#------------------------------------------------------------------------------ #$Date: 2021-08-18 01:14:10 +0300 (Wed, 18 Aug 2021) $ #$Revision: 268103 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/43/1564363.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564363 loop_ _publ_author_name 'Lanquist, Austin P.' 'Gupta, Sayak' 'Al-Afyouni, Kathlyn F.' 'Al-Afyouni, Malik' 'Kodanko, Jeremy J.' 'Turro, Claudia' _publ_section_title ; Trifluoromethyl substitution enhances photoinduced activity against breast cancer cells but reduces ligand exchange in Ru(ii) complex ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC03213E _journal_year 2021 _chemical_formula_moiety 'C43 H40 N5 P Ru, 2(F6 P)' _chemical_formula_sum 'C43 H40 F12 N5 P3 Ru' _chemical_formula_weight 1048.80 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _symmetry_Int_Tables_number 14 _audit_creation_date 2018-04-25 _audit_creation_method ; Olex2 1.2 (compiled 2018.04.18 svn.r3501 for OlexSys, GUI svn.r5488) ; _audit_update_record ; 2020-05-21 deposited with the CCDC. 2021-08-16 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 117.9060(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 20.9185(7) _cell_length_b 11.1390(4) _cell_length_c 21.6643(7) _cell_volume 4461.0(3) _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine (Bourhis et al., 2015)' _diffrn_ambient_temperature 210.15 _diffrn_measured_fraction_theta_full 0.9986 _diffrn_measured_fraction_theta_max 0.9986 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0462 _diffrn_reflns_av_unetI/netI 0.0180 _diffrn_reflns_limit_h_max 27 _diffrn_reflns_limit_h_min -27 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 28 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_number 201564 _diffrn_reflns_theta_full 27.4949 _diffrn_reflns_theta_max 27.49 _diffrn_reflns_theta_min 2.81 _exptl_absorpt_coefficient_mu 0.547 _exptl_crystal_density_diffrn 1.5615 _exptl_crystal_F_000 2117.5751 _refine_diff_density_max 1.6908 _refine_diff_density_min -1.1724 _refine_diff_density_rms 0.1372 _refine_ls_d_res_high 0.7697 _refine_ls_d_res_low 7.2600 _refine_ls_goodness_of_fit_ref 1.1261 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_constraints 34 _refine_ls_number_parameters 657 _refine_ls_number_reflns 10236 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.1261 _refine_ls_R_factor_all 0.0866 _refine_ls_R_factor_gt 0.0747 _refine_ls_shift/su_max 0.0918 _refine_ls_shift/su_mean 0.0106 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0456P)^2^+27.8202P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1731 _refine_ls_wR_factor_ref 0.1915 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 14 _reflns_limit_h_min -27 _reflns_limit_k_max 14 _reflns_limit_k_min 0 _reflns_limit_l_max 28 _reflns_limit_l_min -13 _reflns_number_gt 8764 _reflns_number_total 10236 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL shelx1_a.res in P2(1)/n REM Old TITL Turro 2130 in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.201, Rweak 0.010, Alpha 0.091, Orientation as input REM Formula found by SHELXT: C43 N10 F6 P3 Ru CELL 0.71073 20.9185 11.139 21.6643 90 117.906 90 ZERR 4 0.0007 0.0004 0.0007 0 0.001 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H F N P Ru UNIT 172 160 48 20 12 4 L.S. 4 PLAN 20 TEMP -63 BOND $H list 4 fmap 2 acta WGHT 0.045605 27.820228 FVAR 0.177997 REM REM REM Ru1 6 0.22384 0.49438 0.52719 11.00000 0.04222 0.02541 0.04997 = 0.00047 0.03294 -0.00412 P1 5 0.31843 0.47271 0.49857 11.00000 0.04126 0.02296 0.05013 = 0.00204 0.03264 -0.00164 N1 4 0.27033 0.37415 0.60689 11.00000 0.04041 0.04102 0.04771 = 0.00072 0.02687 -0.00708 N2 4 0.17272 0.63410 0.45982 11.00000 0.05481 0.03187 0.06399 = 0.00789 0.04756 0.00637 N3 4 0.27624 0.63823 0.58974 11.00000 0.05166 0.03833 0.05900 = -0.00796 0.04165 -0.01182 N4 4 0.14126 0.49921 0.55766 11.00000 0.03784 0.03748 0.03818 = -0.00406 0.02207 -0.00355 N5 4 0.15375 0.35670 0.46606 11.00000 0.04551 0.02932 0.04568 = 0.00526 0.03018 0.00116 C1 1 0.29011 0.31247 0.65316 11.00000 0.05334 0.04600 0.05444 = 0.00172 0.03197 -0.00221 C2 1 0.31603 0.23618 0.71445 11.00000 0.07857 0.05785 0.06314 = 0.01821 0.02832 0.00965 AFIX 137 H2a 2 0.32941 0.15840 0.70391 11.00000 -1.50000 H2b 2 0.35791 0.27303 0.75258 11.00000 -1.50000 H2c 2 0.27811 0.22611 0.72782 11.00000 -1.50000 AFIX 0 C3 1 0.11835 0.62528 0.39511 11.00000 0.04731 0.04226 0.06072 = 0.00936 0.03557 0.00426 H3 2 0.10829 0.54915 0.37758 11.00000 0.04267 C4 1 0.07764 0.72221 0.35703 11.00000 0.06988 0.05192 0.08897 = 0.02072 0.04517 0.01534 AFIX 43 H4 2 0.04025 0.71256 0.31114 11.00000 -1.20000 AFIX 0 C5 1 0.09377 0.83366 0.38868 11.00000 0.10565 0.04796 0.10592 = 0.02228 0.06110 0.03186 H5 2 0.06258 0.90578 0.36208 11.00000 0.09741 C6 1 0.14992 0.84616 0.45441 11.00000 0.10350 0.03495 0.10849 = 0.00645 0.06450 0.01412 AFIX 43 H6 2 0.16152 0.92201 0.47589 11.00000 -1.20000 AFIX 0 C7 1 0.18981 0.74560 0.48929 11.00000 0.07519 0.02939 0.07994 = 0.00313 0.05922 0.00152 C8 1 0.25009 0.74840 0.56144 11.00000 0.07360 0.02831 0.07482 = -0.00536 0.05941 -0.01007 C9 1 0.27820 0.85230 0.59976 11.00000 0.10890 0.03436 0.10202 = -0.01238 0.07652 -0.01673 AFIX 43 H9 2 0.26120 0.92755 0.57884 11.00000 -1.20000 AFIX 0 C10 1 0.33057 0.84597 0.66789 11.00000 0.09558 0.05327 0.10390 = -0.03403 0.07016 -0.03592 AFIX 43 H10 2 0.34895 0.91627 0.69436 11.00000 -1.20000 AFIX 0 C11 1 0.35574 0.73594 0.69685 11.00000 0.06678 0.07461 0.06974 = -0.02616 0.04358 -0.03118 H11 2 0.38889 0.71822 0.73935 11.00000 0.03869 C12 1 0.32761 0.63272 0.65633 11.00000 0.05740 0.05355 0.06460 = -0.01100 0.04287 -0.01817 H12 2 0.34603 0.55125 0.67235 11.00000 0.04332 C13 1 0.15401 0.29514 0.41272 11.00000 0.05517 0.03437 0.04642 = 0.00232 0.02872 -0.00206 H13 2 0.19457 0.32300 0.40437 11.00000 0.05599 C14 1 0.10733 0.20168 0.37875 11.00000 0.07114 0.03437 0.05309 = -0.00658 0.03436 -0.00491 H14 2 0.11104 0.15952 0.34096 11.00000 0.09470 C15 1 0.05897 0.16668 0.40110 11.00000 0.06785 0.03582 0.07794 = -0.01249 0.03851 -0.01236 H15 2 0.02351 0.10668 0.37654 11.00000 0.05897 C16 1 0.05611 0.22841 0.45454 11.00000 0.05826 0.04008 0.07460 = -0.00787 0.04017 -0.01283 H16 2 0.01975 0.20370 0.47122 11.00000 0.06619 C17 1 0.10318 0.32420 0.48602 11.00000 0.04129 0.03055 0.04736 = 0.00077 0.02391 -0.00247 C18 1 0.09835 0.40096 0.53912 11.00000 0.04181 0.03934 0.04659 = -0.00009 0.02726 -0.00403 C19 1 0.05158 0.38051 0.56616 11.00000 0.05612 0.05195 0.06360 = -0.00390 0.04069 -0.01399 AFIX 43 H19 2 0.02296 0.31079 0.55423 11.00000 -1.20000 AFIX 0 C20 1 0.04734 0.46463 0.61142 11.00000 0.05779 0.08598 0.06256 = -0.00634 0.04620 -0.01356 AFIX 43 H20 2 0.01628 0.45126 0.63105 11.00000 -1.20000 AFIX 0 C21 1 0.08771 0.56563 0.62733 11.00000 0.05126 0.07789 0.06025 = -0.02180 0.03642 -0.01017 H21 2 0.08294 0.63260 0.65286 11.00000 0.05645 C22 1 0.13580 0.58028 0.60010 11.00000 0.05290 0.05514 0.06077 = -0.01764 0.04079 -0.01307 AFIX 43 H22 2 0.16513 0.64917 0.61199 11.00000 -1.20000 AFIX 0 C23 1 0.33840 0.32037 0.48043 11.00000 0.04201 0.02360 0.04932 = 0.00081 0.02741 0.00016 C24 1 0.31640 0.22025 0.50292 11.00000 0.06613 0.03163 0.06136 = 0.00075 0.04643 -0.00215 H24 2 0.28795 0.22467 0.52375 11.00000 0.04621 C25 1 0.33416 0.10585 0.49093 11.00000 0.07978 0.02618 0.07605 = 0.00229 0.05127 -0.00437 H25 2 0.32019 0.04488 0.50604 11.00000 0.07368 C26 1 0.37475 0.08728 0.45827 11.00000 0.08685 0.03115 0.07805 = -0.00367 0.05539 0.00455 C27 1 0.39394 -0.03808 0.44538 11.00000 0.17137 0.03727 0.16778 = -0.00671 0.13519 0.01067 AFIX 137 H27a 2 0.43161 -0.07076 0.48866 11.00000 -1.50000 H27b 2 0.35143 -0.08894 0.42840 11.00000 -1.50000 H27c 2 0.41107 -0.03483 0.41083 11.00000 -1.50000 AFIX 0 C28 1 0.39799 0.18772 0.43616 11.00000 0.08831 0.04259 0.08858 = -0.00179 0.06992 0.00749 H28 2 0.42695 0.18336 0.41849 11.00000 0.05997 C29 1 0.38038 0.30193 0.44764 11.00000 0.06510 0.03234 0.07010 = 0.00180 0.05026 -0.00234 H29 2 0.39655 0.35743 0.43866 11.00000 0.07680 C30 1 0.40543 0.51782 0.57048 11.00000 0.04475 0.03191 0.05862 = -0.00516 0.03740 -0.00486 C31 1 0.45225 0.43245 0.61511 11.00000 0.05146 0.03252 0.05757 = -0.00947 0.03211 -0.00468 H31 2 0.44187 0.35808 0.60499 11.00000 0.04559 C32 1 0.51827 0.46538 0.67037 11.00000 0.05748 0.04774 0.06731 = -0.01050 0.03287 -0.00126 H32 2 0.54660 0.40184 0.69542 11.00000 0.07651 C33 1 0.54071 0.58420 0.68180 11.00000 0.06013 0.06107 0.06417 = -0.02494 0.04145 -0.01863 C34 1 0.61661 0.61634 0.73623 11.00000 0.07221 0.09422 0.08436 = -0.04855 0.04026 -0.03137 AFIX 137 H34a 2 0.65058 0.59428 0.71940 11.00000 -1.50000 H34b 2 0.61956 0.70206 0.74505 11.00000 -1.50000 H34c 2 0.62838 0.57331 0.77916 11.00000 -1.50000 AFIX 0 C35 1 0.49200 0.66948 0.63901 11.00000 0.07811 0.04207 0.08057 = -0.02318 0.06137 -0.02196 H35 2 0.50033 0.73440 0.64518 11.00000 0.04875 C36 1 0.42578 0.63836 0.58552 11.00000 0.06014 0.03116 0.07771 = -0.00446 0.05329 -0.00547 H36 2 0.39326 0.69148 0.55703 11.00000 0.04473 C37 1 0.31130 0.55527 0.42222 11.00000 0.04621 0.02440 0.06114 = 0.00562 0.03951 0.00310 C38 1 0.36681 0.62311 0.42150 11.00000 0.05274 0.03559 0.06335 = 0.00370 0.04180 -0.00298 AFIX 43 H38 2 0.41098 0.63175 0.46249 11.00000 -1.20000 AFIX 0 C39 1 0.35677 0.67795 0.36009 11.00000 0.06701 0.03537 0.07471 = 0.00520 0.05592 -0.00457 H39 2 0.39217 0.71927 0.36170 11.00000 0.04465 C40 1 0.29402 0.66651 0.29922 11.00000 0.06563 0.04077 0.07464 = 0.01655 0.05301 0.01262 C41 1 0.28442 0.72549 0.23195 11.00000 0.08394 0.07270 0.08797 = 0.03093 0.05867 0.00994 AFIX 137 H41a 2 0.24963 0.79037 0.21949 11.00000 -1.50000 H41b 2 0.33048 0.75721 0.23883 11.00000 -1.50000 H41c 2 0.26704 0.66645 0.19472 11.00000 -1.50000 AFIX 0 C42 1 0.23845 0.59670 0.29890 11.00000 0.05169 0.05641 0.05777 = 0.01457 0.03513 0.01368 AFIX 43 H42 2 0.19516 0.58571 0.25729 11.00000 -1.20000 AFIX 0 C43 1 0.24752 0.54384 0.36021 11.00000 0.04708 0.03939 0.06925 = 0.00956 0.04152 0.00272 H43 2 0.21126 0.50081 0.35669 11.00000 0.04932 P2 5 0.00203 0.43349 0.20795 11.00000 0.06308 0.06609 0.06012 = 0.00537 0.03590 0.01733 F7 3 0.08334 0.43266 0.26243 11.00000 0.06563 0.22547 0.14321 = -0.04391 0.03444 0.00032 F8 3 0.00793 0.54179 0.17758 11.00000 0.52298 0.10341 0.40722 = 0.13388 0.29453 0.03537 F9 3 -0.08142 0.41951 0.15902 11.00000 0.08662 0.20447 0.10900 = -0.05313 0.02392 0.03888 F10 3 0.01637 0.36683 0.15252 11.00000 0.16428 0.18747 0.19926 = -0.07804 0.12677 -0.00030 F11 3 -0.00208 0.29720 0.22517 11.00000 0.26269 0.10864 0.20619 = 0.01127 0.02218 0.00559 F12 3 -0.01465 0.47762 0.26267 11.00000 0.08828 0.55778 0.13296 = -0.20329 0.05793 -0.03345 P3 5 0.37182 0.52056 0.86164 11.00000 0.07366 0.06275 0.07482 = -0.00337 0.03907 0.00381 F1 3 0.29378 0.49763 0.79945 11.00000 0.07649 0.10420 0.13102 = -0.03142 0.02107 0.00928 F2 3 0.33893 0.54954 0.91271 11.00000 0.12920 0.09301 0.13019 = -0.01281 0.09632 -0.00957 F3 3 0.38058 0.38298 0.88158 11.00000 0.16799 0.06307 0.12601 = 0.01967 0.08448 0.02188 F4 3 0.45074 0.54748 0.92146 11.00000 0.08148 0.13907 0.09127 = -0.02246 0.02994 -0.00300 F5 3 0.40392 0.49479 0.80931 11.00000 0.10539 0.11933 0.08922 = 0.00652 0.05808 0.02670 F6 3 0.36264 0.65919 0.84066 11.00000 0.14446 0.06906 0.12675 = 0.00545 0.08336 0.00372 HKLF 4 END Q1 1 0 0.575 0.236111 11 0.05 1.69 Q2 1 0.25 0.525 0.569444 11 0.05 1.23 Q3 1 -0.055556 0.5 0.138889 11 0.05 1.02 Q4 1 -0.027778 0.45 0.263889 11 0.05 0.92 Q5 1 0.027778 0.325 0.194444 11 0.05 0.76 Q6 1 -0.013889 0.275 0.222222 11 0.05 0.75 Q7 1 -0.097222 0.425 0.152778 11 0.05 0.72 Q8 1 0.013889 0.475 0.152778 11 0.05 0.71 Q9 1 0.069444 0.525 0.236111 11 0.05 0.69 Q10 1 0.166667 0.525 0.597222 11 0.05 0.68 Q11 1 0.361111 0.45 0.819444 11 0.05 0.64 Q12 1 0.319444 0.325 0.638889 11 0.05 0.64 Q13 1 -0.055556 0.35 0.194444 11 0.05 0.64 Q14 1 0.305556 0.525 0.513889 11 0.05 0.57 Q15 1 0.013889 0.35 0.138889 11 0.05 0.56 Q16 1 0.180556 0.4 0.486111 11 0.05 0.55 Q17 1 0.416667 0.625 0.861111 11 0.05 0.55 Q18 1 0.430556 0.425 0.847222 11 0.05 0.53 Q19 1 0.236111 0.425 0.527778 11 0.05 0.52 Q20 1 0.277778 0.55 0.444444 11 0.05 0.51 REM The information below was added by Olex2. REM REM R1 = 0.0747 for 8764 Fo > 4sig(Fo) and 0.0866 for all 10236 data REM 657 parameters refined using 0 restraints REM Highest difference peak 1.6908, deepest hole -1.1724 REM Mean Shift 0.0106, Max Shift 0.0918. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0866 REM R1_gt = 0.0747 REM wR_ref = 0.1915 REM GOOF = 1.1261 REM Shift_max = 0.0918 REM Shift_mean = 0.0106 REM Reflections_all = 10236 REM Reflections_gt = 8764 REM Parameters = 657 REM Hole = -1.1724 REM Peak = 1.6908 REM Flack = n/a ; _cod_data_source_file d1sc03213e2.cif _cod_data_source_block Ru(bpy)2P(MePh)3ACN _cod_original_sg_symbol_Hall '-P 2ybc (x-z,y,z)' _cod_database_code 1564363 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C4(H4), C6(H6), C9(H9), C10(H10), C19(H19), C20(H20), C22(H22), C38(H38), C42(H42) 2.b Idealised Me refined as rotating group: C2(H2a,H2b,H2c), C27(H27a,H27b,H27c), C34(H34a,H34b,H34c), C41(H41a,H41b,H41c) ; _iucr_refine_fcf_details ; data_Ru(bpy)2P(MePh)3ACN_CCDC1 _computing_structure_refinement 'olex2.refine (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x+1/2,y+1/2,-z+1/2 3 -x,-y,-z 4 x-1/2,-y-1/2,z-1/2 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/n 1' _space_group_name_Hall '-P 2ybc (x-z,y,z)' _symmetry_space_group_name_H-M 'P 1 21/n 1' _symmetry_space_group_name_Hall '-P 2ybc (x-z,y,z)' _symmetry_Int_Tables_number 14 _cell_length_a 20.9185(7) _cell_length_b 11.1390(4) _cell_length_c 21.6643(7) _cell_angle_alpha 90 _cell_angle_beta 117.9060(10) _cell_angle_gamma 90 _cell_volume 4461.0(3) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -27 0 11 2.836 1.322 22.895 285.378 o -27 0 13 276.932 250.897 28.331 19.977 o -27 0 15 1073.330 984.585 39.825 5.112 o -27 1 11 0.659 -48.071 31.764 164.626 o -27 1 12 151.487 137.705 17.690 37.826 o -27 1 13 104.599 101.309 17.951 52.145 o -27 1 14 417.010 403.683 20.611 13.716 o -27 1 15 16.812 14.288 20.297 196.201 o -26 0 6 246.591 301.830 33.806 19.410 o -26 0 8 479.391 458.017 26.277 11.762 o -26 0 10 42.483 12.212 22.638 118.738 o -26 0 12 534.210 571.023 33.664 9.914 o -26 0 14 1019.520 1119.840 40.875 5.053 o -26 0 16 737.548 603.694 28.275 7.977 o -26 0 18 373.271 288.019 27.201 15.888 o -26 1 6 3.736 7.837 16.621 401.919 o -26 1 7 295.907 275.569 15.213 19.898 o -26 1 8 2.982 53.681 14.319 221.498 o -26 1 9 504.412 582.198 19.994 10.681 o -26 1 10 12.912 28.715 15.869 221.703 o -26 1 11 567.638 524.187 22.212 10.177 o -26 1 12 1.909 13.508 15.929 405.596 o -26 1 13 748.878 694.564 23.489 7.644 o -26 1 14 43.519 124.132 16.998 74.469 o -26 1 15 1579.400 1497.370 34.127 3.406 o -26 1 16 68.159 140.666 16.852 58.569 o -26 1 17 418.934 449.777 19.935 13.215 o -26 1 18 20.898 48.278 16.611 151.030 o -26 1 19 176.748 103.928 18.318 36.343 o -26 2 7 87.468 130.797 17.261 53.289 o -26 2 8 578.391 580.529 23.993 9.671 o -26 2 9 0.144 16.118 14.339 469.819 o -26 2 10 607.565 643.836 23.147 9.051 o -26 2 11 2.088 45.970 17.381 218.976 o -26 2 12 1477.460 1424.480 31.780 3.650 o -26 2 13 8.989 110.640 17.996 110.571 o -26 2 14 1226.070 1247.120 31.197 4.373 o -26 2 15 18.384 106.245 16.779 104.258 o -26 2 16 850.076 854.213 25.504 6.504 o -26 2 17 129.879 168.365 16.947 39.099 o -26 2 18 281.683 306.956 19.061 19.527 o -26 3 8 98.147 109.784 15.977 53.964 o -26 3 9 542.787 580.129 21.141 10.167 o -26 3 10 0.019 24.244 15.505 360.960 o -26 3 11 940.818 905.878 33.230 5.848 o -26 3 12 8.359 61.998 17.350 162.832 o -26 3 13 1023.770 1049.660 33.052 5.248 o -26 3 14 11.547 76.557 16.725 139.381 o -26 3 15 899.708 917.201 27.543 6.079 o -26 3 16 5.741 80.601 18.880 138.666 o -26 3 17 941.644 977.064 32.690 5.702 o -26 4 11 96.320 194.218 16.892 43.024 o -26 4 12 642.359 611.768 21.712 8.900 o -26 4 13 28.909 71.653 17.308 111.771 o -26 4 14 940.970 985.483 41.148 5.570 o -25 0 3 176.207 145.426 25.409 31.603 o -25 0 5 826.218 997.512 53.913 5.776 o -25 0 7 126.140 85.630 18.182 48.163 o -25 0 9 0.384 -63.243 19.236 445.721 o -25 0 11 0.499 -43.620 21.177 367.260 o -25 0 13 346.711 221.348 24.019 18.168 o -25 0 15 1027.250 1066.920 39.296 5.135 o -25 0 17 1568.670 1647.320 45.113 3.252 o -25 0 19 2320.850 1859.730 47.407 2.325 o -25 0 21 2388.530 2042.840 48.897 2.201 o -25 1 3 8.250 40.091 17.254 204.204 o -25 1 4 244.915 170.824 23.435 24.808 o -25 1 5 0.440 6.422 19.752 367.152 o -25 1 6 208.697 222.565 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1403.290 1434.130 36.702 3.750 o -22 1 2 10.365 52.484 14.976 185.873 o -22 1 3 1399.170 1472.750 38.950 3.708 o -22 1 4 125.333 125.038 15.943 44.582 o -22 1 5 34.297 32.071 12.079 155.407 o -22 1 6 30.397 5.925 12.288 218.125 o -22 1 7 0.438 -13.716 11.469 1203.600 o -22 1 8 0.809 -43.449 11.266 1184.510 o -22 1 9 13.018 9.311 12.013 355.879 o -22 1 10 314.261 308.632 14.636 18.458 o -22 1 11 383.317 410.459 14.812 14.676 o -22 1 12 217.944 174.659 12.335 28.493 o -22 1 13 830.753 1027.150 23.572 6.190 o -22 1 14 59.785 80.441 13.415 82.247 o -22 1 15 1170.850 1110.940 25.772 4.744 o -22 1 16 9.089 38.725 12.266 247.628 o -22 1 17 410.875 379.849 14.713 14.377 o -22 1 18 262.590 195.115 13.381 24.090 o -22 1 19 1112.210 1056.140 23.713 5.023 o -22 1 20 21.093 86.056 13.569 122.071 o -22 1 21 485.805 465.442 16.752 11.936 o -22 1 22 144.727 170.953 15.131 36.968 o -22 1 23 1.609 40.438 14.794 269.349 o -22 1 24 10.245 37.353 15.671 214.769 o -22 1 25 126.496 159.843 17.463 40.288 o 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5 8 1076.680 1113.970 24.383 5.039 o -21 5 9 86.078 97.096 12.860 62.752 o -21 5 10 1101.090 1102.320 25.019 4.975 o -21 5 11 10.167 71.553 13.731 161.242 o -21 5 12 1268.180 1295.530 27.861 4.234 o -21 5 13 1112.840 1155.030 26.913 4.843 o -21 5 14 1171.200 1246.640 27.618 4.541 o -21 5 15 8.789 28.191 14.182 268.526 o -21 5 16 34.994 -24.390 13.882 199.451 o -21 5 17 6.424 -41.163 13.773 544.237 o -21 5 18 366.995 347.878 17.376 15.852 o -21 5 19 0.986 17.316 13.362 470.249 o -21 5 20 400.161 409.201 17.549 14.172 o -21 5 21 4.129 11.500 13.918 445.866 o -21 5 22 1077.480 1003.290 26.691 5.204 o -21 5 23 150.065 124.605 18.568 38.868 o -21 6 -1 3.456 -7.794 15.949 527.854 o -21 6 0 132.811 121.459 17.501 42.772 o -21 6 1 236.951 299.381 20.433 21.758 o -21 6 2 509.465 575.389 29.887 10.336 o -21 6 3 1067.430 1345.960 33.070 4.648 o -21 6 4 103.874 152.681 16.961 45.931 o -21 6 5 947.681 919.057 22.297 5.914 o -21 6 6 29.859 56.259 13.238 134.078 o -21 6 7 2364.630 2344.280 34.578 2.146 o -21 6 8 0.263 99.099 15.470 144.243 o -21 6 9 1078.110 1184.490 25.577 4.914 o -21 6 10 11.242 33.846 14.348 230.613 o -21 6 11 708.521 724.942 20.288 7.880 o -21 6 12 195.491 183.902 15.331 29.794 o -21 6 13 958.348 908.837 23.236 5.881 o -21 6 14 25.256 54.326 14.372 142.310 o -21 6 15 325.501 364.296 18.848 16.797 o -21 6 16 17.685 7.409 15.534 263.323 o -21 6 17 1.625 0.437 16.122 571.625 o -21 6 18 282.069 252.097 19.483 20.748 o -21 6 19 391.891 413.452 19.064 14.250 o -21 6 20 35.760 18.710 13.361 165.282 o -21 6 21 136.487 121.044 15.713 42.704 o -21 6 22 19.755 -20.105 14.508 291.232 o -21 7 0 99.687 165.962 24.707 41.723 o -21 7 1 151.638 207.950 17.609 32.891 o -21 7 2 220.776 248.728 17.069 24.713 o -21 7 3 89.469 85.697 15.187 62.244 o -21 7 4 704.914 779.829 28.749 7.559 o -21 7 5 153.262 158.998 14.491 36.730 o -21 7 6 1451.250 1517.120 29.523 3.625 o -21 7 7 93.460 181.259 14.852 45.855 o -21 7 8 1268.120 1375.960 28.373 4.139 o -21 7 9 27.441 76.334 14.434 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11.462 o -15 9 -1 12.525 24.021 14.768 249.534 o -15 9 0 356.149 265.582 17.567 17.516 o -15 9 1 24.719 24.557 12.748 197.790 o -15 9 2 96.654 74.176 13.242 62.908 o -15 9 3 80.030 69.705 14.351 71.573 o -15 9 4 96.558 74.525 15.220 61.576 o -15 9 5 13.659 -18.856 13.171 393.716 o -15 9 6 272.350 315.190 14.418 20.127 o -15 9 7 33.980 25.889 12.142 164.855 o -15 9 8 533.395 663.064 18.770 9.840 o -15 9 9 10.692 31.274 13.841 247.026 o -15 9 10 964.876 1037.140 23.292 5.587 o -15 9 11 608.104 640.322 18.075 9.167 o -15 9 12 3171.160 3050.430 38.068 1.543 o -15 9 13 282.363 320.331 15.835 19.459 o -15 9 14 1772.930 1838.960 29.073 2.925 o -15 9 15 247.578 198.998 14.218 24.903 o -15 9 16 773.192 756.231 19.907 7.317 o -15 9 17 55.933 57.438 14.397 94.238 o -15 9 18 647.543 725.829 22.169 8.332 o -15 9 19 172.927 227.233 18.123 29.397 o -15 9 20 271.688 394.004 19.886 18.094 o -15 9 21 505.110 496.116 21.713 11.234 o -15 10 -4 60.439 58.929 14.800 88.764 o -15 10 -3 289.453 284.994 16.660 19.869 o -15 10 -2 56.304 26.638 15.791 108.803 o -15 10 -1 431.950 442.324 18.728 13.074 o -15 10 0 0.021 3.344 14.481 697.272 o -15 10 1 37.148 47.909 14.831 123.916 o -15 10 2 21.144 5.683 14.110 260.856 o -15 10 3 76.631 29.013 14.664 87.879 o -15 10 4 0.247 -12.268 13.601 886.850 o -15 10 5 150.718 139.402 14.582 38.686 o -15 10 6 162.341 163.601 14.418 35.089 o -15 10 7 901.504 959.665 24.132 6.011 o -15 10 8 136.159 142.126 13.708 41.296 o -15 10 9 1152.440 1149.570 24.583 4.749 o -15 10 10 2.586 27.120 13.229 354.132 o -15 10 11 1040.920 1081.520 24.698 5.212 o -15 10 12 804.133 802.192 20.752 6.968 o -15 10 13 826.220 933.873 25.662 6.419 o -15 10 14 157.734 189.079 15.127 33.849 o -15 10 15 620.499 720.950 21.220 8.606 o -15 10 16 15.846 -1.567 13.155 359.841 o -15 10 17 140.289 192.348 15.642 35.906 o -15 10 18 178.750 146.920 16.583 33.546 o -15 11 -1 3.903 25.682 17.576 271.270 o -15 11 0 228.830 246.550 17.392 24.198 o -15 11 1 89.607 116.435 16.142 55.621 o -15 11 2 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o -14 1 22 34.531 33.704 11.051 156.012 o -14 1 23 2513.510 2557.540 32.844 1.985 o -14 1 24 87.690 58.095 12.787 71.806 o -14 1 25 1623.470 1455.760 26.080 3.403 o -14 1 26 0.709 18.490 15.290 401.688 o -14 1 27 1162.920 1168.100 41.206 4.553 o -14 1 28 2.856 74.966 20.835 142.014 o -14 2 -13 20.400 88.360 31.463 76.710 o -14 2 -12 789.948 1006.260 52.043 5.954 o -14 2 -11 32.179 94.691 21.723 86.093 o -14 2 -10 491.204 368.097 23.850 12.440 o -14 2 -9 2.725 9.582 16.721 401.195 o -14 2 -8 602.854 702.919 25.424 8.762 o -14 2 -7 52.742 86.188 13.845 85.008 o -14 2 -6 388.411 416.743 16.047 14.424 o -14 2 -5 35.875 72.154 9.898 116.970 o -14 2 -4 147.330 164.753 10.758 37.993 o -14 2 -3 10.407 80.944 8.676 164.606 o -14 2 -2 270.774 326.388 13.121 20.026 o -14 2 -1 10.388 51.021 8.554 227.130 o -14 2 0 1022.350 970.911 21.403 5.508 o -14 2 1 1558.310 1528.180 19.421 3.471 o -14 2 2 940.686 1064.880 14.763 5.690 o -14 2 3 526.641 628.556 11.482 10.262 o -14 2 4 4678.140 4869.880 36.748 0.934 o -14 2 5 184.804 103.118 6.588 37.535 o -14 2 6 3267.090 2849.220 24.213 1.557 o -14 2 7 357.521 505.133 10.061 14.295 o -14 2 8 1176.020 1160.680 14.477 4.718 o -14 2 9 166.031 213.289 7.713 32.420 o -14 2 10 967.279 1324.970 16.013 5.104 o -14 2 11 345.338 320.597 8.666 17.350 o -14 2 12 120.748 40.196 6.854 62.786 o -14 2 13 50.849 109.391 7.647 82.966 o -14 2 14 19.546 27.010 7.143 252.798 o -14 2 15 574.876 731.576 13.950 9.107 o -14 2 16 2091.420 1895.080 20.436 2.574 o -14 2 17 279.771 397.985 10.700 18.262 o -14 2 18 937.806 962.850 16.283 5.909 o -14 2 19 201.007 200.877 9.923 29.119 o -14 2 20 3819.670 3417.140 32.805 1.275 o -14 2 21 9.605 38.705 11.046 254.766 o -14 2 22 4742.360 4662.340 49.375 0.935 o -14 2 23 94.507 119.086 13.770 54.783 o -14 2 24 1653.740 1737.770 27.012 3.148 o -14 2 25 5.439 58.452 12.243 211.745 o -14 2 26 1494.300 1552.200 28.502 3.525 o -14 2 27 1.630 90.997 18.452 138.178 o -14 3 -13 331.254 401.036 38.321 14.502 o -14 3 -12 0.877 74.037 22.160 140.650 o -14 3 -11 478.767 462.572 29.482 11.591 o -14 3 -10 10.335 36.521 15.945 214.058 o -14 3 -9 949.864 1028.860 31.643 5.578 o -14 3 -8 3.106 61.637 15.584 192.545 o -14 3 -7 504.832 572.340 24.726 10.600 o -14 3 -6 223.584 153.868 11.757 29.008 o -14 3 -5 57.728 91.237 9.868 83.060 o -14 3 -4 130.495 104.584 9.309 47.928 o -14 3 -3 62.688 70.737 8.398 88.572 o -14 3 -2 30.726 48.021 8.473 154.268 o -14 3 -1 68.139 73.413 8.357 83.037 o -14 3 0 22.914 87.355 8.223 128.647 o -14 3 1 1551.010 1504.520 18.088 3.506 o -14 3 2 136.114 116.369 7.482 45.504 o -14 3 3 9606.480 9491.900 68.230 0.364 o -14 3 4 3550.070 3467.190 28.546 1.349 o -14 3 5 4650.240 4289.110 33.939 0.990 o -14 3 6 995.656 930.317 13.521 5.748 o -14 3 7 1549.580 2044.910 20.123 3.100 o -14 3 8 73.106 84.630 7.005 76.343 o -14 3 9 1366.310 1032.280 14.706 4.377 o -14 3 10 320.094 272.351 8.552 19.262 o -14 3 11 6.460 41.010 7.077 305.171 o -14 3 12 360.298 604.760 11.815 13.097 o -14 3 13 1426.500 1371.600 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79.730 31.633 9.537 89.830 o -14 4 -2 59.295 79.361 9.339 87.017 o -14 4 -1 507.335 418.979 11.011 12.102 o -14 4 0 606.161 609.289 13.416 9.424 o -14 4 1 1078.910 861.033 15.076 5.543 o -14 4 2 1520.710 1648.390 18.905 3.436 o -14 4 3 23.104 26.280 7.607 229.882 o -14 4 4 4271.810 4402.970 36.053 1.050 o -14 4 5 466.438 493.161 14.002 12.103 o -14 4 6 10188.700 9562.860 69.002 0.343 o -14 4 7 299.627 522.100 14.329 15.431 o -14 4 8 1664.890 1737.300 18.597 3.156 o -14 4 9 8.587 -5.000 6.849 815.108 o -14 4 10 8.528 -10.275 7.065 807.698 o -14 4 11 1044.800 1104.190 15.525 5.218 o -14 4 12 131.161 105.299 8.063 47.959 o -14 4 13 398.796 617.384 12.245 12.240 o -14 4 14 580.666 544.262 11.939 10.108 o -14 4 15 198.022 415.928 10.957 21.547 o -14 4 16 2189.980 1918.500 21.248 2.471 o -14 4 17 19.707 117.315 9.460 108.559 o -14 4 18 2460.830 2630.480 26.134 2.004 o -14 4 19 255.360 299.415 12.700 21.482 o -14 4 20 2482.230 2265.370 28.037 