#------------------------------------------------------------------------------ #$Date: 2021-04-24 02:19:36 +0300 (Sat, 24 Apr 2021) $ #$Revision: 264492 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/20/1562051.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1562051 loop_ _publ_author_name 'Kamilya, Sujit' 'Ghosh, Subrata' 'Mehta, Sakshi' 'Mondal, Abhishake' _publ_section_title ; Effect of Ligand Modulation on Metal-to-Metal Electron Transfer in a Series of [Fe2Co2] Molecular Square Complexes ; _journal_name_full 'The Journal of Physical Chemistry A' _journal_paper_doi 10.1021/acs.jpca.1c02032 _journal_year 2021 _chemical_formula_moiety 'C80 H84 B2 Co2 Fe2 N34 O4, 2(C3 H7 N O), 2(B F4)' _chemical_formula_sum 'C86 H98 B4 Co2 F8 Fe2 N36 O6' _chemical_formula_weight 2156.80 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_date 2021-02-18 _audit_creation_method ; Olex2 1.3 (compiled 2020.07.31 svn.rc2a77460 for OlexSys, GUI svn.r6145) ; _cell_angle_alpha 75.022(2) _cell_angle_beta 80.773(2) _cell_angle_gamma 84.036(2) _cell_formula_units_Z 1 _cell_length_a 13.2668(4) _cell_length_b 13.3671(4) _cell_length_c 16.9340(5) _cell_measurement_reflns_used 4797 _cell_measurement_temperature 120(2) _cell_measurement_theta_max 24.20 _cell_measurement_theta_min 2.25 _cell_volume 2857.34(15) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 120(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1960 _diffrn_reflns_av_unetI/netI 0.2117 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_number 116823 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.572 _diffrn_reflns_theta_min 1.558 _diffrn_source 'sealed tube' _exptl_absorpt_coefficient_mu 0.609 _exptl_absorpt_correction_T_max 0.786 _exptl_absorpt_correction_T_min 0.684 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS _exptl_crystal_colour red _exptl_crystal_density_diffrn 1.253 _exptl_crystal_description parallelepiped _exptl_crystal_F_000 1112 _exptl_crystal_size_max 0.47 _exptl_crystal_size_mid 0.29 _exptl_crystal_size_min 0.18 _refine_diff_density_max 0.791 _refine_diff_density_min -0.645 _refine_diff_density_rms 0.096 _refine_ls_extinction_coef 0.0112(12) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 0.944 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 653 _refine_ls_number_reflns 17416 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.944 _refine_ls_R_factor_all 0.2293 _refine_ls_R_factor_gt 0.0870 _refine_ls_shift/su_max 0.968 _refine_ls_shift/su_mean 0.002 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1231P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2044 _refine_ls_wR_factor_ref 0.2695 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6168 _reflns_number_total 17416 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file jp1c02032_si_007.cif _cod_data_source_block Complex3_120K _cod_database_code 1562051 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All B(H) groups, All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: B1(H1) 2.b Me refined with riding coordinates: C8(H8A,H8B,H8C), C7(H7A,H7B,H7C), C12(H12A,H12B,H12C), C13(H13A,H13B,H13C), C17(H17A,H17B,H17C) 2.c Aromatic/amide H refined with riding coordinates: C24(H24), C25(H25), C28(H28), C26(H26), C20(H20), C19(H19), C30(H30), C31(H31), C39(H39), C36(H36), C35(H35), C37(H37), C5(H5), C10(H10), C15(H15), C43(H43) 2.d X=CH2 refined with riding coordinates: C29(H29A,H29B), C27(H27A,H27B), C40(H40A,H40B), C38(H38A,H38B) 2.e Idealised Me refined as rotating group: C42(H42A,H42B,H42C), C41(H41A,H41B,H41C), C18(H18A,H18B,H18C) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL Test_1_a.res in P-1 test_1_a.res created by SHELXL-2018/3 at 14:48:30 on 18-Feb-2021 CELL 0.71073 13.2668 13.3671 16.934 75.022 80.773 84.036 ZERR 1 0.0004 0.0004 0.0005 0.002 0.002 0.002 LATT 1 SFAC C H B Co F Fe N O UNIT 86 98 4 2 8 2 36 6 L.S. 50 PLAN 5 TEMP 23 CONF MORE -1 BOND $H ABIN fmap 2 acta MERG 2 REM REM REM WGHT 0.123100 EXTI 0.011156 FVAR 0.43415 CO1 4 0.704461 0.799355 0.507436 11.00000 0.02821 0.03617 = 0.04828 -0.00997 -0.00400 -0.00250 FE1 6 0.612080 1.106692 0.625673 11.00000 0.02880 0.03422 = 0.05607 -0.00984 -0.00036 -0.00580 O1 8 0.781756 0.770544 0.764743 11.00000 0.04952 0.09354 = 0.07175 -0.03473 -0.00353 -0.01998 C29 1 1.096059 0.741296 0.709026 11.00000 0.04586 0.06522 = 0.09225 -0.03301 -0.01139 -0.00431 AFIX 93 H29A 2 1.140679 0.751109 0.659757 11.00000 -1.20000 H29B 2 1.121352 0.732380 0.758705 11.00000 -1.20000 AFIX 0 C27 1 0.556160 0.612111 0.898253 11.00000 0.16809 0.21422 = 0.09679 0.02619 -0.04558 -0.13149 AFIX 93 H27A 2 0.498269 0.583550 0.891107 11.00000 -1.20000 H27B 2 0.572442 0.604115 0.951041 11.00000 -1.20000 AFIX 0 O4 8 0.712742 0.763781 0.244690 11.00000 0.07108 0.06104 = 0.07078 -0.01892 -0.01727 -0.00501 N1 7 0.681223 0.926238 0.547287 11.00000 0.02554 0.03563 = 0.03770 -0.00929 -0.00388 -0.00085 N2 7 0.746682 1.248914 0.485768 11.00000 0.04418 0.04421 = 0.09603 -0.00740 0.01835 -0.00617 N10 7 0.639791 0.720719 0.619323 11.00000 0.03384 0.04457 = 0.06081 -0.01892 -0.00626 -0.00371 N12 7 0.836628 0.767917 0.552040 11.00000 0.03441 0.05658 = 0.04849 -0.01349 0.00071 -0.01161 N11 7 0.599371 0.679978 0.756119 11.00000 0.03685 0.06816 = 0.05735 -0.02009 0.00108 -0.01455 N14 7 0.768743 0.881839 0.397482 11.00000 0.03241 0.03339 = 0.05936 -0.01022 -0.00732 -0.00247 N15 7 0.809975 0.938438 0.263481 11.00000 0.04506 0.05107 = 0.04728 -0.00439 -0.00169 0.00124 N16 7 0.733133 0.675769 0.460934 11.00000 0.03269 0.04257 = 0.07183 -0.00736 0.00036 -0.00847 N8 7 0.520902 1.011755 0.711784 11.00000 0.03523 0.03313 = 0.03793 -0.00677 -0.00150 -0.00231 N5 7 0.562487 1.195117 0.769467 11.00000 0.04002 0.05741 = 0.05580 -0.02067 -0.00520 -0.00400 N4 7 0.567714 1.219715 0.684459 11.00000 0.03527 0.04298 = 0.05161 -0.01330 -0.00411 -0.00282 N6 7 0.725594 1.061713 0.695605 11.00000 0.03592 0.04247 = 0.06104 -0.02099 -0.01046 0.00006 N3 7 0.428240 1.176692 0.532743 11.00000 0.03508 0.03286 = 0.03928 -0.00857 -0.00521 -0.00018 N18 7 0.882889 0.702666 -0.001927 11.00000 0.12326 0.10950 = 0.13307 -0.05591 0.00224 -0.00773 C42 1 0.906459 0.632923 -0.057040 11.00000 0.19175 0.17971 = 0.12375 -0.06549 0.01108 -0.05811 AFIX 137 H42A 2 0.976530 0.637774 -0.082249 11.00000 -1.50000 H42B 2 0.862479 0.652254 -0.099112 11.00000 -1.50000 H42C 2 0.895858 0.562903 -0.025982 11.00000 -1.50000 AFIX 0 C41 1 0.782819 0.703656 0.045500 11.00000 0.10976 0.19152 = 0.14260 -0.05349 0.00361 0.00207 AFIX 137 H41A 2 0.756390 0.636437 0.056912 11.00000 -1.50000 H41B 2 0.737937 0.754604 0.014734 11.00000 -1.50000 H41C 2 0.787320 0.720587 0.096518 11.00000 -1.50000 AFIX 0 C21 1 0.668282 0.720984 0.690166 11.00000 0.03209 0.06985 = 0.05883 -0.02649 0.00554 -0.01188 C22 1 0.768669 0.754364 0.699716 11.00000 0.04892 0.07399 = 0.06677 -0.02797 -0.00881 -0.01665 C23 1 0.850754 0.759100 0.628549 11.00000 0.03356 0.06530 = 0.05913 -0.01370 0.00182 -0.01300 C24 1 0.932633 0.765121 0.507955 11.00000 0.03680 0.05627 = 0.06468 -0.01256 0.00651 -0.00588 AFIX 43 H24 2 0.946868 0.769295 0.451647 11.00000 -1.20000 AFIX 0 C25 1 1.003262 0.755351 0.559183 11.00000 0.04206 0.06180 = 0.07163 0.00145 0.00393 -0.01208 AFIX 43 H25 2 1.073921 0.751055 0.544615 11.00000 -1.20000 AFIX 0 N13 7 0.952285 0.752939 0.635888 11.00000 0.03093 0.07721 = 0.07502 -0.01532 -0.00282 -0.01685 C28 1 0.998170 0.740040 0.708453 11.00000 0.03871 0.10392 = 0.07257 -0.02244 -0.00622 -0.01055 AFIX 43 H28 2 0.955579 0.730065 0.758741 11.00000 -1.20000 AFIX 0 C26 1 0.608061 0.657709 0.841323 11.00000 0.06454 0.16724 = 0.06588 -0.04113 0.02040 -0.06267 AFIX 43 H26 2 0.664399 0.683836 0.853562 11.00000 -1.20000 AFIX 0 C20 1 0.522019 0.652972 0.722909 11.00000 0.03609 0.04516 = 0.07606 -0.01718 0.00203 -0.00705 AFIX 43 H20 2 0.463232 0.621859 0.752303 11.00000 -1.20000 AFIX 0 C19 1 0.546014 0.679519 0.639453 11.00000 0.03702 0.04142 = 0.07478 -0.01609 -0.01084 -0.00300 AFIX 43 H19 2 0.505349 0.671090 0.602016 11.00000 -1.20000 AFIX 0 C30 1 0.809853 0.975978 0.381160 11.00000 0.03756 0.03569 = 0.06746 -0.00749 -0.00684 -0.00857 AFIX 43 H30 2 0.818721 1.010459 0.420489 11.00000 -1.20000 AFIX 0 C31 1 0.835651 1.011017 0.298252 11.00000 0.04186 0.04028 = 0.07778 -0.01341 -0.00883 -0.00468 AFIX 43 H31 2 0.865226 1.072897 0.270727 11.00000 -1.20000 AFIX 0 C32 1 0.769389 0.860721 0.324669 11.00000 0.03921 0.03844 = 0.06186 -0.00705 -0.00790 -0.00168 C33 1 0.733743 0.766409 0.311906 11.00000 0.03672 0.04423 = 0.06659 -0.00502 -0.01256 -0.00120 C34 1 0.731748 0.674848 0.383809 11.00000 0.04033 0.04223 = 0.07879 -0.01907 -0.00635 -0.00663 N17 7 0.738725 0.573625 0.376210 11.00000 0.03940 0.04475 = 0.09688 -0.02266 0.00202 -0.00656 C39 1 0.737570 0.540083 0.304687 11.00000 0.06196 0.06018 = 0.12371 -0.03705 -0.00894 -0.00391 AFIX 43 H39 2 0.748302 0.588578 0.254209 11.00000 -1.20000 AFIX 0 C40 1 0.722171 0.443548 0.303873 11.00000 0.06063 0.05247 = 0.16977 -0.04078 -0.00935 0.00594 AFIX 93 H40A 2 0.711190 0.393089 0.353239 11.00000 -1.20000 H40B 2 0.722394 0.426561 0.253939 11.00000 -1.20000 AFIX 0 C36 1 0.745077 0.510800 0.453257 11.00000 0.03905 0.03616 = 0.11948 -0.00141 0.01376 -0.00430 AFIX 43 H36 2 0.751475 0.438648 0.467506 11.00000 -1.20000 AFIX 0 C35 1 0.740216 0.574393 0.505037 11.00000 0.03310 0.04158 = 0.09951 0.00945 0.00672 0.00332 AFIX 43 H35 2 0.741506 0.552403 0.561669 11.00000 -1.20000 AFIX 0 C37 1 0.835358 0.941890 0.176888 11.00000 0.06589 0.06568 = 0.08014 -0.02306 -0.00810 -0.00666 AFIX 43 H37 2 0.840649 0.879727 0.161015 11.00000 -1.20000 AFIX 0 C38 1 0.851648 1.028794 0.118387 11.00000 0.10168 0.08660 = 0.07455 -0.00687 -0.01510 -0.03318 AFIX 93 H38A 2 0.846878 1.092099 0.132445 11.00000 -1.20000 H38B 2 0.867816 1.026303 0.063392 11.00000 -1.20000 AFIX 0 C1 1 0.654091 0.996912 0.575297 11.00000 0.02286 0.03759 = 0.03951 0.00403 -0.00036 -0.00618 C2 1 0.697022 1.194698 0.538245 11.00000 0.03432 0.03639 = 0.06845 -0.01332 0.00517 0.00179 N9 7 0.519884 1.012114 0.792486 11.00000 0.04973 0.04519 = 0.04455 -0.01048 -0.00628 -0.00447 B1 3 0.589827 1.083387 0.812498 11.00000 0.04973 0.05783 = 0.05211 -0.02087 -0.01266 0.00457 AFIX 13 H1 2 0.582821 1.075194 0.872288 11.00000 -1.20000 AFIX 0 C6 1 0.530583 1.280010 0.798117 11.00000 0.05747 0.06098 = 0.06961 -0.03646 -0.00872 0.00502 C8 1 0.514511 1.278432 0.886316 11.00000 0.10281 0.07912 = 0.09586 -0.04940 -0.02165 0.01721 AFIX 33 H8A 2 0.491920 1.346723 0.892999 11.00000 -1.50000 H8B 2 0.463536 1.230855 0.914929 11.00000 -1.50000 H8C 2 0.577579 1.256687 0.908642 11.00000 -1.50000 AFIX 0 C5 1 0.514949 1.360414 0.731246 11.00000 0.05526 0.04297 = 0.08390 -0.02998 -0.00825 0.00289 AFIX 43 H5 2 0.492713 1.428367 0.732512 11.00000 -1.20000 AFIX 0 C4 1 0.538249 1.322095 0.661616 11.00000 0.03611 0.03810 = 0.06980 -0.01999 -0.00137 -0.00410 C7 1 0.530589 1.379419 0.575117 11.00000 0.04595 0.03111 = 0.07343 -0.00964 -0.00418 -0.00625 AFIX 33 H7A 2 0.508428 1.450573 0.573285 11.00000 -1.50000 H7B 2 0.596341 1.376201 0.542239 11.00000 -1.50000 H7C 2 0.482035 1.348633 0.553772 11.00000 -1.50000 AFIX 0 N7 7 0.700483 1.053553 0.779010 11.00000 0.04730 0.05684 = 0.06561 -0.02222 -0.01840 -0.00164 C9 1 0.825281 1.031971 0.683337 11.00000 0.03535 0.04858 = 0.08089 -0.02312 -0.01131 -0.00641 C12 1 0.883127 1.029932 0.600057 11.00000 0.02568 0.05193 = 0.10283 -0.02565 -0.00728 -0.00400 AFIX 33 H12A 2 0.953097 1.006251 0.605484 11.00000 -1.50000 H12B 2 0.852766 0.983726 0.577066 11.00000 -1.50000 H12C 2 0.880566 1.098515 0.564286 11.00000 -1.50000 AFIX 0 C10 1 0.862184 1.005382 0.759763 11.00000 0.04581 0.08070 = 0.10595 -0.04252 -0.03586 0.01135 AFIX 43 H10 2 0.929251 0.983342 0.768409 11.00000 -1.20000 AFIX 0 C11 1 0.783943 1.017280 0.818136 11.00000 0.05405 0.08031 = 0.08231 -0.03904 -0.03264 0.01461 C13 1 0.778859 0.997665 0.910201 11.00000 0.10344 0.18189 = 0.09837 -0.07281 -0.05217 0.04517 AFIX 33 H13A 2 0.710443 1.014400 0.933830 11.00000 -1.50000 H13B 2 0.797631 0.925870 0.932977 11.00000 -1.50000 H13C 2 0.825260 1.040207 0.922554 11.00000 -1.50000 AFIX 0 C16 1 0.452843 0.942999 0.841531 11.00000 0.06322 0.05874 = 0.03951 0.00332 -0.00361 -0.01596 C18 1 0.433044 0.928340 0.932851 11.00000 0.11586 0.11972 = 0.04163 -0.00344 0.00141 -0.04134 AFIX 137 H18A 2 0.496103 0.907760 0.955395 11.00000 -1.50000 H18B 2 0.385542 0.875487 0.956397 11.00000 -1.50000 H18C 2 0.404739 0.992333 0.945566 11.00000 -1.50000 AFIX 0 C15 1 0.412280 0.897529 0.792401 11.00000 0.05457 0.05011 = 0.04770 -0.00038 -0.00015 -0.01542 AFIX 43 H15 2 0.365457 0.846405 0.809335 11.00000 -1.20000 AFIX 0 C14 1 0.454434 0.942326 0.710718 11.00000 0.03460 0.03351 = 0.04447 -0.00795 -0.00431 -0.00183 C17 1 0.432288 0.918479 0.634257 11.00000 0.03632 0.04262 = 0.05741 -0.01562 -0.00374 -0.00752 AFIX 33 H17A 2 0.382791 0.866919 0.648590 11.00000 -1.50000 H17B 2 0.405615 0.980458 0.598842 11.00000 -1.50000 H17C 2 0.494187 0.892690 0.606068 11.00000 -1.50000 AFIX 0 C3 1 0.501100 1.148894 0.565358 11.00000 0.03533 0.03067 = 0.04187 -0.00783 0.00707 -0.00341 O44 8 0.950827 0.819115 0.052003 11.00000 0.13818 0.20637 = 0.29229 -0.13481 -0.04114 -0.00655 C43 1 0.962988 0.760332 0.001216 11.00000 0.18428 0.17412 = 0.33559 -0.17275 -0.04706 -0.02123 AFIX 43 H43 2 1.024768 0.756500 -0.033029 11.00000 -1.20000 AFIX 0 F2 5 0.315116 0.565529 0.889253 11.00000 0.16418 0.28497 = 0.31567 -0.05918 -0.04914 -0.06884 F4 5 0.257602 0.634134 0.984619 11.00000 0.57872 0.69872 = 0.25656 -0.31330 -0.26718 0.39500 B2 3 0.229989 0.654228 0.911477 11.00000 0.22567 0.71812 = 0.34251 -0.40000 0.22784 -0.36408 F3 5 0.248098 0.707061 0.870722 11.00000 0.39487 0.21764 = 0.49043 0.09302 -0.16470 -0.19460 F1 5 0.160709 0.593240 0.911679 11.00000 0.13617 0.29662 = 0.31341 0.00686 -0.00065 -0.05692 HKLF 4 REM Test_1_a.res in P-1 REM wR2 = 0.2695, GooF = S = 0.944, Restrained GooF = 0.944 for all data REM R1 = 0.0870 for 6168 Fo > 4sig(Fo) and 0.2293 for all 17416 data REM 653 parameters refined using 0 restraints END WGHT 0.1231 0.0000 REM Highest difference peak 0.791, deepest hole -0.645, 1-sigma level 0.096 Q1 1 0.1805 0.6023 1.0164 11.00000 0.05 0.79 Q2 1 0.2971 0.7032 0.9714 11.00000 0.05 0.74 Q3 1 0.4210 1.0734 0.4999 11.00000 0.05 0.69 Q4 1 0.8379 0.6639 0.5023 11.00000 0.05 0.59 Q5 1 0.2608 0.5448 0.9949 11.00000 0.05 0.50 ; _shelx_res_checksum 30064 _shelx_hkl_file ; -1 0 0 925.91 28.30 1 0 0 1051.59 28.20 1 0 0 1024.50 28.70 1 0 0 1004.00 28.90 1 0 0 1004.60 27.60 -2 0 0 1526.55 47.10 -2 0 0 1568.64 47.10 2 0 0 1601.64 45.90 2 0 0 1542.95 46.90 2 0 0 1542.15 47.30 2 0 0 1532.95 44.80 -3 0 0 593.44 30.90 3 0 0 635.64 30.60 3 0 0 701.43 29.80 3 0 0 647.44 31.80 3 0 0 668.53 28.80 -4 0 0 2997.70 88.59 -4 0 0 2910.91 88.09 4 0 0 2854.11 87.59 4 0 0 2913.31 85.99 4 0 0 2879.61 84.49 4 0 0 2912.61 88.79 -5 0 0 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34.60 26.70 -6 -10 4 0.70 24.50 -6 -10 4 56.09 29.30 -6 -10 4 29.00 29.20 5 10 -4 77.09 39.80 5 10 -4 80.19 26.50 5 10 -4 108.09 37.90 5 10 -4 101.79 32.10 5 10 -4 94.09 28.50 5 10 -4 84.79 33.50 5 10 -4 168.48 42.90 -5 -10 4 30.00 25.20 -5 -10 4 72.59 31.60 -5 -10 4 98.59 36.60 -5 -10 4 122.89 25.20 -5 -10 4 135.79 36.60 4 10 -4 -24.30 17.20 4 10 -4 -6.50 22.50 4 10 -4 18.60 30.30 4 10 -4 -7.80 20.70 4 10 -4 0.20 17.90 4 10 -4 26.50 22.60 4 10 -4 54.49 31.30 -4 -10 4 -31.20 16.10 -4 -10 4 -26.00 20.80 -4 -10 4 9.50 26.70 -4 -10 4 -19.80 22.00 3 10 -4 16.10 27.70 3 10 -4 -5.00 21.30 3 10 -4 3.10 23.20 3 10 -4 -12.20 15.40 3 10 -4 -8.70 19.70 -3 -10 4 6.90 18.30 2 10 -4 42.70 21.70 2 10 -4 -1.80 16.40 2 10 -4 13.00 22.70 2 10 -4 3.70 20.90 2 10 -4 57.49 29.90 -2 -10 4 19.40 18.50 1 10 -4 55.89 28.90 1 10 -4 23.00 19.90 1 10 -4 58.99 30.00 1 10 -4 78.29 25.80 -1 -10 4 -13.60 18.60 -1 -10 4 9.00 19.80 0 10 -4 34.00 24.50 0 10 -4 66.29 21.90 0 10 -4 82.59 30.60 0 10 -4 57.69 29.80 0 10 -4 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-0.0080 1 -6 17 -2.1612 -0.0093 1 -6 18 -2.9285 0.0127 1 -6 19 2.0793 0.0006 1 -6 20 3.0024 -0.0162 1 -5 0 -11.6079 0.0736 1 -5 1 -0.9855 -0.2047 1 -5 2 3.8455 -0.0627 1 -5 3 2.9507 0.0210 1 -5 4 1.8149 -0.0114 1 -5 5 -2.5290 0.0203 1 -5 6 1.3627 -0.0083 1 -5 7 0.8902 -0.0165 1 -5 8 -3.6418 0.0020 1 -5 9 0.4972 -0.0182 1 -5 10 2.0495 -0.0067 1 -5 11 -1.4379 0.0139 1 -5 12 -3.7164 -0.0110 1 -5 13 1.4740 0.0028 1 -5 14 4.4139 0.0043 1 -5 15 -3.1827 -0.0087 1 -5 16 -0.0152 -0.0027 1 -5 17 3.8304 -0.0001 1 -5 18 -3.3076 -0.0126 1 -5 19 -3.8864 -0.0110 1 -5 20 -0.2118 -0.0144 1 -4 0 11.0100 0.1834 1 -4 1 -18.5751 0.0441 1 -4 2 -8.1873 -0.0939 1 -4 3 10.9991 -0.0073 1 -4 4 -0.0166 -0.0134 1 -4 5 -4.3632 -0.0027 1 -4 6 2.5926 0.0107 1 -4 7 2.6587 -0.0019 1 -4 8 0.2237 0.0023 1 -4 9 -1.5804 0.0091 1 -4 10 -0.4052 -0.0097 1 -4 11 2.0293 -0.0014 1 -4 12 4.1406 0.0059 1 -4 13 -2.9234 -0.0022 1 -4 14 -3.5039 0.0047 1 -4 15 2.9756 -0.0008 1 -4 16 -0.2169 0.0102 1 -4 17 1.1643 0.0004 1 -4 18 4.0070 -0.0034 1 -4 19 0.2642 0.0056 1 -4 20 -0.4511 0.0084 1 -4 21 -2.6847 -0.0081 1 -3 0 5.2876 0.0097 1 -3 1 17.1854 0.1488 1 -3 2 -8.2234 -0.0128 1 -3 3 -18.3301 -0.0075 1 -3 4 9.6759 0.0022 1 -3 5 5.2144 -0.0153 1 -3 6 -8.8194 0.0121 1 -3 7 0.8778 -0.0104 1 -3 8 3.3676 -0.0063 1 -3 9 -1.3783 