39.60 15.20 -21 33 0 53.49 19.20 33 -12 0 65.69 16.90 -33 21 0 48.80 18.00 12 -33 0 61.59 26.70 -12 33 0 43.90 15.90 33 -21 0 88.59 24.50 -33 12 0 49.10 19.30 -21 -12 0 64.39 17.30 21 -33 0 80.89 30.00 -11 -22 0 143.49 26.30 33 -11 0 97.69 25.00 -22 33 0 116.59 22.40 22 11 0 142.19 21.70 33 -11 0 167.88 22.50 -33 22 0 138.09 28.90 11 -33 0 153.18 29.30 22 -33 0 149.39 31.80 -22 -11 0 158.98 25.60 -11 33 0 130.09 25.30 -33 11 0 138.59 26.80 33 -22 0 194.08 33.60 -23 33 0 50.79 15.40 33 -10 0 47.10 16.10 -33 23 0 38.50 19.30 23 10 0 43.30 17.60 33 -10 0 39.70 23.10 10 -33 0 48.40 26.20 -33 10 0 47.90 20.60 -23 -10 0 52.39 17.50 23 -33 0 61.59 29.80 -10 33 0 41.00 15.90 24 9 0 1.60 16.70 9 -33 0 5.00 24.90 -24 33 0 12.40 14.70 33 -9 0 10.10 15.10 -33 24 0 1.50 16.50 -24 -9 0 7.00 16.00 -9 33 0 10.30 15.80 24 -33 0 26.50 29.20 33 -24 0 13.10 23.50 33 -8 0 88.19 17.70 -25 33 0 81.59 16.60 8 -33 0 89.89 27.90 25 8 0 73.59 18.80 25 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2.90 33.60 -7 0 5 22.90 30.20 -7 0 -5 14.80 14.50 7 -7 5 55.49 39.50 -7 0 -5 40.00 14.60 -7 8 -5 6.30 14.40 -8 7 5 7.80 30.80 -1 -7 -5 18.00 15.40 7 1 5 16.30 39.70 1 -8 5 -12.50 34.10 1 7 5 25.40 45.60 8 -7 -5 6.60 16.70 -8 1 5 16.70 34.50 7 -8 5 55.89 38.20 -7 -1 -5 15.90 14.20 -1 8 -5 15.00 12.60 7 2 5 -11.10 37.20 2 -9 5 -21.00 33.00 -7 9 -5 11.10 12.70 -9 7 5 4.50 30.70 9 -2 -5 -1.10 14.30 -2 -7 -5 15.30 15.50 9 -7 -5 5.50 15.40 2 7 5 18.20 38.70 7 -9 5 36.20 37.20 -2 9 -5 5.90 12.90 -7 -2 -5 12.60 13.10 -9 2 5 7.70 25.30 7 3 5 21.90 43.90 -10 7 5 -3.90 28.90 -3 -7 -5 23.50 14.50 -7 10 -5 20.60 13.10 -3 -7 -5 45.20 14.40 10 -3 -5 2.60 16.70 3 -10 5 5.20 34.60 3 7 5 2.20 39.00 7 -10 5 25.00 44.60 -7 -3 -5 18.80 14.20 10 -7 -5 14.80 18.10 -3 10 -5 12.60 12.80 -7 -3 -5 31.20 17.00 -10 3 5 12.00 24.00 -4 -7 -5 80.39 16.70 4 -11 5 46.00 36.00 7 4 5 69.79 51.99 -11 7 5 49.99 27.30 -7 11 -5 57.39 16.20 11 -4 -5 100.79 21.60 -4 -7 -5 74.59 16.60 -4 11 -5 59.89 16.20 -7 -4 -5 73.09 15.60 11 -7 -5 61.19 17.50 4 7 5 64.99 38.80 -11 4 5 75.69 25.20 7 -11 5 60.79 46.40 -5 -7 -5 9.10 15.80 -7 12 -5 14.10 14.70 7 5 5 14.30 39.50 12 -5 -5 14.20 17.30 -12 7 5 -1.00 26.60 5 -12 5 7.90 36.60 -5 12 -5 23.10 16.10 -12 5 5 13.40 23.50 -7 -5 -5 24.40 14.40 7 -12 5 35.00 43.60 12 -7 -5 11.80 18.10 -7 -5 -5 7.00 15.50 5 7 5 43.30 40.40 -6 -7 -5 47.80 16.10 -6 -7 -5 61.39 17.10 13 -6 -5 32.70 18.30 -13 7 5 43.30 24.60 7 6 5 53.69 39.30 6 7 5 15.20 39.20 13 -7 -5 40.70 17.50 -7 -6 -5 64.89 14.40 7 -13 5 46.10 43.30 -7 -6 -5 40.30 15.80 -13 6 5 31.00 23.70 7 -14 5 10.20 44.20 -14 7 5 5.40 22.80 14 -7 -5 -3.00 18.10 -7 -7 -5 23.40 16.50 7 7 5 23.90 36.30 -4 -4 5 48.90 26.90 4 4 -5 32.60 15.10 4 -8 -5 32.70 17.30 8 -4 5 91.89 41.80 -8 4 -5 45.30 16.20 -4 8 5 47.90 36.60 3 -8 -5 104.69 19.10 -5 8 5 102.49 35.80 -3 -5 5 105.29 29.30 8 -3 5 132.29 42.00 -8 3 -5 87.49 17.40 -3 8 5 116.79 40.40 8 -5 5 149.19 42.70 -5 -3 5 105.89 27.50 3 5 -5 99.59 15.80 6 2 -5 111.49 17.70 8 -2 5 121.89 39.50 -8 6 -5 138.99 20.20 2 -8 -5 144.19 22.40 -2 -6 5 129.59 31.40 -6 8 5 102.49 38.70 -8 2 -5 140.69 19.60 8 -6 5 145.79 41.30 -6 -2 5 151.78 27.80 -2 8 5 106.19 42.20 2 6 -5 112.49 16.60 8 -1 5 84.19 39.40 1 -8 -5 42.30 17.00 7 1 -5 50.69 14.60 -7 8 5 70.29 35.00 -1 -7 5 45.60 30.20 -1 8 5 40.60 42.10 1 7 -5 53.39 13.50 -8 1 -5 59.79 15.90 8 -7 5 96.29 40.30 8 0 -5 47.70 14.90 8 0 5 55.99 42.90 -8 8 5 51.49 34.10 0 -8 5 35.60 29.90 0 -8 -5 44.20 