#------------------------------------------------------------------------------ #$Date: 2021-04-24 02:20:20 +0300 (Sat, 24 Apr 2021) $ #$Revision: 264495 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/20/1562054.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1562054 loop_ _publ_author_name 'Kamilya, Sujit' 'Ghosh, Subrata' 'Mehta, Sakshi' 'Mondal, Abhishake' _publ_section_title ; Effect of Ligand Modulation on Metal-to-Metal Electron Transfer in a Series of [Fe2Co2] Molecular Square Complexes ; _journal_name_full 'The Journal of Physical Chemistry A' _journal_paper_doi 10.1021/acs.jpca.1c02032 _journal_year 2021 _chemical_formula_moiety 'C72 H84 B2 Co2 Fe2 N34 O4, 2(B F4), 2(C3 H7 N O)' _chemical_formula_sum 'C78 H98 B4 Co2 F8 Fe2 N36 O6' _chemical_formula_weight 2060.72 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_date 2021-02-18 _audit_creation_method ; Olex2 1.3 (compiled 2020.07.31 svn.rc2a77460 for OlexSys, GUI svn.r6145) ; _cell_angle_alpha 88.755(3) _cell_angle_beta 70.514(3) _cell_angle_gamma 82.435(3) _cell_formula_units_Z 1 _cell_length_a 13.1307(6) _cell_length_b 13.1529(6) _cell_length_c 15.5247(7) _cell_measurement_reflns_used 9030 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 24.79 _cell_measurement_theta_min 2.46 _cell_volume 2504.9(2) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.992 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.1024 _diffrn_reflns_av_unetI/netI 0.0709 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.992 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 111720 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.992 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.592 _diffrn_reflns_theta_min 1.775 _diffrn_source 'sealed tube' _exptl_absorpt_coefficient_mu 0.691 _exptl_absorpt_correction_T_max 0.842 _exptl_absorpt_correction_T_min 0.731 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS _exptl_crystal_colour red _exptl_crystal_density_diffrn 1.366 _exptl_crystal_description parallelepiped _exptl_crystal_F_000 1064 _exptl_crystal_size_max 0.51 _exptl_crystal_size_mid 0.32 _exptl_crystal_size_min 0.27 _refine_diff_density_max 4.241 _refine_diff_density_min -1.004 _refine_diff_density_rms 0.166 _refine_ls_extinction_coef 0.0140(19) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.035 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 616 _refine_ls_number_reflns 15283 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.035 _refine_ls_R_factor_all 0.1357 _refine_ls_R_factor_gt 0.0908 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1693P)^2^+2.9263P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2418 _refine_ls_wR_factor_ref 0.2806 _reflns_Friedel_coverage 0.000 _reflns_number_gt 9589 _reflns_number_total 15283 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file jp1c02032_si_003.cif _cod_data_source_block Complex1_100K _cod_database_code 1562054 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All B(H) groups, All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: B1(H1) 2.b Me refined with riding coordinates: C35(H35A,H35B,H35C), C36(H36A,H36B,H36C), C27(H27A,H27B,H27C), C26(H26A,H26B, H26C), C12(H12A,H12B,H12C), C18(H18A,H18B,H18C), C17(H17A,H17B,H17C), C7(H7A, H7B,H7C), C8(H8A,H8B,H8C), C13(H13A,H13B,H13C) 2.c Aromatic/amide H refined with riding coordinates: C34(H34), C33(H33), C29(H29), C28(H28), C24(H24), C25(H25), C20(H20), C19(H19), C10(H10), C15(H15), C5(H5), C39(H39) 2.d Idealised Me refined as rotating group: C37(H37A,H37B,H37C), C38(H38A,H38B,H38C) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL Test_P-1_a.res in P-1 test_p-1_a.res created by SHELXL-2018/3 at 12:20:55 on 18-Feb-2021 CELL 0.71073 13.1307 13.1529 15.5247 88.755 70.514 82.435 ZERR 1 0.0006 0.0006 0.0007 0.003 0.003 0.003 LATT 1 SFAC C H B Co F Fe N O UNIT 78 98 4 2 8 2 36 6 L.S. 50 PLAN 7 TEMP 23 CONF MORE -1 BOND $H ABIN fmap 2 acta MERG 2 REM REM REM WGHT 0.169300 2.926300 EXTI 0.013966 FVAR 0.36124 CO1 4 0.706139 0.294349 0.496441 11.00000 0.01961 0.01863 = 0.02306 0.00085 -0.00944 -0.00615 FE1 6 0.412017 0.354407 0.353694 11.00000 0.01814 0.01801 = 0.03640 0.00280 -0.00873 -0.00588 F1 5 0.048834 0.234279 0.911022 11.00000 0.06962 0.10262 = 0.13573 0.03982 -0.02727 -0.05378 F2 5 0.222231 0.239376 0.893341 11.00000 0.06782 0.18289 = 0.06828 0.02178 -0.03311 -0.02176 F3 5 0.106523 0.384782 0.914370 11.00000 0.12599 0.05980 = 0.07876 -0.00164 0.00123 -0.01025 F4 5 0.159864 0.294506 0.782404 11.00000 0.09006 0.08277 = 0.06851 0.01085 -0.04078 -0.03087 N1 7 0.333466 0.562388 0.452211 11.00000 0.01875 0.02317 = 0.02666 0.00104 -0.00960 -0.00417 N2 7 0.250266 0.261674 0.517729 11.00000 0.03030 0.03267 = 0.04463 0.01007 -0.01133 -0.00877 N3 7 0.583844 0.313480 0.446160 11.00000 0.02047 0.01684 = 0.03230 -0.00014 -0.00838 -0.00301 O2 8 0.694973 0.338590 0.789585 11.00000 0.06082 0.08485 = 0.04045 -0.01668 -0.02037 -0.01684 O1 8 0.785047 0.173362 0.205594 11.00000 0.12677 0.05831 = 0.07594 -0.01839 -0.06137 -0.00272 N8 7 0.518472 0.414729 0.246826 11.00000 0.02068 0.01905 = 0.02830 0.00018 -0.00689 -0.00433 O3 8 0.989704 -0.123143 0.778584 11.00000 0.27454 0.10089 = 0.64020 0.04950 -0.38467 -0.03689 N16 7 0.604293 0.247779 0.616126 11.00000 0.01962 0.03414 = 0.02679 -0.00185 -0.00800 -0.00547 N17 7 0.516429 0.249286 0.764742 11.00000 0.03107 0.03350 = 0.02986 0.00116 -0.00641 -0.00260 N14 7 0.824651 0.272805 0.553083 11.00000 0.02439 0.03007 = 0.03733 -0.00523 -0.00606 -0.01100 N12 7 0.751125 0.151501 0.441038 11.00000 0.04417 0.02906 = 0.06195 0.01603 -0.03621 -0.01696 N10 7 0.803424 0.343149 0.375804 11.00000 0.04107 0.02509 = 0.04179 -0.00015 -0.02465 -0.00161 N6 7 0.464067 0.215971 0.289979 11.00000 0.02389 0.01990 = 0.03771 -0.00136 -0.01352 -0.00501 N7 7 0.476470 0.209968 0.199290 11.00000 0.02968 0.02324 = 0.03818 -0.00312 -0.01225 -0.00600 N9 7 0.526995 0.383670 0.160605 11.00000 0.02445 0.02631 = 0.02908 0.00123 -0.00538 -0.00718 N5 7 0.334887 0.352452 0.198540 11.00000 0.02388 0.02772 = 0.03080 0.00086 -0.00975 -0.00704 N4 7 0.301687 0.380411 0.289120 11.00000 0.01969 0.02326 = 0.03279 0.00138 -0.00891 -0.00655 N18 7 0.854368 -0.077049 0.686342 11.00000 0.31527 0.25219 = 0.06638 0.05919 -0.07853 -0.26632 C1 1 0.363730 0.483372 0.415388 11.00000 0.01787 0.02531 = 0.02752 0.00553 -0.00833 -0.00624 C2 1 0.310579 0.295739 0.456222 11.00000 0.02672 0.02219 = 0.03921 0.00406 -0.01487 -0.00585 C3 1 0.517621 0.329999 0.412180 11.00000 0.02021 0.01773 = 0.03224 0.00113 -0.00609 -0.00500 C34 1 0.503460 0.219586 0.630970 11.00000 0.02565 0.02028 = 0.03745 0.00011 -0.00910 -0.00524 AFIX 43 H34 2 0.475898 0.203036 0.585874 11.00000 -1.20000 AFIX 0 C33 1 0.449901 0.219717 0.722809 11.00000 0.02678 0.02393 = 0.04054 0.00328 -0.00558 -0.00126 AFIX 43 H33 2 0.380181 0.202542 0.751341 11.00000 -1.20000 AFIX 0 C32 1 0.609432 0.267475 0.698742 11.00000 0.02376 0.04794 = 0.02178 -0.00532 -0.00490 -0.00238 C31 1 0.703198 0.301980 0.716760 11.00000 0.03562 0.06001 = 0.03673 -0.00807 -0.01656 -0.00978 C30 1 0.809829 0.285967 0.641428 11.00000 0.02675 0.04444 = 0.04495 -0.01100 -0.01412 -0.00661 N15 7 0.907075 0.281112 0.654523 11.00000 0.03168 0.04160 = 0.07431 -0.00626 -0.02714 -0.01016 C35 1 0.927766 0.290704 0.740554 11.00000 0.06217 0.06775 = 0.10460 -0.01104 -0.05816 -0.01016 AFIX 33 H35A 2 1.004920 0.284033 0.728860 11.00000 -1.50000 H35B 2 0.894537 0.356622 0.768586 11.00000 -1.50000 H35C 2 0.897444 0.237763 0.780780 11.00000 -1.50000 AFIX 0 C29 1 0.985426 0.264392 0.571064 11.00000 0.02457 0.02827 = 0.09996 0.01323 -0.01670 -0.00414 AFIX 43 H29 2 1.060376 0.257118 0.558787 11.00000 -1.20000 AFIX 0 C28 1 0.934206 0.260379 0.509834 11.00000 0.02600 0.02714 = 0.06668 0.00036 0.00334 -0.00409 AFIX 43 H28 2 0.968533 0.250558 0.447129 11.00000 -1.20000 AFIX 0 C36 1 0.492183 0.255578 0.863471 11.00000 0.04813 0.05528 = 0.02723 0.00147 -0.00766 -0.00471 AFIX 33 H36A 2 0.552211 0.278511 0.876281 11.00000 -1.50000 H36B 2 0.427570 0.303244 0.890236 11.00000 -1.50000 H36C 2 0.480822 0.189116 0.888828 11.00000 -1.50000 AFIX 0 C23 1 0.773635 0.126841 0.355129 11.00000 0.07049 0.02574 = 0.07788 0.00233 -0.05221 -0.01263 N13 7 0.785443 0.023199 0.343719 11.00000 0.06546 0.02511 = 0.12633 -0.00512 -0.05943 -0.00461 C24 1 0.767408 -0.017303 0.426389 11.00000 0.03802 0.02916 = 0.13766 0.02565 -0.03912 -0.01073 AFIX 43 H24 2 0.770374 -0.086711 0.439613 11.00000 -1.20000 AFIX 0 C25 1 0.743894 0.062182 0.487528 11.00000 0.03609 0.04178 = 0.11611 0.04259 -0.04219 -0.01966 AFIX 43 H25 2 0.725898 0.056495 0.550513 11.00000 -1.20000 AFIX 0 C27 1 0.815708 -0.036555 0.257616 11.00000 0.08819 0.03952 = 0.16582 -0.02612 -0.06647 -0.00309 AFIX 33 H27A 2 0.824222 0.009395 0.207537 11.00000 -1.50000 H27B 2 0.883106 -0.080307 0.248799 11.00000 -1.50000 H27C 2 0.759513 -0.077680 0.260418 11.00000 -1.50000 AFIX 0 C22 1 0.791042 0.198264 0.278860 11.00000 0.08331 0.03694 = 0.06220 -0.00723 -0.04563 0.00300 C21 1 0.819023 0.300663 0.294143 11.00000 0.05543 0.03424 = 0.04491 0.00175 -0.02476 0.00231 N11 7 0.863464 0.363948 0.226542 11.00000 0.03557 0.04823 = 0.04695 0.00257 -0.01547 0.00671 C26 1 0.902006 0.343850 0.126683 11.00000 0.05393 0.07039 = 0.04683 -0.00673 -0.01357 0.01546 AFIX 33 H26A 2 0.929748 0.403406 0.095509 11.00000 -1.50000 H26B 2 0.958789 0.286576 0.111209 11.00000 -1.50000 H26C 2 0.842492 0.328524 0.108532 11.00000 -1.50000 AFIX 0 C20 1 0.875956 0.450169 0.266916 11.00000 0.01905 0.04980 = 0.05429 0.00708 -0.00487 -0.00599 AFIX 43 H20 2 0.905638 0.506886 0.236994 11.00000 -1.20000 AFIX 0 C19 1 0.837249 0.438349 0.358727 11.00000 0.02087 0.03092 = 0.04654 0.00218 -0.01208 -0.00101 AFIX 43 H19 2 0.834134 0.486614 0.402739 11.00000 -1.20000 AFIX 0 C9 1 0.493183 0.120067 0.314617 11.00000 0.03219 0.01846 = 0.05061 0.00305 -0.02474 -0.00653 C12 1 0.492363 0.091505 0.407637 11.00000 0.03891 0.02221 = 0.05787 0.00654 -0.02898 -0.00963 AFIX 33 H12A 2 0.516242 0.019383 0.408260 11.00000 -1.50000 H12B 2 0.540543 0.129511 0.424731 11.00000 -1.50000 H12C 2 0.419771 0.107110 0.450210 11.00000 -1.50000 AFIX 0 C10 1 0.523395 0.053914 0.238735 11.00000 0.05146 0.01870 = 0.05719 -0.00802 -0.02341 0.00009 AFIX 43 H10 2 0.546520 -0.016193 0.236868 11.00000 -1.20000 AFIX 0 C11 1 0.512288 0.112746 0.166993 11.00000 0.04766 0.02786 = 0.04823 -0.00784 -0.01991 -0.00601 B1 3 0.453236 0.307697 0.150200 11.00000 0.02662 0.02804 = 0.03386 -0.00092 -0.00885 -0.00909 AFIX 13 H1 2 0.466172 0.292877 0.085545 11.00000 -1.20000 AFIX 0 C16 1 0.607077 0.428023 0.098036 11.00000 0.02881 0.03221 = 0.03345 0.00544 -0.00872 -0.01126 C18 1 0.639133 0.406649 -0.002590 11.00000 0.04747 0.05322 = 0.03608 0.00055 -0.00351 -0.02302 AFIX 33 H18A 2 0.696895 0.445293 -0.034871 11.00000 -1.50000 H18B 2 0.663592 0.334754 -0.015134 11.00000 -1.50000 H18C 2 0.577447 0.426209 -0.022224 11.00000 -1.50000 AFIX 0 C15 1 0.648059 0.489954 0.145155 11.00000 0.02511 0.02849 = 0.03761 0.00497 -0.00719 -0.00941 AFIX 43 H15 2 0.702787 0.530894 0.119884 11.00000 -1.20000 AFIX 0 C14 1 0.592455 0.479856 0.237344 11.00000 0.01739 0.02018 = 0.03685 0.00273 -0.00810 -0.00480 C17 1 0.607254 0.531435 0.316055 11.00000 0.02302 0.02094 = 0.03824 0.00160 -0.00943 -0.00690 AFIX 33 H17A 2 0.664001 0.574229 0.293811 11.00000 -1.50000 H17B 2 0.540428 0.572756 0.350022 11.00000 -1.50000 H17C 2 0.626867 0.480550 0.355041 11.00000 -1.50000 AFIX 0 C6 1 0.250631 0.371978 0.166309 11.00000 0.03056 0.03468 = 0.03592 0.00358 -0.01574 -0.01186 C5 1 0.160395 0.414458 0.237538 11.00000 0.02499 0.03997 = 0.04142 0.00312 -0.01876 -0.01010 AFIX 43 H5 2 0.091035 0.436399 0.235349 11.00000 -1.20000 AFIX 0 C4 1 0.195050 0.417688 0.314078 11.00000 0.02005 0.02619 = 0.03643 0.00084 -0.01248 -0.00876 C7 1 0.126850 0.456911 0.407515 11.00000 0.01987 0.03279 = 0.03658 -0.00252 -0.00673 -0.00570 AFIX 33 H7A 2 0.053801 0.479277 0.408644 11.00000 -1.50000 H7B 2 0.126077 0.403200 0.450511 11.00000 -1.50000 H7C 2 0.156697 0.513547 0.423640 11.00000 -1.50000 AFIX 0 C8 1 0.258389 0.346227 0.071967 11.00000 0.04113 0.05891 = 0.04099 0.00036 -0.01952 -0.00992 AFIX 33 H8A 2 0.189245 0.366801 0.063999 11.00000 -1.50000 H8B 2 0.312853 0.381582 0.029533 11.00000 -1.50000 H8C 2 0.278109 0.273569 0.061072 11.00000 -1.50000 AFIX 0 C13 1 0.529614 0.080522 0.072470 11.00000 0.09004 0.04090 = 0.06116 -0.02480 -0.03026 0.00618 AFIX 33 H13A 2 0.555149 0.008387 0.064501 11.00000 -1.50000 H13B 2 0.462166 0.094231 0.060237 11.00000 -1.50000 H13C 2 0.582835 0.117919 0.030982 11.00000 -1.50000 AFIX 0 B2 3 0.133150 0.289588 0.876770 11.00000 0.04353 0.05093 = 0.05338 0.00649 -0.01616 -0.01785 C39 1 0.926232 -0.148404 0.742329 11.00000 0.21296 0.08074 = 0.08390 -0.00824 -0.03877 0.04111 AFIX 43 H39 2 0.916779 -0.217400 0.746679 11.00000 -1.20000 AFIX 0 C37 1 0.922919 -0.013340 0.634431 11.00000 0.04286 0.05627 = 0.07112 0.01856 -0.01179 -0.01315 AFIX 137 H37A 2 0.936436 -0.027693 0.570928 11.00000 -1.50000 H37B 2 0.990496 -0.023910 0.646667 11.00000 -1.50000 H37C 2 0.890245 0.056585 0.649031 11.00000 -1.50000 AFIX 0 C38 1 0.792364 -0.135318 0.677620 11.00000 0.11358 0.10281 = 0.10342 -0.01724 -0.00994 -0.07885 AFIX 137 H38A 2 0.719698 -0.099489 0.694314 11.00000 -1.50000 H38B 2 0.793477 -0.192864 0.716556 11.00000 -1.50000 H38C 2 0.815491 -0.159108 0.615179 11.00000 -1.50000 AFIX 0 HKLF 4 REM Test_P-1_a.res in P-1 REM wR2 = 0.2806, GooF = S = 1.035, Restrained GooF = 1.035 for all data REM R1 = 0.0908 for 9589 Fo > 4sig(Fo) and 0.1357 for all 15283 data REM 616 parameters refined using 0 restraints END WGHT 0.1697 2.8489 REM Highest difference peak 4.241, deepest hole -1.004, 1-sigma level 0.166 Q1 1 1.0007 0.2316 0.6487 11.00000 0.05 4.24 Q2 1 0.8767 0.1232 0.4975 11.00000 0.05 3.77 Q3 1 0.8409 -0.0709 0.3532 11.00000 0.05 2.68 Q4 1 0.8822 -0.1029 0.6907 11.00000 0.05 1.44 Q5 1 0.0859 0.2281 0.8019 11.00000 0.05 1.30 Q6 1 0.8760 0.1625 0.1886 11.00000 0.05 1.24 Q7 1 1.1130 0.2042 0.7119 11.00000 0.05 1.18 ; _shelx_res_checksum 82869 _shelx_hkl_file ; -2 0 0 305.37 18.70 2 0 0 296.87 18.60 -3 0 0 2159.18 127.69 3 0 0 2093.89 127.69 -4 0 0 309.57 19.70 -4 0 0 294.37 18.90 -4 0 0 303.67 19.60 -4 0 0 282.27 18.60 4 0 0 283.67 18.80 -5 0 0 149.88 12.10 -5 0 0 151.68 11.80 -5 0 0 149.88 10.60 -5 0 0 130.69 11.70 -5 0 0 156.58 10.50 5 0 0 167.18 11.10 5 0 0 152.28 11.20 -6 0 0 4.20 4.40 -6 0 0 2.40 2.70 -6 0 0 4.50 2.80 -6 0 0 5.20 4.40 -6 0 0 4.30 4.20 6 0 0 -5.50 3.10 6 0 0 -3.80 2.70 6 0 0 -0.80 3.10 -7 0 0 1.90 2.90 -7 0 0 -0.20 3.20 -7 0 0 6.30 4.70 -7 0 0 -1.60 2.90 -7 0 0 1.00 4.70 -7 0 0 -1.00 4.10 -7 0 0 1.70 3.20 7 0 0 8.10 3.30 7 0 0 1.00 3.10 7 0 0 6.00 3.50 7 0 0 4.40 3.30 -8 0 0 7.90 3.30 -8 0 0 3.60 5.00 -8 0 0 -4.10 2.80 -8 0 0 -11.00 4.20 -8 0 0 -7.10 2.70 -8 0 0 -1.60 4.40 8 0 0 -2.70 3.10 8 0 0 2.60 3.40 8 0 0 -0.80 3.30 8 0 0 -4.40 3.30 -9 0 0 190.28 17.30 -9 0 0 206.08 17.30 -9 0 0 216.78 17.70 9 0 0 205.68 15.50 9 0 0 208.48 16.50 9 0 0 212.48 15.10 9 0 0 220.88 15.70 -10 0 0 388.06 29.10 -10 0 0 415.86 29.40 -10 0 0 387.46 28.90 10 0 0 413.26 27.20 -11 0 0 68.39 11.50 -11 0 0 79.99 11.90 -11 0 0 80.39 12.30 11 0 0 84.29 9.90 -12 0 0 13.30 7.70 -12 0 0 16.40 8.30 -12 0 0 19.70 8.20 -13 0 0 9.30 7.80 -13 0 0 6.50 8.10 -13 0 0 3.70 7.20 13 0 0 -5.20 6.40 -14 0 0 0.60 8.70 -14 0 0 -9.80 7.90 -14 0 0 3.80 8.50 14 0 0 4.00 5.70 14 0 0 10.80 8.70 -15 0 0 -7.50 9.10 -15 0 0 3.60 9.30 -15 0 0 -6.70 7.80 15 0 0 8.90 9.10 -16 0 0 -8.70 9.40 -16 0 0 4.70 10.90 -16 0 0 -3.00 9.80 16 0 0 0.30 9.60 -17 0 0 95.89 16.80 -17 0 0 90.69 16.70 -17 0 0 85.49 16.50 17 0 0 69.89 15.40 17 -1 0 45.80 14.10 -17 1 0 36.90 13.30 -17 1 0 19.30 12.20 -17 1 0 23.30 12.50 16 -1 0 53.89 13.90 -16 1 0 54.39 15.70 -16 1 0 30.70 13.00 -16 1 0 22.10 11.10 15 -1 0 25.60 10.80 15 -1 0 25.20 7.40 -15 1 0 18.30 10.70 -15 1 0 8.50 10.40 -15 1 0 18.60 10.30 14 -1 0 16.50 7.10 14 -1 0 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77.39 8.90 -6 -1 0 79.59 7.60 -6 -1 0 88.59 9.20 -6 -1 0 77.69 7.20 -6 -1 0 71.19 7.40 -6 -1 0 81.99 8.70 6 1 0 91.79 8.70 6 1 0 71.29 7.00 6 1 0 86.89 7.20 -7 -1 0 93.09 10.00 -7 -1 0 95.99 10.40 -7 -1 0 91.29 10.20 -7 -1 0 78.59 7.90 -7 -1 0 84.29 7.90 -7 -1 0 90.69 8.10 -7 -1 0 89.29 8.90 7 1 0 96.29 9.00 7 1 0 101.19 7.80 7 1 0 107.29 10.10 7 1 0 107.19 8.30 -8 -1 0 117.19 9.60 -8 -1 0 81.19 8.80 -8 -1 0 102.39 9.20 -8 -1 0 118.39 12.30 -8 -1 0 110.09 11.70 -8 -1 0 117.19 12.50 -8 -1 0 108.69 9.00 8 1 0 103.89 8.90 8 1 0 119.29 9.20 8 1 0 111.89 9.10 8 1 0 106.09 9.90 -9 -1 0 6.60 5.40 -9 -1 0 17.10 4.70 -9 -1 0 15.30 6.60 -9 -1 0 20.70 6.50 -9 -1 0 17.00 4.40 -9 -1 0 21.80 4.80 9 1 0 10.10 4.20 9 1 0 17.40 6.60 9 1 0 10.30 4.90 -10 -1 0 320.97 23.90 -10 -1 0 291.87 23.90 -10 -1 0 328.77 24.20 10 1 0 325.57 24.10 10 1 0 321.77 22.70 10 1 0 308.97 21.70 -11 -1 0 337.07 25.80 -11 -1 0 338.87 26.10 -11 -1 0 312.97 25.50 11 1 0 353.06 26.00 -12 -1 0 9.00 7.70 -12 -1 0 -3.20 7.00 -12 -1 0 3.70 7.10 12 1 0 -0.50 6.90 -13 -1 0 19.90 9.60 -13 -1 0 1.60 7.80 -13 -1 0 8.20 8.00 13 1 0 7.30 7.70 -14 -1 0 21.10 9.80 -14 -1 0 16.00 10.00 -14 -1 0 14.50 9.60 14 1 0 16.40 9.30 -15 -1 0 2.90 9.30 -15 -1 0 12.40 9.70 -15 -1 0 -11.00 8.20 15 1 0 3.70 9.10 -16 -1 0 4.60 10.00 -16 -1 0 -6.70 9.00 -16 -1 0 -4.90 8.90 16 1 0 7.30 9.80 16 1 0 13.10 9.90 -17 -1 0 12.50 11.20 -17 -1 0 -1.50 10.20 -17 -1 0 -6.40 10.20 17 1 0 17.70 10.80 17 1 0 2.00 10.00 17 -2 0 23.90 12.20 17 -2 0 9.30 8.90 -17 2 0 1.70 11.60 -17 2 0 9.60 12.40 -17 2 0 -0.10 10.60 16 -2 0 -1.40 9.50 16 -2 0 11.30 8.10 -16 2 0 -24.80 8.00 -16 2 0 1.20 9.90 -16 2 0 -2.90 10.80 15 -2 0 13.80 7.30 15 -2 0 12.80 9.80 -15 2 0 5.90 9.10 -15 2 0 20.00 10.80 -15 2 0 16.60 10.20 14 -2 0 14.60 6.50 -14 2 0 10.30 10.00 -14 2 0 9.10 9.20 -14 2 0 -3.90 9.20 13 -2 0 85.09 15.70 13 -2 0 101.29 11.20 -13 2 0 94.79 14.80 -13 2 0 86.99 14.20 -13 2 0 72.29 13.70 12 -2 0 21.80 9.90 12 -2 0 9.70 6.00 12 -2 0 14.90 6.40 -12 2 0 1.70 8.00 -12 2 0 6.00 8.60 -12 2 0 10.40 8.70 11 -2 0 112.19 11.50 11 -2 0 129.99 12.80 -11 2 0 70.09 12.70 -11 2 0 95.39 13.80 -11 2 0 110.09 14.70 10 -2 0 578.24 37.80 10 -2 0 582.14 38.50 -10 2 0 596.84 40.30 -10 2 0 587.24 40.40 -10 2 0 581.64 40.10 9 -2 0 92.69 10.30 9 -2 0 98.89 9.90 9 -2 0 96.89 9.90 -9 2 0 76.09 10.90 8 -2 0 53.49 7.20 8 -2 0 35.20 5.60 8 -2 0 48.20 6.20 -8 2 0 38.20 7.40 -8 2 0 34.90 7.80 -8 2 0 38.20 7.50 7 -2 0 61.89 5.90 7 -2 0 67.89 8.10 7 -2 0 76.29 8.10 7 -2 0 69.69 7.60 7 -2 0 77.19 7.80 -7 2 0 78.99 9.60 -7 2 0 69.89 6.80 -7 2 0 57.29 8.80 -7 2 0 52.39 8.60 6 -2 0 30.30 5.80 6 -2 0 41.20 5.40 6 -2 0 39.90 5.80 6 -2 0 51.19 6.00 -6 2 0 44.40 4.90 -6 2 0 38.10 6.50 -6 2 0 31.50 6.60 -6 2 0 36.00 6.90 5 -2 0 10.10 4.20 5 -2 0 5.70 3.70 5 -2 0 8.30 3.30 -5 2 0 9.30 4.90 -5 2 0 7.20 3.10 -5 2 0 14.10 4.70 -5 2 0 8.60 4.50 4 -2 0 100.99 9.00 4 -2 0 81.69 7.90 4 -2 0 73.89 7.50 -4 2 0 89.39 8.30 -4 2 0 84.49 6.90 -4 2 0 74.89 8.10 -4 2 0 101.59 9.30 3 -2 0 144.19 10.80 3 -2 0 137.99 10.60 -3 2 0 136.99 11.10 -3 2 0 149.99 10.10 -3 2 0 149.09 10.10 -3 2 0 156.78 11.20 2 -2 0 -1.50 2.90 2 -2 0 -1.00 3.50 2 -2 0 -1.40 3.30 -2 2 0 0.30 2.40 1 -2 0 6.60 3.50 1 -2 0 5.90 2.60 1 -2 0 7.10 3.10 -1 2 0 7.20 3.10 -1 2 0 9.40 2.70 0 -2 0 2096.79 114.19 0 -2 0 1785.42 114.19 0 2 0 1831.72 114.19 -1 -2 0 176.98 11.80 1 2 0 195.68 12.10 1 2 0 167.68 12.50 -2 -2 0 500.05 30.60 2 2 0 498.65 30.60 2 2 0 491.15 30.30 2 2 0 482.25 30.40 -3 -2 0 129.89 9.20 -3 -2 0 125.19 9.20 -3 -2 0 115.29 7.70 -3 -2 0 103.49 8.80 3 2 0 104.29 8.60 3 2 0 127.69 9.10 3 2 0 87.19 8.20 3 2 0 124.59 9.30 -4 -2 0 1801.02 111.99 -4 -2 0 1918.41 111.89 -4 -2 0 1788.92 112.09 -4 -2 0 1877.91 111.09 -4 -2 0 1837.92 111.89 -4 -2 0 1869.91 111.79 4 2 0 1783.52 111.59 4 2 0 1955.60 111.99 4 2 0 1811.52 112.19 -5 -2 0 421.06 26.10 -5 -2 0 365.56 25.30 -5 -2 0 407.56 25.70 -5 -2 0 389.56 24.60 -5 -2 0 423.66 25.70 5 2 0 394.56 25.10 5 2 0 320.87 25.60 5 2 0 420.56 25.80 -6 -2 0 97.19 9.50 -6 -2 0 79.59 8.40 -6 -2 0 58.19 7.50 -6 -2 0 78.69 8.80 -6 -2 0 72.39 8.40 -6 -2 0 67.59 6.80 6 2 0 73.99 8.50 6 2 0 68.69 7.30 6 2 0 61.99 8.30 -7 -2 0 924.11 58.39 -7 -2 0 954.40 57.19 -7 -2 0 901.31 58.69 -7 -2 0 881.11 57.79 -7 -2 0 973.70 57.89 -7 -2 0 945.31 57.29 -7 -2 0 884.21 58.29 7 2 0 942.81 57.49 7 2 0 994.10 57.19 7 2 0 915.41 58.39 7 2 0 913.91 58.49 -8 -2 0 397.16 27.00 -8 -2 0 414.26 26.80 -8 -2 0 411.26 25.90 -8 -2 0 410.76 27.70 -8 -2 0 401.46 27.60 -8 -2 0 416.56 28.00 8 2 0 387.16 26.30 8 2 0 346.17 27.00 8 2 0 414.76 26.10 8 2 0 419.06 27.70 -9 -2 0 80.99 9.20 -9 -2 0 67.69 9.10 -9 -2 0 97.09 11.50 -9 -2 0 79.09 10.90 -9 -2 0 57.99 9.70 9 2 0 86.49 11.10 9 2 0 78.89 9.90 9 2 0 72.29 8.40 9 2 0 85.59 8.60 -10 -2 0 1.10 4.80 -10 -2 0 -6.20 5.50 -10 -2 0 0.40 6.10 -10 -2 0 -0.90 4.10 -10 -2 0 -12.70 5.50 10 2 0 -0.10 5.00 10 2 0 3.30 5.70 -11 -2 0 87.09 12.40 -11 -2 0 73.19 11.70 -11 -2 0 66.79 11.80 11 2 0 98.59 13.00 11 2 0 107.19 11.70 -12 -2 0 21.10 8.80 -12 -2 0 26.40 8.70 -12 -2 0 9.50 7.60 12 2 0 17.80 8.40 -13 -2 0 -7.00 6.40 -13 -2 0 -3.50 7.30 -13 -2 0 0.30 7.70 13 2 0 6.10 7.60 -14 -2 0 51.99 11.90 -14 -2 0 29.30 10.30 -14 -2 0 24.80 10.00 14 2 0 27.90 10.60 14 2 0 18.80 9.70 -15 -2 0 10.70 10.20 -15 -2 0 6.80 9.60 -15 -2 0 0.10 9.60 15 2 0 12.60 8.90 15 2 0 -9.80 7.80 -16 -2 0 8.80 10.60 -16 -2 0 -15.20 8.80 -16 -2 0 11.50 10.60 16 2 0 -4.90 8.70 16 2 0 6.50 9.60 -17 -2 0 9.40 10.90 -17 -2 0 -9.50 9.60 17 2 0 15.00 10.70 17 2 0 -1.60 9.40 16 -3 0 21.80 9.00 16 -3 0 15.90 11.30 -16 3 0 18.00 11.20 -16 3 0 24.10 11.90 -16 3 0 27.60 13.40 15 -3 0 11.30 8.10 -15 3 0 -0.10 9.70 -15 3 0 9.40 10.70 -15 3 0 -10.20 9.40 14 -3 0 6.20 7.20 -14 3 0 9.40 9.70 -14 3 0 -2.60 8.20 -14 3 0 7.10 9.60 13 -3 0 13.50 7.00 13 -3 0 -5.10 5.70 -13 3 0 2.10 9.00 -13 3 0 6.90 9.20 -13 3 0 -1.30 7.80 12 -3 0 19.90 9.70 12 -3 0 11.20 6.90 12 -3 0 12.40 6.30 -12 3 0 0.60 7.80 -12 3 0 22.60 9.40 -12 3 0 7.90 8.20 11 -3 0 1.70 5.70 11 -3 0 7.40 8.50 11 -3 0 2.40 5.60 -11 3 0 11.90 7.90 -11 3 0 -4.60 6.80 -11 3 0 6.80 7.60 10 -3 0 90.29 13.50 10 -3 0 135.49 13.00 10 -3 0 107.19 10.80 -10 3 0 84.39 12.60 -10 3 0 113.19 14.20 -10 3 0 67.39 11.70 9 -3 0 754.62 49.00 9 -3 0 750.12 49.00 9 -3 0 815.52 49.90 9 -3 0 800.22 51.99 -9 3 0 738.43 50.69 -9 3 0 751.32 50.79 -9 3 0 826.22 51.59 8 -3 0 -1.20 3.60 8 -3 0 -2.90 5.40 8 -3 0 0.70 4.20 8 -3 0 8.70 5.00 -8 3 0 -0.20 5.20 -8 3 0 7.30 5.30 -8 3 0 7.20 5.50 7 -3 0 237.48 17.40 7 -3 0 259.17 17.80 7 -3 0 244.08 19.80 7 -3 0 251.57 18.10 -7 3 0 233.88 18.90 -7 3 0 236.88 18.70 -7 3 0 265.57 19.10 -7 3 0 249.78 16.70 6 -3 0 13.20 4.50 6 -3 0 1.50 5.20 6 -3 0 14.80 4.50 6 -3 0 12.60 4.00 -6 3 0 6.10 3.50 -6 3 0 17.30 5.50 -6 3 0 18.80 5.80 -6 3 0 8.60 5.10 5 -3 0 259.77 17.80 5 -3 0 246.38 18.10 5 -3 0 262.17 19.40 5 -3 0 254.57 18.00 -5 3 0 252.97 18.90 -5 3 0 268.77 17.20 -5 3 0 263.67 18.60 -5 3 0 267.97 18.60 4 -3 0 154.18 11.60 4 -3 0 155.28 11.40 4 -3 0 154.48 11.60 -4 3 0 144.19 10.60 -4 3 0 157.88 12.00 -4 3 0 158.48 12.10 -4 3 0 137.09 10.50 -4 3 0 136.99 10.50 -4 3 0 144.49 11.70 3 -3 0 88.69 8.50 3 -3 0 84.99 8.30 3 -3 0 76.69 9.00 3 -3 0 82.69 8.50 -3 3 0 88.39 8.70 -3 3 0 86.29 9.40 -3 3 0 117.59 