2.104 o -14 4 21 54.559 102.408 11.909 79.534 o 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3.198 o -14 5 8 15.288 69.516 7.799 169.583 o -14 5 9 1134.200 1133.620 16.411 4.874 o -14 5 10 463.713 375.388 10.558 13.358 o -14 5 11 15.574 72.126 8.174 163.697 o -14 5 12 144.092 220.912 9.445 34.519 o -14 5 13 2.940 17.409 8.209 593.038 o -14 5 14 69.735 110.991 9.013 69.515 o -14 5 15 363.273 372.188 11.202 15.870 o -14 5 16 11.932 55.968 8.987 204.376 o -14 5 17 561.469 682.461 14.543 9.494 o -14 5 18 384.165 425.790 13.745 14.502 o -14 5 19 1325.810 1263.730 22.368 4.166 o -14 5 20 33.229 34.140 11.436 157.704 o -14 5 21 1609.200 1765.210 27.571 3.189 o -14 5 22 21.043 31.358 13.097 196.889 o -14 5 23 1591.470 1417.590 29.627 3.471 o -14 5 24 16.378 16.367 14.049 257.262 o -14 5 25 809.469 854.729 37.409 6.528 o -14 5 26 3.647 27.404 16.074 289.639 o -14 6 -11 1.339 -45.912 21.527 344.319 o -14 6 -10 374.330 361.848 19.636 15.327 o -14 6 -9 2.449 51.700 13.760 235.144 o -14 6 -8 269.710 294.182 16.104 20.627 o -14 6 -7 158.887 182.811 14.379 34.261 o -14 6 -6 246.196 281.915 16.319 22.163 o -14 6 -5 31.564 125.194 18.412 80.299 o -14 6 -4 22.315 59.378 14.646 142.286 o -14 6 -3 159.325 169.290 14.110 35.178 o -14 6 -2 756.043 742.195 21.488 7.458 o -14 6 -1 187.394 264.839 11.452 27.303 o -14 6 0 1499.170 1580.280 21.762 3.519 o -14 6 1 856.717 756.731 16.254 6.839 o -14 6 2 1484.770 1703.080 21.392 3.443 o -14 6 3 34.813 39.292 9.079 153.498 o -14 6 4 641.593 466.053 11.817 9.850 o -14 6 5 724.993 727.614 14.904 7.815 o -14 6 6 3114.240 3526.700 31.914 1.482 o -14 6 7 312.523 327.904 10.829 18.345 o -14 6 8 1113.730 1192.730 17.925 4.839 o -14 6 9 1285.870 1012.290 16.305 4.610 o -14 6 10 18.243 -0.218 8.051 416.674 o -14 6 11 175.343 206.808 9.584 31.520 o -14 6 12 414.274 445.385 11.143 13.653 o -14 6 13 365.924 479.989 11.769 14.349 o -14 6 14 40.310 62.399 9.252 118.673 o -14 6 15 22.203 75.450 8.996 140.593 o -14 6 16 764.615 757.308 15.648 7.420 o -14 6 17 84.130 87.302 10.749 67.230 o -14 6 18 1797.690 1655.180 26.160 3.016 o -14 6 19 5.599 66.588 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878.049 15.789 6.528 o -14 7 9 904.375 1058.300 16.802 5.844 o -14 7 10 297.924 322.751 10.732 19.042 o -14 7 11 328.477 371.562 10.809 16.983 o -14 7 12 13.896 55.398 9.046 196.647 o -14 7 13 16.045 7.352 9.390 370.048 o -14 7 14 48.599 71.836 10.215 100.158 o -14 7 15 33.297 81.883 10.498 112.661 o -14 7 16 240.921 261.879 12.906 23.378 o -14 7 17 1035.720 991.409 22.936 5.406 o -14 7 18 15.965 98.405 13.010 121.658 o -14 7 19 1729.900 1619.280 31.579 3.110 o -14 7 20 97.860 113.196 15.827 53.586 o -14 7 21 1437.940 1471.570 30.498 3.686 o -14 7 22 116.387 132.808 16.344 45.581 o -14 7 23 577.250 566.307 21.402 9.831 o -14 7 24 24.447 21.057 15.320 190.061 o -14 8 -9 0.036 -13.806 18.215 505.629 o -14 8 -8 155.146 135.341 18.805 37.094 o -14 8 -7 38.031 105.757 17.719 83.734 o -14 8 -6 199.215 280.169 17.146 25.117 o -14 8 -5 91.592 146.967 15.799 50.388 o -14 8 -4 0.035 53.343 13.438 248.476 o -14 8 -3 79.436 83.265 13.109 69.159 o -14 8 -2 1137.480 1037.300 23.264 4.975 o -14 8 -1 324.343 266.960 13.781 18.943 o -14 8 0 400.545 351.624 13.438 15.041 o -14 8 1 262.019 220.143 12.269 23.416 o -14 8 2 1278.260 1339.570 23.623 4.182 o -14 8 3 12.818 34.356 10.910 248.615 o -14 8 4 1043.670 937.285 19.545 5.504 o -14 8 5 2.107 45.080 10.555 295.406 o -14 8 6 1413.780 1476.410 21.642 3.764 o -14 8 7 252.761 337.846 12.017 20.679 o -14 8 8 1851.210 1864.100 22.987 2.835 o -14 8 9 63.652 151.776 10.833 61.729 o -14 8 10 584.135 776.949 17.213 8.752 o -14 8 11 943.865 1092.500 21.058 5.579 o -14 8 12 641.755 735.718 18.272 8.405 o -14 8 13 46.666 177.684 12.264 62.714 o -14 8 14 71.985 93.307 11.579 71.615 o -14 8 15 8.618 89.111 11.462 150.075 o -14 8 16 55.252 97.416 12.731 80.046 o -14 8 17 290.425 306.301 15.679 19.425 o -14 8 18 1164.010 1116.840 26.992 4.747 o -14 8 19 304.882 313.636 18.405 18.476 o -14 8 20 1761.740 1629.810 33.000 3.056 o -14 8 21 281.400 266.166 18.086 20.569 o -14 8 22 441.245 406.822 18.791 13.244 o -14 8 23 3.382 -1.969 15.321 565.136 o -14 9 -7 83.341 76.122 16.055 66.632 o -14 9 -6 79.504 117.461 16.695 58.777 o -14 9 -5 0.401 62.986 16.644 193.345 o -14 9 -4 383.267 355.355 17.012 15.305 o -14 9 -3 202.826 144.184 15.014 31.166 o -14 9 -2 26.720 38.863 14.646 156.755 o -14 9 -1 742.531 744.451 22.383 7.530 o -14 9 0 138.411 121.129 12.913 43.176 o -14 9 1 1244.210 1214.820 24.718 4.410 o -14 9 2 386.858 369.410 16.645 15.037 o -14 9 3 1105.610 1109.410 23.865 4.957 o -14 9 4 310.898 262.495 14.334 19.579 o -14 9 5 1636.250 1684.290 27.869 3.207 o -14 9 6 200.808 266.474 13.025 25.990 o -14 9 7 1154.550 1197.240 21.310 4.694 o -14 9 8 14.862 69.218 11.986 158.080 o -14 9 9 1665.080 1534.450 24.935 3.283 o -14 9 10 451.926 571.858 16.848 11.617 o -14 9 11 1551.490 1622.790 30.023 3.370 o -14 9 12 156.847 344.271 15.579 26.087 o -14 9 13 63.309 59.582 12.177 89.280 o -14 9 14 70.357 78.822 12.968 75.892 o -14 9 15 16.025 22.990 12.401 252.838 o -14 9 16 127.106 139.472 13.516 43.448 o -14 9 17 449.599 409.850 18.442 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119.353 15.490 39.803 o -14 12 2 745.551 780.165 28.660 7.285 o -14 12 3 4.297 39.092 15.595 245.079 o -14 12 4 1582.470 1506.620 30.549 3.410 o -14 12 5 5.825 52.765 15.397 201.240 o -14 12 6 1169.100 1067.770 27.631 4.799 o -14 12 7 0.284 58.913 16.347 205.101 o -14 12 8 954.563 908.792 24.876 5.881 o -14 12 9 3.418 12.867 14.431 429.912 o -14 12 10 283.562 270.627 17.536 20.406 o -14 12 11 74.835 93.695 16.247 66.330 o -14 12 12 12.202 71.921 16.950 142.140 o -13 0 -11 105.523 150.441 30.500 38.981 o -13 0 -9 189.081 315.147 37.300 21.195 o -13 0 -7 806.208 1031.820 33.435 6.168 o -13 0 -5 2097.480 1746.570 33.448 2.611 o -13 0 -3 11490.100 11846.100 140.239 0.270 o -13 0 -1 5943.480 5660.480 70.585 0.704 o -13 0 1 790.202 838.607 19.009 6.962 o -13 0 3 3082.830 3261.680 41.694 1.532 o -13 0 5 5447.410 5806.570 69.616 0.750 o -13 0 7 931.938 1006.110 18.798 5.823 o -13 0 9 10822.200 11306.000 109.625 0.296 o -13 0 11 11140.300 12539.600 121.254 0.272 o -13 0 13 3391.300 3494.090 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5.593 o -12 5 -4 2368.980 2238.470 26.383 2.194 o -12 5 -3 4.519 57.355 9.916 235.113 o -12 5 -2 106.309 119.408 8.770 52.843 o -12 5 -1 137.157 151.808 9.516 41.163 o -12 5 0 101.228 95.205 8.120 59.055 o -12 5 1 480.485 536.251 11.303 11.570 o -12 5 2 1404.590 1437.430 16.800 3.836 o -12 5 3 5635.410 5935.260 44.887 0.731 o -12 5 4 264.195 196.620 7.673 24.351 o -12 5 5 8987.660 8634.570 62.616 0.406 o -12 5 6 6369.700 6779.490 50.611 0.619 o -12 5 7 7427.700 7147.790 52.409 0.528 o -12 5 8 1738.320 1706.700 17.993 3.079 o -12 5 9 1553.260 1877.750 18.448 3.214 o -12 5 10 93.632 204.466 7.897 45.065 o -12 5 11 1799.540 1576.730 16.604 3.087 o -12 5 12 27.064 62.712 7.429 147.228 o -12 5 13 57.109 135.106 8.369 70.149 o -12 5 14 746.580 992.137 15.512 6.802 o -12 5 15 216.142 295.771 10.178 24.093 o -12 5 16 1523.300 1371.530 17.998 3.670 o -12 5 17 18.270 -7.411 8.777 403.942 o -12 5 18 133.663 224.229 10.553 35.575 o -12 5 19 114.147 267.941 11.900 35.021 o -12 5 20 54.989 128.393 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14.334 5.996 o -12 6 8 7136.100 6890.300 50.984 0.556 o -12 6 9 1931.790 2421.730 22.323 2.475 o -12 6 10 5185.640 5225.110 38.684 0.831 o -12 6 11 599.072 621.348 12.055 9.453 o -12 6 12 28.625 30.260 8.181 190.991 o -12 6 13 1403.070 1340.900 17.103 3.935 o -12 6 14 1297.750 1305.720 17.399 4.203 o -12 6 15 5.207 31.777 8.364 364.182 o -12 6 16 29.172 25.643 9.339 193.744 o -12 6 17 127.774 130.057 10.659 45.145 o -12 6 18 124.346 100.089 11.836 49.408 o -12 6 19 41.767 50.992 11.771 120.924 o -12 6 20 216.649 187.381 13.709 27.867 o -12 6 21 2.464 33.069 12.571 329.154 o -12 6 22 1362.530 1390.570 27.299 3.926 o -12 6 23 9.683 60.694 16.326 166.374 o -12 6 24 844.449 805.790 33.890 6.536 o -12 6 25 1.923 45.496 17.072 224.270 o -12 7 -11 258.196 267.934 15.624 21.948 o -12 7 -10 60.041 60.975 13.560 89.877 o -12 7 -9 355.940 364.300 15.187 16.044 o -12 7 -8 283.416 306.080 14.262 19.838 o -12 7 -7 633.755 654.318 17.706 8.853 o -12 7 -6 108.369 183.854 13.229 42.810 o -12 7 -5 908.703 948.280 26.384 5.980 o -12 7 -4 14.486 108.553 11.457 119.147 o -12 7 -3 6.833 61.284 10.551 208.144 o -12 7 -2 1175.600 1152.150 18.801 4.712 o -12 7 -1 49.445 101.006 9.383 86.168 o -12 7 0 138.010 82.048 9.179 48.950 o -12 7 1 455.900 668.150 14.439 10.890 o -12 7 2 86.461 162.905 9.611 52.004 o -12 7 3 4749.530 4773.970 39.147 0.929 o -12 7 4 388.326 491.800 11.606 13.702 o -12 7 5 2690.480 2180.720 22.320 2.005 o -12 7 6 374.213 464.399 10.892 14.362 o -12 7 7 4751.430 5179.300 41.632 0.896 o -12 7 8 28.441 150.433 9.312 83.259 o -12 7 9 1621.550 1780.670 20.241 3.182 o -12 7 10 102.265 84.661 9.337 60.292 o -12 7 11 1340.770 1323.510 18.451 4.082 o -12 7 12 0.145 33.730 8.507 433.134 o -12 7 13 231.133 232.660 10.068 25.253 o -12 7 14 24.999 -1.745 8.215 316.179 o -12 7 15 4.581 -10.976 9.382 971.781 o -12 7 16 74.312 52.345 10.023 85.187 o -12 7 17 118.169 66.873 12.122 56.414 o -12 7 18 1.150 52.106 11.885 260.044 o -12 7 19 674.225 619.236 18.801 8.623 o -12 7 20 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688.185 717.523 14.472 8.145 o -12 8 10 1921.800 1918.170 22.011 2.730 o -12 8 11 447.425 460.528 12.357 12.788 o -12 8 12 19.933 72.273 10.272 146.397 o -12 8 13 341.373 339.099 13.096 17.000 o -12 8 14 482.781 414.072 13.655 12.527 o -12 8 15 6.418 12.302 10.746 482.058 o -12 8 16 5.290 -3.348 11.651 718.750 o -12 8 17 80.778 94.552 12.884 65.769 o -12 8 18 289.932 233.309 16.458 21.108 o -12 8 19 41.181 55.143 13.758 114.457 o -12 8 20 295.205 236.600 16.400 20.765 o -12 8 21 3.315 23.688 14.555 340.850 o -12 8 22 756.906 707.670 21.992 7.564 o -12 8 23 27.097 61.537 16.450 124.812 o -12 9 -10 43.120 55.909 15.240 108.101 o -12 9 -9 215.713 208.156 16.936 26.632 o -12 9 -8 92.790 81.331 15.053 61.846 o -12 9 -7 155.424 163.237 19.684 34.764 o -12 9 -6 260.547 234.070 14.340 22.903 o -12 9 -5 422.218 333.319 15.674 14.634 o -12 9 -4 500.865 464.721 16.720 11.694 o -12 9 -3 34.835 81.138 13.942 105.192 o -12 9 -2 1991.630 1861.740 35.831 2.652 o -12 9 -1 283.191 267.874 13.030 20.840 o -12 9 0 1836.750 1650.800 25.655 2.971 o -12 9 1 389.130 484.744 15.039 13.660 o -12 9 2 339.124 282.968 12.470 18.110 o -12 9 3 3487.930 3188.010 32.227 1.411 o -12 9 4 843.265 921.002 18.650 6.441 o -12 9 5 2375.150 2434.040 27.109 2.120 o -12 9 6 171.395 172.738 11.038 33.867 o -12 9 7 3797.450 3497.230 34.571 1.269 o -12 9 8 895.787 914.918 18.978 6.192 o -12 9 9 1074.900 1222.820 22.087 4.888 o -12 9 10 1158.340 1237.200 21.562 4.626 o -12 9 11 688.304 736.001 17.531 8.032 o -12 9 12 84.479 98.483 11.382 64.015 o -12 9 13 1148.620 1120.910 22.165 4.819 o -12 9 14 0.116 2.557 11.942 997.881 o -12 9 15 16.940 -12.632 12.279 361.356 o -12 9 16 115.041 171.324 13.945 42.516 o -12 9 17 6.416 9.091 13.014 450.979 o -12 9 18 35.099 27.564 13.651 153.507 o -12 9 19 252.295 269.075 16.211 22.191 o -12 9 20 55.936 73.647 15.852 84.921 o -12 9 21 569.829 585.406 21.016 9.816 o -12 10 -8 202.568 247.993 20.470 25.571 o -12 10 -7 35.827 20.754 15.186 154.299 o -12 10 -6 118.514 95.518 14.616 50.590 o -12 10 -5 368.731 476.445 25.405 13.731 o -12 10 -4 229.057 239.302 16.258 24.563 o -12 10 -3 575.693 480.963 17.966 10.457 o -12 10 -2 28.305 62.186 13.645 130.209 o -12 10 -1 464.250 394.597 15.023 13.032 o -12 10 0 948.612 990.068 23.156 5.750 o -12 10 1 2063.730 1867.810 29.824 2.595 o -12 10 2 1281.550 1320.960 26.579 4.181 o -12 10 3 670.078 665.111 18.296 8.465 o -12 10 4 1806.420 1753.250 26.137 2.944 o -12 10 5 54.810 35.326 11.573 113.366 o -12 10 6 1943.900 1872.180 26.252 2.722 o -12 10 7 125.416 149.814 12.551 42.996 o -12 10 8 851.948 905.598 20.808 6.415 o -12 10 9 1011.660 916.084 23.166 5.643 o -12 10 10 280.276 397.115 14.558 18.068 o -12 10 11 839.290 758.628 18.731 6.911 o -12 10 12 269.346 315.602 14.564 20.247 o -12 10 13 179.717 199.075 14.121 30.842 o -12 10 14 174.421 222.012 14.396 30.148 o -12 10 15 6.277 94.541 13.528 142.612 o -12 10 16 0.008 38.560 12.731 323.199 o -12 10 17 25.611 99.920 15.313 102.422 o -12 10 18 71.713 78.367 16.332 72.000 o 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113.597 125.130 16.794 46.986 o -12 11 17 23.892 34.285 16.438 162.770 o -12 12 -2 5.213 22.844 15.888 299.553 o -12 12 -1 82.789 60.911 14.747 72.162 o -12 12 0 191.785 183.766 16.416 29.994 o -12 12 1 439.569 354.652 18.262 13.863 o -12 12 2 913.409 900.794 24.114 6.092 o -12 12 3 221.589 200.403 16.784 26.493 o -12 12 4 1259.450 1206.270 27.606 4.365 o -12 12 5 164.170 166.912 16.136 34.241 o -12 12 6 1880.750 1790.560 31.502 