#------------------------------------------------------------------------------ #$Date: 2019-10-28 02:43:27 +0200 (Mon, 28 Oct 2019) $ #$Revision: 219596 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/24/1552492.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1552492 loop_ _publ_author_name 'Tshitenge, Dieudonn\'e Tshitenge' 'Bruhn, Torsten' 'Feineis, Doris' 'Schmidt, David' 'Mudogo, Virima' 'Kaiser, Marcel' 'Brun, Reto' 'W\"urthner, Frank' 'Awale, Suresh' 'Bringmann, Gerhard' _publ_section_title ; Ealamines A-H, a Series of Naphthylisoquinolines with the Rare 7,8'-Coupling Site, from the Congolese Liana Ancistrocladus ealaensis, Targeting Pancreatic Cancer Cells. ; _journal_name_full 'Journal of natural products' _journal_paper_doi 10.1021/acs.jnatprod.9b00755 _journal_year 2019 _chemical_formula_moiety '2 (C25 H30 N O4), 2 (C2 F3 O2), C3 H6 O' _chemical_formula_sum 'C57 H66 F6 N2 O13' _chemical_formula_weight 1101.11 _space_group_crystal_system triclinic _space_group_IT_number 1 _space_group_name_Hall 'P 1' _space_group_name_H-M_alt 'P 1' _symmetry_space_group_name_Hall 'P 1' _symmetry_space_group_name_H-M 'P 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 68.987(6) _cell_angle_beta 73.430(7) _cell_angle_gamma 77.232(7) _cell_formula_units_Z 1 _cell_length_a 8.9167(7) _cell_length_b 11.8688(12) _cell_length_c 14.7500(15) _cell_measurement_reflns_used 9408 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 74.55 _cell_measurement_theta_min 3.30 _cell_volume 1384.3(2) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type Bruker-Kappa-D8Quest_Photon100 _diffrn_measurement_method omega_and_phi_scan _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0186 _diffrn_reflns_av_unetI/netI 0.0132 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 49932 _diffrn_reflns_point_group_measured_fraction_full 0.966 _diffrn_reflns_point_group_measured_fraction_max 0.947 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 74.538 _diffrn_reflns_theta_min 3.295 _diffrn_source Cu/K(alpha)_ImuS_Microsource _exptl_absorpt_coefficient_mu 0.900 _exptl_absorpt_correction_T_max 0.7538 _exptl_absorpt_correction_T_min 0.6956 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details Bruker-SADABS _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.321 _exptl_crystal_description block _exptl_crystal_F_000 580 _exptl_crystal_size_max 0.463 _exptl_crystal_size_mid 0.424 _exptl_crystal_size_min 0.285 _refine_diff_density_max 0.251 _refine_diff_density_min -0.233 _refine_diff_density_rms 0.038 _refine_ls_abs_structure_details ; Flack x determined using 5011 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.053(13) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.051 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 725 _refine_ls_number_reflns 10743 _refine_ls_number_restraints 3 _refine_ls_restrained_S_all 1.051 _refine_ls_R_factor_all 0.0278 _refine_ls_R_factor_gt 0.0277 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0451P)^2^+0.2806P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0744 _refine_ls_wR_factor_ref 0.0745 _reflns_Friedel_coverage 0.906 _reflns_Friedel_fraction_full 0.933 _reflns_Friedel_fraction_max 0.900 _reflns_number_gt 10697 _reflns_number_total 10743 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file np9b00755_si_002.cif _cod_data_source_block ealamineA _cod_database_code 1552492 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; 392_A71P6_fertig.res created by SHELXL-2014/7 TITL 392_A71P6_fertig_a.res in P1 CELL 1.54178 8.91666 11.86881 14.74998 68.9872 73.4304 77.2322 ZERR 1 0.00070 0.00123 0.00150 0.0056 0.0066 0.0068 LATT -1 SFAC C H N O F UNIT 57 66 2 13 6 TEMP -173 L.S. 10 PLAN 20 TEMP -173.15 BOND $H LIST 4 fmap -2 acta MORE -1 CONF WGHT 0.045100 0.280600 FVAR 0.68994 F21 5 0.190158 0.202730 0.434408 11.00000 0.02155 0.04223 = 0.03632 -0.01493 -0.00063 -0.00626 F22 5 0.074146 0.071026 0.564318 11.00000 0.03552 0.02551 = 0.03408 -0.00581 -0.00867 0.00672 F23 5 -0.000852 0.127072 0.426173 11.00000 0.03617 0.03959 = 0.03654 -0.02555 -0.00583 -0.00663 F31 5 0.411995 0.817172 0.555455 11.00000 0.03817 0.04582 = 0.09401 -0.04622 -0.00588 -0.01113 F32 5 0.242459 0.866821 0.465705 11.00000 0.10194 0.03368 = 0.07903 -0.01558 -0.03750 0.01529 F33 5 0.173500 0.784884 0.622144 11.00000 0.04447 0.06837 = 0.07851 -0.05541 0.01886 -0.01311 O1 4 0.956274 0.889359 1.126817 11.00000 0.02207 0.03084 = 0.01939 -0.01126 -0.00639 -0.00287 O2 4 0.671409 0.850091 1.166416 11.00000 0.03138 0.04851 = 0.02085 -0.01847 0.00516 -0.02076 O3 4 0.800426 0.589685 0.840823 11.00000 0.02978 0.01906 = 0.01980 -0.00179 -0.00842 -0.00475 O4 4 0.745206 1.024112 0.716019 11.00000 0.02861 0.01733 = 0.01907 -0.00802 -0.00431 -0.00162 H4O 2 0.764761 1.080678 0.663439 11.00000 0.03359 O5 4 1.053674 0.200621 -0.165653 11.00000 0.02022 0.03345 = 0.01425 -0.00889 -0.00332 -0.00535 O6 4 1.313250 0.169645 -0.113069 11.00000 0.01457 0.04032 = 0.02001 -0.01414 -0.00048 -0.00372 O7 4 0.734238 0.408629 0.188815 11.00000 0.02384 0.01945 = 0.01988 -0.00255 -0.00171 -0.00464 O8 4 0.708785 -0.022660 0.282295 11.00000 0.03037 0.02087 = 0.01774 -0.00865 -0.00307 -0.00290 H8O 2 0.754501 -0.015688 0.221834 11.00000 0.03274 O11 4 0.293608 0.619066 0.113057 11.00000 0.05109 0.03577 = 0.06910 -0.01617 -0.03808 -0.00019 O21 4 -0.018477 0.363609 0.500021 11.00000 0.04949 0.02654 = 0.04728 -0.01948 0.00857 -0.01440 O22 4 -0.206054 0.239561 0.560000 11.00000 0.02243 0.02290 = 0.02925 -0.00728 -0.00705 0.00146 O31 4 0.469794 0.616514 0.507624 11.00000 0.01715 0.02814 = 0.04058 -0.01879 -0.00674 -0.00009 O32 4 0.213148 0.607800 0.535858 11.00000 0.02008 0.03961 = 0.07480 -0.03075 -0.00934 -0.00337 N1 3 0.912636 0.574592 0.548704 11.00000 0.01901 0.01832 = 0.02393 -0.01032 -0.00406 -0.00278 AFIX 23 H1A 2 0.913686 0.502152 0.540204 11.00000 -1.20000 H1B 2 1.014675 0.587488 0.535447 11.00000 -1.20000 AFIX 0 N2 3 0.527969 0.393186 0.482860 11.00000 0.01856 0.01873 = 0.02019 -0.00809 -0.00398 -0.00011 AFIX 23 H2A 2 0.496862 0.464717 0.496764 11.00000 -1.20000 H2B 2 0.620210 0.358941 0.502394 11.00000 -1.20000 AFIX 0 C1 1 0.871175 0.848871 0.910518 11.00000 0.02106 0.01515 = 0.01847 -0.00538 -0.00608 -0.00083 C2 1 1.018300 0.869934 0.841494 11.00000 0.02155 0.02196 = 0.01703 -0.00764 -0.00432 -0.00046 AFIX 43 H2 2 1.032305 0.865511 0.776493 11.00000 -1.20000 AFIX 0 C3 1 1.140110 0.896365 0.866080 11.00000 0.02111 0.02081 = 0.02091 -0.00704 -0.00476 -0.00070 C4 1 1.119667 0.900684 0.963719 11.00000 0.01961 0.02270 = 0.02304 -0.00752 -0.00727 -0.00263 AFIX 43 H4 2 1.205307 0.915918 0.982033 11.00000 -1.20000 AFIX 0 C5 1 0.978945 0.883352 1.032355 11.00000 0.02478 0.01713 = 0.01851 -0.00703 -0.00755 -0.00031 C6 1 0.847149 0.857431 1.008385 11.00000 0.02159 0.01659 = 0.01657 -0.00531 -0.00397 -0.00240 C7 1 0.696035 0.836040 1.075137 11.00000 0.02674 0.02144 = 0.01687 -0.00765 -0.00175 -0.00644 C8 1 0.582528 0.802193 1.047231 11.00000 0.02309 0.02421 = 0.02019 -0.00770 -0.00008 -0.00707 AFIX 43 H8 2 0.484306 0.785881 1.092831 11.00000 -1.20000 AFIX 0 C9 1 0.610903 0.791547 0.951503 11.00000 0.02303 0.02162 = 0.02229 -0.00635 -0.00728 -0.00506 AFIX 43 H9 2 0.531844 0.766352 0.934172 11.00000 -1.20000 AFIX 0 C10 1 0.749196 0.816520 0.882925 11.00000 0.02312 0.01615 = 0.01674 -0.00458 -0.00623 -0.00164 C11 1 0.771675 0.809583 0.780525 11.00000 0.01718 0.02161 = 0.01724 -0.00706 -0.00432 -0.00344 C12 1 0.795019 0.698177 0.762748 11.00000 0.01859 0.01759 = 0.01858 -0.00393 -0.00673 -0.00260 C13 1 0.815470 0.690374 0.667522 11.00000 0.01688 0.01725 = 0.02137 -0.00733 -0.00577 -0.00185 C14 1 0.815102 0.797554 0.586754 11.00000 0.01678 0.01944 = 0.01868 -0.00768 -0.00597 -0.00133 C15 1 0.790339 0.909340 0.603188 11.00000 0.01800 0.01626 = 0.01911 -0.00443 -0.00591 -0.00060 AFIX 43 H15 2 0.788172 0.982382 0.548506 11.00000 -1.20000 AFIX 0 C16 1 0.768791 0.915553 0.698275 11.00000 0.01707 0.01703 = 0.02245 -0.00753 -0.00559 -0.00040 C17 1 0.837451 0.565658 0.655509 11.00000 0.02248 0.01780 = 0.01908 -0.00585 -0.00702 -0.00284 AFIX 13 H17 2 0.911598 0.510081 0.697283 11.00000 -1.20000 AFIX 0 C18 1 0.831274 0.673983 0.474876 11.00000 0.02248 0.02164 = 0.02070 -0.00890 -0.00682 -0.00210 AFIX 13 H18 2 0.716106 0.666274 0.494238 11.00000 -1.20000 AFIX 0 C19 1 0.852472 0.794384 0.480846 11.00000 0.02440 0.01832 = 0.01829 -0.00667 -0.00587 -0.00032 AFIX 23 H19A 2 0.962934 0.809900 0.448689 11.00000 -1.20000 H19B 2 0.782928 0.860625 0.443103 11.00000 -1.20000 AFIX 0 C20 1 1.293688 0.923409 0.790845 11.00000 0.02229 0.04108 = 0.02305 -0.01036 -0.00324 -0.00692 AFIX 137 H20A 2 1.319507 1.000955 0.787817 11.00000 -1.50000 H20B 2 1.283015 0.928744 0.725065 11.00000 -1.50000 H20C 2 1.378177 0.858072 0.810845 11.00000 -1.50000 AFIX 0 C21 1 1.093322 0.891728 1.158192 11.00000 0.02442 0.02786 = 0.02251 -0.00932 -0.01011 -0.00188 AFIX 137 H21A 2 1.062577 0.892389 1.227326 11.00000 -1.50000 H21B 2 1.141687 0.965059 1.115088 11.00000 -1.50000 H21C 2 1.169383 0.819354 1.153611 11.00000 -1.50000 AFIX 0 C22 1 0.520642 0.830144 1.232185 11.00000 0.05326 0.11126 = 0.03280 -0.04418 0.02097 -0.05667 AFIX 137 H22A 2 0.517399 0.843222 1.294691 11.00000 -1.50000 H22B 2 0.502796 0.746395 1.246110 11.00000 -1.50000 H22C 2 0.438195 0.887117 1.200918 11.00000 -1.50000 AFIX 0 C23 1 0.954032 0.551429 0.863193 11.00000 0.03709 0.02374 = 0.03162 -0.00437 -0.01940 0.00190 AFIX 137 H23A 2 0.956522 0.470071 0.912714 11.00000 -1.50000 H23B 2 0.976434 0.608996 0.889913 11.00000 -1.50000 H23C 2 1.033856 0.549139 0.802204 11.00000 -1.50000 AFIX 0 C24 1 0.683180 0.510072 0.689499 11.00000 0.02640 0.02419 = 0.02486 -0.00648 -0.00500 -0.00896 AFIX 137 H24A 2 0.643242 0.494471 0.761463 11.00000 -1.50000 H24B 2 0.702819 0.433345 0.674528 11.00000 -1.50000 H24C 2 0.604845 0.566862 0.654238 11.00000 -1.50000 AFIX 0 C25 1 0.900009 0.660664 0.371514 11.00000 0.04320 0.02572 = 0.02388 -0.01284 -0.00585 -0.00415 AFIX 137 H25A 2 0.851151 0.727948 0.322598 11.00000 -1.50000 H25B 2 0.878811 0.583107 0.371476 11.00000 -1.50000 H25C 2 1.014270 0.662371 0.353994 11.00000 -1.50000 AFIX 0 C31 1 0.977570 0.205041 0.091878 11.00000 0.01679 0.01839 = 0.01691 -0.00538 -0.00465 -0.00119 C32 1 1.057362 0.222036 0.155719 11.00000 0.01935 0.02819 = 0.01757 -0.01001 -0.00380 -0.00246 AFIX 43 H32 2 0.999762 0.227768 0.219259 11.00000 -1.20000 AFIX 0 C33 1 1.215688 0.230318 