8.40 -3 3 0 96.79 7.40 2 -3 0 219.98 15.20 2 -3 0 195.18 14.60 2 -3 0 193.48 15.10 -2 3 0 244.98 14.90 -2 3 0 226.38 14.60 1 -3 0 140.79 9.90 1 -3 0 126.09 9.80 1 -3 0 132.39 9.60 1 -3 0 127.89 10.50 1 -3 0 128.09 9.30 -1 3 0 120.49 9.90 -1 3 0 130.29 9.60 -1 3 0 145.39 9.70 -1 3 0 127.59 10.00 0 -3 0 2174.58 136.49 0 -3 0 2330.77 136.49 0 -3 0 2229.18 136.29 0 3 0 2322.07 136.49 0 3 0 2269.37 136.49 0 3 0 2301.97 136.69 -1 -3 0 147.49 11.80 -1 -3 0 180.98 12.40 -1 -3 0 189.58 11.70 -1 -3 0 184.98 11.60 1 3 0 192.78 13.00 1 3 0 168.88 12.90 1 3 0 196.48 11.80 1 3 0 154.38 12.30 1 3 0 159.08 12.30 -2 -3 0 758.82 43.70 -2 -3 0 690.53 44.10 -2 -3 0 769.82 43.20 -2 -3 0 666.43 43.90 -2 -3 0 652.53 43.40 2 3 0 699.03 44.00 2 3 0 710.73 44.30 2 3 0 799.52 43.60 2 3 0 661.23 43.80 2 3 0 705.53 44.10 -3 -3 0 2.40 3.90 -3 -3 0 8.00 2.20 -3 -3 0 11.00 3.80 -3 -3 0 6.40 4.00 3 3 0 11.00 3.10 3 3 0 7.80 4.00 3 3 0 -2.80 3.80 -4 -3 0 154.38 12.20 -4 -3 0 142.89 11.90 -4 -3 0 159.08 12.10 -4 -3 0 166.08 11.90 -4 -3 0 155.48 10.40 4 3 0 147.89 12.40 4 3 0 164.18 11.90 4 3 0 144.59 11.00 4 3 0 183.58 11.90 -5 -3 0 -1.70 3.90 -5 -3 0 1.60 4.10 -5 -3 0 4.40 3.80 -5 -3 0 -4.60 3.90 5 3 0 1.80 3.80 5 3 0 -2.40 4.40 5 3 0 0.90 3.50 5 3 0 -2.40 3.40 -6 -3 0 185.08 12.60 -6 -3 0 161.28 12.90 -6 -3 0 141.29 12.10 -6 -3 0 151.08 10.80 -6 -3 0 153.78 12.60 6 3 0 165.58 12.60 6 3 0 140.29 11.60 6 3 0 163.38 12.50 6 3 0 142.79 13.10 6 3 0 148.19 11.10 -7 -3 0 641.34 41.00 -7 -3 0 588.34 39.70 -7 -3 0 609.74 41.10 -7 -3 0 673.83 41.40 -7 -3 0 690.03 42.10 -7 -3 0 611.14 39.80 -7 -3 0 668.93 41.30 7 3 0 661.83 41.80 7 3 0 704.33 41.60 7 3 0 690.73 41.50 7 3 0 607.64 39.70 7 3 0 618.64 40.50 -8 -3 0 1377.96 87.99 -8 -3 0 1488.85 88.09 -8 -3 0 1503.35 89.29 -8 -3 0 1415.76 90.19 -8 -3 0 1477.35 89.39 -8 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8 4 0 3.50 4.00 8 4 0 -3.80 3.60 8 4 0 12.20 5.20 8 4 0 6.50 5.00 -9 -4 0 181.08 14.50 -9 -4 0 164.58 14.70 -9 -4 0 158.78 15.30 -9 -4 0 194.08 15.20 9 4 0 177.58 15.00 9 4 0 164.28 13.00 9 4 0 188.28 15.70 9 4 0 171.18 14.00 9 4 0 143.29 14.80 -10 -4 0 139.19 16.30 -10 -4 0 146.29 15.10 -10 -4 0 163.68 14.90 -10 -4 0 163.28 13.90 10 4 0 143.49 13.30 10 4 0 183.98 15.60 10 4 0 141.49 12.70 10 4 0 164.48 14.80 10 4 0 148.59 16.00 -11 -4 0 426.26 31.40 -11 -4 0 433.16 32.40 -11 -4 0 438.86 30.90 -11 -4 0 463.45 30.80 11 4 0 423.66 31.50 11 4 0 445.46 31.80 11 4 0 443.76 31.50 -12 -4 0 47.20 9.40 -12 -4 0 42.70 10.20 -12 -4 0 40.40 9.40 12 4 0 31.70 9.10 12 4 0 54.09 10.20 12 4 0 56.29 10.50 -13 -4 0 3.10 7.30 -13 -4 0 -9.70 6.70 13 4 0 -2.10 7.20 13 4 0 -1.80 7.40 13 4 0 -1.70 6.70 -14 -4 0 14.90 9.20 14 4 0 41.60 11.00 14 4 0 37.60 10.70 -15 -4 0 9.70 9.40 15 4 0 1.30 8.30 15 4 0 -5.50 8.30 -16 -4 0 7.40 10.40 16 4 0 -5.30 8.70 16 4 0 7.00 9.80 -17 -4 0 3.30 10.90 17 4 0 3.40 10.10 17 4 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9.00 7 -5 0 59.89 8.90 7 -5 0 64.29 10.20 7 -5 0 67.19 8.60 7 -5 0 41.80 8.00 -7 5 0 46.10 8.70 -7 5 0 49.80 6.80 -7 5 0 57.79 9.30 -7 5 0 52.19 8.80 6 -5 0 10.30 5.30 6 -5 0 12.40 5.80 6 -5 0 9.70 5.00 6 -5 0 11.80 5.30 -6 5 0 20.50 6.00 -6 5 0 8.40 5.40 -6 5 0 11.40 4.50 -6 5 0 1.90 5.40 -6 5 0 17.80 6.40 5 -5 0 103.89 10.50 5 -5 0 111.99 11.00 5 -5 0 102.39 11.60 5 -5 0 91.09 7.60 5 -5 0 117.99 10.70 -5 5 0 89.29 8.50 -5 5 0 113.79 11.70 -5 5 0 113.39 11.60 -5 5 0 90.49 8.80 -5 5 0 111.39 11.20 -5 5 0 86.89 8.60 4 -5 0 16.80 5.20 4 -5 0 11.10 4.90 4 -5 0 2.20 4.10 4 -5 0 8.70 4.20 4 -5 0 13.70 5.60 4 -5 0 8.20 3.10 -4 5 0 12.10 4.90 -4 5 0 6.50 3.70 -4 5 0 8.60 4.70 -4 5 0 2.40 4.50 -4 5 0 9.60 3.70 3 -5 0 1094.49 64.29 3 -5 0 989.60 63.49 3 -5 0 977.80 62.89 3 -5 0 957.30 63.79 3 -5 0 1108.39 64.09 3 -5 0 1043.50 64.39 -3 5 0 1153.58 62.59 -3 5 0 973.80 63.99 -3 5 0 876.51 63.69 -3 5 0 1059.59 63.49 -3 5 0 1113.09 63.99 2 -5 0 1616.54 94.89 2 -5 0 1533.95 95.19 2 -5 0 1603.24 94.59 2 -5 0 1548.25 95.39 2 -5 0 1527.55 94.99 2 -5 0 1629.54 95.39 -2 5 0 1543.55 95.09 -2 5 0 1555.04 94.09 -2 5 0 1533.65 95.09 -2 5 0 1540.35 94.99 -2 5 0 1517.85 94.79 -2 5 0 1563.24 94.99 1 -5 0 33.40 5.60 1 -5 0 35.60 5.80 1 -5 0 36.20 5.90 1 -5 0 41.10 5.80 1 -5 0 57.19 6.90 1 -5 0 41.70 5.80 -1 5 0 34.90 6.30 -1 5 0 38.30 5.80 -1 5 0 50.79 5.50 -1 5 0 46.00 6.00 -1 5 0 44.30 6.40 -1 5 0 37.20 6.20 -1 5 0 45.60 5.40 -1 5 0 38.80 6.00 0 -5 0 495.05 30.60 0 -5 0 496.85 31.10 0 -5 0 470.65 30.20 0 -5 0 463.15 29.90 0 -5 0 451.25 30.20 0 -5 0 466.85 30.50 0 -5 0 467.65 30.40 0 5 0 492.55 31.10 0 5 0 501.35 30.40 0 5 0 488.45 30.60 0 5 0 452.15 30.70 0 5 0 488.25 30.60 -1 -5 0 74.59 7.10 -1 -5 0 92.89 8.50 -1 -5 0 98.79 8.30 -1 -5 0 99.49 7.40 -1 -5 0 86.29 8.10 -1 -5 0 84.49 8.50 -1 -5 0 112.29 7.90 1 5 0 84.29 8.50 1 5 0 83.19 8.30 1 5 0 82.99 8.20 1 5 0 77.49 8.90 1 5 0 59.99 8.10 -2 -5 0 143.99 11.20 -2 -5 0 146.99 11.30 -2 -5 0 149.69 10.70 -2 -5 0 153.88 11.70 -2 -5 0 142.39 12.20 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14.70 4.80 6 5 0 4.90 5.40 -7 -5 0 544.95 35.10 -7 -5 0 568.94 36.60 -7 -5 0 519.35 36.60 -7 -5 0 555.64 36.10 -7 -5 0 554.24 34.20 -7 -5 0 568.54 36.80 7 5 0 544.15 36.30 7 5 0 549.05 35.20 7 5 0 571.04 36.20 7 5 0 576.04 37.40 7 5 0 533.55 36.00 -8 -5 0 334.37 22.00 -8 -5 0 337.07 23.70 -8 -5 0 342.97 23.90 -8 -5 0 324.07 24.00 8 5 0 331.27 24.50 8 5 0 313.87 22.10 8 5 0 337.57 23.50 8 5 0 286.27 22.70 8 5 0 340.97 23.70 -9 -5 0 11.20 6.00 -9 -5 0 9.30 6.30 -9 -5 0 6.80 5.80 9 5 0 8.80 6.10 9 5 0 8.40 5.30 9 5 0 -6.00 4.90 9 5 0 -11.00 5.10 9 5 0 -1.20 4.20 -10 -5 0 109.89 12.80 -10 -5 0 113.89 13.20 -10 -5 0 97.69 13.50 10 5 0 93.29 12.70 10 5 0 94.09 12.80 10 5 0 89.39 11.40 10 5 0 92.09 12.40 10 5 0 122.99 10.60 -11 -5 0 19.90 7.90 -11 -5 0 12.80 7.10 -11 -5 0 14.90 6.80 11 5 0 18.70 7.90 11 5 0 9.70 7.30 11 5 0 20.80 6.10 11 5 0 10.40 7.20 -12 -5 0 11.50 7.00 -12 -5 0 13.50 7.00 -12 -5 0 4.30 7.80 12 5 0 9.30 7.20 12 5 0 9.30 5.20 12 5 0 8.30 6.70 12 5 0 13.90 7.70 -13 -5 0 70.89 12.90 13 5 0 87.59 13.60 13 5 0 57.19 11.90 13 5 0 54.09 11.30 -14 -5 0 88.59 15.30 14 5 0 117.59 16.20 14 5 0 120.49 16.40 14 5 0 119.49 16.70 -15 -5 0 93.29 15.80 15 5 0 105.19 16.00 15 5 0 104.49 15.80 -16 -5 0 3.90 10.60 16 5 0 -4.90 9.50 16 5 0 -2.30 8.80 -17 -5 0 14.60 12.30 17 5 0 13.30 11.10 17 5 0 11.30 10.20 15 -6 0 24.20 9.20 -15 6 0 12.90 12.00 -15 6 0 1.50 10.30 -15 6 0 5.50 11.70 14 -6 0 15.40 9.40 14 -6 0 -2.10 7.60 -14 6 0 -3.40 9.40 -14 6 0 9.80 10.30 -14 6 0 -5.50 9.30 13 -6 0 10.20 8.40 13 -6 0 -6.80 6.70 -13 6 0 -2.60 8.70 -13 6 0 -6.00 8.40 -13 6 0 -2.60 9.50 12 -6 0 8.60 6.70 12 -6 0 7.30 8.00 -12 6 0 7.60 9.00 -12 6 0 -8.50 7.40 -12 6 0 9.60 8.90 11 -6 0 1.40 6.10 11 -6 0 -0.50 7.80 11 -6 0 -2.70 7.20 -11 6 0 -12.60 6.20 -11 6 0 -2.10 8.00 -11 6 0 1.00 7.60 10 -6 0 3.40 7.30 10 -6 0 6.20 6.40 10 -6 0 -0.50 5.70 10 -6 0 -9.10 6.70 -10 6 0 5.00 7.60 -10 6 0 -6.90 6.40 -10 6 0 -1.90 7.40 9 -6 0 60.09 10.30 9 -6 0 81.69 12.90 9 -6 0 95.99 11.00 9 -6 0 77.39 11.30 -9 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11 0 38.40 11.50 -8 11 0 36.30 10.70 7 -11 0 61.19 11.20 7 -11 0 41.20 10.00 7 -11 0 37.00 10.60 7 -11 0 34.90 10.50 -7 11 0 35.80 8.60 -7 11 0 31.40 10.50 -7 11 0 30.00 10.00 -7 11 0 40.30 11.20 6 -11 0 15.20 8.10 6 -11 0 33.70 10.40 6 -11 0 23.60 8.50 6 -11 0 54.49 10.10 -6 11 0 25.10 7.80 -6 11 0 50.49 10.60 -6 11 0 44.60 10.30 -6 11 0 24.90 9.20 5 -11 0 18.50 8.90 5 -11 0 3.80 7.00 5 -11 0 12.70 6.30 5 -11 0 1.00 6.70 5 -11 0 0.50 6.20 -5 11 0 -1.10 7.40 -5 11 0 3.70 6.50 -5 11 0 7.50 7.60 -5 11 0 -6.20 5.90 -5 11 0 9.20 8.10 4 -11 0 71.19 11.80 4 -11 0 91.99 11.10 4 -11 0 82.79 12.70 4 -11 0 89.19 12.10 -4 11 0 88.69 12.10 -4 11 0 85.09 12.20 -4 11 0 86.29 12.20 -4 11 0 93.09 9.20 -4 11 0 92.99 12.60 -4 11 0 82.09 11.20 3 -11 0 104.29 13.70 3 -11 0 90.39 12.40 3 -11 0 92.49 10.90 3 -11 0 84.79 12.50 3 -11 0 98.59 12.60 -3 11 0 79.09 12.40 -3 11 0 92.49 9.80 -3 11 0 102.49 13.00 -3 11 0 89.09 12.00 -3 11 0 108.39 13.20 -3 11 0 71.79 11.90 2 -11 0 25.90 7.80 2 -11 0 9.50 6.80 2 -11 0 13.00 5.90 2 -11 0 31.10 7.30 2 -11 0 15.10 7.40 -2 11 0 4.50 6.30 -2 11 0 12.20 6.90 -2 11 0 6.90 5.30 -2 11 0 15.30 6.50 -2 11 0 7.90 6.80 -2 11 0 7.80 6.10 1 -11 0 5.10 5.20 1 -11 0 0.80 5.10 1 -11 0 12.90 7.00 1 -11 0 0.70 5.80 1 -11 0 16.50 7.00 1 -11 0 -8.00 5.20 1 -11 0 9.00 5.90 -1 11 0 9.60 6.50 -1 11 0 10.70 6.50 -1 11 0 4.90 5.90 -1 11 0 8.70 6.20 -1 11 0 -2.90 6.30 -1 11 0 7.70 5.20 0 -11 0 37.20 8.00 0 -11 0 43.60 8.10 0 -11 0 36.10 8.20 0 -11 0 47.60 9.20 0 -11 0 37.90 6.70 0 -11 0 24.90 7.50 0 -11 0 45.90 8.50 0 11 0 51.39 8.30 0 11 0 27.80 7.60 0 11 0 35.10 7.70 0 11 0 39.70 9.30 0 11 0 23.30 7.20 0 11 0 45.60 9.60 0 11 0 27.00 6.60 -1 -11 0 89.49 12.00 -1 -11 0 86.59 11.40 -1 -11 0 106.89 11.70 -1 -11 0 83.59 10.70 -1 -11 0 102.09 12.70 -1 -11 0 85.09 9.70 -1 -11 0 102.29 12.00 1 11 0 63.39 11.30 1 11 0 75.29 11.20 1 11 0 111.49 13.30 1 11 0 100.39 13.00 1 11 0 92.69 10.70 1 11 0 81.19 11.10 1 11 0 103.99 11.10 1 11 0 112.49 14.60 -2 -11 0 61.99 10.30 -2 -11 0 71.89 10.60 -2 -11 0 67.69 9.60 -2 -11 0 76.59 8.20 -2 -11 0 72.09 10.70 -2 -11 0 65.19 9.30 -2 -11 0 65.49 9.80 2 11 0 80.29 11.30 2 11 0 69.69 11.60 2 11 0 72.49 9.50 2 11 0 78.29 10.40 2 11 0 49.30 9.80 2 11 0 73.39 9.40 -3 -11 0 0.10 5.60 -3 -11 0 5.10 6.50 -3 -11 0 9.50 7.00 -3 -11 0 9.70 5.50 -3 -11 0 -9.20 5.10 3 11 0 6.80 5.70 3 11 0 8.30 5.70 3 11 0 9.90 7.60 3 11 0 4.40 6.30 3 11 0 8.60 6.50 3 11 0 0.60 5.00 3 11 0 13.20 7.20 -4 -11 0 38.70 8.60 -4 -11 0 49.90 10.20 -4 -11 0 60.79 10.80 -4 -11 0 55.09 8.60 4 11 0 58.59 9.30 4 11 0 55.49 10.40 4 11 0 60.89 10.50 4 11 0 56.19 8.60 4 11 0 46.20 9.50 4 11 0 28.00 8.70 4 11 0 38.00 7.50 -5 -11 0 22.20 6.40 -5 -11 0 28.00 8.40 -5 -11 0 15.00 8.30 -5 -11 0 20.70 7.40 5 11 0 23.50 8.00 5 11 0 21.60 8.10 5 11 0 33.40 8.40 5 11 0 26.30 8.80 5 11 0 23.10 6.70 -6 -11 0 130.59 15.50 -6 -11 0 126.09 13.50 -6 -11 0 120.19 15.70 -6 -11 0 126.59 11.80 6 11 0 118.99 13.20 6 11 0 99.89 13.80 6 11 0 101.39 14.00 6 11 0 96.69 14.30 6 11 0 85.49 13.30 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0 17.60 11.00 -14 -11 0 1.50 10.00 -14 -11 0 9.60 10.20 14 11 0 13.50 8.50 14 11 0 5.20 10.90 14 11 0 12.30 10.00 -15 -11 0 83.89 16.50 -15 -11 0 54.89 14.60 -15 -11 0 73.29 15.50 15 11 0 54.29 12.30 15 11 0 64.69 15.80 15 11 0 41.70 14.00 12 -12 0 10.50 11.00 -12 12 0 -3.30 10.50 11 -12 0 0.60 9.00 11 -12 0 5.70 9.80 11 -12 0 8.00 10.00 -11 12 0 8.20 10.40 -11 12 0 23.00 11.80 -11 12 0 15.40 12.00 10 -12 0 0.50 9.50 10 -12 0 1.70 8.90 10 -12 0 4.60 8.50 -10 12 0 8.10 11.10 -10 12 0 -5.90 10.20 -10 12 0 12.50 11.50 9 -12 0 -4.20 7.90 9 -12 0 7.70 9.70 9 -12 0 10.10 8.70 -9 12 0 4.80 9.20 -9 12 0 16.80 10.80 -9 12 0 14.10 10.50 8 -12 0 62.39 11.90 8 -12 0 94.69 15.70 8 -12 0 75.69 12.60 -8 12 0 39.60 11.80 -8 12 0 66.59 10.40 -8 12 0 57.29 13.00 -8 12 0 80.79 14.20 7 -12 0 152.88 17.60 7 -12 0 135.89 18.20 7 -12 0 120.09 16.70 7 -12 0 149.79 17.70 -7 12 0 147.19 18.10 -7 12 0 134.59 15.40 -7 12 0 141.59 18.70 -7 12 0 149.49 18.30 6 -12 0 7.70 7.60 6 -12 0 4.00 8.10 6 -12 0 14.70 7.80 6 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0 -0.60 6.00 -1 12 0 -6.50 5.50 -1 12 0 3.50 6.40 -1 12 0 -16.20 4.90 -1 12 0 -0.80 6.70 -1 12 0 13.70 5.70 -1 12 0 3.80 6.80 0 -12 0 132.79 12.30 0 -12 0 134.79 14.90 0 -12 0 127.59 14.10 0 -12 0 138.19 14.50 0 -12 0 144.89 16.20 0 -12 0 130.59 14.60 0 12 0 136.49 15.30 0 12 0 106.99 13.90 0 12 0 102.89 12.30 0 12 0 125.69 13.60 0 12 0 127.89 14.30 0 12 0 113.09 14.80 -1 -12 0 -1.70 5.50 -1 -12 0 9.80 