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Information card for entry 1561547
Preview
| Coordinates | 1561547.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C52.5 H100 B Ge9 K N2 O Si8 |
|---|---|
| Calculated formula | C52.5 H100 B Ge9 K N2 O Si8 |
| Title of publication | FLP-type Nitrile Activation and Cyclic Ether Ring Opening by Halo-Borane Nonagermanide-Cluster Lewis Acid-Base-Pairs |
| Authors of publication | Wallach, Chistoph; Geitner, Felix; Fässler, Thomas F |
| Journal of publication | Chemical Science |
| Year of publication | 2021 |
| a | 14.7094 ± 0.0007 Å |
| b | 16.9327 ± 0.0006 Å |
| c | 18.7377 ± 0.0009 Å |
| α | 65.966 ± 0.003° |
| β | 67.528 ± 0.004° |
| γ | 88.951 ± 0.003° |
| Cell volume | 3886.2 ± 0.3 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 8 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0836 |
| Residual factor for significantly intense reflections | 0.0435 |
| Weighted residual factors for significantly intense reflections | 0.088 |
| Weighted residual factors for all reflections included in the refinement | 0.1113 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.114 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 263958 (current) | 2021-04-08 | cif/ Adding structures of 1561547, 1561548, 1561549, 1561550 via cif-deposit CGI script. |
1561547.cif |
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Users of the data should acknowledge the original authors of the
structural data.