0.127455 11.00000 0.02199 0.03083 = 0.02299 -0.00982 -0.00770 -0.00388 C34 1 1.301937 0.215308 0.035128 11.00000 0.01605 0.03423 = 0.02415 -0.01000 -0.00388 -0.00403 AFIX 43 H34 2 1.412464 0.218446 0.016329 11.00000 -1.20000 AFIX 0 C35 1 1.230338 0.196281 -0.028292 11.00000 0.01807 0.02671 = 0.01765 -0.00701 -0.00184 -0.00429 C36 1 1.061972 0.198371 -0.004517 11.00000 0.01697 0.01933 = 0.01689 -0.00585 -0.00403 -0.00233 C37 1 0.975059 0.190803 -0.069843 11.00000 0.01961 0.01935 = 0.01497 -0.00544 -0.00374 -0.00082 C38 1 0.818182 0.175317 -0.035137 11.00000 0.01882 0.02835 = 0.01957 -0.00961 -0.00782 -0.00118 AFIX 43 H38 2 0.762157 0.166472 -0.077635 11.00000 -1.20000 AFIX 0 C39 1 0.740170 0.172493 0.062869 11.00000 0.01346 0.02864 = 0.02179 -0.00858 -0.00474 -0.00144 AFIX 43 H39 2 0.633550 0.156843 0.086666 11.00000 -1.20000 AFIX 0 C40 1 0.813448 0.191655 0.125034 11.00000 0.01663 0.01851 = 0.01640 -0.00589 -0.00320 -0.00041 C41 1 0.722585 0.194186 0.226539 11.00000 0.01131 0.02289 = 0.01655 -0.00673 -0.00423 0.00017 C42 1 0.673485 0.086655 0.299516 11.00000 0.01495 0.02187 = 0.01894 -0.00805 -0.00628 -0.00076 C43 1 0.589010 0.085994 0.394674 11.00000 0.01684 0.01867 = 0.01932 -0.00444 -0.00543 -0.00275 AFIX 43 H43 2 0.555637 0.012341 0.442404 11.00000 -1.20000 AFIX 0 C44 1 0.552809 0.191933 0.420780 11.00000 0.01244 0.02199 = 0.01796 -0.00667 -0.00312 -0.00109 C45 1 0.599701 0.300571 0.349510 11.00000 0.01532 0.01968 = 0.01991 -0.00761 -0.00500 0.00029 C46 1 0.683158 0.300196 0.253505 11.00000 0.01361 0.01923 = 0.01961 -0.00480 -0.00406 -0.00104 C47 1 0.557038 0.419463 0.372381 11.00000 0.02394 0.01961 = 0.01820 -0.00689 -0.00153 -0.00178 AFIX 13 H47 2 0.648305 0.467138 0.339036 11.00000 -1.20000 AFIX 0 C48 1 0.405027 0.309632 0.542350 11.00000 0.01538 0.02422 = 0.01950 -0.00810 -0.00085 -0.00228 AFIX 13 H48 2 0.306060 0.342874 0.517191 11.00000 -1.20000 AFIX 0 C49 1 0.469115 0.185963 0.527332 11.00000 0.01823 0.02195 = 0.01773 -0.00689 -0.00280 -0.00277 AFIX 23 H49A 2 0.543746 0.142247 0.571053 11.00000 -1.20000 H49B 2 0.380414 0.137800 0.548701 11.00000 -1.20000 AFIX 0 C50 1 1.301177 0.251666 0.193833 11.00000 0.02288 0.05359 = 0.03077 -0.02151 -0.00678 -0.00667 AFIX 137 H50A 2 1.382309 0.304349 0.152617 11.00000 -1.50000 H50B 2 1.351002 0.173510 0.231964 11.00000 -1.50000 H50C 2 1.225548 0.290956 0.239878 11.00000 -1.50000 AFIX 0 C51 1 1.480724 0.142773 -0.126285 11.00000 0.01573 0.04253 = 0.02341 -0.01201 -0.00133 -0.00119 AFIX 137 H51A 2 1.525049 0.110628 -0.182413 11.00000 -1.50000 H51B 2 1.506919 0.081978 -0.065483 11.00000 -1.50000 H51C 2 1.525179 0.217264 -0.140033 11.00000 -1.50000 AFIX 0 C52 1 0.965281 0.197326 -0.231364 11.00000 0.02551 0.03761 = 0.01654 -0.00987 -0.00756 -0.00261 AFIX 137 H52A 2 1.032823 0.210043 -0.298565 11.00000 -1.50000 H52B 2 0.874866 0.261737 -0.233045 11.00000 -1.50000 H52C 2 0.927484 0.117935 -0.207584 11.00000 -1.50000 AFIX 0 C53 1 0.673874 0.463209 0.100523 11.00000 0.03833 0.02730 = 0.02160 -0.00110 -0.00708 -0.00317 AFIX 137 H53A 2 0.703331 0.545482 0.066824 11.00000 -1.50000 H53B 2 0.558590 0.467641 0.118470 11.00000 -1.50000 H53C 2 0.718344 0.413897 0.055784 11.00000 -1.50000 AFIX 0 C54 1 0.410840 0.496479 0.334814 11.00000 0.03616 0.02794 = 0.02530 -0.00930 -0.01011 0.00715 AFIX 137 H54A 2 0.438041 0.528834 0.261851 11.00000 -1.50000 H54B 2 0.374904 0.564099 0.362505 11.00000 -1.50000 H54C 2 0.326392 0.445592 0.356140 11.00000 -1.50000 AFIX 0 C55 1 0.371755 0.304806 0.650641 11.00000 0.03077 0.03025 = 0.02142 -0.01201 0.00099 -0.00553 AFIX 137 H55A 2 0.303024 0.242490 0.692409 11.00000 -1.50000 H55B 2 0.319429 0.384274 0.657038 11.00000 -1.50000 H55C 2 0.471378 0.284546 0.672235 11.00000 -1.50000 AFIX 0 C101 1 0.052035 0.565842 0.113848 11.00000 0.04403 0.03278 = 0.07325 -0.01665 -0.02293 -0.00428 AFIX 137 H10A 2 -0.010698 0.613846 0.064543 11.00000 -1.50000 H10B 2 0.012582 0.591362 0.173623 11.00000 -1.50000 H10C 2 0.043409 0.479280 0.131629 11.00000 -1.50000 AFIX 0 C102 1 0.220894 0.585708 0.070796 11.00000 0.04492 0.02129 = 0.05483 -0.00611 -0.02879 -0.00076 C103 1 0.295983 0.563776 -0.026879 11.00000 0.05936 0.03637 = 0.05673 -0.00984 -0.02474 -0.00535 AFIX 137 H10D 2 0.277105 0.483765 -0.023082 11.00000 -1.50000 H10E 2 0.409870 0.566122 -0.042094 11.00000 -1.50000 H10F 2 0.250214 0.627057 -0.079510 11.00000 -1.50000 AFIX 0 C201 1 0.050260 0.166906 0.484749 11.00000 0.02419 0.02242 = 0.02399 -0.00847 -0.00555 -0.00365 C202 1 -0.071018 0.268404 0.517549 11.00000 0.02799 0.01940 = 0.01769 -0.00618 -0.00618 -0.00260 C301 1 0.289652 0.781519 0.544362 11.00000 0.02492 0.03070 = 0.04920 -0.02145 -0.00216 -0.00113 C302 1 0.327914 0.655505 0.528146 11.00000 0.01903 0.02431 = 0.02864 -0.01213 -0.00488 -0.00176 HKLF 4 REM 392_A71P6_fertig_a.res in P1 REM R1 = 0.0277 for 10697 Fo > 4sig(Fo) and 0.0278 for all 10743 data REM 725 parameters refined using 3 restraints END WGHT 0.0451 0.2806 REM Highest difference peak 0.251, deepest hole -0.233, 1-sigma level 0.038 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3147.69 70.99 1 -3 0 3190.68 69.39 1 -3 0 3030.10 74.49 1 -3 0 3174.38 71.99 1 -3 0 3087.39 68.99 1 -3 0 3076.49 69.39 1 -3 0 3119.49 70.19 1 -3 0 3104.89 69.99 1 -3 0 3098.49 69.89 1 -3 0 3030.50 70.19 -1 3 0 3018.20 69.49 -1 3 0 2969.60 69.69 -1 3 0 3189.38 70.89 -1 3 0 3177.98 76.49 -1 3 0 3138.59 69.69 -1 3 0 3125.89 69.79 0 -3 0 9663.23 218.18 0 -3 0 9999.00 220.48 -1 -3 0 1387.16 31.20 -1 -3 0 1303.37 30.20 -1 -3 0 1343.17 30.50 -1 -3 0 1317.87 30.30 -1 -3 0 1296.77 30.60 -1 -3 0 1330.07 29.90 -1 -3 0 1325.67 33.50 -1 -3 0 1348.27 31.10 -1 -3 0 1373.26 31.70 -1 -3 0 1303.17 30.80 1 3 0 1414.06 31.70 1 3 0 1285.37 30.40 1 3 0 1372.36 30.10 1 3 0 1371.66 30.90 1 3 0 1376.26 31.30 1 3 0 1241.48 30.50 1 3 0 1287.77 29.80 1 3 0 1362.26 32.00 -2 -3 0 919.21 21.00 -2 -3 0 945.71 22.40 -2 -3 0 900.91 21.80 -2 -3 0 941.01 20.90 -2 -3 0 927.51 20.60 -2 -3 0 915.31 20.90 -2 -3 0 871.51 20.60 -2 -3 0 949.60 21.00 2 3 0 876.61 20.80 2 3 0 929.11 21.20 2 3 0 916.41 21.80 2 3 0 923.81 30.20 2 3 0 923.91 21.10 2 3 0 926.51 20.70 2 3 0 921.11 21.20 2 3 0 906.11 21.30 -3 -3 0 100.69 2.50 -3 -3 0 106.29 2.90 -3 -3 0 98.29 2.40 -3 -3 0 99.59 2.70 -3 -3 0 95.29 2.40 3 3 0 98.89 2.90 3 3 0 102.49 2.60 3 3 0 103.59 3.30 3 3 0 94.29 2.90 3 3 0 104.89 3.00 3 3 0 99.49 2.40 3 3 0 102.09 2.80 3 3 0 99.49 2.40 3 3 0 99.29 2.50 3 3 0 101.79 2.50 -4 -3 0 211.98 4.90 -4 -3 0 206.78 5.40 4 3 0 218.28 5.20 4 3 0 209.98 4.80 4 3 0 207.58 4.80 4 3 0 193.28 5.50 4 3 0 208.78 6.20 4 3 0 202.68 4.80 4 3 0 218.18 5.40 4 3 0 213.78 5.00 4 3 0 217.18 5.00 -5 -3 0 70.29 2.30 -5 -3 0 70.49 1.90 -5 -3 0 68.49 1.90 5 3 0 70.59 1.80 5 3 0 71.19 1.80 5 3 0 71.79 2.10 5 3 0 74.49 1.80 5 3 0 72.99 3.60 5 3 0 71.69 2.00 -6 -3 0 157.28 3.90 -6 -3 0 159.58 3.90 -6 -3 0 160.58 3.90 -6 -3 0 158.58 3.90 -6 -3 0 160.08 3.80 -6 -3 0 163.28 4.00 -6 -3 0 161.98 3.90 -6 -3 0 159.28 3.90 6 3 0 162.68 4.90 6 3 0 161.08 3.80 6 3 0 156.78 3.90 6 3 0 159.88 4.10 6 3 0 159.28 4.20 6 3 0 164.48 3.90 6 3 0 157.48 3.80 -7 -3 0 84.59 2.20 -7 -3 0 82.09 2.20 -7 -3 0 83.99 2.40 -7 -3 0 82.89 2.10 -7 -3 0 79.49 2.20 -7 -3 0 82.49 2.50 -7 -3 0 83.39 2.20 7 3 0 90.19 2.80 7 3 0 82.59 2.20 7 3 0 83.59 2.20 7 3 0 75.79 2.60 7 3 0 82.09 2.20 7 3 0 79.49 2.20 -8 -3 0 46.00 1.40 -8 -3 0 46.70 1.40 -8 -3 0 46.70 1.40 -8 -3 0 45.80 1.40 -8 -3 0 45.40 1.40 -8 -3 0 45.70 1.30 8 3 0 44.60 1.40 8 3 0 45.40 1.40 8 3 0 46.70 1.50 -9 -3 0 17.30 0.80 -9 -3 0 19.50 0.80 -9 -3 0 18.40 0.80 -9 -3 0 19.40 0.70 -9 -3 0 18.30 0.60 -9 -3 0 18.70 0.70 -9 -3 0 18.90 0.80 9 3 0 18.50 0.70 9 3 0 18.00 0.70 9 3 0 20.00 1.10 9 3 0 19.10 0.80 -10 -3 0 10.10 0.50 -10 -3 0 10.10 0.50 -10 -3 0 9.80 0.50 -10 -3 0 9.50 0.60 10 3 0 10.20 0.50 10 3 0 9.90 0.40 9 -4 0 11.50 0.70 -9 4 0 10.70 0.50 -9 4 0 11.60 0.50 -9 4 0 10.40 0.50 -9 4 0 11.10 0.50 8 -4 0 12.70 0.70 8 -4 0 10.80 0.80 8 -4 0 12.20 0.60 -8 4 0 11.50 0.80 -8 4 0 12.40 0.70 -8 4 0 12.00 0.60 7 -4 0 2.20 0.30 7 -4 0 2.30 0.50 7 -4 0 2.50 0.80 7 -4 0 1.70 0.30 -7 4 0 2.10 0.40 -7 4 0 2.20 0.40 -7 4 0 2.40 0.40 -7 4 0 1.80 0.40 -7 4 0 1.80 0.40 -7 4 0 2.40 0.40 6 -4 0 89.89 2.80 6 -4 0 87.59 2.40 6 -4 0 90.69 2.20 6 -4 0 89.09 2.20 -6 4 0 91.29 2.40 -6 4 0 93.49 2.40 -6 4 0 88.79 2.40 -6 4 0 89.99 2.40 -6 4 0 88.59 2.40 -6 4 0 87.99 2.30 -6 4 0 87.99 2.40 5 -4 0 100.99 2.20 5 -4 0 94.69 2.30 5 -4 0 99.09 2.30 -5 4 0 85.49 2.50 -5 4 0 90.49 2.40 -5 4 0 88.09 2.40 -5 4 0 92.19 2.40 -5 4 0 89.59 2.40 -5 4 0 89.99 2.40 -5 4 0 92.79 2.40 -5 4 0 91.09 2.40 4 -4 0 546.35 13.80 4 -4 0 561.74 12.50 4 -4 0 546.45 14.70 4 -4 0 545.35 12.50 4 -4 0 575.54 12.60 4 -4 0 563.34 12.80 -4 4 0 571.84 12.80 3 -4 0 40.00 1.00 3 -4 0 35.90 1.20 3 -4 0 37.30 1.00 3 -4 0 39.20 2.40 3 -4 0 38.70 1.20 3 -4 0 36.80 1.00 2 -4 0 217.58 5.30 2 -4 0 227.58 6.20 2 -4 0 209.18 5.70 2 -4 0 212.78 5.10 2 -4 0 217.68 5.20 2 -4 0 217.88 5.20 2 -4 0 213.78 5.90 2 -4 0 219.78 5.00 2 -4 0 217.78 4.90 2 -4 0 222.28 5.10 2 -4 0 222.58 4.90 -2 4 0 219.28 5.10 1 -4 0 302.87 7.40 1 -4 0 305.67 7.10 1 -4 0 300.97 7.10 1 -4 0 316.27 6.90 1 -4 0 299.77 7.30 1 -4 0 303.17 7.20 1 -4 0 305.07 6.90 1 -4 0 308.07 7.00 -1 4 0 313.67 7.30 -1 4 0 309.57 7.00 -1 4 0 296.27 6.90 -1 4 0 311.57 7.00 -1 4 0 308.87 8.60 0 -4 0 1071.59 25.20 0 -4 0 1081.99 24.50 0 -4 0 1121.99 25.60 0 -4 0 1047.20 24.30 0 -4 0 1071.69 24.60 0 -4 0 1112.79 24.70 0 -4 0 1085.49 25.20 0 -4 0 1088.19 24.80 0 4 0 1099.29 25.20 0 4 0 1127.09 25.80 0 4 0 1092.89 26.10 0 4 0 1114.19 25.00 0 4 0 1102.49 24.50 -1 -4 0 509.45 11.70 -1 -4 0 507.65 11.80 -1 -4 0 502.45 11.70 -1 -4 0 510.95 12.10 -1 -4 0 510.05 11.60 -1 -4 0 522.65 12.00 -1 -4 0 534.15 12.00 -1 -4 0 511.05 15.10 -1 -4 0 540.95 12.20 -1 -4 0 497.55 11.90 -1 -4 0 525.45 12.20 1 4 0 524.05 11.60 1 4 0 519.85 12.00 1 4 0 532.05 12.00 1 4 0 517.45 11.70 1 4 0 527.35 12.10 1 4 0 523.65 11.80 -2 -4 0 246.88 6.00 -2 -4 0 253.57 6.30 -2 -4 0 248.28 6.30 -2 -4 0 244.98 6.20 -2 -4 0 259.87 5.90 -2 -4 0 248.98 5.80 -2 -4 0 267.87 6.40 -2 -4 0 247.08 5.80 2 4 0 253.87 5.90 2 4 0 229.78 5.80 2 4 0 261.07 6.30 2 4 0 262.27 6.00 2 4 0 257.87 6.70 2 4 0 261.57 5.90 2 4 0 258.17 5.80 -3 -4 0 91.49 3.10 -3 -4 0 96.09 2.30 -3 -4 0 92.59 2.40 -3 -4 0 84.09 3.00 -3 -4 0 94.59 2.70 -3 -4 0 94.69 2.70 -3 -4 0 103.89 2.60 -3 -4 0 95.29 2.30 -3 -4 0 92.79 2.30 3 4 0 94.19 4.80 3 4 0 91.09 2.30 3 4 0 94.79 2.60 3 