15.90 -8 0 5 59.39 34.40 0 8 -5 54.39 13.80 0 8 5 54.89 42.20 -8 0 -5 58.19 16.70 -8 0 -5 66.39 17.60 8 -8 -5 59.49 18.50 8 -8 5 63.89 41.20 -1 -8 -5 53.99 16.60 -9 8 5 34.10 31.10 1 -9 5 20.90 30.80 8 1 5 57.79 41.90 9 -1 -5 25.60 16.40 -8 9 -5 29.20 15.30 -1 9 -5 35.40 13.40 8 -9 5 77.39 48.90 9 -8 -5 27.40 16.30 -9 1 5 43.30 24.30 -8 -1 -5 47.00 15.20 1 8 5 49.40 38.60 -2 -8 -5 20.30 15.10 -10 8 5 22.90 30.30 10 -2 -5 14.10 18.10 2 -10 5 -31.10 36.60 -8 10 -5 9.20 14.20 8 2 5 3.00 38.70 -8 -2 -5 6.70 15.50 10 -8 -5 14.40 18.00 -10 2 5 18.00 23.00 -2 10 -5 14.50 14.80 -8 -2 -5 19.60 14.60 2 8 5 12.40 38.50 -11 8 5 28.80 29.60 -3 -8 -5 14.30 14.20 3 -11 5 9.10 35.60 11 -3 -5 25.40 17.70 -3 -8 -5 27.80 16.10 -11 3 5 25.80 23.10 -8 -3 -5 37.10 15.60 -8 -3 -5 40.80 16.70 8 -11 5 52.39 44.80 11 -8 -5 24.00 16.50 3 8 5 16.40 40.20 -4 -8 -5 46.70 15.90 8 4 5 44.40 40.70 4 -12 5 16.40 35.20 -4 -8 -5 59.89 15.50 -12 8 5 61.39 26.90 -8 12 -5 48.70 16.80 12 -4 -5 52.39 17.00 8 -12 5 45.60 43.80 -8 -4 -5 62.89 16.50 -8 -4 -5 55.69 15.20 12 -8 -5 46.90 18.60 4 8 5 52.49 38.00 -12 4 5 61.79 23.20 8 5 5 98.29 41.00 -5 -8 -5 125.09 17.00 -5 -8 -5 159.18 25.80 -13 8 5 123.59 28.50 13 -5 -5 155.28 24.90 5 -13 5 97.59 43.50 5 8 5 131.59 40.50 8 -13 5 180.78 46.10 -13 5 5 115.19 25.00 -8 -5 -5 137.29 19.80 -8 -5 -5 129.49 24.10 13 -8 -5 124.39 22.00 -6 -8 -5 42.00 15.10 14 -6 -5 43.50 17.30 -14 8 5 27.60 25.00 -6 -8 -5 48.30 14.60 8 6 5 28.10 36.50 -14 6 5 45.80 22.50 -8 -6 -5 37.80 17.50 -6 14 -5 41.60 18.20 14 -8 -5 42.40 19.20 -8 -6 -5 45.00 13.60 6 8 5 8.70 36.70 -5 9 5 34.00 35.20 9 -4 5 72.19 39.00 5 4 -5 18.30 14.40 4 -9 -5 29.80 16.50 -9 5 -5 42.00 13.30 -4 -5 5 41.60 26.40 4 5 -5 20.50 14.90 -5 -4 5 31.40 25.00 9 -5 5 48.50 39.00 -4 9 5 40.70 38.50 5 -9 -5 22.10 18.20 -9 4 -5 27.20 14.70 -3 -6 5 28.90 27.30 -6 9 5 11.00 35.10 9 -3 5 63.09 40.10 3 -9 -5 18.70 15.90 6 3 -5 24.40 15.60 -9 3 -5 30.20 15.00 -6 -3 5 19.80 23.90 9 -6 5 53.59 40.20 -3 9 5 33.70 39.70 7 2 -5 28.20 16.10 9 -2 5 62.39 41.80 2 -9 -5 17.20 16.10 -7 9 5 25.30 34.60 -2 -7 5 14.70 27.20 9 -7 5 74.09 49.60 -9 2 -5 34.30 15.30 -2 9 5 18.30 38.40 9 -1 5 33.60 41.10 -8 9 5 32.20 33.90 1 -9 -5 20.30 16.30 8 1 -5 27.70 18.70 -1 -8 5 25.80 29.40 1 8 -5 29.10 15.50 -1 9 5 5.90 38.00 -9 1 -5 32.90 14.50 -9 1 -5 25.30 16.30 8 -9 -5 20.20 17.20 -8 -1 5 43.90 32.50 9 -8 5 80.79 50.39 0 -9 -5 19.90 14.60 0 -9 5 -2.20 29.70 9 0 5 11.90 39.50 -9 9 5 43.30 33.30 9 0 -5 20.70 17.20 -9 0 -5 28.90 15.00 -9 0 5 22.30 22.80 0 9 5 12.10 38.00 9 -9 -5 12.70 16.30 0 9 -5 18.30 16.30 -1 -9 -5 41.20 16.40 9 1 5 64.29 39.50 10 -1 -5 37.70 16.80 -10 9 5 7.90 30.90 1 -10 5 36.70 30.50 -10 1 5 57.09 23.50 1 9 5 58.09 39.40 -9 -1 -5 53.19 15.90 10 -9 -5 47.00 18.60 -9 -1 -5 7.50 16.30 11 -2 -5 51.29 16.30 -2 -9 -5 82.89 17.00 2 -11 5 77.79 32.90 -11 9 5 75.69 31.90 -11 2 5 75.29 23.40 11 -9 -5 60.09 19.40 -9 -2 -5 93.59 18.30 2 9 5 61.09 39.30 -9 -2 -5 71.99 16.00 9 -11 5 84.29 47.80 3 -12 5 17.50 37.20 -3 -9 -5 29.80 16.00 -12 9 5 13.50 28.80 12 -3 -5 22.40 18.70 9 3 5 6.70 42.30 -3 -9 -5 19.70 15.00 3 9 5 9.20 38.70 -9 -3 -5 29.40 16.10 12 -9 -5 -2.20 17.20 -12 3 5 25.50 22.10 -9 -3 -5 24.20 15.00 9 -12 5 32.90 45.60 -3 12 -5 15.60 16.10 -3 12 -5 65.29 27.20 -4 -9 -5 41.80 15.30 9 4 5 16.20 38.30 -13 9 5 31.40 26.10 4 -13 5 19.90 35.70 13 -4 -5 26.60 18.20 -4 -9 -5 39.70 15.00 9 -13 5 71.79 44.70 -9 -4 -5 51.99 14.10 13 -9 -5 38.30 17.20 -9 -4 -5 29.10 16.30 4 9 5 22.00 39.80 -13 4 5 48.30 22.20 -5 -9 -5 23.00 14.90 5 -14 5 30.00 44.00 9 5 5 22.20 37.20 -14 9 5 21.60 26.00 -5 14 -5 79.69 23.60 5 9 5 22.80 35.50 -9 -5 -5 31.10 17.10 -14 5 5 15.00 21.60 -5 -5 5 93.49 25.10 5 -10 -5 76.29 19.20 -5 10 5 104.39 38.70 5 5 -5 108.29 20.70 -4 -6 5 125.39 28.10 -6 10 5 127.39 37.90 10 -4 5 143.79 43.00 6 4 -5 157.98 23.30 4 -10 -5 136.19 21.20 -4 10 5 140.39 41.90 -6 -4 5 135.09 26.00 -10 4 -5 148.09 20.30 -7 10 5 224.18 40.70 -3 -7 5 212.38 37.00 7 3 -5 225.78 25.00 3 -10 -5 200.58 24.80 10 -3 5 249.78 43.60 -10 3 -5 240.28 22.50 -3 10 5 266.67 45.20 10 -2 5 86.89 40.60 -8 10 5 71.49 35.50 -2 -8 5 71.49 28.10 2 -10 -5 51.89 15.50 -10 2 -5 65.99 15.90 -10 2 -5 43.40 17.50 8 -10 -5 52.39 18.70 -8 -2 5 61.89 32.60 2 8 -5 61.79 17.40 -2 10 5 52.79 38.90 9 1 -5 160.78 20.00 -1 -9 5 190.68 33.10 -9 10 5 197.18 38.10 10 -1 5 228.28 42.80 1 -10 -5 175.38 21.30 -10 9 -5 153.58 21.50 -10 1 -5 189.38 21.30 -9 -1 5 182.58 30.30 -1 10 5 167.48 42.00 1 9 -5 189.18 22.40 9 -10 -5 171.28 22.70 0 -10 -5 78.09 18.40 10 0 5 94.69 41.10 0 -10 5 84.39 31.40 10 0 -5 100.59 17.80 -10 10 -5 84.79 18.50 -10 10 5 80.19 33.10 0 10 -5 73.69 17.10 0 10 5 84.59 39.80 -10 0 5 82.59 22.90 -10 0 -5 102.99 17.80 10 -10 -5 103.29 20.60 -1 -10 -5 93.09 17.50 1 -11 5 93.49 32.50 11 -1 -5 94.99 20.60 10 1 5 54.99 40.70 -11 10 5 57.19 33.00 -10 11 -5 109.69 20.30 -10 -1 -5 129.89 24.60 -10 -1 -5 94.99 17.70 -11 1 5 79.99 22.50 1 10 5 56.99 39.10 -1 11 -5 115.79 24.60 11 -10 -5 63.19 19.80 -2 -10 -5 57.79 17.30 12 -2 -5 74.19 19.80 2 -12 5 49.40 31.50 -12 10 5 43.90 31.00 12 -10 -5 59.99 18.80 -12 2 5 83.99 22.80 -10 -2 -5 76.69 16.00 -2 12 -5 123.29 27.60 2 10 5 54.09 38.10 -2 12 -5 67.49 14.50 10 3 5 36.80 39.00 -3 -10 -5 30.60 15.70 -13 10 5 33.30 29.20 3 -13 5 39.10 36.80 13 -3 -5 23.60 16.20 -3 -10 -5 34.90 16.20 -3 13 -5 85.09 22.90 -10 -3 -5 37.90 16.70 -10 -3 -5 36.10 15.50 -13 3 5 40.00 21.30 13 -10 -5 29.80 18.80 3 10 5 36.10 41.80 -3 13 -5 33.40 13.90 6 5 -5 58.09 14.30 -6 11 5 48.30 35.80 -5 -6 5 45.80 24.00 11 -5 5 87.19 42.60 5 6 -5 52.79 14.50 -11 5 -5 41.40 15.40 -5 11 5 48.00 39.80 11 -6 5 113.09 43.00 -6 -5 5 39.90 23.90 -4 -7 5 34.80 24.70 11 -4 5 52.99 43.20 -7 11 5 76.49 37.90 -4 11 5 26.80 40.70 -11 4 -5 54.79 16.00 4 7 -5 53.49 13.90 7 -11 -5 34.00 19.10 11 -7 5 90.49 40.90 -8 11 5 57.49 35.50 8 3 -5 35.20 16.30 -3 -8 5 29.40 26.10 3 -11 -5 26.70 17.30 11 -3 5 83.99 43.10 -8 -3 5 38.40 22.30 -11 3 -5 36.40 15.80 -11 3 -5 25.00 17.10 11 -8 5 57.19 40.10 -3 11 5 35.70 40.60 8 -11 -5 34.60 16.70 3 8 -5 45.40 13.40 -11 9 -5 35.30 15.60 9 2 -5 35.30 17.50 -9 11 5 31.20 35.40 2 -11 -5 36.80 17.20 -2 -9 5 42.90 26.40 11 -9 5 88.69 40.00 -11 2 -5 38.40 14.80 -9 -2 5 31.30 21.50 2 9 -5 31.80 13.30 -2 11 5 28.20 39.20 9 -11 -5 28.40 17.70 11 -1 5 55.89 40.20 -11 10 -5 49.00 14.10 -10 11 5 23.40 34.90 -1 -10 5 27.60 27.70 10 1 -5 52.29 19.90 1 -11 -5 47.70 17.50 -11 1 -5 55.09 16.10 -1 11 5 47.10 40.00 10 -11 -5 52.89 18.60 -10 -1 5 49.99 21.70 11 -10 5 99.89 39.30 1 10 -5 40.70 13.70 0 -11 -5 27.90 15.80 11 0 -5 6.10 16.50 -11 11 -5 22.30 13.40 11 0 5 14.40 39.00 0 -11 5 17.50 28.30 -11 11 5 -6.00 32.40 0 11 -5 18.20 13.00 -11 0 -5 16.70 16.80 -11 0 5 31.30 20.80 11 -11 -5 18.80 16.10 -11 0 -5 34.50 14.60 0 11 5 36.00 39.80 1 -12 5 37.60 30.90 12 -1 -5 31.00 15.60 -1 -11 -5 42.00 16.20 -12 11 5 41.90 32.40 -12 1 5 33.10 20.50 -11 -1 -5 67.89 17.60 12 -11 -5 38.20 18.40 -1 12 -5 44.80 13.80 -11 -1 -5 55.59 16.00 1 11 5 37.10 40.20 -11 13 -5 52.89 16.40 -13 11 5 31.00 30.00 -2 -11 -5 54.89 15.50 2 -13 5 49.10 31.40 11 2 5 34.40 38.60 13 -2 -5 54.29 20.40 -2 -11 -5 34.10 15.30 -11 -2 -5 43.60 17.90 13 -11 -5 23.70 18.50 -11 -2 -5 62.59 14.80 2 11 5 44.50 40.70 -13 2 5 28.50 21.20 -2 13 -5 79.89 21.60 -2 13 -5 26.30 15.10 12 -6 5 135.99 39.40 -6 12 5 127.99 40.50 -6 -6 5 117.49 32.30 -12 6 -5 149.79 20.90 -7 12 5 298.17 48.70 -5 -7 5 249.58 34.60 12 -5 5 377.46 49.00 -5 12 5 275.67 48.00 12 -7 5 343.97 49.00 -12 5 -5 281.87 25.60 7 -12 -5 280.77 25.90 8 4 -5 118.79 20.00 12 -4 5 121.29 38.50 4 -12 -5 90.49 19.70 -8 12 5 84.39 36.70 -4 -8 5 87.29 26.00 -12 4 -5 89.49 20.30 8 -12 -5 64.89 19.00 -4 12 5 74.79 41.50 12 -8 5 168.48 40.80 -8 -4 5 92.29 23.10 -12 4 -5 116.59 18.90 9 3 -5 39.40 17.10 -3 -9 5 50.89 25.50 3 -12 -5 71.39 17.60 -9 12 5 50.59 35.30 12 -3 5 75.89 38.00 12 -9 5 87.99 38.70 -12 3 -5 67.09 17.10 9 -12 -5 31.40 17.70 -9 -3 5 50.59 21.20 -3 12 5 52.99 39.10 -2 -10 5 53.19 26.50 10 2 -5 44.20 15.10 2 -12 -5 56.59 17.10 -10 12 5 60.39 36.80 12 -2 5 94.19 38.90 10 -12 -5 69.69 19.50 -10 -2 5 55.99 21.50 -2 12 5 22.30 38.40 -12 2 -5 49.80 15.50 11 1 -5 93.39 19.40 -1 -11 5 116.29 31.60 1 -12 -5 115.29 19.70 -12 11 -5 100.79 18.50 -11 12 5 83.79 36.60 12 -1 5 162.08 42.40 -11 -1 5 117.49 22.70 -12 1 -5 161.98 19.40 11 -12 -5 117.69 19.60 -12 1 -5 139.49 26.60 -1 12 5 100.19 39.60 0 -12 -5 42.80 16.20 -12 12 -5 43.00 13.50 -12 12 5 10.60 31.50 0 -12 5 9.30 30.30 12 0 -5 43.10 20.50 12 -12 -5 51.89 17.90 -12 0 -5 53.09 15.20 0 12 5 37.40 38.80 -12 0 -5 58.69 18.20 -12 0 5 24.50 20.50 13 -6 5 101.79 40.30 7 6 -5 56.59 14.70 -7 13 5 26.50 39.50 -6 13 5 23.70 40.90 7 -13 -5 45.90 18.90 -13 6 -5 62.79 21.30 6 7 -5 51.59 14.20 -7 -6 5 48.50 25.20 13 -7 5 91.69 38.00 -13 6 -5 39.70 16.10 -8 13 5 24.20 36.10 -5 -8 5 23.90 23.20 8 5 -5 34.30 13.50 13 -5 5 69.59 39.70 8 -13 -5 24.00 17.80 -8 -5 5 27.00 21.10 13 -8 5 71.79 37.10 -5 13 5 15.50 40.00 5 8 -5 27.30 13.00 -13 5 -5 -6.30 16.10 -13 5 -5 38.00 15.60 -9 13 5 49.60 36.70 4 -13 -5 54.49 19.60 9 4 -5 49.10 16.70 -4 -9 5 48.10 24.50 13 -4 5 63.59 39.80 -13 9 -5 46.10 15.70 -9 -4 5 40.10 21.70 -13 4 -5 50.09 15.90 4 9 -5 54.69 14.00 13 -9 5 73.29 37.90 9 -13 -5 50.89 18.20 -4 13 5 67.09 41.20 -13 10 -5 40.30 16.10 10 3 -5 73.79 21.30 3 -13 -5 48.70 17.80 -10 13 5 51.19 34.70 -3 -10 5 63.59 25.40 13 -3 5 80.79 41.20 -13 3 -5 72.59 15.40 3 10 -5 57.19 14.10 -10 -3 5 48.10 21.50 -3 13 5 43.10 38.10 10 -13 -5 58.89 18.90 13 -2 5 50.59 40.40 -11 13 5 -22.10 34.50 2 -13 -5 16.10 16.70 11 2 -5 2.50 16.90 -2 -11 5 12.30 25.60 -13 2 -5 5.00 17.60 -11 -2 5 30.20 20.60 2 11 -5 8.70 12.80 -2 13 5 6.60 37.90 11 -13 -5 12.70 16.00 -13 2 -5 12.00 14.40 -7 -7 5 100.99 24.50 7 -14 -5 117.79 20.10 -7 14 5 76.29 43.40 -14 7 -5 155.98 31.00 -14 8 -5 79.49 14.90 6 -14 -5 60.69 19.00 -8 14 5 59.19 38.50 14 -8 5 130.49 38.10 -6 14 5 64.39 40.50 -8 -6 5 73.59 22.40 8 -14 -5 76.59 18.60 -14 6 -5 30.90 18.80 -9 14 5 193.28 39.60 14 -5 5 226.58 45.70 14 -9 5 313.47 45.00 -14 5 -5 168.88 29.70 -9 -5 5 215.58 30.10 -5 14 5 211.78 43.70 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 24410 loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'y, x, z' 'x-y, -y, z' '-x, -x+y, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.7352(10) 0.8226(11) 0.385(6) 0.002(7) Uiso 1 1 d D . . . . C2 C 0.7767(10) 