#------------------------------------------------------------------------------ #$Date: 2021-04-24 02:19:50 +0300 (Sat, 24 Apr 2021) $ #$Revision: 264493 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/20/1562052.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1562052 loop_ _publ_author_name 'Kamilya, Sujit' 'Ghosh, Subrata' 'Mehta, Sakshi' 'Mondal, Abhishake' _publ_section_title ; Effect of Ligand Modulation on Metal-to-Metal Electron Transfer in a Series of [Fe2Co2] Molecular Square Complexes ; _journal_name_full 'The Journal of Physical Chemistry A' _journal_paper_doi 10.1021/acs.jpca.1c02032 _journal_year 2021 _chemical_formula_moiety 'C80 H84 B2 Co2 Fe2 N34 O4, 2(B F4), 2(C3 H7 N O)' _chemical_formula_sum 'C86 H98 B4 Co2 F8 Fe2 N36 O6' _chemical_formula_weight 2156.80 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _audit_creation_date 2021-02-18 _audit_creation_method ; Olex2 1.3 (compiled 2020.07.31 svn.rc2a77460 for OlexSys, GUI svn.r6145) ; _cell_angle_alpha 75.871(4) _cell_angle_beta 80.200(4) _cell_angle_gamma 84.287(4) _cell_formula_units_Z 1 _cell_length_a 13.4760(8) _cell_length_b 13.4982(8) _cell_length_c 17.3464(11) _cell_measurement_reflns_used 4826 _cell_measurement_temperature 280(2) _cell_measurement_theta_max 24.50 _cell_measurement_theta_min 2.32 _cell_volume 3009.7(3) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'olex2.solve 1.3 (Bourhis et al., 2015)' _diffrn_ambient_temperature 280(2) _diffrn_measured_fraction_theta_full 0.995 _diffrn_measured_fraction_theta_max 0.954 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1100 _diffrn_reflns_av_unetI/netI 0.2009 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.954 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_number 73854 _diffrn_reflns_point_group_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.954 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.491 _diffrn_reflns_theta_min 1.536 _diffrn_source 'sealed tube' _exptl_absorpt_coefficient_mu 0.578 _exptl_absorpt_correction_T_max 0.784 _exptl_absorpt_correction_T_min 0.682 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS _exptl_crystal_colour red _exptl_crystal_density_diffrn 1.190 _exptl_crystal_description parallelepiped _exptl_crystal_F_000 1112 _exptl_crystal_size_max 0.47 _exptl_crystal_size_mid 0.29 _exptl_crystal_size_min 0.18 _refine_diff_density_max 0.592 _refine_diff_density_min -0.350 _refine_diff_density_rms 0.065 _refine_ls_extinction_coef 0.0028(7) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 0.918 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 657 _refine_ls_number_reflns 17503 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.918 _refine_ls_R_factor_all 0.2303 _refine_ls_R_factor_gt 0.0765 _refine_ls_shift/su_max 2.186 _refine_ls_shift/su_mean 0.004 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1065P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1821 _refine_ls_wR_factor_ref 0.2447 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5591 _reflns_number_total 17503 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file jp1c02032_si_008.cif _cod_data_source_block Complex3_280K _cod_database_code 1562052 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All B(H) groups, All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: B1(H1) 2.b Me refined with riding coordinates: C12(H12A,H12B,H12C) 2.c Aromatic/amide H refined with riding coordinates: C24(H24), C30(H30), C25(H25), C26(H26), C37(H37), C39(H39), C28(H28), C15(H15), C5(H5), C19(H19), C35(H35), C31(H31), C20(H20), C36(H36), C10(H10), C43(H43) 2.d X=CH2 refined with riding coordinates: C40(H40A,H40B), C38(H38A,H38B), C29(H29A,H29B), C27(H27A,H27B) 2.e Idealised Me refined as rotating group: C13(H13A,H13B,H13C), C18(H18A,H18B,H18C), C8(H8A,H8B,H8C), C17(H17A,H17B, H17C), C7(H7A,H7B,H7C), C42(H42A,H42B,H42C), C41(H41A,H41B,H41C) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL Test_2_a.res in P-1 test_2_a.res created by SHELXL-2018/3 at 10:36:00 on 18-Feb-2021 CELL 0.71073 13.476 13.4982 17.3464 75.871 80.2 84.287 ZERR 1 0.0008 0.0008 0.0011 0.004 0.004 0.004 LATT 1 SFAC C H B Co F Fe N O UNIT 86 98 4 2 8 2 36 6 L.S. 50 PLAN 21 TEMP 23 CONF ABIN MORE -1 BOND $H fmap 2 acta MERG 2 REM REM REM WGHT 0.106500 EXTI 0.002790 FVAR 0.43174 CO1 4 0.297125 0.698881 0.494532 11.00000 0.04228 0.05492 = 0.06526 -0.01200 -0.00607 0.00264 FE1 6 0.613503 0.612093 0.629220 11.00000 0.04420 0.05236 = 0.05651 -0.01026 -0.00787 -0.00232 N8 7 0.569294 0.725464 0.686377 11.00000 0.05726 0.05101 = 0.06356 -0.01549 -0.00773 0.00166 O1 8 0.217490 0.726342 0.241481 11.00000 0.08547 0.15147 = 0.09278 -0.04834 -0.00926 -0.01670 O2 8 0.291730 0.741801 0.751089 11.00000 0.13848 0.10769 = 0.09593 -0.02489 -0.03586 -0.01187 N2 7 0.745891 0.750019 0.490493 11.00000 0.05615 0.07374 = 0.07915 -0.00380 0.00679 -0.00473 C40 1 -0.088500 0.759042 0.292692 11.00000 0.07063 0.15715 = 0.15127 -0.05846 -0.04147 0.01625 AFIX 93 H40A 2 -0.132282 0.742737 0.340943 11.00000 -1.20000 H40B 2 -0.113035 0.770782 0.244075 11.00000 -1.20000 AFIX 0 F1 5 0.758281 0.776515 0.148858 11.00000 0.72979 0.40745 = 0.49556 0.06179 -0.31019 -0.40000 C38 1 0.456633 0.868213 0.101476 11.00000 0.14470 0.29698 = 0.06732 -0.00448 0.00479 -0.06332 AFIX 93 H38A 2 0.521226 0.876473 0.110154 11.00000 -1.20000 H38B 2 0.442177 0.880601 0.049294 11.00000 -1.20000 AFIX 0 C29 1 0.148739 0.490423 0.880199 11.00000 0.25510 0.14139 = 0.08341 -0.00562 0.00674 -0.03036 AFIX 93 H29A 2 0.143210 0.428204 0.867690 11.00000 -1.20000 H29B 2 0.136516 0.495563 0.933529 11.00000 -1.20000 AFIX 0 N6 7 0.524072 0.519219 0.711763 11.00000 0.05290 0.06287 = 0.05488 -0.00839 -0.00444 -0.00472 N4 7 0.725186 0.570204 0.695613 11.00000 0.05427 0.05853 = 0.07030 -0.01312 -0.01994 -0.00135 N3 7 0.680480 0.436487 0.544500 11.00000 0.04618 0.05610 = 0.06623 -0.01868 -0.00773 0.00504 N16 7 0.160989 0.732870 0.445707 11.00000 0.04480 0.06719 = 0.07009 -0.00558 -0.00386 -0.00309 N1 7 0.437702 0.676692 0.534077 11.00000 0.05172 0.06190 = 0.06116 -0.00776 -0.01203 -0.00289 N12 7 0.227824 0.619421 0.610833 11.00000 0.04349 0.06322 = 0.07296 -0.00896 -0.00161 -0.00487 N10 7 0.266148 0.828517 0.545398 11.00000 0.05903 0.05082 = 0.07312 -0.01320 -0.00100 0.00287 N14 7 0.361453 0.780361 0.376594 11.00000 0.04658 0.06100 = 0.06819 -0.01119 -0.00316 -0.00502 N11 7 0.258542 0.926606 0.631003 11.00000 0.06918 0.06227 = 0.09786 -0.02662 -0.00101 0.00169 N13 7 0.192625 0.567189 0.742768 11.00000 0.09371 0.07617 = 0.05600 -0.00938 0.00667 -0.00015 N17 7 0.049738 0.748771 0.364120 11.00000 0.04385 0.08305 = 0.08208 -0.00744 -0.01530 0.00531 N15 7 0.398740 0.818377 0.243438 11.00000 0.05931 0.09675 = 0.06993 -0.00884 -0.00306 -0.00188 N9 7 0.564814 0.702326 0.767990 11.00000 0.08093 0.06450 = 0.06097 -0.01970 -0.01109 -0.00237 C34 1 0.149211 0.743070 0.369784 11.00000 0.04587 0.07270 = 0.06645 -0.01105 -0.00884 -0.01034 C23 1 0.229541 0.643350 0.679682 11.00000 0.05724 0.05414 = 0.08387 -0.01197 -0.00644 0.00322 C32 1 0.327076 0.780007 0.309460 11.00000 0.05029 0.07408 = 0.06311 -0.01021 -0.00167 0.00208 C33 1 0.230979 