4 0 90.89 2.40 3 4 0 94.89 2.40 3 4 0 92.39 2.70 3 4 0 95.49 3.00 3 4 0 84.39 3.50 -4 -4 0 557.64 13.40 -4 -4 0 544.75 12.80 -4 -4 0 559.14 12.90 -4 -4 0 572.94 12.90 -4 -4 0 552.74 13.20 -4 -4 0 565.74 12.60 4 4 0 552.14 12.90 4 4 0 541.15 12.50 4 4 0 560.24 12.70 4 4 0 540.85 12.40 4 4 0 558.44 12.60 4 4 0 562.34 13.60 4 4 0 531.95 16.70 4 4 0 537.85 13.10 -5 -4 0 36.50 1.30 -5 -4 0 39.80 1.20 -5 -4 0 38.00 1.70 -5 -4 0 35.30 1.20 5 4 0 35.70 2.80 5 4 0 37.70 1.10 5 4 0 38.70 1.80 5 4 0 39.00 1.30 5 4 0 36.70 1.30 5 4 0 38.50 1.10 5 4 0 38.70 1.10 5 4 0 37.90 2.70 -6 -4 0 118.39 3.00 -6 -4 0 120.09 2.90 -6 -4 0 120.69 3.10 -6 -4 0 115.09 3.00 -6 -4 0 119.09 3.00 -6 -4 0 115.49 3.00 -6 -4 0 117.19 3.00 6 4 0 118.69 3.20 6 4 0 117.89 3.00 6 4 0 121.09 3.30 6 4 0 116.59 3.00 6 4 0 117.49 2.90 6 4 0 115.09 4.00 6 4 0 118.59 2.90 -7 -4 0 15.90 0.70 -7 -4 0 16.40 0.80 -7 -4 0 16.40 0.80 -7 -4 0 15.00 0.80 -7 -4 0 15.90 0.80 -7 -4 0 13.90 0.90 7 4 0 16.00 0.90 7 4 0 15.40 0.70 7 4 0 16.20 1.10 7 4 0 16.40 0.70 7 4 0 16.30 0.80 7 4 0 15.80 0.80 -8 -4 0 161.78 3.90 -8 -4 0 161.28 3.90 -8 -4 0 165.98 3.80 -8 -4 0 159.08 3.90 -8 -4 0 155.28 3.80 -8 -4 0 163.38 3.90 8 4 0 159.28 3.90 8 4 0 158.48 3.90 8 4 0 159.98 3.90 8 4 0 146.99 4.30 8 4 0 160.38 3.90 8 4 0 156.58 4.00 -9 -4 0 65.59 1.70 -9 -4 0 63.59 1.70 -9 -4 0 64.59 1.70 -9 -4 0 63.29 1.70 -9 -4 0 65.29 1.60 -9 -4 0 62.59 1.70 -9 -4 0 68.49 2.00 9 4 0 64.39 1.70 9 4 0 61.49 1.80 9 4 0 64.29 1.80 9 4 0 65.19 1.70 -10 -4 0 18.00 0.70 -10 -4 0 19.50 0.70 10 4 0 19.40 0.60 10 4 0 18.70 0.70 10 4 0 18.40 0.70 -9 5 0 101.39 2.40 -9 5 0 98.99 2.40 -9 5 0 103.19 2.40 -9 5 0 98.89 2.40 8 -5 0 29.50 1.00 -8 5 0 32.70 1.00 -8 5 0 31.70 1.00 -8 5 0 31.80 1.00 -8 5 0 31.20 1.00 -8 5 0 30.20 1.00 7 -5 0 100.39 2.50 7 -5 0 100.39 2.50 -7 5 0 102.39 2.60 -7 5 0 98.89 2.60 -7 5 0 102.99 2.60 -7 5 0 100.29 2.60 -7 5 0 98.29 2.60 6 -5 0 90.59 2.20 6 -5 0 88.29 2.40 6 -5 0 87.99 2.80 6 -5 0 89.59 2.20 -6 5 0 87.69 2.30 -6 5 0 90.39 2.40 -6 5 0 91.09 2.40 -6 5 0 87.49 2.40 -6 5 0 90.19 2.40 -6 5 0 90.19 2.30 5 -5 0 36.10 1.00 5 -5 0 35.50 1.10 5 -5 0 37.00 1.00 -5 5 0 36.20 1.20 -5 5 0 35.70 1.20 -5 5 0 36.90 1.20 -5 5 0 34.20 1.20 -5 5 0 35.20 1.20 -5 5 0 35.60 1.20 -5 5 0 36.40 1.30 -5 5 0 29.40 1.40 4 -5 0 425.66 9.40 4 -5 0 421.06 9.60 4 -5 0 419.66 9.30 4 -5 0 401.96 11.20 4 -5 0 439.06 9.60 -4 5 0 377.96 9.40 -4 5 0 412.66 9.50 -4 5 0 409.86 9.50 -4 5 0 415.46 9.50 -4 5 0 407.46 9.50 -4 5 0 398.36 9.50 3 -5 0 99.99 2.40 3 -5 0 100.59 2.50 3 -5 0 102.19 2.40 2 -5 0 130.79 3.10 2 -5 0 131.09 3.30 2 -5 0 135.09 3.10 2 -5 0 126.29 3.40 2 -5 0 132.39 3.20 2 -5 0 135.09 3.10 2 -5 0 131.89 3.60 2 -5 0 125.79 4.30 -2 5 0 131.59 3.20 1 -5 0 45.30 1.70 1 -5 0 45.80 1.20 1 -5 0 46.00 1.60 1 -5 0 53.39 1.60 1 -5 0 47.00 1.30 1 -5 0 46.60 1.20 1 -5 0 46.80 1.40 1 -5 0 46.20 1.20 -1 5 0 44.10 1.40 -1 5 0 47.20 1.40 -1 5 0 45.80 1.20 -1 5 0 43.40 1.70 0 -5 0 1798.02 41.10 0 -5 0 1713.83 39.90 0 -5 0 1788.52 40.20 0 -5 0 1822.02 40.40 0 -5 0 1770.82 40.20 0 -5 0 1830.22 42.30 0 -5 0 1829.42 40.00 0 -5 0 1822.62 39.90 0 -5 0 1817.92 40.20 0 -5 0 1763.12 40.70 0 -5 0 1667.73 45.60 0 5 0 1565.44 39.80 0 5 0 1794.72 40.80 0 5 0 1847.22 43.90 0 5 0 1818.22 40.40 0 5 0 1738.33 40.30 0 5 0 1839.52 41.20 -1 -5 0 19.70 0.70 -1 -5 0 18.20 1.20 -1 -5 0 18.60 1.00 -1 -5 0 18.50 0.80 -1 -5 0 18.20 0.60 -1 -5 0 19.20 0.90 -1 -5 0 18.00 0.70 -1 -5 0 17.80 0.60 1 5 0 18.00 1.70 1 5 0 21.60 1.00 1 5 0 19.90 1.00 1 5 0 18.40 1.00 1 5 0 18.00 0.80 1 5 0 19.80 0.70 1 5 0 19.00 0.70 -2 -5 0 332.27 8.30 -2 -5 0 341.67 8.10 -2 -5 0 326.67 8.30 -2 -5 0 348.47 7.60 -2 -5 0 335.47 7.60 -2 -5 0 340.67 7.90 -2 -5 0 329.57 7.60 -2 -5 0 322.37 7.70 2 5 0 326.67 7.70 2 5 0 319.57 7.50 2 5 0 332.07 7.60 2 5 0 329.57 7.50 2 5 0 322.97 8.50 2 5 0 335.17 8.20 2 5 0 328.17 7.90 2 5 0 332.97 8.00 -3 -5 0 201.68 4.50 -3 -5 0 194.08 5.30 -3 -5 0 200.18 5.20 -3 -5 0 197.48 5.00 -3 -5 0 193.38 4.50 -3 -5 0 191.78 4.50 -3 -5 0 176.98 4.70 -3 -5 0 188.98 4.70 3 5 0 185.18 4.50 3 5 0 195.78 4.90 3 5 0 199.68 4.70 3 5 0 202.48 4.50 3 5 0 200.48 5.10 3 5 0 194.58 4.50 3 5 0 197.78 4.90 -4 -5 0 637.54 15.50 -4 -5 0 653.73 15.80 -4 -5 0 641.04 14.90 -4 -5 0 622.84 14.70 -4 -5 0 635.84 15.20 -4 -5 0 665.83 14.90 4 5 0 663.63 14.90 4 5 0 671.83 14.70 4 5 0 644.94 16.00 4 5 0 664.13 14.70 4 5 0 652.43 15.00 4 5 0 668.93 14.70 4 5 0 654.43 15.50 -5 -5 0 48.30 1.50 -5 -5 0 48.70 1.50 -5 -5 0 47.00 1.50 -5 -5 0 48.50 2.10 -5 -5 0 49.00 1.50 -5 -5 0 46.60 1.50 5 5 0 50.19 1.40 5 5 0 49.60 1.40 5 5 0 48.60 1.30 5 5 0 48.90 2.30 5 5 0 50.09 1.70 5 5 0 49.30 1.40 5 5 0 48.20 1.60 5 5 0 50.69 1.50 -6 -5 0 92.09 2.50 -6 -5 0 94.79 2.40 -6 -5 0 92.99 2.50 -6 -5 0 97.59 2.70 -6 -5 0 92.89 2.40 -6 -5 0 94.19 2.50 6 5 0 92.39 2.50 6 5 0 91.29 3.80 6 5 0 93.09 2.40 6 5 0 95.29 2.40 6 5 0 93.19 2.70 6 5 0 94.79 2.40 6 5 0 93.59 2.80 6 5 0 91.19 2.50 -7 -5 0 74.89 2.10 -7 -5 0 74.59 2.00 -7 -5 0 74.89 2.10 -7 -5 0 77.29 2.10 -7 -5 0 76.09 2.00 -7 -5 0 74.29 2.40 7 5 0 74.99 2.10 7 5 0 78.39 2.60 7 5 0 74.69 2.00 7 5 0 76.59 2.10 7 5 0 74.39 2.10 7 5 0 75.19 2.00 7 5 0 72.49 2.50 -8 -5 0 69.89 1.90 -8 -5 0 71.59 2.00 -8 -5 0 72.39 2.00 -8 -5 0 72.19 2.00 8 5 0 74.39 2.00 8 5 0 73.69 1.90 8 5 0 73.09 2.10 8 5 0 73.29 2.00 8 5 0 75.09 2.00 -9 -5 0 20.70 0.80 -9 -5 0 20.00 0.80 -9 -5 0 20.80 0.70 -9 -5 0 20.10 0.70 9 5 0 19.80 0.70 9 5 0 21.30 0.80 9 5 0 18.60 0.90 9 5 0 20.80 0.80 -10 -5 0 13.00 0.50 10 5 0 13.30 0.60 10 5 0 12.50 0.50 10 5 0 11.80 0.60 -8 6 0 1.60 0.30 -8 6 0 1.70 0.30 -8 6 0 2.30 0.40 -8 6 0 2.30 0.30 -8 6 0 2.10 0.30 7 -6 0 8.70 0.70 7 -6 0 9.90 0.60 -7 6 0 10.20 0.60 -7 6 0 11.20 0.70 -7 6 0 10.00 0.60 6 -6 0 62.79 1.80 6 -6 0 61.59 2.40 6 -6 0 65.79 1.70 6 -6 0 64.49 1.90 -6 6 0 65.29 1.80 -6 6 0 65.29 1.80 -6 6 0 65.79 1.80 -6 6 0 66.59 1.80 -6 6 0 65.19 1.80 5 -6 0 3.90 0.40 5 -6 0 3.40 0.60 5 -6 0 3.90 0.40 -5 6 0 3.80 0.50 -5 6 0 4.80 0.50 -5 6 0 3.30 0.40 -5 6 0 3.20 0.40 -5 6 0 4.00 0.50 -5 6 0 4.20 0.50 -5 6 0 2.70 0.40 4 -6 0 275.97 6.40 4 -6 0 273.37 6.30 4 -6 0 274.57 6.20 -4 6 0 278.17 6.40 -4 6 0 272.97 6.40 -4 6 0 275.17 6.40 -4 6 0 271.67 6.40 -4 6 0 273.57 6.40 -4 6 0 266.17 6.40 -4 6 0 264.07 6.50 3 -6 0 152.48 3.60 3 -6 0 155.18 3.70 3 -6 0 154.78 3.90 -3 6 0 145.09 3.70 -3 6 0 146.29 3.70 -3 6 0 148.59 3.70 -3 6 0 157.58 3.70 -3 6 0 151.28 3.80 -3 6 0 152.08 3.70 -3 6 0 147.69 3.70 2 -6 0 200.88 4.80 2 -6 0 204.38 4.60 2 -6 0 204.48 4.70 2 -6 0 203.08 4.60 2 -6 0 190.78 5.00 2 -6 0 198.18 5.40 -2 6 0 199.28 4.70 1 -6 0 1736.73 39.00 1 -6 0 1738.23 39.10 1 -6 0 1741.83 39.60 1 -6 0 1784.82 40.50 1 -6 0 1739.43 38.80 1 -6 0 1760.92 39.60 -1 6 0 1692.13 38.80 0 -6 0 367.76 8.20 0 -6 0 333.67 8.90 0 -6 0 345.97 8.10 0 -6 0 359.26 8.40 0 -6 0 355.96 8.10 0 -6 0 370.06 9.00 0 -6 0 362.66 8.60 0 -6 0 358.86 8.10 0 -6 0 366.26 8.20 0 6 0 343.07 8.50 -1 -6 0 518.45 11.90 -1 -6 0 512.45 11.50 -1 -6 0 516.25 11.50 -1 -6 0 489.45 12.40 -1 -6 0 521.85 12.10 -1 -6 0 505.15 11.60 -1 -6 0 513.45 11.50 1 6 0 499.45 14.80 1 6 0 504.55 12.10 1 6 0 507.05 12.20 1 6 0 515.95 11.90 -2 -6 0 7.90 1.90 -2 -6 0 11.40 0.60 -2 -6 0 11.50 0.60 -2 -6 0 11.80 0.90 -2 -6 0 10.50 0.50 -2 -6 0 13.30 0.80 -2 -6 0 12.00 0.50 -2 -6 0 12.10 0.50 2 6 0 10.90 1.00 2 6 0 11.50 0.60 2 6 0 11.30 0.80 2 6 0 12.50 1.20 -3 -6 0 118.29 3.90 -3 -6 0 118.89 2.90 -3 -6 0 117.29 3.00 -3 -6 0 116.69 3.60 -3 -6 0 116.19 3.00 -3 -6 0 118.69 2.90 -3 -6 0 114.99 2.80 3 6 0 124.19 3.10 3 6 0 117.19 2.80 3 6 0 119.49 3.10 3 6 0 115.49 2.80 3 6 0 109.69 2.90 3 6 0 105.59 2.90 3 6 0 115.59 3.90 3 6 0 121.39 3.40 3 6 0 119.19 3.60 -4 -6 0 94.69 2.50 -4 -6 0 98.69 3.10 -4 -6 0 93.39 2.50 -4 -6 0 98.99 2.60 -4 -6 0 95.09 2.50 -4 -6 0 94.39 2.40 -4 -6 0 92.09 2.40 -4 -6 0 96.09 3.40 -4 -6 0 92.49 2.50 -4 -6 0 100.59 2.40 4 6 0 95.89 3.40 4 6 0 96.19 2.40 4 6 0 96.49 2.40 4 6 0 96.09 2.70 4 6 0 93.19 2.50 4 6 0 94.49 3.00 4 6 0 93.59 4.00 4 6 0 94.19 2.40 4 6 0 101.09 2.60 4 6 0 96.59 2.70 4 6 0 94.59 2.40 -5 -6 0 23.60 1.00 -5 -6 0 23.80 0.90 -5 -6 0 22.80 1.00 -5 -6 0 21.60 1.70 -5 -6 0 22.20 0.90 -5 -6 0 19.90 1.10 -5 -6 0 22.80 0.90 5 6 0 22.50 0.90 5 6 0 23.60 0.80 5 6 0 22.30 1.20 5 6 0 25.50 0.80 5 6 0 22.20 1.00 5 6 0 21.10 1.10 5 6 0 22.70 2.20 5 6 0 22.80 1.20 -6 -6 0 115.69 2.90 -6 -6 0 112.69 3.20 -6 -6 0 114.49 2.90 -6 -6 0 115.29 2.90 -6 -6 0 118.09 2.90 -6 -6 0 113.39 3.00 6 6 0 114.29 2.90 6 6 0 112.49 3.10 6 6 0 115.39 3.70 6 6 0 113.09 3.00 6 6 0 113.79 3.00 6 6 0 109.99 3.30 6 6 0 113.59 2.80 -7 -6 0 153.18 4.20 -7 -6 0 160.08 3.90 -7 -6 0 163.68 3.90 -7 -6 0 161.58 3.90 -7 -6 0 160.68 3.90 -7 -6 0 160.78 3.90 7 6 0 155.58 3.90 7 6 0 161.58 3.80 7 6 0 155.68 3.80 7 6 0 152.28 4.00 7 6 0 152.48 4.50 7 6 0 159.58 3.90 -8 -6 0 53.19 1.50 -8 -6 0 53.39 1.50 -8 -6 0 54.19 1.50 8 6 0 52.39 1.60 8 6 0 52.19 1.50 8 6 0 51.29 1.50 8 6 0 52.29 1.60 8 6 0 52.19 1.90 -9 -6 0 10.30 0.50 -9 -6 0 10.50 0.50 -9 -6 0 10.40 0.50 9 6 0 10.80 0.60 9 6 0 10.40 0.50 -10 -6 0 20.00 0.60 10 6 0 17.80 0.60 10 6 0 17.20 0.70 -8 7 0 1.50 0.30 -8 7 0 1.20 0.20 -8 7 0 1.50 0.20 7 -7 0 2.80 0.40 -7 7 0 2.10 0.30 -7 7 0 2.10 0.30 -7 7 0 1.30 0.30 -7 7 0 1.30 0.30 6 -7 0 32.30 1.10 6 -7 0 31.50 1.00 -6 7 0 32.10 1.10 -6 7 0 32.20 1.10 -6 7 0 32.50 1.10 -6 7 0 33.20 1.10 5 -7 0 2.90 0.30 5 -7 0 3.10 0.50 5 -7 0 3.00 0.50 -5 7 0 3.00 0.40 -5 7 0 2.70 0.40 -5 7 0 3.20 0.40 -5 7 0 2.70 0.40 -5 7 0 1.90 0.30 -5 7 0 3.00 0.40 4 -7 0 76.89 2.00 -4 7 0 76.29 2.10 -4 7 0 82.09 2.10 -4 7 0 78.49 2.10 -4 7 0 75.49 2.20 -4 7 0 77.29 2.10 -4 7 0 76.79 2.50 -4 7 0 77.39 2.10 3 -7 0 17.60 0.80 3 -7 0 16.10 0.70 3 -7 0 17.10 1.10 3 -7 0 16.80 0.60 -3 7 0 18.10 0.90 -3 7 0 15.00 0.90 -3 7 0 16.50 0.80 -3 7 0 17.50 0.90 -3 7 0 15.70 0.80 -3 7 0 16.50 0.80 -3 7 0 15.40 1.10 2 -7 0 78.89 2.00 2 -7 0 77.19 2.20 2 -7 0 77.39 1.90 2 -7 0 81.39 2.10 2 -7 0 75.39 2.00 -2 7 0 78.39 2.10 -2 7 0 74.99 2.00 -2 7 0 73.79 2.10 -2 7 0 79.19 2.10 -2 7 0 72.99 1.90 -2 7 0 72.29 2.10 -2 7 0 75.09 2.10 1 -7 0 491.95 12.40 1 -7 0 505.65 11.30 1 -7 0 514.85 11.60 1 -7 0 493.85 11.30 1 -7 0 517.55 11.30 1 -7 0 503.85 11.40 1 -7 0 499.25 11.30 -1 7 0 490.15 11.40 -1 7 0 486.25 11.40 -1 7 0 515.15 11.60 -1 7 0 489.85 11.30 -1 7 0 478.25 11.30 -1 7 0 481.45 11.40 0 -7 0 172.88 4.60 0 -7 0 171.48 4.00 0 -7 0 168.18 4.00 0 -7 0 170.78 4.00 0 -7 0 170.68 4.30 0 -7 0 164.98 5.00 0 -7 0 149.79 4.40 -1 -7 