2.821 o -12 12 7 207.718 204.030 15.289 27.710 o -12 12 8 1466.900 1330.440 28.434 3.773 o -12 12 9 207.118 235.361 17.575 26.144 o -12 12 10 885.749 832.751 24.409 6.389 o -12 12 11 111.507 136.650 17.156 45.938 o -12 12 12 422.133 472.790 18.721 12.967 o -12 12 13 4.742 82.617 15.507 153.316 o -12 12 14 226.907 314.716 18.378 22.117 o -11 0 -9 997.349 1010.980 36.254 5.375 o -11 0 -7 881.392 869.452 41.179 6.068 o -11 0 -5 5227.280 4951.510 77.052 0.825 o -11 0 -3 3080.150 2820.640 33.981 1.631 o -11 0 -1 20019.700 18259.400 210.567 0.123 o -11 0 1 23985.100 22696.700 247.941 0.090 o -11 0 3 9387.870 10968.400 112.781 0.341 o -11 0 5 8103.490 7908.580 80.063 0.461 o -11 0 7 521.265 565.124 15.463 10.677 o -11 0 9 13235.700 14077.700 134.192 0.217 o -11 0 11 9112.350 8580.920 94.603 0.397 o -11 0 13 1458.430 1194.150 21.064 3.958 o -11 0 15 387.336 498.472 14.430 13.569 o -11 0 17 4964.350 4781.940 49.715 0.890 o -11 0 19 959.494 592.393 17.313 6.712 o -11 0 21 409.746 386.570 16.451 14.258 o -11 0 23 289.599 317.523 21.846 18.724 o -11 0 25 0.016 -8.272 20.486 400.267 o -11 0 27 70.606 89.312 23.200 62.536 o -11 1 -10 255.511 230.736 16.298 23.120 o -11 1 -9 4.327 46.209 15.889 220.635 o -11 1 -8 472.185 607.304 32.720 10.496 o -11 1 -7 0.372 28.817 12.430 392.002 o -11 1 -6 2645.170 2447.350 34.015 1.938 o -11 1 -5 4.230 153.557 9.292 105.408 o -11 1 -4 7006.400 6821.990 60.589 0.566 o -11 1 -3 379.079 381.574 9.540 15.338 o -11 1 -2 14012.200 13614.500 109.476 0.210 o -11 1 -1 337.789 356.590 8.711 16.992 o -11 1 0 1275.190 1732.880 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195.713 16.605 50.353 o -11 1 26 122.741 136.688 17.147 43.420 o -11 1 27 0.353 185.205 23.578 73.478 o -11 1 28 91.205 11.924 34.855 55.560 o -11 2 -10 0.165 -18.318 13.778 871.446 o -11 2 -9 403.207 404.147 17.445 14.164 o -11 2 -8 20.234 93.350 17.209 109.076 o -11 2 -7 1253.790 1351.230 24.957 4.219 o -11 2 -6 41.495 85.976 11.788 98.172 o -11 2 -5 2469.440 2344.920 29.289 2.084 o -11 2 -4 96.929 128.273 7.962 54.678 o -11 2 -3 2383.050 2226.720 22.508 2.193 o -11 2 -2 676.871 686.573 19.598 8.295 o -11 2 -1 21567.700 20740.700 154.121 0.108 o -11 2 0 174.877 410.742 13.013 22.856 o -11 2 1 15629.400 14688.200 110.369 0.182 o -11 2 2 2564.670 2879.780 23.545 1.875 o -11 2 3 14395.100 15190.000 105.335 0.194 o -11 2 4 293.519 450.441 8.908 16.897 o -11 2 5 1309.480 1542.730 15.176 3.926 o -11 2 6 781.188 983.843 12.380 6.654 o -11 2 7 1822.680 1514.570 15.156 3.100 o -11 2 8 385.412 507.927 9.876 13.630 o -11 2 9 20.914 -6.828 5.936 396.931 o -11 2 10 574.754 393.226 8.498 11.261 o -11 2 11 1563.650 1429.160 15.569 3.555 o -11 2 12 1313.430 1194.000 14.291 4.309 o -11 2 13 39.233 158.270 7.152 74.404 o -11 2 14 121.905 356.678 8.660 29.355 o -11 2 15 22.688 6.449 6.671 319.780 o -11 2 16 118.550 175.054 8.190 42.794 o -11 2 17 7947.920 7853.910 57.198 0.475 o -11 2 18 1805.360 1666.700 19.257 3.016 o -11 2 19 1150.950 1150.590 16.573 4.797 o -11 2 20 299.151 345.382 10.703 18.532 o -11 2 21 1481.060 1417.590 20.726 3.697 o -11 2 22 62.412 128.959 12.206 66.783 o -11 2 23 513.220 670.960 22.302 9.945 o -11 2 24 31.462 262.141 16.194 50.926 o -11 2 25 2.197 38.888 15.371 263.469 o -11 2 26 0.023 246.078 16.698 65.281 o -11 2 27 26.548 32.579 16.592 156.896 o -11 3 -10 167.291 150.671 12.869 35.617 o -11 3 -9 11.503 -12.231 11.370 490.509 o -11 3 -8 2.684 -31.428 11.055 977.363 o -11 3 -7 4.471 14.344 8.656 577.738 o -11 3 -6 1990.160 1890.250 27.217 2.662 o -11 3 -5 0.033 91.448 16.200 151.039 o -11 3 -4 7993.240 7715.150 64.345 0.475 o -11 3 -3 229.640 206.246 8.113 26.517 o -11 3 -2 8667.350 8356.730 69.293 0.425 o -11 3 -1 3684.880 3297.570 28.856 1.334 o -11 3 0 18020.500 17650.900 126.693 0.142 o -11 3 1 609.933 410.037 10.091 10.620 o -11 3 2 18599.100 19638.500 140.551 0.130 o -11 3 3 64.386 150.525 6.795 63.338 o -11 3 4 3120.560 3121.800 26.642 1.560 o -11 3 5 789.549 531.248 10.741 8.116 o -11 3 6 3115.610 2876.620 24.319 1.613 o -11 3 7 1315.700 1708.890 18.444 3.741 o -11 3 8 1261.110 1693.140 17.021 3.866 o -11 3 9 49.387 153.356 6.811 70.071 o -11 3 10 17.756 -0.027 5.914 461.119 o -11 3 11 266.158 385.037 8.647 19.155 o -11 3 12 427.127 384.655 8.788 14.102 o -11 3 13 1697.120 1753.510 17.775 3.103 o -11 3 14 3193.010 3736.810 30.541 1.419 o -11 3 15 412.950 601.131 11.381 12.153 o -11 3 16 1613.860 1469.560 17.746 3.433 o -11 3 17 7.536 21.041 7.829 424.012 o -11 3 18 434.469 483.441 11.074 12.846 o -11 3 19 142.797 133.937 9.289 41.846 o -11 3 20 995.235 1066.430 17.959 5.453 o -11 3 21 12.283 63.962 9.447 184.330 o -11 3 22 740.784 683.072 17.591 7.832 o -11 3 23 30.220 223.750 13.255 59.408 o -11 3 24 36.685 19.227 14.951 155.057 o -11 3 25 45.318 91.911 14.688 87.729 o -11 3 26 34.238 -12.853 14.548 198.308 o -11 3 27 56.766 105.342 16.906 72.257 o -11 4 -10 20.771 27.905 13.861 200.791 o -11 4 -9 345.654 366.462 18.946 16.123 o -11 4 -8 243.529 180.622 11.057 26.198 o -11 4 -7 187.054 216.637 12.620 29.400 o -11 4 -6 50.266 17.281 10.005 140.582 o -11 4 -5 325.621 376.449 10.955 16.991 o -11 4 -4 53.697 60.233 8.428 103.012 o -11 4 -3 5669.910 5280.600 47.042 0.764 o -11 4 -2 13.895 62.797 8.301 184.567 o -11 4 -1 18570.600 17984.900 134.875 0.136 o -11 4 0 256.853 351.823 8.603 20.320 o -11 4 1 10778.100 10701.300 78.688 0.308 o -11 4 2 48.960 142.097 7.145 73.407 o -11 4 3 12545.400 12929.700 92.338 0.242 o -11 4 4 38.671 65.459 6.272 122.864 o -11 4 5 3047.400 3316.030 27.444 1.550 o -11 4 6 318.680 401.965 8.882 16.868 o -11 4 7 771.848 557.117 10.971 8.152 o -11 4 8 1012.180 993.847 12.723 5.556 o -11 4 9 327.586 551.301 10.225 14.456 o -11 4 10 672.211 786.098 12.249 8.022 o -11 4 11 539.652 646.401 12.221 9.983 o -11 4 12 68.167 108.269 7.392 71.942 o -11 4 13 1955.620 1793.580 18.286 2.767 o -11 4 14 488.419 599.618 11.610 10.968 o -11 4 15 4153.890 4412.070 35.852 1.073 o -11 4 16 54.963 13.855 7.783 138.710 o -11 4 17 1843.500 1944.880 21.855 2.800 o -11 4 18 5.401 56.259 8.956 239.092 o -11 4 19 757.081 889.541 16.658 7.033 o -11 4 20 466.324 466.295 12.828 12.371 o -11 4 21 314.064 332.012 13.056 18.102 o -11 4 22 76.214 89.304 13.510 68.964 o -11 4 23 0.550 -42.704 12.246 1049.700 o -11 4 24 1.353 -19.354 14.656 700.806 o -11 4 25 0.036 -58.265 13.937 862.433 o -11 4 26 90.542 168.534 16.762 47.338 o -11 4 27 200.599 129.794 31.831 28.007 o -11 5 -10 152.266 142.145 14.963 38.102 o -11 5 -9 3.803 2.345 17.896 407.452 o -11 5 -8 133.785 206.550 11.217 36.750 o -11 5 -7 3.047 23.214 11.430 417.528 o -11 5 -6 242.473 309.738 11.582 21.977 o -11 5 -5 47.761 103.104 9.903 86.250 o -11 5 -4 3378.080 3198.480 34.226 1.444 o -11 5 -3 28.449 36.491 8.439 178.985 o -11 5 -2 5566.830 5330.900 43.745 0.774 o -11 5 -1 1837.120 1829.430 21.303 2.874 o -11 5 0 8130.140 8304.960 64.150 0.453 o -11 5 1 2314.960 2546.420 22.968 2.129 o -11 5 2 3857.010 3591.050 28.309 1.244 o -11 5 3 0.600 38.269 6.547 410.795 o -11 5 4 2655.730 2837.220 24.073 1.838 o -11 5 5 24.752 39.473 6.530 193.324 o -11 5 6 4421.360 4440.430 34.212 1.018 o -11 5 7 1249.900 1623.910 16.836 3.960 o -11 5 8 104.356 124.120 7.107 53.157 o -11 5 9 814.402 559.504 10.646 7.815 o -11 5 10 100.018 79.053 6.855 63.365 o -11 5 11 124.859 311.208 8.397 31.453 o -11 5 12 1392.410 1315.560 15.248 3.989 o -11 5 13 2131.650 2183.640 20.216 2.409 o -11 5 14 8190.450 8047.940 59.834 0.457 o -11 5 15 746.727 976.286 16.876 6.835 o -11 5 16 1993.890 2080.970 23.477 2.573 o -11 5 17 0.575 -3.678 8.586 1992.290 o -11 5 18 2916.440 2776.930 27.625 1.720 o -11 5 19 238.249 175.518 11.495 26.783 o -11 5 20 2055.260 1969.520 26.722 2.561 o -11 5 21 48.420 97.556 12.007 85.964 o -11 5 22 509.312 459.131 16.874 11.600 o -11 5 23 528.600 563.765 18.954 10.508 o -11 5 24 27.086 28.272 13.511 177.212 o -11 5 25 195.628 186.655 19.848 28.834 o -11 5 26 73.675 53.413 16.600 78.315 o -11 6 -10 38.990 22.571 14.603 146.437 o -11 6 -9 43.782 36.426 12.191 129.121 o -11 6 -8 214.888 203.587 13.035 27.398 o -11 6 -7 1374.640 1578.670 26.885 3.720 o -11 6 -6 99.828 111.625 10.382 55.725 o -11 6 -5 945.648 1031.440 18.499 5.714 o -11 6 -4 295.011 249.258 10.636 20.861 o -11 6 -3 4372.760 4426.640 40.774 1.026 o -11 6 -2 11.165 35.110 8.592 276.847 o -11 6 -1 8567.180 7848.280 60.200 0.443 o -11 6 0 77.185 122.449 8.267 63.365 o -11 6 1 5209.020 5440.660 42.180 0.812 o -11 6 2 115.273 130.200 7.794 48.925 o -11 6 3 2623.050 2814.970 24.537 1.860 o -11 6 4 595.085 647.768 12.172 9.354 o -11 6 5 803.453 715.895 12.780 7.325 o -11 6 6 349.492 353.671 9.052 16.645 o -11 6 7 2294.720 2425.410 21.654 2.186 o -11 6 8 19.178 82.537 7.500 142.381 o -11 6 9 2801.900 2670.160 23.404 1.806 o -11 6 10 6.456 54.116 7.657 246.766 o -11 6 11 2246.200 2341.380 22.229 2.252 o -11 6 12 44.195 49.954 7.953 124.475 o -11 6 13 1432.720 1436.340 17.500 3.780 o -11 6 14 179.683 168.720 9.188 33.316 o -11 6 15 2008.570 1902.910 21.054 2.650 o -11 6 16 753.691 652.244 14.014 7.892 o -11 6 17 939.945 1011.070 19.729 5.771 o -11 6 18 26.887 39.374 10.637 171.729 o -11 6 19 1286.770 1216.700 22.145 4.315 o -11 6 20 3.129 1.571 11.588 812.515 o -11 6 21 304.090 264.208 14.032 19.865 o -11 6 22 119.325 272.257 18.387 32.731 o -11 6 23 118.138 183.359 15.813 40.197 o -11 6 24 290.651 398.728 19.456 17.352 o -11 6 25 1.242 38.276 16.118 263.432 o -11 7 -10 37.528 19.418 12.747 161.546 o -11 7 -9 109.490 74.365 13.251 57.656 o -11 7 -8 347.057 376.102 15.557 16.116 o -11 7 -7 69.122 125.027 12.540 64.295 o -11 7 -6 1541.830 1704.210 26.451 3.336 o -11 7 -5 351.288 326.528 13.121 16.879 o -11 7 -4 3905.670 3803.390 36.749 1.199 o -11 7 -3 193.833 166.714 11.408 31.469 o -11 7 -2 586.114 557.884 13.369 9.939 o -11 7 -1 57.384 49.533 8.658 104.754 o -11 7 0 7138.990 7760.610 60.536 0.525 o -11 7 1 23.847 89.774 8.789 123.939 o -11 7 2 4998.650 4671.540 36.603 0.899 o -11 7 3 550.402 714.265 13.968 9.451 o -11 7 4 3818.890 4273.320 33.923 1.164 o -11 7 5 6.849 26.306 7.342 395.339 o -11 7 6 422.198 569.929 11.385 12.264 o -11 7 7 3073.320 2926.480 26.159 1.619 o -11 7 8 964.334 1099.040 17.622 5.511 o -11 7 9 1789.590 1662.010 19.238 3.039 o -11 7 10 25.374 58.429 9.123 153.049 o -11 7 11 63.145 125.780 9.261 68.955 o -11 7 12 3066.830 2725.490 26.019 1.665 o -11 7 13 641.782 715.435 14.304 8.549 o -11 7 14 587.121 766.111 14.214 8.818 o -11 7 15 281.020 309.061 10.715 20.090 o -11 7 16 309.067 350.913 12.242 17.974 o -11 7 17 14.106 -12.909 10.197 459.605 o -11 7 18 849.892 900.267 20.257 6.445 o -11 7 19 0.440 0.536 12.808 948.792 o -11 7 20 543.457 584.424 18.355 10.200 o -11 7 21 31.695 56.805 13.308 129.811 o -11 7 22 392.605 452.837 19.513 13.762 o -11 7 23 32.498 140.474 17.097 76.156 o -11 7 24 16.017 8.446 16.161 263.934 o -11 8 -10 0.052 -32.609 13.337 940.035 o -11 8 -9 0.501 -0.063 13.183 918.208 o -11 8 -8 2.747 -13.588 12.695 792.572 o -11 8 -7 1435.550 1527.370 27.003 3.656 o -11 8 -6 192.388 197.334 13.201 29.751 o -11 8 -5 1109.930 1350.850 23.785 4.590 o -11 8 -4 214.958 173.339 12.936 28.759 o -11 8 -3 1644.260 1821.900 25.601 3.109 o -11 8 -2 2.388 13.660 10.580 594.090 o -11 8 -1 2425.550 2161.020 24.165 2.184 o -11 8 0 58.104 41.027 9.339 108.388 o -11 8 1 2772.810 2603.460 25.599 1.836 o -11 8 2 16.167 47.020 8.903 205.871 o -11 8 3 2036.480 2173.810 22.784 2.492 o -11 8 4 44.586 54.299 8.604 119.294 o -11 8 5 195.367 286.364 10.088 25.917 o -11 8 6 188.259 133.319 9.090 34.516 o -11 8 7 712.036 823.203 15.496 7.557 o -11 8 8 32.606 138.334 9.401 84.670 o -11 8 9 365.745 378.875 11.204 15.701 o -11 8 10 1022.600 947.330 17.515 5.580 o -11 8 11 4744.710 4924.220 40.045 0.917 o -11 8 12 1812.630 2016.740 22.306 2.794 o -11 8 13 799.828 910.648 17.106 6.717 o -11 8 14 370.916 402.587 12.395 15.188 o -11 8 15 469.938 485.869 14.455 12.094 o -11 8 16 70.192 38.980 11.999 92.638 o -11 8 17 453.028 615.095 19.125 11.203 o -11 8 18 12.032 6.552 14.298 344.099 o -11 8 19 1011.270 932.205 25.038 5.595 o -11 8 20 1.983 -3.181 12.726 845.944 o -11 8 21 211.837 211.798 14.859 27.084 o -11 8 22 58.634 84.742 14.790 79.997 o -11 8 23 67.458 98.900 17.190 67.886 o -11 9 -10 0.626 22.799 15.360 366.167 o -11 9 -9 51.033 53.648 14.847 100.665 o -11 9 -8 0.507 -1.335 13.898 829.921 o -11 9 -7 8.822 18.413 12.098 349.477 o -11 9 -6 360.001 423.032 15.717 15.079 o -11 9 -5 4.182 18.183 12.706 412.265 o -11 9 -4 1185.770 1161.900 24.480 4.637 o -11 9 -3 180.641 185.553 13.301 31.618 o -11 9 -2 739.945 714.074 17.366 7.726 o -11 9 -1 37.383 8.151 10.898 189.047 o -11 9 0 1768.040 1795.320 23.407 2.972 o -11 9 1 64.538 54.841 9.942 92.768 o -11 9 2 1631.110 1805.160 22.140 3.147 o -11 9 3 280.466 330.874 11.355 19.587 o -11 9 4 809.369 781.956 16.396 7.045 o -11 9 5 10.241 53.586 9.242 217.331 o -11 9 6 230.399 327.576 11.196 22.179 o -11 9 7 1.873 62.632 9.837 235.666 o -11 9 8 86.862 213.776 