0.8177(10) 0.452(6) 0.002(7) Uiso 1 1 d D . . . . C3 C 0.7814(15) 0.7814(15) 0.353(10) 0.015(13) Uiso 1 2 d DS . P . . H3 H 0.761387 0.761388 0.227071 0.018 Uiso 1 2 calc R U P . . C4 C 0.8044(12) 0.8438(13) 0.659(6) 0.019(9) Uiso 1 1 d D . . . . H4 H 0.797703 0.865592 0.730387 0.022 Uiso 1 1 calc R U . . . C5 C 0.841(2) 0.841(2) 0.768(13) 0.045(19) Uiso 1 2 d DS . P A . C6 C 0.873(3) 0.9124(17) 0.962(17) 0.02(2) Uiso 0.5 1 d D . P A -1 H6A H 0.873921 0.918856 1.144229 0.029 Uiso 0.5 1 calc R U P A -1 H6B H 0.846683 0.913166 0.888204 0.029 Uiso 0.5 1 calc R U P A -1 C7 C 0.918(5) 0.951(5) 0.84(4) 0.15(8) Uiso 0.5 1 d D . P A -1 H7A H 0.920169 0.980798 0.867322 0.218 Uiso 0.5 1 calc R U P A -1 H7B H 0.944678 0.951223 0.913348 0.218 Uiso 0.5 1 calc R U P A -1 H7C H 0.917405 0.945525 0.656990 0.218 Uiso 0.5 1 calc R U P A -1 C8 C 0.7155(13) 0.9136(12) 0.105(8) 0.018(9) Uiso 1 1 d D U . . . C9 C 0.7522(10) 0.9593(9) -0.007(5) 0.001(7) Uiso 1 1 d D U . . . C10 C 0.7581(14) 1.000000 0.096(9) 0.006(10) Uiso 1 2 d DS U P . . H10 H 0.739327 1.000000 0.229154 0.007 Uiso 1 2 calc R U P . . C11 C 0.7786(11) 0.9600(12) -0.215(6) 0.019(9) Uiso 1 1 d D U . . . H11 H 0.771067 0.931621 -0.291436 0.022 Uiso 1 1 calc R U . . . C12 C 0.8152(18) 1.000000 -0.315(11) 0.027(15) Uiso 1 2 d DS . P B . C13 C 0.840(2) 0.9573(17) -0.569(13) 0.007(16) Uiso 0.5 1 d D . P B -1 H13A H 0.808658 0.934566 -0.621691 0.009 Uiso 0.5 1 calc R U P B -1 H13B H 0.848439 0.944539 -0.423054 0.009 Uiso 0.5 1 calc R U P B -1 C14 C 0.874(6) 0.967(7) -0.79(3) 0.14(8) Uiso 0.5 1 d D . P B -1 H14A H 0.873088 0.937990 -0.839683 0.203 Uiso 0.5 1 calc R U P B -1 H14B H 0.865871 0.978949 -0.935415 0.203 Uiso 0.5 1 calc R U P B -1 H14C H 0.905545 0.988896 -0.737310 0.203 Uiso 0.5 1 calc R U P B -1 C15 C 0.6173(11) 0.7580(11) 0.578(6) 0.003(8) Uiso 1 1 d D . . . . C16 C 0.5711(16) 0.6741(13) 0.572(9) 0.072(19) Uiso 1 1 d D . . . . H16 H 0.588027 0.673260 0.431191 0.087 Uiso 1 1 calc R U . . . C17 C 0.5348(16) 0.6351(15) 0.689(7) 0.065(18) Uiso 1 1 d D . . . . C18 C 0.5091(17) 0.6348(16) 0.899(8) 0.067(18) Uiso 1 1 d D . . . . H18 H 0.485861 0.606851 0.968889 0.081 Uiso 1 1 calc R U . . . C19 C 0.5190(17) 0.6774(14) 1.002(10) 0.055(16) Uiso 1 1 d D . . . . C20 C 0.5544(14) 0.7182(14) 0.901(7) 0.036(12) Uiso 1 1 d D . . . . H20 H 0.561932 0.747150 0.969495 0.043 Uiso 1 1 calc R U . . . C21 C 0.5784(14) 0.7146(13) 0.694(7) 0.049(14) Uiso 1 1 d D . . . . C22 C 0.472(2) 1.0585(18) 0.679(13) 0.061(9) Uiso 1 1 d D U . . . C23 C 0.496(2) 0.7200(17) 1.292(10) 0.052(15) Uiso 1 1 d D . . . . H23A H 0.490685 0.736851 1.155402 0.063 Uiso 1 1 calc R U . . . H23B H 0.526742 0.740153 1.363383 0.063 Uiso 1 1 calc R U . . . C24 C 0.459(2) 0.707(3) 1.502(12) 0.07(2) Uiso 1 1 d D . . . . H24A H 0.460269 0.734281 1.570084 0.108 Uiso 1 1 calc R U . . . H24B H 0.428214 0.686774 1.429422 0.108 Uiso 1 1 calc R U . . . H24C H 0.464165 0.690066 1.636797 0.108 Uiso 1 1 calc R U . . . C25 C 0.5184(9) 0.9461(12) 0.382(6) 0.050(6) Uiso 1 1 d D U . . . C26 C 0.5516(19) 0.8932(17) 0.312(11) 0.076(15) Uiso 1 1 d D U . . . H26 H 0.565858 0.906344 0.468151 0.091 Uiso 1 1 calc R U . . . C27 C 0.5607(15) 0.8586(16) 0.221(8) 0.058(15) Uiso 1 1 d D U . . . C28 C 0.5320(15) 0.8367(16) 0.009(7) 0.08(2) Uiso 1 1 d D . . . . H28 H 0.534990 0.812704 -0.064703 0.101 Uiso 1 1 calc R U . . . C29 C 0.4998(18) 0.8461(17) -0.105(10) 0.072(14) Uiso 1 1 d D U . . . C30 C 0.4999(19) 