0 396.06 9.10 -1 -7 0 396.16 9.30 -1 -7 0 395.06 9.80 -1 -7 0 397.16 9.10 -1 -7 0 389.66 9.10 -1 -7 0 400.36 9.20 1 7 0 389.16 9.30 1 7 0 441.06 17.30 1 7 0 381.36 9.50 -2 -7 0 61.69 1.70 -2 -7 0 64.19 1.70 -2 -7 0 63.69 1.80 -2 -7 0 63.59 2.40 -2 -7 0 61.59 1.90 -2 -7 0 62.89 1.70 -2 -7 0 68.09 1.90 2 7 0 58.19 1.70 2 7 0 62.09 1.90 2 7 0 61.09 2.20 -3 -7 0 2.00 0.30 -3 -7 0 3.30 1.00 -3 -7 0 2.50 0.40 -3 -7 0 2.10 0.40 -3 -7 0 3.20 0.50 -3 -7 0 2.40 0.40 -3 -7 0 1.80 0.30 3 7 0 2.00 0.50 3 7 0 3.30 0.50 3 7 0 2.30 0.40 3 7 0 2.70 0.60 3 7 0 2.50 0.50 3 7 0 2.00 0.60 3 7 0 2.20 0.40 -4 -7 0 1.90 0.40 -4 -7 0 2.50 0.40 -4 -7 0 2.90 0.40 -4 -7 0 1.10 0.40 -4 -7 0 2.80 0.80 -4 -7 0 1.90 0.40 -4 -7 0 1.60 0.50 -4 -7 0 2.00 0.30 -4 -7 0 1.90 0.50 -4 -7 0 2.00 0.80 4 7 0 2.70 0.50 4 7 0 2.10 0.40 4 7 0 3.50 0.50 4 7 0 1.60 0.40 4 7 0 1.90 0.40 4 7 0 1.70 0.40 4 7 0 1.40 0.40 -5 -7 0 39.00 1.20 -5 -7 0 38.30 1.40 -5 -7 0 37.70 1.30 -5 -7 0 38.80 1.50 -5 -7 0 39.40 1.30 5 7 0 43.60 1.60 5 7 0 39.20 1.40 5 7 0 40.20 1.20 5 7 0 37.90 1.20 -6 -7 0 68.39 1.90 -6 -7 0 66.19 1.90 -6 -7 0 68.49 2.20 -6 -7 0 70.59 1.90 -6 -7 0 66.99 1.90 6 7 0 70.99 1.80 6 7 0 69.09 2.00 6 7 0 69.89 2.00 6 7 0 66.49 1.90 6 7 0 68.89 1.80 -7 -7 0 37.70 1.80 -7 -7 0 39.60 1.30 -7 -7 0 39.00 1.20 -7 -7 0 40.20 1.30 -7 -7 0 39.40 1.20 7 7 0 40.80 1.20 7 7 0 40.40 1.30 7 7 0 39.80 1.20 7 7 0 37.20 1.40 7 7 0 40.20 1.50 -8 -7 0 76.89 2.00 -8 -7 0 78.09 2.00 -8 -7 0 79.59 2.00 -8 -7 0 75.39 2.00 8 7 0 77.59 2.00 8 7 0 79.99 2.10 8 7 0 77.99 2.00 -9 -7 0 21.40 0.70 -9 -7 0 21.50 0.70 9 7 0 22.10 0.70 9 7 0 22.20 0.70 9 7 0 22.20 0.80 -7 8 0 20.70 0.70 -7 8 0 20.50 0.70 -7 8 0 20.60 0.70 -7 8 0 20.90 0.70 6 -8 0 5.20 0.60 -6 8 0 6.40 0.50 -6 8 0 7.00 0.50 -6 8 0 6.20 0.50 -6 8 0 7.00 0.60 -6 8 0 7.00 0.50 5 -8 0 247.08 5.70 5 -8 0 235.78 5.60 5 -8 0 239.38 5.60 -5 8 0 243.78 5.70 -5 8 0 237.68 5.70 -5 8 0 240.68 5.70 -5 8 0 245.18 5.70 -5 8 0 240.38 5.70 -5 8 0 243.28 5.70 4 -8 0 113.59 2.90 4 -8 0 112.69 3.00 4 -8 0 115.39 2.80 -4 8 0 115.69 3.00 -4 8 0 115.79 3.00 -4 8 0 116.89 3.00 -4 8 0 114.99 2.90 -4 8 0 116.99 2.90 -4 8 0 114.19 2.90 3 -8 0 35.00 1.20 3 -8 0 33.20 1.20 3 -8 0 34.50 1.10 3 -8 0 35.40 1.10 -3 8 0 34.00 1.20 -3 8 0 34.40 1.20 -3 8 0 32.40 1.20 -3 8 0 33.70 1.20 -3 8 0 34.60 1.20 -3 8 0 34.90 1.20 -3 8 0 32.20 1.10 -3 8 0 32.10 1.30 2 -8 0 2.60 0.40 2 -8 0 2.70 0.40 2 -8 0 2.90 0.40 2 -8 0 3.00 0.40 -2 8 0 3.50 0.40 -2 8 0 2.20 0.30 -2 8 0 3.00 0.50 -2 8 0 2.30 0.40 -2 8 0 1.90 0.40 -2 8 0 3.90 0.50 -2 8 0 2.50 0.40 -2 8 0 2.60 0.40 -2 8 0 3.60 0.50 1 -8 0 163.48 3.90 1 -8 0 163.78 3.90 1 -8 0 166.48 3.90 1 -8 0 159.58 4.40 1 -8 0 168.08 4.10 -1 8 0 158.08 4.00 -1 8 0 169.48 4.00 -1 8 0 165.58 3.90 -1 8 0 157.28 4.00 -1 8 0 166.68 4.00 -1 8 0 167.88 4.10 0 -8 0 303.47 6.90 0 -8 0 305.57 7.10 0 -8 0 300.67 7.00 0 -8 0 302.27 6.90 0 -8 0 304.27 7.00 0 -8 0 284.67 7.00 0 8 0 296.97 7.00 0 8 0 301.07 7.00 0 8 0 283.57 7.00 0 8 0 309.27 7.00 0 8 0 307.67 7.00 0 8 0 295.27 7.00 0 8 0 296.17 6.90 -1 -8 0 41.10 2.10 -1 -8 0 42.00 1.30 -1 -8 0 42.30 1.40 -1 -8 0 44.70 1.30 -1 -8 0 44.10 1.40 -1 -8 0 42.60 1.30 1 8 0 44.00 1.30 1 8 0 41.20 1.50 1 8 0 43.10 1.30 1 8 0 40.10 1.40 1 8 0 43.60 1.30 1 8 0 42.20 1.40 1 8 0 43.30 1.40 -2 -8 0 79.19 2.00 -2 -8 0 77.49 2.20 -2 -8 0 76.59 2.00 -2 -8 0 75.39 2.10 -2 -8 0 77.19 3.10 -2 -8 0 78.49 2.10 -2 -8 0 76.19 2.10 2 8 0 80.39 2.10 2 8 0 72.79 2.10 2 8 0 74.99 2.20 2 8 0 73.69 2.10 2 8 0 77.49 2.10 2 8 0 77.69 2.10 2 8 0 78.29 2.30 -3 -8 0 86.79 2.30 -3 -8 0 85.79 3.70 -3 -8 0 88.49 2.20 -3 -8 0 87.19 2.30 -3 -8 0 87.09 2.60 -3 -8 0 85.89 2.50 -3 -8 0 90.49 2.30 -3 -8 0 84.89 2.50 -3 -8 0 87.89 2.30 3 8 0 87.09 2.30 3 8 0 84.89 2.30 3 8 0 86.29 2.30 3 8 0 85.19 2.30 3 8 0 86.29 2.40 3 8 0 81.09 3.80 3 8 0 86.39 2.60 -4 -8 0 164.08 3.80 -4 -8 0 158.08 3.90 -4 -8 0 163.48 4.10 -4 -8 0 160.28 4.00 -4 -8 0 160.28 3.90 4 8 0 158.98 3.90 4 8 0 156.78 4.30 4 8 0 148.29 4.40 4 8 0 159.18 3.90 4 8 0 157.78 3.90 -5 -8 0 51.49 1.50 -5 -8 0 52.59 1.60 -5 -8 0 52.39 1.50 -5 -8 0 52.19 1.60 -5 -8 0 52.19 1.80 5 8 0 52.89 1.60 5 8 0 51.99 1.60 5 8 0 50.39 1.40 5 8 0 51.19 1.60 5 8 0 50.29 1.60 5 8 0 52.09 1.90 -6 -8 0 206.98 4.90 -6 -8 0 205.88 5.00 -6 -8 0 207.88 4.90 6 8 0 208.78 4.90 6 8 0 210.08 5.00 6 8 0 205.28 4.80 6 8 0 198.88 5.00 -7 -8 0 16.20 0.70 -7 -8 0 15.40 0.70 -7 -8 0 15.40 0.70 7 8 0 15.80 0.90 7 8 0 16.60 0.70 7 8 0 15.60 0.90 7 8 0 15.50 0.70 -8 -8 0 56.29 1.50 -8 -8 0 57.69 1.50 -8 -8 0 56.89 1.50 8 8 0 57.09 1.50 8 8 0 56.69 1.60 -9 -8 0 44.70 1.20 -9 -8 0 43.40 1.10 9 8 0 41.40 1.20 9 8 0 42.90 1.10 -7 9 0 13.30 0.50 -7 9 0 14.30 0.50 -6 9 0 61.49 1.60 -6 9 0 62.09 1.60 -6 9 0 63.09 1.60 -6 9 0 60.19 1.60 5 -9 0 48.60 1.40 -5 9 0 48.70 1.40 -5 9 0 48.80 1.40 -5 9 0 49.00 1.40 -5 9 0 48.10 1.40 -5 9 0 48.00 1.40 4 -9 0 8.90 0.70 4 -9 0 7.50 0.60 4 -9 0 9.10 0.60 -4 9 0 8.40 0.70 -4 9 0 9.10 0.70 -4 9 0 7.90 0.60 -4 9 0 8.80 0.60 -4 9 0 8.70 0.60 -4 9 0 8.10 0.60 3 -9 0 40.80 1.20 3 -9 0 40.00 1.30 3 -9 0 39.80 1.20 -3 9 0 38.40 1.30 -3 9 0 39.60 1.30 -3 9 0 40.70 1.30 -3 9 0 40.10 1.30 -3 9 0 38.20 1.30 -3 9 0 41.00 1.40 -3 9 0 40.00 1.40 -3 9 0 40.30 1.30 2 -9 0 92.09 2.60 2 -9 0 90.89 2.40 2 -9 0 89.59 2.40 2 -9 0 91.59 2.40 -2 9 0 92.39 2.40 -2 9 0 94.39 2.50 -2 9 0 94.49 2.40 -2 9 0 93.19 2.50 -2 9 0 93.59 2.50 -2 9 0 95.19 2.50 -2 9 0 94.29 2.40 -2 9 0 93.99 2.50 1 -9 0 60.99 2.60 1 -9 0 57.49 2.50 1 -9 0 62.49 1.70 1 -9 0 64.89 1.80 1 -9 0 64.99 1.80 -1 9 0 62.99 1.80 -1 9 0 58.49 1.90 -1 9 0 62.99 1.80 -1 9 0 64.79 1.80 -1 9 0 64.09 1.80 -1 9 0 64.09 1.80 -1 9 0 65.19 1.80 -1 9 0 63.09 1.90 -1 9 0 62.99 1.60 0 -9 0 41.40 1.50 0 -9 0 41.10 1.50 0 -9 0 38.30 1.40 0 -9 0 40.00 1.30 0 -9 0 44.70 1.40 0 -9 0 41.30 1.30 0 9 0 37.10 1.60 0 9 0 40.00 1.40 0 9 0 41.70 1.40 0 9 0 40.90 1.30 0 9 0 45.60 1.40 -1 -9 0 368.16 8.40 -1 -9 0 359.76 8.40 -1 -9 0 372.66 8.40 -1 -9 0 350.06 8.30 -1 -9 0 364.96 8.70 -1 -9 0 347.77 8.50 -1 -9 0 381.36 8.40 1 9 0 350.26 8.40 1 9 0 355.16 8.40 1 9 0 360.96 8.40 1 9 0 355.46 8.40 1 9 0 376.16 8.70 -2 -9 0 168.88 4.30 -2 -9 0 159.48 4.50 -2 -9 0 173.88 4.20 -2 -9 0 168.78 4.40 -2 -9 0 169.08 4.10 -2 -9 0 170.78 4.10 2 9 0 162.58 4.10 2 9 0 167.48 4.50 2 9 0 165.68 4.10 2 9 0 168.78 4.20 2 9 0 166.98 4.00 2 9 0 161.08 4.10 2 9 0 174.78 4.40 -3 -9 0 223.18 5.80 -3 -9 0 221.18 5.40 -3 -9 0 222.48 5.30 -3 -9 0 216.28 5.80 -3 -9 0 223.08 5.30 -3 -9 0 222.58 5.30 -3 -9 0 229.78 5.30 3 9 0 230.18 5.40 3 9 0 224.68 5.30 3 9 0 226.58 5.30 3 9 0 225.18 5.30 3 9 0 224.78 5.80 -4 -9 0 108.99 2.70 -4 -9 0 105.39 2.80 -4 -9 0 105.99 2.90 -4 -9 0 106.09 2.70 -4 -9 0 105.89 2.80 -4 -9 0 108.69 2.80 4 9 0 106.29 2.80 4 9 0 107.19 2.80 4 9 0 107.49 3.40 4 9 0 108.79 2.80 4 9 0 108.49 2.70 -5 -9 0 93.39 2.40 -5 -9 0 91.69 2.50 -5 -9 0 91.09 2.30 -5 -9 0 93.09 2.40 5 9 0 93.29 2.40 5 9 0 92.79 2.50 5 9 0 92.09 2.40 5 9 0 94.39 2.40 -6 -9 0 241.58 5.70 -6 -9 0 248.08 5.80 -6 -9 0 240.48 5.70 6 9 0 245.08 5.80 6 9 0 243.18 5.70 6 9 0 239.78 5.80 -7 -9 0 21.30 0.80 -7 -9 0 20.60 0.80 -7 -9 0 22.00 0.80 7 9 0 21.80 0.80 7 9 0 21.90 0.90 7 9 0 21.10 0.80 -8 -9 0 37.30 1.00 -8 -9 0 37.70 1.10 -8 -9 0 35.60 1.10 8 9 0 39.20 1.10 8 9 0 37.80 1.10 8 9 0 37.00 1.20 -6 10 0 8.90 0.40 -6 10 0 9.20 0.50 -6 10 0 9.20 0.40 5 -10 0 43.00 1.30 -5 10 0 44.90 1.20 -5 10 0 44.40 1.20 -5 10 0 44.10 1.20 -5 10 0 44.60 1.20 4 -10 0 6.20 0.60 4 -10 0 7.00 0.60 -4 10 0 7.10 0.50 -4 10 0 7.80 0.60 -4 10 0 7.20 0.50 -4 10 0 6.80 0.50 -4 10 0 6.30 0.50 3 -10 0 28.20 1.00 -3 10 0 26.70 1.00 -3 10 0 28.20 1.00 -3 10 0 26.90 1.00 -3 10 0 28.20 1.00 -3 10 0 28.10 1.00 -3 10 0 28.00 1.00 2 -10 0 62.79 1.80 2 -10 0 65.09 1.90 2 -10 0 66.39 1.80 2 -10 0 65.59 1.80 -2 10 0 65.69 1.80 -2 10 0 66.59 1.90 -2 10 0 67.19 1.80 -2 10 0 64.09 1.80 -2 10 0 66.59 1.80 -2 10 0 68.09 1.90 1 -10 0 27.40 1.00 1 -10 0 27.30 1.10 1 -10 0 26.10 1.00 1 -10 0 25.00 1.00 -1 10 0 28.10 1.00 -1 10 0 26.80 1.00 -1 10 0 25.90 1.10 -1 10 0 27.00 0.80 -1 10 0 26.90 1.00 -1 10 0 26.90 1.00 -1 10 0 27.20 1.00 -1 10 0 28.10 1.00 0 -10 0 543.25 12.30 0 -10 0 544.95 12.40 0 -10 0 529.25 12.60 0 -10 0 538.85 12.30 0 -10 0 520.35 12.30 0 10 0 552.44 12.30 0 10 0 543.35 12.40 0 10 0 519.25 12.30 0 10 0 543.05 12.20 0 10 0 546.65 12.30 0 10 0 550.94 12.30 0 10 0 541.95 12.30 0 10 0 541.95 12.30 -1 -10 0 174.28 4.20 -1 -10 0 174.48 4.30 -1 -10 0 169.88 4.60 -1 -10 0 169.38 4.20 -1 -10 0 172.18 4.20 -1 -10 0 176.38 4.20 1 10 0 173.88 4.20 1 10 0 175.78 4.20 1 10 0 171.78 4.30 1 10 0 173.98 4.20 1 10 0 170.98 4.20 1 10 0 167.78 4.20 1 10 0 175.08 4.10 1 10 0 176.38 4.20 -2 -10 0 16.30 1.30 -2 -10 0 14.40 0.70 -2 -10 0 15.40 1.30 -2 -10 0 14.70 0.90 -2 -10 0 15.30 0.80 -2 -10 0 14.50 0.70 -2 -10 0 15.30 0.80 2 10 0 13.80 0.90 2 10 0 15.50 0.70 2 10 0 13.70 0.70 2 10 0 15.10 0.80 2 10 0 15.40 0.80 2 10 0 12.80 0.90 2 10 0 15.40 0.70 -3 -10 0 139.59 3.40 -3 -10 0 129.69 4.10 -3 -10 0 139.39 3.50 -3 -10 0 137.49 3.40 -3 -10 0 140.39 3.40 -3 -10 0 136.39 3.80 3 10 0 141.59 3.40 3 10 0 139.99 3.40 3 10 0 138.19 3.40 3 10 0 139.49 3.40 3 10 0 136.29 3.40 3 10 0 137.39 3.50 -4 -10 0 62.39 1.80 -4 -10 0 61.69 1.90 -4 -10 0 64.09 1.70 -4 -10 0 61.19 2.30 -4 -10 0 64.49 1.80 4 10 0 64.59 1.90 4 10 0 63.39 1.80 4 10 0 67.09 1.80 4 10 0 63.09 1.70 -5 -10 0 196.98 4.80 -5 -10 0 197.78 4.70 5 10 0 198.38 4.80 5 10 0 198.18 4.70 5 10 0 202.58 4.80 5 10 0 197.18 4.80 -6 -10 0 70.59 1.90 -6 -10 0 71.59 1.90 -6 -10 0 73.19 1.90 6 10 0 69.99 1.90 6 10 0 72.89 2.00 6 10 0 73.99 1.90 -7 -10 0 27.60 0.90 -7 -10 0 28.20 0.90 -7 -10 0 27.20 0.90 7 10 0 28.00 0.90 7 10 0 28.90 0.90 7 10 0 29.10 0.90 -8 -10 0 37.10 1.00 -8 -10 0 35.20 1.00 -8 -10 0 34.80 1.00 8 10 0 37.60 1.00 -5 11 0 25.90 0.70 -5 11 0 25.70 0.80 -5 11 0 25.50 0.80 4 -11 0 5.20 0.50 4 -11 0 5.00 0.70 -4 11 0 6.10 0.40 -4 11 0 5.00 0.40 -4 11 0 5.30 0.40 -4 11 0 4.80 0.40 3 -11 0 1.70 0.30 3 -11 0 1.80 0.30 3 -11 0 1.70 0.40 -3 11 0 1.80 0.30 -3 11 0 1.40 0.30 -3 11 0 1.90 0.30 -3 11 0 1.60 0.30 2 -11 0 1.20 0.30 2 -11 0 1.00 0.30 2 -11 0 1.50 0.30 -2 11 0 1.00 0.30 -2 11 0 1.00 0.30 -2 11 0 1.30 0.30 -2 11 0 0.60 0.30 -2 11 0 0.80 0.30 -2 11 0 1.20 0.30 1 -11 0 6.60 0.60 1 -11 0 7.30 0.60 1 -11 0 7.10 0.60 1 -11 0 7.70 0.70 -1 11 0 6.90 0.60 -1 11 0 7.50 0.50 -1 11 0 6.50 0.60 -1 11 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4 8.30 0.90 -4 -4 4 10.40 1.30 -4 -4 