11.043 44.829 o -11 9 9 388.521 562.515 14.122 12.896 o -11 9 10 307.187 324.065 12.726 18.539 o -11 9 11 92.800 124.265 11.023 55.718 o -11 9 12 1977.260 1605.020 23.201 2.838 o -11 9 13 426.248 395.382 13.742 13.870 o -11 9 14 1320.320 1284.410 22.676 4.154 o -11 9 15 129.578 176.725 13.925 39.279 o -11 9 16 1167.920 1072.170 24.563 4.818 o -11 9 17 20.158 -6.072 13.323 304.700 o -11 9 18 791.469 840.479 26.086 6.859 o -11 9 19 195.806 155.518 15.819 31.172 o -11 9 20 354.418 308.384 17.599 16.842 o -11 9 21 22.478 73.917 14.220 128.542 o -11 10 -9 0.841 29.344 16.054 308.088 o -11 10 -8 80.423 78.087 16.220 67.461 o -11 10 -7 174.309 199.441 15.980 31.091 o -11 10 -6 61.501 14.649 13.517 114.866 o -11 10 -5 248.921 258.481 19.846 22.297 o -11 10 -4 21.335 23.694 14.186 205.597 o -11 10 -3 1111.930 1234.730 29.463 4.708 o -11 10 -2 3.194 1.747 12.286 742.535 o -11 10 -1 2162.640 2062.520 29.553 2.418 o -11 10 0 1.204 32.116 12.131 359.536 o -11 10 1 644.513 620.725 17.113 8.921 o -11 10 2 7.285 16.925 12.355 377.822 o -11 10 3 1391.820 1470.600 24.427 3.801 o -11 10 4 59.136 52.446 10.969 98.300 o -11 10 5 150.853 281.856 13.631 29.618 o -11 10 6 477.779 524.354 14.890 11.633 o -11 10 7 10.628 -31.480 11.152 522.748 o -11 10 8 14.624 10.575 10.893 344.269 o -11 10 9 277.427 306.224 13.029 20.191 o -11 10 10 247.079 176.089 13.080 25.902 o -11 10 11 218.887 220.484 14.391 26.221 o -11 10 12 27.189 57.192 11.937 142.469 o -11 10 13 1370.710 1224.520 24.193 4.101 o -11 10 14 35.042 52.855 12.792 128.606 o -11 10 15 1838.190 1687.000 27.956 2.941 o -11 10 16 5.891 27.948 13.967 298.137 o -11 10 17 1329.100 1235.060 28.787 4.158 o -11 10 18 167.127 226.837 16.804 30.245 o -11 10 19 825.644 727.379 21.512 7.055 o -11 10 20 3.762 60.141 14.944 197.348 o -11 11 -7 3.963 -39.257 16.221 499.384 o -11 11 -6 86.588 74.486 14.881 66.388 o -11 11 -5 5.915 0.315 14.292 530.450 o -11 11 -4 701.796 729.238 23.161 7.868 o -11 11 -3 168.916 155.113 14.703 34.708 o -11 11 -2 1074.690 1134.590 25.439 5.004 o -11 11 -1 0.295 15.501 12.962 529.848 o -11 11 0 1404.980 1372.440 26.817 3.861 o -11 11 1 1.400 43.303 13.653 273.597 o -11 11 2 589.094 702.001 19.415 9.024 o -11 11 3 43.158 41.797 13.125 123.240 o -11 11 4 354.474 384.311 16.100 15.750 o -11 11 5 1.809 -4.435 12.937 836.699 o -11 11 6 28.150 55.266 12.897 139.652 o -11 11 7 217.431 238.564 14.300 25.650 o -11 11 8 140.361 153.313 13.320 39.594 o -11 11 9 1229.450 1072.600 22.877 4.650 o -11 11 10 99.025 99.877 13.524 56.676 o -11 11 11 33.420 55.416 13.259 128.037 o -11 11 12 1117.900 1071.230 24.568 4.974 o -11 11 13 57.866 99.411 13.830 76.517 o -11 11 14 1428.660 1302.020 30.050 3.867 o -11 11 15 1.699 47.691 13.543 255.573 o -11 11 16 1032.220 1036.850 26.237 5.308 o -11 11 17 11.838 5.899 14.820 340.240 o -11 12 -4 17.010 37.960 16.579 178.166 o -11 12 -3 344.763 365.617 17.085 16.268 o -11 12 -2 5.369 4.219 14.300 489.778 o -11 12 -1 551.867 544.401 18.559 10.342 o -11 12 0 0.804 16.415 13.696 473.812 o -11 12 1 387.973 414.948 19.012 14.329 o -11 12 2 21.903 24.824 15.023 194.753 o -11 12 3 136.809 154.147 15.949 39.431 o -11 12 4 215.116 246.851 16.210 25.290 o -11 12 5 7.202 64.301 14.771 177.057 o -11 12 6 617.454 648.970 20.329 8.988 o -11 12 7 24.165 56.461 13.889 144.029 o -11 12 8 131.199 121.459 14.290 44.265 o -11 12 9 161.205 146.761 16.066 36.077 o -11 12 10 414.388 421.404 18.688 13.664 o -11 12 11 840.017 794.830 22.840 6.755 o -11 12 12 525.688 439.481 18.702 11.445 o -11 12 13 1133.820 987.698 27.141 5.037 o -11 12 14 50.359 80.051 15.600 87.230 o -11 13 2 632.508 612.490 21.753 8.991 o -11 13 3 7.605 29.099 15.021 263.912 o -11 13 4 81.589 63.067 15.288 71.733 o -11 13 5 28.787 19.946 14.968 178.025 o -11 13 6 9.550 21.379 14.870 281.649 o -11 13 7 121.347 131.930 15.460 44.884 o -11 13 8 148.314 145.953 16.401 38.048 o -11 13 9 214.975 238.700 17.296 25.460 o -10 0 -8 2718.650 2856.990 63.351 1.736 o -10 0 -6 1513.110 1862.840 41.730 3.196 o -10 0 -4 1005.710 960.342 48.762 5.257 o -10 0 -2 20987.400 20341.800 213.546 0.111 o -10 0 0 1820.690 1492.380 23.789 3.098 o -10 0 2 1922.480 1725.560 23.832 2.830 o -10 0 4 13886.100 15506.200 151.353 0.196 o -10 0 6 34511.400 33405.500 321.875 0.048 o -10 0 8 60575.000 63497.000 587.877 0.017 o -10 0 10 15741.200 13314.200 126.910 0.188 o -10 0 12 335.580 217.101 10.118 19.727 o -10 0 14 8054.770 7558.010 78.116 0.474 o -10 0 16 894.850 865.851 17.591 6.328 o -10 0 18 0.027 -25.235 10.130 1630.190 o -10 0 20 373.211 376.730 16.357 15.319 o -10 0 22 1518.270 1232.950 34.963 3.734 o -10 0 24 43.528 93.288 28.184 67.945 o -10 0 26 428.478 428.475 27.119 12.895 o -10 1 -9 1461.340 1486.960 33.143 3.617 o -10 1 -8 153.684 177.153 17.229 34.704 o -10 1 -7 758.654 710.131 19.692 7.576 o -10 1 -6 2420.190 2530.860 33.435 2.049 o -10 1 -5 10717.600 10343.200 100.437 0.312 o -10 1 -4 9.698 2.983 6.961 656.419 o -10 1 -3 1758.660 1662.980 17.772 3.081 o -10 1 -2 385.631 383.614 13.948 14.993 o -10 1 -1 0.002 86.326 6.359 199.487 o -10 1 0 927.016 1112.560 14.402 5.651 o -10 1 1 62.205 166.659 6.549 60.874 o -10 1 2 131.628 159.939 5.987 42.011 o -10 1 3 8086.680 7068.560 50.477 0.490 o -10 1 4 1168.080 1161.310 12.722 4.746 o -10 1 5 21277.100 20100.200 135.591 0.112 o -10 1 6 59.236 107.948 5.874 78.337 o -10 1 7 16606.600 17331.700 115.575 0.157 o -10 1 8 1310.110 1212.050 14.281 4.296 o -10 1 9 4377.560 5091.370 37.496 0.966 o -10 1 10 53.182 239.716 6.970 51.167 o -10 1 11 5549.360 4609.180 33.591 0.825 o -10 1 12 1056.560 1190.030 13.963 5.041 o -10 1 13 31385.000 30164.500 203.063 0.058 o -10 1 14 881.936 1197.620 14.181 5.662 o -10 1 15 82.873 68.820 6.705 75.290 o -10 1 16 0.076 138.364 7.494 124.979 o -10 1 17 125.904 144.003 7.789 44.623 o -10 1 18 278.661 277.622 9.349 21.037 o -10 1 19 566.725 469.710 11.619 10.780 o -10 1 20 31.121 -7.932 8.123 261.013 o -10 1 21 236.387 268.025 12.258 23.523 o -10 1 22 51.857 43.419 12.135 110.844 o -10 1 23 220.629 193.991 14.594 27.128 o -10 1 24 32.845 39.386 14.415 141.899 o -10 1 25 426.074 421.577 18.917 13.401 o -10 1 26 12.021 -12.794 15.010 374.918 o -10 1 27 251.331 247.087 18.901 22.596 o -10 2 -9 4.680 -8.041 12.304 705.726 o -10 2 -8 4207.900 4455.140 53.045 1.048 o -10 2 -7 331.679 403.309 23.452 15.705 o -10 2 -6 1327.640 1163.100 17.382 4.302 o -10 2 -5 197.515 263.308 12.271 26.451 o -10 2 -4 29.414 -4.151 6.512 285.548 o -10 2 -3 3496.200 3084.550 34.200 1.424 o -10 2 -2 3856.520 3279.420 29.899 1.286 o -10 2 -1 972.618 901.655 12.698 5.912 o -10 2 0 636.364 388.973 8.454 10.429 o -10 2 1 700.533 680.842 12.127 8.219 o -10 2 2 1292.650 1241.090 13.143 4.306 o -10 2 3 1268.880 1371.410 14.505 4.204 o -10 2 4 9513.960 9514.530 69.628 0.367 o -10 2 5 84.030 133.450 5.892 58.951 o -10 2 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18.371 4.469 o -10 3 -6 1207.690 1108.180 32.369 4.594 o -10 3 -5 4336.690 4077.370 42.957 1.066 o -10 3 -4 271.343 226.996 8.358 22.890 o -10 3 -3 6.617 79.794 8.300 180.072 o -10 3 -2 62.370 91.136 7.991 80.959 o -10 3 -1 26.199 13.993 7.177 251.591 o -10 3 0 288.697 342.688 9.740 19.054 o -10 3 1 1546.850 1921.900 18.103 3.193 o -10 3 2 4986.970 4834.870 37.077 0.888 o -10 3 3 7966.740 7324.960 53.650 0.489 o -10 3 4 1555.810 1597.750 15.347 3.429 o -10 3 5 652.951 627.442 10.711 8.892 o -10 3 6 1167.500 1282.690 13.973 4.572 o -10 3 7 8576.210 8937.030 61.558 0.417 o -10 3 8 428.657 725.038 11.275 10.931 o -10 3 9 8263.760 7556.060 57.066 0.466 o -10 3 10 1359.800 905.776 12.485 4.567 o -10 3 11 8512.170 9027.980 62.861 0.418 o -10 3 12 0.680 75.895 6.776 220.126 o -10 3 13 21879.300 20179.900 137.488 0.108 o -10 3 14 405.565 634.489 11.846 11.983 o -10 3 15 499.482 578.863 11.652 10.957 o -10 3 16 92.706 109.812 7.989 59.579 o -10 3 17 3.806 -14.325 7.477 1328.860 o -10 3 18 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o -10 4 6 8134.940 8219.380 59.403 0.455 o -10 4 7 534.360 1018.480 12.621 8.192 o -10 4 8 5080.380 4852.210 35.288 0.873 o -10 4 9 247.715 160.589 6.819 26.987 o -10 4 10 17634.700 17515.000 115.768 0.147 o -10 4 11 3531.300 4056.660 30.314 1.268 o -10 4 12 11043.500 10476.600 72.424 0.304 o -10 4 13 1823.180 2076.430 20.896 2.753 o -10 4 14 1225.630 1247.280 16.109 4.457 o -10 4 15 4.967 90.770 8.018 168.028 o -10 4 16 1942.010 1934.410 20.281 2.703 o -10 4 17 135.632 153.176 8.923 41.435 o -10 4 18 3.335 11.202 8.522 705.093 o -10 4 19 379.563 483.096 13.614 13.938 o -10 4 20 154.338 127.491 10.786 39.979 o -10 4 21 216.402 148.407 12.047 29.951 o -10 4 22 53.491 49.681 12.844 103.555 o -10 4 23 52.130 -18.715 12.499 149.358 o -10 4 24 90.495 71.889 15.043 65.006 o -10 4 25 74.359 33.350 14.897 87.652 o -10 4 26 424.357 417.521 21.232 13.381 o -10 5 -9 927.358 1077.500 21.307 5.673 o -10 5 -8 254.716 280.512 12.085 22.075 o -10 5 -7 860.604 841.466 21.821 6.527 o -10 5 -6 2566.950 2365.070 28.078 2.018 o -10 5 -5 1294.670 1324.610 19.252 4.181 o -10 5 -4 11.909 60.093 8.254 198.267 o -10 5 -3 1866.730 2007.780 22.046 2.741 o -10 5 -2 167.793 389.005 10.830 24.161 o -10 5 -1 9.781 27.321 7.079 346.338 o -10 5 0 1755.580 1433.260 16.540 3.247 o -10 5 1 465.622 514.358 10.400 12.011 o -10 5 2 195.604 98.218 6.673 36.243 o -10 5 3 2452.840 1987.180 18.502 2.234 o -10 5 4 538.426 809.682 12.118 9.105 o -10 5 5 6544.730 7054.280 50.016 0.594 o -10 5 6 38.987 100.221 6.387 98.854 o -10 5 7 7726.280 7604.210 53.866 0.495 o -10 5 8 2203.240 2167.720 19.372 2.357 o -10 5 9 4807.210 4676.150 34.304 0.929 o -10 5 10 494.393 629.680 11.498 10.676 o -10 5 11 6840.840 7029.100 51.339 0.572 o -10 5 12 682.650 910.198 13.699 7.476 o -10 5 13 3070.970 3051.420 26.004 1.594 o -10 5 14 1333.250 1372.440 16.820 4.050 o -10 5 15 108.154 144.308 9.093 48.632 o -10 5 16 0.240 47.145 8.949 321.887 o -10 5 17 165.405 209.595 10.305 32.423 o -10 5 18 387.838 555.504 15.875 12.926 o -10 5 19 5.648 37.942 9.749 304.436 o -10 5 20 62.912 172.609 11.382 57.620 o -10 5 21 239.328 287.263 14.585 22.563 o -10 5 22 27.980 37.114 12.920 162.893 o -10 5 23 913.836 925.179 31.952 5.940 o -10 5 24 54.776 52.348 17.774 92.201 o -10 5 25 551.035 625.515 24.431 9.713 o -10 5 26 6.036 20.437 15.818 304.589 o -10 6 -9 10.088 -27.438 11.358 531.673 o -10 6 -8 1450.970 1600.240 24.299 3.575 o -10 6 -7 125.394 189.963 10.908 39.546 o -10 6 -6 818.010 735.203 16.860 7.132 o -10 6 -5 342.988 341.711 12.229 16.941 o -10 6 -4 1064.930 1067.170 18.441 5.197 o -10 6 -3 814.340 928.315 16.222 6.596 o -10 6 -2 829.729 890.344 15.729 6.620 o -10 6 -1 563.132 516.095 11.417 10.518 o -10 6 0 215.033 97.852 7.833 33.480 o -10 6 1 739.312 803.068 13.265 7.459 o -10 6 2 1928.640 2263.930 21.215 2.552 o -10 6 3 192.220 232.803 7.565 28.643 o -10 6 4 1445.260 1078.090 14.142 4.136 o -10 6 5 1746.210 1496.780 16.161 3.216 o -10 6 6 4275.690 4472.260 33.655 1.044 o -10 6 7 2603.550 2960.350 24.536 1.832 o -10 6 8 4433.440 4424.530 35.261 1.017 o -10 6 9 3782.230 3411.710 29.084 1.288 o -10 6 10 7464.190 7903.680 56.528 0.501 o -10 6 11 5084.490 5304.690 40.198 0.839 o -10 6 12 2961.250 2774.890 24.440 1.703 o -10 6 13 225.767 293.697 9.302 23.593 o -10 6 14 719.260 713.866 14.369 7.916 o -10 6 15 660.203 709.471 15.050 8.405 o -10 6 16 2177.510 2254.460 24.630 2.335 o -10 6 17 160.288 286.250 11.159 28.801 o -10 6 18 39.706 31.068 10.298 148.327 o -10 6 19 8.682 90.830 11.133 148.775 o -10 6 20 117.383 103.945 12.197 50.694 o -10 6 21 0.472 19.264 13.122 467.411 o -10 6 22 637.894 583.825 21.020 9.094 o -10 6 23 55.236 129.752 14.689 68.427 o -10 6 24 1169.750 1100.110 30.717 4.726 o -10 6 25 0.002 -4.197 16.773 597.509 o -10 7 -9 139.045 134.989 12.984 41.626 o -10 7 -8 39.542 37.580 11.565 137.937 o -10 7 -7 2121.910 2024.880 30.638 2.467 o -10 7 -6 509.878 435.472 13.918 11.857 o -10 7 -5 1283.600 1117.170 18.789 4.464 o -10 7 -4 3.547 44.660 9.757 291.986 o -10 7 -3 1440.230 1479.540 20.672 3.715 o -10 7 -2 6.104 65.021 9.299 209.085 o -10 7 -1 36.176 146.292 9.409 79.031 o -10 7 0 2808.250 2928.320 26.686 1.736 o -10 7 1 163.585 169.415 8.479 35.513 o -10 7 2 1738.090 1623.860 17.773 3.135 o -10 7 3 150.694 224.581 8.595 33.520 o -10 7 4 572.715 665.965 12.628 9.490 o -10 7 5 9422.820 9678.850 66.990 0.368 o -10 7 6 1443.220 1542.960 18.798 3.658 o -10 7 7 8551.980 8567.650 60.170 0.427 o -10 7 8 4906.590 4792.390 37.893 0.903 o -10 7 9 8822.380 8914.470 64.717 0.407 o -10 7 10 551.923 627.560 12.731 9.941 o -10 7 11 4589.500 4392.010 36.142 0.991 o -10 7 12 421.130 447.092 11.184 13.486 o -10 7 13 1494.560 1740.530 20.056 3.401 o -10 7 14 43.831 66.892 8.857 110.804 o -10 7 15 1567.790 1306.230 18.098 3.648 o -10 7 16 54.524 79.632 9.971 90.512 o -10 7 17 34.658 41.529 10.618 147.017 o -10 7 18 79.447 21.596 11.279 92.958 o -10 7 19 0.250 -38.495 12.064 1119.380 o -10 7 20 5.177 13.530 12.516 444.430 o -10 7 21 375.994 