0.8848(17) -0.002(8) 0.072(11) Uiso 1 1 d D U . . . H30 H 0.480838 0.894062 -0.084106 0.086 Uiso 1 1 calc R U . . . C31 C 0.5249(17) 0.9116(16) 0.210(8) 0.058(7) Uiso 1 1 d D U . . . C32 C 0.6007(17) 0.8512(18) 0.297(7) 0.049(15) Uiso 1 1 d D . . . . C33 C 0.432(2) 0.820(3) -0.358(14) 0.10(2) Uiso 1 1 d D U . . . H33A H 0.439659 0.852214 -0.379243 0.121 Uiso 1 1 calc R U . . . H33B H 0.410086 0.805890 -0.218726 0.121 Uiso 1 1 calc R U . . . C34 C 0.413(3) 0.792(3) -0.609(14) 0.09(2) Uiso 1 1 d D U . . . H34A H 0.384999 0.791822 -0.657673 0.134 Uiso 1 1 calc R U . . . H34B H 0.436067 0.806635 -0.743271 0.134 Uiso 1 1 calc R U . . . H34C H 0.406737 0.760692 -0.584071 0.134 Uiso 1 1 calc R U . . . O1 O 0.7146(11) 0.8070(11) 0.155(6) 0.030(8) Uiso 1 1 d . . . . . O2 O 0.7276(9) 0.8493(9) 0.507(5) 0.015(6) Uiso 1 1 d . . . . . O3 O 0.8665(13) 0.8665(13) 0.931(9) 0.034(11) Uiso 1 2 d DS . P . . O4 O 0.6974(8) 0.8774(8) -0.036(5) 0.004(5) Uiso 1 1 d . . . . . O5 O 0.7072(10) 0.9146(10) 0.335(6) 0.020(7) Uiso 1 1 d . . . . . O6 O 0.8421(12) 1.000000 -0.497(8) 0.023(10) Uiso 1 2 d DS . P . . O7 O 0.6232(9) 0.7591(10) 0.351(6) 0.020(6) Uiso 1 1 d . . . . . O8 O 0.6361(10) 0.7965(10) 0.725(6) 0.022(7) Uiso 1 1 d . . . . . O9 O 0.4645(15) 1.0494(15) 0.434(8) 0.057(9) Uiso 1 1 d . U . . . O10 O 0.4966(16) 1.0505(15) 0.778(9) 0.067(9) Uiso 1 1 d . U . . . O11 O 0.4933(16) 0.6784(15) 1.191(8) 0.067(12) Uiso 1 1 d D . . . . O12 O 0.5017(12) 0.9591(12) 0.205(7) 0.049(5) Uiso 1 1 d D U . . . O13 O 0.5278(11) 0.9542(12) 0.612(6) 0.035(5) Uiso 1 1 d D U . . . O14 O 0.6079(10) 0.8263(10) 0.147(6) 0.022(7) Uiso 1 1 d D . . . . O15 O 0.6196(9) 0.8668(10) 0.509(5) 0.020(6) Uiso 1 1 d D . . . . O16 O 0.4738(18) 0.817(2) -0.312(10) 0.096(16) Uiso 1 1 d D U . . . CU1 Cu 0.6581(2) 0.8128(2) 0.126(2) 0.0389(19) Uani 1 1 d . . . . . CU2 Cu 0.67547(19) 0.85935(19) 0.554(2) 0.0258(15) Uani 1 1 d . . . . . CU3 Cu 0.5133(2) 1.000000 0.706(2) 0.0133(16) Uiso 1 2 d S U P . . CU4 Cu 0.4750(2) 1.000000 0.277(2) 0.0182(17) Uiso 1 2 d S U P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 CU1 0.017(3) 0.016(3) 0.084(5) -0.017(3) -0.002(3) 0.008(3) CU2 0.022(3) 0.016(3) 0.040(3) -0.011(2) -0.003(3) 0.010(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0040 0.0020 'Calculated using XDISP in WinGX (Farrugia, 1999)' H H 0.0000 0.0000 'Calculated using XDISP in WinGX (Farrugia, 1999)' O O 0.0132 0.0074 'Calculated using XDISP in WinGX (Farrugia, 1999)' Cu Cu 0.2913 1.4803 'Calculated using XDISP in WinGX (Farrugia, 1999)' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 O2 C1 O1 120(3) . . O2 C1 C2 119(3) . . O1 C1 C2 119(3) . . C3 C2 C4 120(3) . . C3 C2 C1 121(2) . . C4 C2 C1 118(3) . . C2 C3 C2 116(4) 4 . C2 C3 H3 122.0 4 . C2 C3 H3 122.0 . . C5 C4 C2 127(4) . . C5 C4 H4 116.7 . . C2 C4 H4 116.7 . . O3 C5 C4 125(3) . 4 O3 C5 C4 125(3) . . C4 C5 C4 110(5) 4 . O3 C6 C7 114(9) . . O3 C6 H6A 108.7 . . C7 C6 H6A 108.7 . . O3 C6 H6B 108.7 . . C7 C6 H6B 108.7 . . H6A C6 H6B 107.6 . . C6 C7 H7A 109.5 . . C6 C7 H7B 109.5 . . H7A C7 H7B 109.5 . . C6 C7 H7C 109.5 . . H7A C7 H7C 109.5 . . H7B C7 H7C 109.5 . . O5 C8 O4 126(3) . . O5 C8 C9 115(3) . . O4 C8 C9 119(3) . . C10 C9 C11 121(3) . . C10 C9 C8 119(3) . . C11 C9 C8 121(3) . . C9 C10 C9 117(4) 5_675 . C9 C10 H10 121.7 5_675 . C9 C10 H10 121.7 . . C12 C11 C9 124(4) . . C12 C11 H11 118.1 . . C9 C11 H11 118.1 . . O6 C12 C11 123(3) . 