#------------------------------------------------------------------------------ #$Date: 2021-04-25 03:49:09 +0300 (Sun, 25 Apr 2021) $ #$Revision: 264504 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/20/1562058.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1562058 loop_ _publ_author_name 'Guan, Mingming' 'Wang, Shiyu' 'Luo, Yao' 'Cao, Weidi' 'Liu, Xiaohua' 'Feng, Xiaoming' _publ_section_title ; Catalytic asymmetric addition of thiols to silyl glyoxylates for synthesis of multi-hetero-atom substituted carbon stereocenter ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC01096D _journal_year 2021 _chemical_absolute_configuration syn _chemical_formula_moiety 'C39 H56 N4 O4 Y, 3(C F3 O3 S), C4 H10 O, 3(C H4 O)' _chemical_formula_sum 'C49 H78 F9 N4 O17 S3 Y' _chemical_formula_weight 1351.24 _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2021-02-24 deposited with the CCDC. 2021-04-23 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 106.2310(10) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 11.9751(5) _cell_length_b 20.8149(9) _cell_length_c 12.9319(6) _cell_measurement_reflns_used 9839 _cell_measurement_temperature 140(2) _cell_measurement_theta_max 80.63 _cell_measurement_theta_min 3.56 _cell_volume 3094.9(2) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX3' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT (Sheldrick 2008)' _diffrn_ambient_temperature 140(2) _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device_type 'Bruker D8 Venture Photon II' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0393 _diffrn_reflns_av_unetI/netI 0.0229 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 26 _diffrn_reflns_limit_k_min -26 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 127367 _diffrn_reflns_point_group_measured_fraction_full 0.989 _diffrn_reflns_point_group_measured_fraction_max 0.975 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 80.719 _diffrn_reflns_theta_min 3.560 _exptl_absorpt_coefficient_mu 3.102 _exptl_absorpt_correction_T_max 0.8979 _exptl_absorpt_correction_T_min 0.6424 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details 'SADABS (Krause et al., 2015)' _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.450 _exptl_crystal_description block _exptl_crystal_F_000 1408 _exptl_crystal_size_max 0.389 _exptl_crystal_size_mid 0.283 _exptl_crystal_size_min 0.163 _refine_diff_density_max 0.632 _refine_diff_density_min -0.513 _refine_diff_density_rms 0.059 _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack 0.062(8) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.050 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 776 _refine_ls_number_reflns 13286 _refine_ls_number_restraints 8 _refine_ls_restrained_S_all 1.051 _refine_ls_R_factor_all 0.0267 _refine_ls_R_factor_gt 0.0265 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0407P)^2^+1.3804P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0701 _refine_ls_wR_factor_ref 0.0702 _reflns_Friedel_coverage 0.910 _reflns_Friedel_fraction_full 0.980 _reflns_Friedel_fraction_max 0.956 _reflns_number_gt 13233 _reflns_number_total 13286 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1sc01096d2.cif _cod_data_source_block loy015 _cod_original_sg_symbol_H-M 'P 21' _cod_database_code 1562058 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.378 _shelx_estimated_absorpt_t_max 0.632 _shelx_res_file ; TITL loy015.res in P2(1) loy015.res created by SHELXL-2018/3 at 11:37:15 on 08-Aug-2020 REM Old TITL loy015 in P2(1) REM SHELXT solution in P2(1) REM R1 0.108, Rweak 0.047, Alpha 0.008, Orientation as input REM Flack x = 0.117 ( 0.003 ) from Parsons' quotients REM Formula found by SHELXT: C46 N5 O13 F12 S3 Y CELL 1.54178 11.9751 20.8149 12.9319 90.000 106.231 90.000 ZERR 2.000 0.0005 0.0009 0.0006 0.000 0.001 0.000 LATT -1 SYMM -X, 1/2+Y, -Z SFAC C H N O F S Y UNIT 98 156 8 34 18 6 2 TEMP -133.160 SIZE 0.163 0.283 0.389 L.S. 10 ACTA CONF TWIN EQIV $1 1-X, 1/2+Y, 2-Z DFIX 0.90 0.02 N2 H2N N4 H4N DFIX 0.85 0.02 O10S H10O O11S H11O O12S H12O DFIX 1.87 0.05 O7S_$1 H12O DFIX 1.53 0.005 C4S C5S WGHT 0.040700 1.380400 BASF 0.06184 FVAR 0.13281 Y 7 0.446190 0.448593 0.487739 11.00000 0.01771 0.01214 = 0.01703 0.00014 0.00550 -0.00051 O1 4 0.520879 0.524401 0.408164 11.00000 0.01825 0.01481 = 0.02214 0.00696 0.00543 0.00153 O2 4 0.309501 0.469699 0.321664 11.00000 0.02102 0.02234 = 0.01812 0.00257 0.00317 -0.00294 O3 4 0.327167 0.520733 0.530993 11.00000 0.01957 0.01761 = 0.02036 -0.00471 0.00618 0.00068 O4 4 0.552917 0.499231 0.643996 11.00000 0.01950 0.02182 = 0.01920 -0.00446 0.00296 0.00209 N1 3 0.470936 0.573461 0.339167 11.00000 0.01671 0.01580 = 0.02047 0.00432 0.00770 0.00106 N2 3 0.218028 0.497705 0.151231 11.00000 0.01765 0.02526 = 0.01828 0.00250 0.00337 -0.00007 H2N 2 0.209169 0.522160 0.095089 11.00000 0.02826 N3 3 0.328792 0.569828 0.603757 11.00000 0.01512 0.01820 = 0.01900 -0.00130 0.00503 -0.00073 N4 3 0.616025 0.559948 0.793039 11.00000 0.01596 0.02637 = 0.02157 -0.00805 0.00266 0.00156 H4N 2 0.597906 0.586697 0.837984 11.00000 0.02350 C1 1 0.392390 0.615090 0.383937 11.00000 0.01836 0.02053 = 0.02494 0.00049 0.00809 0.00364 AFIX 23 H1A 2 0.318749 0.591761 0.377676 11.00000 -1.20000 H1B 2 0.373410 0.654592 0.339869 11.00000 -1.20000 AFIX 0 C2 1 0.445679 0.633979 0.501229 11.00000 0.02277 0.01509 = 0.02757 -0.00115 0.00876 -0.00193 AFIX 23 H2A 2 0.507348 0.602897 0.535936 11.00000 -1.20000 H2B 2 0.481700 0.677025 0.504687 11.00000 -1.20000 AFIX 0 C3 1 0.353318 0.634999 0.561372 11.00000 0.02470 0.01829 = 0.02432 0.00072 0.00935 0.00066 AFIX 23 H3A 2 0.280142 0.651860 0.512581 11.00000 -1.20000 H3B 2 0.378286 0.665078 0.622824 11.00000 -1.20000 AFIX 0 C11 1 0.567352 0.610570 0.307659 11.00000 0.02025 0.01850 = 0.02735 0.00420 0.01058 -0.00031 AFIX 13 H11 2 0.537525 0.653107 0.275676 11.00000 -1.20000 AFIX 0 C12 1 0.678888 0.619481 0.399420 11.00000 0.01911 0.02189 = 0.03207 -0.00172 0.00719 -0.00311 AFIX 23 H12A 2 0.676510 0.593633 0.463034 11.00000 -1.20000 H12B 2 0.690465 0.665204 0.420810 11.00000 -1.20000 AFIX 0 C13 1 0.775847 0.595812 0.352105 11.00000 0.02223 0.04745 = 0.05429 -0.00840 0.01152 0.00029 AFIX 23 H13A 2 0.801104 0.630348 0.311037 11.00000 -1.20000 H13B 2 0.843910 0.580514 0.409626 11.00000 -1.20000 AFIX 0 C14 1 0.718901 0.540672 0.278034 11.00000 0.02095 0.05139 = 0.05670 -0.02091 0.01189 0.00399 AFIX 23 H14A 2 0.714289 0.501406 0.319845 11.00000 -1.20000 H14B 2 0.762254 0.530823 0.225040 11.00000 -1.20000 AFIX 0 C15 1 0.596419 0.567177 0.221859 11.00000 0.02515 0.03445 = 0.02935 -0.00192 0.01442 -0.00362 AFIX 13 H15 2 0.599516 0.593721 0.158267 11.00000 -1.20000 AFIX 0 C16 1 0.497930 0.517894 0.187703 11.00000 0.02302 0.03060 = 0.02677 -0.00525 0.01287 -0.00113 AFIX 23 H16A 2 0.471201 0.513390 0.108374 11.00000 -1.20000 H16B 2 0.522636 0.475336 0.220286 11.00000 -1.20000 AFIX 0 C17 1 0.403096 0.546985 0.231353 11.00000 0.01963 0.01981 = 0.01776 0.00263 0.00743 -0.00011 AFIX 13 H17 2 0.366938 0.583739 0.183963 11.00000 -1.20000 AFIX 0 C18 1 0.306706 0.501205 0.240010 11.00000 0.01690 0.01825 = 0.02041 -0.00148 0.00717 0.00104 C21 1 0.123855 0.453151 0.145556 11.00000 0.01815 0.02590 = 0.01815 0.00155 0.00210 -0.00250 C22 1 0.133645 0.390529 0.110714 11.00000 0.02572 0.02805 = 0.02390 -0.00043 0.00396 0.00090 C23 1 0.044069 0.347825 0.108356 11.00000 0.03629 0.02871 = 0.03533 -0.00424 0.00173 -0.00544 AFIX 43 H23 2 0.047830 0.305316 0.082801 11.00000 -1.20000 AFIX 0 C24 1 -0.050817 0.366293 0.142747 11.00000 0.02986 0.04071 = 0.03927 0.00323 0.00458 -0.01329 AFIX 43 H24 2 -0.111023 0.336359 0.141651 11.00000 -1.20000 AFIX 0 C25 1 -0.057843 0.428455 0.178744 11.00000 0.01951 0.04675 = 0.03101 -0.00077 0.00724 -0.00372 AFIX 43 H25 2 -0.122679 0.440684 0.203025 11.00000 -1.20000 AFIX 0 C26 1 0.029036 0.473339 0.179814 11.00000 0.01878 0.03433 = 0.02359 -0.00121 0.00262 0.00099 C27 1 0.239952 0.369100 0.078819 11.00000 0.03420 0.02991 = 0.04474 -0.00711 0.01272 0.00530 AFIX 23 H27A 2 0.243944 0.321600 0.081432 11.00000 -1.20000 H27B 2 0.310156 0.385800 0.132232 11.00000 -1.20000 AFIX 0 C28 1 0.241639 0.391245 -0.032784 11.00000 0.05407 0.07285 = 0.04908 -0.00888 0.02536 0.01488 AFIX 137 H28A 2 0.313075 0.376117 -0.047700 11.00000 -1.50000 H28B 2 0.238928 0.438278 -0.035944 11.00000 -1.50000 H28C 2 0.174002 0.373611 -0.086635 11.00000 -1.50000 AFIX 0 C29 1 0.018417 0.541389 0.216298 11.00000 0.02380 0.04035 = 0.03475 -0.00972 0.00982 0.00170 AFIX 23 H29A 2 0.097058 0.558540 0.251137 11.00000 -1.20000 H29B 2 -0.025756 0.541292 0.270578 11.00000 -1.20000 AFIX 0 C30 1 -0.042805 0.585433 0.122846 11.00000 0.06022 0.03800 = 0.04974 -0.00069 0.01389 0.01309 AFIX 137 H30A 2 -0.051779 0.628341 0.150679 11.00000 -1.50000 H30B 2 -0.119612 0.567802 0.086411 11.00000 -1.50000 H30C 2 0.003782 0.588354 0.071618 11.00000 -1.50000 AFIX 0 C31 1 0.211505 0.572850 0.630611 11.00000 0.01640 0.02600 = 0.02334 -0.00147 0.00863 0.00152 AFIX 13 H31 2 0.203282 0.614852 0.665303 11.00000 -1.20000 AFIX 0 C32 1 0.106937 0.561350 0.532754 11.00000 0.01943 0.03991 = 0.02727 -0.00017 0.00435 0.00237 AFIX 23 H32A 2 0.132552 0.548513 0.469276 11.00000 -1.20000 H32B 2 0.058460 0.600510 0.514731 11.00000 -1.20000 AFIX 0 C33 1 0.039215 0.506599 0.567970 11.00000 0.01952 0.04732 = 0.03469 -0.00509 0.00756 -0.00663 AFIX 23 H33A 2 -0.016950 0.523816 0.604413 11.00000 -1.20000 H33B 2 -0.003406 0.480546 0.505302 11.00000 -1.20000 AFIX 0 C34 1 0.133614 0.466487 0.646072 11.00000 0.02749 0.03259 = 0.03567 -0.00221 0.01205 -0.01038 AFIX 23 H34A 2 0.100230 0.440178 0.693880 11.00000 -1.20000 H34B 2 0.173454 0.437868 0.606544 11.00000 -1.20000 AFIX 0 C35 1 0.217160 0.517371 0.710328 11.00000 0.02045 0.02925 = 0.02472 -0.00011 0.01010 -0.00231 AFIX 13 H35 2 0.188393 0.532649 0.771589 11.00000 -1.20000 AFIX 0 C36 1 0.346605 0.499404 0.752553 11.00000 0.02343 0.02703 = 0.02381 0.00546 0.00798 -0.00045 AFIX 23 H36A 2 0.370917 0.496719 0.832158 11.00000 -1.20000 H36B 2 0.362310 0.457689 0.722596 11.00000 -1.20000 AFIX 0 C37 1 0.409838 0.553993 0.713484 11.00000 0.01875 0.02155 = 0.01617 -0.00147 0.00501 -0.00015 AFIX 13 H37 2 0.413884 0.591892 0.761920 11.00000 -1.20000 AFIX 0 C38 1 0.532505 0.536325 0.711942 11.00000 0.01926 0.01744 = 0.01895 0.00071 0.00522 0.00019 C41 1 0.736402 0.540868 0.814051 11.00000 0.01705 0.03222 = 0.01994 -0.00568 0.00402 0.00208 C42 1 0.770176 0.481033 0.862671 11.00000 0.02328 0.03352 = 0.02101 -0.00223 0.00419 0.00164 C43 1 0.887634 0.465161 0.884201 11.00000 0.02559 0.04689 = 0.02558 0.00243 0.00372 0.01101 AFIX 43 H43 2 0.914138 0.424944 0.916574 11.00000 -1.20000 AFIX 0 C44 1 0.966135 0.506840 0.859323 11.00000 0.01915 0.05770 = 0.03081 -0.00229 0.00396 0.00575 AFIX 43 H44 2 1.045975 0.495326 0.876230 11.00000 -1.20000 AFIX 0 C45 1 0.929938 0.564864 0.810309 11.00000 0.02074 0.04901 = 0.03235 -0.00442 0.00835 -0.00445 AFIX 43 H45 2 0.984941 0.592818 0.793232 11.00000 -1.20000 AFIX 0 C46 1 0.813020 0.583082 0.785396 11.00000 0.02204 0.03528 = 0.02673 -0.00612 0.00646 -0.00184 C47 1 0.684744 0.435574 0.889451 11.00000 0.02991 0.03628 = 0.03021 0.00626 0.00744 0.00057 AFIX 23 H47A 2 0.721330 0.392663 0.904577 11.00000 -1.20000 H47B 2 0.616342 0.431416 0.825734 11.00000 -1.20000 AFIX 0 C48 1 0.643038 0.456438 0.986190 11.00000 0.03333 0.06310 = 0.03029 0.00676 0.01169 -0.00159 AFIX 137 H48A 2 0.586530 0.425188 0.997807 11.00000 -1.50000 H48B 2 0.606307 0.498823 0.971977 11.00000 -1.50000 H48C 2 0.709626 0.458634 1.050597 11.00000 -1.50000 AFIX 0 C49 1 0.769299 0.645437 0.728194 11.00000 0.03784 0.03684 = 0.05001 0.00445 0.00974 -0.00032 AFIX 23 H49A 2 0.702649 0.635169 0.665380 11.00000 -1.20000 H49B 2 0.739014 0.672169 0.777663 11.00000 -1.20000 AFIX 0 C50 1 0.850692 0.684479 0.690135 11.00000 0.06255 0.07827 = 0.13576 0.04558 0.01348 -0.02014 AFIX 137 H50A 2 0.807898 0.717778 0.641344 11.00000 -1.50000 H50B 2 0.892564 0.657177 0.651721 11.00000 -1.50000 H50C 2 0.906385 0.704754 0.751730 11.00000 -1.50000 AFIX 0 S1S 6 0.474278 0.301493 0.652087 11.00000 0.05462 0.01722 = 0.03234 0.00551 0.02446 0.00531 S2S 6 0.521318 0.305953 0.349411 11.00000 0.03366 0.01797 = 0.02904 -0.00385 0.01027 0.00137 S3S 6 0.718716 0.136792 1.040759 11.00000 0.04762 0.02494 = 0.02549 -0.00142 0.01350 0.00213 F1S 5 0.465831 0.334475 0.845717 11.00000 0.08376 0.05654 = 0.03830 -0.00742 0.03194 -0.00521 F2S 5 0.379558 0.245312 0.787342 11.00000 0.11704 0.02550 = 0.06844 0.00896 0.06771 0.00236 F3S 5 0.300216 0.335218 0.726981 11.00000 0.06188 0.04455 = 0.07083 0.00573 0.04088 0.00591 F4S 5 0.649821 0.274092 0.225582 11.00000 0.07151 0.04874 = 0.06663 -0.00337 0.04093 0.02466 F5S 5 0.672282 0.372022 0.280192 11.00000 0.04565 0.04662 = 0.07032 0.00249 0.02992 -0.00636 F6S 5 0.520007 0.344645 0.155777 11.00000 0.05657 0.05957 = 0.03695 0.01114 0.02078 0.01309 F7S 5 0.782457 0.186438 0.882381 11.00000 0.09092 0.09347 = 0.04553 0.01584 0.02477 -0.02944 F8S 5 0.902348 0.202873 1.037928 11.00000 0.06397 0.09196 = 0.09951 -0.00086 -0.00474 -0.04417 F9S 5 0.740365 0.256488 0.991309 11.00000 0.13340 0.02930 = 0.08159 0.01294 -0.00660 -0.01231 O1S 4 0.488896 0.369513 0.631166 11.00000 0.04115 0.01976 = 0.02755 0.00670 0.01190 -0.00007 O2S 4 0.390068 0.270257 0.565163 11.00000 0.07090 0.02194 = 0.04229 -0.00264 0.02494 -0.00808 O3S 4 0.578203 0.266717 0.697666 11.00000 0.07106 0.03564 = 0.04836 0.01583 0.03235 0.02346 O4S 4 0.462134 0.365409 0.360745 11.00000 0.03161 0.02616 = 0.02886 -0.00767 0.00873 0.00316 O5S 4 0.616475 0.291544 0.442762 11.00000 0.04475 0.02388 = 0.03572 -0.00150 0.00438 0.00626 O6S 4 0.446592 0.253663 0.303852 11.00000 0.05200 0.02880 = 0.04071 -0.00888 0.01259 -0.00923 O7S 4 0.600370 0.140816 0.971971 11.00000 0.03873 0.05769 = 0.04866 -0.00903 0.01676 0.00079 O8S 4 0.778020 0.079818 1.023361 11.00000 0.05623 0.03469 = 0.03074 -0.00765 0.00923 0.00919 O9S 4 0.734365 0.153946 1.150396 11.00000 0.10693 0.03877 = 0.02498 -0.00106 0.01837 0.01921 C1S 1 0.400992 0.304084 0.758873 11.00000 0.07119 0.02144 = 0.04149 0.00177 0.03385 0.00170 C2S 1 0.595099 0.325309 0.246752 11.00000 0.03801 0.03302 = 0.04094 -0.00007 0.01631 0.00915 C3S 1 0.788794 0.199800 0.984733 11.00000 0.06460 0.04364 = 0.04716 0.00443 0.00618 -0.02007 C4S 1 0.075735 0.756134 0.587472 11.00000 0.10248 0.11175 = 0.10578 -0.00203 0.03014 0.04536 AFIX 33 H4SA 2 0.072962 0.794286 0.631091 11.00000 -1.50000 H4SB 2 0.006195 0.729920 0.581301 11.00000 -1.50000 H4SC 2 0.145271 0.730910 0.621965 11.00000 -1.50000 AFIX 0 C5S 1 0.079992 0.776519 0.477094 11.00000 0.11049 0.09083 = 0.11139 -0.01324 0.02676 0.04014 AFIX 23 H5SA 2 0.010260 0.802320 0.441954 11.00000 -1.20000 H5SB 2 0.149751 0.803313 0.482740 11.00000 -1.20000 AFIX 0 C6S 1 0.121258 0.740337 0.321236 11.00000 0.17712 0.15175 = 0.09172 0.01788 0.05331 0.07084 AFIX 23 H6SA 2 0.138350 0.700654 0.286289 11.00000 -1.20000 H6SB 2 0.194385 0.765248 0.345221 11.00000 -1.20000 AFIX 0 C7S 1 0.034109 0.779102 0.239554 11.00000 0.27501 0.14295 = 0.08401 -0.00668 0.00980 0.12923 AFIX 33 H7SA 2 0.065213 0.789105 0.178911 11.00000 -1.50000 H7SB 2 -0.038040 0.754443 0.213618 11.00000 -1.50000 H7SC 2 0.018085 0.819140 0.272644 11.00000 -1.50000 AFIX 0 O10S 4 0.280590 0.381246 0.475529 11.00000 0.03031 0.02376 = 0.03475 -0.00052 0.01018 -0.00980 H10O 2 0.306286 0.344485 0.496844 11.00000 0.04104 O11S 4 0.646176 0.417289 0.517446 11.00000 0.02268 0.01927 = 0.03386 -0.00372 0.00520 0.00187 H11O 2 0.658830 0.378853 0.512370 11.00000 0.03728 O12S 4 0.589263 0.642033 0.951125 11.00000 0.05725 0.04840 = 0.05955 -0.02351 0.03498 -0.01340 H12O 2 0.516839 0.644422 0.949475 11.00000 0.12448 O13S 4 0.083865 0.722337 0.416638 11.00000 0.11088 