#------------------------------------------------------------------------------ #$Date: 2020-11-18 07:22:41 +0200 (Wed, 18 Nov 2020) $ #$Revision: 259164 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/55/95/1559529.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1559529 _cell_angle_alpha 90 _cell_angle_beta 99.070(4) _cell_angle_gamma 90 _cell_length_a 16.2976(8) _cell_length_b 6.1294(2) _cell_length_c 12.2221(6) _exptl_crystal_F_000 600 _reflns_d_resolution_high 0.8361 _cod_data_source_file sj4217Isup2.hkl _cod_data_source_block I _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 210.85 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 38.92 51.15 22.47 < 3 0 0 2787.39 2765.07 71.92 o 4 0 0 44745.80 44458.50 314.31 o 5 0 0 30512.50 29275.30 289.94 o 6 0 0 9955.82 9492.26 246.37 o 7 0 0 235.32 196.99 69.92 < 8 0 0 4723.68 4411.86 204.49 o 9 0 0 7931.56 7660.24 286.36 o 10 0 0 984.31 900.28 54.81 o 11 0 0 1520.54 1533.98 51.24 o 12 0 0 1768.68 1767.15 66.79 o 13 0 0 1114.50 1088.14 69.41 o 14 0 0 400.27 348.25 42.38 o 15 0 0 1.68 -19.84 35.12 < 16 0 0 28.44 24.03 26.41 < 17 0 0 53.07 58.95 30.72 < 18 0 0 297.52 310.86 34.66 o 19 0 0 319.24 309.85 28.01 o 1 1 0 147.77 214.68 19.94 o 2 1 0 394.80 490.94 29.43 o 3 1 0 12075.50 13449.30 168.77 o 4 1 0 14864.50 15358.20 195.44 o 5 1 0 6179.66 6255.35 142.54 o 6 1 0 3250.44 3060.13 100.30 o 7 1 0 108.15 40.16 35.32 < 8 1 0 715.08 632.08 66.35 o 9 1 0 8450.20 7984.34 142.71 o 10 1 0 8155.50 7970.33 73.53 o 11 1 0 453.24 423.33 32.43 o 12 1 0 622.76 614.90 34.00 o 13 1 0 4508.62 4577.23 70.31 o 14 1 0 2593.60 2718.17 43.94 o 15 1 0 2090.45 2173.39 41.51 o 16 1 0 10.86 13.94 17.60 < 17 1 0 1764.59 1853.72 44.56 o 18 1 0 959.18 1001.00 34.33 o 19 1 0 1119.81 1178.23 45.04 o 0 2 0 12098.40 13483.00 193.89 o 1 2 0 2223.63 2346.56 58.75 o 2 2 0 1.34 -8.00 22.33 < 3 2 0 3061.20 3184.75 85.79 o 4 2 0 5240.10 5335.62 128.31 o 5 2 0 5557.94 5901.07 166.15 o 6 2 0 326.13 399.70 61.56 o 7 2 0 7813.97 8299.22 162.76 o 8 2 0 4324.24 4159.44 81.16 o 9 2 0 1015.27 978.79 36.26 o 10 2 0 99.35 85.93 22.03 o 11 2 0 856.16 825.13 34.68 o 12 2 0 1981.39 1939.46 51.35 o 13 2 0 670.26 657.03 33.53 o 14 2 0 5.93 14.92 18.75 < 15 2 0 271.55 326.50 25.13 o 16 2 0 1006.63 1003.65 34.67 o 17 2 0 219.63 241.82 27.22 o 18 2 0 13.31 27.30 21.04 < 1 3 0 2718.96 2920.93 84.30 o 2 3 0 6076.35 6590.41 128.32 o 3 3 0 2568.89 2676.10 88.38 o 4 3 0 5.75 2.63 32.34 < 5 3 0 2343.31 2250.82 124.25 o 6 