297.340 18.000 16.307 o -10 7 22 14.526 33.114 14.883 210.428 o -10 7 23 874.344 813.599 25.519 6.483 o -10 7 24 42.165 45.887 16.450 113.430 o -10 8 -9 67.981 35.738 12.788 95.379 o -10 8 -8 613.693 541.276 17.223 9.650 o -10 8 -7 356.586 267.352 14.217 17.664 o -10 8 -6 878.333 891.577 19.924 6.326 o -10 8 -5 1214.570 1218.310 21.549 4.499 o -10 8 -4 944.370 959.529 19.928 5.861 o -10 8 -3 341.369 364.590 12.765 16.598 o -10 8 -2 623.393 560.144 13.851 9.496 o -10 8 -1 808.000 794.690 15.806 7.020 o -10 8 0 106.708 97.800 9.220 56.161 o -10 8 1 1281.440 1050.590 16.539 4.568 o -10 8 2 1191.630 1323.280 18.234 4.438 o -10 8 3 3052.780 3150.210 28.740 1.579 o -10 8 4 1228.440 1147.410 16.930 4.579 o -10 8 5 1526.950 1297.510 18.451 3.730 o -10 8 6 4340.560 4142.020 35.312 1.063 o -10 8 7 0.703 178.527 9.601 95.073 o -10 8 8 11910.500 11903.900 91.402 0.265 o -10 8 9 1435.130 1592.480 22.718 3.615 o -10 8 10 6450.280 6528.640 50.544 0.623 o -10 8 11 1078.040 1179.660 17.535 4.972 o -10 8 12 2167.150 2031.040 21.875 2.441 o -10 8 13 116.896 101.340 9.338 52.193 o -10 8 14 448.794 572.812 13.655 11.738 o -10 8 15 0.090 -2.659 10.465 1511.850 o -10 8 16 512.120 540.074 15.868 10.971 o -10 8 17 167.662 146.717 13.399 35.743 o -10 8 18 9.682 -9.744 12.715 492.521 o -10 8 19 30.372 68.695 13.027 122.360 o -10 8 20 230.104 158.467 14.345 27.873 o -10 8 21 7.216 -1.055 12.630 572.989 o -10 8 22 298.053 261.845 17.006 19.977 o -10 8 23 133.548 134.197 16.710 41.635 o -10 9 -9 453.424 484.406 17.126 12.323 o -10 9 -8 58.508 40.683 13.417 102.001 o -10 9 -7 518.819 446.451 15.378 11.588 o -10 9 -6 134.488 111.594 13.267 44.966 o -10 9 -5 803.523 762.257 21.253 7.087 o -10 9 -4 769.299 777.445 19.798 7.275 o -10 9 -3 247.022 159.437 12.661 26.605 o -10 9 -2 436.770 439.894 13.739 13.167 o -10 9 -1 208.496 217.943 11.297 27.520 o -10 9 0 2064.420 1882.800 23.628 2.600 o -10 9 1 152.814 146.504 9.737 38.782 o -10 9 2 1605.060 1505.940 19.219 3.414 o -10 9 3 1631.770 1661.020 19.931 3.254 o -10 9 4 754.912 632.760 13.182 7.966 o -10 9 5 2765.930 2554.960 25.360 1.853 o -10 9 6 795.721 881.475 16.232 6.831 o -10 9 7 5323.140 5298.700 42.407 0.807 o -10 9 8 38.284 152.004 9.726 75.512 o -10 9 9 4176.960 3974.210 36.718 1.115 o -10 9 10 13.403 56.184 10.323 191.525 o -10 9 11 257.077 334.168 12.418 20.533 o -10 9 12 14.862 28.043 10.197 262.491 o -10 9 13 606.735 681.855 16.290 9.004 o -10 9 14 299.853 333.765 14.070 18.564 o -10 9 15 625.626 679.531 17.945 8.807 o -10 9 16 14.985 34.071 13.997 212.603 o -10 9 17 127.815 146.522 14.969 42.126 o -10 9 18 124.975 168.145 15.204 40.522 o -10 9 19 13.227 -2.728 13.866 384.023 o -10 9 20 1.277 10.939 13.473 548.126 o -10 9 21 276.490 207.265 17.384 22.458 o -10 9 22 78.956 85.275 18.158 64.695 o -10 10 -9 6.575 8.592 15.236 387.459 o -10 10 -8 410.942 362.622 15.414 14.560 o -10 10 -7 0.564 -28.997 12.535 1003.100 o -10 10 -6 351.180 294.028 16.219 17.274 o -10 10 -5 27.827 14.672 14.297 196.002 o -10 10 -4 1134.060 1135.400 26.416 4.812 o -10 10 -3 265.496 263.792 13.789 21.815 o -10 10 -2 32.258 48.626 12.121 140.202 o -10 10 -1 604.009 578.546 16.028 9.573 o -10 10 0 77.528 156.394 12.430 54.847 o -10 10 1 235.421 227.103 12.887 24.902 o -10 10 2 792.658 777.742 18.702 7.137 o -10 10 3 1442.060 1275.420 21.204 3.908 o -10 10 4 2037.920 2118.040 26.832 2.508 o -10 10 5 2069.470 2214.410 27.156 2.437 o -10 10 6 1107.140 1128.010 21.069 4.942 o -10 10 7 457.779 372.983 14.306 13.409 o -10 10 8 1161.460 1016.080 20.832 4.948 o -10 10 9 18.236 18.413 10.799 268.428 o -10 10 10 414.684 550.609 16.026 12.458 o -10 10 11 0.837 -10.474 11.560 1127.100 o -10 10 12 392.762 477.352 16.822 13.598 o -10 10 13 0.776 23.653 12.199 439.259 o -10 10 14 61.123 103.192 13.436 73.641 o -10 10 15 49.338 62.942 12.723 100.868 o -10 10 16 60.616 83.430 14.132 79.776 o -10 10 17 0.265 107.422 14.691 137.841 o -10 10 18 1.323 49.908 15.192 233.881 o -10 10 19 0.459 48.477 14.611 250.131 o -10 10 20 284.840 260.452 16.636 20.668 o -10 11 -8 182.113 133.564 16.857 33.910 o -10 11 -7 157.482 93.920 16.076 41.115 o -10 11 -6 29.118 27.607 15.213 163.344 o -10 11 -5 314.626 314.307 18.319 18.094 o -10 11 -4 173.307 168.457 18.720 32.403 o -10 11 -3 144.690 173.773 14.736 36.853 o -10 11 -2 181.463 228.344 14.612 29.099 o -10 11 -1 0.951 43.454 13.514 278.467 o -10 11 0 783.225 646.847 18.947 7.636 o -10 11 1 127.798 132.293 15.001 43.588 o -10 11 2 1775.860 1617.290 28.031 3.062 o -10 11 3 523.800 636.313 18.860 10.111 o -10 11 4 664.937 565.861 18.411 8.966 o -10 11 5 1582.920 1537.670 26.521 3.401 o -10 11 6 1918.780 1791.440 25.775 2.793 o -10 11 7 1612.380 1662.740 26.828 3.260 o -10 11 8 52.304 90.535 13.476 84.055 o -10 11 9 1020.190 1121.480 23.695 5.222 o -10 11 10 29.100 39.094 12.344 159.077 o -10 11 11 1008.830 937.784 22.237 5.619 o -10 11 12 103.185 89.516 13.456 57.081 o -10 11 13 465.767 579.431 18.600 11.294 o -10 11 14 1.325 33.008 13.371 329.789 o -10 11 15 66.254 82.664 13.994 76.348 o -10 11 16 29.960 92.593 15.959 100.402 o -10 11 17 1.628 16.946 16.011 378.793 o -10 11 18 7.559 69.874 15.236 164.498 o -10 12 -5 80.198 70.904 17.163 68.566 o -10 12 -4 239.612 192.884 16.284 25.463 o -10 12 -3 323.767 315.816 16.877 17.822 o -10 12 -2 122.415 158.054 15.294 41.949 o -10 12 -1 478.998 382.715 17.040 12.795 o -10 12 0 3.698 18.689 13.582 394.132 o -10 12 1 332.175 252.787 16.923 18.709 o -10 12 2 194.666 212.377 15.832 28.425 o -10 12 3 1014.800 843.338 22.977 5.782 o -10 12 4 727.494 719.455 20.252 7.759 o -10 12 5 810.526 689.984 21.045 7.275 o -10 12 6 758.403 796.428 20.887 7.270 o -10 12 7 183.731 200.567 14.904 30.213 o -10 12 8 998.715 947.878 23.778 5.626 o -10 12 9 253.067 256.985 15.246 22.585 o -10 12 10 1744.560 1654.440 30.471 3.071 o -10 12 11 99.981 91.698 14.807 57.112 o -10 12 12 1124.750 1171.140 27.327 4.780 o -10 12 13 60.262 125.372 14.774 66.910 o -10 12 14 515.289 529.588 18.691 10.931 o -10 12 15 10.134 43.869 14.124 211.405 o -10 13 -1 2.856 32.897 16.464 267.085 o 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639.920 11.259 8.363 o -5 5 0 7414.100 7055.510 50.143 0.532 o -5 5 1 129.603 82.388 6.130 52.011 o -5 5 2 13507.900 15338.400 104.405 0.205 o -5 5 3 0.270 73.364 5.940 232.878 o -5 5 4 1122.530 887.676 13.036 5.339 o -5 5 5 481.330 500.407 9.643 11.876 o -5 5 6 6103.440 7759.910 53.871 0.600 o -5 5 7 611.983 561.453 10.196 9.663 o -5 5 8 10071.700 8691.970 58.390 0.363 o -5 5 9 128.678 198.311 7.419 38.838 o -5 5 10 1023.650 1262.790 15.654 5.022 o -5 5 11 177.711 312.928 9.037 26.339 o -5 5 12 272.453 234.764 8.360 22.594 o -5 5 13 2619.170 2758.620 25.290 1.877 o -5 5 14 542.994 596.580 13.435 10.227 o -5 5 15 174.119 718.700 30.421 15.169 o -5 5 16 110.445 196.103 9.701 42.015 o -5 5 17 184.275 372.308 11.755 23.561 o -5 5 18 1343.140 1452.450 29.299 3.892 o -5 5 19 304.146 329.673 13.673 18.498 o -5 5 20 2123.590 2220.660 39.220 2.362 o -5 5 21 247.988 247.536 18.870 22.784 o -5 5 22 483.909 483.429 19.023 11.751 o -5 5 23 120.347 84.906 15.703 51.091 o -5 5 24 205.695 258.661 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37.229 23.291 11.006 163.247 o 1 5 17 108.367 204.793 13.077 40.794 o 1 5 18 75.927 51.190 13.997 80.501 o 1 5 19 0.068 10.288 15.359 505.437 o 1 5 20 22.779 -12.759 17.576 229.693 o 1 5 21 8.685 11.026 16.864 306.825 o 1 5 22 69.359 99.337 19.032 65.088 o 1 6 1 355.932 541.683 10.612 13.893 o 1 6 2 174.691 393.307 8.502 23.721 o 1 6 3 2155.510 1832.960 17.429 2.547 o 1 6 4 3183.020 3113.370 24.717 1.538 o 1 6 5 3.887 52.269 6.006 283.154 o 1 6 6 6016.920 6221.910 44.543 0.677 o 1 6 7 6815.080 7074.770 49.309 0.573 o 1 6 8 42.393 47.840 6.817 131.295 o 1 6 9 3226.860 2835.590 25.261 1.575 o 1 6 10 1895.810 1548.190 18.783 2.978 o 1 6 11 1107.180 1105.660 20.918 4.978 o 1 6 12 986.114 855.633 19.279 5.910 o 1 6 13 3086.150 2708.780 37.020 1.649 o 1 6 14 263.215 265.315 13.379 21.930 o 1 6 15 623.182 673.036 19.877 8.827 o 1 6 16 0.218 -1.329 12.380 1068.720 o 1 6 17 390.667 397.826 16.072 14.600 o 1 6 18 18.885 30.661 13.794 203.536 o 1 6 19 12.626 -4.890 13.579 401.490 o 1 6 20 116.189 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12.267 8.900 o 1 9 10 2059.980 2287.420 27.558 2.413 o 1 9 11 88.565 106.188 12.042 60.237 o 1 9 12 740.022 681.069 18.350 7.835 o 1 9 13 6.461 1.789 13.287 537.064 o 1 9 14 991.051 955.556 23.185 5.646 o 1 9 15 139.761 215.323 14.114 34.701 o 1 9 16 279.041 352.623 19.033 18.681 o 1 9 17 13.959 56.388 15.900 162.227 o 1 9 18 44.505 9.673 16.804 140.124 o 1 10 1 46.712 110.964 9.389 84.344 o 1 10 2 1849.380 1834.770 21.168 2.857 o 1 10 3 1253.530 1456.490 19.728 4.123 o 1 10 4 2317.370 2290.840 30.397 2.205 o 1 10 5 1452.340 1422.650 23.636 3.735 o 1 10 6 187.265 276.051 11.326 26.859 o 1 10 7 3137.210 2997.770 33.579 1.571 o 1 10 8 118.249 75.450 10.899 55.408 o 1 10 9 2222.050 2220.540 27.564 2.308 o 1 10 10 335.070 393.868 14.001 16.283 o 1 10 11 1264.380 1211.620 28.215 4.342 o 1 10 12 0.039 -24.767 13.813 877.753 o 1 10 13 501.677 575.975 18.783 10.794 o 1 10 14 46.923 -8.336 13.238 160.482 o 1 10 15 184.582 174.222 15.346 31.466 o 1 10 16 29.438 55.169 17.160 124.062 o 1 10 17 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o 8 6 14 115.316 136.378 18.355 44.575 o 8 6 15 0.997 51.118 17.078 214.201 o 8 6 16 16.267 42.696 17.328 168.242 o 8 6 17 11.007 -11.328 19.637 285.005 o 8 7 8 30.855 27.520 10.388 179.376 o 8 7 9 2522.480 2599.090 34.093 1.965 o 8 7 10 2.105 -2.050 11.359 1000.240 o 8 7 11 589.934 545.729 16.227 9.916 o 8 7 12 8.453 -15.142 12.333 544.138 o 8 7 13 105.831 80.921 13.010 57.925 o 8 7 14 15.920 -1.152 16.150 302.188 o 8 7 15 23.174 59.836 21.718 115.225 o 8 7 16 3.831 -8.267 21.107 325.429 o 8 8 8 2657.070 2666.640 30.404 1.875 o 8 8 9 114.470 202.079 14.192 39.636 o 8 8 10 1236.220 1221.040 23.835 4.427 o 8 8 11 71.613 36.366 13.137 91.095 o 8 8 12 689.513 652.457 21.192 8.305 o 8 8 13 0.890 -26.231 14.882 706.443 o 8 8 14 27.469 53.481 15.351 135.160 o 8 8 15 6.555 1.802 14.921 465.686 o 8 9 8 164.628 158.004 13.181 35.413 o 8 9 9 1862.860 1763.580 27.532 2.868 o 8 9 10 8.240 19.428 13.699 322.703 o 8 9 11 521.828 549.660 17.358 10.733 o 8 9 12 3.121 31.135 13.450 318.481 o 8 9 13 239.364 226.007 19.996 23.846 o 8 9 14 0.091 51.089 18.395 206.416 o 8 10 8 309.388 296.508 15.533 18.841 o 8 10 9 4.507 -8.851 12.353 711.667 o 8 10 10 358.420 376.515 16.053 15.751 o 8 10 11 219.832 211.104 16.154 26.294 o 8 10 12 296.242 342.270 18.010 18.284 o 8 11 8 7.248 -2.570 13.509 530.387 o 8 11 9 478.044 494.938 23.890 11.584 o 8 11 10 46.906 60.034 14.641 102.102 o 9 0 9 158.592 73.961 22.820 40.186 o 9 0 11 0.501 -49.550 19.997 410.862 o 9 0 13 171.526 214.284 23.820 28.947 o 9 0 15 60.051 -2.393 22.323 104.069 o 9 0 17 110.593 109.144 42.427 34.389 o 9 0 19 264.407 279.332 33.930 19.111 o 9 1 9 40.623 150.969 18.237 67.286 o 9 1 10 137.330 126.353 14.584 42.361 o 9 1 11 20.298 35.243 14.189 185.569 o 9 1 12 421.562 401.652 20.422 13.647 o 9 1 13 29.760 26.712 15.374 162.001 o 9 1 14 163.777 138.382 17.724 35.882 o 9 1 15 65.369 4.340 16.950 108.871 o 9 1 16 160.670 153.463 21.123 34.300 o 9 1 17 29.027 -26.565 21.378 168.759 o 9 1 18 121.281 115.338 22.255 43.735 o 9 1 19 60.164 50.323 22.854 79.616 o 9 2 9 239.012 235.459 14.606 24.198 o 9 2 10 31.894 96.259 13.695 100.206 o 9 2 11 53.263 59.064 15.371 94.542 o 9 2 12 2.565 -0.897 17.214 488.835 o 9 2 13 259.876 204.980 19.136 23.322 o 9 2 14 80.641 58.607 17.391 71.454 o 9 2 15 359.819 349.685 26.934 15.415 o 9 2 16 2.016 -48.604 18.430 445.825 o 9 2 17 151.378 140.353 23.744 35.630 o 9 2 18 10.440 -41.263 21.707 252.822 o 9 3 9 347.664 312.812 12.230 17.272 o 9 3 10 2.102 3.325 12.504 743.191 o 9 3 11 17.834 -1.633 12.227 349.827 o 9 3 12 265.701 263.194 20.370 21.201 o 9 3 13 2.524 34.593 17.401 250.629 o 9 3 14 240.539 210.929 22.341 23.924 o 9 3 15 0.117 -13.185 18.145 507.259 o 9 3 16 135.543 80.874 25.566 42.602 o 9 3 17 8.543 -34.424 26.193 199.047 o 9 3 18 92.488 14.919 26.462 65.588 o 9 4 9 7.005 -10.082 9.814 742.912 o 9 4 10 25.547 2.827 12.715 253.803 o 9 4 11 46.226 50.282 14.070 110.144 o 9 4 12 72.668 69.480 13.514 76.926 o 9 4 13 150.074 128.836 14.921 39.619 o 9 4 14 0.741 -31.367 16.753 570.998 o 9 4 15 125.059 91.288 18.307 47.650 o 9 4 16 79.644 75.989 23.876 60.807 o 9 4 17 297.199 358.488 33.397 16.544 o 9 4 18 17.924 20.596 43.993 68.350 o 9 5 9 270.279 266.807 14.014 21.459 o 9 5 10 26.308 -11.170 10.174 283.945 o 9 5 11 50.216 27.154 12.705 124.683 o 9 5 12 74.199 25.337 15.323 90.731 o 9 5 13 0.845 -67.091 14.960 701.996 o 9 5 14 135.454 97.426 15.270 45.680 o 9 5 15 5.697 13.972 16.104 339.819 o 9 5 16 179.064 121.075 18.477 34.746 o 9 5 17 0.675 -8.426 18.096 494.453 o 9 6 9 6.661 -42.532 10.325 730.314 o 9 6 10 0.134 -76.068 10.706 1435.580 o 9 6 11 124.430 47.876 12.214 