0.06840 = 0.10607 0.00212 0.03792 0.01891 C10S 1 0.164571 0.381751 0.407916 11.00000 0.03730 0.05954 = 0.03591 0.00129 0.00668 -0.02047 AFIX 137 H10A 2 0.115031 0.356386 0.441310 11.00000 -1.50000 H10B 2 0.162580 0.363131 0.337820 11.00000 -1.50000 H10C 2 0.136020 0.426084 0.397948 11.00000 -1.50000 AFIX 0 C11S 1 0.753286 0.443964 0.574266 11.00000 0.02168 0.06012 = 0.09089 -0.04654 0.00918 -0.00317 AFIX 137 H11B 2 0.811859 0.434014 0.536755 11.00000 -1.50000 H11C 2 0.777552 0.425853 0.647087 11.00000 -1.50000 H11D 2 0.745298 0.490666 0.578664 11.00000 -1.50000 AFIX 0 C12S 1 0.650767 0.698977 0.971737 11.00000 0.11981 0.06281 = 0.06526 -0.02933 0.05326 -0.04514 AFIX 137 H12C 2 0.611321 0.728774 1.008566 11.00000 -1.50000 H12D 2 0.655047 0.718059 0.903671 11.00000 -1.50000 H12E 2 0.729562 0.690492 1.017594 11.00000 -1.50000 AFIX 0 HKLF 4 REM loy015.res in P2(1) REM wR2 = 0.070224, GooF = S = 1.04988, Restrained GooF = 1.05101 for all data REM R1 = 0.026530 for 13233 Fo > 4sig(Fo) and 0.026688 for all 13286 data REM 776 parameters refined using 8 restraints END WGHT 0.0407 1.3803 REM Highest difference peak 0.632, deepest hole -0.513, 1-sigma level 0.059 Q1 1 0.8377 0.7037 0.7794 11.00000 0.05 0.63 Q2 1 -0.0028 0.7488 0.4576 11.00000 0.05 0.48 Q3 1 0.5678 0.6699 0.8910 11.00000 0.05 0.34 Q4 1 0.5010 0.4487 0.5881 11.00000 0.05 0.31 Q5 1 0.6900 0.1964 0.8814 11.00000 0.05 0.29 Q6 1 0.3898 0.4509 0.3865 11.00000 0.05 0.28 Q7 1 0.0573 0.8009 0.3920 11.00000 0.05 0.28 Q8 1 0.5345 0.4562 0.4765 11.00000 0.05 0.27 Q9 1 0.3639 0.4518 0.5019 11.00000 0.05 0.26 Q10 1 0.1594 0.6987 0.2206 11.00000 0.05 0.26 Q11 1 0.4772 0.4922 0.4816 11.00000 0.05 0.24 Q12 1 0.8010 0.1184 1.0152 11.00000 0.05 0.24 Q13 1 0.7756 0.1498 1.0990 11.00000 0.05 0.23 Q14 1 0.0985 0.7580 0.5739 11.00000 0.05 0.23 Q15 1 0.5425 0.3041 0.4391 11.00000 0.05 0.23 Q16 1 0.7503 0.4215 0.6298 11.00000 0.05 0.23 Q17 1 0.8355 0.1799 1.1566 11.00000 0.05 0.23 Q18 1 0.4025 0.6910 0.1693 11.00000 0.05 0.22 Q19 1 0.8061 0.6798 0.9142 11.00000 0.05 0.22 Q20 1 0.7473 0.3460 0.3630 11.00000 0.05 0.22 ; _shelx_res_checksum 35407 _shelx_hkl_file ; -2 0 0 114.84 6.56 -2 0 0 112.49 6.59 -2 0 0 128.44 6.75 -2 0 0 125.57 6.80 2 0 0 122.68 6.55 2 0 0 119.01 6.80 2 0 0 120.72 6.61 2 0 0 124.81 6.79 2 0 0 127.22 6.57 -2 0 0 122.12 6.82 -2 0 0 115.85 6.85 3 0 0 0.90 0.25 3 0 0 0.92 0.31 3 0 0 0.79 0.14 -3 0 0 0.62 0.22 -3 0 0 0.71 0.32 3 0 0 1.39 0.43 -3 0 0 0.92 0.40 -3 0 0 0.50 0.16 -3 0 0 0.67 0.22 -3 0 0 0.73 0.31 3 0 0 0.63 0.13 -4 0 0 95.42 5.60 4 0 0 95.95 5.61 -4 0 0 90.60 5.34 -4 0 0 91.62 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245.03 12.17 -2 -2 0 229.44 12.21 -2 2 0 206.13 12.23 2 2 0 227.83 12.21 -2 2 0 219.90 12.40 2 2 0 222.25 12.23 2 2 0 207.82 12.25 2 2 0 225.69 12.21 -2 2 0 213.09 12.43 2 2 0 205.53 12.34 -2 2 0 219.13 12.42 -2 2 0 211.98 12.19 2 2 0 213.01 12.20 -2 2 0 228.94 12.31 2 2 0 212.11 12.32 -3 -2 0 48.81 2.81 3 -2 0 50.78 3.09 -3 -2 0 49.63 3.17 3 -2 0 47.09 2.98 3 -2 0 49.22 3.21 -3 -2 0 50.81 3.13 -3 -2 0 49.85 2.84 3 -2 0 51.37 2.95 -3 -2 0 53.06 3.16 3 -2 0 47.06 3.20 -3 -2 0 48.67 3.31 3 -2 0 50.57 3.05 -3 -2 0 48.84 3.11 3 -2 0 48.46 2.99 -3 2 0 46.10 2.87 -3 2 0 46.97 3.11 -3 2 0 45.32 2.98 -3 2 0 43.11 3.11 -3 2 0 47.28 3.15 3 2 0 46.90 2.90 -3 2 0 46.11 2.80 4 -2 0 53.63 3.30 -4 -2 0 52.32 3.67 -4 -2 0 50.74 3.32 -4 -2 0 57.65 3.75 4 -2 0 53.96 3.44 -4 -2 0 57.75 3.69 4 -2 0 54.60 3.85 4 -2 0 56.82 3.42 -4 -2 0 51.09 3.29 -4 -2 0 58.09 3.97 -4 -2 0 57.82 3.81 4 -2 0 53.45 3.80 4 2 0 56.84 3.64 -4 2 0 55.38 3.58 -4 2 0 58.57 3.31 4 2 0 57.33 3.69 -4 2 0 57.00 3.39 -4 2 0 53.29 3.78 4 2 0 60.58 3.46 -4 2 0 62.07 3.80 -4 2 0 63.12 3.88 -5 -2 0 110.17 7.58 -5 -2 0 127.34 7.52 -5 -2 0 114.68 7.23 -5 -2 0 117.02 6.77 5 -2 0 114.76 6.75 -5 -2 0 122.06 7.34 -5 -2 0 123.60 7.41 -5 -2 0 118.70 6.82 5 2 0 122.43 7.34 5 2 0 124.62 7.31 -5 2 0 120.64 6.84 -5 2 0 120.50 6.74 5 2 0 121.99 6.91 -5 2 0 120.55 7.18 -5 2 0 109.91 7.42 6 -2 0 42.00 3.04 -6 -2 0 46.74 3.65 -6 -2 0 42.96 3.11 -6 -2 0 45.98 3.81 -6 -2 0 46.57 3.73 -6 -2 0 45.44 3.10 -6 2 0 50.42 3.09 -6 2 0 50.04 3.98 -6 2 0 56.15 3.99 -6 2 0 54.70 3.87 -6 2 0 53.04 3.67 -6 2 0 50.04 3.19 6 2 0 51.11 3.28 -7 -2 0 17.44 1.95 7 -2 0 15.01 1.03 7 -2 0 14.53 1.34 -7 -2 0 15.19 1.41 7 -2 0 16.05 0.95 7 -2 0 13.29 0.87 7 -2 0 12.64 0.95 -7 -2 0 16.48 1.39 -7 -2 0 15.89 2.04 7 -2 0 13.49 0.92 7 -2 0 15.47 0.94 7 -2 0 15.06 0.94 7 -2 0 14.95 0.95 7 -2 0 14.84 0.90 -7 -2 0 15.35 1.94 7 2 0 14.47 0.91 -7 2 0 15.28 1.35 -7 2 0 15.31 1.99 -7 2 0 15.58 1.90 7 2 0 14.41 1.44 7 2 0 13.96 0.87 7 2 0 13.87 0.91 -7 2 0 15.61 1.45 7 2 0 13.70 0.93 8 -2 0 25.86 1.58 8 -2 0 26.87 1.70 8 -2 0 26.46 1.55 -8 -2 0 23.87 1.55 8 -2 0 25.23 1.57 8 -2 0 22.79 1.61 -8 -2 0 29.01 2.96 -8 -2 0 25.11 1.56 8 -2 0 23.21 1.52 8 -2 0 23.79 1.58 8 -2 0 25.90 1.60 8 -2 0 27.12 1.60 -8 -2 0 27.40 2.24 -8 -2 0 25.64 1.64 -8 -2 0 27.51 2.19 8 -2 0 26.65 1.59 8 2 0 27.20 1.59 -8 2 0 26.11 1.55 8 2 0 29.73 1.59 8 2 0 28.77 1.59 -8 2 0 27.32 1.67 -8 2 0 27.09 1.60 -8 2 0 26.31 1.58 8 2 0 27.09 1.63 8 2 0 27.85 1.57 -8 2 0 25.31 1.56 8 2 0 27.45 2.28 8 2 0 28.22 1.54 8 2 0 28.18 1.57 8 2 0 27.47 1.54 -8 2 0 32.93 3.13 8 2 0 28.01 1.60 -8 2 0 28.42 2.11 -8 2 0 29.41 2.22 -8 2 0 32.33 3.28 -9 -2 0 42.39 2.77 -9 -2 0 51.26 3.57 9 -2 0 49.05 2.81 9 -2 0 49.80 2.76 -9 -2 0 46.11 2.79 -9 -2 0 45.97 2.87 9 -2 0 45.10 2.74 -9 -2 0 45.80 2.77 9 -2 0 44.23 2.92 9 -2 0 49.20 2.80 -9 -2 0 50.55 3.63 9 -2 0 49.79 2.82 9 -2 0 46.69 2.81 9 -2 0 45.82 2.98 -9 2 0 52.36 3.10 -9 2 0 52.92 3.49 9 2 0 50.69 3.05 9 2 0 54.75 2.75 9 2 0 51.87 2.81 -9 2 0 49.45 2.76 9 2 0 54.33 3.77 -9 2 0 46.84 2.76 9 2 0 54.18 2.81 9 2 0 54.08 2.80 -9 2 0 53.07 3.58 10 -2 0 51.79 2.76 10 -2 0 52.06 2.83 10 -2 0 50.86 2.95 -10 -2 0 51.26 2.79 10 -2 0 47.08 2.73 -10 -2 0 51.76 2.87 10 -2 0 52.38 2.81 -10 -2 0 50.29 2.79 10 -2 0 49.98 2.80 -10 -2 0 53.63 3.71 -10 -2 0 49.86 2.74 -10 -2 0 51.56 3.65 10 -2 0 48.01 2.80 10 -2 0 50.90 2.79 -10 -2 0 48.25 2.75 10 2 0 48.15 2.77 -10 2 0 46.21 2.80 -10 2 0 47.20 3.47 10 2 0 48.42 2.79 -10 2 0 42.70 2.72 -10 2 0 44.11 2.72 10 2 0 45.19 2.77 10 2 0 46.57 2.75 10 2 0 47.42 2.76 10 2 0 48.99 2.93 -10 2 0 47.32 3.53 -10 2 0 47.81 2.80 -10 2 0 48.19 2.89 10 2 0 48.11 2.72 10 2 0 51.54 3.77 11 -2 0 2.71 0.32 -11 -2 0 2.79 0.32 11 -2 0 2.42 0.27 11 -2 0 2.70 0.33 -11 -2 0 3.32 0.40 -11 -2 0 2.60 0.29 11 -2 0 3.27 0.34 11 -2 0 2.97 0.30 11 -2 0 2.44 0.39 11 -2 0 2.93 0.33 -11 -2 0 2.70 0.95 11 -2 0 3.07 0.42 -11 -2 0 3.03 0.33 -11 -2 0 2.94 0.30 -11 2 0 4.00 0.95 -11 2 0 2.00 0.64 12 -2 0 9.92 0.72 12 -2 0 9.30 0.66 12 -2 0 9.67 0.68 -12 -2 0 10.44 0.71 12 -2 0 9.72 0.69 12 -2 0 9.77 0.79 -12 -2 0 10.24 0.76 12 -2 0 9.81 0.64 12 -2 0 9.20 0.66 -12 -2 0 9.89 0.70 12 2 0 9.88 0.65 -12 2 0 10.88 0.73 12 2 0 9.87 0.63 12 2 0 9.94 0.71 -12 2 0 10.19 0.72 12 2 0 10.03 0.68 12 2 0 9.84 0.81 -12 2 0 10.96 0.80 12 2 0 9.66 0.67 12 2 0 9.55 0.65 12 2 0 9.77 0.65 -13 -2 0 0.53 0.15 13 -2 0 0.53 0.17 13 -2 0 0.44 0.12 13 -2 0 0.58 0.15 13 -2 0 0.63 0.13 -13 -2 0 0.39 0.11 13 -2 0 0.76 0.21 13 -2 0 0.43 0.11 -13 2 0 0.43 0.14 -13 2 0 0.39 0.12 13 2 0 0.42 0.17 13 2 0 0.33 0.12 -13 2 0 0.47 0.14 13 2 0 0.31 0.14 13 2 0 0.43 0.13 13 2 0 0.43 0.13 -13 2 0 0.28 0.10 -13 2 0 0.36 0.14 -14 -2 0 0.58 0.13 -14 -2 0 0.58 0.12 14 -2 0 0.67 0.16 -14 -2 0 0.37 0.13 -14 -2 0 0.41 0.12 -14 2 0 0.46 0.11 -14 2 0 0.61 0.12 14 2 0 0.55 0.13 -14 2 0 0.72 0.13 -14 2 0 0.70 0.12 14 2 0 0.76 0.17 -14 2 0 0.72 0.15 0 -3 0 0.00 0.06 0 -3 0 0.04 0.05 0 -3 0 0.04 0.04 0 -3 0 -0.01 0.07 0 -3 0 0.10 0.09 0 -3 0 0.06 0.08 0 -3 0 -0.05 0.08 0 -3 0 -0.03 0.10 0 3 0 0.09 0.07 0 3 0 0.12 0.15 0 3 0 0.04 0.13 0 3 0 0.10 0.05 0 3 0 0.07 0.09 0 3 0 0.21 0.09 0 3 0 0.16 0.07 1 -3 0 45.20 2.81 -1 -3 0 48.16 2.87 -1 -3 0 47.43 2.87 1 -3 0 49.77 2.74 -1 -3 0 47.33 2.70 -1 -3 0 47.60 2.90 -1 -3 0 46.12 2.70 1 -3 0 50.61 2.63 1 -3 0 48.05 2.65 1 -3 0 50.71 2.79 1 -3 0 46.45 3.03 -1 -3 0 52.05 2.59 1 -3 0 44.67 2.69 1 -3 0 45.27 2.68 1 -3 0 42.07 2.95 1 3 0 47.67 2.76 -1 3 0 46.53 3.00 -1 3 0 46.48 2.83 -1 3 0 47.85 2.70 1 3 0 48.73 2.71 1 3 0 44.86 2.88 -1 3 0 47.93 2.88 -1 3 0 49.84 2.81 1 3 0 49.68 2.73 1 3 0 47.40 2.71 -1 3 0 47.52 3.05 1 3 0 47.52 2.77 -1 3 0 49.09 2.68 1 3 0 47.23 2.94 -1 3 0 46.80 2.82 -1 3 0 49.02 2.74 1 3 0 46.45 2.83 -2 -3 0 110.35 6.35 -2 -3 0 108.57 6.28 2 -3 0 110.77 6.30 2 -3 0 119.03 6.43 -2 -3 0 108.50 6.29 -2 -3 0 107.66 6.46 2 -3 0 110.22 6.60 2 -3 0 110.49 6.66 -2 -3 0 113.25 6.53 -2 -3 0 118.80 6.35 -2 -3 0 113.62 6.51 2 -3 0 114.91 6.63 2 -3 0 103.82 6.55 2 -3 0 115.81 6.32 -2 3 0 113.71 6.28 2 3 0 124.02 6.45 -2 3 0 113.07 6.69 -2 3 0 115.51 6.65 2 3 0 111.47 6.39 -2 3 0 123.30 6.48 -2 3 0 121.69 6.55 -2 3 0 112.04 6.34 2 3 0 116.37 6.47 -2 3 0 126.73 6.59 2 3 0 117.75 6.30 2 3 0 116.90 6.46 -2 3 0 112.71 6.37 2 3 0 117.33 6.32 2 3 0 117.49 6.36 2 3 0 113.56 6.43 -3 -3 0 89.78 5.66 3 -3 0 85.52 5.48 3 -3 0 88.31 5.36 -3 -3 0 84.62 5.44 3 -3 0 87.62 5.12 -3 -3 0 87.25 5.36 -3 -3 0 90.34 5.42 3 -3 0 89.72 5.20 -3 -3 0 87.01 5.40 -3 -3 0 87.49 5.06 3 -3 0 83.13 5.49 -3 -3 0 88.28 5.08 3 -3 0 89.43 5.27 3 -3 0 86.67 5.40 -3 3 0 99.36 5.73 -3 3 0 91.60 5.24 3 3 0 91.03 5.08 3 3 0 95.60 5.19 3 3 0 94.19 5.05 -3 3 0 97.80 5.77 -3 3 0 91.17 5.13 -3 3 0 91.97 5.05 -3 3 0 91.74 5.40 3 3 0 94.70 5.08 3 3 0 90.68 5.07 4 -3 0 45.68 2.76 -4 -3 0 44.38 3.04 4 -3 0 45.74 2.57 -4 -3 0 44.66 2.63 -4 -3 0 45.80 2.66 4 -3 0 44.78 2.83 4 -3 0 46.72 2.96 -4 -3 0 45.14 3.28 -4 -3 0 48.10 3.06 -4 -3 0 43.49 3.08 4 -3 0 48.01 2.93 4 -3 0 43.03 3.18 -4 -3 0 45.00 3.05 4 -3 0 43.67 3.17 4 3 0 36.10 2.54 -4 3 0 37.32 2.54 4 3 0 37.85 2.57 -4 3 0 37.81 2.78 -4 3 0 37.58 2.63 4 3 0 38.56 2.68 4 3 0 38.07 2.81 -4 3 0 41.33 2.98 -4 3 0 41.82 3.04 4 3 0 35.91 2.82 -5 -3 0 149.75 8.60 -5 -3 0 149.15 8.09 5 -3 0 152.36 7.98 -5 -3 0 154.35 8.72 -5 -3 0 150.82 8.05 -5 -3 0 152.08 9.06 -5 -3 0 163.09 8.76 -5 -3 0 161.20 8.87 -5 3 0 132.75 7.93 5 3 0 129.26 8.38 -5 3 0 134.12 8.04 -5 3 0 124.71 8.57 -5 3 0 133.22 8.51 -5 3 0 122.88 8.29 -5 3 0 140.80 8.66 5 3 0 130.83 8.44 5 3 0 135.52 8.12 -6 -3 0 74.84 4.44 -6 -3 0 80.01 5.30 -6 -3 0 75.59 5.14 -6 -3 0 75.07 4.40 -6 3 0 63.38 4.75 -6 3 0 66.82 4.36 -6 3 0 66.67 4.24 -6 3 0 72.02 5.06 -6 3 0 70.43 5.14 -6 3 0 65.24 5.13 6 3 0 69.61 4.48 -7 -3 0 30.06 3.13 7 -3 0 33.39 1.88 7 -3 0 28.63 1.89 -7 -3 0 31.46 3.05 7 -3 0 27.87 1.80 -7 -3 0 31.96 3.09 7 -3 0 28.07 1.87 7 -3 0 29.56 1.85 7 -3 0 28.21 1.93 7 -3 0 31.80 1.83 7 3 0 33.90 1.80 7 3 0 35.41 1.85 7 3 0 30.98 1.81 -7 3 0 33.89 2.64 7 3 0 34.39 3.39 7 3 0 33.76 1.82 7 3 0 34.57 1.85 7 3 0 35.66 1.86 -7 3 0 33.46 2.76 7 3 0 33.20 1.83 7 3 0 31.00 1.86 -7 3 0 36.08 3.22 -7 3 0 36.35 3.14 8 -3 0 4.32 0.42 8 -3 0 4.25 0.42 -8 -3 0 3.54 0.79 -8 -3 0 7.21 2.51 -8 -3 0 4.08 0.76 -8 -3 0 5.87 1.97 8 -3 0 4.34 0.40 8 -3 0 4.22 0.42 8 -3 0 4.55 0.43 -8 -3 0 6.81 1.51 -8 3 0 5.59 0.44 -8 3 0 5.47 0.43 -8 3 0 5.57 0.44 8 3 0 5.16 0.92 8 3 0 5.59 0.44 -8 3 0 5.63 0.46 8 3 0 5.80 0.42 -8 3 0 6.08 0.52 8 3 0 5.52 0.44 -8 3 0 5.48 0.84 8 3 0 5.23 0.46 -8 3 0 6.24 0.82 -8 3 0 6.53 1.52 8 3 0 5.99 0.41 9 -3 0 3.72 0.33 9 -3 0 4.18 0.49 9 -3 0 4.30 0.40 9 -3 0 4.14 0.40 9 -3 0 4.81 0.42 9 -3 0 4.55 0.37 -9 -3 0 4.77 0.90 9 -3 0 4.61 0.43 -9 -3 0 5.43 0.82 -9 3 0 3.75 0.39 9 3 0 4.07 0.34 9 3 0 3.95 0.37 9 3 0 4.07 0.45 9 3 0 5.33 0.93 9 3 0 3.62 0.34 -9 3 0 2.87 0.74 9 3 0 3.78 0.38 9 3 0 4.22 0.39 9 3 0 3.76 0.37 -9 3 0 3.21 0.38 -9 3 0 3.35 0.67 9 3 0 3.24 0.35 -9 3 0 3.11 0.41 10 -3 0 36.18 2.21 -10 -3 0 37.13 2.27 -10 -3 0 35.61 2.16 10 -3 0 37.70 2.36 10 -3 0 37.42 2.24 10 -3 0 37.01 2.22 -10 -3 0 36.41 3.02 -10 -3 0 35.59 2.17 -10 -3 0 37.07 2.19 10 -3 0 33.86 2.13 10 -3 0 37.21 2.17 -10 -3 0 37.51 2.99 -10 -3 0 36.74 2.19 10 -3 0 37.56 2.23 10 -3 0 36.07 2.20 -10 3 0 38.80 2.33 10 3 0 39.23 2.19 10 3 0 40.08 2.21 -10 3 0 39.84 2.95 -10 3 0 38.91 2.23 10 3 0 39.26 2.21 10 3 0 39.09 2.18 -10 3 0 39.14 2.25 10 3 0 41.89 2.38 10 3 0 39.49 2.15 10 3 0 39.36 2.20 -10 3 0 40.49 3.02 10 3 0 37.40 3.20 11 -3 0 4.29 0.51 -11 -3 0 4.17 1.08 11 -3 0 4.37 0.41 11 -3 0 4.02 0.44 -11 -3 0 4.25 0.41 11 -3 0 3.96 0.40 11 -3 0 4.03 0.41 -11 -3 0 3.90 0.37 -11 -3 0 4.36 0.38 11 -3 0 3.86 0.40 -11 -3 0 4.31 0.40 11 -3 0 3.93 0.37 -11 -3 0 3.95 0.45 -11 3 0 4.82 0.45 11 3 0 4.59 0.43 11 3 0 4.29 0.39 -11 3 0 4.79 0.44 11 3 0 4.54 0.41 11 3 0 4.75 0.40 11 3 0 8.96 2.27 -11 3 0 4.36 0.50 11 3 0 4.90 0.40 11 3 0 5.29 0.54 11 3 0 4.53 0.36 12 -3 0 4.22 0.40 12 -3 0 4.45 0.45 -12 -3 0 4.37 0.34 -12 -3 0 4.30 0.34 12 -3 0 4.22 0.37 12 -3 0 3.69 0.33 12 -3 0 4.11 0.32 12 -3 0 3.78 0.45 -12 -3 0 4.23 0.41 -12 3 0 3.19 0.42 -12 3 0 3.24 0.33 12 3 0 3.61 0.44 12 3 0 3.46 0.31 12 3 0 3.14 0.35 12 3 0 3.13 0.28 12 3 0 3.27 0.30 -12 3 0 3.39 0.36 12 3 0 3.19 0.33 12 3 0 2.98 0.30 12 3 0 3.21 0.32 -12 3 0 3.54 0.38 -12 3 0 3.22 0.36 -13 -3 0 6.74 0.47 13 -3 0 6.66 0.45 13 -3 0 6.64 0.52 13 -3 0 6.83 0.43 -13 -3 0 6.94 0.52 13 -3 0 6.30 0.48 13 -3 0 6.44 0.45 13 -3 0 7.07 0.53 -13 -3 0 7.23 0.48 13 3 0 5.84 0.44 13 3 0 5.27 0.41 -13 3 0 6.21 0.48 -13 3 0 6.11 0.49 13 3 0 5.79 0.45 -13 3 0 6.06 0.53 13 3 0 6.08 0.54 -13 3 0 5.97 0.47 13 3 0 5.88 0.41 -13 3 0 5.95 0.45 -14 -3 0 6.91 0.58 -14 -3 0 7.55 0.55 -14 -3 0 7.00 0.50 -14 -3 0 7.28 0.54 14 -3 0 8.03 0.51 -14 -3 0 8.06 0.53 -14 3 0 7.85 0.54 -14 3 0 7.27 0.47 -14 3 0 7.53 0.49 14 3 0 7.32 0.53 14 3 0 8.79 0.61 0 -4 0 219.22 11.19 0 -4 0 191.31 11.63 0 -4 0 221.64 11.33 0 -4 0 210.43 11.74 0 -4 0 209.59 11.33 0 -4 0 197.69 11.49 0 -4 0 211.91 11.32 0 -4 0 212.54 11.23 0 -4 0 199.97 11.23 0 4 0 216.24 11.20 0 4 0 227.82 11.25 0 4 0 212.37 11.32 0 4 0 220.87 11.36 0 4 0 210.99 11.77 0 4 0 204.86 11.52 0 4 0 182.67 11.63 1 -4 0 161.70 8.55 1 -4 0 160.98 8.40 -1 -4 0 154.20 8.75 -1 -4 0 155.28 8.73 -1 -4 0 160.23 8.82 1 -4 0 150.72 8.95 1 -4 0 140.33 8.84 -1 -4 0 154.08 8.31 1 -4 0 155.25 8.60 1 -4 0 153.22 8.48 1 -4 0 159.85 8.60 -1 -4 0 161.08 8.52 1 -4 0 151.07 8.47 1 -4 0 158.50 8.37 -1 -4 0 158.97 8.50 1 4 0 152.59 8.58 1 4 0 152.40 8.80 1 4 0 162.85 8.50 -1 4 0 148.18 8.95 -1 4 0 159.22 8.49 1 4 0 157.55 8.48 -1 4 0 154.63 8.65 1 4 0 154.40 8.55 -1 4 0 145.50 8.88 -1 4 0 160.33 8.75 1 4 0 160.58 8.52 -1 4 0 156.55 8.63 1 4 0 154.31 8.68 1 4 0 159.27 8.88 -1 4 0 160.90 8.54 2 -4 0 308.16 16.50 2 -4 0 301.63 16.34 2 -4 0 313.74 16.39 2 -4 0 313.28 16.31 -2 -4 0 286.29 16.48 2 -4 0 291.37 16.86 -2 -4 0 281.34 16.64 -2 -4 0 293.45 16.53 -2 -4 0 293.04 16.36 2 -4 0 273.17 16.75 -2 -4 0 300.11 16.38 2 4 0 303.39 16.61 2 4 0 318.26 16.41 -2 4 0 308.65 16.62 2 4 0 317.72 16.48 2 4 0 301.77 16.42 -2 4 0 295.05 16.83 2 4 0 316.78 16.39 -2 4 0 293.45 16.62 2 4 0 283.62 16.47 -2 4 0 327.97 16.77 -2 4 0 310.74 16.43 -2 4 0 325.36 16.48 2 4 0 318.15 16.68 -2 4 0 317.79 16.96 -2 4 0 314.75 16.54 -2 4 0 305.63 16.36 2 4 0 298.36 16.56 -3 -4 0 1.70 0.26 -3 -4 0 1.35 0.45 3 -4 0 1.71 0.26 -3 -4 0 1.50 0.54 3 -4 0 1.22 0.29 3 -4 0 1.28 0.45 3 -4 0 2.02 0.57 -3 -4 0 1.16 0.25 -3 -4 0 1.05 0.24 3 -4 0 1.73 0.58 3 -4 0 1.39 0.43 -3 -4 0 1.20 0.23 -3 -4 0 1.65 0.52 -3 4 0 1.21 0.28 -3 4 0 1.27 0.34 -3 4 0 1.01 0.23 -3 4 0 1.34 0.32 3 4 0 1.56 0.32 3 4 0 1.11 0.25 3 4 0 1.25 0.28 3 4 0 1.25 0.30 3 4 0 1.06 0.27 3 4 0 1.11 0.27 3 4 0 1.60 0.33 -3 4 0 1.33 0.37 -3 4 0 0.99 0.29 4 -4 0 52.00 4.02 -4 -4 0 55.78 3.36 4 -4 0 61.07 3.63 4 -4 0 50.16 3.67 -4 -4 0 56.45 4.08 4 -4 0 50.63 3.95 -4 -4 0 57.18 3.84 -4 -4 0 54.22 3.74 -4 -4 0 54.38 3.77 4 -4 0 55.72 3.22 -4 -4 0 59.42 3.86 4 -4 0 51.58 3.47 4 -4 0 57.39 3.41 4 -4 0 56.61 3.67 -4 -4 0 54.58 3.37 4 4 0 54.59 3.32 4 4 0 54.71 3.35 -4 4 0 56.13 3.76 -4 4 0 53.18 3.54 -4 4 0 58.17 