3 0 2399.74 2268.59 56.74 o 7 3 0 1780.15 1741.68 61.07 o 8 3 0 210.28 177.71 28.96 o 9 3 0 272.68 275.50 32.80 o 10 3 0 1477.19 1560.81 56.70 o 11 3 0 1347.11 1293.93 47.17 o 12 3 0 64.63 49.52 21.96 < 13 3 0 255.16 260.19 25.09 o 14 3 0 208.90 224.21 20.82 o 15 3 0 80.97 87.99 18.95 o 16 3 0 5.29 33.75 16.92 < 17 3 0 51.27 29.08 18.60 < 0 4 0 6.29 13.98 37.02 < 1 4 0 59.26 73.50 30.06 < 2 4 0 444.97 489.17 40.29 o 3 4 0 131.77 122.99 23.99 o 4 4 0 249.32 232.25 26.86 o 5 4 0 240.15 192.73 25.57 o 6 4 0 673.28 664.84 48.84 o 7 4 0 240.39 209.13 37.46 o 8 4 0 1263.93 1157.57 57.70 o 9 4 0 69.32 72.56 29.22 < 10 4 0 320.30 304.84 37.83 o 11 4 0 1026.92 1034.65 40.49 o 12 4 0 1029.15 1098.07 45.20 o 13 4 0 98.48 127.37 25.79 o 14 4 0 45.19 64.29 22.32 < 15 4 0 650.64 749.38 29.32 o 16 4 0 1097.72 1285.78 48.13 o 1 5 0 626.11 660.77 54.87 o 2 5 0 326.77 337.36 43.00 o 3 5 0 1072.75 1091.42 59.87 o 4 5 0 1924.20 2066.42 60.40 o 5 5 0 619.05 615.87 38.38 o 6 5 0 0.75 3.07 28.83 < 7 5 0 718.54 706.91 38.14 o 8 5 0 542.55 501.75 45.23 o 9 5 0 3.61 4.38 26.95 < 10 5 0 158.90 183.39 29.84 o 11 5 0 1.23 12.92 24.55 < 12 5 0 101.04 106.01 22.42 o 13 5 0 106.19 77.42 24.46 o 0 6 0 498.03 534.66 47.96 o 1 6 0 1.75 12.28 21.28 < 2 6 0 56.23 45.15 24.31 < 3 6 0 64.51 34.23 24.30 < 4 6 0 145.10 118.46 36.24 o 5 6 0 20.41 15.76 24.41 < 6 6 0 3.47 29.79 30.44 < 7 6 0 29.13 33.57 29.31 < 8 6 0 1.59 43.30 29.37 < 9 6 0 84.05 101.98 27.18 o 10 6 0 35.97 57.54 26.56 < 11 6 0 0.60 45.31 30.92 < 1 7 0 824.98 777.41 35.68 o 2 7 0 478.00 459.76 36.48 o 3 7 0 1330.35 1300.62 55.19 o 4 7 0 244.68 221.70 29.54 o 5 7 0 235.63 212.94 29.90 o -19 1 1 106.56 80.47 22.01 o -18 1 1 60.42 66.37 18.43 o -17 1 1 109.20 97.90 19.63 o -16 1 1 285.56 285.47 23.35 o -15 1 1 459.81 438.28 30.43 o -14 1 1 558.12 597.95 35.82 o -13 1 1 26.48 21.06 25.90 < -12 1 1 333.02 274.64 25.99 o -11 1 1 1035.90 932.75 28.34 o -10 1 1 3192.95 3080.86 43.60 o -9 1 1 3.82 21.25 25.09 < -8 1 1 793.99 808.82 80.29 o -7 1 1 104.82 62.05 57.98 < -6 1 1 1981.28 1946.18 86.08 o -5 1 1 64.00 86.90 36.40 < -4 1 1 54.44 58.95 25.00 < -3 1 1 933.76 952.84 34.33 o -2 1 1 1376.96 1594.79 42.00 o -1 1 1 298.51 379.77 33.21 o 0 1 1 877.48 1015.53 35.04 o 1 1 1 255.01 304.96 25.98 o 2 1 1 1363.45 1560.45 51.77 o 3 1 1 941.34 1085.15 66.61 o 4 1 1 13915.70 14465.70 221.21 o 5 1 1 262.24 256.08 49.82 o 6 1 1 4.98 9.27 39.49 < 7 1 1 29.20 39.93 38.46 < 8 1 1 517.83 529.55 55.30 o 9 1 1 11.60 6.92 22.72 < 10 1 1 2.96 -18.23 20.42 < 11 1 1 10.56 -18.50 20.88 < 12 1 1 124.05 105.36 20.07 o 13 1 1 111.44 125.32 19.99 o 14 1 1 9.36 10.49 18.38 < 15 1 1 2.80 5.04 16.45 < 16 1 1 434.51 460.97 26.06 o 17 1 1 170.22 178.10 20.79 o 18 1 1 24.86 27.89 18.67 < -18 2 1 79.60 49.49 23.77 < -17 2 1 595.54 623.03 31.95 o -16 2 1 221.03 255.07 31.30 o -15 2 1 46.14 49.03 23.54 < -14 2 1 47.50 -1.07 28.62 < -13 2 1 77.75 80.38 23.54 o -12 2 1 105.07 107.39 23.53 o -11 2 1 1.21 6.47 20.92 < -10 2 1 161.68 157.12 22.38 o -9 2 1 4.42 3.27 20.56 < -8 2 1 32.92 14.70 37.65 < -7 2 1 55.93 38.89 63.97 < -6 2 1 2994.53 3343.37 135.55 o -5 2 1 1338.72 1369.03 77.08 o -4 2 1 372.81 405.30 36.23 o -3 2 1 985.06 933.34 46.23 o -2 2 1 10585.70 11321.00 160.07 o -1 2 1 4053.31 4325.97 92.67 o 0 2 1 1048.13 1165.26 40.21 o 1 2 1 4648.56 5162.44 92.80 o 2 2 1 7083.94 7477.68 120.48 o 3 2 1 9145.29 9620.88 187.51 o 4 2 1 588.10 571.32 62.32 o 5 2 1 78.14 107.30 42.57 < 6 2 1 2736.55 2698.68 111.81 o 7 2 1 12795.10 12724.10 172.95 o 8 2 1 309.88 261.23 25.81 o 9 2 1 228.60 220.20 20.89 o 10 2 1 697.38 595.98 29.99 o 11 2 1 2211.14 2060.71 56.74 o 12 2 1 1378.72 1348.82 45.53 o 13 2 1 21.93 35.13 21.65 < 14 2 1 83.25 89.39 20.92 o 15 2 1 266.49 263.00 22.77 o 16 2 1 129.21 126.48 20.04 o 17 2 1 31.28 2.68 20.06 < 18 2 1 60.49 72.07 21.56 o -17 3 1 88.55 74.53 26.12 < -16 3 1 670.87 813.28 28.06 o -15 3 1 1189.69 1319.56 34.92 o -14 3 1 1197.36 1095.58 36.60 o -13 3 1 554.72 569.73 27.76 o -12 3 1 1227.89 1209.57 34.33 o -11 3 1 2347.30 2313.25 55.52 o -10 3 1 2145.53 1992.22 62.02 o -9 3 1 2.34 2.49 24.07 < -8 3 1 1517.60 1425.63 54.39 o -7 3 1 3875.31 3732.35 78.96 o -6 3 1 4666.21 4759.96 81.61 o -5 3 1 257.40 219.42 54.35 o -4 3 1 1723.16 1696.16 91.83 o -3 3 1 7565.48 8203.61 168.72 o -2 3 1 1224.71 1179.22 59.79 o -1 3 1 16.45 26.82 29.14 < 0 3 1 854.35 873.27 63.67 o 1 3 1 2790.94 2990.28 105.88 o 2 3 1 522.03 492.31 45.57 o 3 3 1 2.98 18.04 28.85 < 4 3 1 2251.75 2152.19 91.10 o 5 3 1 704.57 649.87 53.81 o 6 3 1 360.41 318.13 28.55 o 7 3 1 422.96 404.19 30.11 o 8 3 1 889.59 834.90 45.58 o 9 3 1 3282.16 3137.21 84.58 o 10 3 1 138.57 150.21 26.92 o 11 3 1 1842.02 1878.81 44.99 o 12 3 1 802.86 771.49 35.40 o 13 3 1 1270.93 1347.22 40.39 o 14 3 1 35.72 34.70 21.88 < 15 3 1 176.93 193.16 20.49 o 16 3 1 859.86 914.11 29.35 o 17 3 1 473.14 303.83 31.71 o -15 4 1 25.84 22.82 22.49 < -14 4 1 676.09 678.03 33.30 o -13 4 1 1506.26 1621.49 43.99 o -12 4 1 270.05 