0.0005 1 -3 10 -0.6409 -0.0062 1 -3 11 0.3531 -0.0031 1 -3 12 -1.3356 0.0119 1 -3 13 2.9540 -0.0038 1 -3 14 2.0535 0.0059 1 -3 15 -1.4164 0.0050 1 -3 16 -1.4118 -0.0096 1 -3 17 -1.1879 0.0126 1 -3 18 1.8178 0.0121 1 -3 19 -0.8333 -0.0015 1 -3 20 1.1536 -0.0024 1 -3 21 4.7910 0.0083 1 -3 22 0.0851 0.0037 1 -2 0 15.9071 -0.2912 1 -2 1 14.2537 -0.0419 1 -2 2 5.2345 0.0471 1 -2 3 4.8573 -0.0285 1 -2 4 -13.3051 0.0156 1 -2 5 -0.2894 -0.0054 1 -2 6 7.3628 -0.0038 1 -2 7 -4.8582 0.0093 1 -2 8 0.2211 -0.0057 1 -2 9 4.7291 -0.0014 1 -2 10 -2.2988 0.0008 1 -2 11 -2.7840 -0.0115 1 -2 12 2.4038 -0.0054 1 -2 13 0.7084 0.0058 1 -2 14 -1.0144 -0.0056 1 -2 15 1.0680 0.0054 1 -2 16 2.3947 0.0016 1 -2 17 -0.8474 -0.0002 1 -2 18 -2.6416 -0.0009 1 -2 19 3.3193 0.0063 1 -2 20 -2.9963 0.0090 1 -2 21 -3.5570 0.0047 1 -2 22 1.7685 0.0061 1 -1 0 -78.2661 0.1445 1 -1 1 -7.1817 -0.1634 1 -1 2 35.7032 -0.0286 1 -1 3 -0.9372 -0.0463 1 -1 4 4.0645 -0.0299 1 -1 5 0.6642 -0.0121 1 -1 6 -4.3158 -0.0106 1 -1 7 0.8055 0.0047 1 -1 8 -4.1017 -0.0011 1 -1 9 -1.6110 0.0033 1 -1 10 5.6159 -0.0012 1 -1 11 1.1005 -0.0052 1 -1 12 -5.3489 -0.0050 1 -1 13 -1.0409 0.0030 1 -1 14 2.9203 -0.0003 1 -1 15 -0.0246 0.0036 1 -1 16 -1.3135 0.0021 1 -1 17 1.9681 -0.0088 1 -1 18 1.8931 0.0082 1 -1 19 -3.4937 -0.0010 1 -1 20 3.0277 -0.0019 1 -1 21 1.7624 -0.0021 1 -1 22 -2.4528 0.0001 1 0 0 91.2155 0.2375 1 0 1 -58.0799 0.1450 1 0 2 -49.7171 -0.0041 1 0 3 24.0999 0.0546 1 0 4 0.1423 -0.0213 1 0 5 -2.8005 0.0093 1 0 6 7.3200 -0.0113 1 0 7 3.0057 -0.0067 1 0 8 0.2851 0.0050 1 0 9 -3.1904 0.0008 1 0 10 -4.7897 0.0066 1 0 11 1.5760 0.0031 1 0 12 4.4036 -0.0058 1 0 13 -2.9581 -0.0045 1 0 14 -4.2625 0.0001 1 0 15 -0.5655 -0.0069 1 0 16 0.7035 0.0031 1 0 17 -1.3403 0.0012 1 0 18 -0.1726 -0.0090 1 0 19 1.5023 -0.0002 1 0 20 -3.5671 -0.0012 1 0 21 -0.2221 0.0046 1 0 22 2.7048 0.0032 1 0 23 -0.9089 0.0004 1 1 0 -27.4212 -0.1430 1 1 1 83.1317 0.1580 1 1 2 6.6787 0.0693 1 1 3 -29.9686 0.0457 1 1 4 6.2844 0.0566 1 1 5 -3.0230 0.0093 1 1 6 -7.5784 0.0215 1 1 7 -0.1658 0.0086 1 1 8 3.9471 0.0018 1 1 9 3.3848 0.0100 1 1 10 1.4259 0.0096 1 1 11 -3.2508 0.0032 1 1 12 -1.4393 0.0014 1 1 13 3.7010 -0.0028 1 1 14 1.5825 0.0007 1 1 15 -0.3742 0.0008 1 1 16 -2.1880 0.0016 1 1 17 -0.2450 0.0001 1 1 18 -0.1989 -0.0027 1 1 19 2.3802 -0.0048 1 1 20 -0.0614 -0.0033 1 1 21 -2.5385 -0.0071 1 1 22 -0.7570 -0.0042 1 1 23 1.8044 0.0024 1 2 0 -12.9158 -0.0365 1 2 1 -27.8542 -0.1328 1 2 2 13.5804 0.0281 1 2 3 -0.5657 -0.0195 1 2 4 1.9508 0.0317 1 2 5 10.0692 0.0153 1 2 6 -1.0695 0.0174 1 2 7 -0.6441 0.0082 1 2 8 -3.7656 0.0040 1 2 9 -2.8294 -0.0064 1 2 10 2.0568 0.0082 1 2 11 2.4752 0.0043 1 2 12 -1.5388 0.0033 1 2 13 -1.2160 -0.0006 1 2 14 -0.9359 -0.0045 1 2 15 0.1163 -0.0026 1 2 16 1.6364 -0.0068 1 2 17 -0.5990 0.0032 1 2 18 0.0305 0.0056 1 2 19 -1.6100 0.0031 1 2 20 4.6304 -0.0046 1 2 21 -0.4702 0.0012 1 2 22 -0.0017 0.0025 1 2 23 0.3875 0.0051 1 3 0 -16.5706 -0.0096 1 3 1 -11.8760 -0.0237 1 3 2 23.1475 -0.0380 1 3 3 10.7989 -0.0143 1 3 4 -26.6594 -0.0426 1 3 5 -3.2545 0.0032 1 3 6 7.6306 -0.0203 1 3 7 -4.1231 0.0054 1 3 8 5.3138 0.0037 1 3 9 2.2566 -0.0038 1 3 10 -4.7513 -0.0027 1 3 11 1.7685 0.0085 1 3 12 1.4425 -0.0023 1 3 13 -0.9226 0.0054 1 3 14 2.3698 -0.0012 1 3 15 -0.2662 -0.0012 1 3 16 0.3748 0.0014 1 3 17 -1.1095 -0.0051 1 3 18 -2.6107 -0.0039 1 3 19 0.6112 0.0013 1 3 20 -1.2251 0.0040 1 3 21 2.4395 -0.0032 1 3 22 -3.2689 -0.0077 1 3 23 1.2522 -0.0037 1 4 0 41.0392 -0.0063 1 4 1 -10.4605 0.0216 1 4 2 -42.3303 -0.0090 1 4 3 15.2161 0.0039 1 4 4 29.5152 -0.0139 1 4 5 -11.8087 -0.0140 1 4 6 -5.1304 -0.0016 1 4 7 4.0301 -0.0089 1 4 8 -8.6558 -0.0003 1 4 9 1.1460 0.0013 1 4 10 3.6218 -0.0130 1 4 11 -3.9251 0.0055 1 4 12 2.5236 -0.0003 1 4 13 -0.0363 -0.0014 1 4 14 -2.3862 0.0068 1 4 15 0.0854 -0.0005 1 4 16 -0.9098 0.0011 1 4 17 4.4923 0.0027 1 4 18 1.4298 -0.0021 1 4 19 -2.9059 0.0025 1 4 20 -1.3217 0.0028 1 4 21 1.4037 -0.0046 1 4 22 1.1625 0.0030 1 4 23 -3.7770 -0.0170 1 4 24 1.3976 -0.0178 1 5 0 -22.2086 -0.0822 1 5 1 27.6746 -0.0381 1 5 2 15.6913 0.0132 1 5 3 -23.2375 0.0195 1 5 4 -7.9475 0.0130 1 5 5 13.3339 -0.0072 1 5 6 0.4595 -0.0033 1 5 7 0.9108 -0.0168 1 5 8 5.3221 0.0010 1 5 9 -4.9471 0.0050 1 5 10 -0.8747 0.0055 1 5 11 1.5430 -0.0098 1 5 12 -1.7692 0.0124 1 5 13 3.3327 -0.0052 1 5 14 0.5727 0.0052 1 5 15 0.6008 0.0006 1 5 16 -0.1739 -0.0024 1 5 17 -3.6735 0.0004 1 5 18 1.2930 0.0047 1 5 19 1.0194 -0.0087 1 5 20 0.1483 0.0027 1 5 21 -2.0296 0.0083 1 5 22 1.6193 -0.0050 1 5 23 -1.4684 0.0150 1 5 24 -2.8261 -0.0210 1 6 0 3.9669 -0.0047 1 6 1 -8.7634 -0.0878 1 6 2 3.2703 -0.0528 1 6 3 3.0412 -0.0251 1 6 4 0.4616 0.0005 1 6 5 -0.7908 -0.0030 1 6 6 -0.1952 -0.0049 1 6 7 -1.8517 -0.0061 1 6 8 2.3378 -0.0191 1 6 9 4.9838 -0.0120 1 6 10 -1.3162 -0.0045 1 6 11 -1.3193 -0.0001 1 6 12 -1.6760 -0.0051 1 6 13 -0.7449 -0.0006 1 6 14 2.9182 -0.0087 1 6 15 -0.3699 0.0092 1 6 16 -0.4727 0.0006 1 6 17 1.8930 0.0024 1 6 18 1.1542 -0.0012 1 6 19 1.9581 0.0086 1 6 20 -0.9705 -0.0025 1 6 21 1.9215 0.0002 1 6 22 0.4986 -0.0003 1 6 23 2.3737 -0.0160 1 6 24 -1.9287 0.0263 1 7 0 -5.7154 0.1131 1 7 1 -6.5801 -0.0236 1 7 2 4.6496 -0.0683 1 7 3 7.8877 -0.0384 1 7 4 -9.9654 -0.0125 1 7 5 -3.3967 -0.0045 1 7 6 5.0527 0.0017 1 7 7 0.7287 -0.0039 1 7 8 -4.4305 -0.0132 1 7 9 -1.0124 -0.0045 1 7 10 3.8308 -0.0127 1 7 11 1.1437 -0.0041 1 7 12 -0.1500 -0.0024 1 7 13 -2.6316 0.0074 1 7 14 -2.1234 -0.0076 1 7 15 2.3970 -0.0054 1 7 16 1.9963 -0.0002 1 7 17 -4.1340 -0.0058 1 7 18 -2.1944 0.0003 1 7 19 -0.2152 -0.0001 1 7 20 1.6488 0.0031 1 7 21 -1.4790 0.0058 1 7 22 1.9539 0.0139 1 7 23 2.2385 0.0163 1 8 0 7.8606 0.1231 1 8 1 3.4726 0.1310 1 8 2 -11.9730 0.0169 1 8 3 -2.8433 -0.0122 1 8 4 11.9278 -0.0192 1 8 5 -2.8474 0.0052 1 8 6 -6.1392 0.0040 1 8 7 0.4322 0.0197 1 8 8 2.7244 0.0081 1 8 9 -0.7000 -0.0019 1 8 10 -2.8387 0.0026 1 8 11 1.4898 -0.0089 1 8 12 -0.2100 0.0034 1 8 13 0.3783 0.0002 1 8 14 -0.3779 0.0128 1 8 15 -2.3689 -0.0047 1 8 16 0.3181 0.0052 1 8 17 3.9035 0.0025 1 8 18 -2.4148 -0.0017 1 8 19 -0.8233 -0.0084 1 8 20 -1.4408 0.0041 1 8 21 -1.0387 0.0008 1 8 22 -2.8185 -0.0037 1 8 23 0.0069 -0.0019 1 9 0 -4.1176 -0.0018 1 9 1 0.3351 0.1549 1 9 2 8.2682 0.0862 1 9 3 -2.5599 0.0330 1 9 4 -7.0711 0.0228 1 9 5 3.0392 0.0065 1 9 6 0.9673 0.0131 1 9 7 -0.3053 0.0203 1 9 8 -1.9017 0.0214 1 9 9 -1.3532 0.0073 1 9 10 0.8889 0.0108 1 9 11 -0.2766 0.0029 1 9 12 2.9458 -0.0053 1 9 13 -1.1273 0.0004 1 9 14 -0.1874 -0.0004 1 9 15 -0.6258 0.0077 1 9 16 0.3106 -0.0022 1 9 17 1.1362 0.0034 1 9 18 2.6407 0.0027 1 9 19 -1.1716 -0.0006 1 9 20 0.1326 -0.0165 1 9 21 -0.7760 -0.0049 1 9 22 -0.7757 0.0010 1 9 23 -1.4612 0.0106 1 10 0 1.1199 -0.1375 1 10 1 1.8422 -0.0011 1 10 2 -2.8908 0.0971 1 10 3 2.9397 0.0433 1 10 4 3.2532 0.0223 1 10 5 -0.1400 0.0048 1 10 6 -0.1621 0.0037 1 10 7 -2.9352 -0.0078 1 10 8 1.4674 0.0161 1 10 9 2.2930 0.0108 1 10 10 -2.0151 0.0031 1 10 11 -2.2965 0.0039 1 10 12 -1.2695 -0.0062 1 10 13 3.1633 -0.0017 1 10 14 -0.7484 -0.0042 1 10 15 1.3427 -0.0031 1 10 16 -4.0191 -0.0018 1 10 17 -0.1181 -0.0077 1 10 18 1.4035 -0.0014 1 10 19 2.1867 0.0119 1 10 20 3.8055 -0.0013 1 10 21 1.0369 0.0029 1 10 22 -1.0311 -0.0036 1 10 23 -0.1694 -0.0272 1 11 0 -2.1086 -0.1080 1 11 1 -4.7170 -0.1388 1 11 2 2.3836 -0.0042 1 11 3 0.6780 0.0059 1 11 4 -0.2255 0.0119 1 11 5 -0.8251 0.0083 1 11 6 1.8902 -0.0136 1 11 7 3.7683 0.0008 1 11 8 -2.6594 -0.0103 1 11 9 -2.2103 0.0012 1 11 10 2.5452 -0.0030 1 11 11 1.6976 0.0043 1 11 12 -1.4807 -0.0008 1 11 13 -2.3594 -0.0106 1 11 14 1.7867 -0.0047 1 11 15 -1.5417 -0.0072 1 11 16 3.6179 -0.0012 1 11 17 -3.3743 0.0054 1 11 18 -1.1702 -0.0102 1 11 19 -3.5917 -0.0152 1 11 20 -2.9425 0.0088 1 11 21 5.9050 -0.0274 1 11 22 1.9719 0.0121 1 12 0 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-0.0012 2 0 16 3.7255 0.0030 2 0 17 -1.2622 -0.0016 2 0 18 -2.3509 -0.0010 2 0 19 -1.5795 0.0033 2 0 20 -0.8115 0.0040 2 0 21 3.0494 0.0022 2 0 22 0.7340 -0.0042 2 0 23 -1.3875 0.0101 2 1 0 9.0717 0.0790 2 1 1 43.2722 0.0955 2 1 2 -17.0845 -0.0272 2 1 3 -16.4297 0.0316 2 1 4 9.0727 -0.0086 2 1 5 2.9829 0.0070 2 1 6 -7.3989 0.0031 2 1 7 -4.1467 -0.0006 2 1 8 6.8176 -0.0059 2 1 9 1.9198 0.0027 2 1 10 -1.0142 0.0016 2 1 11 -3.1128 0.0138 2 1 12 -0.6128 0.0014 2 1 13 2.2011 -0.0083 2 1 14 1.7664 0.0033 2 1 15 -3.5965 0.0025 2 1 16 -3.2859 -0.0009 2 1 17 4.0277 -0.0062 2 1 18 1.5790 0.0023 2 1 19 0.5833 -0.0006 2 1 20 -3.7934 -0.0108 2 1 21 -2.7628 -0.0035 2 1 22 0.5464 0.0100 2 1 23 0.8160 0.0006 2 2 0 -10.9269 0.0331 2 2 1 -9.3941 0.0907 2 2 2 13.3329 0.0474 2 2 3 -1.5565 0.0002 2 2 4 -5.1923 0.0249 2 2 5 