57.548 o 9 6 12 8.713 -36.965 13.935 472.406 o 9 6 13 46.208 -30.196 15.100 154.659 o 9 6 14 7.766 -21.482 18.071 357.195 o 9 6 15 49.906 1.038 17.367 135.664 o 9 6 16 0.619 18.463 22.823 238.904 o 9 7 9 3.728 42.154 11.402 284.634 o 9 7 10 48.879 -2.054 11.639 160.993 o 9 7 11 45.449 33.359 12.313 128.579 o 9 7 12 0.312 -37.834 11.582 1201.380 o 9 7 13 53.023 20.108 13.617 123.704 o 9 7 14 56.910 6.132 16.649 120.694 o 9 7 15 1.350 13.768 19.668 311.550 o 9 8 9 125.393 91.838 14.326 49.305 o 9 8 10 16.133 32.893 13.074 216.599 o 9 8 11 51.292 40.296 13.485 111.219 o 9 8 12 109.059 76.948 15.026 56.373 o 9 8 13 12.571 -18.389 13.464 405.509 o 9 8 14 23.913 24.269 13.638 196.446 o 9 9 9 15.428 15.615 13.232 277.175 o 9 9 10 266.050 233.213 14.529 22.585 o 9 9 11 8.458 45.772 13.959 216.341 o 9 9 12 81.288 60.978 15.867 71.954 o 9 9 13 0.675 18.298 17.648 340.464 o 9 10 9 0.094 -14.360 13.484 915.858 o 9 10 10 8.410 46.132 15.314 205.210 o 9 10 11 53.351 79.676 15.331 85.275 o 9 11 9 1.891 22.682 13.945 382.040 o 10 0 10 517.771 565.314 31.609 10.228 o 10 0 12 110.758 151.418 23.618 41.526 o 10 0 14 18.587 -0.319 22.226 200.365 o 10 0 16 28.591 28.671 29.941 99.220 o 10 0 18 8.315 -49.432 33.793 129.690 o 10 1 10 5.744 19.283 14.655 335.994 o 10 1 11 285.505 336.893 19.346 18.712 o 10 1 12 64.414 18.723 16.243 102.685 o 10 1 13 137.400 156.967 17.418 38.643 o 10 1 14 104.832 111.525 17.764 50.668 o 10 1 15 83.064 73.508 18.999 64.747 o 10 1 16 8.499 0.408 20.827 282.429 o 10 1 17 0.013 -54.435 22.030 346.216 o 10 1 18 63.899 4.911 23.033 95.235 o 10 2 10 894.791 925.158 31.423 6.033 o 10 2 11 25.220 -21.582 16.799 223.981 o 10 2 12 418.063 412.508 26.513 13.298 o 10 2 13 46.945 6.451 22.045 118.488 o 10 2 14 204.411 268.560 19.851 24.789 o 10 2 15 1.590 -29.739 22.638 310.181 o 10 2 16 74.910 13.686 20.836 85.922 o 10 2 17 12.686 -73.876 18.939 282.966 o 10 2 18 30.120 -26.247 24.550 144.652 o 10 3 10 15.209 -10.501 12.018 393.961 o 10 3 11 652.159 807.234 24.993 7.916 o 10 3 12 48.727 13.471 15.343 132.697 o 10 3 13 510.639 533.113 23.553 10.827 o 10 3 14 16.680 38.131 21.523 149.114 o 10 3 15 32.388 -14.416 19.604 170.503 o 10 3 16 0.007 -42.951 19.629 436.178 o 10 3 17 1.466 -34.086 22.847 306.112 o 10 4 10 920.750 801.965 21.409 6.323 o 10 4 11 21.891 -20.018 14.280 275.431 o 10 4 12 319.720 296.870 18.173 18.242 o 10 4 13 82.868 11.428 17.899 85.313 o 10 4 14 61.842 67.034 17.590 80.575 o 10 4 15 7.206 11.528 21.038 246.030 o 10 4 16 54.940 64.863 31.111 64.772 o 10 4 17 10.801 3.496 28.488 160.952 o 10 5 10 0.146 -52.662 10.768 1416.780 o 10 5 11 460.353 500.708 18.569 12.014 o 10 5 12 1.625 -26.339 21.353 345.851 o 10 5 13 175.874 127.790 19.488 34.450 o 10 5 14 4.088 -54.125 16.806 469.189 o 10 5 15 1.664 -62.623 18.265 461.216 o 10 5 16 9.560 -44.861 19.588 299.612 o 10 6 10 378.840 361.154 15.393 15.421 o 10 6 11 1.285 -49.791 13.167 852.437 o 10 6 12 104.551 87.424 15.328 55.943 o 10 6 13 10.106 -38.734 18.943 307.692 o 10 6 14 56.526 4.025 16.417 123.759 o 10 6 15 3.847 -51.879 18.515 405.907 o 10 7 10 2.401 -56.565 11.796 915.265 o 10 7 11 313.491 317.713 14.144 18.339 o 10 7 12 0.664 -31.676 13.870 821.289 o 10 7 13 94.790 95.438 14.446 58.565 o 10 7 14 1.234 -44.426 19.401 421.040 o 10 8 10 473.153 458.672 17.786 12.181 o 10 8 11 186.406 169.089 14.900 31.629 o 10 8 12 19.154 -3.364 13.540 311.941 o 10 8 13 0.649 -20.014 12.931 937.804 o 10 9 10 42.608 66.212 15.950 101.033 o 10 9 11 364.490 344.866 17.387 15.970 o 10 9 12 2.273 12.454 14.739 448.355 o 10 10 10 406.033 350.418 18.654 14.695 o 11 0 11 84.135 46.303 22.372 67.219 o 11 0 13 51.937 35.609 26.675 83.658 o 11 0 15 55.264 41.242 29.922 72.836 o 11 0 17 107.082 154.098 36.861 34.986 o 11 1 11 189.981 127.165 16.765 33.334 o 11 1 12 36.367 36.254 18.414 124.296 o 11 1 13 28.852 59.055 19.172 115.664 o 11 1 14 32.920 23.724 17.809 146.234 o 11 1 15 1.309 -40.324 18.843 443.149 o 11 1 16 12.708 -25.561 26.670 177.493 o 11 1 17 0.956 -24.179 22.972 308.203 o 11 2 11 78.374 78.117 17.137 67.667 o 11 2 12 0.691 27.171 18.203 281.912 o 11 2 13 16.986 -33.735 17.936 263.918 o 11 2 14 1.591 -19.892 18.501 452.144 o 11 2 15 1.533 -28.431 22.549 313.105 o 11 2 16 0.005 -65.550 20.216 411.250 o 11 2 17 39.703 -39.034 20.230 146.559 o 11 3 11 6.628 27.524 14.656 283.319 o 11 3 12 33.117 5.261 19.499 160.967 o 11 3 13 7.727 31.363 20.967 192.281 o 11 3 14 38.448 49.480 23.314 97.787 o 11 3 15 20.734 19.860 22.533 156.048 o 11 3 16 57.711 29.242 21.617 92.691 o 11 4 11 30.012 -15.996 16.055 206.220 o 11 4 12 7.495 -28.380 15.860 430.404 o 11 4 13 5.462 -43.499 15.681 484.173 o 11 4 14 14.269 4.297 20.008 238.435 o 11 4 15 29.657 45.401 23.479 110.247 o 11 4 16 0.610 -35.094 26.025 244.126 o 11 5 11 126.827 154.942 21.160 39.321 o 11 5 12 13.954 -5.484 17.758 292.705 o 11 5 13 0.095 -21.670 18.261 501.447 o 11 5 14 20.883 -33.685 19.147 222.867 o 11 5 15 9.301 -13.244 18.671 322.546 o 11 6 11 19.793 -28.885 14.275 294.304 o 11 6 12 113.090 117.285 16.940 48.042 o 11 6 13 16.838 -3.035 16.643 285.146 o 11 6 14 5.097 -45.289 15.672 494.211 o 11 7 11 75.081 80.235 14.875 70.931 o 11 7 12 25.206 13.630 13.636 215.317 o 11 7 13 1.990 28.104 23.316 199.803 o 11 8 11 3.279 -22.636 13.724 674.679 o 11 8 12 57.669 49.701 15.259 94.999 o 11 9 11 19.746 33.754 17.326 171.427 o 12 0 12 265.796 272.884 29.043 19.887 o 12 0 14 436.377 522.639 63.050 9.681 o 12 0 16 106.972 90.866 33.409 42.407 o 12 1 12 11.416 0.029 19.991 274.791 o 12 1 13 393.926 465.784 26.819 13.229 o 12 1 14 54.171 73.427 20.250 79.927 o 12 1 15 215.109 279.181 23.576 23.186 o 12 1 16 2.181 -36.122 22.289 312.897 o 12 2 12 376.223 445.007 35.243 13.260 o 12 2 13 2.168 -19.166 23.267 289.076 o 12 2 14 226.095 208.032 23.321 24.843 o 12 2 15 20.367 -33.517 19.648 219.993 o 12 2 16 48.983 -10.903 21.036 124.231 o 12 3 12 0.080 -6.270 18.575 485.135 o 12 3 13 473.919 501.454 24.011 11.593 o 12 3 14 6.375 -30.587 21.293 294.084 o 12 3 15 191.605 301.660 27.986 23.212 o 12 4 12 869.416 877.421 54.714 5.830 o 12 4 13 2.462 7.982 15.781 455.872 o 12 4 14 204.372 265.592 30.868 22.994 o 12 4 15 1.018 40.268 29.356 134.008 o 12 5 12 0.000 -13.307 15.435 705.619 o 12 5 13 436.659 477.174 29.292 12.179 o 12 5 14 1.702 -28.794 19.569 405.565 o 12 6 12 539.564 546.551 21.081 10.422 o 12 6 13 0.115 -27.204 25.895 249.914 o 12 7 12 0.425 -3.806 18.049 503.868 o 13 0 13 12.863 97.633 39.748 61.638 o 13 0 15 2.612 5.555 31.540 153.558 o 13 1 13 0.135 115.943 23.391 103.264 o 13 1 14 37.720 92.210 30.652 67.224 o 13 1 15 18.263 31.397 21.055 156.492 o 13 2 13 33.361 64.260 25.888 89.006 o 13 2 14 0.637 60.385 25.278 138.748 o 13 2 15 17.025 30.044 22.699 151.375 o 13 3 13 41.756 102.714 23.355 73.720 o 13 3 14 0.438 70.559 22.765 142.242 o 13 4 13 1.118 23.523 23.369 214.112 o 13 4 14 1.390 41.107 25.049 162.442 o 13 5 13 18.056 42.579 18.314 157.620 o 14 0 14 174.645 167.262 34.069 27.960 o 14 1 14 1.381 25.349 24.964 190.151 o 14 2 14 181.363 209.085 24.142 28.202 o ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x+1/2,y+1/2,-z+1/2 3 -x,-y,-z 4 x-1/2,-y-1/2,z-1/2 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn Ru1 Ru 0.22384(2) 0.49438(4) 0.52719(2) 0.03466(13) Uani 1.000000 . P1 P 0.31843(7) 0.47271(11) 0.49857(8) 0.0336(3) Uani 1.000000 . N1 N 0.2703(3) 0.3741(4) 0.6069(3) 0.0405(10) Uani 1.000000 . N2 N 0.1727(3) 0.6341(4) 0.4598(3) 0.0423(11) Uani 1.000000 . N3 N 0.2762(3) 0.6382(4) 0.5897(3) 0.0434(11) Uani 1.000000 . N4 N 0.1413(2) 0.4992(4) 0.5577(2) 0.0361(9) Uani 1.000000 . N5 N 0.1538(2) 0.3567(4) 0.4661(2) 0.0366(10) Uani 1.000000 . C1 C 0.2901(3) 0.3125(6) 0.6532(3) 0.0486(14) Uani 1.000000 . C2 C 0.3160(4) 0.2362(7) 0.7144(4) 0.068(2) Uani 1.000000 . H2a H 0.329(3) 0.1584(19) 0.7039(10) 0.103(3) Uiso 1.000000 GR H2b H 0.358(2) 0.273(3) 0.7526(10) 0.103(3) Uiso 1.000000 GR H2c H 0.2781(12) 0.226(4) 0.7278(19) 0.103(3) Uiso 1.000000 GR C3 C 0.1184(3) 0.6253(6) 0.3951(4) 0.0460(14) Uani 1.000000 . H3 H 0.108(3) 0.549(6) 0.378(3) 0.043(17) Uiso 1.000000 . C4 C 0.0776(4) 0.7222(7) 0.3570(5) 0.067(2) Uani 1.000000 . H4 H 0.0403(4) 0.7126(7) 0.3111(5) 0.080(2) Uiso 1.000000 R C5 C 0.0938(6) 0.8337(7) 0.3887(6) 0.082(3) Uani 1.000000 . H5 H 0.063(5) 0.906(9) 0.362(5) 0.10(3) Uiso 1.000000 . C6 C 0.1499(5) 0.8462(6) 0.4544(5) 0.076(2) Uani 1.000000 . H6 H 0.1615(5) 0.9220(6) 0.4759(5) 0.092(3) Uiso 1.000000 R C7 C 0.1898(4) 0.7456(5) 0.4893(4) 0.0523(16) Uani 1.000000 . C8 C 0.2501(4) 0.7484(5) 0.5614(4) 0.0491(15) Uani 1.000000 . C9 C 0.2782(5) 0.8523(6) 0.5998(5) 0.071(2) Uani 1.000000 . H9 H 0.2612(5) 0.9275(6) 0.5788(5) 0.085(3) Uiso 1.000000 R C10 C 0.3306(5) 0.8460(7) 0.6679(5) 0.075(2) Uani 1.000000 . H10 H 0.3490(5) 0.9163(7) 0.6944(5) 0.090(3) Uiso 1.000000 R C11 C 0.3557(5) 0.7359(8) 0.6968(5) 0.066(2) Uani 1.000000 . H11 H 0.389(3) 0.718(6) 0.739(3) 0.039(17) Uiso 1.000000 . C12 C 0.3276(4) 0.6327(6) 0.6563(4) 0.0528(16) Uani 1.000000 . H12 H 0.346(3) 0.551(6) 0.672(3) 0.043(17) Uiso 1.000000 . C13 C 0.1540(3) 0.2951(5) 0.4127(3) 0.0433(13) Uani 1.000000 . H13 H 0.195(4) 0.323(6) 0.404(3) 0.056(19) Uiso 1.000000 . C14 C 0.1073(4) 0.2017(5) 0.3787(4) 0.0508(15) Uani 1.000000 . H14 H 0.111(5) 0.160(8) 0.341(5) 0.09(3) Uiso 1.000000 . C15 C 0.0590(4) 0.1667(6) 0.4011(4) 0.0588(17) Uani 1.000000 . H15 H 0.024(4) 0.107(6) 0.377(4) 0.06(2) Uiso 1.000000 . C16 C 0.0561(4) 0.2284(6) 0.4545(4) 0.0540(16) Uani 1.000000 . H16 H 0.020(4) 0.204(7) 0.471(4) 0.07(2) Uiso 1.000000 . C17 C 0.1032(3) 0.3242(5) 0.4860(3) 0.0385(11) Uani 1.000000 . C18 C 0.0983(3) 0.4010(5) 0.5391(3) 0.0400(12) Uani 1.000000 . C19 C 0.0516(4) 0.3805(6) 0.5662(4) 0.0522(15) Uani 1.000000 . H19 H 0.0230(4) 0.3108(6) 0.5542(4) 0.0626(18) Uiso 1.000000 R C20 C 0.0473(4) 0.4646(7) 0.6114(4) 0.0616(18) Uani 1.000000 . H20 H 0.0163(4) 0.4513(7) 0.6311(4) 0.074(2) Uiso 1.000000 R C21 C 0.0877(4) 0.5656(7) 0.6273(4) 0.0590(18) Uani 1.000000 . H21 H 0.083(4) 0.633(6) 0.653(4) 0.056(19) Uiso 1.000000 . C22 C 0.1358(3) 0.5803(6) 0.6001(3) 0.0506(15) Uani 1.000000 . H22 H 0.1651(3) 0.6492(6) 0.6120(3) 0.0607(18) Uiso 1.000000 R C23 C 0.3384(3) 0.3204(4) 0.4804(3) 0.0359(11) Uani 1.000000 . C24 C 0.3164(4) 0.2202(5) 0.5029(3) 0.0464(14) Uani 1.000000 . H24 H 0.288(3) 0.225(6) 0.524(3) 0.046(17) Uiso 1.000000 . C25 C 0.3342(4) 0.1059(5) 0.4909(4) 0.0548(17) Uani 1.000000 . H25 H 0.320(4) 0.045(7) 0.506(4) 0.07(2) Uiso 1.000000 . C26 C 0.3748(4) 0.0873(5) 0.4583(4) 0.0586(17) Uani 1.000000 . C27 C 0.3939(7) -0.0381(7) 0.4454(6) 0.103(4) Uani 1.000000 . H27a H 0.432(3) -0.071(3) 0.4887(11) 0.155(6) Uiso 1.000000 GR H27b H 0.3514(12) -0.089(2) 0.428(4) 0.155(6) Uiso 1.000000 GR H27c H 0.411(4) -0.0348(12) 0.411(3) 0.155(6) Uiso 1.000000 GR C28 C 0.3980(5) 0.1877(6) 0.4362(4) 0.0618(19) Uani 1.000000 . H28 H 0.427(4) 0.183(6) 0.418(4) 0.06(2) Uiso 1.000000 . C29 C 0.3804(4) 0.3019(5) 0.4476(4) 0.0484(15) Uani 1.000000 . H29 H 0.397(4) 0.357(8) 0.439(4) 0.08(3) Uiso 1.000000 . C30 C 0.4054(3) 0.5178(5) 0.5705(3) 0.0398(12) Uani 1.000000 . C31 C 0.4523(3) 0.4325(5) 0.6151(3) 0.0445(13) Uani 1.000000 . H31 H 0.442(3) 0.358(6) 0.605(3) 0.046(17) Uiso 1.000000 . C32 C 0.5183(4) 0.4654(6) 0.6704(4) 0.0560(16) Uani 1.000000 . H32 H 0.547(4) 0.402(8) 0.695(4) 0.08(3) Uiso 1.000000 . C33 C 0.5407(4) 0.5842(7) 0.6818(4) 0.0568(17) Uani 1.000000 . C34 C 0.6166(4) 0.6163(9) 0.7362(5) 0.082(3) Uani 1.000000 . H34a H 0.6506(6) 0.594(6) 0.7194(16) 0.123(4) Uiso 1.000000 GR H34b H 0.6196(11) 0.7021(12) 0.745(3) 0.123(4) Uiso 1.000000 GR H34c H 0.6284(14) 0.573(5) 0.7792(12) 0.123(4) Uiso 1.000000 GR C35 C 0.4920(4) 0.6695(6) 0.6390(4) 0.0572(19) Uani 1.000000 . H35 H 0.500(4) 0.734(6) 0.645(3) 0.049(19) Uiso 1.000000 . C36 C 0.4258(4) 0.6384(5) 0.5855(4) 0.0479(15) Uani 1.000000 . H36 H 0.393(3) 0.691(6) 0.557(3) 0.045(18) Uiso 1.000000 . C37 C 0.3113(3) 0.5553(4) 0.4222(3) 0.0382(12) Uani 1.000000 . C38 C 0.3668(3) 0.6231(5) 0.4215(3) 0.0447(13) Uani 1.000000 . H38 H 0.4110(3) 0.6318(5) 0.4625(3) 0.0537(16) Uiso 1.000000 R C39 C 0.3568(4) 0.6779(5) 0.3601(4) 0.0499(15) Uani 1.000000 . H39 H 0.392(3) 0.719(6) 0.362(3) 0.045(17) Uiso 1.000000 . C40 C 0.2940(4) 0.6665(6) 0.2992(4) 0.0523(16) Uani 1.000000 . C41 C 0.2844(5) 0.7255(8) 0.2320(4) 0.074(2) Uani 1.000000 . H41a H 0.250(3) 0.790(4) 0.2195(18) 0.111(3) Uiso 1.000000 GR H41b H 0.3305(8) 0.757(5) 0.2388(11) 0.111(3) Uiso 1.000000 GR H41c H 0.267(3) 0.6664(15) 0.1947(9) 0.111(3) Uiso 1.000000 GR C42 C 0.2384(4) 0.5967(6) 0.2989(4) 0.0515(15) Uani 1.000000 . H42 H 0.1952(4) 0.5857(6) 0.2573(4) 0.0618(18) Uiso 1.000000 R C43 C 0.2475(3) 0.5438(5) 0.3602(4) 0.0462(14) Uani 1.000000 . H43 H 0.211(4) 0.501(6) 0.357(3) 0.049(18) Uiso 1.000000 . P2 P 0.00203(11) 0.43349(19) 0.20795(10) 0.0603(5) Uani 1.000000 . F7 F 0.0833(3) 0.4327(9) 0.2624(4) 0.151(3) Uani 1.000000 . F8 F 0.0079(10) 0.5418(9) 0.1776(9) 0.314(9) Uani 1.000000 . F9 F -0.0814(3) 0.4195(8) 0.1590(3) 0.142(3) Uani 1.000000 . F10 F 0.0164(5) 0.3668(9) 0.1525(5) 0.167(4) Uani 1.000000 . F11 F -0.0021(7) 0.2972(8) 0.2252(6) 0.227(6) Uani 1.000000 . F12 F -0.0146(4) 0.4776(13) 0.2627(4) 0.257(7) Uani 1.000000 . P3 P 0.37182(12) 0.5206(2) 0.86164(12) 0.0687(5) Uani 1.000000 . F1 F 0.2938(3) 0.4976(5) 0.7994(3) 0.115(2) Uani 1.000000 . F2 F 0.3389(3) 0.5495(5) 0.9127(3) 0.1032(18) Uani 1.000000 . F3 F 0.3806(4) 0.3830(5) 0.8816(3) 0.113(2) Uani 1.000000 . F4 F 0.4507(3) 0.5475(6) 0.9215(3) 0.1081(19) Uani 1.000000 . F5 F 0.4039(3) 0.4948(6) 0.8093(3) 0.0996(17) Uani 1.000000 . F6 F 0.3626(4) 0.6592(5) 0.8407(3) 0.1055(18) Uani 1.000000 . