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Information card for entry 1563930
Preview
| Coordinates | 1563930.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C42 H68 Cl14 P4 Rh2 |
|---|---|
| Calculated formula | C42 H68 Cl14 P4 Rh2 |
| Title of publication | Oxidative addition of methylene chloride to Me-DuPhos complexes of palladium and rhodium |
| Authors of publication | Scheetz, Perry M.; Blank, Natalia F.; Gibbons, Sarah K.; Glueck, David S.; Rheingold, Arnold L. |
| Journal of publication | Inorganica Chimica Acta |
| Year of publication | 2018 |
| Journal volume | 483 |
| Pages of publication | 111 - 115 |
| a | 12.6298 ± 0.0006 Å |
| b | 20.0689 ± 0.0009 Å |
| c | 22.7254 ± 0.0009 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 5760.1 ± 0.4 Å3 |
| Cell temperature | 100 K |
| Ambient diffraction temperature | 100 K |
| Number of distinct elements | 5 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0946 |
| Residual factor for significantly intense reflections | 0.0622 |
| Weighted residual factors for significantly intense reflections | 0.1226 |
| Weighted residual factors for all reflections included in the refinement | 0.1376 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.036 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 266990 (current) | 2021-07-05 | cif/ Adding structures of 1563929, 1563930 via cif-deposit CGI script. |
1563930.cif |
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Users of the data should acknowledge the original authors of the
structural data.