3.83 -4 4 0 58.25 3.44 4 4 0 53.98 3.62 4 4 0 52.71 3.55 -4 4 0 57.74 3.32 4 4 0 55.25 3.46 -4 4 0 55.09 3.73 -5 -4 0 4.39 0.83 -5 -4 0 4.21 0.60 -5 -4 0 3.15 0.76 -5 -4 0 3.61 0.75 -5 -4 0 3.75 0.59 5 4 0 5.22 0.87 -5 4 0 5.46 0.87 -6 -4 0 25.00 2.53 -6 -4 0 26.01 2.50 -6 -4 0 24.93 1.92 -6 -4 0 24.07 2.40 -6 -4 0 23.68 1.93 -6 4 0 26.36 2.50 6 4 0 25.58 2.03 -6 4 0 23.88 1.91 -6 4 0 26.12 2.42 -6 4 0 25.14 1.82 -6 4 0 20.66 3.27 -6 4 0 22.21 2.81 7 -4 0 47.72 2.83 7 -4 0 50.69 2.75 -7 -4 0 50.82 4.15 -7 -4 0 51.41 3.43 7 -4 0 42.06 2.85 7 -4 0 54.98 2.78 -7 -4 0 53.36 4.28 -7 -4 0 52.08 4.37 -7 -4 0 53.16 3.41 -7 4 0 51.67 4.20 7 4 0 50.54 2.69 -7 4 0 51.08 3.37 7 4 0 44.36 2.67 -7 4 0 44.91 2.75 7 4 0 43.12 2.65 -7 4 0 43.51 2.80 -7 4 0 50.56 4.07 7 4 0 44.75 2.67 -7 4 0 50.28 3.21 7 4 0 47.97 2.69 7 4 0 48.85 3.44 7 4 0 47.62 2.70 -7 4 0 42.90 2.74 8 -4 0 23.52 1.33 -8 -4 0 23.05 2.03 -8 -4 0 21.24 1.26 8 -4 0 21.74 1.31 -8 -4 0 20.39 1.26 8 -4 0 21.92 1.42 8 -4 0 17.71 1.30 8 -4 0 22.12 1.30 -8 -4 0 20.98 1.34 8 -4 0 21.76 1.32 -8 -4 0 23.44 2.00 8 -4 0 23.52 1.33 -8 -4 0 23.62 2.95 8 -4 0 23.34 1.28 -8 -4 0 23.03 3.12 8 4 0 20.67 1.24 8 4 0 18.35 1.93 -8 4 0 19.45 1.30 -8 4 0 23.82 3.36 -8 4 0 19.87 1.37 -8 4 0 21.24 1.79 8 4 0 20.63 1.26 8 4 0 18.48 1.27 8 4 0 20.51 1.27 8 4 0 19.94 1.24 -8 4 0 20.57 1.87 -8 4 0 26.79 3.59 8 4 0 19.60 1.28 -8 4 0 20.12 1.29 8 4 0 18.97 1.25 8 4 0 20.91 1.27 8 4 0 20.59 1.22 -9 -4 0 71.64 4.11 9 -4 0 76.06 4.18 9 -4 0 76.27 4.12 9 -4 0 73.05 4.17 -9 -4 0 73.04 5.05 -9 -4 0 76.20 5.03 9 -4 0 73.56 4.16 9 -4 0 80.62 4.31 -9 -4 0 72.25 4.21 9 -4 0 77.24 4.17 -9 -4 0 70.33 4.20 9 -4 0 72.25 4.28 9 4 0 77.09 4.09 9 4 0 77.12 4.13 9 4 0 77.58 4.13 9 4 0 75.69 4.12 -9 4 0 75.34 4.17 -9 4 0 75.60 4.82 9 4 0 75.46 4.07 9 4 0 73.24 5.10 9 4 0 70.59 4.13 9 4 0 74.18 4.10 -9 4 0 75.64 4.27 9 4 0 73.53 4.14 -9 4 0 73.81 4.18 9 4 0 70.88 4.10 -9 4 0 74.72 4.93 -10 -4 0 52.92 2.97 10 -4 0 56.86 3.06 10 -4 0 52.70 3.16 10 -4 0 52.97 3.01 -10 -4 0 54.83 4.00 -10 -4 0 55.62 3.94 -10 -4 0 54.46 2.99 10 -4 0 55.75 2.99 -10 -4 0 52.92 2.99 10 -4 0 55.96 3.03 10 -4 0 52.71 3.02 -10 -4 0 54.51 3.08 -10 -4 0 54.67 2.97 10 -4 0 52.07 3.03 -10 4 0 52.81 3.14 10 4 0 52.73 2.99 -10 4 0 50.40 3.04 -10 4 0 52.62 3.78 10 4 0 51.37 2.96 10 4 0 52.30 2.98 10 4 0 52.11 2.93 10 4 0 55.03 3.16 10 4 0 56.72 4.09 10 4 0 45.70 2.97 10 4 0 49.10 2.97 -10 4 0 52.85 3.69 -10 4 0 52.08 3.03 10 4 0 52.75 2.98 10 4 0 49.68 2.99 11 -4 0 15.67 1.14 -11 -4 0 16.19 0.99 11 -4 0 15.39 1.06 -11 -4 0 16.25 1.02 -11 -4 0 15.77 0.98 11 -4 0 15.96 1.03 11 -4 0 14.69 1.01 11 -4 0 15.21 1.03 -11 -4 0 16.08 1.08 11 -4 0 15.34 0.98 -11 -4 0 16.13 1.02 11 -4 0 14.40 1.00 11 4 0 16.17 1.00 11 4 0 15.67 1.02 11 4 0 14.67 0.98 11 4 0 17.28 1.18 -11 4 0 16.08 1.05 -11 4 0 15.47 1.06 11 4 0 15.72 0.99 11 4 0 15.33 1.00 -11 4 0 15.54 1.14 11 4 0 15.18 0.95 -12 -4 0 6.11 0.53 -12 -4 0 6.05 0.48 12 -4 0 5.61 0.43 -12 -4 0 5.59 0.47 12 -4 0 5.41 0.50 -12 -4 0 6.11 0.65 12 -4 0 5.53 0.46 -12 -4 0 5.95 0.44 12 -4 0 5.34 0.44 12 -4 0 5.41 0.45 12 -4 0 5.65 0.48 12 -4 0 5.49 0.54 12 4 0 6.07 0.44 12 4 0 6.50 0.60 12 4 0 6.42 0.45 -12 4 0 6.46 0.48 12 4 0 6.19 0.41 12 4 0 6.38 0.49 -12 4 0 6.32 0.52 -12 4 0 6.66 0.52 12 4 0 6.35 0.47 12 4 0 6.08 0.44 -12 4 0 6.68 0.59 -12 4 0 6.67 0.54 12 4 0 6.29 0.49 -13 -4 0 0.11 0.07 13 -4 0 0.18 0.08 -13 -4 0 0.19 0.09 13 -4 0 0.12 0.09 -13 -4 0 0.17 0.10 13 -4 0 0.19 0.12 13 4 0 0.14 0.07 -13 4 0 0.13 0.09 -13 4 0 0.14 0.10 -13 4 0 0.15 0.09 -13 4 0 0.07 0.09 -13 4 0 0.19 0.12 13 4 0 0.12 0.12 13 4 0 0.22 0.10 13 4 0 0.22 0.10 13 4 0 0.15 0.09 -14 -4 0 3.45 0.27 -14 -4 0 3.60 0.29 -14 -4 0 3.71 0.35 14 -4 0 2.93 0.32 14 4 0 4.13 0.37 -14 4 0 3.23 0.25 -14 4 0 3.89 0.33 14 4 0 3.77 0.32 -14 4 0 3.83 0.28 0 -5 0 0.03 0.07 0 -5 0 -0.13 0.12 0 -5 0 0.11 0.15 0 -5 0 0.09 0.18 0 -5 0 0.00 0.16 0 -5 0 0.01 0.11 0 -5 0 -0.07 0.15 0 5 0 0.08 0.18 0 5 0 0.00 0.15 0 5 0 -0.09 0.06 0 5 0 -0.03 0.18 0 5 0 0.00 0.17 0 5 0 0.13 0.12 0 5 0 -0.03 0.10 1 -5 0 17.89 1.13 1 -5 0 17.56 1.66 1 -5 0 18.89 1.66 1 -5 0 18.70 1.27 -1 -5 0 19.52 1.56 1 -5 0 19.75 1.50 -1 -5 0 17.08 1.54 1 -5 0 18.30 1.32 -1 -5 0 17.48 1.27 -1 -5 0 17.79 1.29 -1 -5 0 18.34 1.49 1 -5 0 18.77 1.28 1 -5 0 19.87 1.40 1 -5 0 17.95 1.35 1 -5 0 18.33 1.17 -1 5 0 20.02 1.71 1 5 0 20.57 1.65 -1 5 0 17.92 1.70 1 5 0 18.74 1.64 -1 5 0 19.62 1.52 -1 5 0 21.40 1.46 1 5 0 20.94 1.27 1 5 0 20.19 1.30 1 5 0 19.44 1.32 1 5 0 21.03 1.51 -1 5 0 19.22 1.41 -1 5 0 19.51 1.33 2 -5 0 126.11 7.62 2 -5 0 105.89 7.23 2 -5 0 132.69 7.04 2 -5 0 126.79 7.55 -2 -5 0 126.68 7.44 -2 -5 0 125.11 7.22 -2 -5 0 138.16 6.83 -2 -5 0 126.64 7.04 2 -5 0 138.51 7.18 -2 -5 0 126.71 7.02 -2 -5 0 123.69 7.26 2 -5 0 131.83 6.95 2 -5 0 134.90 6.87 -2 5 0 123.57 7.23 -2 5 0 127.95 7.07 -2 5 0 123.74 7.26 2 5 0 121.43 7.11 -2 5 0 122.92 6.99 2 5 0 125.93 7.24 2 5 0 125.85 7.02 2 5 0 122.91 7.33 2 5 0 127.02 7.41 -2 5 0 124.50 7.38 -2 5 0 123.64 7.63 2 5 0 125.06 7.08 2 5 0 125.71 7.05 -2 5 0 123.32 7.56 2 5 0 125.53 7.05 3 -5 0 69.75 3.95 -3 -5 0 71.20 3.97 -3 -5 0 69.22 3.94 3 -5 0 67.38 4.06 -3 -5 0 72.54 4.02 3 -5 0 69.00 3.90 3 -5 0 63.84 4.36 -3 -5 0 68.32 4.35 3 -5 0 66.35 4.47 -3 -5 0 67.53 3.95 3 5 0 67.00 4.00 -3 5 0 61.48 4.09 -3 5 0 62.55 4.22 3 5 0 67.03 3.92 -3 5 0 67.07 4.42 3 5 0 65.58 4.03 -3 5 0 64.79 4.20 -3 5 0 67.95 4.04 -3 5 0 67.33 3.98 3 5 0 67.64 4.16 3 5 0 60.94 4.06 3 5 0 59.39 4.02 -3 5 0 66.62 3.88 3 5 0 69.12 3.96 -4 -5 0 113.91 6.80 4 -5 0 112.43 6.20 -4 -5 0 113.88 8.76 4 -5 0 113.86 6.40 -4 -5 0 109.63 6.72 -4 -5 0 115.46 6.24 -4 -5 0 113.14 6.67 4 -5 0 113.01 6.70 4 -5 0 113.03 6.34 -4 -5 0 123.32 7.97 4 -5 0 115.04 6.79 -4 -5 0 115.60 6.27 4 5 0 103.87 6.15 4 5 0 95.41 6.39 -4 5 0 103.93 6.65 -4 5 0 98.64 6.34 -4 5 0 92.28 6.43 -4 5 0 104.45 6.12 -4 5 0 104.76 6.59 -4 5 0 104.78 6.24 4 5 0 102.75 6.37 4 5 0 101.80 6.18 4 5 0 104.33 6.30 -5 -5 0 41.86 2.66 -5 -5 0 37.09 3.15 -5 -5 0 41.27 3.22 -5 -5 0 42.98 2.71 -5 -5 0 41.57 3.17 -5 5 0 37.65 2.51 -5 5 0 37.77 2.87 -5 5 0 39.54 3.14 5 5 0 38.28 2.72 -5 5 0 42.47 3.13 5 5 0 34.72 2.83 -5 5 0 37.74 2.64 -5 5 0 32.92 2.94 5 5 0 36.92 2.83 -6 -5 0 79.64 4.63 -6 -5 0 75.16 5.31 -6 -5 0 71.91 5.37 -6 -5 0 80.07 5.44 -6 -5 0 81.22 4.68 -6 5 0 68.19 4.90 -6 5 0 72.68 5.15 -6 5 0 59.45 4.97 6 5 0 70.39 4.65 -6 5 0 71.30 5.24 -6 5 0 67.10 4.37 -6 5 0 70.59 4.54 7 -5 0 13.58 0.97 -7 -5 0 15.71 2.03 7 -5 0 15.25 0.97 -7 -5 0 16.20 2.18 7 -5 0 16.11 1.04 7 -5 0 13.76 0.99 7 -5 0 14.76 1.00 7 -5 0 13.90 0.98 7 -5 0 16.07 1.01 7 -5 0 13.17 1.05 -7 -5 0 12.83 0.93 -7 -5 0 13.59 1.00 -7 -5 0 14.28 2.10 -7 -5 0 12.93 0.93 -7 -5 0 14.35 1.51 -7 -5 0 16.52 1.53 7 5 0 14.16 0.99 -7 5 0 15.92 1.02 -7 5 0 16.91 1.54 -7 5 0 17.38 1.44 -7 5 0 15.91 1.00 -7 5 0 18.41 2.20 7 5 0 17.13 0.99 7 5 0 17.65 0.99 7 5 0 17.49 0.95 7 5 0 17.07 0.93 7 5 0 17.13 1.66 -7 5 0 16.51 1.09 7 5 0 16.16 1.00 7 5 0 16.52 0.95 8 -5 0 6.21 0.53 -8 -5 0 5.42 0.48 -8 -5 0 5.13 0.99 8 -5 0 7.48 0.57 8 -5 0 5.76 0.53 8 -5 0 6.38 0.51 8 -5 0 6.57 0.55 -8 -5 0 6.16 0.48 8 -5 0 7.22 0.63 -8 -5 0 6.35 0.51 -8 -5 0 6.36 0.48 8 -5 0 5.87 0.52 -8 -5 0 5.45 0.54 -8 -5 0 6.49 1.01 8 5 0 6.53 1.12 8 5 0 6.63 0.51 8 5 0 7.31 0.51 8 5 0 7.07 0.49 -8 5 0 6.95 0.56 -8 5 0 7.63 0.94 8 5 0 7.17 0.47 8 5 0 7.18 0.49 -8 5 0 6.58 0.53 -8 5 0 6.05 0.60 -8 5 0 7.54 1.01 8 5 0 6.94 0.51 -9 -5 0 18.14 1.99 -9 -5 0 17.52 1.11 -9 -5 0 18.31 1.20 9 -5 0 16.94 1.26 9 -5 0 17.83 1.15 9 -5 0 17.02 1.16 9 -5 0 18.79 1.19 9 -5 0 18.86 1.18 9 -5 0 18.07 1.17 -9 -5 0 18.58 1.91 -9 -5 0 17.76 1.11 9 -5 0 18.33 1.13 -9 5 0 20.39 2.20 9 5 0 17.00 1.09 9 5 0 17.67 1.12 9 5 0 17.81 1.07 9 5 0 17.83 1.12 9 5 0 16.54 1.13 9 5 0 18.04 1.12 -9 5 0 17.04 1.16 9 5 0 19.55 1.95 -9 5 0 16.77 1.17 -9 5 0 19.29 1.87 -9 5 0 17.78 1.26 9 5 0 17.83 1.09 10 -5 0 21.89 1.58 10 -5 0 23.82 1.51 10 -5 0 23.90 1.45 10 -5 0 22.95 1.49 -10 -5 0 25.12 2.29 10 -5 0 24.95 1.49 -10 -5 0 23.35 2.22 10 -5 0 21.85 1.47 -10 -5 0 23.13 1.44 10 -5 0 22.77 1.46 -10 -5 0 23.18 1.44 -10 -5 0 24.50 1.53 10 5 0 25.01 1.42 10 5 0 22.74 1.40 -10 5 0 25.56 2.17 10 5 0 22.33 1.44 10 5 0 25.47 1.62 10 5 0 21.36 1.43 10 5 0 25.76 2.42 10 5 0 24.74 1.45 10 5 0 23.09 1.42 -10 5 0 24.91 1.51 -10 5 0 26.10 1.63 10 5 0 25.05 1.46 10 5 0 24.46 1.40 -10 5 0 23.97 1.52 10 5 0 24.94 1.44 -10 5 0 22.97 2.03 11 -5 0 0.68 0.19 -11 -5 0 0.85 0.24 11 -5 0 0.83 0.23 11 -5 0 0.82 0.22 11 -5 0 0.73 0.24 -11 -5 0 0.75 0.19 -11 -5 0 0.87 0.19 11 -5 0 0.70 0.19 -11 -5 0 0.76 0.18 11 -5 0 0.74 0.22 -11 -5 0 0.88 0.20 11 -5 0 0.80 0.19 11 5 0 1.07 0.22 -11 5 0 1.09 0.24 11 5 0 1.08 0.22 11 5 0 0.99 0.18 -11 5 0 1.17 0.32 11 5 0 1.04 0.19 11 5 0 1.03 0.29 -11 5 0 1.04 0.25 -11 5 0 1.16 0.24 11 5 0 1.13 0.17 -11 5 0 1.24 0.23 11 5 0 1.23 0.20 -12 -5 0 10.76 0.69 12 -5 0 10.15 0.74 12 -5 0 10.23 0.72 -12 -5 0 10.48 0.68 12 -5 0 10.78 0.70 12 -5 0 9.86 0.69 -12 -5 0 10.48 0.76 12 -5 0 10.30 0.76 12 -5 0 11.14 0.85 -12 -5 0 10.91 0.72 12 -5 0 10.23 0.67 -12 -5 0 10.78 0.72 12 -5 0 9.45 0.68 -12 5 0 11.18 0.76 12 5 0 11.03 0.69 -12 5 0 10.90 0.77 12 5 0 10.46 0.66 -12 5 0 10.15 0.70 12 5 0 11.54 0.85 12 5 0 9.56 0.65 12 5 0 10.09 0.71 -12 5 0 10.56 0.83 12 5 0 11.37 0.81 -12 5 0 10.53 0.75 12 5 0 10.04 0.64 12 5 0 10.06 0.69 13 -5 0 17.71 1.14 13 -5 0 17.88 1.20 13 -5 0 17.23 1.09 -13 -5 0 18.25 1.07 -13 -5 0 19.21 1.12 -13 -5 0 17.82 1.15 -13 -5 0 17.76 1.06 -13 -5 0 18.13 1.11 -13 5 0 19.06 1.10 -13 5 0 19.06 1.14 -13 5 0 20.37 1.16 13 5 0 17.69 1.10 13 5 0 20.64 1.23 13 5 0 19.24 1.08 -13 5 0 20.45 1.16 -13 5 0 19.84 1.21 -14 -5 0 4.48 0.32 -14 -5 0 4.50 0.33 -14 -5 0 4.46 0.31 14 5 0 4.94 0.36 -14 5 0 4.34 0.36 14 5 0 4.45 0.36 -14 5 0 4.99 0.35 0 -6 0 98.01 6.36 0 -6 0 101.82 5.65 0 -6 0 105.32 5.80 0 -6 0 109.68 5.82 0 -6 0 105.10 5.81 0 -6 0 90.69 6.22 0 -6 0 97.99 6.06 0 6 0 103.41 5.83 0 6 0 95.62 6.32 0 6 0 107.61 5.80 0 6 0 112.52 5.88 0 6 0 105.98 5.69 0 6 0 104.74 6.47 0 6 0 99.74 6.10 1 -6 0 290.89 15.53 1 -6 0 292.96 15.65 1 -6 0 280.34 15.38 -1 -6 0 267.52 15.93 1 -6 0 292.05 15.54 1 -6 0 282.22 15.64 -1 -6 0 288.76 15.56 -1 -6 0 281.32 16.05 1 -6 0 297.95 16.38 1 -6 0 288.15 15.42 -1 -6 0 289.05 15.58 1 -6 0 289.36 15.73 1 -6 0 272.08 16.21 1 -6 0 263.12 16.09 1 6 0 285.84 15.54 -1 6 0 310.65 15.40 1 6 0 299.38 15.50 1 6 0 268.19 16.12 -1 6 0 282.30 15.52 1 6 0 253.06 16.00 1 6 0 301.11 15.61 -1 6 0 330.67 17.85 -1 6 0 286.85 15.92 -1 6 0 269.93 17.00 -1 6 0 284.59 15.59 -1 6 0 291.76 15.72 -1 6 0 289.60 15.74 1 6 0 300.08 15.89 2 -6 0 56.95 3.54 2 -6 0 53.93 3.28 -2 -6 0 54.45 3.76 2 -6 0 52.64 3.92 -2 -6 0 54.20 3.65 -2 -6 0 56.93 3.72 -2 -6 0 52.71 3.69 2 -6 0 54.55 4.02 -2 -6 0 54.84 3.65 2 -6 0 55.12 3.40 2 -6 0 54.84 3.18 -2 6 0 58.65 3.83 2 6 0 59.21 3.83 -2 6 0 61.88 3.78 -2 6 0 57.55 3.65 2 6 0 58.50 3.43 2 6 0 62.58 3.49 -2 6 0 58.39 4.11 -2 6 0 57.25 4.02 -2 6 0 55.98 3.53 2 6 0 60.56 3.43 -2 6 0 64.37 3.84 2 6 0 58.15 3.48 2 6 0 58.78 3.68 2 6 0 56.17 3.86 2 6 0 57.69 3.51 -3 -6 0 8.74 1.03 3 -6 0 7.27 0.74 3 -6 0 7.73 0.86 -3 -6 0 6.97 1.03 3 -6 0 7.99 1.12 -3 -6 0 7.64 1.04 -3 6 0 10.97 1.25 3 6 0 10.66 0.88 3 6 0 11.23 1.11 3 6 0 10.85 0.98 -4 -6 0 156.02 9.62 -4 -6 0 150.28 9.03 -4 -6 0 146.48 8.90 -4 -6 0 151.90 9.02 4 -6 0 158.87 9.61 4 -6 0 146.22 9.04 4 -6 0 145.92 9.61 -4 -6 0 158.24 8.90 -4 6 0 154.91 9.18 -4 6 0 174.98 9.14 -4 6 0 174.22 9.53 -4 6 0 182.93 9.66 -4 6 0 162.48 9.35 4 6 0 161.84 9.21 -4 6 0 171.24 8.97 4 6 0 166.39 9.29 4 6 0 158.22 9.13 -5 -6 0 53.05 3.71 5 -6 0 52.73 4.07 -5 -6 0 53.17 3.69 -5 -6 0 54.73 4.30 -5 6 0 56.69 3.94 -5 6 0 62.93 3.82 -5 6 0 65.41 4.39 5 6 0 55.23 3.94 5 6 0 61.65 3.88 5 6 0 57.26 4.01 -5 6 0 63.71 4.26 -5 6 0 56.10 4.10 -5 6 0 63.23 3.66 6 -6 0 46.87 2.71 6 -6 0 46.36 2.66 6 -6 0 48.84 2.71 6 -6 0 50.86 2.73 -6 -6 0 47.10 3.33 -6 -6 0 46.61 3.28 -6 -6 0 45.69 3.97 -6 -6 0 41.92 3.75 -6 -6 0 48.63 4.05 6 6 0 47.94 2.63 -6 6 0 55.17 4.09 6 6 0 46.07 2.62 6 6 0 49.22 3.41 -6 6 0 46.62 3.81 -6 6 0 50.81 3.90 -6 6 0 46.96 3.11 -6 6 0 47.74 3.28 6 6 0 44.56 2.69 -6 6 0 44.55 3.55 7 -6 0 35.16 1.96 7 -6 0 31.93 1.95 7 -6 0 36.36 1.97 -7 -6 0 29.33 1.90 -7 -6 0 30.11 3.14 -7 -6 0 31.57 3.35 -7 -6 0 28.97 1.94 -7 -6 0 30.14 2.00 7 -6 0 33.43 1.95 -7 -6 0 32.76 1.97 7 -6 0 33.02 1.96 7 -6 0 32.66 1.96 -7 -6 0 34.31 2.65 -7 -6 0 29.84 1.88 -7 -6 0 32.92 2.66 7 -6 0 35.21 1.92 7 -6 0 31.74 1.97 7 -6 0 31.32 2.03 -7 -6 0 30.34 3.37 -7 6 0 36.85 3.36 -7 6 0 37.66 3.50 7 6 0 34.86 1.85 7 6 0 29.48 1.89 7 6 0 34.50 2.72 7 6 0 34.80 1.90 -7 6 0 37.58 2.65 7 6 0 28.82 1.86 -7 6 0 32.94 1.94 7 6 0 33.84 1.93 -7 6 0 30.98 1.97 7 6 0 35.68 1.88 -7 6 0 31.68 2.05 7 6 0 34.70 1.91 -7 6 0 37.11 2.48 7 6 0 33.60 1.88 8 -6 0 13.48 0.93 -8 -6 0 12.46 0.86 8 -6 0 13.33 0.91 8 -6 0 14.00 0.90 8 -6 0 13.61 0.92 8 -6 0 13.51 0.94 8 -6 0 11.49 0.91 8 -6 0 15.24 0.96 -8 -6 0 13.23 1.58 8 -6 0 11.61 0.99 -8 -6 0 12.37 0.86 8 -6 0 11.51 0.89 -8 -6 0 12.32 0.85 -8 -6 0 14.19 1.55 -8 -6 0 14.08 0.96 8 6 0 14.45 0.86 8 6 0 15.56 0.91 8 6 0 12.95 0.90 8 6 0 15.02 1.64 -8 6 0 14.90 1.39 8 6 0 14.94 0.89 -8 6 0 15.36 1.06 -8 6 0 13.74 0.93 8 6 0 14.59 0.84 8 6 0 13.20 0.86 -8 6 0 13.97 1.50 -8 6 0 13.29 0.95 8 6 0 14.57 0.88 -9 -6 0 22.12 1.38 -9 -6 0 21.59 1.37 9 -6 0 23.98 1.46 9 -6 0 20.88 1.53 -9 -6 0 25.69 2.43 -9 -6 0 23.16 1.56 -9 -6 0 23.99 2.35 9 -6 0 21.31 1.44 -9 -6 0 22.81 1.47 -9 -6 0 21.45 1.58 9 -6 0 23.29 1.46 9 -6 0 22.34 1.44 9 -6 0 23.68 1.41 9 -6 0 22.81 1.43 -9 6 0 25.17 1.59 9 6 0 23.59 1.39 9 6 0 23.53 1.34 -9 6 0 23.94 2.14 9 6 0 24.17 1.40 9 6 0 21.32 1.40 -9 6 0 23.14 1.47 -9 6 0 23.08 1.45 9 6 0 23.82 1.37 -9 6 0 24.35 2.03 9 6 0 22.55 1.36 9 6 0 22.68 1.38 9 6 0 24.90 2.34 9 6 0 23.99 1.40 9 6 0 20.35 1.39 10 -6 0 17.78 1.20 -10 -6 0 18.76 1.91 10 -6 0 19.81 1.21 -10 -6 0 20.99 1.97 -10 -6 0 18.25 1.15 -10 -6 0 18.47 1.23 10 -6 0 17.52 1.19 10 -6 0 19.05 1.16 10 -6 0 17.26 1.29 10 -6 0 18.32 1.22 10 -6 0 17.88 1.18 -10 -6 0 18.17 1.14 10 6 0 17.60 1.12 10 6 0 16.84 1.15 10 6 0 19.01 1.16 10 6 0 18.56 1.15 -10 6 0 18.42 1.21 -10 6 0 17.99 1.77 -10 6 0 19.83 1.35 -10 6 0 18.83 1.86 -10 6 0 18.17 1.23 -10 6 0 17.71 1.22 10 6 0 17.48 1.12 10 6 0 18.54 1.10 10 6 0 21.66 2.12 10 6 0 16.26 1.14 10 6 0 18.89 1.15 -10 6 0 19.49 1.17 10 6 0 18.75 1.13 11 -6 0 16.46 1.01 -11 -6 0 16.04 0.97 -11 -6 0 16.36 0.97 -11 -6 0 16.75 1.06 11 -6 0 15.82 1.04 11 -6 0 15.21 0.99 11 -6 0 16.26 0.98 11 -6 0 15.62 1.10 -11 -6 0 16.95 1.00 -11 -6 0 16.61 0.99 11 -6 0 16.07 1.02 11 -6 0 15.79 1.00 11 6 0 14.13 0.96 11 6 0 15.32 1.12 -11 6 0 14.89 1.13 -11 6 0 14.77 1.03 -11 6 0 14.20 1.04 -11 6 0 14.17 0.97 11 6 0 14.37 0.91 11 6 0 13.94 0.97 -11 6 0 14.13 1.03 11 6 0 13.50 0.94 11 6 0 14.23 0.94 11 6 0 13.80 0.95 12 -6 0 9.05 0.73 12 -6 0 8.62 0.66 -12 -6 0 8.75 0.72 -12 -6 0 9.96 0.69 -12 -6 0 8.59 0.74 -12 -6 0 8.93 0.71 -12 -6 0 9.18 0.66 12 -6 0 8.85 0.72 12 -6 0 9.33 0.72 12 6 0 10.60 0.65 -12 6 0 10.90 0.72 -12 6 0 10.77 0.73 12 6 0 9.29 0.67 -12 6 0 10.94 0.81 12 6 0 10.22 0.67 -12 6 0 10.27 0.72 12 6 0 8.57 0.67 -12 6 0 10.21 0.66 12 6 0 9.80 0.66 12 6 0 9.76 0.63 12 6 0 9.09 0.63 12 6 0 11.11 0.81 -13 -6 0 1.73 0.20 -13 -6 0 1.38 0.15 -13 -6 0 1.53 0.18 -13 -6 0 1.69 0.22 13 -6 0 1.77 0.26 13 -6 0 1.74 0.25 -13 -6 0 1.50 0.15 -13 6 0 1.39 0.20 -13 6 0 1.67 0.21 -13 6 0 1.80 0.27 -13 6 0 1.73 0.20 13 6 0 1.30 0.24 -13 6 0 1.45 0.21 13 6 0 1.44 0.16 13 6 0 1.48 0.18 13 6 0 1.47 0.21 -14 -6 0 0.13 0.06 -14 -6 0 0.14 0.06 -14 -6 0 0.12 0.05 14 6 0 0.10 0.06 -14 6 0 0.19 0.07 14 6 0 0.14 0.08 -14 6 0 0.10 0.08 0 -7 0 0.01 0.08 0 -7 0 -0.06 0.20 0 -7 0 0.03 0.15 0 -7 0 -0.07 0.14 0 -7 0 0.01 0.19 0 7 0 -0.02 0.12 0 7 0 0.28 0.27 0 7 0 0.34 0.35 0 7 0 -0.08 