5.60 -1 -12 0 7.60 6.60 -1 -12 0 1.90 6.60 -1 -12 0 3.50 6.30 -1 -12 0 9.20 6.50 1 12 0 1.80 6.40 1 12 0 -0.90 6.80 1 12 0 -3.20 5.40 1 12 0 5.20 6.50 1 12 0 -2.80 5.00 -2 -12 0 360.26 26.70 -2 -12 0 340.37 26.60 -2 -12 0 354.16 25.80 -2 -12 0 365.96 26.80 -2 -12 0 309.97 23.50 -2 -12 0 361.36 25.20 2 12 0 337.57 26.70 2 12 0 334.47 25.80 2 12 0 336.67 24.90 2 12 0 357.26 27.80 2 12 0 364.96 27.40 2 12 0 394.76 27.10 -3 -12 0 11.60 6.60 -3 -12 0 11.70 7.40 -3 -12 0 19.20 6.60 -3 -12 0 21.80 7.70 -3 -12 0 16.30 8.00 3 12 0 33.00 9.50 3 12 0 9.00 7.70 3 12 0 19.10 8.60 3 12 0 20.60 7.30 3 12 0 24.90 8.60 3 12 0 16.60 6.50 -4 -12 0 4.40 5.80 -4 -12 0 0.60 6.00 -4 -12 0 -5.40 6.80 -4 -12 0 -1.30 7.00 4 12 0 -4.70 7.40 4 12 0 7.20 6.20 4 12 0 6.90 7.40 4 12 0 -1.30 6.30 4 12 0 -2.20 5.60 4 12 0 3.10 5.60 -5 -12 0 17.70 8.50 -5 -12 0 13.80 7.90 -5 -12 0 26.30 7.00 -5 -12 0 26.10 8.90 5 12 0 21.40 8.60 5 12 0 27.00 9.50 5 12 0 15.90 7.90 5 12 0 11.10 7.00 5 12 0 53.69 10.60 -6 -12 0 2.20 8.10 -6 -12 0 0.70 4.90 -6 -12 0 -3.60 7.40 -6 -12 0 -2.50 6.20 6 12 0 -1.70 6.30 6 12 0 -1.70 6.40 6 12 0 -0.90 7.20 6 12 0 12.70 6.40 6 12 0 -2.10 7.80 -7 -12 0 9.90 7.00 -7 -12 0 1.60 8.00 -7 -12 0 2.50 4.80 -7 -12 0 -6.10 7.30 7 12 0 6.90 7.70 7 12 0 7.30 8.00 7 12 0 5.60 8.70 7 12 0 6.50 6.40 7 12 0 -3.00 6.30 -8 -12 0 2.80 8.10 -8 -12 0 4.30 7.90 8 12 0 -2.00 7.50 8 12 0 -9.60 7.90 8 12 0 9.60 8.20 8 12 0 19.50 8.10 8 12 0 -8.40 6.40 -9 -12 0 31.80 10.60 -9 -12 0 38.30 11.00 9 12 0 13.70 8.30 9 12 0 29.90 9.80 9 12 0 42.40 14.60 9 12 0 30.20 10.50 9 12 0 46.80 10.40 -10 -12 0 147.89 18.80 -10 -12 0 105.69 16.80 10 12 0 106.09 14.70 10 12 0 131.89 17.40 10 12 0 111.19 17.70 10 12 0 132.79 17.40 -11 -12 0 -4.10 8.70 -11 -12 0 7.50 9.20 11 12 0 -5.30 7.20 11 12 0 6.00 8.40 11 12 0 8.70 10.30 11 12 0 10.00 9.20 -12 -12 0 90.89 15.90 -12 -12 0 94.09 16.60 12 12 0 115.79 18.00 12 12 0 103.39 16.30 12 12 0 115.19 15.60 12 12 0 99.99 17.10 -13 -12 0 62.69 14.20 -13 -12 0 66.39 14.10 13 12 0 75.19 15.40 13 12 0 90.69 13.90 13 12 0 55.89 14.80 -14 -12 0 35.50 12.60 -14 -12 0 33.60 12.70 14 12 0 42.80 13.30 14 12 0 38.10 14.00 14 12 0 41.50 11.30 11 -13 0 2.00 10.70 11 -13 0 24.00 12.70 -11 13 0 20.90 11.90 -11 13 0 32.70 13.50 10 -13 0 2.60 10.20 10 -13 0 1.60 10.50 10 -13 0 13.40 10.10 -10 13 0 11.20 12.20 -10 13 0 4.70 10.90 -10 13 0 13.60 11.00 9 -13 0 12.90 9.80 9 -13 0 1.90 8.70 9 -13 0 -10.60 9.30 -9 13 0 -6.00 9.40 -9 13 0 -7.80 9.80 -9 13 0 7.80 9.70 8 -13 0 -3.20 7.70 8 -13 0 1.80 9.20 8 -13 0 -0.20 7.80 -8 13 0 -7.60 8.50 -8 13 0 1.60 7.20 -8 13 0 -12.00 8.40 -8 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48.90 9.20 -4 -13 0 67.79 12.00 -4 -13 0 60.39 12.00 -4 -13 0 43.00 10.00 4 13 0 60.59 11.70 4 13 0 32.40 9.60 4 13 0 12.30 9.10 4 13 0 60.39 9.40 4 13 0 42.80 10.70 4 13 0 66.49 10.60 -5 -13 0 67.79 12.50 -5 -13 0 57.39 12.00 -5 -13 0 92.59 13.00 -5 -13 0 75.49 10.90 5 13 0 86.59 13.70 5 13 0 62.29 12.40 5 13 0 59.09 11.80 5 13 0 48.90 10.80 5 13 0 61.79 10.50 -6 -13 0 5.00 5.60 -6 -13 0 15.80 7.50 -6 -13 0 10.80 9.40 -6 -13 0 16.80 8.90 6 13 0 5.30 8.00 6 13 0 16.80 9.50 6 13 0 9.10 7.50 6 13 0 6.40 8.00 6 13 0 6.20 9.90 -7 -13 0 10.10 5.60 -7 -13 0 11.70 9.30 -7 -13 0 25.40 8.40 -7 -13 0 11.80 9.20 7 13 0 14.10 9.10 7 13 0 0.90 7.40 7 13 0 5.20 8.40 7 13 0 8.60 7.50 -8 -13 0 5.40 8.40 -8 -13 0 0.90 8.70 8 13 0 6.50 9.40 8 13 0 2.30 7.90 8 13 0 14.20 8.50 8 13 0 8.40 8.70 -9 -13 0 6.50 9.30 -9 -13 0 5.70 9.00 9 13 0 1.80 8.20 9 13 0 -11.50 6.70 9 13 0 4.50 8.70 9 13 0 1.00 7.60 -10 -13 0 -8.00 8.00 -10 -13 0 -11.20 8.10 10 13 0 -12.30 8.70 10 13 0 1.40 7.40 10 13 0 -6.00 7.70 10 13 0 0.90 7.70 -11 -13 0 -8.40 8.40 -11 -13 0 -14.30 8.10 11 13 0 8.90 8.80 11 13 0 -4.70 7.60 11 13 0 -0.70 8.70 11 13 0 -2.20 9.10 -12 -13 0 124.39 18.90 -12 -13 0 111.59 18.10 12 13 0 108.39 18.00 12 13 0 135.59 20.10 12 13 0 106.99 16.60 12 13 0 105.79 15.80 -13 -13 0 77.69 16.70 -13 -13 0 94.19 17.10 13 13 0 101.39 19.60 13 13 0 117.79 16.40 13 13 0 139.49 20.60 -14 -13 0 47.10 14.30 -14 -13 0 49.70 13.60 14 13 0 31.70 10.60 14 13 0 37.50 14.10 14 13 0 33.70 13.60 9 -14 0 0.60 9.80 9 -14 0 -7.70 10.20 -9 14 0 7.70 10.00 -9 14 0 9.20 10.40 -9 14 0 1.70 11.60 8 -14 0 72.89 14.10 8 -14 0 67.19 14.70 -8 14 0 74.09 14.80 -8 14 0 91.49 12.50 -8 14 0 87.99 15.60 -8 14 0 87.69 15.70 7 -14 0 13.10 9.80 7 -14 0 27.80 11.10 -7 14 0 14.70 8.90 -7 14 0 22.20 11.70 -7 14 0 44.00 12.20 -7 14 0 35.60 11.60 6 -14 0 -6.10 7.10 6 -14 0 -7.70 7.60 6 -14 0 -9.00 6.80 -6 14 0 -2.00 9.10 -6 14 0 1.60 9.00 -6 14 0 9.60 8.90 -6 14 0 -2.80 8.80 5 -14 0 0.90 8.50 5 -14 0 2.10 7.80 5 -14 0 6.10 7.80 -5 14 0 6.10 8.00 -5 14 0 1.10 8.90 -5 14 0 3.50 8.80 -5 14 0 3.30 8.40 4 -14 0 -5.10 6.80 4 -14 0 -3.10 7.70 4 -14 0 5.70 6.90 -4 14 0 1.90 6.80 -4 14 0 13.10 8.50 -4 14 0 12.30 6.20 -4 14 0 3.90 8.20 -4 14 0 9.50 9.00 -4 14 0 21.10 9.90 3 -14 0 32.40 9.70 3 -14 0 24.70 7.80 3 -14 0 19.40 9.10 -3 14 0 38.00 9.90 -3 14 0 18.50 8.50 -3 14 0 21.00 9.40 -3 14 0 14.20 9.00 -3 14 0 29.00 7.40 2 -14 0 2.90 7.10 2 -14 0 -3.10 5.80 2 -14 0 11.60 8.70 -2 14 0 -9.80 7.10 -2 14 0 -4.00 7.40 -2 14 0 -0.50 5.90 -2 14 0 14.60 7.90 -2 14 0 -3.70 7.70 1 -14 0 64.59 11.70 1 -14 0 46.80 10.40 1 -14 0 63.79 9.40 1 -14 0 43.70 10.30 1 -14 0 54.39 10.20 -1 14 0 49.30 10.30 -1 14 0 42.60 10.40 -1 14 0 30.30 9.90 -1 14 0 36.40 8.70 -1 14 0 45.70 10.20 0 -14 0 138.99 16.50 0 -14 0 110.29 16.20 0 -14 0 149.69 14.10 0 -14 0 146.89 16.50 0 -14 0 114.49 14.80 0 14 0 85.99 14.50 0 14 0 126.69 16.30 0 14 0 130.39 13.80 0 14 0 139.29 15.60 -1 -14 0 4.70 7.90 -1 -14 0 6.40 7.60 -1 -14 0 8.60 7.20 -1 -14 0 15.10 8.10 -1 -14 0 8.80 6.10 -1 -14 0 5.00 7.40 1 14 0 8.30 8.40 1 14 0 -3.40 6.10 1 14 0 9.60 8.80 1 14 0 12.80 7.50 -2 -14 0 85.59 13.30 -2 -14 0 54.49 8.60 -2 -14 0 68.19 12.20 -2 -14 0 50.29 10.50 -2 -14 0 75.19 12.30 2 14 0 64.19 11.70 2 14 0 50.79 11.00 2 14 0 33.70 10.40 2 14 0 61.89 10.30 2 14 0 63.99 13.10 -3 -14 0 6.60 7.10 -3 -14 0 2.00 8.00 -3 -14 0 0.40 6.80 -3 -14 0 -2.80 8.10 3 14 0 -3.90 7.30 3 14 0 -2.10 7.50 3 14 0 -12.10 7.00 3 14 0 -5.10 6.20 3 14 0 0.30 7.60 -4 -14 0 -9.10 6.30 -4 -14 0 -3.30 7.20 -4 -14 0 2.40 7.60 -4 -14 0 -9.80 7.30 4 14 0 10.30 8.50 4 14 0 -4.40 7.60 4 14 0 13.40 9.60 4 14 0 0.50 6.50 4 14 0 1.60 7.80 -5 -14 0 5.20 8.80 -5 -14 0 -5.60 6.50 -5 -14 0 7.40 8.60 -5 -14 0 -7.30 7.30 5 14 0 14.10 9.30 5 14 0 -4.80 8.30 5 14 0 4.30 7.80 5 14 0 -1.40 8.40 -6 -14 0 27.70 10.50 -6 -14 0 31.70 11.30 -6 -14 0 24.20 7.60 -6 -14 0 35.90 9.80 6 14 0 38.40 11.30 6 14 0 22.10 8.90 6 14 0 16.90 10.10 6 14 0 21.30 9.50 -7 -14 0 26.70 8.70 -7 -14 0 41.00 11.50 -7 -14 0 44.30 11.90 -7 -14 0 37.20 7.80 7 14 0 32.60 10.70 7 14 0 49.10 11.80 7 14 0 37.20 11.30 7 14 0 17.50 9.20 -8 -14 0 2.90 8.60 -8 -14 0 1.90 9.70 8 14 0 5.40 8.60 8 14 0 -1.10 7.30 8 14 0 16.30 9.40 8 14 0 -2.70 8.80 -9 -14 0 33.20 11.60 -9 -14 0 22.90 11.00 9 14 0 36.80 11.50 9 14 0 24.80 9.60 9 14 0 27.30 11.70 9 14 0 33.50 11.10 -10 -14 0 6.40 10.50 -10 -14 0 19.70 10.50 10 14 0 20.90 10.90 10 14 0 3.20 8.30 10 14 0 5.50 8.60 10 14 0 -1.40 8.80 -11 -14 0 3.30 9.90 -11 -14 0 8.40 10.00 11 14 0 3.50 10.60 11 14 0 14.10 10.00 11 14 0 6.50 8.30 11 14 0 -18.40 7.90 -12 -14 0 4.70 10.30 -12 -14 0 18.50 11.20 12 14 0 6.00 11.20 12 14 0 21.90 10.40 12 14 0 0.00 9.40 12 14 0 -7.70 7.30 -13 -14 0 13.70 11.20 -13 -14 0 7.20 10.70 13 14 0 14.90 12.20 13 14 0 1.60 9.30 13 14 0 12.90 10.80 8 -15 0 2.10 10.10 -8 15 0 25.00 14.80 -8 15 0 12.10 10.50 -8 15 0 8.20 11.40 7 -15 0 27.80 11.80 7 -15 0 33.20 10.00 7 -15 0 13.30 9.40 -7 15 0 19.50 11.60 -7 15 0 34.00 10.50 -7 15 0 27.00 12.50 6 -15 0 -0.40 7.30 6 -15 0 2.60 8.90 6 -15 0 -14.80 7.10 -6 15 0 -9.80 10.00 -6 15 0 -8.80 8.80 -6 15 0 3.90 9.20 5 -15 0 29.10 8.90 5 -15 0 17.10 9.80 5 -15 0 31.10 11.30 -5 15 0 16.10 10.90 -5 15 0 23.60 10.30 -5 15 0 25.70 10.60 4 -15 0 21.80 9.80 4 -15 0 42.60 9.60 4 -15 0 39.10 11.20 -4 15 0 19.20 10.40 -4 15 0 37.00 11.10 -4 15 0 34.70 11.00 -4 15 0 40.00 11.70 3 -15 0 7.30 8.50 3 -15 0 25.70 8.30 3 -15 0 18.90 9.10 -3 15 0 15.70 9.30 -3 15 0 21.60 7.30 -3 15 0 4.90 8.80 -3 15 0 25.20 9.90 -3 15 0 5.50 9.10 2 -15 0 -3.60 7.50 2 -15 0 3.20 6.50 2 -15 0 5.90 8.20 -2 15 0 -5.80 5.40 -2 15 0 -5.60 7.70 -2 15 0 -0.60 8.60 -2 15 0 1.60 8.10 -2 15 0 7.60 8.50 1 -15 0 11.50 7.20 1 -15 0 23.00 9.00 1 -15 0 2.30 8.80 1 -15 0 8.40 8.00 -1 15 0 14.30 8.40 -1 15 0 21.60 9.40 -1 15 0 9.70 8.50 -1 15 0 18.40 7.20 -1 15 0 -4.00 7.90 0 -15 0 44.70 11.30 0 -15 0 61.99 11.90 0 -15 0 37.80 8.50 0 -15 0 46.10 10.80 0 -15 0 50.79 10.30 0 15 0 50.89 9.40 0 15 0 53.99 10.90 0 15 0 40.30 11.40 0 15 0 32.00 10.20 -1 -15 0 3.60 7.90 -1 -15 0 -1.90 6.00 -1 -15 0 18.90 9.60 -1 -15 0 2.50 6.50 -1 -15 0 9.10 8.00 -1 -15 0 1.70 8.00 1 15 0 -2.80 7.40 1 15 0 6.60 7.00 1 15 0 12.60 9.20 -2 -15 0 106.59 14.30 -2 -15 0 107.19 15.00 -2 -15 0 101.99 11.20 -2 -15 0 93.09 14.80 -2 -15 0 121.69 16.00 2 15 0 97.49 15.20 2 15 0 113.89 13.20 2 15 0 63.99 13.70 -3 -15 0 206.08 21.70 -3 -15 0 219.78 20.70 -3 -15 0 192.98 21.20 -3 -15 0 192.68 19.80 3 15 0 184.18 18.10 3 15 0 200.48 22.90 3 15 0 208.18 21.80 3 15 0 173.38 21.00 -4 -15 0 72.39 13.50 -4 -15 0 93.39 15.50 -4 -15 0 69.59 11.60 -4 -15 0 81.19 13.70 4 15 0 64.99 13.10 4 15 0 62.39 12.90 4 15 0 61.99 10.90 4 15 0 44.80 12.50 -5 -15 0 3.00 8.50 -5 -15 0 0.40 6.60 -5 -15 0 8.80 9.30 -5 -15 0 -4.10 9.00 5 15 0 11.80 8.30 5 15 0 18.30 11.00 5 15 0 9.10 9.10 5 15 0 -5.80 8.50 -6 -15 0 0.60 9.80 -6 -15 0 17.00 8.90 -6 -15 0 8.80 7.10 -6 -15 0 23.00 10.20 6 15 0 5.70 8.80 6 15 0 11.80 10.60 6 15 0 9.20 10.50 6 15 0 18.30 10.10 -7 -15 0 27.20 11.70 -7 -15 0 39.10 11.60 -7 -15 0 39.60 10.60 -7 -15 0 32.00 7.30 7 15 0 28.10 10.90 7 15 0 21.40 10.60 7 15 0 56.59 14.00 7 15 0 40.50 13.10 -8 -15 0 36.70 11.90 -8 -15 0 35.20 11.50 8 15 0 30.90 11.20 8 15 0 16.40 11.00 8 15 0 17.60 11.30 8 15 0 41.30 12.70 -9 -15 0 24.20 10.70 -9 -15 0 8.60 10.60 9 15 0 -11.90 6.60 9 15 0 -7.50 8.90 9 15 0 -10.70 8.40 9 15 0 1.80 10.10 -10 -15 0 11.10 11.80 -10 -15 0 35.80 13.30 10 15 0 19.40 10.60 10 15 0 31.60 12.00 10 15 0 32.40 10.80 10 15 0 17.60 11.90 -11 -15 0 14.00 11.40 -11 -15 0 22.60 12.20 11 15 0 30.40 11.90 11 15 0 25.40 10.50 11 15 0 25.70 12.20 11 15 0 40.30 12.50 -12 -15 0 25.80 13.20 -12 -15 0 36.50 13.70 12 15 0 18.80 10.30 12 15 0 20.30 11.90 12 15 0 12.50 11.70 12 15 0 33.00 12.90 7 -16 0 1.00 9.90 7 -16 0 3.50 8.20 -7 16 0 23.50 13.20 -7 16 0 1.60 10.40 6 -16 0 20.90 9.00 6 -16 0 8.00 9.80 6 -16 0 12.80 10.40 -6 16 0 17.60 10.90 -6 16 0 24.80 11.60 -6 16 0 3.60 10.40 5 -16 0 5.60 8.00 5 -16 0 -15.70 8.00 5 -16 0 -0.10 8.30 -5 16 0 3.30 9.40 -5 16 0 -0.70 9.90 -5 16 0 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11.50 -3 -16 0 44.10 12.50 -3 -16 0 64.99 13.00 3 16 0 51.99 12.60 3 16 0 45.60 11.90 3 16 0 70.39 10.80 -4 -16 0 41.90 10.70 -4 -16 0 63.19 13.00 -4 -16 0 35.80 12.50 -4 -16 0 29.20 11.30 4 16 0 50.09 11.80 4 16 0 31.80 11.10 4 16 0 46.90 11.10 4 16 0 33.40 10.80 -5 -16 0 2.30 8.80 -5 -16 0 4.40 9.00 -5 -16 0 0.20 9.80 -5 -16 0 3.90 7.50 5 16 0 3.80 8.80 5 16 0 7.50 9.40 5 16 0 3.40 9.80 5 16 0 23.00 8.70 -6 -16 0 56.09 13.00 -6 -16 0 47.10 12.90 -6 -16 0 42.70 9.70 -6 -16 0 42.00 12.20 6 16 0 51.29 13.20 6 16 0 46.60 12.30 6 16 0 52.99 13.20 -7 -16 0 16.00 10.90 -7 -16 0 1.30 9.90 -7 -16 0 -3.20 5.80 -7 -16 0 5.20 9.90 7 16 0 -4.60 8.70 7 16 0 -1.10 10.80 7 16 0 15.30 11.30 7 16 0 13.40 10.20 -8 -16 0 5.60 10.70 -8 -16 0 6.90 10.20 8 16 0 2.30 9.40 8 16 0 15.90 11.50 8 16 0 -3.90 8.60 8 16 0 -4.60 9.90 -9 -16 0 8.00 