0.746864 0.302548 11.00000 0.05808 0.08014 = 0.06930 -0.02181 -0.01365 0.00064 C24 1 0.190754 0.524655 0.630461 11.00000 0.06044 0.06536 = 0.09287 -0.01274 -0.00424 -0.00824 AFIX 43 H24 2 0.182992 0.487146 0.593695 11.00000 -1.20000 AFIX 0 C30 1 0.456232 0.817998 0.354220 11.00000 0.04985 0.07032 = 0.07632 -0.01252 -0.00514 -0.00871 AFIX 43 H30 2 0.498137 0.825692 0.389514 11.00000 -1.20000 AFIX 0 C21 1 0.264329 0.828670 0.621382 11.00000 0.06079 0.05315 = 0.08450 -0.02264 -0.00387 0.00232 C9 1 0.458319 0.450726 0.711041 11.00000 0.04840 0.04826 = 0.08141 -0.00695 -0.00718 0.00033 N7 7 0.525536 0.519906 0.790824 11.00000 0.07968 0.07199 = 0.05920 -0.00817 -0.00551 -0.01785 C3 1 0.655612 0.503938 0.574437 11.00000 0.03553 0.06375 = 0.05702 -0.00832 -0.00879 -0.00795 C12 1 0.435253 0.426885 0.637184 11.00000 0.05529 0.06065 = 0.08939 -0.02136 -0.00864 -0.00705 AFIX 33 H12A 2 0.386322 0.375876 0.651616 11.00000 -1.50000 H12B 2 0.408668 0.487829 0.603681 11.00000 -1.50000 H12C 2 0.495834 0.401515 0.608433 11.00000 -1.50000 AFIX 0 C2 1 0.697662 0.699080 0.542763 11.00000 0.04520 0.05426 = 0.07445 -0.01238 -0.00869 0.00027 C4 1 0.824233 0.540003 0.681686 11.00000 0.05682 0.06197 = 0.09364 -0.01252 -0.02398 -0.00061 C14 1 0.540487 0.825528 0.665113 11.00000 0.05119 0.06247 = 0.08701 -0.02012 -0.01092 -0.00354 C1 1 0.505780 0.651824 0.567955 11.00000 0.04274 0.05221 = 0.05386 -0.00996 -0.00287 -0.00523 N5 7 0.701895 0.567116 0.775514 11.00000 0.07977 0.07676 = 0.06567 -0.01017 -0.03546 -0.00047 C25 1 0.166969 0.493224 0.711027 11.00000 0.07503 0.07693 = 0.09225 -0.00760 0.00965 -0.01415 AFIX 43 H25 2 0.138417 0.432361 0.739226 11.00000 -1.20000 AFIX 0 C26 1 0.255632 0.962227 0.700208 11.00000 0.10113 0.10062 = 0.10876 -0.04847 -0.01747 -0.00321 AFIX 43 H26 2 0.242402 0.915531 0.749387 11.00000 -1.20000 AFIX 0 C37 1 0.388263 0.840055 0.160802 11.00000 0.10437 0.22968 = 0.07472 -0.02221 -0.00622 -0.04324 AFIX 43 H37 2 0.324942 0.832889 0.149005 11.00000 -1.20000 AFIX 0 C39 1 0.004408 0.765248 0.293191 11.00000 0.06519 0.12865 = 0.09810 -0.00921 -0.02838 -0.00128 AFIX 43 H39 2 0.046034 0.781704 0.243858 11.00000 -1.20000 AFIX 0 C27 1 0.269812 1.054811 0.701612 11.00000 0.15326 0.12214 = 0.14659 -0.07540 -0.04286 0.01417 AFIX 93 H27A 2 0.283241 1.103784 0.653698 11.00000 -1.20000 H27B 2 0.266611 1.072610 0.750539 11.00000 -1.20000 AFIX 0 F4 5 0.837563 0.880484 0.090707 11.00000 0.15644 0.40978 = 0.26381 -0.02245 0.00815 -0.11093 C28 1 0.172865 0.567996 0.824722 11.00000 0.19900 0.10063 = 0.07656 -0.00764 0.00770 -0.01736 AFIX 43 H28 2 0.177814 0.629179 0.839038 11.00000 -1.20000 AFIX 0 C15 1 0.518609 0.863663 0.731619 11.00000 0.10331 0.06769 = 0.10038 -0.03707 -0.01210 0.00450 AFIX 43 H15 2 0.497796 0.931100 0.732931 11.00000 -1.20000 AFIX 0 C5 1 0.860170 0.521487 0.754367 11.00000 0.07216 0.11344 = 0.10839 -0.01569 -0.05054 0.01743 AFIX 43 H5 2 0.926365 0.501160 0.762338 11.00000 -1.20000 AFIX 0 C6 1 0.783974 0.537649 0.811300 11.00000 0.10239 0.11356 = 0.10030 -0.01625 -0.04767 0.00445 B1 3 0.591750 0.593543 0.809029 11.00000 0.08369 0.09445 = 0.04978 -0.01536 -0.00598 -0.00599 AFIX 13 H1 2 0.584668 0.586630 0.867241 11.00000 -1.20000 AFIX 0 C13 1 0.446404 0.433655 0.927868 11.00000 0.19758 0.17340 = 0.06496 0.00687 0.01689 -0.08678 AFIX 137 H13A 2 0.400442 0.380496 0.950698 11.00000 -1.50000 H13B 2 0.418944 0.495446 0.943547 11.00000 -1.50000 H13C 2 0.509874 0.413265 0.946926 11.00000 -1.50000 AFIX 0 C11 1 0.461880 0.451946 0.838330 11.00000 0.11135 0.09041 = 0.06697 -0.00435 0.00876 -0.02694 C18 1 0.519168 0.784990 0.883637 11.00000 0.20894 0.12948 = 0.10340 -0.06164 -0.01411 0.01747 AFIX 137 H18A 2 0.583253 0.768739 0.902303 11.00000 -1.50000 H18B 2 0.473127 0.734128 0.912922 11.00000 -1.50000 H18C 2 0.492760 0.850911 0.891974 11.00000 -1.50000 AFIX 0 C8 1 0.785431 0.526050 0.898608 11.00000 0.17438 0.25416 = 0.10041 -0.05401 -0.08126 0.04447 AFIX 137 H8A 2 0.768172 0.591085 0.912169 11.00000 -1.50000 H8B 2 0.851669 0.501679 0.910803 11.00000 -1.50000 H8C 2 0.737391 0.477899 0.929203 11.00000 -1.50000 AFIX 0 C17 1 0.532318 0.882439 0.580170 11.00000 0.06650 0.05857 = 0.09713 -0.01289 -0.00080 -0.00212 AFIX 137 H17A 2 0.463049 0.888467 0.572079 11.00000 -1.50000 H17B 2 0.572002 0.845731 0.543493 11.00000 -1.50000 H17C 2 0.556685 0.949468 0.570685 11.00000 -1.50000 AFIX 0 C19 1 0.262065 0.926675 0.503577 11.00000 0.07001 0.06766 = 0.09383 -0.01200 -0.00191 0.00642 AFIX 43 H19 2 0.263347 0.948484 0.448269 11.00000 -1.20000 AFIX 0 C35 1 0.066686 0.733959 0.488339 11.00000 0.05152 0.09253 = 0.06638 -0.00769 0.00063 0.00354 AFIX 43 H35 2 0.051610 0.728613 0.543495 11.00000 -1.20000 AFIX 0 C31 1 0.478504 0.841628 0.274293 11.00000 0.05223 0.08881 = 0.09062 -0.01145 0.00431 -0.00988 AFIX 43 H31 2 0.537713 0.869068 0.244602 11.00000 -1.20000 AFIX 0 C20 1 0.255747 0.988708 0.555729 11.00000 0.08237 0.04936 = 0.11300 -0.01967 0.00155 0.00055 AFIX 43 H20 2 0.250515 1.059880 0.542754 11.00000 -1.20000 AFIX 0 C36 1 -0.001732 0.744033 0.437977 11.00000 0.04416 0.09307 = 0.10017 0.00695 -0.01756 -0.00067 AFIX 43 H36 2 -0.071535 0.747105 0.451967 11.00000 -1.20000 AFIX 0 C7 1 0.880280 0.531201 0.601413 11.00000 0.04476 0.09235 = 0.10909 -0.01069 -0.01268 -0.00633 AFIX 137 H7A 2 0.947373 0.502266 0.607210 11.00000 -1.50000 H7B 2 0.883617 0.597875 0.565739 11.00000 -1.50000 H7C 2 0.845895 0.487803 0.579667 11.00000 -1.50000 AFIX 0 C16 1 0.532252 0.786853 0.795577 11.00000 0.10762 0.08140 = 0.07344 -0.03546 -0.00554 0.00225 C10 1 0.420411 0.406789 0.789476 11.00000 0.08679 0.08898 = 0.08205 0.00167 0.00998 -0.03679 AFIX 43 H10 2 0.374817 0.355616 0.806366 11.00000 -1.20000 AFIX 0 C22 1 0.264824 0.737478 0.688435 11.00000 0.07409 0.09287 = 0.07020 -0.01836 -0.01019 0.00366 F2 5 0.690294 0.910309 0.109373 11.00000 0.19733 0.47232 = 0.56098 -0.19151 -0.09567 -0.03143 F3 5 0.726385 0.791112 0.050382 11.00000 0.31374 0.50066 = 0.20360 -0.17143 -0.01749 -0.10362 O3 8 0.055767 0.789498 0.721434 11.00000 0.11694 0.18644 = 0.31705 0.04446 0.02651 0.01960 N18 7 -0.129632 0.889829 0.667019 11.00000 0.47445 0.41257 = 0.22231 0.12044 -0.17445 -0.34070 C43 1 -0.043545 0.789218 0.704950 11.00000 0.29450 0.39272 = 0.48091 -0.34642 0.21599 -0.20770 AFIX 43 H43 2 -0.067989 0.724386 0.716074 11.00000 -1.20000 AFIX 0 C42 1 -0.045379 0.943576 0.604126 11.00000 0.19353 0.17920 = 0.21985 0.01912 -0.00280 -0.03896 AFIX 137 H42A 2 -0.054641 0.938669 0.551550 11.00000 -1.50000 H42B 2 0.018904 0.911308 0.615669 11.00000 -1.50000 H42C 2 -0.047768 1.014325 0.605869 11.00000 -1.50000 AFIX 0 C41 1 -0.183905 0.825594 0.663209 11.00000 0.20844 0.22950 = 0.34034 -0.08246 -0.11171 -0.09538 AFIX 137 H41A 2 -0.168580 0.762433 0.700037 11.00000 -1.50000 H41B 2 -0.173142 0.815344 0.609485 11.00000 -1.50000 H41C 2 -0.253088 0.848004 0.677079 11.00000 -1.50000 AFIX 0 B2 3 0.745159 0.829151 0.128736 11.00000 0.16041 0.33979 = 0.92365 -0.40000 -0.27032 0.10221 HKLF 4 REM Test_2_a.res in P-1 REM wR2 = 0.2447, GooF = S = 0.918, Restrained GooF = 0.918 for all data REM R1 = 0.0765 for 5591 Fo > 4sig(Fo) and 0.2303 for all 17503 data REM 657 parameters