0.13 0 7 0 0.02 0.12 0 7 0 -0.09 0.19 1 -7 0 130.04 7.52 1 -7 0 131.71 7.30 1 -7 0 129.76 7.42 -1 -7 0 127.83 7.35 1 -7 0 117.01 7.91 -1 -7 0 119.78 7.84 1 -7 0 132.80 7.29 1 -7 0 134.36 7.67 1 -7 0 125.34 7.39 -1 -7 0 131.39 7.71 -1 -7 0 117.08 7.74 1 -7 0 126.78 7.10 1 -7 0 122.05 8.04 -1 -7 0 129.77 7.33 -1 7 0 124.84 8.02 1 7 0 134.84 7.69 1 7 0 135.42 7.25 -1 7 0 134.16 7.51 -1 7 0 133.24 7.48 -1 7 0 141.29 7.58 -1 7 0 130.30 8.16 -1 7 0 139.38 7.13 1 7 0 132.36 7.31 1 7 0 138.64 7.39 -1 7 0 125.17 7.53 1 7 0 127.67 8.02 1 7 0 128.34 7.94 -1 7 0 133.41 7.77 -2 -7 0 53.96 3.37 -2 -7 0 48.19 3.67 2 -7 0 48.67 3.15 2 -7 0 49.76 3.30 -2 -7 0 48.47 3.66 2 -7 0 51.74 3.93 -2 -7 0 52.35 3.34 2 -7 0 52.92 3.46 -2 -7 0 48.56 3.60 2 -7 0 49.43 3.97 2 7 0 59.64 3.36 -2 7 0 60.94 3.65 2 7 0 51.60 3.86 2 7 0 59.00 3.36 -2 7 0 54.37 4.03 2 7 0 60.54 3.43 2 7 0 56.03 3.65 -2 7 0 58.51 3.85 -2 7 0 54.12 3.39 2 7 0 56.90 3.40 -2 7 0 55.49 4.13 -2 7 0 58.63 3.33 -2 7 0 60.36 3.61 2 7 0 55.28 3.84 2 7 0 55.90 3.43 3 -7 0 66.85 3.95 -3 -7 0 66.17 4.26 -3 -7 0 66.03 4.55 -3 -7 0 64.77 4.06 3 -7 0 65.48 4.78 -3 -7 0 69.33 4.23 -3 -7 0 64.22 4.03 3 -7 0 65.56 4.69 3 7 0 68.12 4.09 3 7 0 66.16 4.48 3 7 0 64.91 4.30 -3 7 0 64.83 4.07 -3 7 0 70.91 4.42 3 7 0 67.70 4.08 3 7 0 65.19 4.08 3 7 0 67.22 4.02 3 7 0 68.20 4.43 -3 7 0 67.90 4.34 3 7 0 61.81 4.10 -3 7 0 68.04 3.98 -4 -7 0 143.80 8.73 -4 -7 0 145.94 8.02 -4 -7 0 141.72 8.06 4 -7 0 146.47 8.03 -4 -7 0 152.42 7.70 4 -7 0 148.03 8.88 4 -7 0 143.56 8.74 -4 -7 0 148.81 7.98 -4 -7 0 148.32 8.06 4 7 0 132.40 8.06 4 7 0 119.09 8.07 -4 7 0 134.67 8.44 4 7 0 125.34 8.04 -4 7 0 130.61 7.86 -4 7 0 132.26 8.01 -4 7 0 135.16 8.38 6 -7 0 86.87 5.04 6 -7 0 94.50 5.04 6 -7 0 103.97 5.09 6 -7 0 95.70 5.03 -6 -7 0 94.28 6.75 6 -7 0 88.33 5.07 6 -7 0 97.53 5.06 6 -7 0 91.59 5.05 -6 7 0 83.53 5.95 6 7 0 90.74 4.99 6 7 0 98.79 4.99 -6 7 0 97.15 6.42 -6 7 0 97.61 6.55 6 7 0 83.34 4.99 -6 7 0 85.84 5.09 -6 7 0 90.67 5.89 -6 7 0 81.49 6.05 -6 7 0 85.32 5.13 -6 7 0 94.79 5.71 6 7 0 89.69 4.94 -7 -7 0 23.35 1.50 -7 -7 0 24.93 2.29 7 -7 0 25.72 1.59 -7 -7 0 25.13 2.25 -7 -7 0 23.43 1.51 7 -7 0 25.10 1.56 7 -7 0 27.05 1.60 -7 -7 0 26.16 3.04 7 -7 0 26.13 1.55 -7 -7 0 25.06 1.60 -7 -7 0 23.30 1.50 7 -7 0 24.97 1.59 -7 -7 0 23.23 1.54 7 -7 0 23.30 1.58 7 -7 0 22.85 1.56 7 -7 0 24.96 1.59 7 7 0 25.29 1.49 7 7 0 28.43 1.52 -7 7 0 29.33 1.55 7 7 0 27.06 1.51 -7 7 0 29.97 3.01 -7 7 0 26.89 1.61 -7 7 0 30.56 2.96 7 7 0 28.06 1.49 -7 7 0 27.49 2.25 -7 7 0 27.46 1.70 7 7 0 24.67 1.48 7 7 0 27.31 1.52 -7 7 0 27.62 2.10 7 7 0 26.21 2.35 7 7 0 25.75 1.56 -7 7 0 27.78 1.62 7 7 0 27.75 1.55 -8 -7 0 24.28 1.43 -8 -7 0 23.59 1.40 8 -7 0 23.51 1.46 -8 -7 0 23.17 2.28 8 -7 0 23.32 1.56 -8 -7 0 23.36 2.24 -8 -7 0 23.69 1.49 -8 -7 0 23.64 1.40 8 -7 0 23.48 1.44 8 -7 0 24.23 1.46 -8 -7 0 29.26 2.69 -8 -7 0 24.57 1.40 8 7 0 22.38 1.37 -8 7 0 22.81 1.97 -8 7 0 22.54 1.41 8 7 0 22.99 2.25 -8 7 0 23.03 2.13 -8 7 0 22.40 1.48 -8 7 0 22.89 1.48 -8 7 0 21.75 1.55 8 7 0 22.96 1.39 -8 7 0 22.51 1.57 -9 -7 0 1.99 0.32 9 -7 0 2.01 0.30 -9 -7 0 2.47 0.86 -9 -7 0 2.00 0.25 9 -7 0 2.01 0.33 9 -7 0 2.03 0.33 -9 -7 0 1.88 0.25 9 -7 0 2.01 0.31 9 -7 0 1.87 0.32 -9 -7 0 1.82 0.24 9 -7 0 2.11 0.30 9 -7 0 1.94 0.35 -9 -7 0 1.98 0.26 9 7 0 2.19 0.25 9 7 0 2.12 0.27 9 7 0 4.02 1.07 9 7 0 2.32 0.29 9 7 0 2.20 0.24 9 7 0 2.03 0.27 -9 7 0 2.19 0.41 -9 7 0 2.05 0.33 -9 7 0 2.24 0.33 -9 7 0 2.11 0.29 9 7 0 2.19 0.26 9 7 0 2.29 0.29 -9 7 0 3.22 0.63 9 7 0 2.23 0.29 -9 7 0 2.23 0.34 -9 7 0 3.40 1.07 9 7 0 2.46 0.27 -10 -7 0 16.84 1.00 -10 -7 0 16.75 1.09 10 -7 0 16.36 1.16 10 -7 0 17.40 1.06 10 -7 0 16.19 1.07 -10 -7 0 16.92 1.00 10 -7 0 15.83 1.04 10 -7 0 16.06 1.06 -10 -7 0 17.91 1.78 10 -7 0 16.41 1.01 10 -7 0 14.91 1.05 10 7 0 14.45 0.96 10 7 0 14.96 0.93 -10 7 0 14.68 1.07 -10 7 0 15.53 1.66 10 7 0 14.37 0.98 10 7 0 12.61 1.10 10 7 0 14.55 0.98 -10 7 0 14.86 1.07 10 7 0 15.36 1.00 -10 7 0 14.09 0.99 -10 7 0 15.05 1.57 -10 7 0 15.15 1.06 10 7 0 14.55 0.97 10 7 0 13.28 1.17 -10 7 0 14.47 1.15 10 7 0 14.21 1.88 10 7 0 15.23 0.97 11 -7 0 2.28 0.35 -11 -7 0 2.42 0.28 11 -7 0 2.37 0.29 11 -7 0 2.03 0.31 11 -7 0 2.18 0.29 11 -7 0 2.19 0.29 11 -7 0 2.16 0.32 -11 -7 0 2.41 0.27 11 -7 0 2.24 0.27 -11 -7 0 2.38 0.27 -11 -7 0 2.37 0.33 -11 -7 0 2.44 0.27 11 7 0 2.85 0.40 11 7 0 2.40 0.26 -11 7 0 2.47 0.32 11 7 0 2.55 0.27 11 7 0 2.58 0.24 11 7 0 2.26 0.28 -11 7 0 2.50 0.41 11 7 0 2.23 0.25 -11 7 0 2.54 0.30 -11 7 0 2.56 0.34 11 7 0 2.63 0.29 -11 7 0 2.46 0.33 12 -7 0 7.92 0.75 12 -7 0 7.04 0.58 -12 -7 0 7.47 0.54 -12 -7 0 8.02 0.63 -12 -7 0 7.71 0.58 12 -7 0 7.33 0.57 12 7 0 6.43 0.48 12 7 0 7.04 0.50 12 7 0 7.80 0.53 -12 7 0 7.35 0.61 12 7 0 6.65 0.47 -12 7 0 7.67 0.59 -12 7 0 7.25 0.67 12 7 0 7.08 0.46 12 7 0 7.97 0.57 12 7 0 8.01 0.66 -12 7 0 8.39 0.74 -12 7 0 8.52 0.74 -13 -7 0 11.04 0.71 -13 -7 0 11.27 0.71 -13 -7 0 11.61 0.75 13 -7 0 10.29 0.77 13 7 0 11.27 0.72 13 7 0 13.11 0.81 13 7 0 12.52 0.73 13 7 0 13.56 0.85 13 7 0 12.81 0.73 -13 7 0 13.36 0.79 -13 7 0 13.00 0.80 -14 -7 0 5.61 0.35 -14 -7 0 5.24 0.32 -14 -7 0 5.00 0.32 -14 7 0 4.54 0.35 14 7 0 5.24 0.37 -14 7 0 5.25 0.34 14 7 0 4.13 0.39 0 -8 0 1.13 0.23 0 -8 0 1.92 0.50 0 -8 0 1.31 0.43 0 -8 0 1.75 0.35 0 -8 0 1.75 0.64 0 8 0 0.57 0.33 0 8 0 0.75 0.42 0 8 0 1.16 0.62 1 -8 0 51.55 3.58 -1 -8 0 51.23 3.24 -1 -8 0 50.73 3.25 1 -8 0 52.76 3.01 -1 -8 0 52.27 3.07 1 -8 0 49.87 3.20 -1 -8 0 53.84 3.28 -1 -8 0 52.90 3.79 1 -8 0 50.40 3.31 1 -8 0 53.75 3.37 -1 -8 0 48.11 3.79 -1 -8 0 53.78 3.67 1 -8 0 53.21 3.98 1 -8 0 53.00 4.12 -2 -8 0 89.43 5.23 2 -8 0 87.84 4.98 2 -8 0 81.78 6.03 2 -8 0 90.32 5.14 2 -8 0 89.62 5.21 2 -8 0 84.70 5.95 2 -8 0 91.78 5.16 -2 -8 0 88.56 5.70 -2 -8 0 89.04 5.73 2 -8 0 91.35 5.39 -2 -8 0 84.98 5.61 -2 -8 0 88.00 5.25 2 8 0 87.06 5.23 -2 8 0 91.58 5.45 -2 8 0 81.27 6.05 -2 8 0 81.71 5.97 2 8 0 90.09 5.18 -2 8 0 88.69 5.16 2 8 0 92.59 5.52 2 8 0 85.77 5.27 2 8 0 88.46 5.83 2 8 0 91.66 5.96 2 8 0 88.39 5.57 -2 8 0 89.27 5.46 -2 8 0 86.15 5.24 3 -8 0 145.21 9.78 -3 -8 0 133.39 7.71 3 -8 0 143.10 9.34 -3 -8 0 130.57 7.93 -3 -8 0 123.51 7.95 -3 -8 0 131.57 7.73 3 -8 0 130.39 7.52 -3 -8 0 127.18 8.24 -3 8 0 138.78 8.03 3 8 0 129.65 8.25 3 8 0 129.88 7.70 3 8 0 130.25 7.91 -3 8 0 133.90 7.73 -3 8 0 143.43 8.12 3 8 0 137.02 8.21 -3 8 0 133.41 7.60 -4 -8 0 6.70 1.05 -4 -8 0 5.85 0.79 -4 -8 0 7.06 0.88 -4 -8 0 6.01 0.81 -4 -8 0 4.30 0.77 4 -8 0 5.27 0.72 4 8 0 5.77 0.77 -4 8 0 6.12 0.93 -4 8 0 5.30 0.77 -4 8 0 6.03 0.96 -4 8 0 5.36 0.69 -5 -8 0 2.21 0.67 -5 -8 0 2.46 0.69 -5 -8 0 2.12 0.75 -5 -8 0 2.09 0.44 -5 8 0 2.08 0.57 5 8 0 1.16 0.50 -5 8 0 1.70 0.65 -5 8 0 1.28 0.47 -6 -8 0 2.93 0.85 -6 -8 0 2.19 0.22 -6 -8 0 2.47 0.72 6 -8 0 2.06 0.27 -6 -8 0 1.89 1.02 6 -8 0 2.11 0.29 -6 8 0 2.75 0.97 6 8 0 0.74 0.54 -6 8 0 1.31 0.43 -6 8 0 1.71 0.23 6 8 0 1.93 0.63 6 8 0 1.90 0.21 6 8 0 1.50 0.22 -6 8 0 1.95 0.73 6 8 0 1.68 0.21 6 8 0 1.74 0.19 -6 8 0 1.59 0.39 -6 8 0 1.73 0.48 6 8 0 1.89 0.22 6 8 0 1.51 0.19 6 8 0 1.54 0.21 -6 8 0 1.67 0.60 6 8 0 1.88 0.24 6 8 0 1.60 0.19 -7 -8 0 0.97 0.75 7 -8 0 1.14 0.26 -7 -8 0 0.27 0.97 -7 -8 0 1.30 0.19 7 -8 0 1.48 0.25 -7 -8 0 2.68 0.70 -7 -8 0 2.05 0.87 7 -8 0 1.40 0.26 -7 -8 0 1.26 0.25 7 -8 0 1.14 0.26 7 -8 0 1.77 0.26 7 -8 0 1.18 0.23 -7 8 0 1.07 0.45 7 8 0 2.05 0.25 -7 8 0 1.76 0.24 7 8 0 1.83 0.24 7 8 0 1.98 0.23 7 8 0 1.75 0.21 7 8 0 1.77 0.20 -7 8 0 1.42 0.64 -7 8 0 1.73 0.34 7 8 0 1.74 0.19 -7 8 0 1.84 0.27 -7 8 0 1.65 0.26 -7 8 0 2.04 0.98 -7 8 0 1.77 0.28 7 8 0 1.89 0.23 7 8 0 2.25 0.79 7 8 0 1.83 0.19 7 8 0 1.84 0.21 8 -8 0 21.53 1.62 8 -8 0 21.91 1.56 8 -8 0 23.69 1.57 -8 -8 0 23.14 2.39 8 -8 0 23.94 1.56 8 -8 0 24.19 1.56 -8 -8 0 21.17 1.49 8 -8 0 23.33 1.56 8 -8 0 23.05 1.56 8 -8 0 23.66 1.56 8 -8 0 23.68 1.52 -8 -8 0 23.40 2.34 8 8 0 27.28 1.45 -8 8 0 25.78 2.13 8 8 0 27.03 1.51 8 8 0 26.91 1.53 8 8 0 26.66 1.55 8 8 0 25.88 2.40 -8 8 0 26.48 1.62 8 8 0 27.62 1.63 8 8 0 27.82 1.49 -8 8 0 26.90 1.64 -8 8 0 25.64 1.58 -8 8 0 26.47 1.72 -8 8 0 25.84 2.28 -8 8 0 26.64 1.57 9 -8 0 36.80 2.23 -9 -8 0 36.47 2.19 9 -8 0 34.09 2.34 9 -8 0 35.92 2.26 -9 -8 0 33.27 2.19 9 -8 0 36.65 2.27 -9 -8 0 37.82 3.20 9 -8 0 36.14 2.27 9 -8 0 33.18 2.23 -9 -8 0 38.07 3.17 9 -8 0 37.36 2.28 -9 -8 0 33.18 2.17 -9 -8 0 35.20 2.28 -9 -8 0 35.21 2.19 9 -8 0 35.86 2.24 -9 8 0 40.40 2.94 -9 8 0 41.00 2.33 9 8 0 42.29 2.23 9 8 0 43.23 2.20 -9 8 0 39.18 2.23 9 8 0 39.20 2.18 -9 8 0 41.36 2.31 -9 8 0 39.56 3.11 9 8 0 41.60 2.25 -9 8 0 41.69 2.45 -9 8 0 40.87 2.33 9 8 0 41.07 2.20 9 8 0 41.32 2.16 9 8 0 39.81 3.32 9 8 0 40.99 2.23 -10 -8 0 2.99 0.32 10 -8 0 2.76 0.40 -10 -8 0 3.54 0.57 -10 -8 0 4.66 0.95 10 -8 0 3.02 0.53 -10 -8 0 3.64 0.46 10 -8 0 3.10 0.37 10 8 0 4.10 0.37 10 8 0 3.99 0.34 10 8 0 3.94 0.36 10 8 0 3.70 0.46 -10 8 0 4.33 0.76 -10 8 0 2.94 0.48 11 -8 0 7.71 0.58 -11 -8 0 7.59 0.51 -11 -8 0 7.12 0.51 -11 -8 0 7.04 0.51 11 -8 0 6.68 0.55 -11 -8 0 7.53 0.52 11 -8 0 6.57 0.58 -11 -8 0 7.72 0.58 11 -8 0 7.05 0.52 -11 8 0 5.61 0.54 -11 8 0 6.16 0.51 11 8 0 6.22 0.50 -11 8 0 5.39 0.54 11 8 0 5.79 0.48 -11 8 0 6.57 0.65 11 8 0 5.98 0.44 -11 8 0 6.61 0.57 11 8 0 5.78 0.47 11 8 0 5.82 0.47 12 -8 0 5.17 0.46 12 -8 0 5.14 0.45 -12 -8 0 5.33 0.43 -12 -8 0 5.51 0.45 -12 -8 0 5.53 0.43 -12 -8 0 5.47 0.44 12 -8 0 5.82 0.58 -12 -8 0 5.76 0.49 -12 8 0 6.43 0.52 -12 8 0 6.78 0.60 -12 8 0 6.74 0.51 -12 8 0 6.67 0.50 12 8 0 6.82 0.57 12 8 0 6.14 0.44 12 8 0 6.18 0.41 12 8 0 6.70 0.45 -12 8 0 6.69 0.45 -13 -8 0 2.36 0.20 -13 -8 0 2.53 0.20 13 -8 0 2.46 0.24 -13 -8 0 2.37 0.22 -13 -8 0 2.57 0.23 -13 -8 0 2.38 0.25 -13 8 0 2.71 0.24 13 8 0 2.56 0.29 -13 8 0 2.80 0.27 13 8 0 2.65 0.27 13 8 0 2.60 0.21 -13 8 0 2.65 0.24 -13 8 0 2.49 0.31 13 8 0 2.27 0.20 -14 -8 0 1.33 0.13 -14 -8 0 1.19 0.12 14 8 0 1.20 0.15 -14 8 0 1.40 0.15 -14 8 0 1.53 0.13 0 -9 0 0.06 0.24 0 -9 0 0.20 0.33 0 -9 0 0.06 0.17 0 -9 0 -0.04 0.20 0 -9 0 0.85 0.49 0 -9 0 0.30 0.55 0 9 0 0.37 0.31 0 9 0 0.17 0.13 0 9 0 0.09 0.18 0 9 0 0.29 0.27 0 9 0 -0.08 0.24 1 -9 0 2.24 0.43 -1 -9 0 2.17 0.44 1 -9 0 2.95 0.52 1 -9 0 2.19 0.43 1 -9 0 2.68 0.34 -1 -9 0 2.05 0.35 1 -9 0 2.62 0.59 -1 -9 0 3.94 0.86 -1 -9 0 3.17 0.76 -1 -9 0 2.20 0.48 -1 -9 0 2.31 0.47 -1 -9 0 2.69 0.74 1 -9 0 2.05 0.54 1 -9 0 2.96 0.53 1 9 0 3.71 1.14 1 9 0 4.23 0.92 -1 9 0 3.33 0.50 -1 9 0 3.84 0.89 -1 9 0 3.43 0.56 -2 -9 0 48.71 3.18 2 -9 0 49.15 3.08 2 -9 0 49.19 2.89 -2 -9 0 46.64 3.60 -2 -9 0 49.06 3.80 2 -9 0 41.01 3.23 -2 -9 0 47.79 3.14 -2 -9 0 52.48 3.80 2 -9 0 49.06 3.06 -2 9 0 44.77 4.00 2 9 0 45.29 3.81 -2 9 0 50.18 3.09 -2 9 0 49.89 3.39 2 9 0 47.78 3.08 -2 9 0 50.12 3.20 2 9 0 47.11 3.77 2 9 0 45.86 3.16 -2 9 0 47.75 3.33 2 9 0 47.35 3.10 -2 9 0 50.34 4.03 3 -9 0 71.47 4.41 -3 -9 0 79.54 5.60 -3 -9 0 74.92 5.39 -3 -9 0 78.82 4.67 -3 -9 0 76.98 4.69 -3 -9 0 74.55 5.22 3 9 0 73.80 5.26 3 9 0 73.52 4.64 3 9 0 68.94 5.09 -3 9 0 74.27 4.94 3 9 0 73.40 4.61 3 9 0 71.17 4.53 -3 9 0 77.63 4.93 -3 9 0 71.53 4.49 -3 9 0 73.99 4.64 4 -9 0 34.15 2.97 5 -9 0 51.17 2.81 -5 -9 0 49.23 3.68 -5 -9 0 48.94 4.21 5 -9 0 45.00 2.79 -5 -9 0 48.89 3.73 5 -9 0 47.96 2.76 5 -9 0 49.24 2.79 5 -9 0 42.92 2.78 5 -9 0 46.32 2.78 5 -9 0 47.53 2.80 5 9 0 51.77 2.73 5 9 0 49.41 2.75 5 9 0 47.18 2.74 5 9 0 51.35 2.71 -5 9 0 53.80 4.06 5 9 0 52.22 3.57 -5 9 0 49.59 2.89 -5 9 0 55.60 3.99 -5 9 0 48.53 2.79 5 9 0 52.17 2.70 -5 9 0 44.94 2.79 5 9 0 50.26 2.75 5 9 0 46.36 2.75 6 -9 0 37.12 2.22 -6 -9 0 29.62 2.58 6 -9 0 30.63 1.88 6 -9 0 28.49 1.88 6 -9 0 30.34 1.90 6 -9 0 27.46 1.99 -6 -9 0 28.42 1.80 6 -9 0 33.31 1.91 -6 -9 0 30.05 2.63 -6 -9 0 28.64 1.80 -6 -9 0 29.30 1.89 -6 -9 0 32.89 3.61 6 -9 0 31.13 1.88 6 -9 0 30.64 1.86 6 -9 0 26.90 1.87 -6 9 0 37.08 3.18 -6 9 0 34.72 3.25 6 9 0 31.87 1.81 6 9 0 35.12 1.89 -6 9 0 32.38 2.20 -6 9 0 29.70 1.89 6 9 0 33.96 1.79 6 9 0 32.21 1.83 6 9 0 30.19 1.84 -6 9 0 30.47 1.89 6 9 0 30.54 1.85 -6 9 0 34.33 2.63 -6 9 0 33.96 2.02 -6 9 0 32.03 2.39 6 9 0 33.26 1.81 6 9 0 33.69 1.85 6 9 0 34.75 1.84 6 9 0 32.07 2.70 -7 -9 0 41.68 3.42 7 -9 0 45.00 2.58 7 -9 0 43.75 2.57 7 -9 0 45.95 2.55 7 -9 0 45.41 2.57 7 -9 0 48.63 2.61 -7 -9 0 45.29 2.59 7 -9 0 41.43 2.56 -7 -9 0 42.46 3.48 -7 -9 0 42.69 2.49 7 -9 0 45.03 2.60 -7 -9 0 42.28 2.48 7 -9 0 39.01 2.64 7 -9 0 41.10 2.58 7 9 0 47.21 2.49 -7 9 0 46.15 3.16 7 9 0 44.61 2.50 7 9 0 43.05 2.47 7 9 0 44.64 2.47 -7 9 0 41.62 2.59 -7 9 0 44.32 3.36 7 9 0 40.51 2.52 7 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0.49 9 9 0 5.05 0.43 -9 9 0 4.92 0.59 -9 9 0 4.48 0.49 9 9 0 4.80 0.37 -9 9 0 4.33 0.48 9 9 0 4.58 0.40 10 -9 0 11.19 0.77 10 -9 0 10.43 0.77 10 -9 0 11.43 0.82 10 -9 0 10.68 0.85 -10 -9 0 10.99 0.74 -10 -9 0 11.15 0.73 10 -9 0 11.51 0.81 -10 -9 0 11.82 0.75 -10 -9 0 11.58 0.84 -10 -9 0 11.30 0.75 10 -9 0 10.38 0.79 10 -9 0 11.35 0.81 10 9 0 11.02 0.74 10 9 0 11.18 0.75 10 9 0 10.48 0.75 -10 9 0 11.15 0.84 10 9 0 10.08 0.71 -10 9 0 10.61 1.44 10 9 0 10.35 0.73 10 9 0 10.36 0.73 -10 9 0 10.80 0.93 10 9 0 10.47 0.75 10 9 0 10.38 0.69 -10 9 0 10.78 0.76 -10 9 0 12.39 1.66 -10 9 0 10.64 0.83 10 9 0 10.04 0.72 10 9 0 14.50 1.91 -10 9 0 10.39 0.83 11 -9 0 6.55 0.51 11 -9 0 7.44 0.55 -11 -9 0 7.70 0.57 11 -9 0 7.34 0.60 -11 9 0 5.87 0.54 11 9 0 5.82 0.45 11 9 0 6.40 0.49 11 9 0 6.00 0.47 11 9 0 6.06 0.46 -11 9 0 6.37 0.50 11 9 0 6.20 0.47 11 9 0 6.08 0.47 11 9 0 6.28 0.46 -11 9 0 6.09 0.63 -11 9 0 6.37 0.55 11 9 0 6.03 0.43 -11 9 0 6.84 0.56 11 9 0 6.60 0.61 -12 -9 0 15.27 0.95 -12 -9 0 16.04 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6.25 -1 10 0 99.89 5.98 1 10 0 103.18 5.91 2 -10 0 28.71 2.53 -2 -10 0 36.45 2.51 -2 -10 0 36.88 2.55 2 -10 0 36.44 2.43 -2 -10 0 34.88 2.29 -2 -10 0 36.58 2.56 2 -10 0 35.71 2.20 -2 -10 0 34.79 2.95 2 -10 0 36.32 2.41 2 10 0 33.02 2.39 2 10 0 35.14 2.54 -2 10 0 31.96 3.24 -2 10 0 34.97 2.41 2 10 0 31.28 3.07 2 10 0 34.62 2.44 2 10 0 33.83 3.22 -2 10 0 33.41 3.35 -2 10 0 34.45 2.52 -2 10 0 35.04 2.64 -2 10 0 34.41 2.68 -3 -10 0 4.49 0.87 3 -10 0 2.02 0.80 -3 -10 0 2.45 0.58 -3 -10 0 2.32 0.53 3 -10 0 2.88 0.46 -3 10 0 3.12 0.54 3 10 0 2.76 0.95 -3 10 0 4.12 0.75 -3 10 0 2.94 0.61 -3 10 0 3.53 0.67 3 10 0 3.08 0.57 3 10 0 3.36 0.82 -4 -10 0 6.44 0.96 4 -10 0 6.42 0.51 4 -10 0 6.00 0.79 4 -10 0 6.11 0.51 4 -10 0 6.42 0.51 -4 -10 0 5.81 1.26 -4 -10 0 4.87 1.23 4 -10 0 6.53 0.52 -4 -10 0 6.07 0.91 4 -10 0 6.44 0.49 4 -10 0 3.80 1.31 4 -10 0 6.29 0.50 4 10 0 5.59 0.42 -4 10 0 5.68 0.79 4 10 0 5.63 0.44 4 10 0 5.33 0.87 4 10 0 5.93 0.50 -4 10 0 6.46 1.10 -4 10 0 5.61 0.88 4 10 0 5.64 0.43 -4 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2.80 6 10 0 48.86 2.76 -6 10 0 49.31 2.98 -6 10 0 46.91 2.87 -6 10 0 52.64 3.46 -6 10 0 58.48 4.55 6 10 0 50.10 2.82 6 10 0 52.39 2.80 -6 10 0 49.48 2.87 6 10 0 49.01 2.75 6 10 0 53.52 2.77 -6 10 0 47.91 2.87 -6 10 0 43.67 2.91 6 10 0 50.62 2.81 6 10 0 49.75 2.81 6 10 0 51.38 2.80 -6 10 0 51.22 3.66 -6 10 0 45.52 2.85 6 10 0 48.61 3.76 6 10 0 51.84 2.75 -6 10 0 44.05 2.90 -7 -10 0 79.42 4.41 7 -10 0 81.77 4.55 -7 -10 0 78.29 4.46 7 -10 0 75.92 4.45 -7 -10 0 76.50 5.46 7 -10 0 82.48 4.72 -7 -10 0 79.23 4.36 7 -10 0 87.50 4.53 -7 -10 0 76.10 5.52 7 -10 0 74.25 4.53 7 -10 0 77.83 4.63 -7 10 0 80.65 5.37 -7 10 0 70.86 4.71 7 10 0 77.11 4.34 7 10 0 83.03 4.58 -7 10 0 81.13 5.13 7 10 0 84.52 4.43 7 10 0 78.05 5.51 7 10 0 86.85 4.43 7 10 0 76.79 4.34 -7 10 0 74.34 4.47 7 10 0 81.76 4.39 -7 10 0 78.85 4.40 7 10 0 81.97 4.53 -8 -10 0 11.66 0.78 -8 -10 0 11.16 0.81 8 -10 0 11.56 0.85 8 -10 0 11.71 0.84 8 -10 0 12.76 0.90 8 -10 0 11.47 0.87 -8 -10 0 11.19 1.71 -8 -10 0 11.56 0.77 8 -10 0 10.83 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11.57 0.80 -10 -10 0 12.47 0.81 -10 -10 0 12.43 0.89 -10 -10 0 12.11 0.80 -10 10 0 13.07 0.91 10 10 0 12.52 0.82 -10 10 0 12.92 1.02 10 10 0 12.59 0.76 10 10 0 11.88 0.82 10 10 0 13.03 0.82 -10 10 0 12.50 0.83 10 10 0 11.88 0.79 10 10 0 11.80 0.79 10 10 0 12.44 0.82 -10 10 0 12.18 0.90 10 10 0 12.36 0.81 -10 10 0 12.57 0.91 10 10 0 11.84 0.78 -11 -10 0 15.64 0.95 -11 -10 0 15.47 1.02 -11 -10 0 16.73 0.97 -11 -10 0 16.17 0.95 -11 -10 0 16.28 0.96 11 -10 0 15.22 1.00 11 10 0 14.68 0.92 11 10 0 15.24 0.95 11 10 0 14.84 0.93 -11 10 0 15.45 1.03 11 10 0 14.85 0.89 11 10 0 13.94 0.91 -11 10 0 15.46 1.01 11 10 0 13.87 0.90 -11 10 0 14.65 0.94 11 10 0 14.91 0.93 -12 -10 0 2.80 0.27 -12 -10 0 2.73 0.26 -12 -10 0 2.74 0.26 12 -10 0 2.70 0.32 -12 -10 0 2.81 0.25 -12 -10 0 2.82 0.29 -12 10 0 3.05 0.26 -12 10 0 3.32 0.33 -12 10 0 3.18 0.29 12 10 0 3.14 0.35 12 10 0 3.08 0.27 12 10 0 3.16 0.27 12 10 0 2.58 0.24 12 10 0 2.98 0.31 -12 10 0 3.12 0.38 -13 -10 0 0.43 0.12 -13 -10 0 0.46 0.11 13 -10 0 0.42 0.17 13 -10 0 0.39 0.11 -13 -10 0 0.38 0.12 13 -10 0 0.46 0.12 -13 10 0 0.58 0.15 -13 10 0 0.55 0.19 0 -11 0 0.46 0.28 0 -11 0 0.11 0.14 0 -11 0 0.04 0.17 0 -11 0 0.08 0.30 0 -11 0 0.87 0.49 0 -11 0 1.01 0.45 0 11 0 0.30 0.28 0 11 0 0.08 0.32 0 11 0 0.34 0.20 0 11 0 0.87 0.59 0 11 0 0.03 0.27 0 11 0 0.77 0.62 0 11 0 0.70 0.40 1 -11 0 6.45 0.62 1 -11 0 5.21 0.77 -1 -11 0 5.49 0.81 1 -11 0 6.28 0.83 -1 -11 0 6.23 0.67 1 -11 0 6.07 0.83 -1 -11 0 5.96 0.82 -1 -11 0 7.59 0.86 1 11 0 8.08 0.91 -1 11 0 8.13 1.93 -1 11 0 8.32 0.91 -1 11 0 7.61 0.97 1 11 0 8.34 1.00 1 11 0 9.18 1.52 -1 11 0 7.48 2.31 -2 -11 0 14.63 1.21 -2 -11 0 15.77 1.45 -2 -11 0 15.87 1.46 2 -11 0 15.38 1.36 2 -11 0 13.08 1.80 -2 -11 0 15.16 1.46 -2 -11 0 14.56 1.81 -2 11 0 15.64 1.49 2 11 0 13.78 1.35 2 11 0 14.10 2.03 2 11 0 14.27 1.45 2 11 0 14.79 1.34 2 11 0 11.71 1.81 -2 11 0 15.06 1.35 -3 -11 0 125.22 7.45 -3 -11 0 127.34 8.24 3 -11 0 110.36 6.78 -3 -11 0 125.92 7.42 3 -11 0 127.69 7.08 -3 11 0 127.19 7.78 -3 11 0 126.82 7.25 3 11 0 139.54 6.85 3 11 0 109.98 6.69 3 11 0 108.59 6.64 3 11 0 124.18 7.36 3 11 0 121.44 6.68 -3 11 0 128.46 7.71 3 11 0 114.64 6.63 -3 11 0 127.25 7.43 -4 -11 0 59.56 3.36 4 -11 0 53.91 3.49 -4 -11 0 57.61 3.41 4 -11 0 57.85 3.39 -4 -11 0 51.72 3.44 -4 -11 0 60.84 4.18 -4 -11 0 57.52 3.36 -4 -11 0 65.09 4.29 -4 -11 0 65.15 3.44 4 -11 0 65.62 3.49 4 -11 0 63.32 3.45 4 -11 0 58.03 3.91 -4 -11 0 57.68 4.87 4 11 0 60.83 4.18 4 11 0 68.55 3.46 4 11 0 58.29 3.38 -4 11 0 61.69 3.98 4 11 0 62.92 3.38 4 11 0 61.00 3.35 -4 11 0 63.73 4.65 4 11 0 63.90 3.60 -4 11 0 63.84 4.20 -4 11 0 63.57 4.56 -5 -11 0 39.06 2.27 -5 -11 0 36.97 4.88 -5 -11 0 36.78 2.20 5 -11 0 38.97 2.27 5 -11 0 39.26 2.30 5 -11 0 34.55 2.32 -5 -11 0 36.34 3.03 -5 -11 0 38.53 3.13 5 -11 0 37.75 2.42 5 -11 0 40.58 2.32 -5 -11 0 36.90 2.20 5 -11 0 36.48 2.22 5 -11 0 41.37 2.30 5 -11 0 36.40 2.29 5 11 0 42.61 2.21 5 11 0 42.52 2.23 -5 11 0 38.11 2.28 -5 11 0 41.55 3.09 -5 11 0 38.92 2.35 5 11 0 41.69 2.25 -5 11 0 41.52 2.87 -5 11 0 32.94 2.32 -5 11 0 37.03 2.29 5 11 0 38.54 2.19 5 11 0 41.48 2.24 -5 11 0 41.63 2.41 -5 11 0 40.29 2.29 5 11 0 37.93 2.18 -5 11 0 39.31 3.51 5 11 0 36.72 2.23 -5 11 0 42.46 3.64 5 11 0 37.07 3.10 5 11 0 38.14 2.23 5 11 0 42.51 2.19 -6 -11 0 61.24 3.63 6 -11 0 61.10 3.61 -6 -11 0 55.56 3.57 -6 -11 0 59.04 3.55 6 -11 0 57.09 3.56 6 -11 0 64.09 3.68 6 -11 0 61.18 3.64 6 -11 0 64.20 3.65 6 -11 0 59.87 3.64 -6 -11 0 54.76 3.63 -6 -11 0 60.21 3.56 6 -11 0 58.47 3.67 -6 -11 0 59.77 4.61 6 -11 0 61.41 3.66 -6 -11 0 59.59 4.56 6 -11 0 65.07 3.68 -6 11 0 69.71 3.69 6 11 0 70.21 3.61 6 11 0 70.81 3.61 -6 11 0 68.94 4.33 6 11 0 70.47 3.54 -6 11 0 65.44 3.68 6 11 0 67.54 3.61 -6 11 0 60.35 3.72 -6 11 0 66.54 4.56 -6 11 0 64.13 3.67 6 11 0 69.78 3.63 6 11 0 70.87 3.60 -6 11 0 65.58 3.73 -6 11 0 69.73 3.82 6 11 0 73.36 3.57 -6 11 0 67.60 3.60 6 11 0 65.07 3.54 6 11 0 65.48 4.72 6 11 0 67.88 3.56 -6 11 0 65.15 3.66 7 -11 0 9.77 0.77 -7 -11 0 8.91 1.50 -7 -11 0 9.32 0.77 -7 -11 0 8.54 0.67 7 -11 0 9.48 0.79 -7 -11 0 8.85 0.68 -7 -11 0 9.92 1.42 7 11 0 11.20 0.67 7 11 0 9.23 0.72 7 11 0 11.00 0.70 7 11 0 10.74 0.72 -7 11 0 10.31 1.39 -7 11 0 12.34 1.25 7 11 0 11.24 1.47 -7 11 0 9.96 0.80 -7 11 0 9.41 0.77 7 11 0 11.56 0.74 7 11 0 10.39 0.68 -7 11 0 10.89 0.81 -7 11 0 10.89 0.85 -7 11 0 11.90 0.76 -7 11 0 8.19 0.79 -7 11 0 9.37 0.80 8 -11 0 3.10 0.41 -8 -11 0 2.87 0.39 -8 -11 0 2.78 0.30 8 -11 0 2.16 0.34 -8 -11 0 2.90 0.30 -8 -11 0 3.17 1.02 -8 -11 0 3.75 1.23 -8 -11 0 2.86 0.32 8 -11 0 2.92 0.39 -8 11 0 1.81 0.30 8 11 0 2.36 0.32 -8 11 0 2.16 0.35 8 11 0 2.30 0.26 8 11 0 2.25 0.26 8 11 0 4.02 0.86 8 11 0 2.30 0.29 -8 11 0 2.14 0.36 8 11 0 2.17 0.30 -8 11 0 2.07 0.35 -8 11 0 2.94 1.18 -8 11 0 2.61 0.62 8 11 0 1.92 0.30 8 11 0 2.19 0.25 -8 11 0 1.79 0.43 -9 -11 0 4.50 0.48 9 -11 0 3.64 0.50 9 -11 0 4.12 0.51 -9 11 0 4.92 0.53 9 11 0 5.03 0.49 9 11 0 4.80 0.43 9 11 0 4.39 0.46 -9 11 0 4.83 0.69 9 11 0 5.01 0.40 -9 11 0 6.73 1.05 9 11 0 5.66 0.56 9 11 0 6.92 1.30 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21.09 1.49 -7 -12 0 20.55 1.44 7 -12 0 22.56 1.50 7 -12 0 20.75 1.48 -7 -12 0 21.13 1.40 -7 -12 0 21.99 2.32 -7 -12 0 22.86 1.51 7 12 0 24.31 2.45 -7 12 0 25.62 2.33 7 12 0 26.30 1.43 -7 12 0 23.58 1.53 -7 12 0 22.29 1.57 7 12 0 26.36 1.39 7 12 0 26.89 1.47 -7 12 0 25.60 1.46 7 12 0 23.75 1.39 -7 12 0 24.23 1.52 7 12 0 23.78 1.47 7 12 0 24.79 1.41 -7 12 0 26.08 1.56 -7 12 0 26.84 2.17 -7 12 0 25.03 1.59 8 -12 0 26.34 1.56 -8 -12 0 27.50 1.53 -8 -12 0 25.38 2.59 -8 -12 0 28.12 1.57 -8 -12 0 28.16 1.50 -8 -12 0 27.35 1.62 8 -12 0 28.71 1.64 -8 -12 0 28.31 1.51 -8 -12 0 26.41 2.68 8 12 0 24.39 1.48 8 12 0 22.33 1.45 -8 12 0 22.98 2.30 8 12 0 22.16 1.50 8 12 0 22.72 1.43 -8 12 0 22.35 1.50 -8 12 0 22.01 2.10 -8 12 0 21.78 1.57 8 12 0 22.77 1.52 8 12 0 22.35 1.44 8 12 0 20.18 2.50 -9 -12 0 19.71 1.15 -9 -12 0 19.55 1.17 9 -12 0 17.27 1.17 -9 -12 0 20.88 1.17 -9 -12 0 19.17 2.58 9 -12 0 19.90 1.26 -9 -12 0 19.72 1.26 -9 -12 0 20.10 1.20 9 12 0 18.60 1.18 9 12 0 18.07 1.16 -9 12 0 16.72 1.84 9 12 0 17.10 1.10 -9 12 0 18.77 1.36 -9 12 0 18.63 1.27 9 12 0 17.54 1.15 -9 12 0 17.61 1.24 9 12 0 17.26 1.11 -9 12 0 17.83 2.06 -9 12 0 16.72 1.15 9 12 0 18.31 1.14 9 12 0 17.72 1.09 -10 -12 0 17.04 1.10 -10 -12 0 17.89 1.02 -10 -12 0 18.18 1.05 10 -12 0 17.20 1.10 -10 -12 0 18.14 1.03 -10 -12 0 17.93 1.03 -10 12 0 16.32 1.20 10 12 0 15.70 0.96 -10 12 0 15.38 1.01 10 12 0 15.67 1.01 10 12 0 16.03 1.03 10 12 0 15.61 0.98 -10 12 0 16.21 1.09 10 12 0 15.13 1.00 10 12 0 14.60 0.99 10 12 0 15.67 1.02 -10 12 0 16.76 1.12 10 12 0 15.55 1.03 10 12 0 15.26 0.98 11 -12 0 9.93 0.75 -11 -12 0 9.16 0.64 -11 -12 0 9.20 0.69 -11 -12 0 11.29 0.73 -11 -12 0 10.74 0.69 -11 -12 0 9.33 0.65 11 12 0 9.32 0.67 -11 12 0 9.83 0.78 11 12 0 9.55 0.58 -11 12 0 10.07 0.68 11 12 0 9.30 0.60 11 12 0 8.51 0.64 -11 12 0 10.01 0.64 11 12 0 9.72 0.61 -11 12 0 10.07 0.72 11 12 0 9.81 0.71 11 12 0 11.32 0.73 11 12 0 11.35 0.80 -12 -12 0 1.38 0.24 12 -12 0 1.32 0.20 -12 -12 0 1.45 0.17 -12 -12 0 1.26 0.19 -12 -12 0 1.35 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1.58 0.28 2 -13 0 1.58 0.30 -2 -13 0 1.26 0.24 2 -13 0 1.71 0.30 -2 -13 0 2.07 0.52 2 -13 0 1.49 0.22 -2 -13 0 1.22 0.21 2 -13 0 1.61 0.26 2 -13 0 1.54 0.29 2 -13 0 1.98 0.38 2 -13 0 1.65 0.27 -2 -13 0 1.35 0.58 2 13 0 1.55 0.20 -2 13 0 1.53 0.24 2 13 0 1.61 0.21 2 13 0 1.32 0.20 2 13 0 1.55 0.20 -2 13 0 2.41 0.71 -2 13 0 1.47 0.24 -2 13 0 1.73 0.25 2 13 0 1.85 0.30 -2 13 0 1.92 0.31 2 13 0 1.41 0.21 2 13 0 1.30 0.19 -2 13 0 2.65 0.88 -2 13 0 1.48 0.21 2 13 0 1.47 0.22 2 13 0 2.44 0.76 3 -13 0 38.04 2.48 -3 -13 0 37.91 2.32 -3 -13 0 37.04 3.12 3 -13 0 41.67 2.41 -3 -13 0 37.19 3.07 -3 -13 0 39.81 2.38 -3 -13 0 38.77 2.38 -3 -13 0 37.07 3.10 3 -13 0 38.53 2.37 3 -13 0 37.26 2.29 -3 -13 0 37.08 2.43 -3 -13 0 37.38 2.66 -3 -13 0 41.85 4.04 3 -13 0 40.42 2.39 3 -13 0 40.70 2.43 3 -13 0 37.52 2.34 -3 -13 0 37.97 2.31 3 -13 0 37.33 2.70 3 -13 0 38.18 2.39 -3 -13 0 35.78 2.76 -3 13 0 47.39 2.49 3 13 0 46.20 2.34 -3 13 0 45.78 3.05 3 13 0 46.78 2.34 -3 13 0 45.03 3.23 3 13 0 46.68 2.32 -3 13 0 45.18 2.40 3 13 0 44.35 3.12 3 13 0 45.77 2.34 3 13 0 43.90 2.35 3 13 0 44.11 2.35 4 -13 0 91.51 4.86 -4 -13 0 84.13 4.72 -4 -13 0 83.92 5.73 -4 -13 0 83.50 6.69 -4 -13 0 83.75 4.78 -4 -13 0 80.41 4.84 -4 -13 0 86.22 5.73 4 -13 0 85.85 4.90 4 -13 0 92.31 4.83 4 -13 0 86.20 4.83 -4 -13 0 87.14 4.73 4 -13 0 86.63 4.80 4 -13 0 84.80 4.75 4 -13 0 91.07 4.82 -4 -13 0 89.82 4.80 -4 13 0 88.63 5.50 -4 13 0 82.10 4.71 -4 13 0 78.33 4.78 4 13 0 85.64 4.74 -4 13 0 79.40 4.84 4 13 0 90.67 4.73 4 13 0 88.96 4.71 -4 13 0 83.08 4.79 4 13 0 92.76 4.78 4 13 0 86.05 4.75 4 13 0 88.82 4.74 -4 13 0 83.19 4.79 -4 13 0 88.08 4.88 4 13 0 88.49 4.73 -4 13 0 85.25 4.85 -4 13 0 85.95 5.70 4 13 0 90.10 4.71 4 13 0 79.57 5.64 5 -13 0 26.14 1.57 5 -13 0 26.35 1.60 -5 -13 0 26.74 1.57 -5 -13 0 24.10 1.59 5 -13 0 24.73 1.64 -5 -13 0 25.64 2.39 -5 -13 0 21.91 2.14 5 -13 0 25.00 1.70 -5 -13 0 25.94 1.49 -5 -13 0 25.15 1.49 -5 -13 0 23.83 2.57 5 -13 0 25.82 1.66 5 -13 0 25.63 1.58 -5 -13 0 25.70 2.47 5 -13 0 24.01 1.71 -5 -13 0 25.01 1.54 5 -13 0 24.77 1.51 5 13 0 25.31 1.53 5 13 0 26.38 1.48 -5 13 0 25.03 1.62 -5 13 0 24.54 1.49 5 13 0 24.28 1.55 -5 13 0 25.17 2.34 -5 13 0 24.75 1.59 -5 13 0 23.03 1.61 5 13 0 23.25 2.33 5 13 0 23.49 1.51 -5 13 0 23.07 1.55 5 13 0 23.27 1.44 5 13 0 26.37 1.54 -5 13 0 24.00 1.56 5 13 0 25.74 1.51 -5 13 0 25.56 2.15 5 13 0 26.92 1.49 -5 13 0 26.28 1.69 5 13 0 24.20 1.46 -6 -13 0 3.89 0.46 6 -13 0 4.38 0.46 6 -13 0 4.42 0.43 6 -13 0 4.13 0.45 6 -13 0 4.30 0.45 -6 -13 0 4.33 0.37 -6 -13 0 4.28 0.36 6 -13 0 3.91 0.36 -6 -13 0 3.52 0.49 6 -13 0 3.82 0.45 -6 -13 0 6.21 1.58 -6 -13 0 6.56 1.75 -6 13 0 3.25 0.42 6 13 0 4.74 0.95 6 13 0 3.11 0.32 -6 13 0 3.67 0.59 -6 13 0 3.18 0.78 -6 13 0 3.54 0.52 -6 13 0 4.48 0.67 6 13 0 3.33 0.37 6 13 0 3.38 0.34 6 13 0 3.29 0.32 6 13 0 3.05 0.36 -6 13 0 3.16 0.36 6 13 0 3.53 0.37 6 13 0 3.34 0.37 -6 13 0 3.45 0.50 -7 -13 0 3.82 0.35 7 -13 0 4.09 0.46 -7 -13 0 3.98 0.36 -7 -13 0 3.66 0.40 -7 -13 0 2.90 1.21 7 -13 0 3.79 0.42 -7 -13 0 2.95 1.00 -7 -13 0 3.95 0.37 -7 13 0 2.68 0.38 -7 13 0 3.17 0.35 -7 13 0 3.98 0.70 -7 13 0 2.76 0.42 7 13 0 2.90 0.35 7 13 0 2.85 0.31 7 13 0 2.98 0.35 -7 13 0 4.39 0.86 -7 13 0 3.46 0.45 7 13 0 3.19 0.33 -7 13 0 3.63 0.54 7 13 0 2.81 0.29 -7 13 0 2.67 0.39 7 13 0 3.05 0.30 -7 13 0 3.24 0.43 8 -13 0 14.86 1.10 -8 -13 0 16.17 1.87 -8 -13 0 15.47 1.04 -8 -13 0 15.57 0.95 -8 -13 0 15.94 0.93 8 -13 0 15.17 1.03 -8 -13 0 15.18 0.92 -8 -13 0 15.01 0.97 8 13 0 12.27 0.93 8 13 0 12.75 0.85 -8 13 0 12.63 1.01 -8 13 0 11.35 1.01 8 13 0 11.86 0.86 -8 13 0 13.15 1.11 8 13 0 12.46 0.91 -8 13 0 13.50 1.51 -8 13 0 16.77 1.73 8 13 0 13.18 0.90 -8 13 0 12.72 0.93 9 -13 0 0.66 0.20 -9 -13 0 0.96 0.20 9 -13 0 0.72 0.19 -9 -13 0 0.87 0.18 -9 -13 0 1.01 0.20 -9 -13 0 1.00 0.25 -9 -13 0 0.83 0.19 9 13 0 0.83 0.21 9 13 0 0.86 0.20 9 13 0 0.86 0.16 -9 13 0 0.85 0.20 -9 13 0 0.92 0.30 -9 13 0 1.13 0.28 9 13 0 0.77 0.20 9 13 0 0.80 0.20 9 13 0 0.70 0.16 -9 13 0 0.80 0.21 9 13 0 0.91 0.17 -10 -13 0 0.92 0.20 -10 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14 0 72.25 4.33 0 14 0 71.57 4.18 0 14 0 69.16 4.16 0 14 0 70.14 5.03 0 14 0 70.37 4.19 0 14 0 74.71 4.25 0 14 0 67.78 4.16 0 14 0 70.11 4.87 0 14 0 65.14 4.19 1 -14 0 53.78 2.91 -1 -14 0 53.36 3.68 1 -14 0 49.93 2.98 -1 -14 0 51.87 3.64 1 -14 0 52.72 3.55 -1 -14 0 47.06 4.59 -1 -14 0 51.27 2.83 -1 -14 0 49.19 2.93 -1 -14 0 52.23 3.63 -1 -14 0 51.28 2.81 1 -14 0 51.99 3.57 1 -14 0 52.73 3.10 1 -14 0 46.35 3.57 1 -14 0 51.17 2.84 1 -14 0 56.71 2.94 -1 -14 0 55.06 2.91 -1 -14 0 52.74 3.15 1 -14 0 50.41 2.79 -1 -14 0 51.76 2.87 1 14 0 49.64 2.81 1 14 0 54.51 4.00 -1 14 0 51.62 2.91 -1 14 0 49.53 2.84 1 14 0 50.89 2.98 1 14 0 48.83 2.84 1 14 0 47.77 2.81 -1 14 0 44.47 2.86 -1 14 0 50.77 2.87 -1 14 0 49.17 3.69 -1 14 0 46.41 2.82 1 14 0 46.14 2.82 1 14 0 50.77 2.83 1 14 0 45.08 2.83 -1 14 0 49.46 3.52 -1 14 0 48.31 2.83 1 14 0 44.55 2.81 -1 14 0 46.44 2.97 1 14 0 51.24 3.39 1 14 0 55.38 3.86 -1 14 0 43.91 2.79 2 -14 0 53.66 3.12 -2 -14 0 50.63 3.33 -2 -14 0 53.50 3.78 2 -14 0 59.88 3.08 -2 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15 0 14.29 1.19 3 15 0 14.46 1.65 -3 15 0 15.87 1.06 -3 15 0 15.91 1.05 3 15 0 15.24 0.95 -3 15 0 17.25 1.60 -3 15 0 15.25 1.71 -3 15 0 15.93 1.07 -3 15 0 15.89 1.00 3 15 0 14.35 0.88 3 15 0 15.62 0.91 -4 -15 0 24.73 1.36 -4 -15 0 23.82 1.50 -4 -15 0 24.82 1.36 4 -15 0 24.08 1.38 4 -15 0 24.84 1.48 4 -15 0 25.42 1.56 -4 -15 0 21.65 2.23 4 -15 0 21.23 1.53 -4 -15 0 24.70 1.43 -4 -15 0 22.10 2.26 -4 -15 0 22.09 2.46 -4 -15 0 23.84 1.96 4 15 0 20.17 1.32 4 15 0 19.20 1.34 -4 15 0 18.92 1.38 -4 15 0 20.82 1.93 4 15 0 18.35 2.03 4 15 0 20.07 1.30 4 15 0 21.33 1.38 -4 15 0 20.03 2.07 -4 15 0 19.87 1.47 4 15 0 19.92 1.33 4 15 0 18.73 1.32 -5 -15 0 28.40 2.59 -5 -15 0 28.62 2.25 5 -15 0 27.98 1.66 5 -15 0 27.61 1.58 -5 -15 0 28.32 1.63 -5 -15 0 28.48 1.58 -5 -15 0 27.69 1.71 5 -15 0 30.27 1.77 5 -15 0 28.63 1.66 -5 -15 0 28.44 1.57 -5 -15 0 25.25 2.60 5 -15 0 29.45 1.68 -5 -15 0 29.54 1.67 5 15 0 26.00 1.60 5 15 0 24.49 1.56 5 15 0 23.94 1.58 -5 15 0 23.61 1.66 -5 15 0 23.12 1.68 5 15 0 23.02 1.52 -5 15 0 23.06 2.41 5 15 0 22.72 1.57 -5 15 0 24.68 1.65 -5 15 0 23.64 1.62 5 15 0 24.72 1.52 5 15 0 23.19 1.56 5 15 0 24.31 1.53 -5 15 0 25.23 1.74 -5 15 0 25.31 2.25 -6 -15 0 47.92 3.90 -6 -15 0 38.67 3.51 6 -15 0 39.88 2.45 -6 -15 0 45.89 3.23 -6 -15 0 40.21 2.42 -6 -15 0 39.75 3.56 6 -15 0 44.18 2.55 -6 -15 0 43.91 2.50 6 -15 0 43.12 2.46 -6 -15 0 43.16 2.39 -6 -15 0 42.06 2.39 -6 -15 0 39.73 2.49 -6 15 0 41.92 2.51 -6 15 0 38.59 2.53 6 15 0 43.52 2.36 6 15 0 38.33 2.32 -6 15 0 43.68 3.47 -6 15 0 38.74 3.13 6 15 0 44.00 2.42 6 15 0 40.23 2.42 6 15 0 43.53 2.38 6 15 0 42.61 2.43 -6 15 0 43.98 2.63 6 15 0 40.32 2.41 -6 15 0 39.48 2.46 -6 15 0 39.62 2.51 6 15 0 41.25 2.36 6 15 0 37.90 3.51 -7 -15 0 8.28 1.37 -7 -15 0 6.43 0.70 -7 -15 0 7.44 0.71 7 -15 0 5.82 0.67 7 -15 0 7.33 0.85 -7 -15 0 6.24 0.61 -7 -15 0 7.95 0.81 -7 -15 0 6.09 0.57 -7 -15 0 6.30 0.52 -7 -15 0 6.14 0.57 7 15 0 6.35 0.56 -7 15 0 10.47 1.94 7 15 0 6.61 0.49 -7 15 0 6.53 0.69 7 15 0 7.02 0.54 -7 15 0 6.51 0.73 7 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21 0 0.09 0.12 8 21 0 0.18 0.05 9 21 0 0.80 0.10 0 -22 0 15.55 1.15 0 -22 0 15.59 1.06 0 -22 0 15.12 0.99 0 -22 0 16.56 1.09 0 22 0 14.62 0.99 0 22 0 14.52 1.02 0 22 0 15.05 1.01 0 22 0 14.72 0.98 0 22 0 16.59 1.16 1 -22 0 23.00 1.36 -1 -22 0 21.88 1.35 -1 -22 0 23.17 1.45 -1 -22 0 20.58 1.36 -1 -22 0 22.49 1.43 -1 -22 0 22.96 1.36 1 -22 0 23.67 1.52 -1 -22 0 23.11 1.53 1 -22 0 23.04 1.43 1 -22 0 22.51 1.43 1 22 0 20.72 1.38 1 22 0 21.27 1.34 -1 22 0 21.29 1.38 1 22 0 24.01 1.52 -1 22 0 21.58 1.36 1 22 0 22.43 1.36 -1 22 0 23.30 1.54 -1 22 0 21.67 1.36 -1 22 0 21.15 1.39 1 22 0 22.03 1.37 -2 -22 0 23.23 1.58 2 -22 0 24.63 1.49 -2 -22 0 24.47 1.43 -2 -22 0 23.79 1.51 -2 -22 0 24.80 1.50 -2 -22 0 22.48 1.46 -2 -22 0 23.22 1.43 2 -22 0 23.19 1.50 2 -22 0 24.32 1.55 2 -22 0 24.67 1.49 2 -22 0 24.45 1.42 2 22 0 23.94 1.44 -2 22 0 23.57 1.46 -2 22 0 23.09 1.44 -2 22 0 24.13 1.61 -2 22 0 23.03 1.44 -2 22 0 22.89 1.48 2 22 0 24.03 1.41 2 22 0 23.19 1.46 -3 -22 0 24.19 1.56 -3 -22 0 23.93 1.41 3 -22 0 23.91 1.45 -3 -22 0 24.21 1.44 -3 -22 0 23.36 1.48 3 -22 0 24.21 1.39 3 -22 0 26.02 1.51 3 -22 0 23.96 1.56 -3 -22 0 23.31 1.48 -3 -22 0 24.65 1.47 -3 -22 0 24.11 1.44 3 -22 0 26.29 1.75 3 22 0 21.18 1.37 -3 22 0 23.35 1.44 -3 22 0 23.20 1.47 3 22 0 23.91 1.45 3 22 0 23.02 1.42 -3 22 0 22.32 1.43 -3 22 0 22.83 1.45 -3 22 0 23.21 1.60 3 22 0 23.16 1.39 -4 -22 0 14.65 0.87 -4 -22 0 14.34 0.83 -4 -22 0 13.50 0.94 -4 -22 0 14.25 1.02 4 -22 0 12.95 0.86 4 -22 0 13.65 0.83 -4 -22 0 14.39 0.91 -4 -22 0 15.48 1.14 -4 -22 0 15.07 0.95 -4 22 0 13.86 0.92 4 22 0 13.89 0.90 -4 22 0 12.90 0.89 4 22 0 13.33 0.84 -4 22 0 13.59 1.07 4 22 0 12.62 0.88 -4 22 0 12.92 0.90 4 22 0 12.72 0.83 -4 22 0 14.24 0.93 -5 -22 0 3.23 0.28 -5 -22 0 2.86 0.30 -5 -22 0 3.10 0.34 -5 -22 0 2.97 0.29 -5 -22 0 3.09 0.23 -5 -22 0 3.20 0.32 -5 -22 0 3.05 0.34 5 22 0 2.66 0.28 5 22 0 2.75 0.25 -5 22 0 2.87 0.30 5 22 0 2.57 0.23 -5 22 0 2.76 0.30 -5 22 0 2.60 0.30 -5 22 0 2.63 0.28 -5 22 0 2.42 0.39 5 22 0 2.56 0.28 -6 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58.72 3.53 0 4 9 63.52 3.50 0 4 9 62.47 3.70 0 4 9 58.84 3.55 0 4 9 58.15 3.45 0 4 9 60.32 3.49 0 4 9 61.87 3.45 0 4 9 60.45 3.50 0 4 9 58.34 3.44 0 4 9 54.90 3.51 0 4 9 58.59 3.44 0 4 -9 54.54 3.78 0 4 9 58.38 3.46 0 4 9 59.46 3.49 0 4 9 55.07 3.53 0 4 -9 54.96 3.73 0 4 9 56.86 3.47 0 4 9 58.98 3.50 1 -4 9 23.50 1.65 1 -4 9 25.19 1.56 1 -4 9 25.95 1.34 1 -4 9 24.11 2.05 -1 -4 -9 18.69 4.30 1 -4 9 24.68 1.32 1 -4 9 27.41 2.21 1 -4 9 20.94 2.92 1 4 9 19.45 1.42 1 4 9 21.82 1.33 1 4 9 20.26 1.32 1 4 9 21.03 1.61 1 4 9 20.67 1.31 1 4 9 20.35 1.31 1 4 9 22.23 1.59 1 4 9 19.90 1.38 1 4 9 19.38 1.27 1 4 9 20.44 1.36 1 4 9 21.57 1.50 1 4 9 21.79 1.37 1 4 9 20.49 1.35 1 4 9 18.83 1.38 1 4 9 20.65 1.33 2 -4 9 27.74 1.73 2 -4 9 27.88 1.68 2 -4 9 29.36 1.80 2 -4 9 29.05 1.79 2 -4 9 27.00 1.91 2 -4 9 29.44 1.98 2 -4 9 27.43 1.76 2 -4 9 27.99 1.72 2 -4 9 28.75 1.79 2 -4 9 26.31 2.56 2 -4 9 28.58 1.86 2 -4 9 26.16 2.36 2 -4 9 27.97 1.89 2 -4 9 28.28 1.70 2 -4 9 29.66 1.76 2 -4 9 28.49 1.86 2 -4 9 27.30 1.79 2 -4 9 28.55 1.87 2 -4 9 28.25 1.76 2 -4 9 26.14 1.76 2 -4 9 27.62 1.69 2 4 9 28.53 1.82 2 4 9 30.19 1.74 2 4 9 30.05 1.73 2 4 9 30.37 1.92 2 4 9 28.48 1.73 2 4 9 29.80 1.81 2 4 9 29.91 1.75 2 4 9 31.88 1.73 2 4 9 31.11 1.77 2 4 9 29.48 1.85 2 4 9 30.03 1.80 2 4 9 29.41 1.75 2 4 9 31.80 1.79 2 4 9 30.09 1.72 2 4 9 30.51 1.80 2 4 9 31.10 2.05 2 4 9 28.65 1.68 2 4 9 30.48 1.72 2 4 9 29.72 1.77 2 4 9 29.06 1.69 3 -4 9 26.93 1.71 3 -4 9 23.63 1.58 3 -4 9 24.65 1.60 3 -4 9 25.48 1.76 3 -4 9 25.56 1.55 3 -4 9 23.74 1.61 3 -4 9 25.60 1.57 3 -4 9 25.63 1.59 3 -4 9 24.46 1.59 3 -4 9 26.28 1.50 3 -4 9 25.97 2.42 3 -4 9 24.42 1.51 3 -4 9 26.40 1.72 3 -4 9 25.32 1.57 3 -4 9 23.60 1.76 3 -4 9 22.14 2.11 3 -4 9 26.47 1.58 3 -4 9 24.59 1.64 3 -4 9 26.89 1.50 3 -4 9 25.13 1.50 3 -4 9 24.93 1.68 3 4 9 24.21 1.48 3 4 9 27.06 1.58 3 4 9 22.17 1.47 3 4 9 23.35 1.64 3 4 9 24.96 1.48 3 4 9 24.40 1.60 3 4 9 25.42 1.55 3 4 9 24.55 1.81 3 4 9 27.34 1.52 3 4 9 27.26 1.63 3 4 9 25.71 1.51 3 4 9 27.04 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15.85 1.05 -7 12 9 15.94 1.10 -7 12 9 14.72 0.97 -7 12 9 16.59 1.06 -7 12 9 16.00 1.11 7 12 -9 16.18 1.01 -7 12 9 14.52 1.10 7 12 -9 14.95 1.10 -6 -12 9 21.77 2.95 6 -12 -9 16.98 1.26 -6 -12 9 17.89 1.26 -6 -12 9 17.56 2.01 6 -12 -9 17.50 1.21 -6 12 9 16.65 1.09 -6 12 9 17.21 1.11 6 12 -9 17.80 1.13 -6 12 9 17.61 1.52 -6 12 9 20.70 1.33 -6 12 9 18.94 1.32 6 12 -9 16.91 1.20 6 12 -9 17.67 1.24 6 12 -9 16.36 1.10 6 12 -9 17.60 1.15 6 12 -9 20.64 2.17 -6 12 9 17.10 1.30 -5 -12 9 36.83 3.97 -5 -12 9 33.77 2.12 5 -12 -9 34.17 2.00 5 -12 -9 34.58 2.06 -5 -12 9 34.47 2.93 5 12 -9 32.35 1.94 -5 12 9 31.32 1.94 -5 12 9 30.58 1.91 -5 12 9 32.55 1.98 5 12 -9 31.91 1.92 -5 12 9 32.66 1.97 5 12 -9 30.67 3.00 5 12 -9 31.41 3.20 -5 12 9 32.34 1.91 -5 12 9 31.86 2.16 -5 12 9 32.16 2.11 -5 12 9 33.01 1.97 4 -12 -9 17.67 1.25 -4 -12 9 16.63 1.22 4 -12 -9 17.42 1.24 -4 -12 9 19.20 1.99 -4 -12 9 18.28 1.40 4 -12 -9 17.17 1.28 -4 -12 9 21.52 2.83 -4 -12 9 20.17 1.36 4 -12 -9 18.28 1.35 -4 -12 9 20.81 1.97 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47.58 2.61 2 2 10 46.24 2.94 2 2 10 44.86 2.69 3 -2 10 14.69 0.99 3 -2 10 14.40 0.92 3 -2 10 13.81 0.96 3 -2 10 14.95 1.00 3 -2 10 13.98 1.09 3 -2 10 13.93 1.02 3 -2 10 18.10 2.57 3 -2 10 13.53 1.04 3 -2 10 13.94 0.93 3 -2 10 14.22 1.04 3 -2 10 14.78 0.93 3 -2 10 14.87 1.01 3 -2 10 14.03 1.13 3 -2 10 13.57 1.07 3 -2 10 13.28 1.20 3 -2 10 14.81 0.92 3 -2 10 17.74 1.95 3 -2 10 15.29 1.11 3 -2 10 15.33 1.03 3 -2 10 15.00 1.00 3 -2 10 13.26 1.09 3 2 10 13.34 1.08 3 2 10 14.72 0.98 3 2 10 14.57 1.08 3 2 10 14.02 1.23 3 2 10 13.41 1.04 3 2 10 13.95 1.03 3 2 10 15.04 0.95 3 2 10 13.83 0.98 3 2 10 13.27 1.07 3 2 10 14.67 1.00 3 2 10 15.14 1.04 3 2 10 14.73 0.94 3 2 10 15.63 0.94 3 2 10 14.73 0.98 3 2 10 14.42 0.95 3 2 10 13.52 1.00 4 -2 10 15.96 1.09 4 -2 10 15.36 1.17 4 -2 10 15.84 1.11 4 -2 10 16.37 1.20 4 -2 10 16.16 1.02 4 -2 10 16.03 1.21 4 -2 10 16.34 1.06 4 -2 10 16.63 1.10 4 -2 10 16.05 1.30 4 -2 10 16.77 1.02 4 -2 10 15.82 1.06 4 -2 10 16.87 1.14 4 -2 10 16.17 1.03 4 -2 10 15.40 1.15 4 -2 10 17.22 1.11 4 -2 10 16.45 1.12 4 -2 10 16.36 1.15 4 -2 10 16.39 1.02 4 -2 10 14.97 1.22 4 2 10 16.60 1.05 4 2 10 16.61 1.14 4 2 10 17.01 1.19 4 2 10 16.47 1.08 4 2 10 15.71 1.20 4 2 10 16.37 1.03 4 2 10 16.79 1.32 4 2 10 16.61 1.14 4 2 10 16.17 1.02 4 2 10 16.89 1.09 4 2 10 17.08 1.12 4 2 10 16.67 1.09 4 2 10 15.93 1.16 4 2 10 16.81 1.04 4 2 10 17.00 1.09 5 -2 10 8.24 0.59 5 -2 10 7.90 0.65 5 -2 10 9.23 0.68 5 -2 10 8.80 0.70 5 -2 10 8.80 0.64 5 -2 10 8.81 0.69 5 -2 10 8.56 0.84 5 -2 10 8.31 0.59 5 -2 10 8.64 0.61 5 -2 10 8.70 0.71 5 -2 10 8.35 0.65 5 -2 10 7.56 0.77 5 -2 10 8.02 0.73 5 -2 10 7.60 0.69 5 -2 10 8.84 0.78 5 2 10 8.50 0.73 5 2 10 9.07 0.71 5 2 10 8.66 0.61 5 2 10 9.20 0.63 5 2 10 8.93 0.60 5 2 10 8.81 0.66 5 2 10 8.53 0.61 5 2 10 9.26 0.76 5 2 10 8.06 0.64 5 2 10 9.28 0.67 5 2 10 9.10 0.71 5 2 10 9.18 0.66 5 2 10 9.50 0.63 5 2 10 9.38 0.79 5 2 10 9.04 0.84 5 2 10 9.01 0.69 5 2 10 9.23 0.67 6 -2 10 5.52 0.44 6 -2 10 5.16 0.55 6 -2 10 5.34 0.44 6 -2 10 5.00 0.46 6 -2 10 5.11 0.53 6 -2 10 5.35 0.37 6 -2 10 4.64 0.55 6 -2 10 5.22 0.48 6 -2 10 4.94 0.43 6 -2 10 5.46 0.43 6 2 10 4.74 0.42 6 2 10 4.74 0.48 6 2 10 4.47 0.54 6 2 10 4.76 0.40 6 2 10 5.03 0.42 6 2 10 4.72 0.45 6 2 10 5.08 0.41 6 2 10 4.52 0.50 6 2 10 5.08 0.53 6 2 10 4.82 0.41 6 2 10 4.76 0.37 6 2 10 4.68 0.43 6 2 10 4.72 0.45 7 -2 10 11.58 0.72 7 -2 10 11.52 0.72 7 -2 10 10.91 0.70 7 -2 10 11.18 0.83 7 -2 10 11.77 0.71 7 -2 10 10.93 0.74 7 -2 10 11.18 0.75 7 -2 10 11.50 0.81 7 -2 10 10.18 0.81 7 2 10 11.24 0.70 7 2 10 10.69 0.68 7 2 10 11.42 0.79 7 2 10 11.27 0.72 7 2 10 10.47 0.72 7 2 10 10.89 0.70 7 2 10 10.79 0.79 7 2 10 10.61 0.72 7 2 10 11.09 0.74 7 2 10 10.51 0.78 8 -2 10 4.57 0.33 8 -2 10 4.58 0.34 8 -2 10 4.37 0.30 8 -2 10 4.51 0.31 8 -2 10 4.40 0.38 8 -2 10 4.06 0.35 8 -2 10 4.25 0.28 8 -2 10 4.79 0.38 8 2 10 3.83 0.30 8 2 10 3.55 0.29 8 2 10 3.48 0.30 8 2 10 3.90 0.36 8 2 10 3.96 0.36 8 2 10 3.79 0.27 8 2 10 3.39 0.27 8 2 10 3.33 0.31 13 -3 -10 5.43 0.36 13 -3 -10 4.80 0.38 13 -3 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0.44 -4 -3 10 3.70 0.49 -4 -3 10 3.83 1.10 -4 -3 10 3.74 0.38 -4 -3 10 3.66 0.43 -4 -3 10 4.43 0.83 -4 -3 10 3.25 0.30 -4 3 10 3.37 0.38 -4 3 10 3.61 0.88 4 3 -10 2.82 0.80 -4 3 10 3.42 0.36 -4 3 10 3.67 0.50 -4 3 10 3.24 0.36 -4 3 10 3.64 0.41 -4 3 10 3.11 0.29 -4 3 10 3.33 0.40 4 3 -10 3.20 0.94 -3 -3 10 9.42 0.75 -3 -3 10 8.14 0.77 -3 -3 10 8.11 0.69 -3 -3 10 7.81 0.60 -3 -3 10 7.84 1.22 -3 -3 10 7.07 1.14 -3 -3 10 7.26 0.71 -3 -3 10 7.51 0.57 -3 -3 10 8.28 0.63 -3 3 10 7.41 0.57 3 3 -10 7.26 0.99 -3 3 10 7.52 0.58 3 3 -10 6.65 0.94 -3 3 10 7.81 0.66 -3 3 10 8.40 0.63 -3 3 10 8.18 0.80 -3 3 10 7.82 0.62 -3 3 10 7.16 1.20 -2 -3 10 7.13 1.12 -2 -3 10 10.78 2.02 -2 -3 10 7.42 0.58 -2 -3 10 7.32 0.55 -2 -3 10 7.52 0.62 -2 -3 10 8.37 0.67 -2 -3 10 8.22 0.61 -2 -3 10 7.65 0.69 -2 -3 10 7.81 0.63 -2 -3 10 7.79 0.77 -2 -3 10 6.96 1.19 -2 3 10 7.67 0.59 -2 3 10 7.51 0.59 -2 3 10 7.56 0.60 -2 3 10 7.54 0.61 -2 3 10 7.38 0.63 -2 3 10 7.33 1.23 2 3 -10 7.39 0.91 2 3 -10 8.80 0.90 -2 3 10 7.42 0.77 -2 3 10 7.45 0.57 -2 3 10 7.73 0.62 -2 3 10 7.87 0.79 -2 3 10 7.47 0.66 -1 -3 10 1.95 0.40 -1 -3 10 1.95 0.41 -1 -3 10 1.79 0.27 -1 -3 10 1.46 0.74 -1 -3 10 2.09 0.27 -1 -3 10 3.06 1.23 -1 -3 10 1.84 0.25 -1 -3 10 1.70 0.24 -1 -3 10 1.71 0.33 -1 -3 10 1.99 0.30 -1 -3 10 1.97 0.26 -1 -3 10 2.46 0.80 -1 -3 10 1.87 0.24 -1 -3 10 1.97 0.31 -1 3 10 1.45 0.29 -1 3 10 1.58 0.41 -1 3 10 1.52 0.24 -1 3 10 1.63 0.25 -1 3 10 1.47 0.23 -1 3 10 1.43 0.23 -1 3 10 1.48 0.27 -1 3 10 1.48 0.58 -1 3 10 1.53 0.27 -1 3 10 1.74 0.30 -1 3 10 1.44 0.28 -1 3 10 1.31 0.26 -1 3 10 1.55 0.27 -1 3 10 1.52 0.25 -1 3 10 1.41 0.40 -1 3 10 1.40 0.30 -1 3 10 1.30 0.23 1 3 -10 1.82 0.67 -1 3 10 1.63 0.26 0 -3 10 20.79 1.32 0 -3 10 24.20 1.61 0 -3 10 20.00 1.45 0 -3 10 18.94 2.87 0 -3 10 21.79 1.40 0 -3 10 24.17 1.48 0 -3 10 21.37 1.33 0 -3 10 23.11 1.40 0 -3 10 22.28 1.33 0 -3 10 21.45 1.29 0 -3 10 20.77 1.47 0 -3 10 22.24 1.37 0 -3 10 21.26 1.31 0 -3 10 22.71 1.38 0 -3 10 23.65 2.12 0 -3 10 22.24 1.32 0 -3 10 23.75 1.55 0 -3 10 22.89 2.06 0 3 10 20.22 1.34 0 3 10 19.74 1.39 0 3 10 21.03 1.32 0 3 10 21.88 1.38 0 3 10 21.51 1.38 0 3 10 20.02 1.31 0 3 10 18.91 1.41 0 3 10 20.90 1.38 0 3 10 21.91 1.33 0 3 10 22.07 1.38 0 3 10 21.00 1.32 0 3 10 21.62 1.44 0 3 10 21.64 1.37 0 3 10 22.80 1.58 0 3 10 19.78 1.32 0 3 10 20.50 1.31 0 3 10 21.85 1.32 0 3 10 23.37 1.64 1 -3 10 24.58 1.36 1 -3 10 26.36 1.45 1 -3 10 24.96 1.39 1 -3 10 23.44 1.57 1 -3 10 23.33 1.38 1 -3 10 25.72 1.43 1 -3 10 27.21 2.43 1 -3 10 24.32 1.55 1 -3 10 18.12 3.14 1 -3 10 24.80 1.58 1 -3 10 26.68 2.14 1 -3 10 26.32 1.40 1 -3 10 24.78 1.38 1 -3 10 26.38 1.62 1 -3 10 25.70 1.46 1 -3 10 25.95 1.45 1 -3 10 25.42 1.48 1 3 10 21.56 1.59 1 3 10 21.82 1.68 1 3 10 21.15 1.38 1 3 10 20.57 1.40 1 3 10 20.12 1.36 1 3 10 19.75 1.36 1 3 10 20.77 1.43 1 3 10 19.25 1.38 1 3 10 21.45 1.37 1 3 10 19.75 1.44 1 3 10 20.98 1.42 1 3 10 20.38 1.49 1 3 10 19.72 1.37 1 3 10 20.23 1.35 1 3 10 20.56 1.41 1 3 10 19.72 1.41 1 3 10 20.39 1.44 2 -3 10 43.92 2.59 2 -3 10 41.37 2.45 2 -3 10 42.61 2.56 2 -3 10 43.69 2.48 2 -3 10 43.92 2.52 2 -3 10 44.67 2.55 2 -3 10 43.20 2.53 2 -3 10 41.12 2.66 2 -3 10 44.70 2.58 2 -3 10 43.40 2.66 2 -3 10 45.42 2.81 2 -3 10 41.78 2.55 2 -3 10 39.52 2.67 2 -3 10 41.83 2.58 2 -3 10 42.95 2.48 2 -3 10 40.71 2.64 2 -3 10 43.35 2.48 2 -3 10 43.48 2.66 2 -3 10 41.22 2.54 2 -3 10 39.22 3.25 2 -3 10 40.33 3.51 2 3 10 44.47 2.53 2 3 10 47.73 2.87 2 3 10 45.83 2.59 2 3 10 44.98 2.50 2 3 10 43.60 2.54 2 3 10 44.59 2.49 2 3 10 42.78 2.46 2 3 10 46.26 2.57 2 3 10 44.91 2.53 2 3 10 41.98 2.61 2 3 10 43.51 2.51 2 3 10 44.04 2.59 2 3 10 47.72 2.50 2 3 10 42.81 2.50 2 3 10 44.02 2.50 2 3 10 44.81 2.54 2 3 10 44.54 2.59 2 3 10 45.28 2.71 2 3 10 43.42 2.64 3 -3 10 8.64 0.65 3 -3 10 8.69 0.76 3 -3 10 9.48 0.75 3 -3 10 8.16 0.80 3 -3 10 8.67 0.69 3 -3 10 8.14 0.60 3 -3 10 8.49 0.69 3 -3 10 9.30 0.81 3 -3 10 8.49 0.73 3 -3 10 7.74 0.76 3 -3 10 8.05 0.68 3 -3 10 8.16 0.61 3 -3 10 7.97 0.76 3 -3 10 9.48 0.74 3 -3 10 8.86 0.63 3 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0.10 -1 -8 15 0.39 0.09 -1 -8 15 0.42 0.13 -1 -8 15 0.47 0.11 0 -8 15 0.38 0.07 0 -8 15 0.41 0.08 0 -8 15 0.43 0.07 0 -8 15 0.45 0.08 0 -8 15 0.42 0.07 0 8 15 0.57 0.08 0 8 15 0.56 0.08 -7 -9 15 6.69 0.44 7 -9 -15 6.61 0.47 7 9 -15 7.93 0.45 7 9 -15 7.92 0.52 -7 9 15 6.53 0.43 6 -9 -15 2.07 0.17 -6 -9 15 2.14 0.18 6 9 -15 1.76 0.15 -6 9 15 1.71 0.17 6 9 -15 1.82 0.19 -6 9 15 1.65 0.15 -6 9 15 1.85 0.16 6 9 -15 1.91 0.19 -5 -9 15 0.83 0.11 -5 -9 15 0.83 0.10 -5 -9 15 0.75 0.15 5 -9 -15 0.90 0.15 -5 -9 15 0.62 0.14 -5 -9 15 0.90 0.12 -5 9 15 0.78 0.12 -5 9 15 0.66 0.11 -5 9 15 0.88 0.11 -5 9 15 0.63 0.10 -5 9 15 0.59 0.13 -4 -9 15 3.38 0.23 -4 -9 15 2.89 0.30 -4 -9 15 3.32 0.24 -4 -9 15 3.27 0.24 -4 -9 15 3.27 0.24 -4 9 15 2.58 0.31 -4 9 15 2.81 0.25 -4 9 15 3.12 0.23 -4 9 15 2.97 0.24 -4 9 15 3.10 0.23 -3 -9 15 1.01 0.14 -3 -9 15 0.84 0.13 -3 -9 15 0.97 0.19 -3 -9 15 1.04 0.13 -3 -9 15 1.08 0.12 -3 -9 15 0.99 0.12 -3 9 15 1.29 0.13 -3 9 15 1.24 0.14 -3 9 15 1.13 0.21 -3 9 15 0.72 0.19 -3 9 15 1.34 0.13 -3 9 15 1.14 0.13 -2 -9 15 6.79 0.52 -2 -9 15 7.05 0.47 -2 -9 15 7.42 0.45 -2 -9 15 7.03 0.45 -2 -9 15 6.67 0.45 -2 9 15 8.29 0.46 -2 9 15 8.18 0.45 -2 9 15 8.15 0.48 -2 9 15 6.98 0.54 -1 -9 15 6.26 0.47 -1 -9 15 6.61 0.45 -1 -9 15 6.32 0.42 -1 -9 15 7.15 0.43 -1 -9 15 6.86 0.43 -1 9 15 7.81 0.43 -1 9 15 7.29 0.43 -1 9 15 6.96 0.49 -1 9 15 7.90 0.43 6 -10 -15 9.99 0.58 6 10 -15 9.16 0.64 -6 10 15 9.24 0.60 6 10 -15 10.05 0.58 6 10 -15 10.51 0.63 -5 -10 15 8.44 0.50 5 -10 -15 8.60 0.56 -5 -10 15 6.96 0.56 -5 -10 15 8.66 0.49 -5 -10 15 8.91 0.51 -5 10 15 8.50 0.49 -5 10 15 9.16 0.50 -5 10 15 7.21 0.61 -4 -10 15 15.74 0.92 -4 -10 15 15.54 0.92 -4 -10 15 14.39 0.97 -4 -10 15 16.36 0.92 -4 10 15 14.80 0.99 -4 10 15 17.38 0.92 -4 10 15 16.51 0.94 -4 10 15 17.92 0.96 -4 10 15 17.99 0.92 -3 -10 15 7.76 0.54 -3 -10 15 8.35 0.48 -3 -10 15 8.27 0.48 -3 10 15 8.16 0.48 -3 10 15 7.09 0.55 -3 10 15 7.78 0.47 -3 10 15 7.85 0.48 -2 -10 15 6.47 0.45 -2 -10 15 7.33 0.44 -2 -10 15 7.61 0.44 -2 -10 15 6.82 0.50 -2 10 15 8.03 0.46 -2 10 15 7.96 0.44 -2 10 15 7.29 0.52 -2 10 15 7.74 0.47 -4 -11 15 0.55 0.10 -4 -11 15 0.56 0.08 -4 11 15 0.55 0.09 -3 -11 15 0.22 0.08 -3 11 15 0.17 0.08 -3 11 15 0.20 0.05 -7 0 16 1.88 0.16 -7 0 16 1.69 0.18 -7 0 16 1.66 0.15 -6 0 16 1.52 0.19 -6 0 16 1.45 0.16 -6 0 16 1.27 0.16 -6 0 16 1.21 0.14 -6 0 16 1.32 0.13 -5 0 16 0.00 0.05 -5 0 16 0.06 0.06 -5 0 16 0.02 0.08 -5 0 16 0.00 0.06 -5 0 16 0.04 0.06 -5 0 16 -0.01 0.06 -4 0 16 0.11 0.06 -4 0 16 0.10 0.07 -4 0 16 0.12 0.08 -4 0 16 0.09 0.10 -4 0 16 0.13 0.07 -3 0 16 2.74 0.20 -3 0 16 2.28 0.28 -3 0 16 2.66 0.22 -3 0 16 2.50 0.22 -3 0 16 2.73 0.22 -3 0 16 2.84 0.23 -3 0 16 2.33 0.20 -2 0 16 5.53 0.37 -2 0 16 5.42 0.44 -2 0 16 5.18 0.35 -2 0 16 5.61 0.37 -2 0 16 5.75 0.38 -2 0 16 5.63 0.35 -2 0 16 5.60 0.35 -1 0 16 0.50 0.11 -1 0 16 0.34 0.14 -1 0 16 0.46 0.10 -1 0 16 0.48 0.12 -1 0 16 0.51 0.10 -7 -1 16 11.75 0.63 -7 -1 16 9.69 0.61 7 -1 -16 9.92 0.62 7 -1 -16 10.41 0.64 -7 1 16 10.22 0.67 -7 1 16 9.39 0.61 -6 -1 16 2.87 0.23 -6 -1 16 2.88 0.22 -6 -1 16 2.58 0.23 -6 -1 16 2.84 0.24 -6 -1 16 2.76 0.22 -6 1 16 2.45 0.21 -6 1 16 2.43 0.21 -6 1 16 2.58 0.23 -6 1 16 2.45 0.22 -6 1 16 2.56 0.20 -5 -1 16 1.41 0.16 -5 -1 16 1.35 0.16 -5 -1 16 1.30 0.20 -5 -1 16 1.47 0.15 -5 -1 16 1.52 0.17 -5 1 16 1.39 0.16 -5 1 16 1.36 0.13 -5 1 16 1.35 0.15 -5 1 16 1.43 0.17 -5 1 16 1.53 0.17 -5 1 16 1.15 0.19 -4 -1 16 1.78 0.18 -4 -1 16 1.99 0.20 -4 -1 16 1.54 0.23 -4 -1 16 1.59 0.18 -4 -1 16 1.69 0.17 -4 1 16 1.59 0.24 -4 1 16 1.96 0.18 -4 1 16 1.94 0.18 -4 1 16 1.71 0.19 -4 1 16 2.08 0.20 -4 1 16 2.01 0.19 -3 -1 16 0.26 0.11 -3 -1 16 0.27 0.08 -3 -1 16 0.26 0.07 -3 1 16 0.16 0.07 -3 1 16 0.11 0.10 -3 1 16 0.09 0.09 -3 1 16 0.15 0.06 -3 1 16 0.22 0.08 -3 1 16 0.15 0.07 -3 1 16 0.18 0.09 -2 -1 16 1.18 0.13 -2 -1 16 1.11 0.13 -2 -1 16 1.14 0.12 -2 -1 16 1.11 0.19 -2 -1 16 1.17 0.11 -2 -1 16 1.00 0.11 -2 -1 16 1.06 0.13 -2 1 16 0.85 0.13 -2 1 16 0.97 0.11 -2 1 16 0.80 0.13 -2 1 16 0.70 0.17 -2 1 16 0.83 0.12 -1 -1 16 6.58 0.44 -1 -1 16 6.36 0.39 -1 -1 16 6.13 0.48 -1 1 16 5.93 0.38 -1 1 16 6.54 0.41 -1 1 16 5.25 0.45 -7 -2 16 7.01 0.44 -7 2 16 6.98 0.44 -6 -2 16 16.27 0.96 -6 -2 16 16.31 0.94 -6 -2 16 15.64 0.95 -6 2 16 17.02 0.93 -6 2 16 16.70 0.94 -6 2 16 16.60 0.94 -6 2 16 16.57 0.94 -5 -2 16 17.13 1.00 -5 -2 16 14.99 1.01 -5 -2 16 15.71 0.95 -5 -2 16 16.23 0.97 -5 -2 16 16.61 0.97 -5 2 16 18.31 0.96 -5 2 16 16.84 0.97 -5 2 16 17.56 0.98 -5 2 16 17.04 0.94 -5 2 16 17.02 0.97 -5 2 16 15.75 1.02 -5 2 16 17.98 0.99 -4 -2 16 11.40 0.70 -4 -2 16 10.81 0.70 -4 -2 16 11.50 0.70 -4 -2 16 12.17 0.71 -4 -2 16 10.85 0.77 -4 -2 16 12.15 0.72 -4 -2 16 12.36 0.74 -4 2 16 12.00 0.71 -4 2 16 12.92 0.72 -4 2 16 12.13 0.68 -4 2 16 12.01 0.72 -4 2 16 11.27 0.78 -4 2 16 12.55 0.72 -4 2 16 12.06 0.72 -3 -2 16 4.52 0.39 -3 -2 16 4.49 0.30 -3 -2 16 4.65 0.32 -3 -2 16 4.51 0.31 -3 -2 16 4.60 