12.10 -9 -16 0 12.00 11.10 9 16 0 12.70 10.20 9 16 0 -11.80 9.90 9 16 0 -3.40 10.00 9 16 0 0.30 9.80 -10 -16 0 13.50 11.70 -10 -16 0 9.90 10.80 10 16 0 4.60 11.10 10 16 0 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-1.00 9.40 2 17 0 3.00 8.30 2 17 0 16.90 9.60 2 17 0 6.10 10.10 -3 -17 0 46.10 12.50 -3 -17 0 37.20 11.60 -3 -17 0 58.89 12.30 -3 -17 0 46.10 12.60 3 17 0 38.00 12.60 3 17 0 38.20 10.30 3 17 0 31.20 11.30 -4 -17 0 10.40 10.40 -4 -17 0 13.70 10.40 -4 -17 0 9.60 10.30 -4 -17 0 8.60 8.90 4 17 0 15.50 10.30 4 17 0 5.60 7.60 4 17 0 17.00 10.40 -5 -17 0 -0.30 9.90 -5 -17 0 -11.80 7.90 -5 -17 0 3.50 10.50 -5 -17 0 2.70 9.70 5 17 0 0.20 8.70 5 17 0 -22.70 8.20 5 17 0 -4.60 8.50 5 17 0 -13.80 7.80 -6 -17 0 7.50 10.20 -6 -17 0 19.20 8.20 -6 -17 0 9.30 10.80 -6 -17 0 -3.00 9.30 6 17 0 23.20 11.40 6 17 0 -2.40 9.40 6 17 0 8.30 11.80 -7 -17 0 39.90 13.50 -7 -17 0 42.00 8.70 -7 -17 0 48.70 14.30 7 17 0 32.60 13.10 7 17 0 43.00 12.20 7 17 0 28.50 13.60 -8 -17 0 -8.40 10.50 -8 -17 0 8.70 11.00 8 17 0 -2.10 10.30 8 17 0 5.50 10.90 8 17 0 -0.10 10.30 8 17 0 -8.00 9.90 -9 -17 0 12.40 12.40 -9 -17 0 10.60 11.50 9 17 0 28.30 12.30 9 17 0 24.80 12.60 9 17 0 14.60 11.10 9 17 0 14.20 12.30 2 -18 0 -14.70 8.60 2 -18 0 9.60 9.60 2 -18 0 11.60 8.40 -2 18 0 13.10 7.80 -2 18 0 -7.50 9.10 -2 18 0 5.00 10.80 -2 18 0 -16.90 8.10 1 -18 0 4.70 7.70 1 -18 0 11.80 11.20 -1 18 0 13.20 8.30 -1 18 0 -0.50 10.40 -1 18 0 -6.80 10.20 0 -18 0 14.30 8.20 0 -18 0 12.50 10.60 0 -18 0 37.80 11.50 0 18 0 17.00 8.60 0 18 0 6.10 10.20 0 18 0 -11.40 9.20 -1 -18 0 17.90 7.60 -1 -18 0 15.10 10.40 -1 -18 0 29.90 12.10 1 18 0 16.30 8.90 1 18 0 15.40 11.70 1 18 0 -7.50 8.50 -2 -18 0 14.90 11.60 -2 -18 0 19.70 9.90 -2 -18 0 12.10 10.90 2 18 0 17.80 11.30 2 18 0 19.10 10.90 2 18 0 4.60 7.80 -3 -18 0 65.29 15.00 -3 -18 0 83.99 15.50 -3 -18 0 39.40 12.10 3 18 0 78.19 14.60 3 18 0 64.29 14.50 3 18 0 78.29 12.60 -4 -18 0 45.90 13.10 -4 -18 0 20.40 12.10 -4 -18 0 48.80 12.70 -4 -18 0 42.50 12.00 4 18 0 43.10 12.60 4 18 0 30.40 9.90 4 18 0 46.80 13.50 -5 -18 0 28.50 12.60 -5 -18 0 20.20 10.60 -5 -18 0 15.30 10.60 5 18 0 13.00 9.50 5 18 0 15.50 11.60 5 18 0 13.30 11.40 -6 -18 0 3.80 10.60 -6 -18 0 -6.00 9.40 -6 -18 0 3.60 9.70 6 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77.29 12.50 8 12 -3 48.80 12.10 8 12 -3 78.99 12.70 8 12 -3 76.39 13.40 8 12 -3 66.39 12.40 -8 -12 3 70.59 13.70 -8 -12 3 87.29 14.30 7 12 -3 96.69 15.40 7 12 -3 89.39 14.10 7 12 -3 76.59 12.70 7 12 -3 90.39 14.00 7 12 -3 110.39 14.80 7 12 -3 63.89 12.40 -7 -12 3 75.69 13.60 -7 -12 3 78.89 9.90 -7 -12 3 64.69 13.50 6 12 -3 32.60 8.70 6 12 -3 25.80 9.50 6 12 -3 31.90 9.10 6 12 -3 16.90 9.60 6 12 -3 -2.10 6.70 6 12 -3 15.10 8.20 -6 -12 3 10.30 8.70 -6 -12 3 13.10 6.40 -6 -12 3 21.30 8.90 5 12 -3 12.90 8.40 5 12 -3 21.80 8.70 5 12 -3 17.10 8.20 5 12 -3 8.10 7.00 5 12 -3 15.40 8.10 5 12 -3 25.80 9.30 -5 -12 3 21.10 7.20 -5 -12 3 -4.90 7.50 -5 -12 3 13.80 6.90 -5 -12 3 21.70 9.40 4 12 -3 100.89 11.40 4 12 -3 61.19 12.20 4 12 -3 59.09 11.40 4 12 -3 76.39 13.30 4 12 -3 89.29 13.60 4 12 -3 67.69 10.80 -4 -12 3 108.29 11.90 -4 -12 3 75.39 11.50 -4 -12 3 69.89 12.60 -4 -12 3 86.39 13.70 3 12 -3 32.70 16.50 3 12 -3 43.80 8.60 3 12 -3 21.40 8.30 3 12 -3 38.40 9.60 3 12 -3 45.60 9.40 3 12 -3 42.90 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24.80 9.40 9 10 -3 39.60 9.90 9 10 -3 57.69 11.10 9 10 -3 48.00 10.80 -9 -10 3 45.80 11.50 -9 -10 3 42.60 11.00 -9 -10 3 39.00 11.10 -9 -10 3 39.60 10.40 8 10 -3 16.50 8.30 8 10 -3 22.40 7.70 8 10 -3 14.80 8.00 8 10 -3 19.50 7.90 8 10 -3 4.10 7.60 8 10 -3 1.70 6.80 -8 -10 3 17.90 8.80 -8 -10 3 16.90 7.70 -8 -10 3 25.30 9.70 -8 -10 3 12.70 8.30 7 10 -3 13.80 7.50 7 10 -3 11.50 8.60 7 10 -3 14.30 7.60 7 10 -3 1.80 6.40 7 10 -3 12.20 7.10 7 10 -3 14.20 7.30 -7 -10 3 0.40 6.90 -7 -10 3 20.00 8.00 -7 -10 3 20.60 7.30 -7 -10 3 9.60 4.80 -7 -10 3 21.80 9.00 6 10 -3 8.90 7.20 6 10 -3 -1.10 5.70 6 10 -3 4.20 7.50 6 10 -3 4.30 6.80 6 10 -3 22.70 8.00 6 10 -3 15.20 7.20 -6 -10 3 6.80 5.20 -6 -10 3 7.90 7.50 -6 -10 3 11.40 7.40 -6 -10 3 12.10 7.40 5 10 -3 -8.20 5.60 5 10 -3 -1.60 6.00 5 10 -3 5.50 6.40 5 10 -3 8.20 6.70 5 10 -3 -2.20 6.80 5 10 -3 9.40 6.50 -5 -10 3 8.70 7.20 -5 -10 3 1.40 6.70 -5 -10 3 5.90 6.30 -5 -10 3 5.70 5.30 -5 -10 3 3.10 5.20 4 10 -3 -0.20 7.10 4 10 -3 12.70 6.60 4 10 -3 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9.70 9.50 6 12 -4 32.10 10.10 6 12 -4 23.40 9.00 -6 -12 4 11.70 8.90 -6 -12 4 20.20 9.50 -6 -12 4 5.60 6.80 5 12 -4 161.38 18.00 5 12 -4 194.68 20.20 5 12 -4 180.18 17.90 5 12 -4 137.79 18.40 5 12 -4 145.69 17.80 5 12 -4 148.79 18.60 -5 -12 4 167.28 19.10 -5 -12 4 146.29 16.10 -5 -12 4 167.78 19.50 -5 -12 4 150.28 18.30 4 12 -4 42.90 8.30 4 12 -4 48.50 11.30 4 12 -4 54.79 10.70 4 12 -4 40.20 10.10 4 12 -4 48.00 10.70 4 12 -4 41.70 10.50 4 12 -4 41.50 9.20 -4 -12 4 75.29 12.70 -4 -12 4 32.60 8.90 -4 -12 4 51.29 9.60 -4 -12 4 58.49 11.60 -4 -12 4 44.20 9.70 3 12 -4 -2.90 5.30 3 12 -4 -1.60 6.20 3 12 -4 -2.30 5.60 3 12 -4 -2.50 6.30 3 12 -4 -7.70 5.50 3 12 -4 3.20 7.90 -3 -12 4 6.50 6.00 -3 -12 4 0.60 6.40 -3 -12 4 5.60 7.00 -3 -12 4 -3.90 7.30 -3 -12 4 5.40 7.30 -3 -12 4 4.80 4.60 2 12 -4 38.90 9.40 2 12 -4 34.40 7.80 2 12 -4 8.00 7.50 2 12 -4 22.20 8.80 2 12 -4 12.00 7.50 2 12 -4 18.60 7.90 -2 -12 4 12.00 7.90 -2 -12 4 16.30 7.50 -2 -12 4 29.60 10.20 -2 -12 4 22.10 8.30 -2 -12 4 18.40 7.70 -2 -12 4 20.00 6.00 1 12 -4 0.30 6.00 1 12 -4 1.30 6.50 1 12 -4 -4.80 5.20 1 12 -4 6.20 6.60 1 12 -4 7.50 7.30 1 12 -4 2.60 6.20 -1 -12 4 -2.40 6.20 -1 -12 4 -11.40 5.80 -1 -12 4 1.00 7.30 -1 -12 4 2.60 5.00 -1 -12 4 -9.20 6.50 -1 -12 4 -5.60 6.50 0 12 -4 18.30 7.70 0 12 -4 9.50 6.10 0 12 -4 22.80 7.70 0 12 -4 15.40 7.40 0 12 -4 5.10 7.20 0 12 -4 12.90 7.20 0 12 -4 21.70 8.40 0 -12 4 13.10 6.40 0 -12 4 32.30 8.40 0 -12 4 26.80 6.90 0 -12 4 14.80 7.70 0 -12 4 31.60 8.90 0 -12 4 20.30 8.20 0 -12 4 15.00 8.60 -1 12 -4 5.10 5.60 -1 12 -4 6.60 8.10 -1 12 -4 5.00 7.40 -1 12 -4 15.50 7.10 -1 12 -4 14.10 7.70 -1 12 -4 16.20 7.70 1 -12 4 9.30 6.20 1 -12 4 12.20 7.70 1 -12 4 14.30 6.40 1 -12 4 0.30 7.50 1 -12 4 20.40 8.10 1 -12 4 11.90 7.60 1 -12 4 11.40 7.80 -2 12 -4 52.79 10.50 -2 12 -4 56.09 10.00 -2 12 -4 49.00 10.40 -2 12 -4 48.20 8.30 -2 12 -4 45.80 9.10 -2 12 -4 41.40 9.70 2 -12 4 58.79 10.80 2 -12 4 63.09 10.30 2 -12 4 33.70 8.10 2 -12 4 45.30 10.20 2 -12 4 57.79 10.40 2 -12 4 69.19 10.30 -3 12 -4 109.09 13.30 -3 12 -4 112.69 11.10 -3 12 -4 110.69 14.40 -3 12 -4 92.49 13.40 -3 12 -4 89.09 12.40 -3 12 -4 119.99 15.30 3 -12 4 105.19 14.00 3 -12 4 105.49 17.20 3 -12 4 84.59 12.30 3 -12 4 94.59 11.60 3 -12 4 112.69 14.80 3 -12 4 93.89 13.00 -4 12 -4 12.30 7.40 -4 12 -4 1.30 7.00 -4 12 -4 5.30 7.20 -4 12 -4 8.40 7.90 -4 12 -4 9.10 6.90 4 -12 4 11.00 6.40 4 -12 4 14.00 8.10 4 -12 4 5.60 7.10 4 -12 4 4.70 6.90 4 -12 4 6.00 6.80 -5 12 -4 66.59 12.10 -5 12 -4 47.10 9.90 -5 12 -4 47.30 10.20 -5 12 -4 60.69 11.90 5 -12 4 60.39 12.00 5 -12 4 38.00 10.40 5 -12 4 71.59 13.50 5 -12 4 59.09 10.70 5 -12 4 64.99 10.20 -6 12 -4 64.69 12.80 -6 12 -4 65.49 12.70 -6 12 -4 52.29 11.10 -6 12 -4 63.79 10.70 6 -12 4 77.39 12.40 6 -12 4 53.59 11.50 6 -12 4 45.80 10.20 6 -12 4 68.69 12.30 -7 12 -4 23.60 10.30 -7 12 -4 -1.80 7.20 -7 12 -4 6.20 6.60 -7 12 -4 15.80 9.30 7 -12 4 6.20 7.80 7 -12 4 4.80 8.80 7 -12 4 4.00 7.30 7 -12 4 -5.80 7.80 -8 12 -4 10.10 9.00 -8 12 -4 8.90 6.50 -8 12 -4 0.70 9.30 -8 12 -4 6.10 10.00 8 -12 4 11.50 8.40 8 -12 4 14.20 8.70 8 -12 4 8.90 9.10 -9 12 -4 29.00 11.40 -9 12 -4 15.20 10.50 9 -12 4 39.40 11.00 9 -12 4 -0.40 8.80 9 -12 4 18.90 10.00 -10 12 -4 72.99 14.70 -10 12 -4 42.80 13.40 10 -12 4 57.49 13.60 10 -12 4 66.09 13.00 10 -12 4 33.40 10.90 -11 12 -4 -10.20 9.10 -11 12 -4 2.50 10.20 11 -12 4 7.40 10.00 11 -12 4 6.20 9.30 11 -12 4 11.80 11.20 -12 12 -4 77.19 16.50 -12 12 -4 54.59 15.50 12 -12 4 92.69 16.50 12 -12 4 55.89 13.70 14 11 -4 15.50 11.30 14 11 -4 50.09 14.60 14 11 -4 29.80 13.00 -14 -11 4 42.40 15.10 -14 -11 4 66.09 14.70 13 11 -4 8.90 9.80 13 11 -4 29.40 12.50 13 11 -4 22.90 11.20 13 11 -4 15.80 10.00 13 11 -4 19.20 12.40 -13 -11 4 15.90 11.50 -13 -11 4 28.20 12.80 12 11 -4 44.20 13.10 12 11 -4 24.40 11.10 12 11 -4 23.30 10.50 12 11 -4 25.90 9.30 12 11 -4 7.20 9.90 -12 -11 4 29.40 11.30 -12 -11 4 31.50 12.50 -12 -11 4 20.10 10.30 11 11 -4 20.80 11.60 11 11 -4 19.90 9.50 11 11 -4 26.80 11.30 11 11 -4 24.00 10.90 11 11 -4 27.50 10.00 -11 -11 4 37.90 11.50 -11 -11 4 33.50 11.70 -11 -11 4 24.80 11.30 10 11 -4 40.10 10.80 10 11 -4 63.79 13.40 10 11 -4 50.39 12.80 10 11 -4 25.10 11.60 10 11 -4 57.09 11.50 -10 -11 4 39.50 12.20 -10 -11 4 40.70 12.00 -10 -11 4 57.59 13.30 9 11 -4 7.10 8.10 9 11 -4 27.50 11.10 9 11 -4 5.40 8.30 9 11 -4 16.00 8.20 9 11 -4 11.20 8.10 9 11 -4 -0.20 7.00 -9 -11 4 -3.10 8.20 -9 -11 4 13.50 9.00 -9 -11 4 -3.30 9.30 8 11 -4 103.89 15.00 8 11 -4 100.19 14.90 8 11 -4 94.29 14.70 8 11 -4 100.79 14.50 8 11 -4 112.39 15.20 8 11 -4 95.29 15.40 -8 -11 4 104.19 15.20 -8 -11 4 90.29 14.50 7 11 -4 103.99 15.40 7 11 -4 81.29 13.90 7 11 -4 92.89 13.50 7 11 -4 100.19 13.90 7 11 -4 93.69 13.80 7 11 -4 112.39 14.60 -7 -11 4 101.29 13.80 -7 -11 4 76.39 13.40 -7 -11 4 108.19 15.30 -7 -11 4 85.99 10.30 6 11 -4 0.00 7.00 6 11 -4 4.60 7.30 6 11 -4 13.30 7.80 6 11 -4 -14.00 6.40 6 11 -4 7.00 7.40 6 11 -4 -2.60 6.10 -6 -11 4 6.60 5.80 -6 -11 4 -1.90 7.60 -6 -11 4 1.00 7.60 -6 -11 4 -5.40 7.00 5 11 -4 14.20 8.00 5 11 -4 12.40 7.20 5 11 -4 11.40 8.10 5 11 -4 8.70 7.00 5 11 -4 21.80 9.00 5 11 -4 19.20 7.60 -5 -11 4 23.90 7.20 -5 -11 4 6.00 8.10 -5 -11 4 32.30 8.80 -5 -11 4 8.20 8.40 4 11 -4 247.08 21.70 4 11 -4 245.88 21.20 4 11 -4 226.58 18.40 4 11 -4 255.77 21.10 4 11 -4 252.77 20.00 4 11 -4 220.98 20.00 4 11 -4 235.98 20.30 -4 -11 4 244.68 20.80 -4 -11 4 222.18 20.20 -4 -11 4 245.68 19.30 -4 -11 4 247.68 21.60 -4 -11 4 221.98 19.00 3 11 -4 5.00 6.60 3 11 -4 6.70 6.70 3 11 -4 8.50 5.40 3 11 -4 1.10 5.90 3 11 -4 10.00 6.50 3 11 -4 3.00 7.00 3 11 -4 3.00 6.00 -3 -11 4 -4.40 7.00 -3 -11 4 4.70 6.50 -3 -11 4 -0.90 7.20 -3 -11 4 0.10 6.00 -3 -11 4 4.30 6.10 -3 -11 4 5.30 4.40 2 11 -4 89.19 12.60 2 11 -4 78.39 10.60 2 11 -4 90.79 12.60 2 11 -4 128.79 13.90 2 11 -4 106.59 13.80 2 11 -4 96.49 13.60 2 11 -4 113.69 13.40 -2 -11 4 124.69 13.70 -2 -11 4 127.09 14.20 -2 -11 4 117.99 14.10 -2 -11 4 96.49 13.80 -2 -11 4 104.89 10.50 -2 -11 4 99.29 12.90 1 11 -4 294.07 22.30 1 11 -4 292.97 22.80 1 11 -4 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5.20 4.60 4 3 -7 165.98 14.70 4 3 -7 160.68 12.50 4 3 -7 147.39 13.10 4 3 -7 178.98 15.40 4 3 -7 169.28 14.80 4 3 -7 184.98 15.10 -4 -3 7 183.68 14.50 -4 -3 7 175.68 15.60 -4 -3 7 176.58 14.70 -4 -3 7 169.08 13.80 -4 -3 7 177.78 14.20 3 3 -7 1.60 3.00 3 3 -7 2.50 3.80 3 3 -7 1.00 2.50 3 3 -7 1.60 4.80 3 3 -7 -2.00 4.20 3 3 -7 -1.00 4.40 3 3 -7 2.50 4.80 3 3 -7 -0.20 4.10 -3 -3 7 0.60 3.90 -3 -3 7 -0.20 5.40 -3 -3 7 -1.70 4.10 -3 -3 7 3.10 4.50 -3 -3 7 3.10 3.30 -3 -3 7 -4.60 4.20 2 3 -7 59.89 5.90 2 3 -7 60.99 7.20 2 3 -7 64.69 8.80 2 3 -7 59.49 8.70 2 3 -7 65.09 8.70 2 3 -7 64.29 7.40 2 3 -7 71.29 8.00 -2 -3 7 58.09 8.30 -2 -3 7 51.99 7.30 -2 -3 7 46.20 7.90 -2 -3 7 54.89 7.90 -2 -3 7 53.09 8.10 -2 -3 7 56.79 6.50 -2 -3 7 53.59 7.50 1 3 -7 660.33 41.30 1 3 -7 650.73 41.80 1 3 -7 654.13 42.30 1 3 -7 669.13 41.60 1 3 -7 663.83 40.60 1 3 -7 640.64 42.20 1 3 -7 710.23 42.60 1 3 -7 668.53 42.60 -1 -3 7 646.84 41.10 -1 -3 7 624.84 40.70 -1 -3 7 658.53 41.90 -1 -3 7 640.14 42.80 -1 -3 7 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3 -7 17.50 11.00 16 -3 7 60.69 12.70 -17 3 -7 18.40 