262.54 26.84 o -11 4 1 146.20 155.29 28.09 o -10 4 1 3250.88 3247.40 62.57 o -9 4 1 4325.58 4273.78 74.61 o -8 4 1 2120.28 2042.35 75.23 o -7 4 1 605.89 572.08 41.52 o -6 4 1 6329.31 6069.06 120.24 o -5 4 1 4663.92 4383.44 78.92 o -4 4 1 3936.07 4014.23 76.31 o -3 4 1 184.78 222.55 29.02 o -2 4 1 3861.45 4109.31 90.53 o -1 4 1 7877.89 8288.48 123.94 o 0 4 1 4884.07 5315.13 110.45 o 1 4 1 151.38 165.06 28.75 o 2 4 1 1585.74 1641.16 81.32 o 3 4 1 3686.61 3767.40 99.24 o 4 4 1 2189.44 2240.48 81.17 o 5 4 1 217.44 202.72 31.81 o 6 4 1 3202.16 3038.57 87.60 o 7 4 1 1080.27 1042.78 60.27 o 8 4 1 33.12 24.73 32.93 < 9 4 1 31.96 22.41 26.51 < 10 4 1 1236.71 1193.50 49.77 o 11 4 1 688.10 675.65 39.02 o 12 4 1 76.56 112.42 26.33 o 13 4 1 336.68 362.99 29.85 o 14 4 1 982.36 1059.81 33.84 o 15 4 1 846.61 921.38 29.86 o -14 5 1 1124.95 1194.34 48.82 o -13 5 1 163.13 167.59 21.04 o -12 5 1 49.89 85.37 26.78 o -11 5 1 1001.72 1071.27 45.99 o -10 5 1 643.00 668.29 38.48 o -9 5 1 74.33 62.44 31.89 < -8 5 1 177.01 166.61 32.03 o -7 5 1 605.80 620.01 41.44 o -6 5 1 365.64 365.09 40.17 o -5 5 1 303.62 324.25 36.97 o -4 5 1 3794.44 4008.22 80.37 o -3 5 1 1078.74 1189.67 59.29 o -2 5 1 6.69 40.25 27.80 < -1 5 1 1142.80 1242.77 55.88 o 0 5 1 5062.52 5568.03 164.57 o 1 5 1 4174.63 4460.44 118.02 o 2 5 1 1970.90 2022.72 87.14 o 3 5 1 4085.04 4377.62 123.17 o 4 5 1 7399.31 7845.98 163.84 o 5 5 1 3753.14 3834.60 118.28 o 6 5 1 2597.20 2626.73 82.05 o 7 5 1 375.71 366.38 32.23 o 8 5 1 4708.86 4643.81 74.96 o 9 5 1 5491.17 5714.11 100.67 o 10 5 1 1223.85 1240.73 42.00 o 11 5 1 3.97 20.36 21.44 < 12 5 1 1041.33 1117.49 33.11 o 13 5 1 1687.56 1883.47 38.39 o -11 6 1 0.49 13.74 20.86 < -10 6 1 1573.07 1526.01 50.04 o -9 6 1 3326.19 3404.62 66.62 o -8 6 1 1622.65 1579.76 59.45 o -7 6 1 3.01 15.95 29.86 < -6 6 1 1757.53 1769.94 65.04 o -5 6 1 4311.21 4131.93 118.14 o -4 6 1 2070.13 2234.38 128.42 o -3 6 1 193.20 199.68 30.07 o -2 6 1 876.20 894.99 48.06 o -1 6 1 8889.24 9219.79 117.19 o 0 6 1 214.12 219.06 27.11 o 1 6 1 2.87 2.34 20.86 < 2 6 1 26.67 42.86 26.52 < 3 6 1 2674.16 2745.75 97.56 o 4 6 1 923.75 828.31 59.51 o 5 6 1 42.86 53.69 33.53 < 6 6 1 858.79 812.98 46.87 o 7 6 1 667.92 719.57 53.77 o 8 6 1 233.62 223.96 32.59 o 9 6 1 108.45 99.67 26.97 o 10 6 1 320.66 294.80 31.68 o -5 7 1 20.53 3.19 31.49 < -4 7 1 1559.68 1578.06 86.52 o -3 7 1 897.48 862.09 67.77 o -2 7 1 121.34 116.88 39.73 < -1 7 1 158.12 179.95 42.45 o 0 7 1 1009.91 988.78 49.04 o 1 7 1 