0.34 -3 -2 16 4.51 0.32 -3 -2 16 4.56 0.30 -3 2 16 4.52 0.33 -3 2 16 4.70 0.33 -3 2 16 4.58 0.32 -3 2 16 4.76 0.32 -3 2 16 4.62 0.40 -3 2 16 4.20 0.31 -2 -2 16 7.84 0.57 -2 -2 16 8.51 0.53 -2 -2 16 8.90 0.52 -2 -2 16 8.14 0.51 -2 -2 16 8.07 0.50 -2 -2 16 8.73 0.50 -2 -2 16 7.89 0.51 -2 2 16 8.40 0.52 -2 2 16 8.49 0.51 -2 2 16 8.11 0.58 -2 2 16 8.98 0.51 -1 -2 16 2.76 0.23 -1 -2 16 2.49 0.20 -1 -2 16 2.17 0.21 -1 2 16 2.01 0.22 -1 2 16 2.37 0.20 -7 -3 16 12.57 0.83 -7 -3 16 13.47 0.80 -7 3 16 16.31 0.86 -6 -3 16 14.07 0.85 -6 -3 16 14.45 0.85 -6 -3 16 14.89 0.87 -6 3 16 15.32 0.87 -6 3 16 12.48 0.85 -6 3 16 16.48 0.92 -6 3 16 15.03 0.83 -6 3 16 15.04 0.85 -5 -3 16 7.36 0.48 -5 -3 16 7.28 0.46 -5 -3 16 6.55 0.49 -5 -3 16 7.53 0.46 -5 3 16 7.20 0.45 -5 3 16 7.15 0.45 -5 3 16 7.33 0.44 -5 3 16 7.12 0.45 -5 3 16 6.69 0.50 -5 3 16 7.42 0.45 -4 -3 16 1.26 0.14 -4 -3 16 1.33 0.20 -4 -3 16 1.58 0.15 -4 -3 16 1.50 0.16 -4 -3 16 1.51 0.17 -4 -3 16 1.33 0.15 -4 -3 16 1.59 0.15 -4 3 16 1.48 0.16 -4 3 16 1.44 0.14 -4 3 16 1.44 0.21 -4 3 16 1.52 0.16 -4 3 16 1.35 0.16 -4 3 16 1.45 0.16 -4 3 16 1.44 0.13 -3 -3 16 1.16 0.12 -3 -3 16 1.12 0.11 -3 -3 16 1.12 0.12 -3 -3 16 1.10 0.19 -3 -3 16 1.12 0.13 -3 -3 16 1.19 0.15 -3 3 16 1.13 0.14 -3 3 16 0.90 0.18 -3 3 16 0.87 0.12 -3 3 16 0.93 0.13 -3 3 16 0.89 0.13 -2 -3 16 1.06 0.13 -2 -3 16 1.09 0.11 -2 -3 16 1.14 0.12 -2 -3 16 1.07 0.12 -2 -3 16 1.16 0.14 -2 -3 16 1.22 0.18 -2 3 16 1.04 0.11 -2 3 16 0.97 0.12 -2 3 16 0.93 0.12 -2 3 16 0.94 0.18 -1 -3 16 3.82 0.24 -1 -3 16 3.82 0.25 -1 -3 16 3.43 0.24 -1 3 16 3.78 0.26 -7 -4 16 6.24 0.39 -7 4 16 5.96 0.37 -6 -4 16 10.37 0.70 -6 -4 16 11.12 0.66 -6 -4 16 11.42 0.66 -6 4 16 11.29 0.64 -6 4 16 11.89 0.65 -5 -4 16 18.50 1.12 -5 -4 16 18.33 1.20 -5 -4 16 19.01 1.14 -5 -4 16 18.87 1.12 -5 4 16 22.17 1.12 -5 4 16 20.00 1.12 -5 4 16 19.89 1.11 -5 4 16 23.46 1.32 -5 4 16 19.17 1.12 -4 -4 16 22.24 1.45 -4 -4 16 24.50 1.40 -4 -4 16 23.09 1.39 -4 -4 16 26.95 1.45 -4 -4 16 26.02 1.43 -4 -4 16 24.78 1.40 -4 4 16 25.29 1.40 -4 4 16 23.56 1.47 -4 4 16 27.86 1.39 -4 4 16 26.50 1.38 -4 4 16 26.20 1.41 -4 4 16 25.10 1.41 -3 -4 16 20.15 1.03 -3 -4 16 17.25 1.06 -3 -4 16 18.93 1.04 -3 -4 16 18.37 1.03 -3 -4 16 17.59 1.11 -3 4 16 18.67 1.04 -3 4 16 16.78 1.11 -3 4 16 18.62 1.05 -3 4 16 18.40 1.04 -3 4 16 19.35 1.05 -2 -4 16 15.73 0.99 -2 -4 16 17.39 0.94 -2 -4 16 18.74 0.94 -2 -4 16 16.43 0.93 -2 -4 16 14.41 0.94 -2 4 16 16.54 0.96 -2 4 16 16.81 0.95 -2 4 16 15.76 1.00 -6 -5 16 1.25 0.14 -6 -5 16 1.55 0.17 -6 5 16 1.30 0.13 -6 5 16 1.26 0.14 -5 -5 16 3.14 0.33 -5 -5 16 3.10 0.28 -5 -5 16 3.64 0.25 -5 -5 16 3.30 0.25 -5 5 16 3.80 0.24 -5 5 16 3.32 0.35 -5 5 16 3.62 0.25 -4 -5 16 2.48 0.19 -4 -5 16 2.38 0.24 -4 -5 16 2.44 0.19 -4 -5 16 2.61 0.18 -4 5 16 1.99 0.24 -4 5 16 2.16 0.19 -4 5 16 2.37 0.19 -4 5 16 2.40 0.18 -4 5 16 2.37 0.19 -3 -5 16 2.11 0.18 -3 -5 16 1.94 0.21 -3 5 16 1.73 0.21 -3 5 16 1.43 0.16 -3 5 16 1.70 0.16 -3 5 16 1.55 0.15 -3 5 16 1.81 0.16 -2 -5 16 2.38 0.26 -2 -5 16 2.57 0.18 -2 -5 16 2.62 0.24 -2 -5 16 2.40 0.18 -2 -5 16 2.70 0.21 -2 5 16 2.14 0.18 -2 5 16 2.03 0.26 -5 6 16 1.05 0.12 -5 6 16 1.05 0.12 -4 -6 16 4.79 0.36 -4 -6 16 4.96 0.34 -4 6 16 4.97 0.35 -4 6 16 5.44 0.33 -4 6 16 4.22 0.37 -4 6 16 4.98 0.32 -4 6 16 5.68 0.37 -3 -6 16 2.14 0.16 -3 -6 16 1.74 0.22 -3 -6 16 2.09 0.16 -3 6 16 1.70 0.23 -3 6 16 1.52 0.17 -3 6 16 1.66 0.15 -3 6 16 1.55 0.14 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 89473 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Y Y 0.44619(2) 0.44859(2) 0.48774(2) 0.01549(6) Uani 1 1 d . . . . . O1 O 0.52088(16) 0.52440(9) 0.40816(16) 0.0184(4) Uani 1 1 d . . . . . O2 O 0.30950(17) 0.46970(10) 0.32166(16) 0.0210(4) Uani 1 1 d . . . . . O3 O 0.32717(17) 0.52073(9) 0.53099(16) 0.0191(4) Uani 1 1 d . . . . . O4 O 0.55292(17) 0.49923(10) 0.64400(16) 0.0207(4) Uani 1 1 d . . . . . N1 N 0.4709(2) 0.57346(11) 0.33917(18) 0.0172(4) Uani 1 1 d . . . . . N2 N 0.2180(2) 0.49771(12) 0.1512(2) 0.0207(5) Uani 1 1 d D . . . . H2N H 0.209(4) 0.5222(18) 0.095(3) 0.028(10) Uiso 1 1 d D . . . . N3 N 0.32879(19) 0.56983(11) 0.60376(18) 0.0174(4) Uani 1 1 d . . . . . N4 N 0.6160(2) 0.55995(12) 0.79304(19) 0.0218(5) Uani 1 1 d D . . . . H4N H 0.598(3) 0.5867(16) 0.838(3) 0.023(9) Uiso 1 1 d D . . . . C1 C 0.3924(2) 0.61509(14) 0.3839(2) 0.0209(5) Uani 1 1 d . . . . . H1A H 0.318749 0.591761 0.377676 0.025 Uiso 1 1 calc R U . . . H1B H 0.373410 0.654592 0.339869 0.025 Uiso 1 1 calc R U . . . C2 C 0.4457(2) 0.63398(14) 0.5012(2) 0.0215(5) Uani 1 1 d . . . . . H2A H 0.507348 0.602897 0.535936 0.026 Uiso 1 1 calc R U . . . H2B H 0.481700 0.677025 0.504687 0.026 Uiso 1 1 calc R U . . . C3 C 0.3533(3) 0.63500(14) 0.5614(2) 0.0219(6) Uani 1 1 d . . . . . H3A H 0.280142 0.651860 0.512581 0.026 Uiso 1 1 calc R U . . . H3B H 0.378286 0.665078 0.622824 0.026 Uiso 1 1 calc R U . . . C11 C 0.5674(2) 0.61057(14) 0.3077(2) 0.0212(5) Uani 1 1 d . . . . . H11 H 0.537525 0.653107 0.275676 0.025 Uiso 1 1 calc R U . . . C12 C 0.6789(2) 0.61948(14) 0.3994(3) 0.0243(6) Uani 1 1 d . . . . . H12A H 0.676510 0.593633 0.463034 0.029 Uiso 1 1 calc R U . . . H12B H 0.690465 0.665204 0.420810 0.029 Uiso 1 1 calc R U . . . C13 C 0.7758(3) 0.5958(2) 0.3521(4) 0.0412(8) Uani 1 1 d . . . . . H13A H 0.801104 0.630348 0.311037 0.049 Uiso 1 1 calc R U . . . H13B H 0.843910 0.580514 0.409626 0.049 Uiso 1 1 calc R U . . . C14 C 0.7189(3) 0.5407(2) 0.2780(4) 0.0428(9) Uani 1 1 d . . . . . H14A H 0.714289 0.501406 0.319845 0.051 Uiso 1 1 calc R U . . . H14B H 0.762254 0.530823 0.225040 0.051 Uiso 1 1 calc R U . . . C15 C 0.5964(3) 0.56718(17) 0.2219(3) 0.0283(7) Uani 1 1 d . . . . . H15 H 0.599516 0.593721 0.158267 0.034 Uiso 1 1 calc R U . . . C16 C 0.4979(3) 0.51789(16) 0.1877(2) 0.0256(6) Uani 1 1 d . . . . . H16A H 0.471201 0.513390 0.108374 0.031 Uiso 1 1 calc R U . . . H16B H 0.522636 0.475336 0.220286 0.031 Uiso 1 1 calc R U . . . C17 C 0.4031(2) 0.54699(13) 0.2314(2) 0.0186(5) Uani 1 1 d . . . . . H17 H 0.366938 0.583739 0.183963 0.022 Uiso 1 1 calc R U . . . C18 C 0.3067(2) 0.50121(13) 0.2400(2) 0.0181(5) Uani 1 1 d . . . . . C21 C 0.1239(2) 0.45315(17) 0.1456(2) 0.0213(5) Uani 1 1 d . . . . . C22 C 0.1336(3) 0.39053(15) 0.1107(2) 0.0265(6) Uani 1 1 d . . . . . C23 C 0.0441(3) 0.34783(17) 0.1084(3) 0.0351(7) Uani 1 1 d . . . . . H23 H 0.047830 0.305316 0.082801 0.042 Uiso 1 1 calc R U . . . C24 C -0.0508(3) 0.36629(19) 0.1427(3) 0.0376(8) Uani 1 1 d . . . . . H24 H -0.111023 0.336359 0.141651 0.045 Uiso 1 1 calc R U . . . C25 C -0.0578(3) 0.42845(18) 0.1787(3) 0.0324(7) Uani 1 1 d . . . . . H25 H -0.122679 0.440684 0.203025 0.039 Uiso 1 1 calc R U . . . C26 C 0.0290(3) 0.47334(16) 0.1798(2) 0.0262(6) Uani 1 1 d . . . . . C27 C 0.2400(3) 0.36910(18) 0.0788(3) 0.0359(7) Uani 1 1 d . . . . . H27A H 0.243944 0.321600 0.081432 0.043 Uiso 1 1 calc R U . . . H27B H 0.310156 0.385800 0.132232 0.043 Uiso 1 1 calc R U . . . C28 C 0.2416(4) 0.3912(3) -0.0328(4) 0.0565(12) Uani 1 1 d . . . . . H28A H 0.313075 0.376117 -0.047700 0.085 Uiso 1 1 calc R U . . . H28B H 0.238928 0.438278 -0.035944 0.085 Uiso 1 1 calc R U . . . H28C H 0.174002 0.373611 -0.086635 0.085 Uiso 1 1 calc R U . . . C29 C 0.0184(3) 0.54139(18) 0.2163(3) 0.0326(7) Uani 1 1 d . . . . . H29A H 0.097058 0.558540 0.251137 0.039 Uiso 1 1 calc R U . . . H29B H -0.025756 0.541292 0.270578 0.039 Uiso 1 1 calc R U . . . C30 C -0.0428(4) 0.5854(2) 0.1228(4) 0.0496(10) Uani 1 1 d . . . . . H30A H -0.051779 0.628341 0.150679 0.074 Uiso 1 1 calc R U . . . H30B H -0.119612 0.567802 0.086411 0.074 Uiso 1 1 calc R U . . . H30C H 0.003782 0.588354 0.071618 0.074 Uiso 1 1 calc R U . . . C31 C 0.2115(2) 0.57285(14) 0.6306(2) 0.0213(5) Uani 1 1 d . . . . . H31 H 0.203282 0.614852 0.665303 0.026 Uiso 1 1 calc R U . . . C32 C 0.1069(3) 0.56135(17) 0.5328(3) 0.0293(6) Uani 1 1 d . . . . . H32A H 0.132552 0.548513 0.469276 0.035 Uiso 1 1 calc R U . . . H32B H 0.058460 0.600510 0.514731 0.035 Uiso 1 1 calc R U . . . C33 C 0.0392(3) 0.50660(19) 0.5680(3) 0.0338(7) Uani 1 1 d . . . . . H33A H -0.016950 0.523816 0.604413 0.041 Uiso 1 1 calc R U . . . H33B H -0.003406 0.480546 0.505302 0.041 Uiso 1 1 calc R U . . . C34 C 0.1336(3) 0.46649(16) 0.6461(3) 0.0313(7) Uani 1 1 d . . . . . H34A H 0.100230 0.440178 0.693880 0.038 Uiso 1 1 calc R U . . . H34B H 0.173454 0.437868 0.606544 0.038 Uiso 1 1 calc R U . . . C35 C 0.2172(2) 0.51737(15) 0.7103(2) 0.0240(6) Uani 1 1 d . . . . . H35 H 0.188393 0.532649 0.771589 0.029 Uiso 1 1 calc R U . . . C36 C 0.3466(3) 0.49940(15) 0.7526(2) 0.0245(6) Uani 1 1 d . . . . . H36A H 0.370917 0.496719 0.832158 0.029 Uiso 1 1 calc R U . . . H36B H 0.362310 0.457689 0.722596 0.029 Uiso 1 1 calc R U . . . C37 C 0.4098(2) 0.55399(13) 0.7135(2) 0.0188(5) Uani 1 1 d . . . . . H37 H 0.413884 0.591892 0.761920 0.023 Uiso 1 1 calc R U . . . C38 C 0.5325(2) 0.53632(13) 0.7119(2) 0.0186(5) Uani 1 1 d . . . . . C41 C 0.7364(2) 0.54087(15) 0.8141(2) 0.0233(6) Uani 1 1 d . . . . . C42 C 0.7702(3) 0.48103(16) 0.8627(2) 0.0263(6) Uani 1 1 d . . . . . C43 C 0.8876(3) 0.46516(18) 0.8842(3) 0.0334(8) Uani 1 1 d . . . . . H43 H 0.914138 0.424944 0.916574 0.040 Uiso 1 1 calc R U . . . C44 C 0.9661(3) 0.5068(2) 0.8593(3) 0.0365(8) Uani 1 1 d . . . . . H44 H 1.045975 0.495326 0.876230 0.044 Uiso 1 1 calc R U . . . C45 C 0.9299(3) 0.56486(19) 0.8103(3) 0.0338(7) Uani 1 1 d . . . . . H45 H 0.984941 0.592818 0.793232 0.041 Uiso 1 1 calc R U . . . C46 C 0.8130(3) 0.58308(16) 0.7854(3) 0.0281(6) Uani 1 1 d . . . . . C47 C 0.6847(3) 0.43557(16) 0.8895(3) 0.0323(7) Uani 1 1 d . . . . . H47A H 0.721330 0.392663 0.904577 0.039 Uiso 1 1 calc R U . . . H47B H 0.616342 0.431416 0.825734 0.039 Uiso 1 1 calc R U . . . C48 C 0.6430(3) 0.4564(2) 0.9862(3) 0.0417(9) Uani 1 1 d . . . . . H48A H 0.586530 0.425188 0.997807 0.063 Uiso 1 1 calc R U . . . H48B H 0.606307 0.498823 0.971977 0.063 Uiso 1 1 calc R U . . . H48C H 0.709626 0.458634 1.050597 0.063 Uiso 1 1 calc R U . . . C49 C 0.7693(3) 0.64544(19) 0.7282(3) 0.0421(8) Uani 1 1 d . . . . . H49A H 0.702649 0.635169 0.665380 0.050 Uiso 1 1 calc R U . . . H49B H 0.739014 0.672169 0.777663 0.050 Uiso 1 1 calc R U . . . C50 C 0.8507(6) 0.6845(4) 0.6901(7) 0.095(3) Uani 1 1 d . . . . . H50A H 0.807898 0.717778 0.641344 0.143 Uiso 1 1 calc R U . . . H50B H 0.892564 0.657177 0.651721 0.143 Uiso 1 1 calc R U . . . H50C H 0.906385 0.704754 0.751730 0.143 Uiso 1 1 calc R U . . . S1S S 0.47428(8) 0.30149(4) 0.65209(7) 0.03224(17) Uani 1 1 d . . . . . S2S S 0.52132(7) 0.30595(3) 0.34941(6) 0.02658(15) Uani 1 1 d . . . . . S3S S 0.71872(8) 0.13679(4) 1.04076(6) 0.03202(17) Uani 1 1 d . . . . . F1S F 0.4658(3) 0.33447(14) 0.8457(2) 0.0565(7) Uani 1 1 d . . . . . F2S F 0.3796(3) 0.24531(11) 0.7873(2) 0.0619(8) Uani 1 1 d . . . . . F3S F 0.3002(2) 0.33522(13) 0.7270(2) 0.0546(6) Uani 1 1 d . . . . . F4S F 0.6498(3) 0.27409(13) 0.2256(2) 0.0579(7) Uani 1 1 d . . . . . F5S F 0.6723(2) 0.37202(13) 0.2802(2) 0.0514(6) Uani 1 1 d . . . . . F6S F 0.5200(2) 0.34465(13) 0.15578(19) 0.0495(6) Uani 1 1 d . . . . . F7S F 0.7825(3) 0.18644(19) 0.8824(2) 0.0755(9) Uani 1 1 d . . . . . F8S F 0.9023(3) 0.20287(19) 1.0379(4) 0.0907(13) Uani 1 1 d . . . . . F9S F 0.7404(4) 0.25649(13) 0.9913(3) 0.0888(13) Uani 1 1 d . . . . . O1S O 0.4889(2) 0.36951(11) 0.63117(18) 0.0290(5) Uani 1 1 d . . . . . O2S O 0.3901(3) 0.27026(12) 0.5652(2) 0.0432(7) Uani 1 1 d . . . . . O3S O 0.5782(3) 0.26672(14) 0.6977(2) 0.0485(7) Uani 1 1 d . . . . . O4S O 0.4621(2) 0.36541(11) 0.36075(19) 0.0288(5) Uani 1 1 d . . . . . O5S O 0.6165(2) 0.29154(11) 0.4428(2) 0.0362(5) Uani 1 1 d . . . . . O6S O 0.4466(3) 0.25366(12) 0.3039(2) 0.0406(6) Uani 1 1 d . . . . . O7S O 0.6004(2) 0.14082(16) 0.9720(2) 0.0474(7) Uani 1 1 d . . . . . O8S O 0.7780(3) 0.07982(13) 1.0234(2) 0.0411(6) Uani 1 1 d . . . . . O9S O 0.7344(4) 0.15395(15) 1.1504(2) 0.0569(9) Uani 1 1 d . . . . . C1S C 0.4010(4) 0.30408(17) 0.7589(3) 0.0410(9) Uani 1 1 d . . . . . C2S C 0.5951(4) 0.32531(19) 0.2468(3) 0.0363(8) Uani 1 1 d . . . . . C3S C 0.7888(5) 0.1998(2) 0.9847(4) 0.0537(11) Uani 1 1 d . . . . . C4S C 0.0757(8) 0.7561(5) 0.5875(6) 0.106(3) Uani 1 1 d D . . . . H4SA H 0.072962 0.794286 0.631091 0.160 Uiso 1 1 calc R U . . . H4SB H 0.006195 0.729920 0.581301 0.160 Uiso 1 1 calc R U . . . H4SC H 0.145271 0.730910 0.621965 0.160 Uiso 1 1 calc R U . . . C5S C 0.0800(8) 0.7765(4) 0.4771(6) 0.105(3) Uani 1 1 d D . . . . H5SA H 0.010260 0.802320 0.441954 0.126 Uiso 1 1 calc R U . . . H5SB H 0.149751 0.803313 0.482740 0.126 Uiso 1 1 calc R U . . . C6S C 0.1213(11) 0.7403(6) 0.3212(8) 0.137(4) Uani 1 1 d . . . . . H6SA H 0.138350 0.700654 0.286289 0.164 Uiso 1 1 calc R U . . . H6SB H 0.194385 0.765248 0.345221 0.164 Uiso 1 1 calc R U . . . C7S C 0.0341(13) 0.7791(6) 0.2396(8) 0.175(7) Uani 1 1 d . . . . . H7SA H 0.065213 0.789105 0.178911 0.263 Uiso 1 1 calc R U . . . H7SB H -0.038040 0.754443 0.213618 0.263 Uiso 1 1 calc R U . . . H7SC H 0.018085 0.819140 0.272644 0.263 Uiso 1 1 calc R U . . . O10S O 0.2806(2) 0.38125(11) 0.4755(2) 0.0294(5) Uani 1 1 d D . . . . H10O H 0.306(4) 0.3445(15) 0.497(4) 0.041(12) Uiso 1 1 d D . . . . O11S O 0.64618(18) 0.41729(11) 0.51745(18) 0.0258(4) Uani 1 1 d D . . . . H11O H 0.659(4) 0.3789(13) 0.512(4) 0.037(11) Uiso 1 1 d D . . . . O12S O 0.5893(3) 0.64203(16) 0.9511(3) 0.0513(7) Uani 1 1 d D . . . . H12O H 0.517(3) 0.644(5) 0.949(6) 0.12(3) Uiso 1 1 d D . . . . O13S O 0.0839(5) 0.7223(2) 0.4166(5) 0.0936(15) Uani 1 1 d . . . . . C10S C 0.1646(3) 0.3818(2) 0.4079(3) 0.0450(9) Uani 1 1 d . . . . . H10A H 0.115031 0.356386 0.441310 0.067 Uiso 1 1 calc R U . . . H10B H 0.162580 0.363131 0.337820 0.067 Uiso 1 1 calc R U . . . H10C H 0.136020 0.426084 0.397948 0.067 Uiso 1 1 calc R U . . . C11S C 0.7533(3) 0.4440(3) 0.5743(4) 0.0589(13) Uani 1 1 d . . . . . H11B H 0.811859 0.434014 0.536755 0.088 Uiso 1 1 calc R U . . . H11C H 0.777552 0.425853 0.647087 0.088 Uiso 1 1 calc R U . . . H11D H 0.745298 0.490666 0.578664 0.088 Uiso 1 1 calc R U . . . C12S C 0.6508(7) 0.6990(3) 0.9717(5) 0.0771(19) Uani 1 1 d . . . . . H12C H 0.611321 0.728774 1.008566 0.116 Uiso 1 1 calc R U . . . H12D H 0.655047 0.718059 0.903671 0.116 Uiso 1 1 calc R U . . . H12E H 0.729562 0.690492 1.017594 0.116 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Y 0.01771(9) 0.01214(9) 0.01703(9) 0.00014(9) 0.00550(7) -0.00051(9) O1 0.0182(8) 0.0148(9) 0.0221(9) 0.0070(7) 0.0054(7) 0.0015(7) O2 0.0210(9) 0.0223(9) 0.0181(9) 0.0026(7) 0.0032(7) -0.0029(7) O3 0.0196(9) 0.0176(9) 0.0204(9) -0.0047(7) 0.0062(7) 0.0007(7) O4 0.0195(9) 0.0218(9) 0.0192(9) -0.0045(7) 0.0030(7) 0.0021(7) N1 0.0167(10) 0.0158(10) 0.0205(11) 0.0043(8) 0.0077(9) 0.0011(8) N2 0.0176(11) 0.0253(12) 0.0183(11) 0.0025(9) 0.0034(9) -0.0001(9) N3 0.0151(10) 0.0182(10) 0.0190(10) -0.0013(8) 0.0050(8) -0.0007(8) N4 0.0160(10) 0.0264(12) 0.0216(11) -0.0081(9) 0.0027(8) 0.0016(9) C1 0.0184(12) 0.0205(12) 0.0249(13) 0.0005(10) 0.0081(10) 0.0036(10) C2 0.0228(13) 0.0151(12) 0.0276(14) -0.0011(10) 0.0088(11) -0.0019(10) C3 0.0247(13) 0.0183(13) 0.0243(13) 0.0007(11) 0.0093(11) 0.0007(10) C11 0.0203(12) 0.0185(12) 0.0274(14) 0.0042(10) 0.0106(11) -0.0003(10) C12 0.0191(12) 0.0219(13) 0.0321(15) -0.0017(11) 0.0072(11) -0.0031(10) C13 0.0222(15) 0.047(2) 0.054(2) -0.0084(17) 0.0115(15) 0.0003(14) C14 0.0209(15) 0.051(2) 0.057(2) -0.0209(19) 0.0119(15) 0.0040(15) C15 0.0251(15) 0.0344(17) 0.0293(16) -0.0019(13) 0.0144(12) -0.0036(13) C16 0.0230(13) 0.0306(15) 0.0268(14) -0.0052(12) 0.0129(11) -0.0011(11) C17 0.0196(12) 0.0198(12) 0.0178(11) 0.0026(10) 0.0074(10) -0.0001(10) C18 0.0169(11) 0.0183(12) 0.0204(12) -0.0015(10) 0.0072(10) 0.0010(9) C21 0.0181(10) 