4 10.30 0.70 -4 -4 4 11.00 0.70 -4 -4 4 9.00 0.90 3 4 -4 78.09 2.60 3 4 -4 85.49 2.50 3 4 -4 73.49 2.10 3 4 -4 80.99 2.30 3 4 -4 78.19 2.20 3 4 -4 77.69 7.20 -3 -4 4 81.39 2.60 -3 -4 4 77.39 2.90 -3 -4 4 79.59 2.00 -3 -4 4 79.39 2.20 -3 -4 4 74.69 3.20 -3 -4 4 76.89 2.10 -3 -4 4 81.29 2.20 -3 -4 4 75.59 2.10 2 4 -4 65.09 2.10 2 4 -4 64.19 1.80 -2 -4 4 60.39 1.70 -2 -4 4 60.99 1.60 -2 -4 4 61.09 1.60 -2 -4 4 61.49 1.80 -2 -4 4 62.59 1.60 -2 -4 4 54.69 2.20 -2 -4 4 61.79 2.20 1 4 -4 168.78 4.00 1 4 -4 169.98 5.70 1 4 -4 170.48 4.10 1 4 -4 166.38 4.30 -1 -4 4 171.18 4.30 -1 -4 4 169.28 3.90 -1 -4 4 172.58 4.50 -1 -4 4 166.08 4.00 -1 -4 4 168.78 4.10 -1 -4 4 172.58 4.10 -1 -4 4 160.28 3.90 0 4 -4 520.05 13.50 0 4 -4 518.55 11.80 0 4 -4 519.85 12.00 0 4 -4 498.55 12.90 0 4 -4 521.95 11.70 0 -4 4 515.25 12.00 0 -4 4 519.15 11.60 0 -4 4 519.85 11.80 0 -4 4 519.95 12.10 -1 4 -4 248.88 7.40 -1 4 -4 247.98 5.60 1 -4 4 243.18 5.50 1 -4 4 235.78 6.30 1 -4 4 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31.50 1.00 -4 7 -7 30.40 1.30 -4 7 -7 30.70 1.00 -4 7 -7 28.10 1.10 4 -7 7 28.40 1.20 4 -7 7 32.00 1.20 -5 7 -7 35.20 1.10 -5 7 -7 35.00 1.10 -5 7 -7 35.50 1.10 -5 7 -7 34.70 1.10 -6 7 -7 41.00 1.30 -6 7 -7 40.80 1.10 -6 7 -7 35.70 1.20 -6 7 -7 40.60 1.10 7 6 -7 30.90 0.90 -7 -6 7 30.00 0.90 -7 -6 7 30.90 0.90 6 6 -7 4.00 0.50 6 6 -7 4.70 0.40 6 6 -7 4.30 0.40 -6 -6 7 5.10 0.50 -6 -6 7 5.30 0.40 5 6 -7 43.50 1.30 5 6 -7 45.40 1.30 5 6 -7 45.70 1.30 -5 -6 7 43.50 1.30 -5 -6 7 43.90 1.30 -5 -6 7 45.50 1.40 4 6 -7 32.10 1.10 4 6 -7 30.60 1.10 4 6 -7 31.30 1.00 -4 -6 7 34.00 1.40 -4 -6 7 30.70 1.10 -4 -6 7 31.30 1.00 3 6 -7 33.60 1.30 3 6 -7 34.50 1.10 3 6 -7 35.40 1.20 3 6 -7 34.60 1.20 3 6 -7 35.00 1.20 -3 -6 7 37.00 1.20 -3 -6 7 35.50 1.30 -3 -6 7 34.50 1.90 -3 -6 7 36.20 1.20 -3 -6 7 36.40 1.20 2 6 -7 77.69 2.10 2 6 -7 79.09 2.20 2 6 -7 75.69 2.10 2 6 -7 75.89 2.10 2 6 -7 75.89 2.20 2 6 -7 76.59 2.20 2 6 -7 75.39 2.10 -2 -6 7 78.49 2.10 -2 -6 7 79.39 2.10 -2 -6 7 77.69 2.10 -2 -6 7 74.39 2.60 -2 -6 7 79.09 2.10 -2 -6 7 76.79 2.20 1 6 -7 204.58 5.10 1 6 -7 209.88 5.00 1 6 -7 200.38 5.00 1 6 -7 210.88 5.10 1 6 -7 205.88 4.90 1 6 -7 206.58 5.00 1 6 -7 208.08 5.00 1 6 -7 207.48 5.00 -1 -6 7 207.18 5.00 -1 -6 7 207.98 5.00 -1 -6 7 207.68 5.00 -1 -6 7 214.18 5.00 -1 -6 7 211.28 4.90 -1 -6 7 203.48 5.30 -1 -6 7 209.68 5.30 0 6 -7 16.60 0.80 0 6 -7 18.10 0.80 0 6 -7 16.90 0.80 0 6 -7 16.60 0.90 0 6 -7 17.30 0.90 0 6 -7 17.40 0.70 0 6 -7 17.40 0.90 0 -6 7 17.60 1.10 0 -6 7 17.90 0.80 0 -6 7 17.30 0.80 0 -6 7 17.80 1.00 0 -6 7 18.60 1.10 0 -6 7 17.30 0.70 0 -6 7 16.80 0.90 -1 6 -7 102.79 2.60 -1 6 -7 100.79 2.60 -1 6 -7 99.89 2.60 -1 6 -7 102.29 2.60 -1 6 -7 99.99 2.60 -1 6 -7 100.99 2.70 -1 6 -7 96.89 2.40 -1 6 -7 98.09 2.70 1 -6 7 101.39 2.90 1 -6 7 100.59 2.50 1 -6 7 99.49 2.50 1 -6 7 96.59 3.00 1 -6 7 101.49 2.60 1 -6 7 98.19 2.80 -2 6 -7 1.60 0.40 -2 6 -7 1.30 0.40 -2 6 -7 1.00 0.30 -2 6 -7 0.40 0.40 -2 6 -7 1.30 0.40 -2 6 -7 1.80 0.30 -2 6 -7 1.40 1.00 -2 6 -7 0.90 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4.30 -4 -5 7 163.18 3.90 -4 -5 7 161.78 4.00 -4 -5 7 159.88 3.80 3 5 -7 46.60 1.50 3 5 -7 46.50 1.50 3 5 -7 45.00 1.40 3 5 -7 46.00 1.50 3 5 -7 46.40 1.40 -3 -5 7 46.60 1.40 -3 -5 7 46.20 1.40 -3 -5 7 47.30 1.60 -3 -5 7 46.60 1.50 -3 -5 7 45.00 1.40 -3 -5 7 44.90 1.80 -3 -5 7 49.10 2.20 2 5 -7 187.88 4.50 2 5 -7 184.68 4.40 2 5 -7 182.18 4.40 2 5 -7 183.08 4.50 2 5 -7 180.48 4.50 2 5 -7 173.08 4.60 -2 -5 7 184.08 4.70 -2 -5 7 182.88 4.40 -2 -5 7 181.08 4.40 -2 -5 7 180.58 4.40 -2 -5 7 183.68 4.50 -2 -5 7 183.78 4.40 1 5 -7 42.70 1.40 1 5 -7 39.50 1.40 1 5 -7 40.60 1.60 1 5 -7 41.50 1.60 1 5 -7 45.30 1.40 -1 -5 7 43.70 1.30 -1 -5 7 45.10 1.40 -1 -5 7 44.20 1.60 -1 -5 7 43.90 1.40 -1 -5 7 46.50 1.40 -1 -5 7 44.00 1.60 -1 -5 7 42.20 1.30 0 5 -7 14.10 0.70 0 5 -7 13.90 0.90 0 5 -7 14.20 0.80 0 5 -7 15.40 0.80 0 5 -7 15.60 0.80 0 5 -7 13.90 0.80 0 5 -7 14.50 0.80 0 -5 7 15.00 0.70 0 -5 7 15.00 0.90 0 -5 7 14.70 0.70 0 -5 7 14.20 0.70 0 -5 7 14.70 0.90 0 -5 7 14.60 1.00 -1 5 -7 44.50 1.40 -1 5 -7 42.80 1.50 -1 5 -7 42.60 1.40 -1 5 -7 44.30 1.40 -1 5 -7 44.60 1.50 -1 5 -7 42.80 1.30 -1 5 -7 42.50 1.40 -1 5 -7 43.10 1.30 1 -5 7 43.50 1.30 1 -5 7 44.60 1.30 1 -5 7 45.60 1.50 1 -5 7 43.50 1.50 1 -5 7 44.00 1.30 1 -5 7 42.50 2.10 -2 5 -7 139.59 3.50 -2 5 -7 133.79 3.60 -2 5 -7 126.69 3.30 -2 5 -7 132.39 3.50 -2 5 -7 126.89 3.30 2 -5 7 134.09 3.20 2 -5 7 130.79 3.50 2 -5 7 132.99 3.20 2 -5 7 130.09 3.40 2 -5 7 132.39 3.20 -3 5 -7 35.10 1.20 -3 5 -7 34.20 1.30 -3 5 -7 35.30 1.20 -3 5 -7 34.50 1.20 -3 5 -7 35.10 1.80 -3 5 -7 34.10 1.20 -3 5 -7 35.00 1.20 -3 5 -7 33.30 1.20 3 -5 7 34.40 1.40 3 -5 7 33.30 1.00 -4 5 -7 18.60 1.30 -4 5 -7 19.80 0.90 -4 5 -7 19.10 1.00 -4 5 -7 18.10 0.80 -4 5 -7 19.30 0.90 -4 5 -7 18.40 0.90 4 -5 7 19.80 0.80 4 -5 7 20.80 0.90 -5 5 -7 145.19 3.50 -5 5 -7 139.09 3.50 -5 5 -7 141.89 3.60 -5 5 -7 141.49 4.10 -5 5 -7 141.69 3.50 -5 5 -7 145.49 3.50 -6 5 -7 26.70 1.10 -6 5 -7 28.20 1.00 -6 5 -7 28.40 1.00 -7 5 -7 22.20 0.90 -7 5 -7 23.40 0.90 8 4 -7 8.80 0.40 -8 -4 7 8.90 0.40 7 4 -7 20.90 0.70 7 4 -7 20.80 0.70 -7 -4 7 20.00 0.70 -7 -4 7 19.90 0.70 -7 -4 7 20.80 0.70 6 4 -7 46.00 1.40 6 4 -7 44.60 1.30 6 4 -7 44.60 1.40 -6 -4 7 46.30 1.30 -6 -4 7 45.00 1.30 -6 -4 7 44.50 1.30 5 4 -7 29.70 1.00 5 4 -7 30.10 1.10 5 4 -7 28.90 1.10 -5 -4 7 27.90 1.00 -5 -4 7 26.30 1.10 -5 -4 7 27.40 1.00 -5 -4 7 30.00 1.10 4 4 -7 119.89 3.60 4 4 -7 125.49 3.10 4 4 -7 125.99 3.10 4 4 -7 117.69 3.20 4 4 -7 126.29 3.20 -4 -4 7 125.39 3.10 -4 -4 7 125.09 3.00 -4 -4 7 117.69 3.00 -4 -4 7 124.89 3.10 -4 -4 7 120.79 3.40 -4 -4 7 118.99 3.10 3 4 -7 192.18 4.60 3 4 -7 188.08 4.60 3 4 -7 193.88 4.50 3 4 -7 186.78 4.90 3 4 -7 195.88 4.70 3 4 -7 181.98 4.70 -3 -4 7 186.78 4.60 -3 -4 7 187.38 4.70 -3 -4 7 194.48 5.10 -3 -4 7 185.08 4.70 -3 -4 7 193.08 4.50 -3 -4 7 185.38 5.00 -3 -4 7 191.68 4.50 -3 -4 7 182.48 4.90 2 4 -7 19.10 1.00 2 4 -7 19.20 1.00 2 4 -7 19.20 1.00 2 4 -7 18.70 0.80 2 4 -7 18.60 1.10 2 4 -7 19.70 0.80 2 4 -7 18.80 1.00 -2 -4 7 19.50 0.80 -2 -4 7 19.10 1.00 -2 -4 7 20.30 2.20 -2 -4 7 19.00 0.70 -2 -4 7 18.80 1.10 -2 -4 7 19.40 0.80 -2 -4 7 18.60 0.80 -2 -4 7 18.80 0.80 1 4 -7 118.69 2.90 1 4 -7 119.19 3.00 1 4 -7 114.49 3.00 1 4 -7 115.69 3.00 1 4 -7 114.19 2.90 1 4 -7 117.59 3.10 -1 -4 7 117.99 2.90 -1 -4 7 117.59 3.10 -1 -4 7 118.69 3.00 -1 -4 7 114.59 3.10 -1 -4 7 114.99 2.90 -1 -4 7 117.69 2.90 0 4 -7 20.20 0.90 0 4 -7 19.70 0.90 0 4 -7 18.40 0.80 0 4 -7 18.10 0.80 0 4 -7 19.10 1.00 0 4 -7 18.30 0.90 0 -4 7 19.30 0.70 0 -4 7 19.40 0.90 0 -4 7 18.20 0.90 0 -4 7 19.80 0.70 0 -4 7 20.20 0.70 0 -4 7 18.70 1.10 -1 4 -7 278.27 6.60 -1 4 -7 283.67 6.70 -1 4 -7 291.37 6.80 -1 4 -7 281.87 6.70 -1 4 -7 273.47 6.60 -1 4 -7 279.77 6.60 -1 4 -7 274.77 6.50 -1 4 -7 278.17 6.60 1 -4 7 295.07 6.70 1 -4 7 281.67 7.00 1 -4 7 285.37 6.60 1 -4 7 287.97 6.80 1 -4 7 289.87 6.60 1 -4 7 294.27 6.60 -2 4 -7 100.49 2.70 -2 4 -7 106.09 2.80 -2 4 -7 103.59 2.80 -2 4 -7 95.49 2.60 -2 4 -7 103.69 2.70 -2 4 -7 107.29 2.90 -2 4 -7 106.19 2.70 -2 4 -7 103.29 2.70 2 -4 7 111.09 3.10 2 -4 7 107.79 2.70 2 -4 7 107.69 2.60 2 -4 7 101.79 2.70 2 -4 7 104.19 2.50 2 -4 7 106.89 2.80 -3 4 -7 60.99 1.90 -3 4 -7 59.29 1.70 -3 4 -7 59.79 1.70 -3 4 -7 59.79 1.80 -3 4 -7 61.79 1.70 -3 4 -7 66.29 1.80 -3 4 -7 60.49 1.80 -3 4 -7 55.49 1.80 3 -4 7 61.09 1.90 3 -4 7 61.09 1.70 3 -4 7 61.69 1.60 3 -4 7 59.49 1.60 -4 4 -7 80.39 2.10 -4 4 -7 83.89 2.60 -4 4 -7 79.59 2.10 -4 4 -7 76.99 2.40 -4 4 -7 77.39 2.20 -4 4 -7 76.89 2.20 4 -4 7 77.49 2.40 4 -4 7 77.89 1.90 -5 4 -7 53.49 1.60 -5 4 -7 52.99 1.60 -5 4 -7 53.39 1.60 -5 4 -7 52.19 1.60 -5 4 -7 54.69 2.00 -5 4 -7 56.69 1.60 -6 4 -7 39.80 1.30 -6 4 -7 38.40 1.40 -6 4 -7 38.40 1.90 -6 4 -7 40.90 1.30 -6 4 -7 42.30 1.30 -6 4 -7 39.40 1.30 -7 4 -7 65.39 1.70 -7 4 -7 60.19 1.80 -7 4 -7 63.59 1.70 8 3 -7 32.80 1.00 -8 -3 7 33.70 1.00 -8 -3 7 34.80 0.90 7 3 -7 36.30 1.10 7 3 -7 37.10 1.10 -7 -3 7 35.20 1.10 -7 -3 7 36.00 1.10 -7 -3 7 36.20 1.10 6 3 -7 28.80 1.00 6 3 -7 27.90 1.00 6 3 -7 26.60 0.90 -6 -3 7 29.40 1.00 -6 -3 7 29.00 1.00 -6 -3 7 28.70 1.00 5 3 -7 151.28 3.60 5 3 -7 148.99 4.30 5 3 -7 153.48 3.80 5 3 -7 151.48 3.70 5 3 -7 145.09 3.70 -5 -3 7 152.38 3.70 -5 -3 7 147.89 3.70 -5 -3 7 151.68 3.70 4 3 -7 260.57 6.00 4 3 -7 263.17 6.00 4 3 -7 221.48 6.60 4 3 -7 246.28 6.10 4 3 -7 252.97 5.80 4 3 -7 262.17 6.10 -4 -3 7 260.17 6.00 -4 -3 7 253.77 5.90 -4 -3 7 260.57 6.00 -4 -3 7 247.78 6.20 -4 -3 7 260.47 6.00 3 3 -7 329.57 7.60 3 3 -7 321.07 7.60 3 3 -7 301.27 8.50 3 3 -7 323.67 7.50 3 3 -7 321.37 7.50 3 3 -7 315.77 7.70 3 3 -7 320.07 7.40 -3 -3 7 318.17 7.50 -3 -3 7 326.27 7.50 -3 -3 7 318.47 7.50 -3 -3 7 323.37 7.50 -3 -3 7 330.57 7.40 -3 -3 7 318.27 7.40 -3 -3 7 311.17 7.80 -3 -3 7 326.47 7.70 -3 -3 7 325.27 7.50 2 3 -7 19.30 0.80 2 3 -7 16.90 1.00 2 3 -7 19.40 1.00 2 3 -7 19.00 0.80 2 3 -7 17.70 1.00 2 3 -7 19.90 1.00 2 3 -7 19.10 1.60 -2 -3 7 16.50 0.70 -2 -3 7 20.20 0.80 -2 -3 7 13.70 1.10 -2 -3 7 18.40 0.70 -2 -3 7 17.00 0.80 -2 -3 7 18.20 1.70 -2 -3 7 18.40 1.00 -2 -3 7 18.40 0.90 1 3 -7 378.06 8.80 1 3 -7 374.66 8.90 1 3 -7 412.06 9.30 1 3 -7 375.56 8.70 -1 -3 7 382.06 8.90 -1 -3 7 380.96 8.80 -1 -3 7 375.36 8.90 -1 -3 7 378.96 8.70 -1 -3 7 371.66 9.60 -1 -3 7 379.96 8.70 0 3 -7 42.00 1.40 0 3 -7 42.70 1.40 0 3 -7 41.40 1.40 0 3 -7 39.00 1.30 0 3 -7 40.80 1.40 0 3 -7 42.00 1.30 0 -3 7 42.50 1.30 0 -3 7 42.70 1.20 0 -3 7 41.30 3.00 0 -3 7 42.20 1.20 0 -3 7 44.30 1.40 -1 3 -7 186.68 4.70 -1 3 -7 193.28 4.90 -1 3 -7 192.18 4.80 -1 3 -7 202.58 4.80 -1 3 -7 198.78 4.80 -1 3 -7 207.78 4.90 1 -3 7 199.28 4.70 1 -3 7 208.18 5.00 1 -3 7 201.88 4.80 1 -3 7 196.08 6.60 1 -3 7 204.48 4.70 1 -3 7 207.18 4.90 1 -3 7 204.68 4.70 -2 3 -7 429.36 9.70 -2 3 -7 411.36 9.70 -2 3 -7 409.36 9.70 -2 3 -7 408.16 9.80 -2 3 -7 423.66 9.70 -2 3 -7 421.26 9.70 -2 3 -7 433.06 9.80 2 -3 7 417.96 9.80 2 -3 7 432.56 9.50 2 -3 7 435.26 9.70 2 -3 7 420.16 9.50 -3 3 -7 8.70 0.90 -3 3 -7 8.50 0.60 -3 3 -7 8.60 1.00 -3 3 -7 8.20 0.70 -3 3 -7 9.10 0.70 -3 3 -7 9.40 0.70 3 -3 7 9.60 0.60 3 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1 -4 -17 65.39 1.60 1 -4 -17 66.69 1.60 -1 4 17 67.59 1.60 0 -4 -17 19.80 0.70 0 -4 -17 19.70 0.60 0 4 17 19.70 0.60 -1 -4 -17 23.60 0.80 -1 -4 -17 24.00 0.80 -1 -4 -17 24.80 0.70 -1 -4 -17 23.50 0.70 1 4 17 22.80 0.80 1 4 17 24.40 0.90 -2 -4 -17 12.10 0.50 -2 -4 -17 12.50 0.50 -2 -4 -17 12.20 0.60 -2 -4 -17 11.60 0.60 2 4 17 12.40 0.70 2 4 17 12.20 0.50 2 4 17 12.50 0.50 -3 -4 -17 53.89 1.30 -3 -4 -17 54.39 1.50 -3 -4 -17 53.39 1.40 -3 -4 -17 53.99 1.50 3 4 17 54.09 1.40 3 4 17 53.99 1.40 3 4 17 53.19 1.40 -4 -4 -17 11.80 0.50 -4 -4 -17 10.70 0.70 -4 -4 -17 10.80 0.50 4 4 17 11.30 0.50 4 4 17 10.90 0.50 4 4 17 10.80 0.50 -5 -4 -17 0.50 0.20 -5 -4 -17 0.30 0.20 -5 -4 -17 0.50 0.20 5 4 17 0.40 0.20 5 4 17 0.40 0.20 5 4 17 0.50 0.20 -6 -4 -17 0.70 0.20 -6 -4 -17 1.00 0.20 6 4 17 0.70 0.20 6 4 17 0.80 0.30 1 -5 -17 0.50 0.20 1 -5 -17 0.50 0.20 -1 5 17 0.80 0.20 0 -5 -17 19.50 0.70 0 -5 -17 20.60 0.60 0 5 17 19.60 0.70 -1 -5 -17 10.80 0.50 -1 -5 -17 11.20 0.50 -1 -5 -17 10.00 0.50 -1 -5 -17 10.90 0.50 1 5 17 10.70 0.50 1 5 17 9.70 0.70 -2 -5 -17 4.00 0.40 -2 -5 -17 3.80 0.30 -2 -5 -17 3.80 0.40 -2 -5 -17 3.60 0.40 2 5 17 4.00 0.40 2 5 17 4.00 0.50 2 5 17 4.30 0.40 -3 -5 -17 21.20 0.80 -3 -5 -17 22.00 0.80 -3 -5 -17 21.70 0.70 -3 -5 -17 21.80 0.70 3 5 17 21.60 0.90 3 5 17 22.60 0.70 3 5 17 21.60 0.80 3 5 17 22.60 0.70 -4 -5 -17 22.30 0.80 -4 -5 -17 23.80 0.80 -4 -5 -17 23.30 0.80 4 5 17 23.60 1.00 4 5 17 23.70 0.70 4 5 17 23.80 0.80 4 5 17 24.80 0.80 -5 -5 -17 9.00 0.50 -5 -5 -17 8.30 0.50 -5 -5 -17 9.20 0.40 5 5 17 8.60 0.40 5 5 17 8.80 0.50 5 5 17 7.50 0.90 5 5 17 8.50 0.40 -6 -5 -17 19.00 0.70 -6 -5 -17 20.00 0.70 -6 -5 -17 17.50 0.80 6 5 17 18.80 0.70 6 5 17 19.70 0.60 6 5 17 18.80 0.70 -7 -5 -17 14.50 0.50 7 5 17 13.10 0.50 0 -6 -17 36.90 1.00 0 -6 -17 37.30 1.00 0 6 17 35.10 1.20 0 6 17 37.90 1.00 -1 -6 -17 32.00 1.00 -1 -6 -17 31.90 0.90 -1 -6 -17 32.70 0.90 1 6 17 32.30 0.90 -2 -6 -17 4.20 0.30 -2 -6 -17 4.40 0.40 -2 -6 -17 3.90 0.40 -2 -6 -17 4.70 0.50 2 6 17 4.20 0.40 2 6 17 3.70 0.60 2 6 17 4.40 0.40 -3 -6 -17 1.50 0.20 -3 -6 -17 1.90 0.30 -3 -6 -17 1.30 0.20 -3 -6 -17 2.40 0.40 3 6 17 1.70 0.30 3 6 17 1.40 0.40 3 6 17 1.80 0.40 3 6 17 1.60 0.20 -4 -6 -17 13.90 0.70 -4 -6 -17 14.30 0.60 -4 -6 -17 14.30 0.50 -4 -6 -17 14.70 0.60 4 6 17 15.50 0.60 4 6 17 15.30 1.00 4 6 17 14.70 0.50 4 6 17 14.30 0.60 -5 -6 -17 31.80 0.90 -5 -6 -17 32.40 1.00 -5 -6 -17 30.20 1.00 5 6 17 32.30 0.90 5 6 17 32.00 0.90 5 6 17 32.20 0.90 -6 -6 -17 61.79 1.50 -6 -6 -17 62.49 1.60 -6 -6 -17 58.89 1.50 6 6 17 60.59 1.50 6 6 17 59.39 1.50 -7 -6 -17 0.70 0.20 0 -7 -17 28.00 0.80 0 -7 -17 26.50 0.80 0 7 17 27.70 0.80 -1 -7 -17 19.10 0.60 -1 -7 -17 18.50 0.70 -1 -7 -17 20.00 0.60 1 7 17 19.30 0.80 1 7 17 19.20 0.60 -2 -7 -17 14.10 0.50 -2 -7 -17 14.90 0.60 -2 -7 -17 14.80 0.60 -2 -7 -17 14.30 0.60 2 7 17 15.40 0.70 2 7 17 14.70 0.60 2 7 17 15.60 0.90 -3 -7 -17 41.90 1.10 -3 -7 -17 41.60 1.10 -3 -7 -17 39.70 1.10 -3 -7 -17 38.30 1.20 3 7 17 40.70 1.20 3 7 17 41.70 1.10 3 7 17 39.50 1.20 3 7 17 39.30 1.10 -4 -7 -17 1.40 0.20 -4 -7 -17 2.10 0.30 -4 -7 -17 1.40 0.20 4 7 17 1.50 0.40 4 7 17 1.50 0.40 4 7 17 1.70 0.20 4 7 17 2.00 0.30 -5 -7 -17 6.00 0.40 -5 -7 -17 6.50 0.40 -5 -7 -17 5.70 0.40 5 7 17 5.30 0.40 5 7 17 5.30 0.50 5 7 17 6.10 0.40 5 7 17 6.10 0.60 -6 -7 -17 21.50 0.70 -6 -7 -17 21.70 0.70 -6 -7 -17 23.30 0.70 6 7 17 21.80 0.60 6 7 17 20.40 0.80 6 7 17 18.30 1.10 0 -8 -17 106.39 2.50 0 8 17 102.59 2.50 -1 -8 -17 90.99 2.20 -1 -8 -17 90.79 2.10 1 8 17 87.69 2.10 1 8 17 86.89 2.10 -2 -8 -17 9.90 0.60 -2 -8 -17 10.80 0.50 -2 -8 -17 11.00 0.40 2 8 17 10.20 0.60 2 8 17 10.80 0.50 2 8 17 11.00 0.50 -3 -8 -17 3.70 0.30 -3 -8 -17 3.00 0.30 -3 -8 -17 2.30 0.40 3 8 17 3.10 0.50 3 8 17 3.60 0.50 3 8 17 4.20 0.40 -4 -8 -17 24.50 0.80 -4 -8 -17 24.10 0.70 -4 -8 -17 24.50 0.70 4 8 17 24.60 0.90 4 8 17 24.40 0.80 4 8 17 25.10 0.80 -5 -8 -17 40.40 1.20 -5 -8 -17 40.50 1.10 -5 -8 -17 41.80 1.00 -5 -8 -17 38.50 1.10 5 8 17 39.90 1.10 5 8 17 42.60 1.10 5 8 17 40.00 1.10 -6 -8 -17 7.20 0.40 -6 -8 -17 7.80 0.40 6 8 17 6.80 0.40 6 8 17 6.40 0.50 -1 -9 -17 5.20 0.40 1 9 17 4.90 0.40 -2 -9 -17 49.70 1.30 -2 -9 -17 49.50 1.30 2 9 17 49.10 1.30 -3 -9 -17 12.70 0.50 -3 -9 -17 11.90 0.60 3 9 17 13.30 0.50 3 9 17 12.50 0.50 3 9 17 13.70 0.90 -4 -9 -17 6.70 0.40 4 9 17 7.20 0.40 4 9 17 6.60 0.40 -5 -9 -17 74.09 1.90 -5 -9 -17 78.69 1.90 -5 -9 -17 77.89 1.80 5 9 17 76.49 1.80 5 9 17 77.29 1.80 -3 -10 -17 22.40 0.60 3 10 17 21.30 0.70 -4 -10 -17 93.39 2.20 -4 -10 -17 93.49 2.20 4 10 17 88.49 2.20 2 3 18 15.40 0.60 -3 -3 -18 1.10 0.20 3 3 18 0.60 0.20 -4 -3 -18 30.40 0.80 4 3 18 30.10 0.80 -1 -4 -18 19.40 0.60 -2 -4 -18 34.60 1.00 -2 -4 -18 36.10 1.00 2 4 18 35.30 0.90 2 4 18 35.20 1.00 -3 -4 -18 0.40 0.20 -3 -4 -18 0.30 0.20 3 4 18 0.70 0.20 3 4 18 -0.10 0.20 -4 -4 -18 3.90 0.30 -4 -4 -18 3.90 0.30 4 4 18 4.80 0.60 4 4 18 3.90 0.30 5 4 18 24.30 0.70 -1 -5 -18 57.29 1.40 1 5 18 57.19 1.40 -2 -5 -18 21.00 0.90 -2 -5 -18 19.80 0.70 -2 -5 -18 20.80 0.60 -2 -5 -18 21.00 0.60 2 5 18 19.90 0.60 -3 -5 -18 17.00 0.70 -3 -5 -18 14.80 0.70 3 5 18 17.30 0.60 -4 -5 -18 1.40 0.20 -4 -5 -18 1.40 0.20 4 5 18 1.30 0.20 4 5 18 1.40 0.20 -5 -5 -18 35.80 1.00 5 5 18 36.10 0.90 5 5 18 35.30 1.00 -1 -6 -18 30.20 1.00 1 6 18 31.80 0.80 -2 -6 -18 13.80 0.60 -2 -6 -18 14.20 0.50 -2 -6 -18 12.10 0.50 2 6 18 13.30 0.50 -3 -6 -18 0.00 0.20 -3 -6 -18 0.20 0.20 -3 -6 -18 -0.50 0.30 3 6 18 0.30 0.30 -4 -6 -18 12.30 0.50 -4 -6 -18 12.40 0.50 4 6 18 11.80 0.50 4 6 18 12.30 0.50 -5 -6 -18 114.19 2.70 -5 -6 -18 118.89 2.70 5 6 18 110.09 2.70 -2 -7 -18 1.70 0.20 2 7 18 2.50 0.30 -3 -7 -18 30.10 0.90 -3 -7 -18 29.40 0.80 -3 -7 -18 31.30 0.80 3 7 18 30.10 0.80 -4 -7 -18 18.80 0.60 -4 -7 -18 19.70 0.60 4 7 18 20.90 0.60 5 7 18 33.40 0.90 -3 -8 -18 5.00 0.30 -4 -8 -18 7.20 0.40 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 80437 loop_ _space_group_symop_operation_xyz 'x, y, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp F21 F 0.19016(15) 0.20273(13) 0.43441(10) 0.0336(3) Uani 1 1 d . . F22 F 0.07415(16) 0.07103(11) 0.56432(10) 0.0344(3) Uani 1 1 d . . F23 F -0.00085(16) 0.12707(12) 0.42617(10) 0.0339(3) Uani 1 1 d . . F31 F 0.41199(19) 0.81717(15) 0.55545(15) 0.0535(4) Uani 1 1 d . . F32 F 0.2425(3) 0.86682(17) 0.46570(17) 0.0725(6) Uani 1 1 d . . F33 F 0.1735(2) 0.78488(18) 0.62214(15) 0.0609(5) Uani 1 1 d . . O1 O 0.95627(16) 0.88936(13) 1.12682(10) 0.0229(3) Uani 1 1 d . . O2 O 0.67141(18) 0.85009(16) 1.16642(11) 0.0313(3) Uani 1 1 d . . O3 O 0.80043(17) 0.58969(12) 0.84082(10) 0.0232(3) Uani 1 1 d . . O4 O 0.74521(16) 1.02411(12) 0.71602(10) 0.0215(3) Uani 1 1 d . . H4O H 0.765(3) 1.081(3) 0.663(2) 0.034(7) Uiso 1 1 d . . O5 O 1.05367(15) 0.20062(13) -0.16565(9) 0.0221(3) Uani 1 1 d . . O6 O 1.31325(15) 0.16964(14) -0.11307(10) 0.0244(3) Uani 1 1 d . . O7 O 0.73424(16) 0.40863(12) 0.18882(10) 0.0225(3) Uani 1 1 d . . O8 O 0.70878(17) -0.02266(12) 0.28229(10) 0.0229(3) Uani 1 1 d . . H8O H 0.755(3) -0.016(3) 0.222(2) 0.033(7) Uiso 1 1 d . . O11 O 0.2936(2) 0.61907(17) 0.11306(16) 0.0476(5) Uani 1 1 d . . O21 O -0.0185(2) 0.36361(15) 0.50002(14) 0.0416(4) Uani 1 1 d . . O22 O -0.20605(17) 0.23956(12) 0.56000(11) 0.0256(3) Uani 1 1 d . . O31 O 0.46979(16) 0.61651(13) 0.50762(12) 0.0268(3) Uani 1 1 d . . O32 O 0.21315(19) 0.60780(16) 0.53586(16) 0.0416(4) Uani 1 1 d . . N1 N 0.91264(19) 0.57459(14) 0.54870(12) 0.0195(3) Uani 1 1 d . . H1A H 0.9137 0.5022 0.5402 0.023 Uiso 1 1 calc R U H1B H 1.0147 0.5875 0.5354 0.023 Uiso 1 1 calc R U N2 N 0.52797(18) 0.39319(14) 0.48286(11) 0.0191(3) Uani 1 1 d . . H2A H 0.4969 0.4647 0.4968 0.023 Uiso 1 1 calc R U H2B H 0.6202 0.3589 0.5024 0.023 Uiso 1 1 calc R U C1 C 0.8712(2) 0.84887(16) 0.91052(13) 0.0181(3) Uani 1 1 d . . C2 C 1.0183(2) 0.86993(17) 0.84149(14) 0.0202(4) Uani 1 1 d . . H2 H 1.0323 0.8655 0.7765 0.024 Uiso 1 1 calc R U C3 C 1.1401(2) 0.89636(17) 0.86608(14) 0.0212(4) Uani 1 1 d . . C4 C 1.1197(2) 0.90068(17) 0.96372(14) 0.0212(4) Uani 1 1 d . . H4 H 1.2053 0.9159 0.9820 0.025 Uiso 1 1 calc R U C5 C 0.9789(2) 0.88335(16) 1.03236(14) 0.0196(4) Uani 1 1 d . . C6 C 0.8471(2) 0.85743(16) 1.00838(13) 0.0183(3) Uani 1 1 d . . C7 C 0.6960(2) 0.83604(17) 1.07514(14) 0.0214(4) Uani 1 1 d . . C8 C 0.5825(2) 0.80219(18) 1.04723(14) 0.0227(4) Uani 1 1 d . . H8 H 0.4843 0.7859 1.0928 0.027 Uiso 1 1 calc R U C9 C 0.6109(2) 0.79155(17) 0.95150(14) 0.0217(4) Uani 1 1 d . . H9 H 0.5318 0.7664 0.9342 0.026 Uiso 1 1 calc R U C10 C 0.7492(2) 0.81652(16) 0.88292(13) 0.0186(3) Uani 1 1 d . . C11 C 0.7717(2) 0.80958(17) 0.78053(13) 0.0182(3) Uani 1 1 d . . C12 C 0.7950(2) 0.69818(16) 0.76275(13) 0.0182(3) Uani 1 1 d . . C13 C 0.8155(2) 0.69037(16) 0.66752(14) 0.0179(3) Uani 1 1 d . . C14 C 0.8151(2) 0.79755(17) 0.58675(13) 0.0176(3) Uani 1 1 d . . C15 C 0.7903(2) 0.90934(16) 0.60319(14) 0.0180(3) Uani 1 1 d . . H15 H 0.7882 0.9824 0.5485 0.022 Uiso 1 1 calc R U C16 C 0.7688(2) 0.91555(16) 0.69827(14) 0.0185(3) Uani 1 1 d . . C17 C 0.8375(2) 0.56566(17) 0.65551(13) 0.0192(4) Uani 1 1 d . . H17 H 0.9116 0.5101 0.6973 0.023 Uiso 1 1 calc R U C18 C 0.8313(2) 0.67398(17) 0.47488(14) 0.0207(4) Uani 1 1 d . . H18 H 0.7161 0.6663 0.4942 0.025 Uiso 1 1 calc R U C19 C 0.8525(2) 0.79438(16) 0.48085(13) 0.0203(4) Uani 1 1 d . . H19A H 0.9629 0.8099 0.4487 0.024 Uiso 1 1 calc R U H19B H 0.7829 0.8606 0.4431 0.024 Uiso 1 1 calc R U C20 C 1.2937(2) 0.9234(2) 0.79085(16) 0.0287(4) Uani 1 1 d . . H20A H 1.3195 1.0010 0.7878 0.043 Uiso 1 1 calc R U H20B H 1.2830 0.9287 0.7251 0.043 Uiso 1 1 calc R U H20C H 1.3782 0.8581 0.8108 0.043 Uiso 1 1 calc R U C21 C 1.0933(2) 0.89173(19) 1.15819(15) 0.0238(4) Uani 1 1 d . . H21A H 1.0626 0.8924 1.2273 0.036 Uiso 1 1 calc R U H21B H 1.1417 0.9651 1.1151 0.036 Uiso 1 1 calc R U H21C H 1.1694 0.8194 1.1536 0.036 Uiso 1 1 calc R U C22 C 0.5206(4) 0.8301(4) 1.2322(2) 0.0588(10) Uani 1 1 d . . H22A H 0.5174 0.8432 1.2947 0.088 Uiso 1 1 calc R U H22B H 0.5028 0.7464 1.2461 0.088 Uiso 1 1 calc R U H22C H 0.4382 0.8871 1.2009 0.088 Uiso 1 1 calc R U C23 C 0.9540(3) 0.5514(2) 0.86319(17) 0.0305(4) Uani 1 1 d . . H23A H 0.9565 0.4701 0.9127 0.046 Uiso 1 1 calc R U H23B H 0.9764 0.6090 0.8899 0.046 Uiso 1 1 calc R U H23C H 1.0339 0.5491 0.8022 0.046 Uiso 1 1 calc R U C24 C 0.6832(2) 0.51007(19) 0.68950(15) 0.0248(4) Uani 1 1 d . . H24A H 0.6432 0.4945 0.7615 0.037 Uiso 1 1 calc R U H24B H 0.7028 0.4333 0.6745 0.037 Uiso 1 1 calc R U H24C H 0.6048 0.5669 0.6542 0.037 Uiso 1 1 calc R U C25 C 0.9000(3) 0.6607(2) 0.37151(15) 0.0300(4) Uani 1 1 d . . H25A H 0.8512 0.7279 0.3226 0.045 Uiso 1 1 calc R U H25B H 0.8788 0.5831 0.3715 0.045 Uiso 1 1 calc R U H25C H 1.0143 