11.50 -17 3 -7 24.50 11.70 17 -3 7 11.70 9.80 14 2 -7 43.50 10.50 14 2 -7 9.20 10.90 14 2 -7 17.80 12.20 -14 -2 7 33.30 13.40 13 2 -7 41.50 13.20 13 2 -7 54.29 11.70 13 2 -7 34.50 12.40 -13 -2 7 44.20 13.60 12 2 -7 12.40 8.70 12 2 -7 14.50 10.50 12 2 -7 -7.60 8.10 -12 -2 7 3.80 9.10 11 2 -7 2.30 7.30 11 2 -7 -0.90 7.00 11 2 -7 -3.50 8.80 -11 -2 7 -1.00 8.50 10 2 -7 7.20 7.30 10 2 -7 0.60 8.00 10 2 -7 -4.70 6.60 -10 -2 7 -5.60 7.30 9 2 -7 61.79 10.20 9 2 -7 76.49 12.90 9 2 -7 58.69 10.90 9 2 -7 59.69 11.90 -9 -2 7 37.30 10.70 8 2 -7 24.10 7.50 8 2 -7 29.60 8.90 8 2 -7 20.90 7.80 8 2 -7 15.00 8.10 -8 -2 7 34.30 9.20 7 2 -7 16.80 7.30 7 2 -7 9.10 6.60 7 2 -7 7.20 6.00 7 2 -7 12.30 6.80 -7 -2 7 11.80 4.50 -7 -2 7 21.30 6.60 -7 -2 7 21.60 8.30 -7 -2 7 26.80 7.90 6 2 -7 23.60 7.60 6 2 -7 20.60 7.10 6 2 -7 32.20 7.90 6 2 -7 27.10 6.90 -6 -2 7 19.90 5.30 -6 -2 7 27.60 8.30 -6 -2 7 23.20 5.80 -6 -2 7 23.70 6.40 -6 -2 7 36.20 8.60 5 2 -7 114.59 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2 -7 6.60 5.70 8 -2 7 0.00 5.20 8 -2 7 -3.20 4.20 8 -2 7 3.80 4.30 8 -2 7 -0.70 3.90 -9 2 -7 21.50 6.50 -9 2 -7 38.40 7.40 -9 2 -7 24.40 6.90 -9 2 -7 30.10 7.50 -9 2 -7 5.50 5.60 9 -2 7 21.60 5.30 9 -2 7 17.30 4.90 9 -2 7 26.30 6.70 9 -2 7 8.90 6.80 -10 2 -7 176.58 15.70 -10 2 -7 177.88 16.20 -10 2 -7 184.68 15.70 -10 2 -7 166.28 15.90 -10 2 -7 173.78 15.90 10 -2 7 165.48 14.40 10 -2 7 167.18 18.10 10 -2 7 166.88 15.40 -11 2 -7 136.89 15.50 -11 2 -7 112.99 14.60 -11 2 -7 156.78 16.20 -11 2 -7 167.18 16.90 -11 2 -7 166.88 17.00 11 -2 7 136.89 13.10 11 -2 7 174.08 15.50 11 -2 7 139.69 16.60 -12 2 -7 27.00 8.10 -12 2 -7 26.60 8.60 -12 2 -7 17.10 8.00 -12 2 -7 14.10 7.60 -12 2 -7 32.50 8.80 12 -2 7 35.80 8.60 12 -2 7 23.20 9.10 12 -2 7 39.00 9.30 -13 2 -7 41.80 9.70 -13 2 -7 21.70 8.60 -13 2 -7 29.10 8.60 -13 2 -7 7.00 7.20 -13 2 -7 23.20 8.30 13 -2 7 18.80 7.60 13 -2 7 36.10 9.60 13 -2 7 13.80 8.40 -14 2 -7 5.50 7.60 -14 2 -7 0.50 7.10 -14 2 -7 11.60 8.10 14 -2 7 12.30 8.40 14 -2 7 6.40 8.70 14 -2 7 7.10 7.00 -15 2 -7 -2.30 8.10 -15 2 -7 0.50 8.10 15 -2 7 2.60 7.20 15 -2 7 -7.70 7.40 -16 2 -7 2.30 8.60 -16 2 -7 9.50 9.50 16 -2 7 -3.40 7.50 -17 2 -7 8.10 10.90 -17 2 -7 3.50 9.60 17 -2 7 2.70 9.10 -18 2 -7 -18.70 9.70 -18 2 -7 18.80 11.40 14 1 -7 22.30 12.20 14 1 -7 4.30 8.50 14 1 -7 21.60 11.90 -14 -1 7 4.50 11.30 13 1 -7 38.30 12.90 13 1 -7 2.70 10.10 13 1 -7 15.40 8.90 -13 -1 7 21.80 11.10 12 1 -7 15.90 8.60 12 1 -7 0.70 9.60 12 1 -7 28.00 10.20 -12 -1 7 34.60 11.70 11 1 -7 125.79 15.50 11 1 -7 119.59 16.70 11 1 -7 125.29 17.30 -11 -1 7 89.49 15.60 10 1 -7 77.99 13.40 10 1 -7 58.49 11.00 10 1 -7 82.59 14.00 -10 -1 7 59.19 12.80 9 1 -7 -3.50 6.00 9 1 -7 4.70 6.70 9 1 -7 -0.70 7.00 -9 -1 7 4.20 7.60 8 1 -7 3.10 6.80 8 1 -7 16.50 6.80 8 1 -7 11.20 7.00 8 1 -7 -7.00 5.00 -8 -1 7 5.90 7.60 7 1 -7 0.00 6.00 7 1 -7 0.20 5.10 7 1 -7 -13.10 5.60 7 1 -7 22.20 7.40 -7 -1 7 5.60 6.70 -7 -1 7 3.10 4.50 6 1 -7 39.30 7.50 6 1 -7 30.50 8.40 6 1 -7 40.30 8.40 6 1 -7 50.19 9.00 -6 -1 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67.49 11.80 -5 10 -9 42.30 8.70 -5 10 -9 24.10 9.30 -5 10 -9 35.80 10.10 -5 10 -9 36.80 10.00 5 -10 9 53.79 9.30 5 -10 9 32.40 9.20 5 -10 9 31.60 10.10 5 -10 9 42.90 9.50 5 -10 9 27.60 10.20 5 -10 9 40.00 9.70 5 -10 9 33.10 9.50 -6 10 -9 9.40 8.10 -6 10 -9 2.40 7.20 -6 10 -9 5.20 8.20 -6 10 -9 4.70 5.70 6 -10 9 3.90 7.40 6 -10 9 4.30 7.00 6 -10 9 13.40 9.30 6 -10 9 -10.40 5.90 6 -10 9 8.30 7.80 6 -10 9 -1.30 7.70 -7 10 -9 101.99 15.00 -7 10 -9 105.79 15.40 -7 10 -9 118.19 16.10 -7 10 -9 90.29 11.40 7 -10 9 139.49 16.50 7 -10 9 111.49 14.60 7 -10 9 112.59 16.00 7 -10 9 107.09 15.10 7 -10 9 89.59 13.20 -8 10 -9 16.60 8.50 -8 10 -9 18.20 9.50 -8 10 -9 16.00 9.00 8 -10 9 24.40 10.30 8 -10 9 16.30 8.50 8 -10 9 21.30 9.20 8 -10 9 31.30 8.90 -9 10 -9 4.90 8.20 -9 10 -9 5.60 9.00 -9 10 -9 -1.60 8.00 9 -10 9 7.60 9.20 9 -10 9 4.40 8.50 9 -10 9 -4.90 6.80 -10 10 -9 23.90 10.50 -10 10 -9 31.10 10.50 -10 10 -9 19.70 10.90 10 -10 9 22.40 9.90 10 -10 9 32.90 10.50 10 -10 9 25.20 10.90 -11 10 -9 14.10 10.40 -11 10 -9 3.60 9.10 -11 10 -9 1.70 8.70 11 -10 9 14.10 9.80 11 -10 9 -2.60 8.50 11 -10 9 6.50 9.10 -12 10 -9 -2.00 9.70 -12 10 -9 -1.20 11.60 -12 10 -9 7.20 10.80 12 -10 9 2.10 8.80 12 -10 9 -5.10 9.30 12 -10 9 9.70 9.00 -13 10 -9 -5.90 9.50 -13 10 -9 10.30 12.10 13 -10 9 1.50 9.40 13 -10 9 4.10 9.60 13 -10 9 24.00 10.60 -14 10 -9 -3.30 10.60 -14 10 -9 24.70 12.50 14 -10 9 6.80 11.10 14 -10 9 2.10 10.10 12 9 -9 -10.90 9.90 12 9 -9 -2.70 9.00 12 9 -9 -8.20 9.70 12 9 -9 -21.60 8.70 12 9 -9 0.30 10.30 -12 -9 9 -0.10 10.30 11 9 -9 -8.10 8.50 11 9 -9 7.80 9.80 11 9 -9 -3.30 9.80 11 9 -9 9.70 10.30 11 9 -9 -3.50 9.80 -11 -9 9 19.10 11.40 -11 -9 9 -12.20 9.40 10 9 -9 25.50 11.30 10 9 -9 19.20 9.80 10 9 -9 20.00 10.50 10 9 -9 -0.20 10.00 10 9 -9 15.20 11.20 -10 -9 9 23.70 11.50 -10 -9 9 13.30 10.80 9 9 -9 11.20 9.30 9 9 -9 0.50 9.40 9 9 -9 10.80 9.70 9 9 -9 20.90 9.60 9 9 -9 39.10 11.40 -9 -9 9 8.10 10.10 -9 -9 9 -1.10 9.20 -9 -9 9 17.20 10.60 8 9 -9 -6.10 7.80 8 9 -9 -11.00 7.20 8 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24.70 7.60 3 9 -9 2.70 5.30 3 9 -9 2.90 6.40 3 9 -9 10.30 8.00 -3 -9 9 24.80 8.30 -3 -9 9 43.50 8.30 -3 -9 9 0.10 6.90 -3 -9 9 12.30 7.60 -3 -9 9 5.10 8.00 -3 -9 9 16.20 5.60 2 9 -9 21.90 8.20 2 9 -9 17.80 7.90 2 9 -9 14.70 6.10 2 9 -9 9.80 7.90 2 9 -9 16.70 8.00 -2 -9 9 -3.40 6.40 -2 -9 9 9.70 7.70 -2 -9 9 11.50 8.20 -2 -9 9 7.60 5.60 -2 -9 9 18.70 7.90 1 9 -9 14.60 7.80 1 9 -9 21.70 8.20 1 9 -9 14.20 6.50 1 9 -9 19.00 7.50 1 9 -9 22.80 8.00 1 9 -9 15.70 8.00 -1 -9 9 12.60 5.70 -1 -9 9 21.10 8.90 -1 -9 9 9.20 8.80 -1 -9 9 15.30 7.70 -1 -9 9 18.10 7.50 -1 -9 9 13.40 7.90 0 9 -9 94.49 12.90 0 9 -9 86.09 12.70 0 9 -9 69.29 11.00 0 9 -9 88.39 12.80 0 9 -9 99.29 12.90 0 9 -9 89.09 10.50 0 -9 9 99.19 14.10 0 -9 9 85.69 10.30 0 -9 9 88.29 13.30 0 -9 9 68.09 11.30 0 -9 9 91.29 12.00 0 -9 9 94.69 11.60 -1 9 -9 219.68 17.50 -1 9 -9 182.58 17.60 -1 9 -9 173.38 16.70 -1 9 -9 204.98 15.40 -1 9 -9 226.28 17.80 -1 9 -9 151.18 17.80 1 -9 9 205.08 18.10 1 -9 9 198.98 19.00 1 -9 9 161.78 16.70 1 -9 9 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-1.5637 0.0578 17 4 1 -1.3097 0.0376 17 4 2 -0.6411 0.0135 17 4 3 -0.2669 -0.0048 17 4 4 -0.3931 0.0055 17 4 5 -0.3471 0.0203 17 4 6 -0.0466 0.0120 17 4 11 1.7055 0.0010 17 4 12 1.3636 0.0234 17 4 13 0.7348 -0.0021 17 4 14 0.5826 -0.0457 17 4 15 0.6808 -0.0388 17 5 0 1.2347 0.0378 17 5 1 0.6945 0.0189 17 5 2 -0.0448 -0.0067 17 5 3 -0.8009 -0.0364 17 5 4 -1.3077 -0.0420 17 5 5 -1.1841 -0.0307 17 5 6 -0.6939 -0.0335 17 5 9 -0.8204 0.0034 17 5 10 0.1211 -0.0090 17 5 11 0.8181 -0.0007 17 5 12 0.4811 0.0236 17 5 13 -0.4186 -0.0014 17 5 14 -0.8222 -0.0693 17 5 15 -0.3550 -0.1001 17 6 0 1.8727 -0.0018 17 6 1 1.8630 -0.0240 17 6 2 1.3293 -0.0443 17 6 3 0.4598 -0.0601 17 6 4 -0.2731 -0.0514 17 6 5 -0.5176 -0.0194 17 6 6 -0.6138 0.0018 17 6 7 -1.1067 0.0091 17 6 8 -1.7396 0.0203 17 6 9 -1.6947 0.0159 17 6 10 -0.7707 -0.0116 17 6 11 0.3352 -0.0148 17 6 12 0.7880 0.0110 17 6 13 0.3472 -0.0028 17 6 14 -0.3807 -0.0690 17 7 0 1.2886 -0.0480 17 7 1 1.3501 -0.0500 17 7 2 0.8885 -0.0267 17 7 3 0.1377 0.0061 17 7 4 -0.1938 0.0302 17 7 5 0.2464 0.0404 17 7 6 0.7054 0.0342 17 7 7 0.3212 0.0266 17 7 8 -0.5852 0.0290 17 7 9 -1.0936 0.0130 17 7 10 -0.9172 -0.0307 17 7 11 -0.3325 -0.0444 17 7 12 0.2904 -0.0049 17 7 13 0.4735 0.0179 17 8 1 0.7445 -0.0234 17 8 2 0.9115 -0.0428 17 8 3 0.3756 -0.0013 17 8 4 -0.1621 0.0546 17 8 5 0.1620 0.0700 17 8 6 0.8896 0.0368 17 8 7 0.9491 -0.0020 17 8 8 0.3924 -0.0157 17 8 9 0.0104 -0.0353 17 8 10 -0.0294 -0.0804 17 8 11 0.1104 -0.0925 17 8 12 0.5320 -0.0350 17 9 2 -0.0008 -0.0682 17 9 3 -0.2228 -0.0098 17 9 4 -0.6350 0.0605 17 9 5 -0.3063 0.0670 17 9 6 0.6110 0.0043 17 9 7 0.9476 -0.0487 17 9 8 0.4470 -0.0402 17 9 9 -0.1380 -0.0257 17 9 10 -0.5635 -0.0664 17 9 11 -0.9458 -0.1095 17 10 5 -1.0176 0.1437 17 10 6 -0.0322 0.0607 17 10 7 0.9002 -0.0449 17 10 8 1.0395 -0.0628 18 -2 4 -0.3132 -0.0221 18 -2 5 -0.0994 0.0018 18 -2 6 0.3520 0.0048 18 -2 7 1.3476 -0.0037 18 -2 8 2.1926 -0.0151 18 -2 9 1.8466 -0.0558 18 -2 10 0.7751 -0.1227 18 -1 3 0.1934 -0.1087 18 -1 4 -0.3259 -0.0816 18 -1 5 -0.5610 -0.0455 18 -1 6 -0.3669 -0.0250 18 -1 7 0.7599 -0.0211 18 -1 8 2.2170 -0.0198 18 -1 9 2.6158 -0.0393 18 -1 10 1.9636 -0.0939 18 -1 11 1.2807 -0.1132 18 0 2 0.2465 -0.1031 18 0 3 0.6333 -0.0743 18 0 4 0.8920 -0.0370 18 0 5 0.8252 -0.0067 18 0 6 0.4069 0.0055 18 0 7 0.5565 0.0013 18 0 8 1.4384 0.0041 18 0 10 1.4481 -0.0130 18 0 11 0.9621 -0.0343 18 0 12 0.6830 0.0277 18 1 2 1.0219 -0.0060 18 1 3 0.9533 0.0056 18 1 4 1.0450 0.0218 18 1 5 1.0625 0.0364 18 1 6 0.5317 0.0435 18 1 7 0.1599 0.0307 18 1 11 0.5868 -0.0006 18 1 12 0.4404 0.0213 18 1 13 0.0726 0.1039 18 2 2 1.4870 0.0497 18 2 3 1.2042 0.0346 18 2 4 1.0911 0.0075 18 2 5 1.0333 -0.0134 18 2 6 0.4125 -0.0071 18 2 12 -0.0127 -0.0501 18 2 13 -0.0501 -0.0234 18 3 2 1.9075 -0.0071 18 3 3 0.9797 0.0011 18 3 4 0.2083 -0.0134 18 3 5 -0.1277 -0.0388 18 3 12 0.2375 -0.0991 18 3 13 -0.1746 -0.1194 18 4 2 0.7140 -0.0409 18 4 3 0.5866 -0.0127 18 4 4 0.2333 0.0057 18 4 5 -0.0462 -0.0029 18 4 12 0.9530 -0.1034 18 5 2 -0.5106 -0.0466 18 5 3 -0.8427 -0.0186 18 5 4 -1.0201 0.0154 18 5 5 -0.9549 0.0134 18 5 12 0.8947 -0.0651 18 6 3 -0.5201 -0.0798 18 6 4 -0.8885 -0.0340 18 6 5 -1.2109 -0.0078 18 6 6 -1.5132 -0.0047 18 6 10 1.4511 -0.0266 18 6 11 1.6415 -0.0064 18 7 5 -0.5775 0.0126 18 7 6 -0.7520 0.0125 18 7 9 -0.1603 0.0106 0 0 0 0.0 0.0 ; _shelx_fab_checksum 68774 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co1 Co 0.70614(4) 0.29435(4) 0.49644(3) 0.01951(15) Uani 1 1 d . . . . . Fe1 Fe 0.41202(4) 0.35441(4) 0.35369(4) 0.02398(16) Uani 1 1 d . . . . . F1 F 0.0488(4) 0.2343(4) 0.9110(4) 0.1010(17) Uani 1 1 d . . . . . F2 F 0.2222(4) 0.2394(5) 0.8933(3) 0.1035(18) Uani 1 1 d . . . . . F3 F 0.1065(5) 0.3848(3) 0.9144(3) 0.0973(17) Uani 1 1 d . . . . . F4 F 0.1599(4) 0.2945(3) 0.7824(3) 0.0751(11) Uani 1 1 d . . . . . N1 N 0.3335(3) 0.5624(2) 0.4522(2) 0.0222(6) Uani 1 1 d . . . . . N2 N 0.2503(3) 0.2617(3) 0.5177(3) 0.0359(8) Uani 1 1 d . . . . . N3 N 0.5838(3) 0.3135(2) 0.4462(2) 0.0232(6) Uani 1 1 d . . . . . O2 O 0.6950(4) 0.3386(4) 0.7896(3) 0.0602(11) Uani 1 1 d . . . . . O1 O 0.7850(5) 0.1734(4) 0.2056(4) 0.0806(16) Uani 1 1 d . . . . . N8 N 0.5185(3) 0.4147(2) 0.2468(2) 0.0228(6) Uani 1 1 d . . . . . O3 O 0.9897(11) -0.1231(7) 0.7786(14) 0.279(10) Uani 1 1 d . . . . . N16 N 0.6043(3) 0.2478(3) 0.6161(2) 0.0266(7) Uani 1 1 d . . . . . N17 N 0.5164(3) 0.2493(3) 0.7647(2) 0.0326(8) Uani 1 1 d . . . . . N14 N 0.8247(3) 0.2728(3) 0.5531(3) 0.0309(7) Uani 1 1 d . . . . . N12 N 0.7511(4) 0.1515(3) 0.4410(3) 0.0395(9) Uani 1 1 d . . . . . N10 N 0.8034(3) 0.3431(3) 0.3758(3) 0.0335(8) Uani 1 1 d . . . . . N6 N 0.4641(3) 0.2160(2) 0.2900(2) 0.0261(7) Uani 1 1 d . . . . . N7 N 0.4765(3) 0.2100(3) 0.1993(3) 0.0298(7) Uani 1 1 d . . . . . N9 N 0.5270(3) 0.3837(3) 0.1606(2) 0.0272(7) Uani 1 1 d . . . . . N5 N 0.3349(3) 0.3525(3) 0.1985(2) 0.0270(7) Uani 1 1 d . . . . . N4 N 0.3017(3) 0.3804(2) 0.2891(2) 0.0249(6) Uani 1 1 d . . . . . N18 N 0.8544(11) -0.0770(9) 0.6863(5) 0.187(7) Uani 1 1 d . . . . . C1 C 0.3637(3) 0.4834(3) 0.4154(3) 0.0231(7) Uani 1 1 d . . . . . C2 C 0.3106(3) 0.2957(3) 0.4562(3) 0.0282(8) Uani 1 1 d . . . . . C3 C 0.5176(3) 0.3300(3) 0.4122(3) 0.0238(7) Uani 1 1 d . . . . . C34 C 0.5035(3) 0.2196(3) 0.6310(3) 0.0279(8) Uani 1 1 d . . . . . H34 H 0.475898 0.203036 0.585874 0.034 Uiso 1 1 calc R U . . . C33 C 0.4499(4) 