4.3232 0.0032 2 2 6 9.2031 0.0246 2 2 7 -2.0136 -0.0060 2 2 8 -8.9606 0.0086 2 2 9 1.7594 -0.0061 2 2 10 1.6850 0.0060 2 2 11 0.3466 -0.0054 2 2 12 0.6980 0.0089 2 2 13 -1.1590 0.0003 2 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0.0003 10 0 20 1.6753 -0.0018 10 0 21 -0.4265 -0.0151 10 1 0 0.7260 0.0027 10 1 1 -3.1841 0.0021 10 1 2 0.5823 0.0155 10 1 3 0.3110 -0.0050 10 1 4 2.6993 0.0013 10 1 5 1.0684 -0.0065 10 1 6 -7.7013 -0.0074 10 1 7 -0.1139 0.0131 10 1 8 4.9973 0.0037 10 1 9 1.2870 0.0021 10 1 10 -2.7004 -0.0024 10 1 11 -2.8660 0.0044 10 1 12 0.1916 -0.0029 10 1 13 1.7628 -0.0035 10 1 14 -0.9944 -0.0000 10 1 15 -0.9987 0.0053 10 1 16 0.7501 0.0016 10 1 17 -1.1953 -0.0067 10 1 18 0.6718 0.0051 10 1 19 1.1558 0.0028 10 1 20 -0.1614 -0.0211 10 1 21 -0.8571 -0.0222 10 2 0 1.7460 0.0157 10 2 1 1.2225 -0.0062 10 2 2 -2.0145 0.0020 10 2 3 0.3417 0.0198 10 2 4 -0.9029 -0.0042 10 2 5 -0.8741 0.0034 10 2 6 1.5754 -0.0090 10 2 7 -2.4276 -0.0024 10 2 8 -1.3253 0.0019 10 2 9 0.3120 -0.0045 10 2 10 1.7893 0.0006 10 2 11 2.9848 -0.0061 10 2 12 -0.1815 0.0068 10 2 13 -2.9709 0.0076 10 2 14 -1.6042 -0.0075 10 2 15 0.4571 0.0049 10 2 16 1.1491 0.0036 10 2 17 0.8429 -0.0057 10 2 18 -2.7235 0.0053 10 2 19 -2.6666 0.0123 10 2 20 0.1828 0.0232 10 2 21 2.5738 -0.0176 10 2 22 -0.9249 -0.0609 10 3 0 -1.9907 -0.0048 10 3 1 -0.7707 0.0039 10 3 2 -0.8747 -0.0129 10 3 3 -1.7772 0.0092 10 3 4 0.6483 0.0142 10 3 5 3.8676 0.0030 10 3 6 -0.8085 0.0063 10 3 7 -4.8907 -0.0044 10 3 8 -2.5272 0.0056 10 3 9 3.3171 0.0065 10 3 10 -0.5040 -0.0009 10 3 11 -3.5851 -0.0029 10 3 12 1.3576 -0.0055 10 3 13 3.5244 -0.0033 10 3 14 1.6944 0.0040 10 3 15 -1.7983 -0.0021 10 3 16 -0.8592 0.0040 10 3 17 0.4766 0.0033 10 3 18 2.1031 0.0007 10 3 19 1.3556 0.0098 10 3 20 -1.6216 0.0110 10 3 21 -2.9732 0.0331 10 3 22 0.9122 0.0163 10 4 0 -0.0574 -0.0072 10 4 1 1.7946 0.0146 10 4 2 0.7672 -0.0041 10 4 3 -0.1405 -0.0198 10 4 4 -1.9071 0.0070 10 4 5 -4.0312 -0.0008 10 4 6 4.4046 0.0015 10 4 7 5.8751 0.0056 10 4 8 -3.8891 0.0029 10 4 9 -7.2087 0.0026 10 4 10 2.6257 0.0063 10 4 11 2.7945 0.0078 10 4 12 -1.8153 0.0010 10 4 13 -2.5981 0.0044 10 4 14 -0.8982 -0.0002 10 4 15 2.0335 -0.0025 10 4 16 0.4092 0.0029 10 4 17 0.9518 -0.0025 10 4 18 0.8968 -0.0111 10 4 19 -0.3826 0.0013 10 4 20 0.1267 0.0094 10 4 21 1.4730 0.0147 10 4 22 0.4330 0.0234 10 5 0 1.4831 -0.0052 10 5 1 -1.4222 -0.0139 10 5 2 1.8860 0.0120 10 5 3 0.3350 -0.0056 10 5 4 1.1088 -0.0067 10 5 5 2.2661 0.0035 10 5 6 -3.5727 -0.0109 10 5 7 -0.6463 -0.0015 10 5 8 6.0245 -0.0047 10 5 9 1.7798 -0.0022 10 5 10 -5.4986 0.0054 10 5 11 -0.9652 0.0004 10 5 12 0.3491 -0.0005 10 5 13 0.8908 0.0074 10 5 14 -0.5004 -0.0003 10 5 15 -1.3821 -0.0055 10 5 16 -0.7066 0.0025 10 5 17 -0.9919 0.0068 10 5 18 -1.3603 -0.0046 10 5 19 3.0676 -0.0180 10 5 20 2.5141 -0.0066 10 5 21 -1.3445 -0.0066 10 5 22 -1.5358 0.0113 10 6 0 0.6632 0.0003 10 6 1 1.1350 -0.0023 10 6 2 -1.9861 0.0024 10 6 3 2.2852 0.0045 10 6 4 0.4854 -0.0122 10 6 5 -0.7041 0.0039 10 6 6 1.8366 -0.0030 10 6 7 -0.6552 -0.0134 10 6 8 -1.5242 0.0041 10 6 9 3.3593 -0.0055 10 6 10 3.0815 -0.0170 10 6 11 -0.4926 0.0047 10 6 12 1.2078 -0.0041 10 6 13 -0.7821 -0.0128 10 6 14 -0.9868 0.0152 10 6 15 -1.1718 0.0009 10 6 16 -0.0374 -0.0180 10 6 17 -0.8567 0.0030 10 6 18 2.1142 0.0037 10 6 19 -4.5887 -0.0096 10 6 20 -1.5689 -0.0179 10 6 21 1.7132 -0.0052 10 6 22 2.1227 -0.0160 10 7 0 -3.0943 0.0028 10 7 1 1.0000 -0.0027 10 7 2 1.5719 -0.0079 10 7 3 -3.2873 0.0077 10 7 4 0.4381 0.0035 10 7 5 1.6171 0.0006 10 7 6 0.6384 0.0091 10 7 7 1.8332 -0.0067 10 7 8 -0.8274 -0.0086 10 7 9 -2.2514 -0.0002 10 7 10 1.0729 -0.0014 10 7 11 0.1389 -0.0049 10 7 12 0.1214 0.0033 10 7 13 3.3168 -0.0114 10 7 14 2.3665 -0.0065 10 7 15 0.4325 0.0054 10 7 16 -1.0407 -0.0015 10 7 17 0.1025 -0.0125 10 7 18 -3.7489 0.0104 10 7 19 5.0067 0.0066 10 7 20 -0.7038 -0.0134 10 7 21 -1.9313 -0.0265 10 7 22 -3.3654 0.0012 10 8 0 1.5792 0.0093 10 8 1 -3.1263 0.0017 10 8 2 0.0712 -0.0065 10 8 3 2.6994 0.0040 10 8 4 -2.8841 0.0053 10 8 5 -1.9729 -0.0046 10 8 6 -0.3558 0.0152 10 8 7 -0.6074 0.0093 10 8 8 2.8014 0.0003 10 8 9 0.1861 0.0106 10 8 10 -0.5736 -0.0047 10 8 11 1.7023 -0.0144 10 8 12 -1.9106 0.0143 10 8 13 -2.3375 0.0089 10 8 14 0.7393 -0.0171 10 8 15 1.9893 0.0211 10 8 16 1.4948 0.0093 10 8 17 -0.6566 -0.0050 10 8 18 1.6204 -0.0058 10 8 19 -4.2324 0.0151 10 8 20 3.2355 0.0161 10 8 21 0.8755 0.0035 10 9 0 1.7771 -0.0190 10 9 1 2.5075 0.0207 10 9 2 -1.9145 0.0070 10 9 3 -0.9380 -0.0208 10 9 4 3.3648 0.0043 10 9 5 -0.9580 -0.0001 10 9 6 -1.1211 -0.0026 10 9 7 -0.4334 0.0127 10 9 8 -2.1120 0.0004 10 9 9 1.3257 0.0067 10 9 10 -1.9658 0.0132 10 9 11 -1.3361 0.0037 10 9 12 3.0972 -0.0126 10 9 13 0.6893 0.0075 10 9 14 -1.2748 0.0028 10 9 15 -1.0958 -0.0148 10 9 16 -0.0647 0.0159 10 9 17 2.7846 0.0047 10 9 18 -1.0312 -0.0002 10 9 19 0.4830 0.0158 10 9 20 -3.0715 0.0324 10 9 21 1.8226 0.0083 10 10 0 -1.8128 0.0162 10 10 1 -0.8102 -0.0240 10 10 2 2.2682 0.0140 10 10 3 -0.9737 0.0087 10 10 4 -1.4590 -0.0102 10 10 5 0.9131 0.0022 10 10 6 -1.3374 -0.0162 10 10 7 0.3451 0.0072 10 10 8 -0.0564 -0.0016 10 10 9 -1.4552 -0.0060 10 10 10 2.3827 0.0194 10 10 11 -1.1231 -0.0058 10 10 12 -3.4850 -0.0062 10 10 13 -0.1002 0.0083 10 10 14 0.8259 -0.0046 10 10 15 1.1241 -0.0160 10 10 16 -0.3543 0.0059 10 10 17 -2.3087 0.0025 10 10 18 2.3793 -0.0171 10 10 19 -0.2758 -0.0405 10 10 20 1.2564 -0.0033 10 10 21 -0.7231 0.0623 10 11 0 -0.8823 -0.0069 10 11 1 -0.2406 -0.0027 10 11 2 -1.5244 -0.0026 10 11 3 0.9603 0.0103 10 11 4 -1.2377 -0.0100 10 11 5 2.1305 -0.0038 10 11 6 0.6703 0.0039 10 11 7 -2.6081 -0.0230 10 11 8 0.9353 0.0122 10 11 9 -0.2671 -0.0122 10 11 10 -1.9068 -0.0089 10 11 11 0.8957 0.0220 10 11 12 1.0834 -0.0007 10 11 13 -1.2357 -0.0083 10 11 14 -0.6098 0.0161 10 11 15 -0.9573 -0.0054 10 11 16 1.3094 -0.0182 10 11 17 1.5427 0.0160 10 11 18 -0.0590 0.0008 10 11 19 1.1824 0.0054 10 11 20 -3.4452 -0.0520 10 12 0 -0.3038 0.0068 10 12 1 -1.5985 0.0058 10 12 2 -0.5619 -0.0240 10 12 3 0.3702 0.0099 10 12 4 1.9338 0.0066 10 12 5 -4.2068 -0.0056 10 12 6 1.6779 0.0006 10 12 7 1.6717 -0.0025 10 12 8 -1.4167 -0.0173 10 12 9 1.2178 0.0003 10 12 10 0.8101 -0.0124 10 12 11 0.1426 0.0020 10 12 12 -0.9356 -0.0045 10 12 13 -0.5151 -0.0062 10 12 14 -1.1718 0.0033 10 12 15 -0.2688 0.0113 10 12 16 -1.7322 -0.0109 10 12 17 -0.1564 0.0043 10 12 18 -0.9504 0.0241 10 12 19 2.9078 -0.0027 10 13 0 3.3345 -0.0175 10 13 1 2.5971 0.0026 10 13 2 0.9155 -0.0044 10 13 3 -1.6929 -0.0109 10 13 4 -1.5879 0.0225 10 13 5 3.8108 -0.0101 10 13 6 -1.4519 0.0071 10 13 7 0.0464 0.0087 10 13 8 0.8704 -0.0009 10 13 9 -0.7078 0.0066 10 13 10 -0.3957 -0.0009 10 13 11 0.2521 -0.0116 10 13 12 2.5716 0.0143 10 13 13 0.9426 0.0049 10 13 14 0.5858 -0.0030 10 13 15 -0.1666 0.0010 10 13 16 -1.2821 0.0066 10 13 17 -1.8916 -0.0214 10 13 18 0.3073 0.0005 10 13 19 -4.6773 0.0158 10 14 0 -1.8533 -0.0060 10 14 1 0.2503 0.0029 10 14 2 0.4286 0.0271 10 14 3 2.6834 -0.0212 10 14 4 2.9872 0.0097 10 14 5 -1.5290 0.0121 10 14 6 0.8433 -0.0081 10 14 7 -0.2638 0.0163 10 14 8 -0.7635 -0.0020 10 14 9 1.6519 -0.0088 10 14 10 1.2986 0.0012 10 14 11 -0.7548 0.0067 10 14 12 -2.0274 0.0002 10 14 13 0.6796 -0.0116 10 14 14 -0.0807 0.0045 10 14 15 1.4269 0.0124 10 14 16 3.1775 0.0018 10 14 17 -1.0824 0.0193 10 15 0 -0.4025 0.1359 10 15 1 -0.2741 -0.0134 10 15 2 0.8703 -0.0215 10 15 3 -1.6448 0.0051 10 15 4 -2.9239 -0.0214 10 15 5 1.2142 0.0572 10 15 6 1.8802 -0.0268 10 15 7 1.9555 0.0080 10 15 8 0.5458 0.0304 10 15 9 -2.3435 -0.0087 10 15 10 -0.4306 0.0100 10 15 11 1.2008 0.0023 10 15 12 1.8327 -0.0162 10 15 13 -0.4776 -0.0018 10 15 14 0.6025 -0.0021 10 15 15 -2.0391 -0.0027 10 15 16 -0.7023 -0.0188 10 16 0 -0.7180 -0.1895 10 16 1 -2.5371 0.0961 10 16 2 -1.5979 0.0338 10 16 3 0.4081 0.0098 10 16 4 1.9923 -0.0433 10 16 5 -1.5904 -0.0609 10 16 6 -3.7851 0.0806 10 16 7 -0.5744 -0.0610 10 16 8 0.8116 0.0115 10 16 9 1.5561 0.0336 10 16 10 0.7187 -0.0372 10 16 11 -0.5936 -0.0077 10 16 12 -1.6267 0.0654 10 16 13 0.5483 0.0038 10 16 14 -0.4381 -0.0518 10 17 5 0.7154 -0.0190 10 17 6 1.6053 -0.0733 10 17 7 -2.7311 0.0637 10 17 8 -0.5408 -0.0644 10 17 9 -1.2968 -0.0075 10 17 10 -1.6509 0.0482 11 -14 0 -0.3761 0.0818 11 -14 1 -0.1873 -0.0730 11 -13 0 0.1180 -0.0258 11 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0.0013 11 -9 5 -0.7715 0.0042 11 -9 6 0.6270 0.0039 11 -9 7 0.9312 0.0139 11 -9 8 -0.4129 -0.0017 11 -9 9 -1.6446 0.0091 11 -9 10 3.6537 -0.0228 11 -9 11 4.1898 -0.0447 11 -9 12 0.2287 0.0458 11 -9 13 -1.2052 0.0233 11 -8 0 -1.1431 0.0075 11 -8 1 -0.2799 -0.0096 11 -8 2 0.2557 0.0164 11 -8 3 1.3672 -0.0157 11 -8 4 -0.2099 -0.0006 11 -8 5 0.2917 -0.0058 11 -8 6 -0.4350 -0.0004 11 -8 7 -0.2501 -0.0036 11 -8 8 1.0301 0.0096 11 -8 9 0.5082 0.0011 11 -8 10 -2.8604 -0.0149 11 -8 11 0.4858 0.0187 11 -8 12 1.4446 -0.0299 11 -8 13 3.2889 -0.0123 11 -8 14 -0.0943 0.0676 11 -7 0 0.2446 -0.0034 11 -7 1 -1.0867 0.0071 11 -7 2 2.2617 -0.0142 11 -7 3 -1.1622 0.0132 11 -7 4 1.6706 -0.0136 11 -7 5 0.6811 0.0041 11 -7 6 -0.2243 -0.0040 11 -7 7 -0.0996 -0.0032 11 -7 8 -0.6243 -0.0007 11 -7 9 -0.9680 0.0051 11 -7 10 -0.3377 0.0081 11 -7 11 -0.6548 -0.0109 11 -7 12 1.8628 0.0106 11 -7 13 -2.4240 -0.0046 11 -7 14 2.2552 -0.0530 11 -7 15 -0.3521 -0.0297 11 -6 0 4.0405 0.0029 11 -6 1 -1.9648 0.0026 11 -6 2 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0.0275 16 5 7 0.8041 -0.0085 16 5 8 0.3905 0.0018 16 5 9 0.5489 0.0111 16 5 10 -2.7415 0.0060 16 5 11 -2.6076 -0.0194 16 5 12 1.4056 0.0130 16 5 13 0.5437 0.0397 16 5 14 -2.0541 -0.0603 16 5 15 0.6602 -0.0579 16 5 16 -0.2486 0.0332 16 6 0 0.4565 -0.0193 16 6 1 -1.0573 -0.0016 16 6 2 1.1535 0.0052 16 6 3 0.4507 -0.0157 16 6 4 1.2011 0.0145 16 6 5 -0.3164 -0.0118 16 6 6 -2.5312 -0.0215 16 6 7 -0.0940 0.0224 16 6 8 -2.2088 -0.0347 16 6 9 0.1093 0.0316 16 6 10 4.3654 0.0009 16 6 11 0.2415 -0.0212 16 6 12 -1.9379 0.0072 16 6 13 -0.7515 0.0170 16 6 14 -0.0221 0.0445 16 6 15 -1.7765 -0.0102 16 7 0 0.4858 0.0006 16 7 1 1.2426 -0.0019 16 7 2 -1.6732 0.0106 16 7 3 1.3587 0.0044 16 7 4 1.0610 0.0306 16 7 5 -1.2805 -0.0014 16 7 6 1.6068 -0.0108 16 7 7 0.9243 0.0234 16 7 8 1.4834 -0.0036 16 7 9 -3.4861 -0.0232 16 7 10 -2.5054 0.0340 16 7 11 1.2055 -0.0147 16 7 12 0.6053 -0.0052 16 7 13 2.3725 0.0105 16 7 14 0.6786 -0.0224 16 7 15 -0.6162 0.0107 16 8 0 0.0565 0.0508 16 8 1 1.1174 -0.0359 16 8 2 0.8563 0.0396 16 8 3 -2.7335 0.0071 16 8 4 0.6655 -0.0320 16 8 5 4.1282 0.0439 16 8 6 -1.1492 -0.0100 16 8 7 -0.5055 -0.0116 16 8 8 0.7504 0.0408 16 8 9 2.9010 -0.0444 16 8 10 -0.1515 0.0381 16 8 11 0.6372 0.0167 16 8 12 -0.3968 -0.0449 16 8 13 -2.9632 0.0579 16 8 14 0.7822 0.0335 16 8 15 1.9851 -0.0624 16 9 0 -0.2475 0.0179 16 9 1 -0.1319 0.0362 16 9 2 1.6794 -0.0832 16 9 3 1.4441 0.0056 16 9 4 -1.5614 0.0082 16 9 5 -2.2732 0.0074 16 9 6 1.9859 -0.0021 16 9 7 1.1424 -0.0226 16 9 8 -0.1697 0.0063 16 9 9 -0.8047 0.0274 16 9 10 0.5146 -0.0820 16 9 11 -0.9559 0.0538 16 9 12 1.7918 -0.0275 16 9 13 2.1870 -0.0906 16 9 14 -0.6426 0.0915 16 10 0 0.0232 -0.0984 16 10 1 -0.5105 -0.0138 16 10 2 0.7668 0.0296 16 10 3 0.8862 0.0084 16 10 4 -0.1863 -0.0467 16 10 5 1.0020 -0.0602 16 10 6 -0.3544 0.0860 16 10 7 -0.4730 -0.0411 16 10 8 1.1680 -0.0121 16 10 9 0.2147 0.0275 16 10 10 -0.3931 0.0033 16 10 11 0.5782 -0.0253 16 10 12 -0.8359 0.0796 16 10 13 -0.2405 -0.0434 16 11 2 -2.8208 -0.0082 16 11 3 -0.0820 -0.0557 16 11 4 0.6047 0.0830 16 11 5 -1.5414 -0.0214 16 11 6 -0.3765 -0.0924 16 11 7 0.4850 0.1107 16 11 8 -0.5747 -0.0868 16 11 9 0.6367 0.0120 16 11 10 -0.3916 0.0473 16 11 11 -0.3982 -0.0693 17 -6 0 -1.7189 0.0617 17 -6 1 -0.3152 -0.0143 17 -5 0 3.1237 -0.0450 17 -5 1 -0.6358 0.0831 17 -5 5 -1.0579 0.0158 17 -5 6 -2.7643 -0.0409 17 -5 7 -0.4490 0.0335 17 -4 0 -2.9990 -0.0766 17 -4 1 4.2708 -0.1019 17 -4 6 -0.2642 0.0107 17 -4 7 -3.6479 -0.0473 17 -4 8 -0.5102 -0.0302 17 -4 9 1.6188 0.0894 17 -3 0 -1.6311 0.1081 17 -3 1 -3.0070 -0.0035 17 -3 6 3.6500 0.0251 17 -3 7 3.9563 -0.0020 17 -3 8 -4.0277 -0.0084 17 -3 9 -2.1596 -0.0697 17 -3 10 1.1815 0.0164 17 -2 0 3.4285 0.0375 17 -2 1 -1.8998 0.0031 17 -2 6 -4.8657 -0.0124 17 -2 7 0.1794 0.0051 17 -2 8 5.5027 0.0148 17 -2 9 1.5686 0.0241 17 -2 10 -0.2199 -0.0524 17 -2 11 -1.2495 -0.0595 17 -1 0 -2.0120 -0.0515 17 -1 6 0.3997 0.0106 17 -1 7 -1.8411 -0.0060 17 -1 8 -1.7639 -0.0289 17 -1 9 -0.7215 0.0314 17 -1 10 2.4748 0.0108 17 -1 11 2.8201 0.0247 17 -1 12 -1.6766 0.0041 17 0 0 2.5597 -0.0286 17 0 1 2.7266 0.0068 17 0 6 3.2254 -0.0064 17 0 7 -3.7806 0.0052 17 0 8 -2.4951 -0.0033 17 0 9 0.7766 -0.0196 17 0 10 -1.5692 0.0439 17 0 11 0.5779 -0.0513 17 0 12 2.8426 -0.0031 17 1 0 -0.7233 0.0065 17 1 1 2.6616 -0.0326 17 1 2 6.0094 0.0245 17 1 3 -4.5765 -0.0191 17 1 5 -3.6679 0.0152 17 1 6 -1.2328 -0.0152 17 1 7 8.5536 0.0291 17 1 8 0.4473 -0.0093 17 1 9 -4.6179 -0.0101 17 1 10 -2.7018 -0.0126 17 1 11 -1.0726 0.0332 17 1 12 -1.1770 -0.0162 17 1 13 -0.2606 -0.0400 17 2 0 -0.9209 0.0069 17 2 1 0.5513 -0.0000 17 2 2 3.0081 -0.0124 17 2 3 3.8523 -0.0027 17 2 4 -1.9776 -0.0128 17 2 5 2.8588 0.0078 17 2 6 -1.2720 0.0094 17 2 7 -5.8684 -0.0093 17 2 8 2.3300 0.0282 17 2 9 4.7125 -0.0121 17 2 10 0.7817 0.0303 17 2 11 -2.5368 -0.0033 17 2 12 0.2233 -0.0377 17 2 13 -0.7466 0.0121 17 3 0 -0.9243 0.0038 17 3 1 -3.9073 -0.0015 17 3 2 -1.1335 -0.0030 17 3 3 3.7827 0.0025 17 3 4 1.2767 -0.0192 17 3 5 -1.8995 0.0102 17 3 6 1.0935 -0.0155 17 3 7 3.3206 -0.0096 17 3 8 1.3819 0.0110 17 3 9 -1.3387 -0.0094 17 3 10 1.2637 -0.0127 17 3 11 0.8820 0.0619 17 3 12 -1.2817 0.0048 17 3 13 1.0515 -0.0258 17 4 0 0.8282 0.0018 17 4 1 1.4966 -0.0058 17 4 2 -0.9604 0.0108 17 4 3 -1.8506 -0.0036 17 4 4 2.5914 0.0053 17 4 5 0.5993 -0.0049 17 4 6 -0.2028 0.0102 17 4 7 -3.2383 -0.0037 17 4 8 -2.5123 -0.0068 17 4 9 2.4184 0.0072 17 4 10 1.9801 -0.0631 17 4 11 2.5965 0.0028 17 4 12 -0.0068 0.0580 17 4 13 -0.8260 -0.0600 17 4 14 0.4672 -0.0162 17 5 0 0.4409 0.0485 17 5 1 -1.4862 0.0132 17 5 2 -1.7285 -0.0096 17 5 3 -0.0944 0.0230 17 5 4 -1.6584 -0.0192 17 5 5 0.9521 0.0058 17 5 6 0.7453 0.0183 17 5 7 1.8743 -0.0202 17 5 8 1.2759 0.0177 17 5 9 -2.9954 0.0156 17 5 10 -4.0331 0.0220 17 5 11 -0.6836 -0.0680 17 5 12 2.1589 0.0177 17 5 13 -0.0518 0.0476 17 5 14 0.1676 -0.0917 17 6 0 -0.3149 -0.0329 17 6 1 0.7801 0.0183 17 6 2 -0.1503 -0.0034 17 6 3 -2.1047 -0.0036 17 6 4 0.1022 0.0051 17 6 5 -1.3990 -0.0238 17 6 6 -1.5218 0.0125 17 6 7 -0.9456 -0.0053 17 6 8 -1.8922 -0.0193 17 6 9 3.9645 0.0268 17 6 10 3.3154 -0.0149 17 6 11 -2.6840 0.0132 17 6 12 -1.3309 -0.0324 17 6 13 -0.5862 0.0355 17 7 0 0.1720 -0.0931 17 7 1 1.1232 -0.0013 17 7 2 1.1239 -0.0277 17 7 3 1.1405 -0.0138 17 7 4 -1.4407 0.0382 17 7 5 -0.6707 -0.0425 17 7 6 0.9274 -0.0031 17 7 7 -0.1678 0.0478 17 7 8 -0.7449 -0.0673 17 7 9 -5.3787 0.0190 17 7 10 0.0510 0.0304 17 7 11 2.5983 -0.0242 17 7 12 0.0742 0.0188 17 7 13 1.9763 -0.0364 17 8 0 -0.6712 0.0820 17 8 1 -1.2527 -0.0384 17 8 2 -0.7058 0.0969 17 8 3 -0.0707 -0.0372 17 8 4 2.7743 -0.0370 17 8 5 1.8084 0.0594 17 8 6 -1.4259 -0.0624 17 8 7 0.8028 0.0095 17 8 8 1.5863 0.0630 17 8 9 1.3999 -0.0857 17 8 10 -2.2519 0.0740 17 8 11 -0.3432 -0.0197 17 8 12 -0.9094 -0.0246 17 9 1 0.9440 -0.0037 17 9 2 0.7460 -0.0761 17 9 3 -0.9409 0.0937 17 9 4 -2.0712 0.0404 17 9 5 -0.4119 0.0028 17 9 6 1.6533 0.0082 17 9 7 -0.1976 -0.0286 17 9 8 -0.0349 0.0124 17 9 9 0.7978 0.0054 17 9 10 0.1298 -0.0773 17 9 11 -0.5085 0.1051 17 10 4 0.1237 -0.0725 17 10 5 1.1699 0.0368 17 10 6 0.1889 0.0759 17 10 7 0.0074 -0.0581 17 10 8 0.6032 0.0333 18 -3 0 -0.5761 0.1395 18 -2 0 1.0506 0.0763 18 -1 0 0.0925 -0.0426 18 -1 8 -0.9095 -0.0255 18 -1 9 3.2914 0.0603 18 0 8 -0.6479 0.0006 18 0 9 -0.7967 -0.0252 18 1 0 1.1225 0.0031 18 1 1 1.4749 -0.0383 18 1 2 -0.1915 0.0293 18 1 7 4.9723 0.0121 18 1 8 -1.9946 -0.0215 18 1 9 -3.2733 -0.0151 18 1 10 -2.2434 0.0005 18 2 0 1.8664 0.0355 18 2 1 1.8597 -0.0065 18 2 2 1.4137 -0.0146 18 2 3 0.4349 0.0097 18 2 4 -0.7185 0.0004 18 2 6 -4.3111 0.0127 18 2 7 -3.3043 -0.0117 18 2 8 1.8771 0.0214 18 2 9 2.6813 -0.0114 18 2 10 -1.8807 -0.0060 18 3 0 -3.0673 0.0065 18 3 1 0.2819 0.0107 18 3 2 2.2783 -0.0105 18 3 3 0.6776 -0.0077 18 3 4 -1.0424 -0.0137 18 3 5 1.3335 0.0085 18 3 6 1.8698 -0.0043 18 3 7 2.8712 0.0057 18 3 8 0.3239 0.0172 18 3 9 -2.2216 -0.0064 18 3 10 1.4480 0.0287 18 3 11 -1.9149 0.0584 18 4 0 0.2037 -0.0527 18 4 1 -1.3507 -0.0038 18 4 2 1.2852 0.0136 18 4 3 2.5925 -0.0126 18 4 4 -0.0031 -0.0070 18 4 5 -1.9397 -0.0067 18 4 6 1.0803 0.0115 18 4 7 -3.0539 -0.0072 18 4 8 0.4535 -0.0091 18 4 9 3.9139 -0.0004 18 4 10 1.4226 -0.0644 18 4 11 2.6764 0.0565 18 5 0 1.7653 0.0552 18 5 1 -1.2438 -0.0189 18 5 2 -2.4753 -0.0040 18 5 3 1.1315 0.0167 18 5 4 2.5438 -0.0171 18 5 5 0.8957 0.0062 18 5 6 -0.4826 -0.0014 18 5 7 2.7809 -0.0045 18 5 8 -0.4973 0.0198 18 5 9 -3.3155 0.0262 18 5 10 -1.3884 -0.0043 18 6 0 -1.1794 0.0775 18 6 1 0.3858 0.0290 18 6 2 -1.2861 0.0126 18 6 3 -2.1855 0.0243 18 6 4 0.0143 0.0002 18 6 5 -0.3637 -0.0074 18 6 6 -0.8164 0.0206 18 6 7 -0.9830 -0.0221 18 6 8 0.4765 0.0013 18 6 9 3.9945 -0.0010 18 6 10 0.3953 0.0144 18 7 2 0.0587 -0.0577 18 7 3 -1.7881 0.0063 18 7 4 -1.7215 0.0373 18 7 5 0.5591 -0.0516 18 7 6 0.2400 0.0294 18 7 7 -1.2409 0.0275 18 7 8 -1.8331 -0.0684 18 7 9 -3.3866 0.0607 0 