1595.50 1530.65 48.24 o 2 7 1 1396.19 1378.37 47.01 o 3 7 1 1425.34 1379.81 46.82 o 4 7 1 1124.02 1030.41 51.13 o 5 7 1 1210.56 1159.19 75.59 o -19 0 2 1539.53 1664.15 55.10 o -18 0 2 1668.49 1897.39 69.19 o -17 0 2 497.52 511.23 66.57 o -16 0 2 335.80 213.31 52.09 o -15 0 2 2758.47 2811.68 120.87 o -14 0 2 3948.84 3848.33 105.58 o -13 0 2 1314.64 1233.20 75.11 o -12 0 2 170.98 158.59 32.45 o -11 0 2 3211.85 3019.80 86.50 o -10 0 2 11419.50 11587.70 150.16 o -9 0 2 5208.60 5143.87 237.94 o -8 0 2 619.39 579.68 96.28 o -7 0 2 4696.49 4691.09 199.20 o -6 0 2 9723.07 9623.46 253.95 o -5 0 2 9975.19 9640.39 288.09 o -4 0 2 91.42 69.36 53.45 < -3 0 2 902.40 932.72 79.79 o -2 0 2 11151.40 12154.20 253.97 o -1 0 2 2612.70 2747.95 62.49 o 0 0 2 128.60 153.91 37.90 o 1 0 2 2347.36 2055.57 103.47 o 2 0 2 6928.55 7133.69 202.47 o 3 0 2 82.82 98.70 65.47 < 4 0 2 3127.39 3275.92 193.57 o 5 0 2 18017.60 18302.70 495.41 o 6 0 2 1775.91 1536.26 178.83 o 7 0 2 144.75 144.07 96.11 < 8 0 2 7191.55 6866.75 377.58 o 9 0 2 10008.90 9793.19 260.31 o 10 0 2 5855.86 5797.98 102.52 o 11 0 2 94.32 127.81 27.70 o 12 0 2 3458.88 3534.53 84.48 o 13 0 2 3667.86 3652.57 76.95 o 14 0 2 3912.66 4083.14 94.21 o 15 0 2 838.12 919.26 50.42 o 16 0 2 61.54 55.52 26.46 < 17 0 2 1675.45 1760.41 55.12 o 18 0 2 1920.87 2048.10 61.99 o -19 1 2 65.67 37.30 21.06 < -18 1 2 0.41 -11.48 16.07 < -17 1 2 197.80 202.26 25.46 o -16 1 2 809.79 862.95 47.02 o -15 1 2 164.47 159.55 31.96 o -14 1 2 180.85 159.07 49.59 o -13 1 2 1605.86 1531.41 51.19 o -12 1 2 2046.38 1978.39 47.07 o -11 1 2 246.40 225.54 20.08 o -10 1 2 2027.91 2029.95 37.48 o -9 1 2 1649.22 1469.08 47.43 o -8 1 2 7246.44 7347.34 255.01 o -7 1 2 1113.74 1080.54 99.63 o -6 1 2 4767.78 4892.94 154.33 o -5 1 2 8369.08 8804.72 144.02 o -4 1 2 11127.30 11526.50 133.27 o -3 1 2 851.80 947.22 43.60 o -2 1 2 2341.66 2440.48 75.75 o -1 1 2 17265.60 17880.50 185.37 o 0 1 2 16070.90 17478.10 193.67 o 1 1 2 13427.90 14446.20 100.90 o 2 1 2 17373.50 17844.80 176.32 o 3 1 2 8768.17 8650.53 130.30 o 4 1 2 5855.94 5519.15 191.44 o 5 1 2 9543.44 9801.36 177.25 o 6 1 2 955.65 845.24 57.62 o 7 1 2 5765.62 5466.37 144.18 o 8 1 2 6562.35 6454.94 140.62 o 9 1 2 871.54 764.17 39.12 o 10 1 2 35.23 9.95 20.84 < 11 1 2 1451.43 1389.63 43.13 o 12 1 2 1086.45 1049.63 34.35 o 13 1 2 568.98 572.23 27.20 o 14 1 2 134.87 139.97 20.14 o 15 1 2 914.13 953.04 32.86 o 16 1 2 90.02 84.85 18.75 o 17 1 2 1.10 -10.14 16.31 < 18 1 2 162.37 146.57 25.32 o -18 2 2 367.62 338.73 26.13 o -17 2 2 18.31 22.88 21.95 < -16 2 2 0.57 5.44 25.34 < -15 2 2 668.29 630.51 46.79 o -14 2 2 1530.37 1583.15 43.82 o -13 2 2 126.64 145.26 25.76 o -12 2 2 167.97 143.40 24.62 o -11 2 2 3656.95 4108.52 63.28 o -10 2 2 2908.99 2781.81 57.66 o -9 2 2 42.90 36.96 16.66 < -8 2 2 688.40 620.09 42.41 o -7 2 2 7677.69 7695.84 200.92 o -6 2 2 2616.34 2393.62 155.87 o -5 2 2 3329.04 3437.83 115.86 o -4 2 2 168.11 159.28 34.90 o -3 2 2 12241.60 13110.00 162.88 o -2 2 2 13868.60 14607.60 171.67 o -1 2 2 5721.61 6140.54 130.20 o 0 2 2 995.29 1108.40 53.26 o 1 2 2 8320.65 9047.20 116.06 o 2 2 2 6946.50 7240.57 117.94 o 3 2 2 3365.42 3522.86 103.41 o 4 2 2 197.07 195.48 48.20 o 5 2 2 8951.32 9392.89 196.76 o 6 2 2 742.92 602.50 62.96 o 7 2 2 76.69 55.74 18.56 o 8 2 2 748.04 712.82 27.08 o 9 2 2 2313.31 2195.52 48.57 o 10 2 2 1352.66 1299.55 40.98 o 11 2 2 144.87 144.89 26.42 o 12 2 2 272.61 248.92 23.80 o 13 2 2 1978.84 2190.99 41.93 o 14 2 2 287.07 295.27 25.47 o 15 2 2 22.44 54.29 21.32 < 16 2 2 89.77 94.29 21.57 o 17 2 2 856.72 936.93 47.20 o -17 3 2 354.65 377.96 32.86 o -16 3 2 1176.93 1197.05 33.25 o -15 3 2 1234.84 1259.61 46.51 o -14 3 2 16.79 17.07 21.56 < -13 3 2 111.10 117.45 23.45 o -12 3 2 502.74 518.95 28.26 o -11 3 2 2144.64 2079.11 54.49 o -10 3 2 91.73 86.50 26.23 o -9 3 2 126.83 101.89 25.26 o -8 3 2 827.82 733.47 40.05 o -7 3 2 567.39 534.77 30.01 o -6 3 2 25.44 26.74 15.50 < -5 3 2 553.26 582.02 39.67 o -4 3 2 1422.20 1559.25 105.59 o -3 3 2 576.05 714.57 55.94 o -2 3 2 873.34 869.22 58.34 o -1 3 2 384.22 335.89 49.07 o 0 3 2 2370.76 2622.42 110.20 o 1 3 2 24.41 12.57 33.98 < 2 3 2 2075.46 2274.70 92.45 o 3 3 2 4136.00 4303.25 130.79 o 4 3 2 1294.71 1283.62 79.81 o 5 3 2 104.32 69.30 29.55 < 6 3 2 1800.71 1641.58 63.72 o 7 3 2 2790.52 2586.64 69.42 o 8 3 2 4466.17 4309.02 81.39 o 9 3 2 55.71 62.34 29.34 < 10 3 2 3100.07 3036.85 70.14 o 11 3 2 440.73 434.94 31.04 o 12 3 2 1771.46 1810.40 53.00 o 13 3 2 686.86 669.92 32.23 o 14 3 2 314.64 333.81 22.64 o 15 3 2 802.55 904.13 30.63 o 16 3 2 736.98 758.20 31.11 o -16 4 2 258.30 755.97 46.79 o -15 4 2 0.49 26.30 24.89 < -14 4 2 0.08 -3.23 27.02 < -13 4 2 45.33 54.05 23.37 < -12 4 2 607.09 589.97 35.40 o -11 4 2 1175.93 1113.08 39.85 o -10 4 2 150.96 174.49 24.32 o -9 4 2 4.13 4.41 21.30 < -8 4 2 411.73 355.28 35.55 o -7 4 2 4026.11 3943.31 88.82 o -6 4 2 2274.49 2196.76 67.42 o -5 4 2 9.56 6.45 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