refined using 0 restraints END WGHT 0.1067 0.0000 REM Highest difference peak 0.592, deepest hole -0.350, 1-sigma level 0.065 Q1 1 0.7364 0.7733 0.1890 11.00000 0.05 0.59 Q2 1 0.5220 0.7057 0.6255 11.00000 0.05 0.52 Q3 1 0.7659 0.8278 0.1020 11.00000 0.05 0.49 Q4 1 0.6996 0.8221 0.1718 11.00000 0.05 0.49 Q5 1 0.4119 0.6018 0.5066 11.00000 0.05 0.45 Q6 1 0.0027 0.7891 0.7936 11.00000 0.05 0.38 Q7 1 0.7248 0.5089 0.6309 11.00000 0.05 0.37 Q8 1 0.7385 0.9151 0.0314 11.00000 0.05 0.35 Q9 1 -0.1799 1.0482 0.6623 11.00000 0.05 0.33 Q10 1 -0.1560 1.0205 0.6587 11.00000 0.05 0.33 Q11 1 0.6857 0.3991 0.5050 11.00000 0.05 0.33 Q12 1 0.8182 0.8915 0.0197 11.00000 0.05 0.31 Q13 1 0.6014 1.0211 0.1140 11.00000 0.05 0.31 Q14 1 0.6387 0.5224 0.6275 11.00000 0.05 0.30 Q15 1 0.1860 0.7994 0.5015 11.00000 0.05 0.28 Q16 1 0.5000 0.5000 0.5000 10.50000 0.05 0.28 Q17 1 0.3018 0.7117 0.5601 11.00000 0.05 0.27 Q18 1 0.3139 0.7369 0.5570 11.00000 0.05 0.27 Q19 1 0.0250 0.8562 0.7695 11.00000 0.05 0.26 Q20 1 0.1479 0.6310 0.3486 11.00000 0.05 0.25 Q21 1 -0.0863 0.8525 0.6591 11.00000 0.05 0.25 ; _shelx_res_checksum 38225 _shelx_hkl_file ; -1 0 0 1412.06 56.19 -1 0 0 1394.86 54.89 -1 0 0 1406.16 54.99 1 0 0 1406.56 55.09 1 0 0 1407.36 54.79 -2 0 0 2121.69 85.39 -2 0 0 2208.68 87.99 -2 0 0 2145.59 85.09 2 0 0 2272.77 88.19 2 0 0 2152.38 85.49 2 0 0 2070.79 85.99 2 0 0 2170.18 85.09 -3 0 0 1161.38 50.59 -3 0 0 1141.39 47.60 -3 0 0 1117.79 48.90 -3 0 0 1141.09 52.09 3 0 0 1087.69 48.50 3 0 0 1092.19 47.80 3 0 0 1084.79 51.49 3 0 0 1158.28 47.40 3 0 0 1116.29 48.90 -4 0 0 2468.45 102.19 -4 0 0 2530.85 102.99 -4 0 0 2479.75 105.49 -4 0 0 2505.35 100.69 -4 0 0 2465.65 100.19 4 0 0 2431.96 99.89 4 0 0 2435.26 102.09 4 0 0 2486.55 105.29 4 0 0 2458.75 101.89 4 0 0 2527.65 101.09 -5 0 0 79.29 13.40 -5 0 0 129.59 13.90 -5 0 0 109.49 17.40 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27.90 8 -3 0 100.09 21.60 8 -3 0 95.49 15.70 8 -3 0 114.19 15.60 8 -3 0 99.69 17.40 -8 3 0 81.49 20.30 -8 3 0 68.39 19.10 -8 3 0 101.99 18.40 -8 3 0 82.99 13.80 7 -3 0 209.18 28.70 7 -3 0 175.08 18.20 7 -3 0 166.78 20.60 7 -3 0 195.08 23.70 7 -3 0 171.88 17.70 7 -3 0 206.98 20.40 -7 3 0 163.38 24.20 -7 3 0 185.18 26.90 -7 3 0 194.48 22.50 -7 3 0 185.98 24.40 -7 3 0 184.98 20.00 -7 3 0 191.98 19.10 6 -3 0 249.38 22.50 6 -3 0 259.67 18.10 6 -3 0 357.76 34.90 6 -3 0 278.67 18.80 6 -3 0 247.78 18.50 6 -3 0 257.67 18.30 6 -3 0 237.38 20.30 -6 3 0 272.07 21.60 -6 3 0 241.58 17.90 -6 3 0 275.07 19.20 -6 3 0 277.27 27.50 -6 3 0 309.37 31.70 -6 3 0 277.47 29.70 5 -3 0 7.20 6.70 5 -3 0 6.40 9.20 5 -3 0 11.90 8.20 5 -3 0 6.60 6.90 5 -3 0 13.00 7.10 5 -3 0 27.50 12.50 5 -3 0 1.80 5.90 -5 3 0 16.30 6.50 -5 3 0 -0.50 9.10 -5 3 0 12.80 8.80 -5 3 0 6.90 12.40 -5 3 0 5.00 11.40 4 -3 0 47.50 10.80 4 -3 0 49.10 8.50 4 -3 0 45.30 7.80 4 -3 0 60.69 8.90 4 -3 0 67.59 14.30 4 -3 0 44.10 10.20 4 -3 0 40.20 8.20 -4 3 0 65.29 7.50 -4 3 0 62.39 7.10 -4 3 0 40.10 12.00 -4 3 0 20.90 13.10 -4 3 0 26.20 12.40 -4 3 0 35.10 10.00 3 -3 0 4430.66 170.38 3 -3 0 4414.66 170.28 3 -3 0 4398.16 172.48 3 -3 0 4388.06 172.48 3 -3 0 4276.57 168.98 3 -3 0 4458.95 177.68 -3 3 0 4420.76 172.78 -3 3 0 4456.55 179.58 -3 3 0 4442.36 179.88 -3 3 0 4278.97 174.58 2 -3 0 1969.30 78.99 2 -3 0 2155.98 84.99 2 -3 0 1959.60 76.49 2 -3 0 1877.61 76.29 -2 3 0 1955.00 80.19 -2 3 0 1953.60 78.89 -2 3 0 1977.60 85.79 -2 3 0 2038.00 86.29 1 -3 0 3102.19 123.89 1 -3 0 3052.59 123.29 1 -3 0 2967.50 116.99 -1 3 0 3026.70 123.49 -1 3 0 3060.49 123.89 -1 3 0 2988.10 116.69 -1 3 0 3036.10 116.59 0 -3 0 2792.92 111.19 0 -3 0 2705.13 110.99 0 -3 0 2738.83 105.89 0 -3 0 2862.01 112.19 0 3 0 2658.43 110.49 0 3 0 2791.42 110.89 0 3 0 2695.63 105.39 0 3 0 2694.93 106.89 -1 -3 0 1921.91 76.09 -1 -3 0 1925.61 74.49 -1 -3 0 1909.91 77.59 -1 -3 0 1923.81 74.69 -1 -3 0 1875.81 75.69 -1 -3 0 1936.41 75.89 -1 -3 0 1917.81 77.39 1 3 0 1966.50 77.59 1 3 0 1905.81 77.19 1 3 0 1883.91 77.29 1 3 0 1839.62 76.69 1 3 0 1939.91 75.79 -2 -3 0 4.00 5.70 -2 -3 0 14.20 4.70 -2 -3 0 16.40 5.30 -2 -3 0 4.40 4.10 -2 -3 0 6.60 5.10 -2 -3 0 15.20 7.20 2 3 0 15.00 8.10 2 3 0 16.80 3.90 2 3 0 11.00 5.70 2 3 0 36.50 8.70 -3 -3 0 177.28 13.60 -3 -3 0 192.68 10.90 -3 -3 0 200.58 19.10 -3 -3 0 190.98 17.40 -3 -3 0 200.08 14.70 -3 -3 0 226.88 13.60 -3 -3 0 202.58 14.20 3 3 0 203.38 19.60 3 3 0 201.98 13.00 3 3 0 224.88 14.60 3 3 0 204.58 20.10 3 3 0 191.18 14.80 3 3 0 182.28 15.00 -4 -3 0 32.00 11.00 -4 -3 0 29.00 11.10 -4 -3 0 14.40 8.30 -4 -3 0 23.90 6.40 -4 -3 0 43.60 9.30 -4 -3 0 27.60 7.80 4 3 0 21.60 7.80 4 3 0 30.80 9.30 4 3 0 22.30 11.40 4 3 0 17.10 8.30 4 3 0 24.90 7.80 -5 -3 0 79.99 12.90 -5 -3 0 82.69 13.20 -5 -3 0 89.79 11.20 -5 -3 0 61.29 10.90 -5 -3 0 46.40 13.20 -5 -3 0 62.89 15.00 5 3 0 79.09 15.70 5 3 0 80.09 14.00 5 3 0 89.69 14.30 5 3 0 62.29 11.80 5 3 0 71.49 10.90 -6 -3 0 229.48 26.40 -6 -3 0 225.08 22.90 -6 -3 0 235.98 20.80 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12.80 9 3 0 25.50 11.70 -10 -3 0 416.16 31.10 -10 -3 0 416.96 33.00 -10 -3 0 332.27 35.30 -10 -3 0 370.16 27.80 10 3 0 361.36 29.00 10 3 0 418.26 34.80 10 3 0 353.36 34.90 10 3 0 284.07 38.60 10 3 0 393.86 39.70 -11 -3 0 274.17 33.70 -11 -3 0 264.37 29.90 11 3 0 255.67 30.40 11 3 0 257.97 33.20 11 3 0 299.77 32.80 -12 -3 0 12.60 16.80 -12 -3 0 58.89 17.00 12 3 0 29.40 14.60 12 3 0 16.70 17.20 -13 -3 0 49.40 20.40 -13 -3 0 56.19 19.50 13 3 0 115.99 25.40 -14 -3 0 19.60 17.00 14 3 0 -7.00 15.90 -15 -3 0 15.60 20.30 15 3 0 18.90 19.80 16 3 0 -4.20 16.80 17 3 0 -5.50 20.20 18 3 0 -17.60 20.30 17 -4 0 2.60 17.80 16 -4 0 -6.30 16.20 16 -4 0 20.40 22.90 16 -4 0 -4.50 16.00 -16 4 0 -9.80 17.80 -16 4 0 12.00 17.40 15 -4 0 17.10 16.60 15 -4 0 -13.10 13.10 15 -4 0 -23.70 15.80 -15 4 0 29.10 21.90 -15 4 0 -20.50 24.00 -15 4 0 7.50 15.70 14 -4 0 -12.30 13.40 14 -4 0 -0.80 26.50 14 -4 0 12.20 14.60 14 -4 0 2.40 16.00 -14 4 0 -6.20 15.40 -14 4 0 -19.10 12.10 -14 4 0 11.50 24.20 13 -4 0 29.70 17.80 13 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132.29 8.70 -2 4 0 101.99 8.70 1 -4 0 93.39 14.50 1 -4 0 124.09 16.50 1 -4 0 89.89 7.00 -1 4 0 76.49 5.90 -1 4 0 120.69 16.50 -1 4 0 84.59 5.70 -1 4 0 99.49 14.60 0 -4 0 1823.12 80.89 0 -4 0 1923.91 74.59 0 -4 0 1968.40 82.99 0 -4 0 1822.62 74.19 0 4 0 1887.01 80.59 0 4 0 1885.91 74.09 0 4 0 1929.91 73.99 0 4 0 1915.01 80.79 -1 -4 0 5431.96 219.28 -1 -4 0 5886.51 221.78 -1 -4 0 5745.83 225.08 -1 -4 0 5767.12 225.08 -1 -4 0 5658.63 219.28 1 4 0 5862.51 224.98 1 4 0 5910.61 224.68 1 4 0 5718.73 222.88 1 4 0 5732.93 223.28 1 4 0 5725.93 221.68 -2 -4 0 707.23 27.50 -2 -4 0 632.54 27.80 -2 -4 0 610.24 29.80 -2 -4 0 756.12 31.70 -2 -4 0 600.24 29.60 -2 -4 0 646.14 31.60 -2 -4 0 544.35 28.00 -2 -4 0 590.64 29.70 -2 -4 0 606.14 27.30 2 4 0 652.43 29.30 2 4 0 605.24 29.70 2 4 0 667.63 32.80 2 4 0 660.43 33.20 2 4 0 623.04 29.00 -3 -4 0 90.59 9.70 -3 -4 0 92.39 11.80 -3 -4 0 108.29 11.00 -3 -4 0 95.19 13.50 -3 -4 0 92.49 8.60 -3 -4 0 80.09 12.60 -3 -4 0 97.79 11.00 3 4 0 82.79 9.10 3 4 0 112.69 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3 47.70 11.40 5 -7 3 49.70 7.00 -6 7 -3 78.99 23.00 -6 7 -3 83.09 