0.2197(3) 0.7228(3) 0.0321(9) Uani 1 1 d . . . . . H33 H 0.380181 0.202542 0.751341 0.039 Uiso 1 1 calc R U . . . C32 C 0.6094(3) 0.2675(4) 0.6987(3) 0.0320(9) Uani 1 1 d . . . . . C31 C 0.7032(4) 0.3020(4) 0.7168(3) 0.0425(11) Uani 1 1 d . . . . . C30 C 0.8098(4) 0.2860(4) 0.6414(3) 0.0378(10) Uani 1 1 d . . . . . N15 N 0.9071(3) 0.2811(3) 0.6545(4) 0.0462(11) Uani 1 1 d . . . . . C35 C 0.9278(6) 0.2907(6) 0.7406(5) 0.070(2) Uani 1 1 d . . . . . H35A H 1.004920 0.284033 0.728860 0.105 Uiso 1 1 calc R U . . . H35B H 0.894537 0.356622 0.768586 0.105 Uiso 1 1 calc R U . . . H35C H 0.897444 0.237763 0.780780 0.105 Uiso 1 1 calc R U . . . C29 C 0.9854(4) 0.2644(4) 0.5711(5) 0.0521(15) Uani 1 1 d . . . . . H29 H 1.060376 0.257118 0.558787 0.062 Uiso 1 1 calc R U . . . C28 C 0.9342(4) 0.2604(3) 0.5098(4) 0.0446(12) Uani 1 1 d . . . . . H28 H 0.968533 0.250558 0.447129 0.054 Uiso 1 1 calc R U . . . C36 C 0.4922(5) 0.2556(4) 0.8635(3) 0.0450(12) Uani 1 1 d . . . . . H36A H 0.552211 0.278511 0.876281 0.067 Uiso 1 1 calc R U . . . H36B H 0.427570 0.303244 0.890236 0.067 Uiso 1 1 calc R U . . . H36C H 0.480822 0.189116 0.888828 0.067 Uiso 1 1 calc R U . . . C23 C 0.7736(5) 0.1268(4) 0.3551(4) 0.0505(14) Uani 1 1 d . . . . . N13 N 0.7854(5) 0.0232(3) 0.3437(5) 0.0654(16) Uani 1 1 d . . . . . C24 C 0.7674(5) -0.0173(4) 0.4264(6) 0.066(2) Uani 1 1 d . . . . . H24 H 0.770374 -0.086711 0.439613 0.079 Uiso 1 1 calc R U . . . C25 C 0.7439(4) 0.0622(4) 0.4875(5) 0.0597(18) Uani 1 1 d . . . . . H25 H 0.725898 0.056495 0.550513 0.072 Uiso 1 1 calc R U . . . C27 C 0.8157(7) -0.0366(5) 0.2576(7) 0.092(3) Uani 1 1 d . . . . . H27A H 0.824222 0.009395 0.207537 0.138 Uiso 1 1 calc R U . . . H27B H 0.883106 -0.080307 0.248799 0.138 Uiso 1 1 calc R U . . . H27C H 0.759513 -0.077680 0.260418 0.138 Uiso 1 1 calc R U . . . C22 C 0.7910(6) 0.1983(4) 0.2789(4) 0.0563(15) Uani 1 1 d . . . . . C21 C 0.8190(5) 0.3007(4) 0.2941(4) 0.0436(11) Uani 1 1 d . . . . . N11 N 0.8635(4) 0.3639(3) 0.2265(3) 0.0443(10) Uani 1 1 d . . . . . C26 C 0.9020(5) 0.3438(5) 0.1267(4) 0.0600(16) Uani 1 1 d . . . . . H26A H 0.929748 0.403406 0.095509 0.090 Uiso 1 1 calc R U . . . H26B H 0.958789 0.286576 0.111209 0.090 Uiso 1 1 calc R U . . . H26C H 0.842492 0.328524 0.108532 0.090 Uiso 1 1 calc R U . . . C20 C 0.8760(4) 0.4502(4) 0.2669(4) 0.0429(11) Uani 1 1 d . . . . . H20 H 0.905638 0.506886 0.236994 0.051 Uiso 1 1 calc R U . . . C19 C 0.8372(3) 0.4383(3) 0.3587(3) 0.0328(9) Uani 1 1 d . . . . . H19 H 0.834134 0.486614 0.402739 0.039 Uiso 1 1 calc R U . . . C9 C 0.4932(4) 0.1201(3) 0.3146(3) 0.0307(9) Uani 1 1 d . . . . . C12 C 0.4924(4) 0.0915(3) 0.4076(3) 0.0360(10) Uani 1 1 d . . . . . H12A H 0.516242 0.019383 0.408260 0.054 Uiso 1 1 calc R U . . . H12B H 0.540543 0.129511 0.424731 0.054 Uiso 1 1 calc R U . . . H12C H 0.419771 0.107110 0.450210 0.054 Uiso 1 1 calc R U . . . C10 C 0.5234(4) 0.0539(3) 0.2387(4) 0.0414(11) Uani 1 1 d . . . . . H10 H 0.546520 -0.016193 0.236868 0.050 Uiso 1 1 calc R U . . . C11 C 0.5123(4) 0.1127(3) 0.1670(4) 0.0400(10) Uani 1 1 d . . . . . B1 B 0.4532(4) 0.3077(4) 0.1502(3) 0.0293(9) Uani 1 1 d . . . . . H1 H 0.466172 0.292877 0.085545 0.035 Uiso 1 1 calc R U . . . C16 C 0.6071(4) 0.4280(3) 0.0980(3) 0.0313(9) Uani 1 1 d . . . . . C18 C 0.6391(5) 0.4066(4) -0.0026(3) 0.0467(12) Uani 1 1 d . . . . . H18A H 0.696895 0.445293 -0.034871 0.070 Uiso 1 1 calc R U . . . H18B H 0.663592 0.334754 -0.015134 0.070 Uiso 1 1 calc R U . . . H18C H 0.577447 0.426209 -0.022224 0.070 Uiso 1 1 calc R U . . . C15 C 0.6481(3) 0.4900(3) 0.1452(3) 0.0307(8) Uani 1 1 d . . . . . H15 H 0.702787 0.530894 0.119884 0.037 Uiso 1 1 calc R U . . . C14 C 0.5925(3) 0.4799(3) 0.2373(3) 0.0249(7) Uani 1 1 d . . . . . C17 C 0.6073(3) 0.5314(3) 0.3161(3) 0.0272(8) Uani 1 1 d . . . . . H17A H 0.664001 0.574229 0.293811 0.041 Uiso 1 1 calc R U . . . H17B H 0.540428 0.572756 0.350022 0.041 Uiso 1 1 calc R U . . . H17C H 0.626867 0.480550 0.355041 0.041 Uiso 1 1 calc R U . . . C6 C 0.2506(4) 0.3720(3) 0.1663(3) 0.0319(9) Uani 1 1 d . . . . . C5 C 0.1604(4) 0.4145(3) 0.2375(3) 0.0330(9) Uani 1 1 d . . . . . H5 H 0.091035 0.436399 0.235349 0.040 Uiso 1 1 calc R U . . . C4 C 0.1950(3) 0.4177(3) 0.3141(3) 0.0262(8) Uani 1 1 d . . . . . C7 C 0.1269(3) 0.4569(3) 0.4075(3) 0.0302(8) Uani 1 1 d . . . . . H7A H 0.053801 0.479277 0.408644 0.045 Uiso 1 1 calc R U . . . H7B H 0.126077 0.403200 0.450511 0.045 Uiso 1 1 calc R U . . . H7C H 0.156697 0.513547 0.423640 0.045 Uiso 1 1 calc R U . . . C8 C 0.2584(4) 0.3462(4) 0.0720(4) 0.0452(12) Uani 1 1 d . . . . . H8A H 0.189245 0.366801 0.063999 0.068 Uiso 1 1 calc R U . . . H8B H 0.312853 0.381582 0.029533 0.068 Uiso 1 1 calc R U . . . H8C H 0.278109 0.273569 0.061072 0.068 Uiso 1 1 calc R U . . . C13 C 0.5296(6) 0.0805(5) 0.0725(4) 0.0638(18) Uani 1 1 d . . . . . H13A H 0.555149 0.008387 0.064501 0.096 Uiso 1 1 calc R U . . . H13B H 0.462166 0.094231 0.060237 0.096 Uiso 1 1 calc R U . . . H13C H 0.582835 0.117919 0.030982 0.096 Uiso 1 1 calc R U . . . B2 B 0.1331(5) 0.2896(5) 0.8768(5) 0.0483(14) Uani 1 1 d . . . . . C39 C 0.9262(13) -0.1484(8) 0.7423(7) 0.134(5) Uani 1 1 d . . . . . H39 H 0.916779 -0.217400 0.746679 0.161 Uiso 1 1 calc R U . . . C37 C 0.9229(5) -0.0133(5) 0.6344(5) 0.0582(15) Uani 1 1 d . . . . . H37A H 0.936436 -0.027693 0.570928 0.087 Uiso 1 1 calc R U . . . H37B H 0.990496 -0.023910 0.646667 0.087 Uiso 1 1 calc R U . . . H37C H 0.890245 0.056585 0.649031 0.087 Uiso 1 1 calc R U . . . C38 C 0.7924(8) -0.1353(7) 0.6776(7) 0.107(4) Uani 1 1 d . . . . . H38A H 0.719698 -0.099489 0.694314 0.160 Uiso 1 1 calc R U . . . H38B H 0.793477 -0.192864 0.716556 0.160 Uiso 1 1 calc R U . . . H38C H 0.815491 -0.159108 0.615179 0.160 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co1 0.0196(3) 0.0186(2) 0.0231(3) 0.00085(17) -0.00944(19) -0.00615(18) Fe1 0.0181(3) 0.0180(3) 0.0364(3) 0.0028(2) -0.0087(2) -0.00588(19) F1 0.070(3) 0.103(4) 0.136(4) 0.040(3) -0.027(3) -0.054(3) F2 0.068(3) 0.183(6) 0.068(3) 0.022(3) -0.033(2) -0.022(3) F3 0.126(4) 0.060(3) 0.079(3) -0.002(2) 0.001(3) -0.010(3) F4 0.090(3) 0.083(3) 0.069(2) 0.011(2) -0.041(2) -0.031(2) N1 0.0187(14) 0.0232(14) 0.0267(15) 0.0010(12) -0.0096(12) -0.0042(11) N2 0.0303(19) 0.0327(18) 0.045(2) 0.0101(16) -0.0113(17) -0.0088(15) N3 0.0205(15) 0.0168(13) 0.0323(17) -0.0001(11) -0.0084(13) -0.0030(11) O2 0.061(3) 0.085(3) 0.040(2) -0.017(2) -0.0204(19) -0.017(2) O1 0.127(5) 0.058(3) 0.076(3) -0.018(2) -0.061(3) -0.003(3) N8 0.0207(15) 0.0190(13) 0.0283(16) 0.0002(11) -0.0069(12) -0.0043(11) O3 0.275(14) 0.101(6) 0.64(3) 0.049(11) -0.385(19) -0.037(7) N16 0.0196(15) 0.0341(17) 0.0268(16) -0.0019(13) -0.0080(13) -0.0055(13) N17 0.0311(19) 0.0335(18) 0.0299(18) 0.0012(14) -0.0064(15) -0.0026(14) N14 0.0244(17) 0.0301(17) 0.0373(19) -0.0052(14) -0.0061(15) -0.0110(13) N12 0.044(2) 0.0291(18) 0.062(3) 0.0160(17) -0.036(2) -0.0170(16) N10 0.041(2) 0.0251(16) 0.042(2) -0.0002(14) -0.0246(17) -0.0016(15) N6 0.0239(16) 0.0199(14) 0.0377(18) -0.0014(13) -0.0135(14) -0.0050(12) N7 0.0297(18) 0.0232(15) 0.0382(19) -0.0031(13) -0.0123(15) -0.0060(13) N9 0.0244(16) 0.0263(15) 0.0291(17) 0.0012(13) -0.0054(13) -0.0072(13) N5 0.0239(16) 0.0277(16) 0.0308(17) 0.0009(13) -0.0098(14) -0.0070(13) N4 0.0197(15) 0.0233(14) 0.0328(17) 0.0014(12) -0.0089(13) -0.0065(12) N18 0.315(14) 0.252(11) 0.066(4) 0.059(6) -0.079(7) -0.266(12) C1 0.0179(16) 0.0253(17) 0.0275(18) 0.0055(14) -0.0083(14) -0.0062(13) C2 0.027(2) 0.0222(17) 0.039(2) 0.0041(15) -0.0149(17) -0.0059(14) C3 0.0202(17) 0.0177(15) 0.0322(19) 0.0011(13) -0.0061(15) -0.0050(13) C34 0.0257(19) 0.0203(16) 0.037(2) 0.0001(15) -0.0091(16) -0.0052(14) C33 0.027(2) 0.0239(18) 0.041(2) 0.0033(16) -0.0056(17) -0.0013(15) C32 0.024(2) 0.048(2) 0.0218(18) -0.0053(16) -0.0049(15) -0.0024(17) C31 0.036(3) 0.060(3) 0.037(2) -0.008(2) -0.017(2) -0.010(2) C30 0.027(2) 0.044(2) 0.045(3) -0.011(2) -0.0141(19) -0.0066(18) N15 0.032(2) 0.042(2) 0.074(3) -0.006(2) -0.027(2) -0.0102(17) C35 0.062(4) 0.068(4) 0.105(6) -0.011(4) -0.058(4) -0.010(3) C29 0.025(2) 0.028(2) 0.100(5) 0.013(3) -0.017(3) -0.0041(18) C28 0.026(2) 0.027(2) 0.067(3) 0.000(2) 0.003(2) -0.0041(17) C36 0.048(3) 0.055(3) 0.027(2) 0.001(2) -0.008(2) -0.005(2) C23 0.070(4) 0.026(2) 0.078(4) 0.002(2) -0.052(3) -0.013(2) N13 0.065(3) 0.025(2) 0.126(5) -0.005(3) -0.059(4) -0.005(2) C24 0.038(3) 0.029(2) 0.138(6) 0.026(3) -0.039(4) -0.011(2) C25 0.036(3) 0.042(3) 0.116(5) 0.043(3) -0.042(3) -0.020(2) C27 0.088(6) 0.040(3) 0.166(9) -0.026(4) -0.066(6) -0.003(3) C22 0.083(5) 0.037(3) 0.062(4) -0.007(2) -0.046(3) 0.003(3) C21 0.055(3) 0.034(2) 0.045(3) 0.0017(19) -0.025(2) 0.002(2) N11 0.036(2) 0.048(2) 0.047(2) 0.0026(19) -0.0155(19) 0.0067(18) C26 0.054(4) 0.070(4) 0.047(3) -0.007(3) -0.014(3) 0.015(3) C20 0.019(2) 0.050(3) 0.054(3) 0.007(2) -0.005(2) -0.0060(19) C19 0.0209(19) 0.031(2) 0.047(3) 0.0022(17) -0.0121(18) -0.0010(15) C9 0.032(2) 0.0185(16) 0.051(3) 0.0030(16) -0.0247(19) -0.0065(15) C12 0.039(2) 0.0222(18) 0.058(3) 0.0065(18) -0.029(2) -0.0096(17) C10 0.051(3) 0.0187(18) 0.057(3) -0.0080(18) -0.023(2) 0.0001(18) C11 0.048(3) 0.028(2) 0.048(3) -0.0078(18) -0.020(2) -0.0060(19) B1 0.027(2) 0.028(2) 0.034(2) -0.0009(17) -0.0089(19) -0.0091(17) C16 0.029(2) 0.032(2) 0.033(2) 0.0054(16) -0.0087(17) -0.0113(16) C18 0.047(3) 0.053(3) 0.036(2) 0.001(2) -0.004(2) -0.023(2) C15 0.0251(19) 0.0285(19) 0.038(2) 0.0050(16) -0.0072(17) -0.0094(15) C14 0.0174(16) 0.0202(16) 0.037(2) 0.0027(14) -0.0081(15) -0.0048(13) C17 0.0230(18) 0.0209(16) 0.038(2) 0.0016(15) -0.0094(16) -0.0069(14) C6 0.031(2) 0.035(2) 0.036(2) 0.0036(17) -0.0157(18) -0.0119(17) C5 0.025(2) 0.040(2) 0.041(2) 0.0031(18) -0.0188(18) -0.0101(17) C4 0.0200(17) 0.0262(17) 0.036(2) 0.0008(15) -0.0125(16) -0.0088(14) C7 0.0199(18) 0.033(2) 0.037(2) -0.0025(16) -0.0067(16) -0.0057(15) C8 0.041(3) 0.059(3) 0.041(3) 0.000(2) -0.020(2) -0.010(2) C13 0.090(5) 0.041(3) 0.061(4) -0.025(3) -0.030(4) 0.006(3) B2 0.044(3) 0.051(3) 0.053(4) 0.006(3) -0.016(3) -0.018(3) C39 0.213(15) 0.081(7) 0.084(7) -0.008(5) -0.039(8) 0.041(8) C37 0.043(3) 0.056(3) 0.071(4) 0.019(3) -0.012(3) -0.013(3) C38 0.114(7) 0.103(7) 0.103(7) -0.017(5) -0.010(6) -0.079(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Co1 N16 88.30(13) 2_666 . ? N1 Co1 N14 89.21(13) 2_666 . ? N1 Co1 N12 177.83(15) 2_666 . ? N1 Co1 N10 91.07(14) 2_666 . ? N3 Co1 N1 90.69(12) . 2_666 ? N3 Co1 N16 89.98(13) . . ? N3 Co1 N14 177.18(14) . . ? N3 Co1 N12 89.99(14) . . ? N3 Co1 N10 88.18(14) . . ? N14 Co1 N16 87.20(14) . . ? N14 Co1 N10 94.64(15) . . ? N12 Co1 N16 93.77(16) . . ? N12 Co1 N14 90.22(15) . . ? N12 Co1 N10 86.88(16) . . ? N10 Co1 N16 178.05(14) . . ? N8 Fe1 N6 88.62(13) . . ? N8 Fe1 N4 88.21(13) . . ? N4 Fe1 N6 89.45(13) . . ? C1 Fe1 N8 91.97(14) . . ? C1 Fe1 N6 178.96(15) . . ? C1 Fe1 N4 91.42(15) . . ? C1 Fe1 C2 88.31(16) . . ? C2 Fe1 N8 179.62(16) . . ? C2 Fe1 N6 91.09(16) . . ? C2 Fe1 N4 92.04(15) . . ? C3 Fe1 N8 90.82(15) . . ? C3 Fe1 N6 90.10(15) . . ? C3 Fe1 N4 178.94(15) . . ? C3 Fe1 C1 89.03(16) . . ? C3 Fe1 C2 88.93(17) . . ? C1 N1 Co1 173.3(3) . 