0.6624 0.3540 0.045 Uiso 1 1 calc R U C31 C 0.9776(2) 0.20504(16) 0.09188(13) 0.0174(3) Uani 1 1 d . . C32 C 1.0574(2) 0.22204(18) 0.15572(14) 0.0211(4) Uani 1 1 d . . H32 H 0.9998 0.2278 0.2193 0.025 Uiso 1 1 calc R U C33 C 1.2157(2) 0.23032(19) 0.12746(15) 0.0243(4) Uani 1 1 d . . C34 C 1.3019(2) 0.2153(2) 0.03513(15) 0.0246(4) Uani 1 1 d . . H34 H 1.4125 0.2184 0.0163 0.030 Uiso 1 1 calc R U C35 C 1.2303(2) 0.19628(18) -0.02829(14) 0.0211(4) Uani 1 1 d . . C36 C 1.0620(2) 0.19837(16) -0.00452(13) 0.0177(3) Uani 1 1 d . . C37 C 0.9751(2) 0.19080(16) -0.06984(13) 0.0183(3) Uani 1 1 d . . C38 C 0.8182(2) 0.17532(18) -0.03514(14) 0.0212(4) Uani 1 1 d . . H38 H 0.7622 0.1665 -0.0776 0.025 Uiso 1 1 calc R U C39 C 0.7402(2) 0.17249(18) 0.06287(14) 0.0212(4) Uani 1 1 d . . H39 H 0.6335 0.1568 0.0867 0.025 Uiso 1 1 calc R U C40 C 0.8134(2) 0.19166(16) 0.12503(13) 0.0175(3) Uani 1 1 d . . C41 C 0.7226(2) 0.19419(17) 0.22654(13) 0.0169(3) Uani 1 1 d . . C42 C 0.6735(2) 0.08665(17) 0.29952(13) 0.0179(3) Uani 1 1 d . . C43 C 0.5890(2) 0.08599(17) 0.39467(14) 0.0184(3) Uani 1 1 d . . H43 H 0.5556 0.0123 0.4424 0.022 Uiso 1 1 calc R U C44 C 0.5528(2) 0.19193(17) 0.42078(13) 0.0176(3) Uani 1 1 d . . C45 C 0.5997(2) 0.30057(16) 0.34951(13) 0.0181(3) Uani 1 1 d . . C46 C 0.6832(2) 0.30020(17) 0.25351(14) 0.0180(3) Uani 1 1 d . . C47 C 0.5570(2) 0.41946(17) 0.37238(14) 0.0212(4) Uani 1 1 d . . H47 H 0.6483 0.4671 0.3390 0.025 Uiso 1 1 calc R U C48 C 0.4050(2) 0.30963(17) 0.54235(14) 0.0201(4) Uani 1 1 d . . H48 H 0.3061 0.3429 0.5172 0.024 Uiso 1 1 calc R U C49 C 0.4691(2) 0.18596(17) 0.52733(13) 0.0194(4) Uani 1 1 d . . H49A H 0.5437 0.1422 0.5711 0.023 Uiso 1 1 calc R U H49B H 0.3804 0.1378 0.5487 0.023 Uiso 1 1 calc R U C50 C 1.3012(3) 0.2517(2) 0.19383(17) 0.0330(5) Uani 1 1 d . . H50A H 1.3823 0.3043 0.1526 0.049 Uiso 1 1 calc R U H50B H 1.3510 0.1735 0.2320 0.049 Uiso 1 1 calc R U H50C H 1.2255 0.2910 0.2399 0.049 Uiso 1 1 calc R U C51 C 1.4807(2) 0.1428(2) -0.12629(15) 0.0279(4) Uani 1 1 d . . H51A H 1.5250 0.1106 -0.1824 0.042 Uiso 1 1 calc R U H51B H 1.5069 0.0820 -0.0655 0.042 Uiso 1 1 calc R U H51C H 1.5252 0.2173 -0.1400 0.042 Uiso 1 1 calc R U C52 C 0.9653(2) 0.1973(2) -0.23136(14) 0.0258(4) Uani 1 1 d . . H52A H 1.0328 0.2100 -0.2986 0.039 Uiso 1 1 calc R U H52B H 0.8749 0.2617 -0.2330 0.039 Uiso 1 1 calc R U H52C H 0.9275 0.1179 -0.2076 0.039 Uiso 1 1 calc R U C53 C 0.6739(3) 0.4632(2) 0.10052(15) 0.0311(4) Uani 1 1 d . . H53A H 0.7033 0.5455 0.0668 0.047 Uiso 1 1 calc R U H53B H 0.5586 0.4676 0.1185 0.047 Uiso 1 1 calc R U H53C H 0.7183 0.4139 0.0558 0.047 Uiso 1 1 calc R U C54 C 0.4108(3) 0.4965(2) 0.33481(16) 0.0308(5) Uani 1 1 d . . H54A H 0.4380 0.5288 0.2619 0.046 Uiso 1 1 calc R U H54B H 0.3749 0.5641 0.3625 0.046 Uiso 1 1 calc R U H54C H 0.3264 0.4456 0.3561 0.046 Uiso 1 1 calc R U C55 C 0.3718(3) 0.3048(2) 0.65064(15) 0.0277(4) Uani 1 1 d . . H55A H 0.3030 0.2425 0.6924 0.041 Uiso 1 1 calc R U H55B H 0.3194 0.3843 0.6570 0.041 Uiso 1 1 calc R U H55C H 0.4714 0.2845 0.6722 0.041 Uiso 1 1 calc R U C101 C 0.0520(3) 0.5658(2) 0.1138(3) 0.0481(7) Uani 1 1 d . . H10A H -0.0107 0.6138 0.0645 0.072 Uiso 1 1 calc R U H10B H 0.0126 0.5914 0.1736 0.072 Uiso 1 1 calc R U H10C H 0.0434 0.4793 0.1316 0.072 Uiso 1 1 calc R U C102 C 0.2209(3) 0.5857(2) 0.0708(2) 0.0388(5) Uani 1 1 d . . C103 C 0.2960(4) 0.5638(3) -0.0269(2) 0.0498(7) Uani 1 1 d . . H10D H 0.2771 0.4838 -0.0231 0.075 Uiso 1 1 calc R U H10E H 0.4099 0.5661 -0.0421 0.075 Uiso 1 1 calc R U H10F H 0.2502 0.6271 -0.0795 0.075 Uiso 1 1 calc R U C201 C 0.0503(2) 0.16691(18) 0.48475(15) 0.0231(4) Uani 1 1 d . . C202 C -0.0710(2) 0.26840(17) 0.51755(14) 0.0215(4) Uani 1 1 d . . C301 C 0.2897(3) 0.7815(2) 0.54436(19) 0.0342(5) Uani 1 1 d . . C302 C 0.3279(2) 0.65550(18) 0.52815(15) 0.0232(4) Uani 1 1 d . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 F21 0.0215(6) 0.0422(7) 0.0363(7) -0.0149(6) -0.0006(5) -0.0063(5) F22 0.0355(7) 0.0255(6) 0.0341(7) -0.0058(5) -0.0087(5) 0.0067(5) F23 0.0362(7) 0.0396(7) 0.0365(7) -0.0255(6) -0.0058(5) -0.0066(6) F31 0.0382(8) 0.0458(9) 0.0940(13) -0.0462(9) -0.0059(8) -0.0111(7) F32 0.1019(16) 0.0337(8) 0.0790(13) -0.0156(8) -0.0375(12) 0.0153(9) F33 0.0445(9) 0.0684(11) 0.0785(12) -0.0554(10) 0.0189(8) -0.0131(8) O1 0.0221(7) 0.0308(7) 0.0194(6) -0.0113(5) -0.0064(5) -0.0029(6) O2 0.0314(8) 0.0485(9) 0.0209(7) -0.0185(6) 0.0052(6) -0.0208(7) O3 0.0298(7) 0.0191(6) 0.0198(6) -0.0018(5) -0.0084(5) -0.0047(6) O4 0.0286(7) 0.0173(6) 0.0191(6) -0.0080(5) -0.0043(5) -0.0016(5) O5 0.0202(6) 0.0335(7) 0.0143(6) -0.0089(5) -0.0033(5) -0.0053(6) O6 0.0146(6) 0.0403(8) 0.0200(6) -0.0141(6) -0.0005(5) -0.0037(6) O7 0.0238(7) 0.0195(6) 0.0199(6) -0.0026(5) -0.0017(5) -0.0046(5) O8 0.0304(7) 0.0209(6) 0.0177(6) -0.0087(5) -0.0031(5) -0.0029(5) O11 0.0511(11) 0.0358(9) 0.0691(13) -0.0162(9) -0.0381(10) -0.0002(8) O21 0.0495(10) 0.0265(8) 0.0473(10) -0.0195(7) 0.0086(8) -0.0144(7) O22 0.0224(7) 0.0229(7) 0.0293(7) -0.0073(6) -0.0070(6) 0.0015(6) O31 0.0172(6) 0.0281(7) 0.0406(8) -0.0188(6) -0.0067(6) -0.0001(5) O32 0.0201(7) 0.0396(9) 0.0748(12) -0.0307(9) -0.0093(8) -0.0034(7) N1 0.0190(7) 0.0183(7) 0.0239(8) -0.0103(6) -0.0041(6) -0.0028(6) N2 0.0186(7) 0.0187(7) 0.0202(7) -0.0081(6) -0.0040(6) -0.0001(6) C1 0.0211(9) 0.0152(8) 0.0185(8) -0.0054(6) -0.0061(7) -0.0008(7) C2 0.0215(9) 0.0220(9) 0.0170(8) -0.0076(7) -0.0043(7) -0.0005(7) C3 0.0211(9) 0.0208(9) 0.0209(9) -0.0070(7) -0.0048(7) -0.0007(7) C4 0.0196(9) 0.0227(9) 0.0230(9) -0.0075(7) -0.0073(7) -0.0026(7) C5 0.0248(9) 0.0171(8) 0.0185(8) -0.0070(7) -0.0076(7) -0.0003(7) C6 0.0216(9) 0.0166(8) 0.0166(8) -0.0053(7) -0.0040(7) -0.0024(7) C7 0.0267(10) 0.0214(9) 0.0169(8) -0.0077(7) -0.0018(7) -0.0064(8) C8 0.0231(9) 0.0242(9) 0.0202(9) -0.0077(7) -0.0001(7) -0.0071(8) C9 0.0230(9) 0.0216(9) 0.0223(9) -0.0063(7) -0.0073(7) -0.0051(8) C10 0.0231(9) 0.0162(8) 0.0167(8) -0.0046(6) -0.0062(7) -0.0016(7) C11 0.0172(8) 0.0216(9) 0.0172(8) -0.0071(7) -0.0043(7) -0.0034(7) C12 0.0186(9) 0.0176(8) 0.0186(8) -0.0039(7) -0.0067(7) -0.0026(7) C13 0.0169(8) 0.0172(8) 0.0214(8) -0.0073(7) -0.0058(7) -0.0019(7) C14 0.0168(8) 0.0194(8) 0.0187(8) -0.0077(7) -0.0060(7) -0.0013(7) C15 0.0180(8) 0.0163(8) 0.0191(8) -0.0044(7) -0.0059(7) -0.0006(7) C16 0.0171(8) 0.0170(8) 0.0225(9) -0.0075(7) -0.0056(7) -0.0004(7) C17 0.0225(9) 0.0178(8) 0.0191(8) -0.0058(7) -0.0070(7) -0.0028(7) C18 0.0225(9) 0.0216(9) 0.0207(9) -0.0089(7) -0.0068(7) -0.0021(7) C19 0.0244(9) 0.0183(8) 0.0183(8) -0.0067(7) -0.0059(7) -0.0003(7) C20 0.0223(10) 0.0411(12) 0.0230(9) -0.0104(9) -0.0032(8) -0.0069(9) C21 0.0244(9) 0.0279(10) 0.0225(9) -0.0093(7) -0.0101(8) -0.0019(8) C22 0.0533(16) 0.111(3) 0.0328(13) -0.0442(16) 0.0210(12) -0.0567(18) C23 0.0371(12) 0.0237(10) 0.0316(10) -0.0044(8) -0.0194(9) 0.0019(9) C24 0.0264(10) 0.0242(9) 0.0249(9) -0.0065(7) -0.0050(8) -0.0090(8) C25 0.0432(12) 0.0257(10) 0.0239(10) -0.0128(8) -0.0059(9) -0.0041(9) C31 0.0168(8) 0.0184(8) 0.0169(8) -0.0054(6) -0.0046(7) -0.0012(6) C32 0.0193(9) 0.0282(9) 0.0176(8) -0.0100(7) -0.0038(7) -0.0025(8) C33 0.0220(10) 0.0308(10) 0.0230(9) -0.0098(8) -0.0077(8) -0.0039(8) C34 0.0160(9) 0.0342(10) 0.0241(9) -0.0100(8) -0.0039(7) -0.0040(8) C35 0.0181(9) 0.0267(9) 0.0176(8) -0.0070(7) -0.0018(7) -0.0043(7) C36 0.0170(9) 0.0193(8) 0.0169(8) -0.0058(7) -0.0040(7) -0.0023(7) C37 0.0196(9) 0.0193(8) 0.0150(8) -0.0054(6) -0.0037(7) -0.0008(7) C38 0.0188(9) 0.0284(9) 0.0196(9) -0.0096(7) -0.0078(7) -0.0012(7) C39 0.0135(8) 0.0286(10) 0.0218(9) -0.0086(7) -0.0047(7) -0.0014(7) C40 0.0166(8) 0.0185(8) 0.0164(8) -0.0059(7) -0.0032(7) -0.0004(7) C41 0.0113(7) 0.0229(9) 0.0166(8) -0.0067(7) -0.0042(6) 0.0002(7) C42 0.0150(8) 0.0219(9) 0.0189(8) -0.0081(7) -0.0063(7) -0.0008(7) C43 0.0168(8) 0.0187(8) 0.0193(8) -0.0044(7) -0.0054(7) -0.0027(7) C44 0.0124(8) 0.0220(9) 0.0180(8) -0.0067(7) -0.0031(6) -0.0011(7) C45 0.0153(8) 0.0197(9) 0.0199(8) -0.0076(7) -0.0050(7) 0.0003(7) C46 0.0136(8) 0.0192(8) 0.0196(8) -0.0048(7) -0.0041(7) -0.0010(7) C47 0.0239(9) 0.0196(9) 0.0182(8) -0.0069(7) -0.0015(7) -0.0018(7) C48 0.0154(8) 0.0242(9) 0.0195(8) -0.0081(7) -0.0009(7) -0.0023(7) C49 0.0182(9) 0.0220(9) 0.0177(8) -0.0069(7) -0.0028(7) -0.0028(7) C50 0.0229(10) 0.0536(14) 0.0308(11) -0.0215(10) -0.0068(8) -0.0067(10) C51 0.0157(9) 0.0425(12) 0.0234(9) -0.0120(9) -0.0013(7) -0.0012(8) C52 0.0255(10) 0.0376(11) 0.0165(9) -0.0099(8) -0.0076(8) -0.0026(9) C53 0.0383(12) 0.0273(10) 0.0216(9) -0.0011(8) -0.0071(9) -0.0032(9) C54 0.0362(12) 0.0279(10) 0.0253(10) -0.0093(8) -0.0101(9) 0.0071(9) C55 0.0308(11) 0.0303(10) 0.0214(9) -0.0120(8) 0.0010(8) -0.0055(9) C101 0.0440(15) 0.0328(12) 0.0733(19) -0.0166(13) -0.0229(14) -0.0043(11) C102 0.0449(14) 0.0213(10) 0.0548(15) -0.0061(10) -0.0288(12) -0.0008(10) C103 0.0594(18) 0.0364(13) 0.0567(17) -0.0098(12) -0.0247(14) -0.0054(13) C201 0.0242(10) 0.0224(9) 0.0240(9) -0.0085(7) -0.0056(7) -0.0036(8) C202 0.0280(10) 0.0194(9) 0.0177(8) -0.0062(7) -0.0062(7) -0.0026(7) C301 0.0249(10) 0.0307(11) 0.0492(13) -0.0214(10) -0.0022(10) -0.0011(9) C302 0.0190(9) 0.0243(9) 0.0286(10) -0.0121(8) -0.0049(8) -0.0018(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C5 O1 C21 117.24(15) C7 O2 C22 117.19(16) C12 O3 C23 112.09(15) C16 O4 H4O 111(2) C37 O5 C52 117.22(14) C35 O6 C51 116.97(15) C46 O7 C53 117.06(15) C42 O8 H8O 112.0(19) C17 N1 C18 114.15(14) C17 N1 H1A 108.7 C18 N1 H1A 108.7 C17 N1 H1B 108.7 C18 N1 H1B 108.7 H1A N1 H1B 107.6 C47 N2 C48 113.61(14) C47 N2 H2A 108.8 C48 N2 H2A 108.8 C47 N2 H2B 108.8 C48 N2 H2B 108.8 H2A N2 H2B 107.7 C2 C1 C10 119.88(16) C2 C1 C6 119.78(17) C10 C1 C6 120.33(16) C3 C2 C1 121.80(17) C3 C2 H2 119.1 C1 C2 H2 119.1 C2 C3 C4 118.90(17) C2 C3 C20 121.31(17) C4 C3 C20 119.78(18) C5 C4 C3 121.46(18) C5 C4 H4 119.3 C3 C4 H4 119.3 C4 C5 O1 122.19(17) C4 C5 C6 121.08(16) O1 C5 C6 116.73(16) C1 C6 C7 117.61(16) C1 C6 C5 116.92(16) C7 C6 C5 125.44(16) O2 C7 C8 122.11(17) O2 C7 C6 117.27(16) C8 C7 C6 120.62(16) C7 C8 C9 120.45(18) C7 C8 H8 119.8 C9 C8 H8 119.8 C10 C9 C8 121.70(18) C10 C9 H9 119.1 C8 C9 H9 119.1 C9 C10 C1 119.18(17) C9 C10 C11 119.99(17) C1 C10 C11 120.83(16) C12 C11 C16 117.27(16) C12 C11 C10 121.83(16) C16 C11 C10 120.89(16) O3 C12 C13 117.34(16) O3 C12 C11 120.21(16) C13 C12 C11 122.44(16) C14 C13 C12 118.92(16) C14 C13 C17 122.27(16) C12 C13 C17 118.80(16) C15 C14 