12.00 -6 7 -3 57.19 13.80 6 -7 3 68.29 9.30 6 -7 3 68.29 14.30 6 -7 3 85.29 9.60 6 -7 3 60.99 21.20 -7 7 -3 5.10 15.90 -7 7 -3 18.20 11.40 -7 7 -3 3.90 7.20 7 -7 3 -1.10 8.80 7 -7 3 34.10 17.80 7 -7 3 19.00 7.10 -8 7 -3 17.10 9.50 -8 7 -3 16.30 11.70 -8 7 -3 -20.60 12.80 8 -7 3 5.70 10.70 8 -7 3 1.20 16.30 8 -7 3 1.60 7.40 -9 7 -3 20.00 19.90 -9 7 -3 -3.40 9.90 -9 7 -3 -7.60 10.20 9 -7 3 27.20 12.80 9 -7 3 9.60 18.20 9 -7 3 0.20 8.10 -10 7 -3 15.60 20.10 -10 7 -3 46.00 14.90 -10 7 -3 40.90 16.60 10 -7 3 36.70 15.10 10 -7 3 34.50 20.50 10 -7 3 31.50 12.00 -11 7 -3 -12.90 12.30 -11 7 -3 -16.90 17.80 -11 7 -3 12.80 13.00 11 -7 3 11.70 10.70 11 -7 3 26.30 14.30 11 -7 3 5.90 21.50 -12 7 -3 18.80 25.90 -12 7 -3 21.40 13.70 -12 7 -3 65.59 22.40 12 -7 3 82.59 21.40 12 -7 3 58.09 14.20 12 -7 3 52.09 26.40 -13 7 -3 101.09 25.70 -13 7 -3 50.99 18.10 13 -7 3 64.09 16.00 13 -7 3 66.29 20.10 -14 7 -3 -5.70 16.30 -14 7 -3 -13.30 15.30 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469.95 22.60 2 -8 5 441.06 22.40 -3 8 -5 61.69 11.10 -3 8 -5 59.29 14.10 -3 8 -5 78.79 20.80 3 -8 5 42.50 18.60 3 -8 5 42.90 7.50 3 -8 5 92.49 15.40 3 -8 5 63.79 8.50 -4 8 -5 119.79 18.20 -4 8 -5 81.29 11.90 -4 8 -5 125.69 27.50 4 -8 5 101.19 10.00 4 -8 5 85.49 9.60 4 -8 5 65.09 21.30 4 -8 5 81.29 15.20 -5 8 -5 113.89 19.00 -5 8 -5 69.09 12.00 -5 8 -5 19.10 18.00 5 -8 5 75.79 24.00 5 -8 5 57.39 14.70 5 -8 5 71.59 9.70 5 -8 5 70.19 8.80 -6 8 -5 -0.30 9.10 -6 8 -5 4.50 10.90 -6 8 -5 1.30 16.20 6 -8 5 1.40 9.30 6 -8 5 14.30 18.40 6 -8 5 9.30 6.30 -7 8 -5 6.30 9.50 -7 8 -5 -6.00 14.40 -7 8 -5 18.50 12.00 7 -8 5 3.20 16.70 7 -8 5 6.90 7.00 7 -8 5 -4.60 8.70 -8 8 -5 -1.40 17.50 -8 8 -5 12.20 11.80 -8 8 -5 33.00 12.00 8 -8 5 38.10 10.50 8 -8 5 -13.30 10.70 8 -8 5 23.60 22.80 -9 8 -5 16.80 12.40 -9 8 -5 72.29 27.30 -9 8 -5 41.60 16.60 9 -8 5 44.10 10.90 9 -8 5 52.09 25.80 9 -8 5 21.90 13.90 -10 8 -5 -1.40 12.60 -10 8 -5 -5.00 12.50 -10 8 -5 11.80 21.40 10 -8 5 0.60 8.70 10 -8 5 4.70 21.20 10 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-0.3682 0.0610 16 8 1 4.0385 0.0460 16 8 2 2.4256 0.0194 16 8 3 -1.2567 -0.0113 16 8 4 -1.1532 -0.0261 16 8 5 -0.7263 -0.0182 16 8 6 -1.9985 -0.0001 16 8 7 -2.0037 0.0110 16 8 8 -1.0138 0.0088 16 8 9 -0.2793 -0.0032 16 8 10 1.5087 -0.0161 16 8 11 3.0593 -0.0124 16 8 12 1.6716 0.0119 16 8 13 -0.8565 0.0271 16 8 14 -1.6295 0.0148 16 9 0 1.8623 -0.0890 16 9 1 4.0366 -0.0717 16 9 2 2.9258 -0.0296 16 9 3 0.9880 0.0038 16 9 4 1.9048 0.0152 16 9 5 1.1423 0.0101 16 9 6 -2.8307 -0.0004 16 9 7 -4.4237 -0.0074 16 9 8 -2.2466 -0.0056 16 9 9 -0.0488 0.0007 16 9 10 0.6857 0.0023 16 9 11 0.1580 0.0037 16 9 12 -1.5302 0.0091 16 9 13 -2.5484 0.0038 16 10 1 0.1866 -0.0410 16 10 2 -1.2573 -0.0209 16 10 3 -1.6551 -0.0022 16 10 4 0.9617 0.0073 16 10 5 1.3310 0.0072 16 10 6 -2.2065 0.0004 16 10 7 -3.5960 -0.0080 16 10 8 -1.0057 -0.0107 16 10 9 0.7026 -0.0089 16 10 10 -0.6497 -0.0136 16 10 11 -2.6607 -0.0200 16 11 5 1.3881 -0.0103 16 11 6 -1.0369 0.0032 16 11 7 -1.5504 0.0132 16 11 8 1.2195 0.0124 16 11 9 2.6781 0.0075 16 12 8 0.3088 -0.0056 17 -7 0 -0.0532 -0.1178 17 -7 1 -0.2624 -0.0424 17 -7 2 -1.1182 0.0045 17 -7 3 -1.9734 0.0185 17 -6 0 1.6564 -0.0393 17 -6 1 2.0630 0.0003 17 -6 2 1.5460 0.0091 17 -6 3 1.2039 0.0084 17 -6 4 2.1619 0.0009 17 -6 5 3.1397 -0.0073 17 -6 6 1.9827 0.0041 17 -6 7 -0.5150 0.0183 17 -5 0 -0.3896 0.1716 17 -5 1 -0.7137 0.1094 17 -5 2 -1.7967 0.0143 17 -5 3 -2.2143 -0.0296 17 -5 4 -1.2400 -0.0226 17 -5 5 -0.1501 0.0042 17 -5 6 -0.3529 0.0393 17 -4 0 -4.7552 0.0428 17 -4 1 -5.5831 0.0174 17 -4 2 -4.1385 -0.0151 17 -4 3 -2.0325 -0.0112 17 -4 4 -1.9623 0.0039 17 -4 5 -4.7358 0.0122 17 -4 6 -7.4213 0.0314 17 -4 7 -5.9445 0.0394 17 -4 8 -1.2509 0.0039 17 -3 0 -1.5132 -0.1423 17 -3 1 -1.0601 -0.1138 17 -3 2 2.2533 -0.0434 17 -3 3 5.2768 0.0248 17 -3 4 4.8020 0.0282 17 -3 5 0.4321 -0.0135 17 -3 6 -4.2563 -0.0254 17 -3 7 -4.3033 -0.0070 17 -3 8 -0.4298 -0.0064 17 -3 9 1.6872 0.0020 17 -2 0 0.8929 0.0622 17 -2 1 2.1254 0.0321 17 -2 2 2.3737 0.0122 17 -2 3 1.0071 0.0113 17 -2 4 -0.2196 -0.0033 17 -2 5 -0.5587 -0.0257 17 -2 6 -0.6362 -0.0147 17 -2 7 0.6545 0.0130 17 -2 8 2.7078 0.0079 17 -2 9 1.9795 -0.0054 17 -2 10 -0.2615 0.0193 17 -2 11 0.7971 0.0431 17 -1 0 1.9765 0.1240 17 -1 1 2.2842 0.0833 17 -1 2 0.4001 0.0189 17 -1 3 -2.1968 -0.0172 17 -1 4 -1.8056 -0.0243 17 -1 5 0.4729 -0.0145 17 -1 6 0.4422 0.0089 17 -1 7 -0.0833 0.0186 17 -1 8 2.2744 -0.0088 17 -1 9 3.8281 -0.0327 17 -1 10 1.7089 -0.0109 17 -1 11 0.0675 0.0105 17 -1 12 0.4825 -0.0147 17 0 0 1.6911 -0.1262 17 0 1 1.4064 -0.0891 17 0 2 -1.5886 -0.0379 17 0 3 -4.5510 0.0129 17 0 4 -2.8798 0.0301 17 0 5 0.8335 0.0112 17 0 6 -0.3206 -0.0068 17 0 7 -3.8882 -0.0062 17 0 8 -2.2481 -0.0023 17 0 9 1.9354 0.0048 17 0 10 1.8074 0.0249 17 0 11 -0.3404 0.0259 17 0 12 -0.4535 -0.0193 17 0 13 -0.6514 -0.0608 17 1 0 -1.6217 -0.0209 17 1 1 1.6114 -0.0154 17 1 2 1.6608 -0.0111 17 1 3 -0.7552 0.0031 17 1 4 -0.8374 0.0107 17 1 5 1.3785 -0.0018 17 1 6 0.5990 -0.0189 17 1 7 -1.6994 -0.0205 17 1 8 0.9545 -0.0069 17 1 9 4.9933 0.0095 17 1 10 2.6659 0.0178 17 1 11 -1.6615 0.0051 17 1 12 -0.3203 -0.0271 17 1 13 3.1099 -0.0367 17 1 14 2.6396 0.0024 17 2 0 -1.2435 0.1461 17 2 1 2.7739 0.1054 17 2 2 3.4146 0.0291 17 2 3 1.8111 -0.0286 17 2 4 1.8561 -0.0400 17 2 5 3.6541 -0.0155 17 2 6 2.7574 0.0130 17 2 7 0.1363 0.0192 17 2 8 2.4350 0.0057 17 2 9 6.9838 -0.0098 17 2 10 4.4024 -0.0133 17 2 11 -2.5419 -0.0016 17 2 12 -3.6782 0.0138 17 2 13 0.0052 0.0284 17 2 14 1.1280 0.0472 17 3 0 -1.2073 -0.0684 17 3 1 1.9718 -0.0375 17 3 2 1.4763 0.0006 17 3 3 -0.4522 0.0242 17 3 4 -1.1021 0.0238 17 3 5 -0.1094 0.0113 17 3 6 -0.5515 -0.0006 17 3 7 -3.0208 -0.0069 17 3 8 -2.0628 0.0002 17 4 0 0.1351 -0.0977 17 4 1 1.6697 -0.0690 17 4 2 2.7121 -0.0229 17 4 3 3.7139 0.0119 17 4 4 3.0022 0.0170 17 4 5 1.3246 0.0031 17 4 6 0.2684 -0.0149 17 4 7 -0.7468 -0.0276 17 4 8 -0.2556 -0.0166 17 4 9 2.1022 0.0097 17 4 10 1.4348 0.0126 17 4 11 -2.3470 -0.0082 17 4 12 -2.1215 -0.0190 17 4 13 2.4244 -0.0137 17 4 14 4.1135 -0.0041 17 5 0 0.5401 0.1282 17 5 1 -1.3083 0.0799 17 5 2 -3.7142 0.0257 17 5 3 -4.0122 -0.0172 17 5 4 -4.2954 -0.0351 17 5 5 -4.3532 -0.0173 17 5 6 -1.7229 0.0134 17 5 7 1.1634 0.0191 17 5 8 2.3429 0.0053 17 5 9 3.5081 -0.0051 17 5 10 3.3304 -0.0127 17 5 11 0.6725 -0.0100 17 5 12 -0.1469 0.0118 17 5 13 2.2554 0.0206 17 5 14 3.0620 -0.0068 17 6 0 -3.2747 0.0151 17 6 1 -3.2695 0.0023 17 6 2 -4.3587 0.0087 17 6 3 -3.7273 0.0111 17 6 4 -3.6126 -0.0002 17 6 5 -4.3090 -0.0035 17 6 6 -2.4151 0.0057 17 6 7 -0.0145 0.0064 17 6 8 -0.0862 0.0003 17 6 9 0.3826 -0.0004 17 6 10 2.4090 -0.0038 17 6 11 2.6472 -0.0078 17 6 12 1.1758 -0.0030 17 6 13 0.1128 -0.0104 17 7 0 -1.1854 -0.0923 17 7 1 -0.3153 -0.0772 17 7 2 -0.8210 -0.0218 17 7 3 0.6532 0.0262 17 7 4 1.3237 0.0312 17 7 5 -0.7555 0.0091 17 7 6 -1.5842 -0.0111 17 7 7 -1.1616 -0.0170 17 7 8 -2.6045 -0.0025 17 7 9 -3.6099 0.0207 17 7 10 -1.7499 0.0231 17 7 11 0.2904 0.0054 17 7 12 0.7769 -0.0075 17 8 0 1.7882 0.0649 17 8 1 2.4826 0.0322 17 8 2 -0.9509 0.0188 17 8 3 -2.7011 0.0112 17 8 4 -2.9987 -0.0003 17 8 5 -4.1717 -0.0056 17 