5_675 O6 C12 C11 123(2) . . C11 C12 C11 113(5) 5_675 . O6 C13 C14 109(9) . . O6 C13 H13A 109.8 . . C14 C13 H13A 109.8 . . O6 C13 H13B 109.8 . . C14 C13 H13B 109.8 . . H13A C13 H13B 108.2 . . C13 C14 H14A 109.5 . . C13 C14 H14B 109.5 . . H14A C14 H14B 109.5 . . C13 C14 H14C 109.5 . . H14A C14 H14C 109.5 . . H14B C14 H14C 109.5 . . O7 C15 O8 123(3) . . O7 C15 C21 119(3) . . O8 C15 C21 117(3) . . C21 C16 C17 110(5) . . C21 C16 H16 124.9 . . C17 C16 H16 124.9 . . C18 C17 C16 127(4) . . C18 C17 C22 105(4) . 6_655 C16 C17 C22 125(4) . 6_655 C17 C18 C19 118(4) . . C17 C18 H18 121.1 . . C19 C18 H18 121.1 . . O11 C19 C20 120(4) . . O11 C19 C18 119(4) . . C20 C19 C18 120(5) . . C19 C20 C21 117(4) . . C19 C20 H20 121.3 . . C21 C20 H20 121.3 . . C20 C21 C16 128(4) . . C20 C21 C15 119(3) . . C16 C21 C15 113(3) . . O10 C22 O9 119(5) . . O10 C22 C17 132(6) . 6_665 O9 C22 C17 98(4) . 6_665 O11 C23 C24 109(5) . . O11 C23 H23A 109.9 . . C24 C23 H23A 109.9 . . O11 C23 H23B 109.9 . . C24 C23 H23B 109.9 . . H23A C23 H23B 108.3 . . C23 C24 H24A 109.5 . . C23 C24 H24B 109.5 . . H24A C24 H24B 109.5 . . C23 C24 H24C 109.5 . . H24A C24 H24C 109.5 . . H24B C24 H24C 109.5 . . O13 C25 O12 138(4) . . O13 C25 C31 128(4) . . O12 C25 C31 94(3) . . O13 C25 CU3 45(2) . . O12 C25 CU3 93(3) . . C31 C25 CU3 173(3) . . C31 C26 C27 131(5) . . C31 C26 H26 114.3 . . C27 C26 H26 114.3 . . C28 C27 C26 109(4) . . C28 C27 C32 123(4) . . C26 C27 C32 127(4) . . C29 C28 C27 129(5) . . C29 C28 H28 115.7 . . C27 C28 H28 115.7 . . C28 C29 C30 113(6) . . C28 C29 O16 117(5) . . C30 C29 O16 129(5) . . C29 C30 C31 128(5) . . C29 C30 H30 115.9 . . C31 C30 H30 115.9 . . C30 C31 C26 109(4) . . C30 C31 C25 132(4) . . C26 C31 C25 117(4) . . O14 C32 O15 128(4) . . O14 C32 C27 114(3) . . O15 C32 C27 118(3) . . O16 C33 C34 103(6) . . O16 C33 H33A 111.2 . . C34 C33 H33A 111.2 . . O16 C33 H33B 111.2 . . C34 C33 H33B 111.2 . . H33A C33 H33B 109.1 . . C33 C34 H34A 109.5 . . C33 C34 H34B 109.5 . . H34A C34 H34B 109.5 . . C33 C34 H34C 109.5 . . H34A C34 H34C 109.5 . . H34B C34 H34C 109.5 . . C1 O1 CU1 111(2) . . C1 O2 CU2 136(2) . . C5 O3 C6 121(4) . . C8 O4 CU1 120(2) . . C8 O4 CU2 138(2) . 1_554 CU1 O4 CU2 99.4(10) . 1_554 C8 O5 CU2 124(2) . . C12 O6 C13 120(3) . . C15 O7 CU1 129(2) . . C15 O8 CU2 119(2) . . C15 O8 CU1 136(2) . 1_556 CU2 O8 CU1 101.7(12) . 1_556 C22 O9 CU4 120(3) . . C22 O10 CU3 130(4) . . C19 O11 C23 125(4) . . C25 O12 CU4 121(3) . . C25 O13 CU3 107(3) . . C32 O14 CU1 131(3) . . C32 O15 CU2 111(2) . . C29 O16 C33 111(5) . . O14 CU1 O7 89.5(12) . . O14 CU1 O1 169.9(13) . . O7 CU1 O1 91.3(12) . . O14 CU1 O4 87.3(11) . . O7 CU1 O4 167.4(11) . . O1 CU1 O4 89.8(11) . . O14 CU1 O8 83.7(11) . 1_554 O7 CU1 O8 112.0(11) . 1_554 O1 CU1 O8 105.3(12) . 1_554 O4 CU1 O8 79.8(9) . 1_554 O14 CU1 CU2 77.1(8) . . O7 CU1 CU2 83.1(8) . . O1 CU1 CU2 93.0(9) . . O4 CU1 CU2 84.2(7) . . O8 CU1 CU2 155.5(8) 1_554 . O2 CU2 O5 88.8(12) . . O2 CU2 O15 165.7(11) . . O5 CU2 O15 85.1(12) . . O2 CU2 O8 92.8(11) . . O5 CU2 O8 170.0(12) . . O15 CU2 O8 91.1(12) . . O2 CU2 O4 88.2(10) . 1_556 O5 CU2 O4 110.8(10) . 1_556 O15 CU2 O4 106.0(10) . 1_556 O8 CU2 O4 79.1(9) . 1_556 O2 CU2 CU1 75.0(8) . . O5 CU2 CU1 84.8(9) . . O15 CU2 CU1 91.6(8) . . O8 CU2 CU1 86.0(9) . . O4 CU2 CU1 157.0(6) 1_556 . O2 CU2 O12 151.2(8) . 5_676 O5 CU2 O12 79.8(9) . 5_676 O15 CU2 O12 39.5(8) . 5_676 O8 CU2 O12 103.0(9) . 5_676 O4 CU2 O12 71.7(6) 1_556 5_676 CU1 CU2 O12 129.4(3) . 5_676 O13 CU3 O13 89(2) . 