0 0 0.0 0.0 ; _shelx_fab_checksum 27031 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co1 Co 0.70446(5) 0.79936(5) 0.50744(4) 0.0378(2) Uani 1 1 d . . . . . Fe1 Fe 0.61208(5) 1.10669(5) 0.62567(5) 0.0403(2) Uani 1 1 d . . . . . O1 O 0.7818(3) 0.7705(3) 0.7647(3) 0.0684(12) Uani 1 1 d . . . . . C29 C 1.0961(4) 0.7413(5) 0.7090(4) 0.0650(17) Uani 1 1 d . . . . . H29A H 1.140679 0.751109 0.659757 0.078 Uiso 1 1 calc R U . . . H29B H 1.121352 0.732380 0.758705 0.078 Uiso 1 1 calc R U . . . C27 C 0.5562(9) 0.6121(9) 0.8983(6) 0.160(5) Uani 1 1 d . . . . . H27A H 0.498269 0.583550 0.891107 0.192 Uiso 1 1 calc R U . . . H27B H 0.572442 0.604115 0.951041 0.192 Uiso 1 1 calc R U . . . O4 O 0.7127(3) 0.7638(3) 0.2447(3) 0.0662(11) Uani 1 1 d . . . . . N1 N 0.6812(3) 0.9262(3) 0.5473(2) 0.0331(9) Uani 1 1 d . . . . . N2 N 0.7467(4) 1.2489(4) 0.4858(3) 0.0663(15) Uani 1 1 d . . . . . N10 N 0.6398(3) 0.7207(3) 0.6193(3) 0.0452(11) Uani 1 1 d . . . . . N12 N 0.8366(3) 0.7679(3) 0.5520(3) 0.0465(11) Uani 1 1 d . . . . . N11 N 0.5994(3) 0.6800(4) 0.7561(3) 0.0533(12) Uani 1 1 d . . . . . N14 N 0.7687(3) 0.8818(3) 0.3975(3) 0.0418(10) Uani 1 1 d . . . . . N15 N 0.8100(3) 0.9384(4) 0.2635(3) 0.0501(11) Uani 1 1 d . . . . . N16 N 0.7331(3) 0.6758(3) 0.4609(3) 0.0507(12) Uani 1 1 d . . . . . N8 N 0.5209(3) 1.0118(3) 0.7118(2) 0.0362(9) Uani 1 1 d . . . . . N5 N 0.5625(3) 1.1951(4) 0.7695(3) 0.0499(11) Uani 1 1 d . . . . . N4 N 0.5677(3) 1.2197(3) 0.6845(3) 0.0432(10) Uani 1 1 d . . . . . N6 N 0.7256(3) 1.0617(3) 0.6956(3) 0.0447(11) Uani 1 1 d . . . . . N3 N 0.4282(3) 1.1767(3) 0.5327(2) 0.0359(9) Uani 1 1 d . . . . . N18 N 0.8829(7) 0.7027(6) -0.0019(5) 0.119(3) Uani 1 1 d . . . . . C42 C 0.9065(9) 0.6329(9) -0.0570(6) 0.160(5) Uani 1 1 d . . . . . H42A H 0.976530 0.637774 -0.082249 0.240 Uiso 1 1 calc R U . . . H42B H 0.862479 0.652254 -0.099112 0.240 Uiso 1 1 calc R U . . . H42C H 0.895858 0.562903 -0.025982 0.240 Uiso 1 1 calc R U . . . C41 C 0.7828(8) 0.7037(9) 0.0455(7) 0.149(4) Uani 1 1 d . . . . . H41A H 0.756390 0.636437 0.056912 0.223 Uiso 1 1 calc R U . . . H41B H 0.737937 0.754604 0.014734 0.223 Uiso 1 1 calc R U . . . H41C H 0.787320 0.720587 0.096518 0.223 Uiso 1 1 calc R U . . . C21 C 0.6683(4) 0.7210(5) 0.6902(4) 0.0523(15) Uani 1 1 d . . . . . C22 C 0.7687(4) 0.7544(5) 0.6997(4) 0.0602(16) Uani 1 1 d . . . . . C23 C 0.8508(4) 0.7591(5) 0.6285(4) 0.0532(15) Uani 1 1 d . . . . . C24 C 0.9326(4) 0.7651(4) 0.5080(4) 0.0544(15) Uani 1 1 d . . . . . H24 H 0.946868 0.769295 0.451647 0.065 Uiso 1 1 calc R U . . . C25 C 1.0033(5) 0.7554(5) 0.5592(4) 0.0625(17) Uani 1 1 d . . . . . H25 H 1.073921 0.751055 0.544615 0.075 Uiso 1 1 calc R U . . . N13 N 0.9523(3) 0.7529(4) 0.6359(3) 0.0612(14) Uani 1 1 d . . . . . C28 C 0.9982(5) 0.7400(5) 0.7085(4) 0.0713(19) Uani 1 1 d . . . . . H28 H 0.955579 0.730065 0.758741 0.086 Uiso 1 1 calc R U . . . C26 C 0.6081(5) 0.6577(7) 0.8413(5) 0.096(3) Uani 1 1 d . . . . . H26 H 0.664399 0.683836 0.853562 0.115 Uiso 1 1 calc R U . . . C20 C 0.5220(4) 0.6530(4) 0.7229(4) 0.0528(15) Uani 1 1 d . . . . . H20 H 0.463232 0.621859 0.752303 0.063 Uiso 1 1 calc R U . . . C19 C 0.5460(4) 0.6795(4) 0.6395(4) 0.0504(14) Uani 1 1 d . . . . . H19 H 0.505349 0.671090 0.602016 0.060 Uiso 1 1 calc R U . . . C30 C 0.8099(4) 0.9760(4) 0.3812(4) 0.0475(13) Uani 1 1 d . . . . . H30 H 0.818721 1.010459 0.420489 0.057 Uiso 1 1 calc R U . . . C31 C 0.8357(4) 1.0110(4) 0.2983(4) 0.0533(15) Uani 1 1 d . . . . . H31 H 0.865226 1.072897 0.270727 0.064 Uiso 1 1 calc R U . . . C32 C 0.7694(4) 0.8607(4) 0.3247(4) 0.0475(13) Uani 1 1 d . . . . . C33 C 0.7337(4) 0.7664(4) 0.3119(4) 0.0503(14) Uani 1 1 d . . . . . C34 C 0.7317(4) 0.6748(4) 0.3838(4) 0.0529(15) Uani 1 1 d . . . . . N17 N 0.7387(3) 0.5736(4) 0.3762(4) 0.0604(14) Uani 1 1 d . . . . . C39 C 0.7376(5) 0.5401(5) 0.3047(5) 0.080(2) Uani 1 1 d . . . . . H39 H 0.748302 0.588578 0.254209 0.096 Uiso 1 1 calc R U . . . C40 C 0.7222(5) 0.4435(5) 0.3039(6) 0.093(3) Uani 1 1 d . . . . . H40A H 0.711190 0.393089 0.353239 0.112 Uiso 1 1 calc R U . . . H40B H 0.722394 0.426561 0.253939 0.112 Uiso 1 1 calc R U . . . C36 C 0.7451(4) 0.5108(5) 0.4533(5) 0.071(2) Uani 1 1 d . . . . . H36 H 0.751475 0.438648 0.467506 0.085 Uiso 1 1 calc R U . . . C35 C 0.7402(4) 0.5744(5) 0.5050(5) 0.0653(18) Uani 1 1 d . . . . . H35 H 0.741506 0.552403 0.561669 0.078 Uiso 1 1 calc R U . . . C37 C 0.8354(5) 0.9419(5) 0.1769(4) 0.0697(18) Uani 1 1 d . . . . . H37 H 0.840649 0.879727 0.161015 0.084 Uiso 1 1 calc R U . . . C38 C 0.8516(6) 1.0288(6) 0.1184(5) 0.088(2) Uani 1 1 d . . . . . H38A H 0.846878 1.092099 0.132445 0.105 Uiso 1 1 calc R U . . . H38B H 0.867816 1.026303 0.063392 0.105 Uiso 1 1 calc R U . . . C1 C 0.6541(3) 0.9969(4) 0.5753(3) 0.0360(11) Uani 1 1 d . . . . . C2 C 0.6970(4) 1.1947(4) 0.5382(4) 0.0480(14) Uani 1 1 d . . . . . N9 N 0.5199(3) 1.0121(3) 0.7925(3) 0.0465(11) Uani 1 1 d . . . . . B1 B 0.5898(5) 1.0834(5) 0.8125(4) 0.0518(16) Uani 1 1 d . . . . . H1 H 0.582821 1.075194 0.872288 0.062 Uiso 1 1 calc R U . . . C6 C 0.5306(5) 1.2800(5) 0.7981(4) 0.0595(16) Uani 1 1 d . . . . . C8 C 0.5145(6) 1.2784(6) 0.8863(4) 0.088(2) Uani 1 1 d . . . . . H8A H 0.491920 1.346723 0.892999 0.132 Uiso 1 1 calc R U . . . H8B H 0.463536 1.230855 0.914929 0.132 Uiso 1 1 calc R U . . . H8C H 0.577579 1.256687 0.908642 0.132 Uiso 1 1 calc R U . . . C5 C 0.5149(4) 1.3604(5) 0.7312(4) 0.0586(16) Uani 1 1 d . . . . . H5 H 0.492713 1.428367 0.732512 0.070 Uiso 1 1 calc R U . . . C4 C 0.5382(4) 1.3221(4) 0.6616(4) 0.0473(13) Uani 1 1 d . . . . . C7 C 0.5306(4) 1.3794(4) 0.5751(3) 0.0510(14) Uani 1 1 d . . . . . H7A H 0.508428 1.450573 0.573285 0.076 Uiso 1 1 calc R U . . . H7B H 0.596341 1.376201 0.542239 0.076 Uiso 1 1 calc R U . . . H7C H 0.482035 1.348633 0.553772 0.076 Uiso 1 1 calc R U . . . N7 N 0.7005(3) 1.0536(4) 0.7790(3) 0.0542(12) Uani 1 1 d . . . . . C9 C 0.8253(4) 1.0320(4) 0.6833(4) 0.0530(15) Uani 1 1 d . . . . . C12 C 0.8831(4) 1.0299(4) 0.6001(4) 0.0590(16) Uani 1 1 d . . . . . H12A H 0.953097 1.006251 0.605484 0.088 Uiso 1 1 calc R U . . . H12B H 0.852766 0.983726 0.577066 0.088 Uiso 1 1 calc R U . . . H12C H 0.880566 1.098515 0.564286 0.088 Uiso 1 1 calc R U . . . C10 C 0.8622(5) 1.0054(5) 0.7598(5) 0.072(2) Uani 1 1 d . . . . . H10 H 0.929251 0.983342 0.768409 0.087 Uiso 1 1 calc R U . . . C11 C 0.7839(5) 1.0173(5) 0.8181(4) 0.0674(18) Uani 1 1 d . . . . . C13 C 0.7789(7) 0.9977(8) 0.9102(5) 0.120(3) Uani 1 1 d . . . . . H13A H 0.710443 1.014400 0.933830 0.181 Uiso 1 1 calc R U . . . H13B H 0.797631 0.925870 0.932977 0.181 Uiso 1 1 calc R U . . . H13C H 0.825260 1.040207 0.922554 0.181 Uiso 1 1 calc R U . . . C16 C 0.4528(5) 0.9430(5) 0.8415(3) 0.0562(15) Uani 1 1 d . . . . . C18 C 0.4330(6) 0.9283(6) 0.9329(4) 0.094(3) Uani 1 1 d . . . . . H18A H 0.496103 0.907760 0.955395 0.142 Uiso 1 1 calc R U . . . H18B H 0.385542 0.875487 0.956397 0.142 Uiso 1 1 calc R U . . . H18C H 0.404739 0.992333 0.945566 0.142 Uiso 1 1 calc R U . . . C15 C 0.4123(4) 0.8975(4) 0.7924(3) 0.0529(14) Uani 1 1 d . . . . . H15 H 0.365457 0.846405 0.809335 0.063 Uiso 1 1 calc R U . . . C14 C 0.4544(4) 0.9423(4) 0.7107(3) 0.0380(11) Uani 1 1 d . . . . . C17 C 0.4323(4) 0.9185(4) 0.6343(3) 0.0448(13) Uani 1 1 d . . . . . H17A H 0.382791 0.866919 0.648590 0.067 Uiso 1 1 calc R U . . . H17B H 0.405615 0.980458 0.598842 0.067 Uiso 1 1 calc R U . . . H17C H 0.494187 0.892690 0.606068 0.067 Uiso 1 1 calc R U . . . C3 C 0.5011(4) 1.1489(4) 0.5654(3) 0.0375(11) Uani 1 1 d . . . . . O44 O 0.9508(6) 0.8191(8) 0.0520(7) 0.198(4) Uani 1 1 d . . . . . C43 C 0.9630(12) 0.7603(11) 0.0012(11) 0.209(7) Uani 1 1 d . . . . . H43 H 1.024768 0.756500 -0.033029 0.251 Uiso 1 1 calc R U . . . F2 F 0.3151(7) 0.5655(9) 0.8893(8) 0.252(4) Uani 1 1 d . . . . . F4 F 0.2576(13) 0.6341(15) 0.9846(7) 0.483(15) Uani 1 1 d . . . . . B2 B 0.230(2) 0.654(4) 0.911(2) 0.38(3) Uani 1 1 d . . . . . F3 F 0.2481(14) 0.7071(11) 0.8707(11) 0.377(11) Uani 1 1 d . . . . . F1 F 0.1607(6) 0.5932(8) 0.9117(7) 0.264(5) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co1 0.0282(4) 0.0362(4) 0.0483(4) -0.0100(3) -0.0040(3) -0.0025(3) Fe1 0.0288(4) 0.0342(4) 0.0561(5) -0.0098(3) -0.0004(3) -0.0058(3) O1 0.050(3) 0.094(3) 0.072(3) -0.035(3) -0.004(2) -0.020(2) C29 0.046(4) 0.065(4) 0.092(5) -0.033(4) -0.011(3) -0.004(3) C27 0.168(10) 0.214(12) 0.097(7) 0.026(7) -0.046(7) -0.131(10) O4 0.071(3) 0.061(3) 0.071(3) -0.019(2) -0.017(2) -0.005(2) N1 0.026(2) 0.036(2) 0.038(2) -0.0093(19) -0.0039(16) -0.0009(17) N2 0.044(3) 0.044(3) 0.096(4) -0.007(3) 