8 6 -3.3376 -0.0017 17 8 7 -0.2206 0.0035 17 8 8 1.1634 0.0090 17 8 9 0.9526 0.0108 17 8 10 1.7441 0.0028 17 8 11 2.7166 -0.0001 17 9 3 1.1300 -0.0070 17 9 4 1.1330 -0.0165 17 9 5 -1.0233 -0.0136 17 9 6 -2.3632 0.0017 17 9 7 -0.7787 0.0127 17 9 8 0.7524 0.0086 18 -2 0 2.6675 -0.0988 18 -2 1 2.8418 -0.0935 18 -2 2 1.8470 -0.0240 18 -2 3 2.2124 0.0445 18 -2 4 4.1262 0.0242 18 -2 5 4.2786 -0.0232 18 -2 6 2.2390 -0.0199 18 -1 0 0.0546 0.1102 18 -1 1 -0.1982 0.0538 18 -1 2 -1.4564 0.0111 18 -1 3 0.0140 0.0016 18 -1 4 3.7215 -0.0167 18 -1 5 3.8446 -0.0143 18 -1 6 -0.0157 0.0306 18 -1 7 -1.2021 0.0451 18 -1 8 1.4961 0.0125 18 0 0 -1.5667 0.0355 18 0 1 -3.9961 -0.0087 18 0 2 -7.1807 -0.0262 18 0 3 -5.8592 -0.0084 18 0 4 -0.3291 -0.0078 18 0 5 1.6843 -0.0098 18 0 6 -1.9898 0.0193 18 0 7 -3.5267 0.0313 18 0 8 0.1246 -0.0002 18 0 9 2.1606 -0.0208 18 0 10 0.1063 -0.0165 18 1 0 0.8694 -0.0860 18 1 1 1.1874 -0.0645 18 1 2 -0.7659 -0.0214 18 1 3 -1.2836 0.0260 18 1 4 0.7148 0.0276 18 1 5 0.4770 -0.0037 18 1 6 -3.3060 -0.0138 18 1 7 -3.8150 -0.0033 18 1 8 0.9588 0.0079 18 1 9 2.7549 0.0246 18 1 10 -1.3841 0.0268 18 1 11 -4.0207 -0.0120 18 2 0 -1.0758 0.0232 18 2 1 1.9730 0.0337 18 2 2 4.0507 0.0190 18 2 3 6.2655 0.0017 18 2 4 8.2658 -0.0115 18 2 5 6.6241 -0.0132 18 2 6 0.9119 0.0026 18 2 7 -1.9192 0.0138 18 2 8 1.6082 0.0066 18 2 9 3.5752 -0.0012 18 2 10 -1.3620 -0.0024 18 2 11 -6.3896 -0.0046 18 2 12 -5.8443 -0.0019 18 3 0 -0.7912 0.0845 18 3 1 0.7165 0.0486 18 3 2 1.8525 -0.0055 18 3 3 2.6313 -0.0361 18 3 4 3.0441 -0.0289 18 3 5 2.2788 -0.0061 18 3 6 -0.5676 0.0048 18 3 7 -2.3005 -0.0059 18 3 8 0.3302 -0.0226 18 4 6 -2.2749 -0.0001 18 4 7 -1.7777 -0.0182 18 4 8 0.9364 -0.0102 18 4 9 3.0653 0.0138 18 4 10 1.1411 0.0154 18 4 11 -1.3969 -0.0096 18 4 12 -0.1596 -0.0326 18 5 0 0.3038 -0.0417 18 5 1 -0.1170 -0.0244 18 5 2 1.2942 0.0051 18 5 3 1.8265 0.0172 18 5 4 0.0265 0.0151 18 5 5 -0.7068 0.0079 18 5 6 0.4302 -0.0055 18 5 7 0.6459 -0.0117 18 5 8 0.2596 0.0065 18 5 9 0.1543 0.0279 18 5 10 -1.4563 0.0179 18 5 11 -3.4997 -0.0103 18 6 0 -0.8367 0.0977 18 6 1 -2.4449 0.0490 18 6 2 -1.7590 0.0151 18 6 3 -0.4759 -0.0136 18 6 4 -0.9577 -0.0211 18 6 5 -0.7602 -0.0011 18 6 6 1.0140 0.0144 18 6 7 1.1059 0.0064 18 6 8 -0.2989 -0.0078 18 6 9 -0.4869 -0.0176 18 6 10 -0.4997 -0.0272 18 7 2 -0.2472 -0.0040 18 7 3 2.8883 0.0048 18 7 4 2.0949 0.0020 18 7 5 -0.4376 0.0041 18 7 6 -1.0220 0.0019 18 7 7 -1.0164 -0.0088 18 7 8 -1.5452 -0.0105 19 1 4 -2.0414 -0.0029 19 2 2 3.2003 0.0347 19 2 3 4.4024 0.0137 19 2 4 4.0738 -0.0010 19 2 5 0.7539 0.0014 19 2 6 -3.5085 0.0250 19 2 7 -4.0182 0.0349 19 3 2 4.0379 -0.0364 19 3 3 3.9833 -0.0218 19 3 4 3.3625 0.0013 19 3 5 1.9334 0.0023 19 3 6 -0.5698 -0.0090 19 3 7 -1.6280 -0.0176 0 0 0 0.0 0.0 ; _shelx_fab_checksum 43188 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co1 Co 0.29713(4) 0.69888(5) 0.49453(4) 0.0551(2) Uani 1 1 d . . . . . Fe1 Fe 0.61350(4) 0.61209(5) 0.62922(4) 0.0514(2) Uani 1 1 d . . . . . N8 N 0.5693(3) 0.7255(3) 0.6864(2) 0.0574(10) Uani 1 1 d . . . . . O1 O 0.2175(3) 0.7263(4) 0.2415(3) 0.1062(14) Uani 1 1 d . . . . . O2 O 0.2917(4) 0.7418(3) 0.7511(3) 0.1113(14) Uani 1 1 d . . . . . N2 N 0.7459(3) 0.7500(3) 0.4905(3) 0.0741(12) Uani 1 1 d . . . . . C40 C -0.0885(5) 0.7590(6) 0.2927(5) 0.121(2) Uani 1 1 d . . . . . H40A H -0.132282 0.742737 0.340943 0.145 Uiso 1 1 calc R U . . . H40B H -0.113035 0.770782 0.244075 0.145 Uiso 1 1 calc R U . . . F1 F 0.7583(19) 0.7765(15) 0.1489(13) 0.522(18) Uani 1 1 d . . . . . C38 C 0.4566(7) 0.8682(8) 0.1015(5) 0.175(4) Uani 1 1 d . . . . . H38A H 0.521226 0.876473 0.110154 0.210 Uiso 1 1 calc R U . . . H38B H 0.442177 0.880601 0.049294 0.210 Uiso 1 1 calc R U . . . C29 C 0.1487(7) 0.4904(7) 0.8802(5) 0.166(4) Uani 1 1 d . . . . . H29A H 0.143210 0.428204 0.867690 0.199 Uiso 1 1 calc R U . . . H29B H 0.136516 0.495563 0.933529 0.199 Uiso 1 1 calc R U . . . N6 N 0.5241(3) 0.5192(3) 0.7118(2) 0.0582(10) Uani 1 1 d . . . . . N4 N 0.7252(3) 0.5702(3) 0.6956(2) 0.0602(10) Uani 1 1 d . . . . . N3 N 0.6805(3) 0.4365(3) 0.5445(2) 0.0560(10) Uani 1 1 d . . . . . N16 N 0.1610(3) 0.7329(3) 0.4457(3) 0.0631(11) Uani 1 1 d . . . . . N1 N 0.4377(3) 0.6767(3) 0.5341(2) 0.0590(10) Uani 1 1 d . . . . . N12 N 0.2278(3) 0.6194(3) 0.6108(3) 0.0618(10) Uani 1 1 d . . . . . N10 N 0.2661(3) 0.8285(3) 0.5454(3) 0.0627(10) Uani 1 1 d . . . . . N14 N 0.3615(3) 0.7804(3) 0.3766(2) 0.0598(10) Uani 1 1 d . . . . . N11 N 0.2585(3) 0.9266(4) 0.6310(3) 0.0768(13) Uani 1 1 d . . . . . N13 N 0.1926(3) 0.5672(4) 0.7428(3) 0.0788(13) Uani 1 1 d . . . . . N17 N 0.0497(3) 0.7488(3) 0.3641(3) 0.0717(12) Uani 1 1 d . . . . . N15 N 0.3987(3) 0.8184(4) 0.2434(3) 0.0782(13) Uani 1 1 d . . . . . N9 N 0.5648(3) 0.7023(3) 0.7680(3) 0.0680(11) Uani 1 1 d . . . . . C34 C 0.1492(4) 0.7431(4) 0.3698(3) 0.0621(13) Uani 1 1 d . . . . . C23 C 0.2295(4) 0.6433(4) 0.6797(4) 0.0668(14) Uani 1 1 d . . . . . C32 C 0.3271(4) 0.7800(4) 0.3095(3) 0.0647(13) Uani 1 1 d . . . . . C33 C 0.2310(4) 0.7469(4) 0.3025(3) 0.0682(14) Uani 1 1 d . . . . . C24 C 0.1908(4) 0.5247(4) 0.6305(4) 0.0744(15) Uani 1 1 d . . . . . H24 H 0.182992 0.487146 0.593695 0.089 Uiso 1 1 calc R U . . . C30 C 0.4562(4) 0.8180(4) 0.3542(3) 0.0665(13) Uani 1 1 d . . . . . H30 H 0.498137 0.825692 0.389514 0.080 Uiso 1 1 calc R U . . . C21 C 0.2643(4) 0.8287(4) 0.6214(4) 0.0662(14) Uani 1 1 d . . . . . C9 C 0.4583(3) 0.4507(4) 0.7110(3) 0.0613(13) Uani 1 1 d . . . . . N7 N 0.5255(3) 0.5199(3) 0.7908(3) 0.0712(12) Uani 1 1 d . . . . . C3 C 0.6556(3) 0.5039(4) 0.5744(3) 0.0525(11) Uani 1 1 d . . . . . C12 C 0.4353(4) 0.4269(4) 0.6372(3) 0.0678(14) Uani 1 1 d . . . . . H12A H 0.386322 0.375876 0.651616 0.102 Uiso 1 1 calc R U . . . H12B H 0.408668 0.487829 0.603681 0.102 Uiso 1 1 calc R U . . . H12C H 0.495834 0.401515 0.608433 0.102 Uiso 1 1 calc R U . . . C2 C 0.6977(3) 0.6991(4) 0.5428(3) 0.0587(12) Uani 1 1 d . . . . . C4 C 0.8242(4) 0.5400(4) 0.6817(4) 0.0705(14) Uani 1 1 d . . . . . C14 C 0.5405(3) 0.8255(4) 0.6651(3) 0.0663(14) Uani 1 1 d . . . . . C1 C 0.5058(3) 0.6518(3) 0.5680(3) 0.0504(11) Uani 1 1 d . . . . . N5 N 0.7019(3) 0.5671(3) 0.7755(3) 0.0725(12) Uani 1 1 d . . . . . C25 C 0.1670(4) 0.4932(5) 0.7110(4) 0.0855(17) Uani 1 1 d . . . . . H25 H 0.138417 0.432361 0.739226 0.103 Uiso 1 1 calc R U . . . C26 C 0.2556(5) 0.9622(6) 0.7002(4) 0.099(2) Uani 1 1 d . . . . . H26 H 0.242402 0.915531 0.749387 0.119 Uiso 1 1 calc R U . . . C37 C 0.3883(6) 0.8401(7) 0.1608(4) 0.137(3) Uani 1 1 d . . . . . H37 H 0.324942 0.832889 0.149005 0.165 Uiso 1 1 calc R U . . . C39 C 0.0044(5) 0.7652(5) 0.2932(4) 0.099(2) Uani 1 1 d . . . . . H39 H 0.046034 0.781704 0.243858 0.118 Uiso 1 1 calc R U . . . C27 C 0.2698(6) 1.0548(6) 0.7016(5) 0.132(3) Uani 1 1 d . . . . . H27A H 0.283241 1.103784 0.653698 0.158 Uiso 1 1 calc R U . . . H27B H 0.266611 1.072610 0.750539 0.158 Uiso 1 1 calc R U . . . F4 F 0.8376(6) 0.8805(8) 0.0907(5) 0.285(4) Uani 1 1 d . . . . . C28 C 0.1729(6) 0.5680(6) 0.8247(4) 0.131(3) Uani 1 1 d . . . . . H28 H 0.177814 0.629179 0.839038 0.157 Uiso 1 1 calc R U . . . C15 C 0.5186(5) 0.8637(5) 0.7316(4) 