C13 119.42(16) C15 C14 C19 119.18(16) C13 C14 C19 121.26(16) C16 C15 C14 120.92(17) C16 C15 H15 119.5 C14 C15 H15 119.5 O4 C16 C15 121.91(17) O4 C16 C11 117.09(16) C15 C16 C11 121.00(16) N1 C17 C13 109.14(14) N1 C17 C24 110.52(15) C13 C17 C24 113.12(16) N1 C17 H17 108.0 C13 C17 H17 108.0 C24 C17 H17 108.0 N1 C18 C19 107.23(14) N1 C18 C25 109.30(16) C19 C18 C25 113.17(16) N1 C18 H18 109.0 C19 C18 H18 109.0 C25 C18 H18 109.0 C14 C19 C18 113.11(15) C14 C19 H19A 109.0 C18 C19 H19A 109.0 C14 C19 H19B 109.0 C18 C19 H19B 109.0 H19A C19 H19B 107.8 C3 C20 H20A 109.5 C3 C20 H20B 109.5 H20A C20 H20B 109.5 C3 C20 H20C 109.5 H20A C20 H20C 109.5 H20B C20 H20C 109.5 O1 C21 H21A 109.5 O1 C21 H21B 109.5 H21A C21 H21B 109.5 O1 C21 H21C 109.5 H21A C21 H21C 109.5 H21B C21 H21C 109.5 O2 C22 H22A 109.5 O2 C22 H22B 109.5 H22A C22 H22B 109.5 O2 C22 H22C 109.5 H22A C22 H22C 109.5 H22B C22 H22C 109.5 O3 C23 H23A 109.5 O3 C23 H23B 109.5 H23A C23 H23B 109.5 O3 C23 H23C 109.5 H23A C23 H23C 109.5 H23B C23 H23C 109.5 C17 C24 H24A 109.5 C17 C24 H24B 109.5 H24A C24 H24B 109.5 C17 C24 H24C 109.5 H24A C24 H24C 109.5 H24B C24 H24C 109.5 C18 C25 H25A 109.5 C18 C25 H25B 109.5 H25A C25 H25B 109.5 C18 C25 H25C 109.5 H25A C25 H25C 109.5 H25B C25 H25C 109.5 C32 C31 C36 120.03(16) C32 C31 C40 120.00(16) C36 C31 C40 119.96(16) C33 C32 C31 121.24(17) C33 C32 H32 119.4 C31 C32 H32 119.4 C32 C33 C34 118.97(18) C32 C33 C50 121.69(18) C34 C33 C50 119.31(18) C35 C34 C33 121.80(18) C35 C34 H34 119.1 C33 C34 H34 119.1 O6 C35 C34 122.74(17) O6 C35 C36 116.93(16) C34 C35 C36 120.27(17) C31 C36 C37 118.38(16) C31 C36 C35 117.21(16) C37 C36 C35 124.38(16) O5 C37 C38 122.62(16) O5 C37 C36 117.41(16) C38 C37 C36 119.97(16) C37 C38 C39 120.40(17) C37 C38 H38 119.8 C39 C38 H38 119.8 C40 C39 C38 121.91(17) C40 C39 H39 119.0 C38 C39 H39 119.0 C39 C40 C31 118.82(16) C39 C40 C41 119.70(16) C31 C40 C41 121.45(16) C46 C41 C42 117.34(16) C46 C41 C40 122.78(16) C42 C41 C40 119.88(16) O8 C42 C43 116.34(16) O8 C42 C41 122.39(16) C43 C42 C41 121.25(17) C42 C43 C44 120.69(17) C42 C43 H43 119.7 C44 C43 H43 119.7 C43 C44 C45 119.33(16) C43 C44 C49 119.12(16) C45 C44 C49 121.50(16) C44 C45 C46 119.36(16) C44 C45 C47 121.56(16) C46 C45 C47 119.04(16) O7 C46 C41 121.50(16) O7 C46 C45 116.33(16) C41 C46 C45 122.02(16) N2 C47 C45 109.03(15) N2 C47 C54 109.80(15) C45 C47 C54 112.28(16) N2 C47 H47 108.5 C45 C47 H47 108.5 C54 C47 H47 108.5 N2 C48 C55 107.89(15) N2 C48 C49 107.64(14) C55 C48 C49 113.05(16) N2 C48 H48 109.4 C55 C48 H48 109.4 C49 C48 H48 109.4 C44 C49 C48 114.40(15) C44 C49 H49A 108.7 C48 C49 H49A 108.7 C44 C49 H49B 108.7 C48 C49 H49B 108.7 H49A C49 H49B 107.6 C33 C50 H50A 109.5 C33 C50 H50B 109.5 H50A C50 H50B 109.5 C33 C50 H50C 109.5 H50A C50 H50C 109.5 H50B C50 H50C 109.5 O6 C51 H51A 109.5 O6 C51 H51B 109.5 H51A C51 H51B 109.5 O6 C51 H51C 109.5 H51A C51 H51C 109.5 H51B C51 H51C 109.5 O5 C52 H52A 109.5 O5 C52 H52B 109.5 H52A C52 H52B 109.5 O5 C52 H52C 109.5 H52A C52 H52C 109.5 H52B C52 H52C 109.5 O7 C53 H53A 109.5 O7 C53 H53B 109.5 H53A C53 H53B 109.5 O7 C53 H53C 109.5 H53A C53 H53C 109.5 H53B C53 H53C 109.5 C47 C54 H54A 109.5 C47 C54 H54B 109.5 H54A C54 H54B 109.5 C47 C54 H54C 109.5 H54A C54 H54C 109.5 H54B C54 H54C 109.5 C48 C55 H55A 109.5 C48 C55 H55B 109.5 H55A C55 H55B 109.5 C48 C55 H55C 109.5 H55A C55 H55C 109.5 H55B C55 H55C 109.5 C102 C101 H10A 109.5 C102 C101 H10B 109.5 H10A C101 H10B 109.5 C102 C101 H10C 109.5 H10A C101 H10C 109.5 H10B C101 H10C 109.5 O11 C102 C101 121.5(3) O11 C102 C103 121.6(3) C101 C102 C103 116.8(2) C102 C103 H10D 109.5 C102 C103 H10E 109.5 H10D C103 H10E 109.5 C102 C103 H10F 109.5 H10D C103 H10F 109.5 H10E C103 H10F 109.5 F21 C201 F23 106.92(16) F21 C201 F22 107.27(17) F23 C201 F22 107.26(16) F21 C201 C202 113.21(16) F23 C201 C202 111.36(16) F22 C201 C202 110.53(15) O21 C202 O22 130.12(19) O21 C202 C201 115.21(18) O22 C202 C201 114.64(16) F33 C301 F31 107.7(2) F33 C301 F32 106.0(2) F31 C301 F32 106.8(2) F33 C301 C302 112.51(19) F31 C301 C302 113.33(18) F32 C301 C302 110.1(2) O32 C302 O31 128.41(19) O32 C302 C301 115.90(18) O31 C302 C301 115.68(17) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance F21 C201 1.330(2) F22 C201 1.340(2) F23 C201 1.338(2) F31 C301 1.323(3) F32 C301 1.340(3) F33 C301 1.314(3) O1 C5 1.375(2) O1 C21 1.434(2) O2 C7 1.366(2) O2 C22 1.427(3) O3 C12 1.388(2) O3 C23 1.438(3) O4 C16 1.365(2) O4 H4O 0.83(3) O5 C37 1.362(2) O5 C52 1.428(2) O6 C35 1.365(2) O6 C51 1.427(2) O7 C46 1.380(2) O7 C53 1.430(3) O8 C42 1.363(2) O8 H8O 0.85(3) O11 C102 1.219(3) O21 C202 1.232(3) O22 C202 1.248(2) O31 C302 1.237(2) O32 C302 1.235(3) N1 C17 1.501(2) N1 C18 1.502(3) N1 H1A 0.9100 N1 H1B 0.9100 N2 C47 1.500(2) N2 C48 1.504(2) N2 H2A 0.9100 N2 H2B 0.9100 C1 C2 1.422(3) C1 C10 1.430(3) C1 C6 1.435(2) C2 C3 1.366(3) C2 H2 0.9500 C3 C4 1.417(3) C3 C20 1.511(3) C4 C5 1.372(3) C4 H4 0.9500 C5 C6 1.441(3) C6 C7 1.437(3) C7 C8 1.375(3) C8 C9 1.408(3) C8 H8 0.9500 C9 C10 1.366(3) C9 H9 0.9500 C10 C11 1.496(2) C11 C12 1.399(2) C11 C16 1.401(3) C12 C13 1.398(2) C13 C14 1.397(3) C13 C17 1.517(2) C14 C15 1.392(3) C14 C19 1.514(2) C15 C16 1.387(3) C15 H15 0.9500 C17 C24 1.533(3) C17 H17 1.0000 C18 C19 1.518(2) C18 C25 1.524(3) C18 H18 1.0000 C19 H19A 0.9900 C19 H19B 0.9900 C20 H20A 0.9800 C20 H20B 0.9800 C20 H20C 0.9800 C21 H21A 0.9800 C21 H21B 0.9800 C21 H21C 0.9800 C22 H22A 0.9800 C22 H22B 0.9800 C22 H22C 0.9800 C23 H23A 0.9800 C23 H23B 0.9800 C23 H23C 0.9800 C24 H24A 0.9800 C24 H24B 0.9800 C24 H24C 0.9800 C25 H25A 0.9800 C25 H25B 0.9800 C25 H25C 0.9800 C31 C32 1.420(2) C31 C36 1.428(2) C31 C40 1.430(2) C32 C33 1.368(3) C32 H32 0.9500 C33 C34 1.412(3) C33 C50 1.514(3) C34 C35 1.375(3) C34 H34 0.9500 C35 C36 1.438(3) C36 C37 1.434(2) C37 C38 1.375(3) C38 C39 1.406(3) C38 H38 0.9500 C39 C40 1.370(3) C39 H39 0.9500 C40 C41 1.493(2) C41 C46 1.396(3) C41 C42 1.404(3) C42 C43 1.389(2) C43 C44 1.389(3) C43 H43 0.9500 C44 C45 1.399(3) C44 C49 1.519(2) C45 C46 1.400(2) C45 C47 1.510(2) C47 C54 1.538(3) C47 H47 1.0000 C48 C55 1.521(3) C48 C49 1.523(2) C48 H48 1.0000 C49 H49A 0.9900 C49 H49B 0.9900 C50 H50A 0.9800 C50 H50B 0.9800 C50 H50C 0.9800 C51 H51A 0.9800 C51 H51B 0.9800 C51 H51C 0.9800 C52 H52A 0.9800 C52 H52B 0.9800 C52 H52C 0.9800 C53 H53A 0.9800 C53 H53B 0.9800 C53 H53C 0.9800 C54 H54A 0.9800 C54 H54B 0.9800 C54 H54C 0.9800 C55 H55A 0.9800 C55 H55B 0.9800 C55 H55C 0.9800 C101 C102 1.493(4) C101 H10A 0.9800 C101 H10B 0.9800 C101 H10C 0.9800 C102 C103 1.494(4) C103 H10D 0.9800 C103 H10E 0.9800 C103 H10F 0.9800 C201 C202 1.549(3) C301 C302 1.548(3) loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C10 C1 C2 C3 -177.41(17) C6 C1 C2 C3 1.1(3) C1 C2 C3 C4 1.1(3) C1 C2 C3 C20 -177.58(18) C2 C3 C4 C5 -2.4(3) C20 C3 C4 C5 176.33(19) C3 C4 C5 O1 -178.84(17) C3 C4 C5 C6 1.3(3) C21 O1 C5 C4 -11.5(3) C21 O1 C5 C6 168.38(16) C2 C1 C6 C7 179.63(17) C10 C1 C6 C7 -1.8(2) C2 C1 C6 C5 -2.1(2) C10 C1 C6 C5 176.40(17) C4 C5 C6 C1 0.9(3) O1 C5 C6 C1 -178.89(15) C4 C5 C6 C7 179.00(18) O1 C5 C6 C7 -0.8(3) C22 O2 C7 C8 -1.0(3) C22 O2 C7 C6 179.3(2) C1 C6 C7 O2 -176.93(17) C5 C6 C7 O2 5.0(3) C1 C6 C7 C8 3.4(3) C5 C6 C7 C8 -174.62(19) O2 C7 C8 C9 178.43(18) C6 C7 C8 C9 -1.9(3) C7 C8 C9 C10 -1.3(3) C8 C9 C10 C1 2.9(3) C8 C9 C10 C11 -177.20(18) C2 C1 C10 C9 177.26(17) C6 C1 C10 C9 -1.3(3) C2 C1 C10 C11 -2.6(3) C6 C1 C10 C11 178.84(16) C9 C10 C11 C12 -72.6(2) C1 C10 C11 C12 107.3(2) C9 C10 C11 C16 106.9(2) C1 C10 C11 C16 -73.2(2) C23 O3 C12 C13 96.4(2) C23 O3 C12 C11 -82.9(2) C16 C11 C12 O3 179.47(16) C10 C11 C12 O3 -1.0(3) C16 C11 C12 C13 0.2(3) C10 C11 C12 C13 179.70(17) O3 C12 C13 C14 -178.25(16) C11 C12 C13 C14 1.0(3) O3 C12 C13 C17 1.7(2) C11 C12 C13 C17 -179.03(17) C12 C13 C14 C15 -1.7(3) C17 C13 C14 C15 178.38(17) C12 C13 C14 C19 173.97(17) C17 C13 C14 C19 -6.0(3) C13 C14 C15 C16 1.1(3) C19 C14 C15 C16 -174.62(17) C14 C15 C16 O4 179.63(17) C14 C15 C16 C11 0.2(3) C12 C11 C16 O4 179.69(16) C10 C11 C16 O4 0.2(3) C12 C11 C16 C15 -0.8(3) C10 C11 C16 C15 179.70(17) C18 N1 C17 C13 -51.07(19) C18 N1 C17 C24 73.94(19) C14 C13 C17 N1 19.9(2) C12 C13 C17 N1 -160.08(16) C14 C13 C17 C24 -103.6(2) C12 C13 C17 C24 76.4(2) C17 N1 C18 C19 66.48(19) C17 N1 C18 C25 -170.49(15) C15 C14 C19 C18 -163.86(17) C13 C14 C19 C18 20.5(2) N1 C18 C19 C14 -47.6(2) C25 C18 C19 C14 -168.24(17) C36 C31 C32 C33 -1.1(3) C40 C31 C32 C33 177.41(18) C31 C32 C33 C34 -3.3(3) C31 C32 C33 C50 178.4(2) C32 C33 C34 C35 2.0(3) C50 C33 C34 C35 -179.7(2) C51 O6 C35 C34 9.7(3) C51 O6 C35 C36 -167.43(17) C33 C34 C35 O6 -173.36(19) C33 C34 C35 C36 3.7(3) C32 C31 C36 C37 -175.16(17) C40 C31 C36 C37 6.3(3) C32 C31 C36 C35 6.5(3) C40 C31 C36 C35 -171.95(17) O6 C35 C36 C31 169.41(16) C34 C35 C36 C31 -7.8(3) O6 C35 C36 C37 -8.8(3) C34 C35 C36 C37 173.97(19) C52 O5 C37 C38 1.6(3) C52 O5 C37 C36 -177.86(17) C31 C36 C37 O5 171.59(16) C35 C36 C37 O5 -10.2(3) C31 C36 C37 C38 -7.8(3) C35 C36 C37 C38 170.32(19) O5 C37 C38 C39 -176.43(18) C36 C37 C38 C39 3.0(3) C37 C38 C39 C40 3.7(3) C38 C39 C40 C31 -5.2(3) C38 C39 C40 C41 176.77(17) C32 C31 C40 C39 -178.48(18) C36 C31 C40 C39 0.0(3) C32 C31 C40 C41 -0.4(3) C36 C31 C40 C41 178.05(16) C39 C40 C41 C46 -111.0(2) C31 C40 C41 C46 71.0(2) C39 C40 C41 C42 69.1(2) C31 C40 C41 C42 -108.9(2) C46 C41 C42 O8 -178.30(16) C40 C41 C42 O8 1.6(3) C46 C41 C42 C43 0.0(3) C40 C41 C42 C43 179.90(17) O8 C42 C43 C44 177.40(16) C41 C42 C43 C44 -1.0(3) C42 C43 C44 C45 1.2(3) C42 C43 C44 C49 -176.27(16) C43 C44 C45 C46 -0.5(3) C49 C44 C45 C46 176.98(16) C43 C44 C45 C47 177.15(17) C49 C44 C45 C47 -5.4(3) C53 O7 C46 C41 66.1(2) C53 O7 C46 C45 -118.29(19) C42 C41 C46 O7 176.10(16) C40 C41 C46 O7 -3.8(3) C42 C41 C46 C45 0.8(3) C40 C41 C46 C45 -179.11(17) C44 C45 C46 O7 -176.12(16) C47 C45 C46 O7 6.2(2) C44 C45 C46 C41 -0.5(3) C47 C45 C46 C41 -178.21(17) C48 N2 C47 C45 -55.4(2) C48 N2 C47 C54 68.0(2) C44 C45 C47 N2 24.3(2) C46 C45 C47 N2 -158.13(16) C44 C45 C47 C54 -97.7(2) C46 C45 C47 C54 80.0(2) C47 N2 C48 C55 -172.43(16) C47 N2 C48 C49 65.27(19) C43 C44 C49 C48 -167.81(16) C45 C44 C49 C48 14.8(2) N2 C48 C49 C44 -41.9(2) C55 C48 C49 C44 -160.99(16) F21 C201 C202 O21 -5.6(3) F23 C201 C202 O21 -126.1(2) F22 C201 C202 O21 114.7(2) F21 C201 C202 O22 176.11(16) F23 C201 C202 O22 55.6(2) F22 C201 C202 O22 -63.5(2) F33 C301 C302 O32 44.6(3) F31 C301 C302 O32 167.0(2) F32 C301 C302 O32 -73.4(3) F33 C301 C302 O31 -136.4(2) F31 C301 C302 O31 -14.0(3) F32 C301 C302 O31 105.6(2)