0.0259(13) 0.0182(10) 0.0015(12) 0.0021(8) -0.0025(12) C22 0.0257(14) 0.0280(15) 0.0239(14) -0.0004(11) 0.0040(11) 0.0009(11) C23 0.0363(17) 0.0287(16) 0.0353(17) -0.0042(13) 0.0017(14) -0.0054(13) C24 0.0299(16) 0.0407(19) 0.0393(18) 0.0032(15) 0.0046(14) -0.0133(14) C25 0.0195(13) 0.0468(19) 0.0310(15) -0.0008(13) 0.0072(11) -0.0037(12) C26 0.0188(13) 0.0343(15) 0.0236(14) -0.0012(11) 0.0026(11) 0.0010(11) C27 0.0342(17) 0.0299(16) 0.0447(19) -0.0071(14) 0.0127(15) 0.0053(13) C28 0.054(2) 0.073(3) 0.049(2) -0.009(2) 0.025(2) 0.015(2) C29 0.0238(13) 0.0403(18) 0.0348(16) -0.0097(14) 0.0098(12) 0.0017(13) C30 0.060(3) 0.038(2) 0.050(2) -0.0007(17) 0.014(2) 0.0131(18) C31 0.0164(11) 0.0260(14) 0.0233(13) -0.0015(10) 0.0086(10) 0.0015(10) C32 0.0194(13) 0.0399(17) 0.0273(14) -0.0002(13) 0.0043(11) 0.0024(12) C33 0.0195(13) 0.047(2) 0.0347(17) -0.0051(14) 0.0076(12) -0.0066(13) C34 0.0275(14) 0.0326(17) 0.0357(16) -0.0022(12) 0.0120(12) -0.0104(11) C35 0.0204(13) 0.0292(14) 0.0247(13) -0.0001(11) 0.0101(11) -0.0023(11) C36 0.0234(13) 0.0270(14) 0.0238(14) 0.0055(11) 0.0080(11) -0.0004(11) C37 0.0187(12) 0.0216(13) 0.0162(11) -0.0015(10) 0.0050(9) -0.0001(10) C38 0.0193(11) 0.0174(12) 0.0189(12) 0.0007(10) 0.0052(10) 0.0002(9) C41 0.0171(12) 0.0322(15) 0.0199(12) -0.0057(11) 0.0040(10) 0.0021(11) C42 0.0233(14) 0.0335(16) 0.0210(13) -0.0022(12) 0.0042(11) 0.0016(12) C43 0.0256(14) 0.047(2) 0.0256(14) 0.0024(12) 0.0037(11) 0.0110(12) C44 0.0192(13) 0.058(2) 0.0308(16) -0.0023(15) 0.0040(12) 0.0057(14) C45 0.0207(14) 0.049(2) 0.0323(16) -0.0044(14) 0.0083(12) -0.0044(13) C46 0.0220(13) 0.0353(16) 0.0267(14) -0.0061(12) 0.0065(11) -0.0018(12) C47 0.0299(14) 0.036(2) 0.0302(15) 0.0063(12) 0.0074(12) 0.0006(12) C48 0.0333(15) 0.063(3) 0.0303(15) 0.0068(18) 0.0117(12) -0.0016(18) C49 0.0378(18) 0.0368(19) 0.050(2) 0.0045(16) 0.0097(16) -0.0003(15) C50 0.063(3) 0.078(4) 0.136(7) 0.046(4) 0.013(4) -0.020(3) S1S 0.0546(5) 0.0172(3) 0.0323(4) 0.0055(3) 0.0245(4) 0.0053(3) S2S 0.0337(4) 0.0180(3) 0.0290(4) -0.0038(3) 0.0103(3) 0.0014(3) S3S 0.0476(4) 0.0249(4) 0.0255(3) -0.0014(3) 0.0135(3) 0.0021(3) F1S 0.0838(19) 0.0565(15) 0.0383(12) -0.0074(11) 0.0319(13) -0.0052(14) F2S 0.117(2) 0.0255(10) 0.0684(16) 0.0090(11) 0.0677(18) 0.0024(12) F3S 0.0619(15) 0.0445(13) 0.0708(17) 0.0057(12) 0.0409(14) 0.0059(12) F4S 0.0715(17) 0.0487(14) 0.0666(17) -0.0034(12) 0.0409(14) 0.0247(13) F5S 0.0457(13) 0.0466(13) 0.0703(17) 0.0025(12) 0.0299(12) -0.0064(11) F6S 0.0566(14) 0.0596(15) 0.0370(12) 0.0111(11) 0.0208(11) 0.0131(12) F7S 0.091(2) 0.093(2) 0.0455(15) 0.0158(15) 0.0248(15) -0.0294(19) F8S 0.0640(19) 0.092(3) 0.100(3) -0.001(2) -0.0047(19) -0.0442(19) F9S 0.133(3) 0.0293(13) 0.082(2) 0.0129(14) -0.007(2) -0.0123(17) O1S 0.0412(12) 0.0198(10) 0.0276(11) 0.0067(8) 0.0119(9) -0.0001(9) O2S 0.071(2) 0.0219(12) 0.0423(15) -0.0026(10) 0.0249(14) -0.0081(12) O3S 0.071(2) 0.0356(14) 0.0484(16) 0.0158(12) 0.0323(15) 0.0235(13) O4S 0.0316(11) 0.0262(11) 0.0289(11) -0.0077(9) 0.0087(9) 0.0032(9) O5S 0.0448(13) 0.0239(11) 0.0357(12) -0.0015(9) 0.0044(11) 0.0063(10) O6S 0.0520(15) 0.0288(12) 0.0407(14) -0.0089(10) 0.0126(12) -0.0092(11) O7S 0.0387(14) 0.0577(18) 0.0487(15) -0.0090(14) 0.0168(12) 0.0008(13) O8S 0.0562(16) 0.0347(13) 0.0307(12) -0.0076(10) 0.0092(11) 0.0092(11) O9S 0.107(3) 0.0388(15) 0.0250(12) -0.0011(11) 0.0184(15) 0.0192(16) C1S 0.071(3) 0.0214(15) 0.0415(19) 0.0018(14) 0.0339(19) 0.0017(16) C2S 0.0380(19) 0.0330(18) 0.0409(19) -0.0001(15) 0.0163(16) 0.0091(15) C3S 0.065(3) 0.044(2) 0.047(2) 0.0044(17) 0.006(2) -0.020(2) C4S 0.102(6) 0.112(6) 0.106(6) -0.002(5) 0.030(5) 0.045(5) C5S 0.110(6) 0.091(5) 0.111(6) -0.013(5) 0.027(5) 0.040(5) C6S 0.177(11) 0.152(9) 0.092(6) 0.018(6) 0.053(7) 0.071(8) C7S 0.275(17) 0.143(9) 0.084(6) -0.007(6) 0.010(8) 0.129(11) O10S 0.0303(11) 0.0238(11) 0.0347(12) -0.0005(9) 0.0102(9) -0.0098(9) O11S 0.0227(10) 0.0193(10) 0.0339(11) -0.0037(9) 0.0052(8) 0.0019(8) O12S 0.0573(18) 0.0484(17) 0.0596(18) -0.0235(14) 0.0350(15) -0.0134(14) O13S 0.111(4) 0.068(3) 0.106(4) 0.002(3) 0.038(3) 0.019(3) C10S 0.0373(19) 0.060(3) 0.0359(18) 0.0013(17) 0.0067(15) -0.0205(18) C11S 0.0217(14) 0.060(3) 0.091(3) -0.047(3) 0.0092(17) -0.0032(19) C12S 0.120(5) 0.063(3) 0.065(3) -0.029(3) 0.053(4) -0.045(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Y Y -0.2670 2.0244 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Y O3 90.36(7) . . ? O1 Y O4 83.39(7) . . ? O3 Y O4 73.31(7) . . ? O1 Y O2 73.11(7) . . ? O3 Y O2 76.95(7) . . ? O4 Y O2 141.68(7) . . ? O1 Y O10S 145.44(8) . . ? O3 Y O10S 80.59(8) . . ? O4 Y O10S 124.55(8) . . ? O2 Y O10S 72.36(8) . . ? O1 Y O11S 75.70(7) . . ? O3 Y O11S 144.45(7) . . ? O4 Y O11S 72.70(7) . . ? O2 Y O11S 127.19(7) . . ? O10S Y O11S 128.32(8) . . ? O1 Y O1S 144.71(8) . . ? O3 Y O1S 106.03(8) . . ? O4 Y O1S 72.25(8) . . ? O2 Y O1S 140.37(8) . . ? O10S Y O1S 69.34(8) . . ? O11S Y O1S 72.93(8) . . ? O1 Y O4S 94.34(8) . . ? O3 Y O4S 145.06(8) . . ? O4 Y O4S 141.62(7) . . ? O2 Y O4S 71.44(8) . . ? O10S Y O4S 76.04(8) . . ? O11S Y O4S 69.66(8) . . ? O1S Y O4S 89.64(8) . . ? N1 O1 Y 132.32(15) . . ? C18 O2 Y 136.56(18) . . ? N3 O3 Y 140.60(15) . . ? C38 O4 Y 136.70(18) . . ? O1 N1 C17 110.6(2) . . ? O1 N1 C1 112.4(2) . . ? C17 N1 C1 109.4(2) . . ? O1 N1 C11 108.79(19) . . ? C17 N1 C11 100.9(2) . . ? C1 N1 C11 114.1(2) . . ? C18 N2 C21 120.1(2) . . ? O3 N3 C37 111.1(2) . . ? O3 N3 C3 112.3(2) . . ? C37 N3 C3 113.2(2) . . ? O3 N3 C31 110.05(19) . . ? C37 N3 C31 100.58(19) . . ? C3 N3 C31 109.0(2) . . ? C38 N4 C41 122.6(2) . . ? N1 C1 C2 113.4(2) . . ? C3 C2 C1 110.5(2) . . ? C2 C3 N3 114.4(2) . . ? C12 C11 N1 114.4(2) . . ? C12 C11 C15 107.8(2) . . ? N1 C11 C15 103.5(2) . . ? C11 C12 C13 104.2(3) . . ? C14 C13 C12 103.6(3) . . ? C13 C14 C15 103.0(3) . . ? C16 C15 C11 106.8(2) . . ? C16 C15 C14 116.7(3) . . ? C11 C15 C14 104.2(3) . . ? C17 C16 C15 102.7(2) . . ? N1 C17 C18 112.6(2) . . ? N1 C17 C16 102.9(2) . . ? C18 C17 C16 115.8(2) . . ? O2 C18 N2 122.2(2) . . ? O2 C18 C17 123.7(2) . . ? N2 C18 C17 114.1(2) . . ? C26 C21 C22 122.3(3) . . ? C26 C21 N2 118.9(3) . . ? C22 C21 N2 118.7(2) . . ? C23 C22 C21 118.1(3) . . ? C23 C22 C27 120.7(3) . . ? C21 C22 C27 121.2(3) . . ? C24 C23 C22 120.9(3) . . ? C23 C24 C25 120.0(3) . . ? C24 C25 C26 120.9(3) . . ? C21 C26 C25 117.8(3) . . ? C21 C26 C29 122.0(3) . . ? C25 C26 C29 120.2(3) . . ? C22 C27 C28 113.9(3) . . ? C26 C29 C30 112.3(3) . . ? C32 C31 C35 108.0(2) . . ? C32 C31 N3 113.2(2) . . ? C35 C31 N3 104.4(2) . . ? C31 C32 C33 104.4(3) . . ? C34 C33 C32 104.2(2) . . ? C35 C34 C33 103.3(3) . . ? C34 C35 C31 104.8(2) . . ? C34 C35 C36 117.7(3) . . ? C31 C35 C36 105.8(2) . . ? C37 C36 C35 104.2(2) . . ? N3 C37 C38 114.1(2) . . ? N3 C37 C36 103.0(2) . . ? C38 C37 C36 113.2(2) . . ? O4 C38 N4 122.4(2) . . ? O4 C38 C37 122.7(2) . . ? N4 C38 C37 114.7(2) . . ? C46 C41 C42 123.4(3) . . ? C46 C41 N4 118.2(3) . . ? C42 C41 N4 118.4(3) . . ? C43 C42 C41 116.6(3) . . ? C43 C42 C47 121.2(3) . . ? C41 C42 C47 122.2(3) . . ? C44 C43 C42 121.2(3) . . ? C45 C44 C43 120.7(3) . . ? C44 C45 C46 120.7(3) . . ? C41 C46 C45 117.3(3) . . ? C41 C46 C49 120.5(3) . . ? C45 C46 C49 122.2(3) . . ? C42 C47 C48 114.0(3) . . ? C50 C49 C46 118.1(4) . . ? O3S S1S O2S 115.86(19) . . ? O3S S1S O1S 115.79(18) . . ? O2S S1S O1S 112.79(15) . . ? O3S S1S C1S 104.56(18) . . ? O2S S1S C1S 102.91(19) . . ? O1S S1S C1S 102.62(15) . . ? O6S S2S O5S 116.41(16) . . ? O6S S2S O4S 115.07(16) . . ? O5S S2S O4S 112.73(14) . . ? O6S S2S C2S 104.01(18) . . ? O5S S2S C2S 102.95(18) . . ? O4S S2S C2S 103.48(16) . . ? O9S S3S O8S 115.56(17) . . ? O9S S3S O7S 115.5(2) . . ? O8S S3S O7S 113.21(18) . . ? O9S S3S C3S 105.7(2) . . ? O8S S3S C3S 103.4(2) . . ? O7S S3S C3S 101.3(2) . . ? S1S O1S Y 142.07(15) . . ? S2S O4S Y 143.82(14) . . ? F2S C1S F3S 107.9(4) . . ? F2S C1S F1S 108.5(3) . . ? F3S C1S F1S 107.1(3) . . ? F2S C1S S1S 110.7(2) . . ? F3S C1S S1S 111.4(3) . . ? F1S C1S S1S 111.1(3) . . ? F4S C2S F5S 108.6(3) . . ? F4S C2S F6S 108.3(3) . . ? F5S C2S F6S 107.7(3) . . ? F4S C2S S2S 109.9(3) . . ? F5S C2S S2S 110.9(3) . . ? F6S C2S S2S 111.4(3) . . ? F9S C3S F7S 110.1(4) . . ? F9S C3S F8S 108.8(4) . . ? F7S C3S F8S 106.7(5) . . ? F9S C3S S3S 111.0(4) . . ? F7S C3S S3S 110.0(3) . . ? F8S C3S S3S 110.2(3) . . ? O13S C5S C4S 108.8(7) . . ? O13S C6S C7S 114.4(10) . . ? C10S O10S Y 133.3(2) . . ? C11S O11S Y 134.4(2) . . ? C5S O13S C6S 109.4(7) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Y O1 2.2053(18) . ? Y O3 2.2461(18) . ? Y O4 2.3203(19) . ? Y O2 2.3494(19) . ? Y O10S 2.397(2) . ? Y O11S 2.407(2) . ? Y O1S 2.425(2) . ? Y O4S 2.430(2) . ? O1 N1 1.378(3) . ? O2 C18 1.235(3) . ? O3 N3 1.386(3) . ? O4 C38 1.244(3) . ? N1 C17 1.508(3) . ? N1 C1 1.508(3) . ? N1 C11 1.536(3) . ? N2 C18 1.330(4) . ? N2 C21 1.446(4) . ? N3 C37 1.515(3) . ? N3 C3 1.522(4) . ? N3 C31 1.539(3) . ? N4 C38 1.325(4) . ? N4 C41 1.446(3) . ? C1 C2 1.524(4) . ? C2 C3 1.520(4) . ? C11 C12 1.530(4) . ? C11 C15 1.544(4) . ? C12 C13 1.537(4) . ? C13 C14 1.528(5) . ? C14 C15 1.545(5) . ? C15 C16 1.532(4) . ? C16 C17 1.528(4) . ? C17 C18 1.525(4) . ? C21 C26 1.394(4) . ? C21 C22 1.395(5) . ? C22 C23 1.387(5) . ? C22 C27 1.511(5) . ? C23 C24 1.385(6) . ? C24 C25 1.386(6) . ? C25 C26 1.395(5) . ? C26 C29 1.510(5) . ? C27 C28 1.521(6) . ? C29 C30 1.531(6) . ? C31 C32 1.530(4) . ? C31 C35 1.537(4) . ? C32 C33 1.540(5) . ? C33 C34 1.535(5) . ? C34 C35 1.532(4) . ? C35 C36 1.539(4) . ? C36 C37 1.528(4) . ? C37 C38 1.520(4) . ? C41 C46 1.393(4) . ? C41 C42 1.403(5) . ? C42 C43 1.395(4) . ? C42 C47 1.503(5) . ? C43 C44 1.382(5) . ? C44 C45 1.376(6) . ? C45 C46 1.398(4) . ? C46 C49 1.513(5) . ? C47 C48 1.534(5) . ? C49 C50 1.456(7) . ? S1S O3S 1.418(3) . ? S1S O2S 1.439(3) . ? S1S O1S 1.461(2) . ? S1S C1S 1.832(4) . ? S2S O6S 1.428(3) . ? S2S O5S 1.441(3) . ? S2S O4S 1.454(2) . ? S2S C2S 1.833(4) . ? S3S O9S 1.423(3) . ? S3S O8S 1.432(3) . ? S3S O7S 1.450(3) . ? S3S C3S 1.814(5) . ? F1S C1S 1.333(5) . ? F2S C1S 1.323(4) . ? F3S C1S 1.330(5) . ? F4S C2S 1.320(4) . ? F5S C2S 1.328(5) . ? F6S C2S 1.328(5) . ? F7S C3S 1.334(6) . ? F8S C3S 1.343(6) . ? F9S C3S 1.328(7) . ? C4S C5S 1.504(6) . ? C5S O13S 1.380(9) . ? C6S O13S 1.474(11) . ? C6S C7S 1.497(13) . ? O10S C10S 1.420(4) . ? O11S C11S 1.402(4) . ? O12S C12S 1.382(6) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Y O1 N1 C17 -68.7(3) . . . . ? Y O1 N1 C1 53.9(3) . . . . ? Y O1 N1 C11 -178.70(17) . . . . ? Y O3 N3 C37 -36.7(3) . . . . ? Y O3 N3 C3 91.2(3) . . . . ? Y O3 N3 C31 -147.2(2) . . . . ? O1 N1 C1 C2 45.9(3) . . . . ? C17 N1 C1 C2 169.2(2) . . . . ? C11 N1 C1 C2 -78.6(3) . . . . ? N1 C1 C2 C3 -143.0(2) . . . . ? C1 C2 C3 N3 84.2(3) . . . . ? O3 N3 C3 C2 -40.5(3) . . . . ? C37 N3 C3 C2 86.3(3) . . . . ? C31 N3 C3 C2 -162.7(2) . . . . ? O1 N1 C11 C12 -38.7(3) . . . . ? C17 N1 C11 C12 -155.1(2) . . . . ? C1 N1 C11 C12 87.7(3) . . . . ? O1 N1 C11 C15 78.2(3) . . . . ? C17 N1 C11 C15 -38.1(3) . . . . ? C1 N1 C11 C15 -155.3(2) . . . . ? N1 C11 C12 C13 128.6(3) . . . . ? C15 C11 C12 C13 14.1(3) . . . . ? C11 C12 C13 C14 -34.6(4) . . . . ? C12 C13 C14 C15 42.0(4) . . . . ? C12 C11 C15 C16 135.6(3) . . . . ? N1 C11 C15 C16 14.1(3) . . . . ? C12 C11 C15 C14 11.5(3) . . . . ? N1 C11 C15 C14 -110.1(3) . . . . ? C13 C14 C15 C16 -150.2(3) . . . . ? C13 C14 C15 C11 -32.7(4) . . . . ? C11 C15 C16 C17 15.2(3) . . . . ? C14 C15 C16 C17 131.3(3) . . . . ? O1 N1 C17 C18 59.0(3) . . . . ? C1 N1 C17 C18 -65.4(3) . . . . ? C11 N1 C17 C18 174.0(2) . . . . ? O1 N1 C17 C16 -66.4(3) . . . . ? C1 N1 C17 C16 169.3(2) . . . . ? C11 N1 C17 C16 48.7(2) . . . . ? C15 C16 C17 N1 -39.6(3) . . . . ? C15 C16 C17 C18 -162.8(2) . . . . ? Y O2 C18 N2 171.81(19) . . . . ? Y O2 C18 C17 -8.1(4) . . . . ? C21 N2 C18 O2 -3.8(4) . . . . ? C21 N2 C18 C17 176.1(2) . . . . ? N1 C17 C18 O2 -26.5(4) . . . . ? C16 C17 C18 O2 91.4(3) . . . . ? N1 C17 C18 N2 153.6(2) . . . . ? C16 C17 C18 N2 -88.5(3) . . . . ? C18 N2 C21 C26 89.3(3) . . . . ? C18 N2 C21 C22 -87.7(3) . . . . ? C26 C21 C22 C23 1.4(4) . . . . ? N2 C21 C22 C23 178.3(3) . . . . ? C26 C21 C22 C27 -177.2(3) . . . . ? N2 C21 C22 C27 -0.3(4) . . . . ? C21 C22 C23 C24 -1.9(5) . . . . ? C27 C22 C23 C24 176.7(3) . . . . ? C22 C23 C24 C25 0.9(5) . . . . ? C23 C24 C25 C26 0.7(5) . . . . ? C22 C21 C26 C25 0.2(4) . . . . ? N2 C21 C26 C25 -176.8(3) . . . . ? C22 C21 C26 C29 -179.3(3) . . . . ? N2 C21 C26 C29 3.7(4) . . . . ? C24 C25 C26 C21 -1.2(5) . . . . ? C24 C25 C26 C29 178.3(3) . . . . ? C23 C22 C27 C28 103.4(4) . . . . ? C21 C22 C27 C28 -78.1(4) . . . . ? C21 C26 C29 C30 88.7(4) . . . . ? C25 C26 C29 C30 -90.8(4) . . . . ? O3 N3 C31 C32 -39.6(3) . . . . ? C37 N3 C31 C32 -156.8(2) . . . . ? C3 N3 C31 C32 84.0(3) . . . . ? O3 N3 C31 C35 77.7(2) . . . . ? C37 N3 C31 C35 -39.5(3) . . . . ? C3 N3 C31 C35 -158.7(2) . . . . ? C35 C31 C32 C33 11.3(3) . . . . ? N3 C31 C32 C33 126.4(3) . . . . ? C31 C32 C33 C34 -31.4(3) . . . . ? C32 C33 C34 C35 39.7(3) . . . . ? C33 C34 C35 C31 -32.3(3) . . . . ? C33 C34 C35 C36 -149.5(3) . . . . ? C32 C31 C35 C34 13.1(3) . . . . ? N3 C31 C35 C34 -107.7(2) . . . . ? C32 C31 C35 C36 138.2(2) . . . . ? N3 C31 C35 C36 17.4(3) . . . . ? C34 C35 C36 C37 128.1(3) . . . . ? C31 C35 C36 C37 11.4(3) . . . . ? O3 N3 C37 C38 53.7(3) . . . . ? C3 N3 C37 C38 -73.8(3) . . . . ? C31 N3 C37 C38 170.2(2) . . . . ? O3 N3 C37 C36 -69.5(2) . . . . ? C3 N3 C37 C36 163.1(2) . . . . ? C31 N3 C37 C36 47.0(2) . . . . ? C35 C36 C37 N3 -36.6(3) . . . . ? C35 C36 C37 C38 -160.3(2) . . . . ? Y O4 C38 N4 -176.9(2) . . . . ? Y O4 C38 C37 7.9(4) . . . . ? C41 N4 C38 O4 -4.8(4) . . . . ? C41 N4 C38 C37 170.7(3) . . . . ? N3 C37 C38 O4 -44.6(4) . . . . ? C36 C37 C38 O4 72.8(3) . . . . ? N3 C37 C38 N4 139.9(2) . . . . ? C36 C37 C38 N4 -102.7(3) . . . . ? C38 N4 C41 C46 103.7(3) . . . . ? C38 N4 C41 C42 -76.6(4) . . . . ? C46 C41 C42 C43 1.3(4) . . . . ? N4 C41 C42 C43 -178.3(3) . . . . ? C46 C41 C42 C47 -178.0(3) . . . . ? N4 C41 C42 C47 2.3(4) . . . . ? C41 C42 C43 C44 0.5(5) . . . . ? C47 C42 C43 C44 179.8(3) . . . . ? C42 C43 C44 C45 -1.4(5) . . . . ? C43 C44 C45 C46 0.5(5) . . . . ? C42 C41 C46 C45 -2.2(5) . . . . ? N4 C41 C46 C45 177.5(3) . . . . ? C42 C41 C46 C49 177.0(3) . . . . ? N4 C41 C46 C49 -3.4(4) . . . . ? C44 C45 C46 C41 1.2(5) . . . . ? C44 C45 C46 C49 -177.9(3) . . . . ? C43 C42 C47 C48 107.4(4) . . . . ? C41 C42 C47 C48 -73.3(4) . . . . ? C41 C46 C49 C50 -173.7(5) . . . . ? C45 C46 C49 C50 5.4(7) . . . . ? O3S S1S O1S Y 122.1(2) . . . . ? O2S S1S O1S Y -14.6(3) . . . . ? C1S S1S O1S Y -124.7(3) . . . . ? O6S S2S O4S Y 127.0(2) . . . . ? O5S S2S O4S Y -9.8(3) . . . . ? C2S S2S O4S Y -120.3(3) . . . . ? O3S S1S C1S F2S -59.4(4) . . . . ? O2S S1S C1S F2S 62.0(4) . . . . ? O1S S1S C1S F2S 179.3(3) . . . . ? O3S S1S C1S F3S -179.5(3) . . . . ? O2S S1S C1S F3S -58.0(3) . . . . ? O1S S1S C1S F3S 59.3(3) . . . . ? O3S S1S C1S F1S 61.2(3) . . . . ? O2S S1S C1S F1S -177.4(3) . . . . ? O1S S1S C1S F1S -60.1(3) . . . . ? O6S S2S C2S F4S -57.2(3) . . . . ? O5S S2S C2S F4S 64.6(3) . . . . ? O4S S2S C2S F4S -177.8(3) . . . . ? O6S S2S C2S F5S -177.3(3) . . . . ? O5S S2S C2S F5S -55.5(3) . . . . ? O4S S2S C2S F5S 62.1(3) . . . . ? O6S S2S C2S F6S 62.7(3) . . . . ? O5S S2S C2S F6S -175.4(3) . . . . ? O4S S2S C2S F6S -57.8(3) . . . . ? O9S S3S C3S F9S -60.3(4) . . . . ? O8S S3S C3S F9S 177.9(3) . . . . ? O7S S3S C3S F9S 60.5(4) . . . . ? O9S S3S C3S F7S 177.6(4) . . . . ? O8S S3S C3S F7S 55.8(4) . . . . ? O7S S3S C3S F7S -61.6(4) . . . . ? O9S S3S C3S F8S 60.3(4) . . . . ? O8S S3S C3S F8S -61.5(4) . . . . ? O7S S3S C3S F8S -178.9(4) . . . . ? C4S C5S O13S C6S -164.0(8) . . . . ? C7S C6S O13S C5S -69.2(13) . . . . ?