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Ru1 0.0422(2) 0.0254(2) 0.0500(3) -0.00412(16) 0.0329(2) 0.00047(17) P1 0.0413(7) 0.0230(6) 0.0501(8) -0.0016(5) 0.0326(6) 0.0020(5) N1 0.040(2) 0.041(2) 0.048(3) -0.007(2) 0.027(2) 0.001(2) N2 0.055(3) 0.032(2) 0.064(3) 0.006(2) 0.048(3) 0.008(2) N3 0.052(3) 0.038(2) 0.059(3) -0.012(2) 0.042(3) -0.008(2) N4 0.038(2) 0.037(2) 0.038(2) -0.0035(19) 0.0221(19) -0.0041(19) N5 0.046(2) 0.029(2) 0.046(3) 0.0012(18) 0.030(2) 0.0053(18) C1 0.053(3) 0.046(3) 0.054(4) -0.002(3) 0.032(3) 0.002(3) C2 0.079(5) 0.058(4) 0.063(4) 0.010(4) 0.028(4) 0.018(4) C3 0.047(3) 0.042(3) 0.061(4) 0.004(3) 0.036(3) 0.009(3) C4 0.070(5) 0.052(4) 0.089(6) 0.015(3) 0.045(4) 0.021(4) C5 0.106(7) 0.048(4) 0.106(7) 0.032(5) 0.061(6) 0.022(5) C6 0.104(7) 0.035(3) 0.108(7) 0.014(4) 0.065(6) 0.006(4) C7 0.075(4) 0.029(3) 0.080(5) 0.002(3) 0.059(4) 0.003(3) C8 0.074(4) 0.028(3) 0.075(4) -0.010(3) 0.059(4) -0.005(3) C9 0.109(6) 0.034(3) 0.102(6) -0.017(4) 0.077(6) -0.012(4) C10 0.096(6) 0.053(4) 0.104(7) -0.036(4) 0.070(6) -0.034(4) C11 0.067(5) 0.075(5) 0.070(5) -0.031(4) 0.044(4) -0.026(4) C12 0.057(4) 0.054(4) 0.065(4) -0.018(3) 0.043(4) -0.011(3) C13 0.055(3) 0.034(3) 0.046(3) -0.002(2) 0.029(3) 0.002(2) C14 0.071(4) 0.034(3) 0.053(4) -0.005(3) 0.034(3) -0.007(3) C15 0.068(4) 0.036(3) 0.078(5) -0.012(3) 0.039(4) -0.012(3) C16 0.058(4) 0.040(3) 0.075(5) -0.013(3) 0.040(4) -0.008(3) C17 0.041(3) 0.031(2) 0.047(3) -0.002(2) 0.024(2) 0.001(2) C18 0.042(3) 0.039(3) 0.047(3) -0.004(2) 0.027(3) -0.000(2) C19 0.056(4) 0.052(4) 0.064(4) -0.014(3) 0.041(3) -0.004(3) C20 0.058(4) 0.086(5) 0.063(4) -0.014(4) 0.046(4) -0.006(4) C21 0.051(4) 0.078(5) 0.060(4) -0.010(3) 0.036(3) -0.022(4) C22 0.053(3) 0.055(4) 0.061(4) -0.013(3) 0.041(3) -0.018(3) C23 0.042(3) 0.024(2) 0.049(3) 0.000(2) 0.027(3) 0.001(2) C24 0.066(4) 0.032(3) 0.061(4) -0.002(3) 0.046(3) 0.001(3) C25 0.080(5) 0.026(3) 0.076(5) -0.004(3) 0.051(4) 0.002(3) C26 0.087(5) 0.031(3) 0.078(5) 0.005(3) 0.055(4) -0.004(3) C27 0.171(10) 0.037(4) 0.168(10) 0.011(5) 0.135(9) -0.007(5) C28 0.088(5) 0.043(3) 0.089(5) 0.007(3) 0.070(5) -0.002(3) C29 0.065(4) 0.032(3) 0.070(4) -0.002(3) 0.050(4) 0.002(3) C30 0.045(3) 0.032(3) 0.059(3) -0.005(2) 0.037(3) -0.005(2) C31 0.051(3) 0.033(3) 0.058(4) -0.005(2) 0.032(3) -0.009(3) C32 0.057(4) 0.048(4) 0.067(4) -0.001(3) 0.033(4) -0.010(3) C33 0.060(4) 0.061(4) 0.064(4) -0.019(3) 0.041(4) -0.025(3) C34 0.072(5) 0.094(6) 0.084(6) -0.031(5) 0.040(5) -0.049(5) C35 0.078(5) 0.042(4) 0.081(5) -0.022(3) 0.061(4) -0.023(3) C36 0.060(4) 0.031(3) 0.078(4) -0.005(3) 0.053(4) -0.004(3) C37 0.046(3) 0.024(2) 0.061(3) 0.003(2) 0.040(3) 0.006(2) C38 0.053(3) 0.036(3) 0.063(4) -0.003(2) 0.042(3) 0.004(3) C39 0.067(4) 0.035(3) 0.075(4) -0.005(3) 0.056(4) 0.005(3) C40 0.066(4) 0.041(3) 0.075(4) 0.013(3) 0.053(4) 0.017(3) C41 0.084(5) 0.073(5) 0.088(6) 0.010(4) 0.059(5) 0.031(4) C42 0.052(3) 0.056(4) 0.058(4) 0.014(3) 0.035(3) 0.015(3) C43 0.047(3) 0.039(3) 0.069(4) 0.003(2) 0.042(3) 0.010(3) P2 0.0631(11) 0.0661(12) 0.0601(11) 0.0173(9) 0.0359(9) 0.0054(9) F7 0.066(3) 0.225(9) 0.143(6) 0.000(5) 0.034(4) -0.044(6) F8 0.52(2) 0.103(7) 0.41(2) 0.035(10) 0.29(2) 0.134(10) F9 0.087(4) 0.204(8) 0.109(5) 0.039(5) 0.024(4) -0.053(5) F10 0.164(7) 0.187(8) 0.199(8) -0.000(6) 0.127(7) -0.078(7) F11 0.263(12) 0.109(7) 0.206(10) 0.006(7) 0.022(9) 0.011(7) F12 0.088(4) 0.56(2) 0.133(6) -0.033(8) 0.058(4) -0.203(10) P3 0.0737(13) 0.0628(12) 0.0748(13) 0.0038(10) 0.0391(11) -0.0034(10) F1 0.076(3) 0.104(4) 0.131(5) 0.009(3) 0.021(3) -0.031(4) F2 0.129(5) 0.093(4) 0.130(5) -0.010(3) 0.096(4) -0.013(3) F3 0.168(6) 0.063(3) 0.126(5) 0.022(3) 0.084(5) 0.020(3) F4 0.081(4) 0.139(5) 0.091(4) -0.003(4) 0.030(3) -0.022(4) F5 0.105(4) 0.119(5) 0.089(4) 0.027(3) 0.058(3) 0.007(3) F6 0.144(5) 0.069(3) 0.127(5) 0.004(3) 0.083(4) 0.005(3) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source Ru -1.23940 0.83517 19.26740 12.91820 4.86337 1.56756 0.80852 8.43467 24.79970 94.29280 5.37873983383 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' C 0.00347 0.00161 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.215599998832 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' F 0.01794 0.01033 3.53920 2.64120 1.51700 1.02430 10.28250 4.29440 0.26150 26.14760 0.277599990368 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.0030380000826 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' N 0.00653 0.00323 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.5290002823 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' P 0.10434 0.09671 6.43450 4.17910 1.78000 1.49080 1.90670 27.15700 0.52600 68.16450 1.11489999294 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Ru1 P1 91.68(13) . . ? N2 Ru1 P1 96.49(12) . . ? N2 Ru1 N1 169.08(18) . . ? N3 Ru1 P1 89.94(13) . . ? N3 Ru1 N1 93.3(2) . . ? N3 Ru1 N2 79.5(2) . . ? N4 Ru1 P1 174.94(13) . . ? N4 Ru1 N1 83.57(18) . . ? N4 Ru1 N2 88.45(17) . . ? N4 Ru1 N3 92.05(17) . . ? N5 Ru1 P1 100.60(12) . . ? N5 Ru1 N1 88.28(18) . . ? N5 Ru1 N2 97.30(19) . . ? N5 Ru1 N3 169.29(17) . . ? N5 Ru1 N4 77.60(16) . . ? C23 P1 Ru1 117.17(17) . . ? C30 P1 Ru1 111.90(17) . . ? C30 P1 C23 101.6(2) . . ? C37 P1 Ru1 117.60(17) . . ? C37 P1 C23 101.6(2) . . ? C37 P1 C30 105.0(3) . . ? C1 N1 Ru1 171.8(5) . . ? C3 N2 Ru1 126.5(4) . . ? C7 N2 Ru1 114.9(4) . . ? C7 N2 C3 117.8(5) . . ? C8 N3 Ru1 115.3(4) . . ? C12 N3 Ru1 126.0(4) . . ? C12 N3 C8 118.4(5) . . ? C18 N4 Ru1 114.3(3) . . ? C22 N4 Ru1 125.3(4) . . ? C22 N4 C18 119.7(5) . . ? C13 N5 Ru1 129.0(4) . . ? C17 N5 Ru1 114.1(4) . . ? C17 N5 C13 116.9(5) . . ? C2 C1 N1 178.1(7) . . ? H2a C2 C1 109.5 . . ? H2b C2 C1 109.5 . . ? H2b C2 H2a 109.5 . . ? H2c C2 C1 109.5 . . ? H2c C2 H2a 109.5 . . ? H2c C2 H2b 109.5 . . ? H3 C3 N2 115(4) . . ? C4 C3 N2 123.6(7) . . ? C4 C3 H3 121(4) . . ? H4 C4 C3 121.1(5) . . ? C5 C4 C3 117.8(8) . . ? C5 C4 H4 121.1(5) . . ? H5 C5 C4 119(5) . . ? C6 C5 C4 120.0(7) . . ? C6 C5 H5 121(5) . . ? H6 C6 C5 120.3(4) . . ? C7 C6 C5 119.3(7) . . ? C7 C6 H6 120.3(5) . . ? C6 C7 N2 121.3(7) . . ? C8 C7 N2 114.9(5) . . ? C8 C7 C6 123.7(6) . . ? C7 C8 N3 114.8(5) . . ? C9 C8 N3 120.9(7) . . ? C9 C8 C7 124.3(6) . . ? H9 C9 C8 119.8(5) . . ? C10 C9 C8 120.3(7) . . ? C10 C9 H9 119.8(4) . . ? H10 C10 C9 120.5(4) . . ? C11 C10 C9 119.0(7) . . ? C11 C10 H10 120.5(5) . . ? H11 C11 C10 129(4) . . ? C12 C11 C10 119.4(8) . . ? C12 C11 H11 112(4) . . ? C11 C12 N3 121.9(7) . . ? H12 C12 N3 114(4) . . ? H12 C12 C11 124(4) . . ? H13 C13 N5 110(4) . . ? C14 C13 N5 123.8(6) . . ? C14 C13 H13 126(4) . . ? H14 C14 C13 120(5) . . ? C15 C14 C13 118.8(6) . . ? C15 C14 H14 121(5) . . ? H15 C15 C14 121(4) . . ? C16 C15 C14 119.2(6) . . ? C16 C15 H15 119(4) . . ? H16 C16 C15 120(4) . . ? C17 C16 C15 119.8(6) . . ? C17 C16 H16 120(4) . . ? C16 C17 N5 121.5(5) . . ? C18 C17 N5 116.1(5) . . ? C18 C17 C16 122.3(5) . . ? C17 C18 N4 115.0(4) . . ? C19 C18 N4 120.9(5) . . ? C19 C18 C17 124.0(5) . . ? H19 C19 C18 120.6(4) . . ? C20 C19 C18 118.9(6) . . ? C20 C19 H19 120.6(4) . . ? H20 C20 C19 119.9(4) . . ? C21 C20 C19 120.2(6) . . ? C21 C20 H20 119.9(4) . . ? H21 C21 C20 125(4) . . ? C22 C21 C20 118.6(6) . . ? C22 C21 H21 116(4) . . ? C21 C22 N4 121.7(6) . . ? H22 C22 N4 119.2(3) . . ? H22 C22 C21 119.2(4) . . ? C24 C23 P1 121.7(4) . . ? C29 C23 P1 120.8(4) . . ? C29 C23 C24 117.4(5) . . ? H24 C24 C23 123(4) . . ? C25 C24 C23 120.9(5) . . ? C25 C24 H24 116(4) . . ? H25 C25 C24 119(5) . . ? C26 C25 C24 121.9(6) . . ? C26 C25 H25 119(5) . . ? C27 C26 C25 121.6(6) . . ? C28 C26 C25 117.6(6) . . ? C28 C26 C27 120.8(6) . . ? H27a C27 C26 109.5 . . ? H27b C27 C26 109.5 . . ? H27b C27 H27a 109.5 . . ? H27c C27 C26 109.5 . . ? H27c C27 H27a 109.5 . . ? H27c C27 H27b 109.5 . . ? H28 C28 C26 123(5) . . ? C29 C28 C26 120.9(6) . . ? C29 C28 H28 116(5) . . ? C28 C29 C23 121.2(6) . . ? H29 C29 C23 118(6) . . ? H29 C29 C28 121(6) . . ? C31 C30 P1 120.3(4) . . ? C36 C30 P1 122.4(5) . . ? C36 C30 C31 117.3(6) . . ? H31 C31 C30 118(4) . . ? C32 C31 C30 121.0(6) . . ? C32 C31 H31 120(4) . . ? H32 C32 C31 114(5) . . ? C33 C32 C31 121.5(7) . . ? C33 C32 H32 124(5) . . ? C34 C33 C32 120.6(8) . . ? C35 C33 C32 117.0(7) . . ? C35 C33 C34 122.3(7) . . ? H34a C34 C33 109.5 . . ? H34b C34 C33 109.5 . . ? H34b C34 H34a 109.5 . . ? H34c C34 C33 109.5 . . ? H34c C34 H34a 109.5 . . ? H34c C34 H34b 109.5 . . ? H35 C35 C33 121(5) . . ? C36 C35 C33 121.9(6) . . ? C36 C35 H35 117(6) . . ? C35 C36 C30 121.1(7) . . ? H36 C36 C30 115(4) . . ? H36 C36 C35 124(4) . . ? C38 C37 P1 124.4(5) . . ? C43 C37 P1 117.5(4) . . ? C43 C37 C38 117.9(5) . . ? H38 C38 C37 120.1(4) . . ? C39 C38 C37 119.8(6) . . ? C39 C38 H38 120.1(4) . . ? H39 C39 C38 117(4) . . ? C40 C39 C38 122.1(6) . . ? C40 C39 H39 121(4) . . ? C41 C40 C39 121.4(6) . . ? C42 C40 C39 118.7(6) . . ? C42 C40 C41 119.9(7) . . ? H41a C41 C40 109.5 . . ? H41b C41 C40 109.5 . . ? H41b C41 H41a 109.5 . . ? H41c C41 C40 109.5 . . ? H41c C41 H41a 109.5 . . ? H41c C41 H41b 109.5 . . ? H42 C42 C40 120.2(4) . . ? C43 C42 C40 119.5(7) . . ? C43 C42 H42 120.2(4) . . ? C42 C43 C37 121.9(6) . . ? H43 C43 C37 123(4) . . ? H43 C43 C42 115(4) . . ? F8 P2 F7 93.2(8) . . ? F9 P2 F7 171.9(5) . . ? F9 P2 F8 94.7(8) . . ? F10 P2 F7 92.6(4) . . ? F10 P2 F8 87.6(8) . . ? F10 P2 F9 89.2(4) . . ? F11 P2 F7 88.6(6) . . ? F11 P2 F8 164.5(8) . . ? F11 P2 F9 84.1(5) . . ? F11 P2 F10 77.0(6) . . ? F12 P2 F7 88.7(4) . . ? F12 P2 F8 101.3(9) . . ? F12 P2 F9 88.2(4) . . ? F12 P2 F10 170.9(7) . . ? F12 P2 F11 94.1(8) . . ? F2 P3 F1 90.9(4) . . ? F3 P3 F1 91.0(4) . . ? F3 P3 F2 92.3(3) . . ? F4 P3 F1 177.2(4) . . ? F4 P3 F2 91.0(3) . . ? F4 P3 F3 91.0(4) . . ? F5 P3 F1 88.6(4) . . ? F5 P3 F2 178.5(3) . . ? F5 P3 F3 89.2(3) . . ? F5 P3 F4 89.5(3) . . ? F6 P3 F1 88.6(4) . . ? F6 P3 F2 88.2(3) . . ? F6 P3 F3 179.4(4) . . ? F6 P3 F4 89.4(4) . . ? F6 P3 F5 90.4(3) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ru1 P1 2.3465(13) . ? Ru1 N1 2.037(5) . ? Ru1 N2 2.058(5) . ? Ru1 N3 2.053(5) . ? Ru1 N4 2.119(4) . ? Ru1 N5 2.107(5) . ? P1 C23 1.834(5) . ? P1 C30 1.827(6) . ? P1 C37 1.837(5) . ? N1 C1 1.122(8) . ? N2 C3 1.333(8) . ? N2 C7 1.365(8) . ? N3 C8 1.366(8) . ? N3 C12 1.337(9) . ? N4 C18 1.352(7) . ? N4 C22 1.331(7) . ? N5 C13 1.346(7) . ? N5 C17 1.366(7) . ? C1 C2 1.451(9) . ? C2 H2a 0.9700 . ? C2 H2b 0.9700 . ? C2 H2c 0.9700 . ? C3 H3 0.91(6) . ? C3 C4 1.384(9) . ? C4 H4 0.9400 . ? C4 C5 1.382(12) . ? C5 H5 1.03(9) . ? C5 C6 1.364(13) . ? C6 H6 0.9400 . ? C6 C7 1.390(10) . ? C7 C8 1.480(10) . ? C8 C9 1.385(9) . ? C9 H9 0.9400 . ? C9 C10 1.367(12) . ? C10 H10 0.9400 . ? C10 C11 1.365(12) . ? C11 H11 0.88(6) . ? C11 C12 1.398(10) . ? C12 H12 0.98(6) . ? C13 H13 1.00(7) . ? C13 C14 1.381(8) . ? C14 H14 0.98(9) . ? C14 C15 1.367(10) . ? C15 H15 0.95(7) . ? C15 C16 1.372(10) . ? C16 H16 1.02(7) . ? C16 C17 1.394(8) . ? C17 C18 1.474(8) . ? C18 C19 1.374(7) . ? C19 H19 0.9400 . ? C19 C20 1.389(9) . ? C20 H20 0.9400 . ? C20 C21 1.351(10) . ? C21 H21 0.96(7) . ? C21 C22 1.394(8) . ? C22 H22 0.9400 . ? C23 C24 1.379(7) . ? C23 C29 1.379(8) . ? C24 H24 0.90(6) . ? C24 C25 1.385(8) . ? C25 H25 0.86(8) . ? C25 C26 1.352(9) . ? C26 C27 1.515(9) . ? C26 C28 1.391(9) . ? C27 H27a 0.9700 . ? C27 H27b 0.9700 . ? C27 H27c 0.9700 . ? C28 H28 0.86(7) . ? C28 C29 1.379(8) . ? C29 H29 0.77(8) . ? C30 C31 1.383(8) . ? C30 C36 1.400(7) . ? C31 H31 0.86(6) . ? C31 C32 1.388(9) . ? C32 H32 0.92(8) . ? C32 C33 1.387(9) . ? C33 C34 1.512(10) . ? C33 C35 1.384(11) . ? C34 H34a 0.9700 . ? C34 H34b 0.9700 . ? C34 H34c 0.9700 . ? C35 H35 0.74(7) . ? C35 C36 1.371(10) . ? C36 H36 0.89(6) . ? C37 C38 1.392(7) . ? C37 C43 1.387(9) . ? C38 H38 0.9400 . ? C38 C39 1.388(8) . ? C39 H39 0.86(6) . ? C39 C40 1.363(10) . ? C40 C41 1.524(9) . ? C40 C42 1.396(9) . ? C41 H41a 0.9700 . ? C41 H41b 0.9700 . ? C41 H41c 0.9700 . ? C42 H42 0.9400 . ? C42 C43 1.382(8) . ? C43 H43 0.87(7) . ? P2 F7 1.552(6) . ? P2 F8 1.407(8) . ? P2 F9 1.569(6) . ? P2 F10 1.556(7) . ? P2 F11 1.575(10) . ? P2 F12 1.468(6) . ? P3 F1 1.577(6) . ? P3 F2 1.586(5) . ? P3 F3 1.579(6) . ? P3 F4 1.579(6) . ? P3 F5 1.591(5) . ? P3 F6 1.596(6) . ?