5_675 O13 CU3 O10 90.0(16) . 5_675 O13 CU3 O10 175.4(16) 5_675 5_675 O13 CU3 O10 175.4(16) . . O13 CU3 O10 90.0(16) 5_675 . O10 CU3 O10 90(2) 5_675 . O13 CU3 C25 88.7(14) . 5_675 O13 CU3 C25 28.0(9) 5_675 5_675 O10 CU3 C25 147.5(15) 5_675 5_675 O10 CU3 C25 88.5(13) . 5_675 O13 CU3 C25 28.0(9) . . O13 CU3 C25 88.7(13) 5_675 . O10 CU3 C25 88.5(13) 5_675 . O10 CU3 C25 147.5(15) . . C25 CU3 C25 75.5(12) 5_675 . O13 CU3 CU4 95.7(10) . . O13 CU3 CU4 95.7(10) 5_675 . O10 CU3 CU4 79.9(13) 5_675 . O10 CU3 CU4 79.9(13) . . C25 CU3 CU4 67.9(8) 5_675 . C25 CU3 CU4 68.0(8) . . O13 CU3 O12 83.2(12) . 1_556 O13 CU3 O12 117.1(12) 5_675 1_556 O10 CU3 O12 67.3(15) 5_675 1_556 O10 CU3 O12 101.2(15) . 1_556 C25 CU3 O12 144.5(13) 5_675 1_556 C25 CU3 O12 108.3(11) . 1_556 CU4 CU3 O12 147.1(8) . 1_556 O12 CU4 O12 72(2) . 5_675 O12 CU4 O9 96.7(16) . 5_675 O12 CU4 O9 161.4(16) 5_675 5_675 O12 CU4 O9 161.4(16) . . O12 CU4 O9 96.7(16) 5_675 . O9 CU4 O9 90(2) 5_675 . O12 CU4 CU3 77.0(10) . . O12 CU4 CU3 77.0(10) 5_675 . O9 CU4 CU3 86.0(12) 5_675 . O9 CU4 CU3 86.0(12) . . O12 CU4 O10 65.3(13) . 5_674 O12 CU4 O10 98.9(14) 5_675 5_674 O9 CU4 O10 89.5(15) 5_675 5_674 O9 CU4 O10 132.5(15) . 5_674 CU3 CU4 O10 141.2(9) . 5_674 O12 CU4 O10 98.9(14) . 1_554 O12 CU4 O10 65.3(13) 5_675 1_554 O9 CU4 O10 132.5(15) 5_675 1_554 O9 CU4 O10 89.5(15) . 1_554 CU3 CU4 O10 141.2(9) . 1_554 O10 CU4 O10 58.1(17) 5_674 1_554 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 C1 O2 1.21(4) . C1 O1 1.35(4) . C1 C2 1.50(3) . C2 C3 1.38(3) . C2 C4 1.40(3) . C3 C2 1.38(3) 4 C3 H3 0.9300 . C4 C5 1.37(3) . C4 H4 0.9300 . C5 O3 1.21(7) . C5 C4 1.37(3) 4 C6 O3 1.43(4) . C6 C7 1.53(6) . C6 H6A 0.9700 . C6 H6B 0.9700 . C7 H7A 0.9600 . C7 H7B 0.9600 . C7 H7C 0.9600 . C8 O5 1.23(5) . C8 O4 1.27(5) . C8 C9 1.50(3) . C9 C10 1.37(2) . C9 C11 1.38(3) . C10 C9 1.37(3) 5_675 C10 H10 0.9300 . C11 C12 1.37(3) . C11 H11 0.9300 . C12 O6 1.30(6) . C12 C11 1.37(3) 5_675 C13 O6 1.43(4) . C13 C14 1.54(5) . C13 H13A 0.9700 . C13 H13B 0.9700 . C14 H14A 0.9600 . C14 H14B 0.9600 . C14 H14C 0.9600 . C15 O7 1.20(4) . C15 O8 1.34(5) . C15 C21 1.49(3) . C16 C21 1.39(2) . C16 C17 1.39(2) . C16 H16 0.9300 . C17 C18 1.38(2) . C17 C22 1.51(4) 6_655 C18 C19 1.38(3) . C18 H18 0.9300 . C19 O11 1.31(6) . C19 C20 1.37(3) . C20 C21 1.38(2) . C20 H20 0.9300 . C22 O10 1.10(6) . C22 O9 1.30(7) . C22 C17 1.51(4) 6_665 C23 O11 1.43(4) . C23 C24 1.54(5) . C23 H23A 0.9700 . C23 H23B 0.9700 . C24 H24A 0.9600 . C24 H24B 0.9600 . C24 H24C 0.9600 . C25 O13 1.23(3) . C25 O12 1.25(3) . C25 C31 1.55(3) . C25 CU3 2.52(4) . C26 C31 1.40(2) . C26 C27 1.40(2) . C26 H26 0.9300 . C27 C28 1.39(2) . C27 C32 1.51(3) . C28 C29 1.38(3) . C28 H28 0.9300 . C29 C30 1.39(3) . C29 O16 1.41(8) . C30 C31 1.39(2) . C30 H30 0.9300 . C32 O14 1.24(3) . C32 O15 1.24(3) . C33 O16 1.43(4) . C33 C34 1.54(5) . C33 H33A 0.9700 . C33 H33B 0.9700 . C34 H34A 0.9600 . C34 H34B 0.9600 . C34 H34C 0.9600 . O1 CU1 1.97(3) . O2 CU2 1.93(3) . O4 CU1 2.05(2) . O4 CU2 2.24(2) 1_554 O5 CU2 1.95(3) . O7 CU1 1.95(3) . O8 CU2 2.02(3) . O8 CU1 2.19(3) 1_556 O9 CU4 2.00(4) . O10 CU3 2.04(5) . O12 CU4 1.98(4) . O13 CU3 1.87(3) . O14 CU1 1.92(3) . O15 CU2 1.99(3) . CU1 O8 2.19(3) 1_554 CU1 CU2 2.600(8) . CU2 O4 2.24(2) 1_556 CU2 O12 9.65(4) 5_676 CU3 O13 1.87(3) 5_675 CU3 O10 2.04(5) 5_675 CU3 C25 2.52(4) 5_675 CU3 CU4 2.566(10) . CU3 O12 2.87(3) 1_556 CU4 O12 1.98(4) 5_675 CU4 O9 2.00(4) 5_675 CU4 O10 2.98(4) 5_674 CU4 O10 2.98(4) 1_554