2_666 ? C3 N3 Co1 174.5(3) . . ? N9 N8 Fe1 118.1(2) . . ? C14 N8 Fe1 134.7(3) . . ? C14 N8 N9 107.2(3) . . ? C34 N16 Co1 126.7(3) . . ? C32 N16 Co1 124.6(3) . . ? C32 N16 C34 106.1(3) . . ? C33 N17 C32 107.4(4) . . ? C33 N17 C36 125.3(4) . . ? C32 N17 C36 127.3(4) . . ? C30 N14 Co1 125.2(3) . . ? C30 N14 C28 106.0(4) . . ? C28 N14 Co1 127.9(4) . . ? C23 N12 Co1 126.0(3) . . ? C23 N12 C25 106.6(5) . . ? C25 N12 Co1 126.3(5) . . ? C21 N10 Co1 124.5(3) . . ? C21 N10 C19 106.1(4) . . ? C19 N10 Co1 126.8(3) . . ? N7 N6 Fe1 117.8(2) . . ? C9 N6 Fe1 135.5(3) . . ? C9 N6 N7 106.6(3) . . ? N6 N7 B1 119.2(3) . . ? C11 N7 N6 110.4(4) . . ? C11 N7 B1 130.4(4) . . ? N8 N9 B1 118.8(3) . . ? C16 N9 N8 109.3(3) . . ? C16 N9 B1 131.8(4) . . ? N4 N5 B1 119.4(3) . . ? C6 N5 N4 110.1(3) . . ? C6 N5 B1 130.4(4) . . ? N5 N4 Fe1 117.6(2) . . ? C4 N4 Fe1 135.2(3) . . ? C4 N4 N5 107.2(3) . . ? C37 N18 C39 105.4(10) . . ? C38 N18 C39 102.7(11) . . ? C38 N18 C37 138.8(8) . . ? N1 C1 Fe1 179.0(4) . . ? N2 C2 Fe1 179.3(4) . . ? N3 C3 Fe1 178.3(4) . . ? N16 C34 H34 125.6 . . ? C33 C34 N16 108.7(4) . . ? C33 C34 H34 125.6 . . ? N17 C33 C34 107.5(4) . . ? N17 C33 H33 126.2 . . ? C34 C33 H33 126.2 . . ? N16 C32 N17 110.2(4) . . ? N16 C32 C31 125.6(4) . . ? N17 C32 C31 124.1(4) . . ? O2 C31 C32 122.0(5) . . ? O2 C31 C30 121.3(5) . . ? C32 C31 C30 116.7(4) . . ? N14 C30 C31 126.2(4) . . ? N14 C30 N15 110.1(4) . . ? N15 C30 C31 123.6(5) . . ? C30 N15 C35 128.0(5) . . ? C30 N15 C29 107.0(5) . . ? C29 N15 C35 125.0(5) . . ? N15 C35 H35A 109.5 . . ? N15 C35 H35B 109.5 . . ? N15 C35 H35C 109.5 . . ? H35A C35 H35B 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? N15 C29 H29 126.5 . . ? C28 C29 N15 107.0(4) . . ? C28 C29 H29 126.5 . . ? N14 C28 H28 125.1 . . ? C29 C28 N14 109.8(5) . . ? C29 C28 H28 125.1 . . ? N17 C36 H36A 109.5 . . ? N17 C36 H36B 109.5 . . ? N17 C36 H36C 109.5 . . ? H36A C36 H36B 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? N12 C23 N13 110.4(5) . . ? N12 C23 C22 126.1(4) . . ? N13 C23 C22 123.4(6) . . ? C23 N13 C27 127.9(6) . . ? C24 N13 C23 107.2(6) . . ? C24 N13 C27 124.8(6) . . ? N13 C24 H24 126.5 . . ? N13 C24 C25 107.1(5) . . ? C25 C24 H24 126.5 . . ? N12 C25 H25 125.7 . . ? C24 C25 N12 108.6(6) . . ? C24 C25 H25 125.7 . . ? N13 C27 H27A 109.5 . . ? N13 C27 H27B 109.5 . . ? N13 C27 H27C 109.5 . . ? H27A C27 H27B 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? O1 C22 C23 121.2(5) . . ? O1 C22 C21 121.6(6) . . ? C23 C22 C21 117.1(5) . . ? N10 C21 C22 125.3(5) . . ? N10 C21 N11 110.7(4) . . ? N11 C21 C22 124.1(5) . . ? C21 N11 C26 128.3(5) . . ? C21 N11 C20 107.0(4) . . ? C20 N11 C26 124.4(5) . . ? N11 C26 H26A 109.5 . . ? N11 C26 H26B 109.5 . . ? N11 C26 H26C 109.5 . . ? H26A C26 H26B 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? N11 C20 H20 126.2 . . ? C19 C20 N11 107.6(4) . . ? C19 C20 H20 126.2 . . ? N10 C19 H19 125.7 . . ? C20 C19 N10 108.6(4) . . ? C20 C19 H19 125.7 . . ? N6 C9 C12 124.8(4) . . ? N6 C9 C10 109.0(4) . . ? C10 C9 C12 126.2(4) . . ? C9 C12 H12A 109.5 . . ? C9 C12 H12B 109.5 . . ? C9 C12 H12C 109.5 . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C9 C10 H10 126.7 . . ? C11 C10 C9 106.6(4) . . ? C11 C10 H10 126.7 . . ? N7 C11 C10 107.4(4) . . ? N7 C11 C13 123.6(5) . . ? C10 C11 C13 129.0(5) . . ? N7 B1 H1 110.9 . . ? N9 B1 N7 107.9(4) . . ? N9 B1 H1 110.9 . . ? N5 B1 N7 107.5(3) . . ? N5 B1 N9 108.7(3) . . ? N5 B1 H1 110.9 . . ? N9 C16 C18 122.4(4) . . ? N9 C16 C15 107.4(4) . . ? C15 C16 C18 130.2(4) . . ? C16 C18 H18A 109.5 . . ? C16 C18 H18B 109.5 . . ? C16 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C16 C15 H15 126.5 . . ? C16 C15 C14 107.1(4) . . ? C14 C15 H15 126.5 . . ? N8 C14 C15 108.9(4) . . ? N8 C14 C17 123.4(3) . . ? C15 C14 C17 127.7(3) . . ? C14 C17 H17A 109.5 . . ? C14 C17 H17B 109.5 . . ? C14 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? N5 C6 C5 107.7(4) . . ? N5 C6 C8 123.6(4) . . ? C5 C6 C8 128.7(4) . . ? C6 C5 H5 127.0 . . ? C6 C5 C4 106.0(4) . . ? C4 C5 H5 127.0 . . ? N4 C4 C5 109.0(4) . . ? N4 C4 C7 124.7(4) . . ? C5 C4 C7 126.3(4) . . ? C4 C7 H7A 109.5 . . ? C4 C7 H7B 109.5 . . ? C4 C7 H7C 109.5 . . ? H7A C7 H7B 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C6 C8 H8A 109.5 . . ? C6 C8 H8B 109.5 . . ? C6 C8 H8C 109.5 . . ? H8A C8 H8B 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C11 C13 H13A 109.5 . . ? C11 C13 H13B 109.5 . . ? C11 C13 H13C 109.5 . . ? H13A C13 H13B 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? F1 B2 F2 108.7(6) . . ? F1 B2 F4 109.5(5) . . ? F2 B2 F4 106.9(5) . . ? F3 B2 F1 110.3(6) . . ? F3 B2 F2 111.3(6) . . ? F3 B2 F4 110.1(5) . . ? O3 C39 N18 129.6(11) . . ? O3 C39 H39 115.2 . . ? N18 C39 H39 115.2 . . ? N18 C37 H37A 109.5 . . ? N18 C37 H37B 109.5 . . ? N18 C37 H37C 109.5 . . ? H37A C37 H37B 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? N18 C38 H38A 109.5 . . ? N18 C38 H38B 109.5 . . ? N18 C38 H38C 109.5 . . ? H38A C38 H38B 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Co1 N1 1.997(3) 2_666 ? Co1 N3 1.993(3) . ? Co1 N16 2.031(3) . ? Co1 N14 2.015(4) . ? Co1 N12 2.014(4) . ? Co1 N10 2.030(4) . ? Fe1 N8 2.006(3) . ? Fe1 N6 2.015(3) . ? Fe1 N4 2.011(3) . ? Fe1 C1 1.892(4) . ? Fe1 C2 1.925(4) . ? Fe1 C3 1.887(4) . ? F1 B2 1.357(7) . ? F2 B2 1.364(8) . ? F3 B2 1.346(8) . ? F4 B2 1.390(8) . ? N1 C1 1.153(5) . ? N2 C2 1.145(6) . ? N3 C3 1.155(5) . ? O2 C31 1.204(6) . ? O1 C22 1.221(7) . ? N8 N9 1.372(5) . ? N8 C14 1.348(5) . ? O3 C39 1.231(16) . ? N16 C34 1.366(5) . ? N16 C32 1.339(5) . ? N17 C33 1.348(6) . ? N17 C32 1.353(5) . ? N17 C36 1.460(6) . ? N14 C30 1.331(6) . ? N14 C28 1.358(6) . ? N12 C23 1.305(7) . ? N12 C25 1.363(6) . ? N10 C21 1.337(6) . ? N10 C19 1.374(5) . ? N6 N7 1.365(5) . ? N6 C9 1.354(5) . ? N7 C11 1.349(6) . ? N7 B1 1.528(6) . ? N9 B1 1.526(5) . ? N9 C16 1.358(5) . ? N5 N4 1.369(5) . ? N5 B1 1.525(6) . ? N5 C6 1.353(5) . ? N4 C4 1.348(5) . ? N18 C39 1.675(17) . ? N18 C37 1.359(8) . ? N18 C38 1.229(9) . ? C34 H34 0.9300 . ? C34 C33 1.363(6) . ? C33 H33 0.9300 . ? C32 C31 1.477(6) . ? C31 C30 1.488(7) . ? C30 N15 1.352(6) . ? N15 C35 1.460(8) . ? N15 C29 1.360(8) . ? C35 H35A 0.9600 . ? C35 H35B 0.9600 . ? C35 H35C 0.9600 . ? C29 H29 0.9300 . ? C29 C28 1.340(9) . ? C28 H28 0.9300 . ? C36 H36A 0.9600 . ? C36 H36B 0.9600 . ? C36 H36C 0.9600 . ? C23 N13 1.360(6) . ? C23 C22 1.471(8) . ? N13 C24 1.337(9) . ? N13 C27 1.474(10) . ? C24 H24 0.9300 . ? C24 C25 1.361(10) . ? C25 H25 0.9300 . ? C27 H27A 0.9600 . ? C27 H27B 0.9600 . ? C27 H27C 0.9600 . ? C22 C21 1.486(7) . ? C21 N11 1.348(7) . ? N11 C26 1.479(7) . ? N11 C20 1.362(7) . ? C26 H26A 0.9600 . ? C26 H26B 0.9600 . ? C26 H26C 0.9600 . ? C20 H20 0.9300 . ? C20 C19 1.357(7) . ? C19 H19 0.9300 . ? C9 C12 1.481(6) . ? C9 C10 1.394(6) . ? C12 H12A 0.9600 . ? C12 H12B 0.9600 . ? C12 H12C 0.9600 . ? C10 H10 0.9300 . ? C10 C11 1.379(7) . ? C11 C13 1.471(7) . ? B1 H1 0.9800 . ? C16 C18 1.499(7) . ? C16 C15 1.376(6) . ? C18 H18A 0.9600 . ? C18 H18B 0.9600 . ? C18 H18C 0.9600 . ? C15 H15 0.9300 . ? C15 C14 1.385(6) . ? C14 C17 1.490(6) . ? C17 H17A 0.9600 . ? C17 H17B 0.9600 . ? C17 H17C 0.9600 . ? C6 C5 1.385(7) . ? C6 C8 1.478(7) . ? C5 H5 0.9300 . ? C5 C4 1.410(6) . ? C4 C7 1.489(6) . ? C7 H7A 0.9600 . ? C7 H7B 0.9600 . ? C7 H7C 0.9600 . ? C8 H8A 0.9600 . ? C8 H8B 0.9600 . ? C8 H8C 0.9600 . ? C13 H13A 0.9600 . ? C13 H13B 0.9600 . ? C13 H13C 0.9600 . ? C39 H39 0.9300 . ? C37 H37A 0.9600 . ? C37 H37B 0.9600 . ? C37 H37C 0.9600 . ? C38 H38A 0.9600 . ? C38 H38B 0.9600 . ? C38 H38C 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Co1 N16 C34 C33 -164.2(3) . . . . ? Co1 N16 C32 N17 164.9(3) . . . . ? Co1 N16 C32 C31 -16.4(7) . . . . ? Co1 N14 C30 C31 10.7(7) . . . . ? Co1 N14 C30 N15 -170.3(3) . . . . ? Co1 N14 C28 C29 170.3(3) . . . . ? Co1 N12 C23 N13 -171.1(4) . . . . ? Co1 N12 C23 C22 12.4(9) . . . . ? Co1 N12 C25 C24 171.4(3) . . . . ? Co1 N10 C21 C22 -15.6(7) . . . . ? Co1 N10 C21 N11 164.0(3) . . . . ? Co1 N10 C19 C20 -164.1(3) . . . . ? Fe1 N8 N9 B1 1.8(4) . . . . ? Fe1 N8 N9 C16 -176.5(3) . . . . ? Fe1 N8 C14 C15 176.7(3) . . . . ? Fe1 N8 C14 C17 -4.0(6) . . . . ? Fe1 N6 N7 C11 179.6(3) . . . . ? Fe1 N6 N7 B1 1.4(5) . . . . ? Fe1 N6 C9 C12 0.5(7) . . . . ? Fe1 N6 C9 C10 -179.6(3) . . . . ? Fe1 N4 C4 C5 -178.1(3) . . . . ? Fe1 N4 C4 C7 2.7(6) . . . . ? O2 C31 C30 N14 -160.8(5) . . . . ? O2 C31 C30 N15 20.3(9) . . . . ? O1 C22 C21 N10 163.8(6) . . . . ? O1 C22 C21 N11 -15.8(10) . . . . ? N8 N9 B1 N7 -59.6(5) . . . . ? N8 N9 B1 N5 56.7(5) . . . . ? N8 N9 C16 C18 177.9(4) . . . . ? N8 N9 C16 C15 -1.4(5) . . . . ? N16 C34 C33 N17 0.9(5) . . . . ? N16 C32 C31 O2 164.1(5) . . . . ? N16 C32 C31 C30 -18.0(8) . . . . ? N17 C32 C31 O2 -17.2(9) . . . . ? N17 C32 C31 C30 160.7(5) . . . . ? N14 C30 N15 C35 -179.5(5) . . . . ? N14 C30 N15 C29 0.1(6) . . . . ? N12 C23 N13 C24 1.2(7) . . . . ? N12 C23 N13 C27 -177.0(6) . . . . ? N12 C23 C22 O1 -161.7(6) . . . . ? N12 C23 C22 C21 19.9(10) . . . . ? N10 C21 N11 C26 174.5(5) . . . . ? N10 C21 N11 C20 -0.4(6) . . . . ? N6 N7 C11 C10 0.0(5) . . . . ? N6 N7 C11 C13 177.6(5) . . . . ? N6 N7 B1 N9 57.7(5) . . . . ? N6 N7 B1 N5 -59.4(5) . . . . ? N6 C9 C10 C11 0.3(6) . . . . ? N7 N6 C9 C12 179.8(4) . . . . ? N7 N6 C9 C10 -0.3(5) . . . . ? N9 N8 C14 C15 -0.1(4) . . . . ? N9 N8 C14 C17 179.2(3) . . . . ? N9 C16 C15 C14 1.3(5) . . . . ? N5 N4 C4 C5 -0.7(4) . . . . ? N5 N4 C4 C7 -180.0(3) . . . . ? N5 C6 C5 C4 -0.9(5) . . . . ? N4 N5 B1 N7 60.2(4) . . . . ? N4 N5 B1 N9 -56.3(5) . . . . ? N4 N5 C6 C5 0.4(4) . . . . ? N4 N5 C6 C8 -177.2(4) . . . . ? C34 N16 C32 N17 2.0(5) . . . . ? C34 N16 C32 C31 -179.2(5) . . . . ? C33 N17 C32 N16 -1.5(5) . . . . ? C33 N17 C32 C31 179.7(5) . . . . ? C32 N16 C34 C33 -1.7(5) . . . . ? C32 N17 C33 C34 0.3(5) . . . . ? C32 C31 C30 N14 21.3(8) . . . . ? C32 C31 C30 N15 -157.6(5) . . . . ? C31 C30 N15 C35 -0.5(9) . . . . ? C31 C30 N15 C29 179.1(5) . . . . ? C30 N14 C28 C29 0.9(5) . . . . ? C30 N15 C29 C28 0.5(6) . . . . ? N15 C29 C28 N14 -0.9(5) . . . . ? C35 N15 C29 C28 -180.0(5) . . . . ? C28 N14 C30 C31 -179.6(5) . . . . ? C28 N14 C30 N15 -0.6(5) . . . . ? C36 N17 C33 C34 -177.3(4) . . . . ? C36 N17 C32 N16 176.1(4) . . . . ? C36 N17 C32 C31 -2.7(8) . . . . ? C23 N12 C25 C24 2.6(6) . . . . ? C23 N13 C24 C25 0.5(7) . . . . ? C23 C22 C21 N10 -17.8(9) . . . . ? C23 C22 C21 N11 162.7(6) . . . . ? N13 C23 C22 O1 22.3(10) . . . . ? N13 C23 C22 C21 -156.2(6) . . . . ? N13 C24 C25 N12 -1.9(6) . . . . ? C25 N12 C23 N13 -2.3(6) . . . . ? C25 N12 C23 C22 -178.8(6) . . . . ? C27 N13 C24 C25 178.8(6) . . . . ? C22 C23 N13 C24 177.8(6) . . . . ? C22 C23 N13 C27 -0.4(10) . . . . ? C22 C21 N11 C26 -5.8(9) . . . . ? C22 C21 N11 C20 179.3(5) . . . . ? C21 N10 C19 C20 -2.0(5) . . . . ? C21 N11 C20 C19 -0.9(6) . . . . ? N11 C20 C19 N10 1.8(5) . . . . ? C26 N11 C20 C19 -176.0(5) . . . . ? C19 N10 C21 C22 -178.2(5) . . . . ? C19 N10 C21 N11 1.4(5) . . . . ? C9 N6 N7 C11 0.2(5) . . . . ? C9 N6 N7 B1 -178.0(3) . . . . ? C9 C10 C11 N7 -0.2(6) . . . . ? C9 C10 C11 C13 -177.5(6) . . . . ? C12 C9 C10 C11 -179.8(4) . . . . ? C11 N7 B1 N9 -120.1(5) . . . . ? C11 N7 B1 N5 122.8(5) . . . . ? B1 N7 C11 C10 177.9(4) . . . . ? B1 N7 C11 C13 -4.5(8) . . . . ? B1 N9 C16 C18 0.0(7) . . . . ? B1 N9 C16 C15 -179.4(4) . . . . ? B1 N5 N4 Fe1 -2.5(4) . . . . ? B1 N5 N4 C4 179.6(3) . . . . ? B1 N5 C6 C5 -178.9(4) . . . . ? B1 N5 C6 C8 3.5(7) . . . . ? C16 N9 B1 N7 118.1(5) . . . . ? C16 N9 B1 N5 -125.5(5) . . . . ? C16 C15 C14 N8 -0.8(5) . . . . ? C16 C15 C14 C17 180.0(4) . . . . ? C18 C16 C15 C14 -177.9(5) . . . . ? C14 N8 N9 B1 179.2(3) . . . . ? C14 N8 N9 C16 1.0(4) . . . . ? C6 N5 N4 Fe1 178.1(3) . . . . ? C6 N5 N4 C4 0.2(4) . . . . ? C6 N5 B1 N7 -120.5(4) . . . . ? C6 N5 B1 N9 123.0(4) . . . . ? C6 C5 C4 N4 1.0(5) . . . . ? C6 C5 C4 C7 -179.8(4) . . . . ? C8 C6 C5 C4 176.6(5) . . . . ? C37 N18 C39 O3 41(2) . . . . ? C38 N18 C39 O3 -169.6(18) . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.000 0.000 0.000 321.3 84.2 '2 DMF'