0.0884(18) Uani 1 1 d . . . . . H15 H 0.497796 0.931100 0.732931 0.106 Uiso 1 1 calc R U . . . C5 C 0.8602(5) 0.5215(5) 0.7544(4) 0.097(2) Uani 1 1 d . . . . . H5 H 0.926365 0.501160 0.762338 0.116 Uiso 1 1 calc R U . . . C6 C 0.7840(6) 0.5376(5) 0.8113(4) 0.104(2) Uani 1 1 d . . . . . B1 B 0.5918(5) 0.5935(5) 0.8090(4) 0.0767(18) Uani 1 1 d . . . . . H1 H 0.584668 0.586630 0.867241 0.092 Uiso 1 1 calc R U . . . C13 C 0.4464(7) 0.4337(6) 0.9279(4) 0.151(3) Uani 1 1 d . . . . . H13A H 0.400442 0.380496 0.950698 0.226 Uiso 1 1 calc R U . . . H13B H 0.418944 0.495446 0.943547 0.226 Uiso 1 1 calc R U . . . H13C H 0.509874 0.413265 0.946926 0.226 Uiso 1 1 calc R U . . . C11 C 0.4619(5) 0.4519(5) 0.8383(4) 0.0932(19) Uani 1 1 d . . . . . C18 C 0.5192(7) 0.7850(6) 0.8836(4) 0.144(3) Uani 1 1 d . . . . . H18A H 0.583253 0.768739 0.902303 0.216 Uiso 1 1 calc R U . . . H18B H 0.473127 0.734128 0.912922 0.216 Uiso 1 1 calc R U . . . H18C H 0.492760 0.850911 0.891974 0.216 Uiso 1 1 calc R U . . . C8 C 0.7854(7) 0.5260(8) 0.8986(4) 0.171(4) Uani 1 1 d . . . . . H8A H 0.768172 0.591085 0.912169 0.256 Uiso 1 1 calc R U . . . H8B H 0.851669 0.501679 0.910803 0.256 Uiso 1 1 calc R U . . . H8C H 0.737391 0.477899 0.929203 0.256 Uiso 1 1 calc R U . . . C17 C 0.5323(4) 0.8824(4) 0.5802(3) 0.0765(15) Uani 1 1 d . . . . . H17A H 0.463049 0.888467 0.572079 0.115 Uiso 1 1 calc R U . . . H17B H 0.572002 0.845731 0.543493 0.115 Uiso 1 1 calc R U . . . H17C H 0.556685 0.949468 0.570685 0.115 Uiso 1 1 calc R U . . . C19 C 0.2621(4) 0.9267(4) 0.5036(4) 0.0803(16) Uani 1 1 d . . . . . H19 H 0.263347 0.948484 0.448269 0.096 Uiso 1 1 calc R U . . . C35 C 0.0667(4) 0.7340(4) 0.4883(3) 0.0737(15) Uani 1 1 d . . . . . H35 H 0.051610 0.728613 0.543495 0.088 Uiso 1 1 calc R U . . . C31 C 0.4785(4) 0.8416(4) 0.2743(4) 0.0803(16) Uani 1 1 d . . . . . H31 H 0.537713 0.869068 0.244602 0.096 Uiso 1 1 calc R U . . . C20 C 0.2557(4) 0.9887(4) 0.5557(4) 0.0837(17) Uani 1 1 d . . . . . H20 H 0.250515 1.059880 0.542754 0.100 Uiso 1 1 calc R U . . . C36 C -0.0017(4) 0.7440(4) 0.4380(4) 0.0837(17) Uani 1 1 d . . . . . H36 H -0.071535 0.747105 0.451967 0.100 Uiso 1 1 calc R U . . . C7 C 0.8803(4) 0.5312(4) 0.6014(4) 0.0840(17) Uani 1 1 d . . . . . H7A H 0.947373 0.502266 0.607210 0.126 Uiso 1 1 calc R U . . . H7B H 0.883617 0.597875 0.565739 0.126 Uiso 1 1 calc R U . . . H7C H 0.845895 0.487803 0.579667 0.126 Uiso 1 1 calc R U . . . C16 C 0.5323(5) 0.7869(5) 0.7956(4) 0.0860(17) Uani 1 1 d . . . . . C10 C 0.4204(4) 0.4068(5) 0.7895(4) 0.0903(18) Uani 1 1 d . . . . . H10 H 0.374817 0.355616 0.806366 0.108 Uiso 1 1 calc R U . . . C22 C 0.2648(4) 0.7375(5) 0.6884(4) 0.0798(16) Uani 1 1 d . . . . . F2 F 0.6903(9) 0.9103(13) 0.1094(11) 0.392(7) Uani 1 1 d . . . . . F3 F 0.7264(8) 0.7911(10) 0.0504(5) 0.321(5) Uani 1 1 d . . . . . O3 O 0.0558(5) 0.7895(6) 0.7214(5) 0.234(4) Uani 1 1 d . . . . . N18 N -0.1296(15) 0.8898(14) 0.6670(8) 0.367(13) Uani 1 1 d . . . . . C43 C -0.0435(15) 0.7892(17) 0.7049(14) 0.366(16) Uani 1 1 d . . . . . H43 H -0.067989 0.724386 0.716074 0.440 Uiso 1 1 calc R U . . . C42 C -0.0454(8) 0.9436(8) 0.6041(7) 0.210(5) Uani 1 1 d . . . . . H42A H -0.054641 0.938669 0.551550 0.316 Uiso 1 1 calc R U . . . H42B H 0.018904 0.911308 0.615669 0.316 Uiso 1 1 calc R U . . . H42C H -0.047768 1.014325 0.605869 0.316 Uiso 1 1 calc R U . . . C41 C -0.1839(9) 0.8256(10) 0.6632(8) 0.242(6) Uani 1 1 d . . . . . H41A H -0.168580 0.762433 0.700037 0.364 Uiso 1 1 calc R U . . . H41B H -0.173142 0.815344 0.609485 0.364 Uiso 1 1 calc R U . . . H41C H -0.253088 0.848004 0.677079 0.364 Uiso 1 1 calc R U . . . B2 B 0.745(2) 0.829(3) 0.129(4) 0.42(4) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co1 0.0423(4) 0.0549(4) 0.0653(5) -0.0120(3) -0.0061(3) 0.0026(3) Fe1 0.0442(4) 0.0524(4) 0.0565(4) -0.0103(3) -0.0079(3) -0.0023(3) N8 0.057(2) 0.051(3) 0.064(3) -0.015(2) -0.008(2) 0.0017(18) O1 0.085(3) 0.151(4) 0.093(3) -0.048(3) -0.009(2) -0.017(3) O2 0.138(4) 0.108(3) 0.096(3) -0.025(3) -0.036(3) -0.012(3) N2 0.056(3) 0.074(3) 0.079(3) -0.004(2) 0.007(2) -0.005(2) C40 0.071(4) 0.157(7) 0.151(7) -0.058(5) -0.041(4) 0.016(4) F1 0.73(4) 0.41(2) 0.50(2) 0.062(18) -0.31(2) -0.40(3) C38 0.145(8) 0.297(13) 0.067(5) -0.004(6) 0.005(5) -0.063(8) C29 0.255(11) 0.141(8) 0.083(6) -0.006(5) 0.007(6) -0.030(7) N6 0.053(2) 0.063(3) 0.055(3) -0.0084(19) -0.0044(19) -0.0047(19) N4 0.054(3) 0.059(3) 0.070(3) -0.013(2) -0.020(2) -0.0013(19) N3 0.046(2) 0.056(3) 0.066(3) -0.019(2) -0.0077(19) 0.0050(18) N16 0.045(2) 0.067(3) 0.070(3) -0.006(2) -0.004(2) -0.0031(19) N1 0.052(2) 0.062(3) 0.061(3) -0.0078(19) -0.012(2) -0.0029(19) N12 0.043(2) 0.063(3) 0.073(3) -0.009(2) -0.002(2) -0.0049(19) N10 0.059(3) 0.051(3) 0.073(3) -0.013(2) -0.001(2) 0.0029(19) N14 0.047(2) 0.061(3) 0.068(3) -0.011(2) -0.003(2) -0.0050(19) N11 0.069(3) 0.062(3) 0.098(4) -0.027(3) -0.001(3) 0.002(2) N13 0.094(3) 0.076(3) 0.056(3) -0.009(3) 0.007(3) 0.000(3) N17 0.044(2) 0.083(3) 0.082(3) -0.007(2) -0.015(2) 0.005(2) N15 0.059(3) 0.097(4) 0.070(3) -0.009(3) -0.003(3) -0.002(2) N9 0.081(3) 0.065(3) 0.061(3) -0.020(2) -0.011(2) -0.002(2) C34 0.046(3) 0.073(3) 0.066(4) -0.011(3) -0.009(3) -0.010(2) C23 0.057(3) 0.054(3) 0.084(4) -0.012(3) -0.006(3) 0.003(2) C32 0.050(3) 0.074(4) 0.063(4) -0.010(3) -0.002(3) 0.002(2) C33 0.058(3) 0.080(4) 0.069(4) -0.022(3) -0.014(3) 0.001(3) C24 0.060(3) 0.065(4) 0.093(5) -0.013(3) -0.004(3) -0.008(3) C30 0.050(3) 0.070(3) 0.076(4) -0.013(3) -0.005(3) -0.009(2) C21 0.061(3) 0.053(3) 0.084(4) -0.023(3) -0.004(3) 0.002(2) C9 0.048(3) 0.048(3) 0.081(4) -0.007(3) -0.007(3) 0.000(2) N7 0.080(3) 0.072(3) 0.059(3) -0.008(2) -0.006(2) -0.018(2) C3 0.036(2) 0.064(3) 0.057(3) -0.008(2) -0.009(2) -0.008(2) C12 0.055(3) 0.061(3) 0.089(4) -0.021(3) -0.009(3) -0.007(2) C2 0.045(3) 0.054(3) 0.074(4) -0.012(3) -0.009(3) 0.000(2) C4 0.057(3) 0.062(3) 0.094(4) -0.013(3) -0.024(3) -0.001(3) C14 0.051(3) 0.062(4) 0.087(4) -0.020(3) -0.011(3) -0.004(2) C1 0.043(3) 0.052(3) 0.054(3) -0.010(2) -0.003(2) -0.005(2) N5 0.080(3) 0.077(3) 0.066(3) -0.010(2) -0.035(3) 0.000(2) C25 0.075(4) 0.077(4) 0.092(5) -0.008(4) 0.010(3) -0.014(3) C26 0.101(5) 0.101(5) 0.109(5) -0.048(4) -0.017(4) -0.003(4) C37 0.104(6) 0.230(10) 0.075(5) -0.022(6) -0.006(5) -0.043(6) C39 0.065(4) 0.129(6) 0.098(5) -0.009(4) -0.028(4) -0.001(4) C27 0.153(7) 0.122(7) 0.147(7) -0.075(5) -0.043(5) 0.014(5) F4 0.156(6) 0.410(13) 0.264(8) -0.022(8) 0.008(5) -0.111(7) C28 0.199(8) 0.101(6) 0.077(5) -0.008(4) 0.008(5) -0.017(5) C15 0.103(5) 0.068(4) 0.100(5) -0.037(4) -0.012(4) 0.005(3) C5 0.072(4) 0.113(5) 0.108(5) -0.016(4) -0.051(4) 0.017(4) C6 0.102(5) 0.114(5) 0.100(6) -0.016(4) -0.048(5) 0.004(4) B1 0.084(5) 0.094(5) 0.050(4) -0.015(3) -0.006(3) -0.006(4) C13 0.198(9) 0.173(8) 0.065(5) 0.007(5) 0.017(5) -0.087(7) C11 0.111(5) 0.090(5) 0.067(4) -0.004(3) 0.009(4) -0.027(4) C18 0.209(9) 0.129(7) 0.103(6) -0.062(5) -0.014(6) 0.017(6) C8 0.174(8) 0.254(11) 0.100(6) -0.054(6) -0.081(6) 0.044(8) C17 0.067(3) 0.059(3) 0.097(4) -0.013(3) -0.001(3) -0.002(3) C19 0.070(4) 0.068(4) 0.094(4) -0.012(3) -0.002(3) 0.006(3) C35 