0.018(3) -0.006(2) N10 0.034(2) 0.045(3) 0.061(3) -0.019(2) -0.006(2) -0.0037(19) N12 0.034(2) 0.057(3) 0.048(3) -0.013(2) 0.001(2) -0.012(2) N11 0.037(3) 0.068(3) 0.057(3) -0.020(3) 0.001(2) -0.015(2) N14 0.032(2) 0.033(2) 0.059(3) -0.010(2) -0.007(2) -0.0025(18) N15 0.045(3) 0.051(3) 0.047(3) -0.004(2) -0.002(2) 0.001(2) N16 0.033(2) 0.043(3) 0.072(3) -0.007(2) 0.000(2) -0.0085(19) N8 0.035(2) 0.033(2) 0.038(2) -0.0068(18) -0.0015(17) -0.0023(17) N5 0.040(3) 0.057(3) 0.056(3) -0.021(2) -0.005(2) -0.004(2) N4 0.035(2) 0.043(3) 0.052(3) -0.013(2) -0.0041(19) -0.0028(19) N6 0.036(3) 0.042(3) 0.061(3) -0.021(2) -0.010(2) 0.0001(19) N3 0.035(2) 0.033(2) 0.039(2) -0.0086(18) -0.0052(19) -0.0002(18) N18 0.123(7) 0.109(6) 0.133(7) -0.056(5) 0.002(5) -0.008(5) C42 0.192(12) 0.180(11) 0.124(9) -0.065(8) 0.011(8) -0.058(10) C41 0.110(8) 0.192(12) 0.143(9) -0.053(8) 0.004(7) 0.002(8) C21 0.032(3) 0.070(4) 0.059(4) -0.026(3) 0.006(3) -0.012(3) C22 0.049(4) 0.074(4) 0.067(4) -0.028(3) -0.009(3) -0.017(3) C23 0.034(3) 0.065(4) 0.059(4) -0.014(3) 0.002(3) -0.013(3) C24 0.037(3) 0.056(4) 0.065(4) -0.013(3) 0.007(3) -0.006(3) C25 0.042(3) 0.062(4) 0.072(4) 0.001(3) 0.004(3) -0.012(3) N13 0.031(3) 0.077(4) 0.075(4) -0.015(3) -0.003(2) -0.017(2) C28 0.039(4) 0.104(6) 0.073(5) -0.022(4) -0.006(3) -0.011(3) C26 0.065(5) 0.167(8) 0.066(5) -0.041(5) 0.020(4) -0.063(5) C20 0.036(3) 0.045(3) 0.076(4) -0.017(3) 0.002(3) -0.007(2) C19 0.037(3) 0.041(3) 0.075(4) -0.016(3) -0.011(3) -0.003(2) C30 0.038(3) 0.036(3) 0.067(4) -0.007(3) -0.007(3) -0.009(2) C31 0.042(3) 0.040(3) 0.078(4) -0.013(3) -0.009(3) -0.005(2) C32 0.039(3) 0.038(3) 0.062(4) -0.007(3) -0.008(3) -0.002(2) C33 0.037(3) 0.044(3) 0.067(4) -0.005(3) -0.013(3) -0.001(2) C34 0.040(3) 0.042(3) 0.079(5) -0.019(3) -0.006(3) -0.007(2) N17 0.039(3) 0.045(3) 0.097(4) -0.023(3) 0.002(3) -0.007(2) C39 0.062(4) 0.060(5) 0.124(7) -0.037(4) -0.009(4) -0.004(3) C40 0.061(5) 0.052(4) 0.170(8) -0.041(5) -0.009(5) 0.006(3) C36 0.039(3) 0.036(3) 0.119(6) -0.001(4) 0.014(4) -0.004(3) C35 0.033(3) 0.042(4) 0.100(5) 0.009(4) 0.007(3) 0.003(2) C37 0.066(4) 0.066(4) 0.080(5) -0.023(4) -0.008(4) -0.007(3) C38 0.102(6) 0.087(6) 0.075(5) -0.007(4) -0.015(4) -0.033(5) C1 0.023(2) 0.038(3) 0.040(3) 0.004(2) 0.000(2) -0.006(2) C2 0.034(3) 0.036(3) 0.068(4) -0.013(3) 0.005(3) 0.002(2) N9 0.050(3) 0.045(3) 0.045(3) -0.010(2) -0.006(2) -0.004(2) B1 0.050(4) 0.058(4) 0.052(4) -0.021(3) -0.013(3) 0.005(3) C6 0.057(4) 0.061(4) 0.070(4) -0.036(4) -0.009(3) 0.005(3) C8 0.103(6) 0.079(5) 0.096(6) -0.049(4) -0.022(5) 0.017(4) C5 0.055(4) 0.043(3) 0.084(5) -0.030(3) -0.008(3) 0.003(3) C4 0.036(3) 0.038(3) 0.070(4) -0.020(3) -0.001(3) -0.004(2) C7 0.046(3) 0.031(3) 0.073(4) -0.010(3) -0.004(3) -0.006(2) N7 0.047(3) 0.057(3) 0.066(3) -0.022(3) -0.018(2) -0.002(2) C9 0.035(3) 0.049(3) 0.081(4) -0.023(3) -0.011(3) -0.006(2) C12 0.026(3) 0.052(3) 0.103(5) -0.026(3) -0.007(3) -0.004(2) C10 0.046(4) 0.081(5) 0.106(6) -0.043(4) -0.036(4) 0.011(3) C11 0.054(4) 0.080(5) 0.082(5) -0.039(4) -0.033(4) 0.015(3) C13 0.103(7) 0.182(10) 0.098(6) -0.073(6) -0.052(5) 0.045(6) C16 0.063(4) 0.059(4) 0.040(3) 0.003(3) -0.004(3) -0.016(3) C18 0.116(7) 0.120(7) 0.042(4) -0.003(4) 0.001(4) -0.041(5) C15 0.055(4) 0.050(3) 0.048(3) 0.000(3) 0.000(3) -0.015(3) C14 0.035(3) 0.034(3) 0.044(3) -0.008(2) -0.004(2) -0.002(2) C17 0.036(3) 0.043(3) 0.057(3) -0.016(3) -0.004(2) -0.008(2) C3 0.035(3) 0.031(3) 0.042(3) -0.008(2) 0.007(2) -0.003(2) O44 0.138(7) 0.206(9) 0.292(12) -0.135(9) -0.041(7) -0.007(6) C43 0.184(14) 0.174(13) 0.34(2) -0.173(14) -0.047(13) -0.021(11) F2 0.164(8) 0.285(13) 0.316(13) -0.059(10) -0.049(8) -0.069(8) F4 0.58(3) 0.70(3) 0.257(12) -0.313(17) -0.267(15) 0.40(2) B2 0.23(2) 0.72(7) 0.34(4) -0.40(5) 0.23(3) -0.36(4) F3 0.39(2) 0.218(12) 0.49(2) 0.093(12) -0.165(17) -0.195(14) F1 0.136(7) 0.297(12) 0.313(12) 0.007(9) -0.001(7) -0.057(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Co1 N10 88.50(16) . . ? N1 Co1 N12 90.16(17) . . ? N1 Co1 N14 89.62(16) . . ? N1 Co1 N16 176.48(17) . . ? N12 Co1 N10 86.67(17) . . ? N12 Co1 N14 93.07(17) . . ? N12 Co1 N16 89.47(19) . . ? N14 Co1 N10 178.10(17) . . ? N16 Co1 N10 94.98(18) . . ? N16 Co1 N14 86.90(18) . . ? N3 Co1 N1 91.39(15) 2_676 . ? N3 Co1 N10 90.74(17) 2_676 . ? N3 Co1 N12 176.95(17) 2_676 . ? N3 Co1 N14 89.57(16) 2_676 . ? N3 Co1 N16 89.14(17) 2_676 . ? N8 Fe1 N4 89.34(16) . . ? N8 Fe1 N6 89.25(17) . . ? N4 Fe1 N6 88.67(17) . . ? C1 Fe1 N8 88.81(17) . . ? C1 Fe1 N4 177.45(19) . . ? C1 Fe1 N6 89.54(19) . . ? C1 Fe1 C2 88.8(2) . . ? C1 Fe1 C3 92.4(2) . . ? C2 Fe1 N8 176.7(2) . . ? C2 Fe1 N4 93.1(2) . . ? C2 Fe1 N6 93.0(2) . . ? C3 Fe1 N8 88.47(18) . . ? C3 Fe1 N4 89.33(19) . . ? C3 Fe1 N6 176.98(19) . . ? C3 Fe1 C2 89.3(2) . . ? H29A C29 H29B 120.0 . . ? C28 C29 H29A 120.0 . . ? C28 C29 H29B 120.0 . . ? H27A C27 H27B 120.0 . . ? C26 C27 H27A 120.0 . . ? C26 C27 H27B 120.0 . . ? C1 N1 Co1 170.6(4) . . ? C21 N10 Co1 125.2(4) . . ? C21 N10 C19 105.3(5) . . ? C19 N10 Co1 127.7(4) . . ? C23 N12 Co1 126.6(4) . . ? C23 N12 C24 105.7(5) . . ? C24 N12 Co1 127.1(4) . . ? C21 N11 C26 129.0(5) . . ? C21 N11 C20 104.8(5) . . ? C20 N11 C26 125.9(5) . . ? C30 N14 Co1 127.1(4) . . ? C32 N14 Co1 126.2(3) . . ? C32 N14 C30 106.4(4) . . ? C31 N15 C37 123.5(5) . . ? C32 N15 C31 108.0(5) . . ? C32 N15 C37 128.0(5) . . ? C34 N16 Co1 125.9(4) . . ? C34 N16 C35 107.0(5) . . ? C35 N16 Co1 126.2(5) . . ? N9 N8 Fe1 118.2(3) . . ? C14 N8 Fe1 134.9(3) . . ? C14 N8 N9 106.9(4) . . ? N4 N5 B1 117.6(4) . . ? C6 N5 N4 110.0(5) . . ? C6 N5 B1 132.4(5) . . ? N5 N4 Fe1 118.3(3) . . ? C4 N4 Fe1 135.6(4) . . ? C4 N4 N5 106.1(4) . . ? N7 N6 Fe1 117.2(3) . . ? C9 N6 Fe1 136.4(4) . . ? C9 N6 N7 106.4(4) . . ? C3 N3 Co1 169.4(4) . 2_676 ? C41 N18 C42 118.6(9) . . ? C43 N18 C42 115.3(10) . . ? C43 N18 C41 126.0(10) . . ? N18 C42 H42A 109.5 . . ? N18 C42 H42B 109.5 . . ? N18 C42 H42C 109.5 . . ? H42A C42 H42B 109.5 . . ? H42A C42 H42C 109.5 . . ? H42B C42 H42C 109.5 . . ? N18 C41 H41A 109.5 . . ? N18 C41 H41B 109.5 . . ? N18 C41 H41C 109.5 . . ? H41A C41 H41B 109.5 . . ? H41A C41 H41C 109.5 . . ? H41B C41 H41C 109.5 . . ? N10 C21 N11 112.8(5) . . ? N10 C21 C22 124.8(5) . . ? N11 C21 C22 122.2(5) . . ? O1 C22 C21 120.4(5) . . ? O1 C22 C23 123.3(5) . . ? C23 C22 C21 116.2(5) . . ? N12 C23 C22 125.5(5) . . ? N12 C23 N13 111.5(5) . . ? N13 C23 C22 123.0(5) . . ? N12 C24 H24 125.4 . . ? C25 C24 N12 109.3(5) . . ? C25 C24 H24 125.4 . . ? C24 C25 H25 126.2 . . ? C24 C25 N13 107.5(5) . . ? N13 C25 H25 126.2 . . ? C23 N13 C28 128.4(5) . . ? C25 N13 C23 105.9(5) . . ? C25 N13 C28 125.7(5) . . ? C29 C28 N13 124.2(6) . . ? C29 C28 H28 117.9 . . ? N13 C28 H28 117.9 . . ? C27 C26 N11 130.3(8) . . ? C27 C26 H26 114.8 . . ? N11 C26 H26 114.8 . . ? N11 C20 H20 126.0 . . ? C19 C20 N11 108.0(5) . . ? C19 C20 H20 126.0 . . ? N10 C19 H19 125.5 . . ? C20 C19 N10 109.0(5) . . ? C20 C19 H19 125.5 . . ? N14 C30 H30 125.5 . . ? C31 C30 N14 109.1(5) . . ? C31 C30 H30 125.5 . . ? N15 C31 C30 106.7(5) . . ? N15 C31 H31 126.6 . . ? C30 C31 H31 126.6 . . ? N14 C32 N15 109.8(5) . . ? N14 C32 C33 125.7(5) . . ? N15 C32 C33 124.5(5) . . ? O4 C33 C32 121.1(5) . . ? O4 C33 C34 123.4(5) . . ? C32 C33 C34 115.4(5) . . ? N16 C34 C33 126.5(5) . . ? N16 C34 N17 110.1(5) . . ? N17 C34 C33 123.1(6) . . ? C34 N17 C39 127.5(6) . . ? C36 N17 C34 106.8(5) . . ? C36 N17 C39 125.7(6) . . ? N17 C39 H39 117.7 . . ? C40 C39 N17 124.5(8) . . ? C40 C39 H39 117.7 . . ? C39 C40 H40A 120.0 . . ? C39 C40 H40B 120.0 . . ? H40A C40 H40B 120.0 . . ? N17 C36 H36 126.7 . . ? C35 C36 N17 106.6(5) . . ? C35 C36 H36 126.7 . . ? N16 C35 H35 125.2 . . ? C36 C35 N16 109.5(6) . . ? C36 C35 H35 125.2 . . ? N15 C37 H37 118.1 . . ? C38 C37 N15 123.8(7) . . ? C38 C37 H37 118.1 . . ? C37 C38 H38A 120.0 . . ? C37 C38 H38B 120.0 . . ? H38A C38 H38B 120.0 . . ? N1 C1 Fe1 177.1(4) . . ? N2 C2 Fe1 178.8(5) . . ? N8 N9 B1 118.4(4) . . ? N8 N9 C16 109.4(4) . . ? C16 N9 B1 132.1(5) . . ? N5 B1 N9 109.4(5) . . ? N5 B1 H1 110.2 . . ? N5 B1 N7 108.9(5) . . ? N9 B1 H1 110.2 . . ? N9 B1 N7 107.8(5) . . ? N7 B1 H1 110.2 . . ? N5 C6 C8 123.1(6) . . ? N5 C6 C5 107.3(5) . . ? C5 C6 C8 129.5(6) . . ? C6 C8 H8A 109.5 . . ? C6 C8 H8B 109.5 . . ? C6 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C6 C5 H5 126.2 . . ? C6 C5 C4 107.6(5) . . ? C4 C5 H5 126.2 . . ? N4 C4 C5 109.1(5) . . ? N4 C4 C7 123.6(5) . . ? C5 C4 C7 127.3(5) . . ? C4 C7 H7A 109.5 . . ? C4 C7 H7B 109.5 . . ? C4 C7 H7C 109.5 . . ? H7A C7 H7B 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? N6 N7 B1 118.7(4) . . ? C11 N7 N6 110.1(5) . . ? C11 N7 B1 131.2(5) . . ? N6 C9 C12 123.4(5) . . ? N6 C9 C10 108.4(6) . . ? C10 C9 C12 128.2(6) . . ? C9 C12 H12A 109.5 . . ? C9 C12 H12B 109.5 . . ? C9 C12 H12C 109.5 . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C9 C10 H10 125.9 . . ? C11 C10 C9 108.1(6) . . ? C11 C10 H10 125.9 . . ? N7 C11 C13 122.1(6) . . ? C10 C11 N7 106.9(6) . . ? C10 C11 C13 131.0(6) . . ? C11 C13 H13A 109.5 . . ? C11 C13 H13B 109.5 . . ? C11 C13 H13C 109.5 . . ? H13A C13 H13B 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? N9 C16 C18 121.8(6) . . ? C15 C16 N9 108.0(5) . . ? C15 C16 C18 130.1(6) . . ? C16 C18 H18A 109.5 . . ? C16 C18 H18B 109.5 . . ? C16 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C16 C15 H15 126.6 . . ? C16 C15 C14 106.8(5) . . ? C14 C15 H15 126.6 . . ? N8 C14 C15 108.7(4) . . ? N8 C14 C17 124.2(4) . . ? C15 C14 C17 127.0(5) . . ? C14 C17 H17A 109.5 . . ? C14 C17 H17B 109.5 . . ? C14 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? N3 C3 Fe1 175.3(4) . . ? N18 C43 H43 120.3 . . ? O44 C43 N18 119.4(14) . . ? O44 C43 H43 120.3 . . ? F4 B2 F2 89(4) . . ? F3 B2 F2 100(3) . . ? F3 B2 F4 125(3) . . ? F3 B2 F1 125(5) . . ? F1 B2 F2 88(2) . . ? F1 B2 F4 110(3) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Co1 N1 1.960(4) . ? Co1 N10 2.017(4) . ? Co1 N12 1.982(4) . ? Co1 N14 2.009(4) . ? Co1 N16 1.985(5) . ? Co1 N3 1.954(4) 2_676 ? Fe1 N8 1.999(4) . ? Fe1 N4 2.006(4) . ? Fe1 N6 2.012(4) . ? Fe1 C1 1.875(6) . ? Fe1 C2 1.920(6) . ? Fe1 C3 1.882(6) . ? O1 C22 1.217(7) . ? C29 H29A 0.9300 . ? C29 H29B 0.9300 . ? C29 C28 1.302(8) . ? C27 H27A 0.9300 . ? C27 H27B 0.9300 . ? C27 C26 1.160(10) . ? O4 C33 1.224(6) . ? N1 C1 1.163(6) . ? N2 C2 1.152(6) . ? N10 C21 1.315(7) . ? N10 C19 1.370(6) . ? N12 C23 1.312(7) . ? N12 C24 1.371(6) . ? N11 C21 1.358(6) . ? N11 C26 1.417(8) . ? N11 C20 1.366(7) . ? N14 C30 1.368(6) . ? N14 C32 1.333(7) . ? N15 C31 1.354(7) . ? N15 C32 1.350(7) . ? N15 C37 1.441(8) . ? N16 C34 1.312(7) . ? N16 C35 1.370(7) . ? N8 N9 1.366(5) . ? N8 C14 1.350(6) . ? N5 N4 1.383(6) . ? N5 B1 1.517(8) . ? N5 C6 1.349(7) . ? N4 C4 1.356(6) . ? N6 N7 1.376(6) . ? N6 C9 1.340(7) . ? N3 C3 1.170(6) . ? N18 C42 1.461(11) . ? N18 C41 1.438(11) . ? N18 C43 1.391(14) . ? C42 H42A 0.9600 . ? C42 H42B 0.9600 . ? C42 H42C 0.9600 . ? C41 H41A 0.9600 . ? C41 H41B 0.9600 . ? C41 H41C 0.9600 . ? C21 C22 1.493(7) . ? C22 C23 1.482(8) . ? C23 N13 1.365(7) . ? C24 H24 0.9300 . ? C24 C25 1.351(8) . ? C25 H25 0.9300 . ? C25 N13 1.359(7) . ? N13 C28 1.421(8) . ? C28 H28 0.9300 . ? C26 H26 0.9300 . ? C20 H20 0.9300 . ? C20 C19 1.358(8) . ? C19 H19 0.9300 . ? C30 H30 0.9300 . ? C30 C31 1.359(8) . ? C31 H31 0.9300 . ? C32 C33 1.469(7) . ? C33 C34 1.486(8) . ? C34 N17 1.384(7) . ? N17 C39 1.399(8) . ? N17 C36 1.367(8) . ? C39 H39 0.9300 . ? C39 C40 1.331(8) . ? C40 H40A 0.9300 . ? C40 H40B 0.9300 . ? C36 H36 0.9300 . ? C36 C35 1.361(9) . ? C35 H35 0.9300 . ? C37 H37 0.9300 . ? C37 C38 1.329(9) . ? C38 H38A 0.9300 . ? C38 H38B 0.9300 . ? N9 B1 1.528(8) . ? N9 C16 1.368(6) . ? B1 H1 0.9800 . ? B1 N7 1.538(8) . ? C6 C8 1.469(8) . ? C6 C5 1.371(8) . ? C8 H8A 0.9600 . ? C8 H8B 0.9600 . ? C8 H8C 0.9600 . ? C5 H5 0.9300 . ? C5 C4 1.382(7) . ? C4 C7 1.481(8) . ? C7 H7A 0.9600 . ? C7 H7B 0.9600 . ? C7 H7C 0.9600 . ? N7 C11 1.363(7) . ? C9 C12 1.499(8) . ? C9 C10 1.404(8) . ? C12 H12A 0.9600 . ? C12 H12B 0.9600 . ? C12 H12C 0.9600 . ? C10 H10 0.9300 . ? C10 C11 1.341(9) . ? C11 C13 1.504(9) . ? C13 H13A 0.9600 . ? C13 H13B 0.9600 . ? C13 H13C 0.9600 . ? C16 C18 1.491(8) . ? C16 C15 1.351(8) . ? C18 H18A 0.9600 . ? C18 H18B 0.9600 . ? C18 H18C 0.9600 . ? C15 H15 0.9300 . ? C15 C14 1.406(7) . ? C14 C17 1.490(7) . ? C17 H17A 0.9600 . ? C17 H17B 0.9600 . ? C17 H17C 0.9600 . ? O44 C43 1.289(13) . ? C43 H43 0.9300 . ? F2 B2 1.62(4) . ? F4 B2 1.30(4) . ? B2 F3 0.87(5) . ? B2 F1 1.289(19) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Co1 N10 C21 N11 167.0(4) . . . . ? Co1 N10 C21 C22 -17.6(8) . . . . ? Co1 N10 C19 C20 -167.0(4) . . . . ? Co1 N12 C23 C22 10.4(8) . . . . ? Co1 N12 C23 N13 -170.6(4) . . . . ? Co1 N12 C24 C25 171.5(4) . . . . ? Co1 N14 C30 C31 -173.6(3) . . . . ? Co1 N14 C32 N15 173.6(3) . . . . ? Co1 N14 C32 C33 -7.6(7) . . . . ? Co1 N16 C34 C33 15.9(8) . . . . ? Co1 N16 C34 N17 -170.2(3) . . . . ? Co1 N16 C35 C36 170.8(4) . . . . ? Fe1 N8 N9 B1 -1.1(6) . . . . ? Fe1 N8 N9 C16 179.6(4) . . . . ? Fe1 N8 C14 C15 179.6(4) . . . . ? Fe1 N8 C14 C17 0.2(8) . . . . ? Fe1 N4 C4 C5 179.3(4) . . . . ? Fe1 N4 C4 C7 0.9(8) . . . . ? Fe1 N6 N7 B1 -2.5(6) . . . . ? Fe1 N6 N7 C11 176.8(4) . . . . ? Fe1 N6 C9 C12 3.0(8) . . . . ? Fe1 N6 C9 C10 -177.3(4) . . . . ? O1 C22 C23 N12 -162.2(6) . . . . ? O1 C22 C23 N13 18.9(10) . . . . ? O4 C33 C34 N16 -165.5(6) . . . . ? O4 C33 C34 N17 21.4(8) . . . . ? N10 C21 C22 O1 166.3(6) . . . . ? N10 C21 C22 C23 -17.6(9) . . . . ? N12 C23 N13 C25 -1.7(7) . . . . ? N12 C23 N13 C28 -178.1(6) . . . . ? N12 C24 C25 N13 -0.6(7) . . . . ? N11 C21 C22 O1 -18.7(9) . . . . ? N11 C21 C22 C23 157.3(5) . . . . ? N11 C20 C19 N10 1.7(6) . . . . ? N14 C30 C31 N15 0.2(6) . . . . ? N14 C32 C33 O4 161.4(5) . . . . ? N14 C32 C33 C34 -22.3(8) . . . . ? N15 C32 C33 O4 -20.1(8) . . . . ? N15 C32 C33 C34 156.2(5) . . . . ? N16 C34 N17 C39 178.5(5) . . . . ? N16 C34 N17 C36 -0.3(6) . . . . ? N8 N9 B1 N5 59.8(6) . . . . ? N8 N9 B1 N7 -58.5(6) . . . . ? N8 N9 C16 C18 -178.3(6) . . . . ? N8 N9 C16 C15 0.9(6) . . . . ? N5 N4 C4 C5 -0.1(6) . . . . ? N5 N4 C4 C7 -178.5(5) . . . . ? N5 B1 N7 N6 -57.9(6) . . . . ? N5 B1 N7 C11 122.9(6) . . . . ? N5 C6 C5 C4 -0.1(7) . . . . ? N4 N5 B1 N9 -58.1(6) . . . . ? N4 N5 B1 N7 59.4(6) . . . . ? N4 N5 C6 C8 178.3(6) . . . . ? N4 N5 C6 C5 0.0(6) . . . . ? N6 N7 C11 C10 1.8(7) . . . . ? N6 N7 C11 C13 -178.3(6) . . . . ? N6 C9 C10 C11 1.2(7) . . . . ? C42 N18 C43 O44 -175.8(13) . . . . ? C41 N18 C43 O44 2(2) . . . . ? C21 N10 C19 C20 -1.9(6) . . . . ? C21 N11 C26 C27 -169.9(12) . . . . ? C21 N11 C20 C19 -0.8(6) . . . . ? C21 C22 C23 N12 21.9(9) . . . . ? C21 C22 C23 N13 -157.0(6) . . . . ? C22 C23 N13 C25 177.3(5) . . . . ? C22 C23 N13 C28 0.9(10) . . . . ? C23 N12 C24 C25 -0.4(6) . . . . ? C23 N13 C28 C29 -175.6(6) . . . . ? C24 N12 C23 C22 -177.7(6) . . . . ? C24 N12 C23 N13 1.3(6) . . . . ? C24 C25 N13 C23 1.4(7) . . . . ? C24 C25 N13 C28 177.9(6) . . . . ? C25 N13 C28 C29 8.7(11) . . . . ? C26 N11 C21 N10 172.9(6) . . . . ? C26 N11 C21 C22 -2.6(10) . . . . ? C26 N11 C20 C19 -174.4(6) . . . . ? C20 N11 C21 N10 -0.4(6) . . . . ? C20 N11 C21 C22 -175.9(5) . . . . ? C20 N11 C26 C27 2.1(17) . . . . ? C19 N10 C21 N11 1.4(6) . . . . ? C19 N10 C21 C22 176.8(6) . . . . ? C30 N14 C32 N15 0.3(6) . . . . ? C30 N14 C32 C33 179.0(5) . . . . ? C31 N15 C32 N14 -0.1(6) . . . . ? C31 N15 C32 C33 -178.9(5) . . . . ? C31 N15 C37 C38 -25.3(9) . . . . ? C32 N14 C30 C31 -0.3(6) . . . . ? C32 N15 C31 C30 -0.1(6) . . . . ? C32 N15 C37 C38 163.2(6) . . . . ? C32 C33 C34 N16 18.3(8) . . . . ? C32 C33 C34 N17 -154.8(5) . . . . ? C33 C34 N17 C39 -7.4(8) . . . . ? C33 C34 N17 C36 173.8(5) . . . . ? C34 N16 C35 C36 1.1(6) . . . . ? C34 N17 C39 C40 -164.6(6) . . . . ? C34 N17 C36 C35 0.9(6) . . . . ? N17 C36 C35 N16 -1.3(6) . . . . ? C39 N17 C36 C35 -177.9(5) . . . . ? C36 N17 C39 C40 14.0(10) . . . . ? C35 N16 C34 C33 -174.4(5) . . . . ? C35 N16 C34 N17 -0.5(6) . . . . ? C37 N15 C31 C30 -173.1(5) . . . . ? C37 N15 C32 N14 172.5(5) . . . . ? C37 N15 C32 C33 -6.3(9) . . . . ? N9 N8 C14 C15 -0.8(5) . . . . ? N9 N8 C14 C17 179.7(4) . . . . ? N9 B1 N7 N6 60.7(6) . . . . ? N9 B1 N7 C11 -118.6(6) . . . . ? N9 C16 C15 C14 -1.4(7) . . . . ? B1 N5 N4 Fe1 -0.6(6) . . . . ? B1 N5 N4 C4 178.9(4) . . . . ? B1 N5 C6 C8 -0.3(10) . . . . ? B1 N5 C6 C5 -178.6(5) . . . . ? B1 N9 C16 C18 2.6(10) . . . . ? B1 N9 C16 C15 -178.2(6) . . . . ? B1 N7 C11 C10 -179.0(6) . . . . ? B1 N7 C11 C13 0.9(11) . . . . ? C6 N5 N4 Fe1 -179.5(4) . . . . ? C6 N5 N4 C4 0.1(5) . . . . ? C6 N5 B1 N9 120.4(6) . . . . ? C6 N5 B1 N7 -122.1(6) . . . . ? C6 C5 C4 N4 0.1(6) . . . . ? C6 C5 C4 C7 178.4(5) . . . . ? C8 C6 C5 C4 -178.2(6) . . . . ? N7 N6 C9 C12 -179.8(5) . . . . ? N7 N6 C9 C10 -0.1(6) . . . . ? C9 N6 N7 B1 179.6(5) . . . . ? C9 N6 N7 C11 -1.0(6) . . . . ? C9 C10 C11 N7 -1.8(7) . . . . ? C9 C10 C11 C13 178.3(8) . . . . ? C12 C9 C10 C11 -179.2(6) . . . . ? C16 N9 B1 N5 -121.2(6) . . . . ? C16 N9 B1 N7 120.6(6) . . . . ? C16 C15 C14 N8 1.4(6) . . . . ? C16 C15 C14 C17 -179.2(5) . . . . ? C18 C16 C15 C14 177.7(7) . . . . ? C14 N8 N9 B1 179.2(4) . . . . ? C14 N8 N9 C16 0.0(5) . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.000 0.500 0.500 512.8 160.7 '4 DMF'