0.052(3) 0.093(4) 0.066(4) -0.008(3) 0.001(3) 0.004(3) C31 0.052(3) 0.089(4) 0.091(5) -0.011(3) 0.004(3) -0.010(3) C20 0.082(4) 0.049(3) 0.113(5) -0.020(4) 0.002(4) 0.001(3) C36 0.044(3) 0.093(4) 0.100(5) 0.007(3) -0.018(3) -0.001(3) C7 0.045(3) 0.092(4) 0.109(5) -0.011(3) -0.013(3) -0.006(3) C16 0.108(5) 0.081(4) 0.073(4) -0.035(4) -0.006(3) 0.002(4) C10 0.087(4) 0.089(4) 0.082(4) 0.002(3) 0.010(3) -0.037(3) C22 0.074(4) 0.093(5) 0.070(4) -0.018(4) -0.010(3) 0.004(3) F2 0.197(10) 0.47(2) 0.56(2) -0.192(19) -0.096(12) -0.031(12) F3 0.314(10) 0.501(17) 0.204(7) -0.171(9) -0.017(7) -0.104(11) O3 0.117(5) 0.186(7) 0.317(10) 0.044(6) 0.027(6) 0.020(5) N18 0.47(3) 0.41(2) 0.222(12) 0.120(13) -0.174(15) -0.34(2) C43 0.29(2) 0.39(3) 0.48(3) -0.35(3) 0.22(2) -0.21(2) C42 0.194(11) 0.179(10) 0.220(12) 0.019(9) -0.003(9) -0.039(8) C41 0.208(12) 0.230(13) 0.340(18) -0.082(12) -0.112(11) -0.095(10) B2 0.16(2) 0.34(4) 0.92(10) -0.40(5) -0.27(4) 0.10(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3 Co1 N16 90.01(15) 2_666 . ? N3 Co1 N1 91.83(14) 2_666 . ? N3 Co1 N12 90.79(16) 2_666 . ? N3 Co1 N10 174.17(16) 2_666 . ? N3 Co1 N14 89.51(15) 2_666 . ? N16 Co1 N12 94.84(15) . . ? N16 Co1 N10 89.94(16) . . ? N16 Co1 N14 83.14(15) . . ? N1 Co1 N16 174.51(15) . . ? N1 Co1 N12 90.31(14) . . ? N1 Co1 N10 88.75(15) . . ? N1 Co1 N14 91.70(15) . . ? N12 Co1 N14 177.96(14) . . ? N10 Co1 N12 83.41(17) . . ? N10 Co1 N14 96.27(16) . . ? N6 Fe1 N8 90.10(16) . . ? N6 Fe1 N4 89.93(16) . . ? N4 Fe1 N8 88.96(16) . . ? C3 Fe1 N8 179.89(19) . . ? C3 Fe1 N6 89.94(17) . . ? C3 Fe1 N4 91.15(17) . . ? C3 Fe1 C2 87.07(19) . . ? C2 Fe1 N8 92.88(18) . . ? C2 Fe1 N6 175.91(19) . . ? C2 Fe1 N4 92.91(18) . . ? C1 Fe1 N8 90.38(17) . . ? C1 Fe1 N6 89.25(17) . . ? C1 Fe1 N4 178.95(18) . . ? C1 Fe1 C3 89.52(18) . . ? C1 Fe1 C2 87.94(18) . . ? N9 N8 Fe1 117.6(3) . . ? C14 N8 Fe1 136.3(4) . . ? C14 N8 N9 106.2(4) . . ? H40A C40 H40B 120.0 . . ? C39 C40 H40A 120.0 . . ? C39 C40 H40B 120.0 . . ? H38A C38 H38B 120.0 . . ? C37 C38 H38A 120.0 . . ? C37 C38 H38B 120.0 . . ? H29A C29 H29B 120.0 . . ? C28 C29 H29A 120.0 . . ? C28 C29 H29B 120.0 . . ? C9 N6 Fe1 135.5(4) . . ? C9 N6 N7 107.7(4) . . ? N7 N6 Fe1 116.9(3) . . ? C4 N4 Fe1 135.7(4) . . ? C4 N4 N5 107.0(4) . . ? N5 N4 Fe1 117.3(3) . . ? C3 N3 Co1 169.1(4) . 2_666 ? C34 N16 Co1 127.3(3) . . ? C34 N16 C35 106.2(4) . . ? C35 N16 Co1 125.9(4) . . ? C1 N1 Co1 167.1(4) . . ? C23 N12 Co1 126.4(4) . . ? C23 N12 C24 105.6(5) . . ? C24 N12 Co1 126.9(4) . . ? C21 N10 Co1 126.0(3) . . ? C21 N10 C19 107.7(5) . . ? C19 N10 Co1 125.4(4) . . ? C32 N14 Co1 124.2(3) . . ? C32 N14 C30 106.9(4) . . ? C30 N14 Co1 126.9(4) . . ? C21 N11 C26 130.0(6) . . ? C21 N11 C20 105.8(5) . . ? C20 N11 C26 124.2(5) . . ? C23 N13 C28 127.9(6) . . ? C25 N13 C23 106.8(5) . . ? C25 N13 C28 124.8(6) . . ? C34 N17 C39 127.9(5) . . ? C36 N17 C34 107.6(4) . . ? C36 N17 C39 124.4(5) . . ? C32 N15 C37 127.5(5) . . ? C31 N15 C32 106.1(5) . . ? C31 N15 C37 126.0(5) . . ? N8 N9 B1 117.9(4) . . ? C16 N9 N8 109.1(4) . . ? C16 N9 B1 133.0(5) . . ? N16 C34 N17 109.8(4) . . ? N16 C34 C33 125.1(4) . . ? N17 C34 C33 125.0(5) . . ? N12 C23 N13 110.7(5) . . ? N12 C23 C22 125.2(5) . . ? N13 C23 C22 124.1(6) . . ? N14 C32 N15 109.3(4) . . ? N14 C32 C33 127.2(5) . . ? N15 C32 C33 123.5(5) . . ? O1 C33 C34 120.6(5) . . ? O1 C33 C32 120.8(5) . . ? C32 C33 C34 118.5(5) . . ? N12 C24 H24 125.0 . . ? C25 C24 N12 110.1(5) . . ? C25 C24 H24 125.0 . . ? N14 C30 H30 125.2 . . ? C31 C30 N14 109.6(5) . . ? C31 C30 H30 125.2 . . ? N10 C21 N11 110.5(5) . . ? N10 C21 C22 125.9(5) . . ? N11 C21 C22 123.6(5) . . ? N6 C9 C12 124.5(5) . . ? N6 C9 C10 108.0(5) . . ? C10 C9 C12 127.5(5) . . ? N6 N7 B1 118.7(4) . . ? C11 N7 N6 108.9(4) . . ? C11 N7 B1 132.4(5) . . ? N3 C3 Fe1 177.3(4) . . ? C9 C12 H12A 109.5 . . ? C9 C12 H12B 109.5 . . ? C9 C12 H12C 109.5 . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? N2 C2 Fe1 178.3(5) . . ? N4 C4 C5 106.9(5) . . ? N4 C4 C7 124.5(5) . . ? C5 C4 C7 128.6(5) . . ? N8 C14 C15 109.3(5) . . ? N8 C14 C17 123.9(5) . . ? C15 C14 C17 126.8(5) . . ? N1 C1 Fe1 176.8(4) . . ? N4 N5 B1 118.1(4) . . ? C6 N5 N4 110.1(5) . . ? C6 N5 B1 131.8(6) . . ? N13 C25 H25 126.6 . . ? C24 C25 N13 106.7(5) . . ? C24 C25 H25 126.6 . . ? N11 C26 H26 117.4 . . ? C27 C26 N11 125.2(7) . . ? C27 C26 H26 117.4 . . ? C38 C37 N15 126.5(7) . . ? C38 C37 H37 116.7 . . ? N15 C37 H37 116.7 . . ? C40 C39 N17 124.5(7) . . ? C40 C39 H39 117.7 . . ? N17 C39 H39 117.7 . . ? C26 C27 H27A 120.0 . . ? C26 C27 H27B 120.0 . . ? H27A C27 H27B 120.0 . . ? C29 C28 N13 123.8(8) . . ? C29 C28 H28 118.1 . . ? N13 C28 H28 118.1 . . ? C14 C15 H15 126.0 . . ? C16 C15 C14 107.9(6) . . ? C16 C15 H15 126.0 . . ? C4 C5 H5 125.6 . . ? C6 C5 C4 108.8(6) . . ? C6 C5 H5 125.6 . . ? N5 C6 C5 107.2(6) . . ? N5 C6 C8 124.3(7) . . ? C5 C6 C8 128.5(7) . . ? N9 B1 N7 111.0(5) . . ? N9 B1 N5 107.8(5) . . ? N9 B1 H1 110.0 . . ? N7 B1 N5 108.0(5) . . ? N7 B1 H1 110.0 . . ? N5 B1 H1 110.0 . . ? H13A C13 H13B 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? C11 C13 H13A 109.5 . . ? C11 C13 H13B 109.5 . . ? C11 C13 H13C 109.5 . . ? N7 C11 C13 122.3(6) . . ? N7 C11 C10 107.6(5) . . ? C10 C11 C13 130.1(6) . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C16 C18 H18A 109.5 . . ? C16 C18 H18B 109.5 . . ? C16 C18 H18C 109.5 . . ? C6 C8 H8A 109.5 . . ? C6 C8 H8B 109.5 . . ? C6 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C14 C17 H17A 109.5 . . ? C14 C17 H17B 109.5 . . ? C14 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? N10 C19 H19 125.7 . . ? N10 C19 C20 108.7(5) . . ? C20 C19 H19 125.7 . . ? N16 C35 H35 125.4 . . ? C36 C35 N16 109.2(5) . . ? C36 C35 H35 125.4 . . ? N15 C31 H31 126.0 . . ? C30 C31 N15 108.0(5) . . ? C30 C31 H31 126.0 . . ? N11 C20 H20 126.4 . . ? C19 C20 N11 107.3(5) . . ? C19 C20 H20 126.4 . . ? N17 C36 C35 107.2(5) . . ? N17 C36 H36 126.4 . . ? C35 C36 H36 126.4 . . ? C4 C7 H7A 109.5 . . ? C4 C7 H7B 109.5 . . ? C4 C7 H7C 109.5 . . ? H7A C7 H7B 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? N9 C16 C18 121.4(6) . . ? C15 C16 N9 107.5(5) . . ? C15 C16 C18 131.1(6) . . ? C9 C10 H10 126.1 . . ? C11 C10 C9 107.8(5) . . ? C11 C10 H10 126.1 . . ? O2 C22 C23 120.5(6) . . ? O2 C22 C21 120.6(6) . . ? C23 C22 C21 118.9(5) . . ? C42 N18 C43 91.4(15) . . ? C41 N18 C43 88.1(15) . . ? C41 N18 C42 130.1(16) . . ? O3 C43 N18 131.7(15) . . ? O3 C43 H43 114.1 . . ? N18 C43 H43 114.1 . . ? N18 C42 H42A 109.5 . . ? N18 C42 H42B 109.5 . . ? N18 C42 H42C 109.5 . . ? H42A C42 H42B 109.5 . . ? H42A C42 H42C 109.5 . . ? H42B C42 H42C 109.5 . . ? N18 C41 H41A 109.5 . . ? N18 C41 H41B 109.5 . . ? N18 C41 H41C 109.5 . . ? H41A C41 H41B 109.5 . . ? H41A C41 H41C 109.5 . . ? H41B C41 H41C 109.5 . . ? F1 B2 F4 109(4) . . ? F1 B2 F2 158(6) . . ? F1 B2 F3 90(4) . . ? F4 B2 F3 96(3) . . ? F2 B2 F4 92(3) . . ? F2 B2 F3 91(3) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Co1 N3 2.077(4) 2_666 ? Co1 N16 2.113(4) . ? Co1 N1 2.092(4) . ? Co1 N12 2.143(4) . ? Co1 N10 2.121(4) . ? Co1 N14 2.153(4) . ? Fe1 N8 2.009(4) . ? Fe1 N6 1.978(4) . ? Fe1 N4 2.003(4) . ? Fe1 C3 1.920(5) . ? Fe1 C2 1.934(5) . ? Fe1 C1 1.902(5) . ? N8 N9 1.365(5) . ? N8 C14 1.346(6) . ? O1 C33 1.204(6) . ? O2 C22 1.219(6) . ? N2 C2 1.141(5) . ? C40 H40A 0.9300 . ? C40 H40B 0.9300 . ? C40 C39 1.265(7) . ? F1 B2 0.73(5) . ? C38 H38A 0.9300 . ? C38 H38B 0.9300 . ? C38 C37 1.268(9) . ? C29 H29A 0.9300 . ? C29 H29B 0.9300 . ? C29 C28 1.264(9) . ? N6 C9 1.346(6) . ? N6 N7 1.377(5) . ? N4 C4 1.355(6) . ? N4 N5 1.359(5) . ? N3 C3 1.150(5) . ? N16 C34 1.325(6) . ? N16 C35 1.358(6) . ? N1 C1 1.151(5) . ? N12 C23 1.315(6) . ? N12 C24 1.363(6) . ? N10 C21 1.315(6) . ? N10 C19 1.347(6) . ? N14 C32 1.326(6) . ? N14 C30 1.380(6) . ? N11 C21 1.365(6) . ? N11 C26 1.391(7) . ? N11 C20 1.373(7) . ? N13 C23 1.367(6) . ? N13 C25 1.350(7) . ? N13 C28 1.404(8) . ? N17 C34 1.354(6) . ? N17 C39 1.425(7) . ? N17 C36 1.339(7) . ? N15 C32 1.395(6) . ? N15 C37 1.420(8) . ? N15 C31 1.373(6) . ? N9 B1 1.505(7) . ? N9 C16 1.349(6) . ? C34 C33 1.457(7) . ? C23 C22 1.450(8) . ? C32 C33 1.444(7) . ? C24 H24 0.9300 . ? C24 C25 1.349(7) . ? C30 H30 0.9300 . ? C30 C31 1.332(7) . ? C21 C22 1.473(7) . ? C9 C12 1.483(6) . ? C9 C10 1.376(7) . ? N7 B1 1.520(8) . ? N7 C11 1.343(6) . ? C12 H12A 0.9600 . ? C12 H12B 0.9600 . ? C12 H12C 0.9600 . ? C4 C5 1.384(7) . ? C4 C7 1.493(7) . ? C14 C15 1.352(7) . ? C14 C17 1.503(7) . ? N5 C6 1.339(7) . ? N5 B1 1.540(8) . ? C25 H25 0.9300 . ? C26 H26 0.9300 . ? C26 C27 1.290(8) . ? C37 H37 0.9300 . ? C39 H39 0.9300 . ? C27 H27A 0.9300 . ? C27 H27B 0.9300 . ? F4 B2 1.46(4) . ? C28 H28 0.9300 . ? C15 H15 0.9300 . ? C15 C16 1.345(8) . ? C5 H5 0.9300 . ? C5 C6 1.339(8) . ? C6 C8 1.487(9) . ? B1 H1 0.9800 . ? C13 H13A 0.9600 . ? C13 H13B 0.9600 . ? C13 H13C 0.9600 . ? C13 C11 1.493(8) . ? C11 C10 1.372(8) . ? C18 H18A 0.9600 . ? C18 H18B 0.9600 . ? C18 H18C 0.9600 . ? C18 C16 1.502(8) . ? C8 H8A 0.9600 . ? C8 H8B 0.9600 . ? C8 H8C 0.9600 . ? C17 H17A 0.9600 . ? C17 H17B 0.9600 . ? C17 H17C 0.9600 . ? C19 H19 0.9300 . ? C19 C20 1.362(7) . ? C35 H35 0.9300 . ? C35 C36 1.350(7) . ? C31 H31 0.9300 . ? C20 H20 0.9300 . ? C36 H36 0.9300 . ? C7 H7A 0.9600 . ? C7 H7B 0.9600 . ? C7 H7C 0.9600 . ? C10 H10 0.9300 . ? F2 B2 1.27(3) . ? F3 B2 1.63(4) . ? O3 C43 1.42(2) . ? N18 C43 1.77(3) . ? N18 C42 1.537(17) . ? N18 C41 1.209(13) . ? C43 H43 0.9300 . ? C42 H42A 0.9600 . ? C42 H42B 0.9600 . ? C42 H42C 0.9600 . ? C41 H41A 0.9600 . ? C41 H41B 0.9600 . ? C41 H41C 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Co1 N16 C34 N17 170.4(3) . . . . ? Co1 N16 C34 C33 -9.2(7) . . . . ? Co1 N16 C35 C36 -171.1(4) . . . . ? Co1 N12 C23 N13 -169.9(3) . . . . ? Co1 N12 C23 C22 10.5(7) . . . . ? Co1 N12 C24 C25 170.7(3) . . . . ? Co1 N10 C21 N11 170.0(3) . . . . ? Co1 N10 C21 C22 -12.0(7) . . . . ? Co1 N10 C19 C20 -170.9(3) . . . . ? Co1 N14 C32 N15 -165.6(3) . . . . ? Co1 N14 C32 C33 15.0(7) . . . . ? Co1 N14 C30 C31 165.3(3) . . . . ? Fe1 N8 N9 B1 -0.9(5) . . . . ? Fe1 N8 N9 C16 -179.0(3) . . . . ? Fe1 N8 C14 C15 179.8(4) . . . . ? Fe1 N8 C14 C17 1.3(7) . . . . ? Fe1 N6 C9 C12 -0.2(7) . . . . ? Fe1 N6 C9 C10 178.2(4) . . . . ? Fe1 N6 N7 B1 2.2(6) . . . . ? Fe1 N6 N7 C11 -179.2(4) . . . . ? Fe1 N4 C4 C5 -179.9(4) . . . . ? Fe1 N4 C4 C7 0.8(8) . . . . ? Fe1 N4 N5 C6 179.8(4) . . . . ? Fe1 N4 N5 B1 1.3(6) . . . . ? N8 N9 B1 N7 -57.2(6) . . . . ? N8 N9 B1 N5 60.9(6) . . . . ? N8 N9 C16 C15 -1.5(6) . . . . ? N8 N9 C16 C18 179.7(6) . . . . ? N8 C14 C15 C16 -0.9(7) . . . . ? N6 C9 C10 C11 1.8(7) . . . . ? N6 N7 B1 N9 57.2(6) . . . . ? N6 N7 B1 N5 -60.8(6) . . . . ? N6 N7 C11 C13 179.6(6) . . . . ? N6 N7 C11 C10 0.7(7) . . . . ? N4 C4 C5 C6 1.5(7) . . . . ? N4 N5 C6 C5 -0.2(7) . . . . ? N4 N5 C6 C8 -180.0(7) . . . . ? N4 N5 B1 N9 -61.6(6) . . . . ? N4 N5 B1 N7 58.4(6) . . . . ? N16 C34 C33 O1 158.1(5) . . . . ? N16 C34 C33 C32 -24.5(8) . . . . ? N16 C35 C36 N17 0.3(6) . . . . ? N12 C23 C22 O2 -158.3(5) . . . . ? N12 C23 C22 C21 23.8(8) . . . . ? N12 C24 C25 N13 -2.2(6) . . . . ? N10 C21 C22 O2 158.8(5) . . . . ? N10 C21 C22 C23 -23.3(8) . . . . ? N10 C19 C20 N11 1.5(6) . . . . ? N14 C32 C33 O1 -161.7(5) . . . . ? N14 C32 C33 C34 21.0(8) . . . . ? N14 C30 C31 N15 -0.8(6) . . . . ? N11 C21 C22 O2 -23.4(8) . . . . ? N11 C21 C22 C23 154.5(5) . . . . ? N13 C23 C22 O2 22.2(8) . . . . ? N13 C23 C22 C21 -155.8(5) . . . . ? N17 C34 C33 O1 -21.4(8) . . . . ? N17 C34 C33 C32 155.9(5) . . . . ? N15 C32 C33 O1 18.9(8) . . . . ? N15 C32 C33 C34 -158.4(5) . . . . ? N9 N8 C14 C15 0.0(5) . . . . ? N9 N8 C14 C17 -178.6(4) . . . . ? C34 N16 C35 C36 0.5(6) . . . . ? C34 N17 C39 C40 172.2(6) . . . . ? C34 N17 C36 C35 -0.9(6) . . . . ? C23 N12 C24 C25 2.1(6) . . . . ? C23 N13 C25 C24 1.4(6) . . . . ? C23 N13 C28 C29 -172.2(8) . . . . ? C32 N14 C30 C31 0.9(6) . . . . ? C32 N15 C37 C38 -174.7(9) . . . . ? C32 N15 C31 C30 0.3(6) . . . . ? C24 N12 C23 N13 -1.2(5) . . . . ? C24 N12 C23 C22 179.2(5) . . . . ? C30 N14 C32 N15 -0.7(5) . . . . ? C30 N14 C32 C33 179.9(5) . . . . ? C21 N10 C19 C20 -1.1(6) . . . . ? C21 N11 C26 C27 165.7(6) . . . . ? C21 N11 C20 C19 -1.3(6) . . . . ? C9 N6 N7 B1 -178.2(4) . . . . ? C9 N6 N7 C11 0.5(6) . . . . ? N7 N6 C9 C12 -179.8(4) . . . . ? N7 N6 C9 C10 -1.4(5) . . . . ? N7 C11 C10 C9 -1.5(7) . . . . ? C12 C9 C10 C11 -179.9(5) . . . . ? C4 N4 N5 C6 1.1(6) . . . . ? C4 N4 N5 B1 -177.4(5) . . . . ? C4 C5 C6 N5 -0.8(8) . . . . ? C4 C5 C6 C8 179.0(7) . . . . ? C14 N8 N9 B1 179.0(4) . . . . ? C14 N8 N9 C16 0.9(5) . . . . ? C14 C15 C16 N9 1.5(7) . . . . ? C14 C15 C16 C18 -179.9(7) . . . . ? N5 N4 C4 C5 -1.6(6) . . . . ? N5 N4 C4 C7 179.2(5) . . . . ? C25 N13 C23 N12 -0.1(6) . . . . ? C25 N13 C23 C22 179.5(5) . . . . ? C25 N13 C28 C29 15.9(13) . . . . ? C26 N11 C21 N10 -179.5(5) . . . . ? C26 N11 C21 C22 2.5(8) . . . . ? C26 N11 C20 C19 178.8(5) . . . . ? C37 N15 C32 N14 -173.5(6) . . . . ? C37 N15 C32 C33 6.0(9) . . . . ? C37 N15 C31 C30 174.2(6) . . . . ? C39 N17 C34 N16 176.4(5) . . . . ? C39 N17 C34 C33 -4.0(9) . . . . ? C39 N17 C36 C35 -176.3(5) . . . . ? C28 N13 C23 N12 -173.1(6) . . . . ? C28 N13 C23 C22 6.5(9) . . . . ? C28 N13 C25 C24 174.7(6) . . . . ? C6 N5 B1 N9 120.3(6) . . . . ? C6 N5 B1 N7 -119.7(6) . . . . ? B1 N9 C16 C15 -179.1(6) . . . . ? B1 N9 C16 C18 2.1(10) . . . . ? B1 N7 C11 C13 -2.0(11) . . . . ? B1 N7 C11 C10 179.0(6) . . . . ? B1 N5 C6 C5 178.1(6) . . . . ? B1 N5 C6 C8 -1.8(11) . . . . ? C13 C11 C10 C9 179.6(7) . . . . ? C11 N7 B1 N9 -121.1(6) . . . . ? C11 N7 B1 N5 121.0(6) . . . . ? C17 C14 C15 C16 177.6(5) . . . . ? C19 N10 C21 N11 0.3(6) . . . . ? C19 N10 C21 C22 178.3(5) . . . . ? C35 N16 C34 N17 -1.0(6) . . . . ? C35 N16 C34 C33 179.4(5) . . . . ? C31 N15 C32 N14 0.2(6) . . . . ? C31 N15 C32 C33 179.7(5) . . . . ? C31 N15 C37 C38 12.7(13) . . . . ? C20 N11 C21 N10 0.6(6) . . . . ? C20 N11 C21 C22 -177.5(5) . . . . ? C20 N11 C26 C27 -14.4(10) . . . . ? C36 N17 C34 N16 1.2(6) . . . . ? C36 N17 C34 C33 -179.2(5) . . . . ? C36 N17 C39 C40 -13.3(10) . . . . ? C7 C4 C5 C6 -179.3(6) . . . . ? C16 N9 B1 N7 120.2(6) . . . . ? C16 N9 B1 N5 -121.6(6) . . . . ? C42 N18 C43 O3 42(2) . . . . ? C41 N18 C43 O3 172.5(17) . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.000 0.000 0.000 666.4 156.2 '4 DMF'