#------------------------------------------------------------------------------ #$Date: 2021-09-23 01:11:52 +0300 (Thu, 23 Sep 2021) $ #$Revision: 269243 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/47/1564703.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564703 loop_ _publ_author_name 'Yi, Xiaofeng' 'Wang, Di' 'Li, Fan' 'Zhang, Jian' 'Zhang, Lei' _publ_section_title ; Molecular Bixbyite-Like In12-Oxo Clusters with Tunable Functionalization Sites for Lithography Patterning Applications ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC04491E _journal_year 2021 _chemical_formula_moiety 'C56 H88 Cl4 F4 In12 N8 O26, 2(Cl)' _chemical_formula_sum 'C56 H88 Cl6 F4 In12 N8 O26' _chemical_formula_weight 2955.88 _chemical_name_systematic InOC-5 _space_group_crystal_system tetragonal _space_group_IT_number 82 _space_group_name_Hall 'I -4' _space_group_name_H-M_alt 'I -4' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _audit_creation_date 2021-01-24 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-04-19 deposited with the CCDC. 2021-09-20 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 15.9744(2) _cell_length_b 15.9744(2) _cell_length_c 19.4804(5) _cell_measurement_reflns_used 8429 _cell_measurement_temperature 100.03(19) _cell_measurement_theta_max 74.5180 _cell_measurement_theta_min 3.8890 _cell_volume 4971.04(16) _computing_cell_refinement 'CrysAlisPro 1.171.40.67a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.67a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.67a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'olex2.solve (Bourhis et al., 2015)' _diffrn_ambient_temperature 100.03(19) _diffrn_detector_area_resol_mean 5.1734 _diffrn_detector_type Atlas _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 6.00 82.00 1.00 1.50 -- 41.04 -99.00-180.00 76 2 \w 27.00 97.00 1.00 1.50 -- 41.04-125.00 150.00 70 3 \w 27.00 97.00 1.00 1.50 -- 41.04-125.00 -90.00 70 4 \w 97.00 178.00 1.00 6.00 -- 108.23 125.00 60.00 81 5 \w 26.00 106.00 1.00 6.00 -- 108.23 -94.00 -30.00 80 6 \w 103.00 178.00 1.00 6.00 -- 108.23 110.00 -49.00 75 7 \w 82.00 178.00 1.00 6.00 -- 108.23 45.00 30.00 96 8 \w 13.00 114.00 1.00 1.50 -- 41.04 57.00 150.00 101 9 \w 13.00 114.00 1.00 1.50 -- 41.04 57.00 -60.00 101 10 \w 80.00 174.00 1.00 6.00 -- 108.23 30.00-150.00 94 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, Atlas' _diffrn_measurement_method '\w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0303 _diffrn_reflns_av_unetI/netI 0.0257 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 10192 _diffrn_reflns_point_group_measured_fraction_full 0.970 _diffrn_reflns_point_group_measured_fraction_max 0.970 _diffrn_reflns_theta_full 58.930 _diffrn_reflns_theta_max 58.930 _diffrn_reflns_theta_min 3.913 _exptl_absorpt_coefficient_mu 23.891 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.41355 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.67a (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear light' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_density_diffrn 1.975 _exptl_crystal_description block _exptl_crystal_F_000 2828 _exptl_crystal_size_max 0.08 _exptl_crystal_size_mid 0.06 _exptl_crystal_size_min 0.05 _refine_diff_density_max 1.480 _refine_diff_density_min -0.583 _refine_diff_density_rms 0.107 _refine_ls_abs_structure_details ; Flack x determined using 1540 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.028(7) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.086 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 254 _refine_ls_number_reflns 3465 _refine_ls_number_restraints 36 _refine_ls_restrained_S_all 1.130 _refine_ls_R_factor_all 0.0280 _refine_ls_R_factor_gt 0.0275 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0358P)^2^+32.2449P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0709 _refine_ls_wR_factor_ref 0.0712 _reflns_Friedel_coverage 0.872 _reflns_Friedel_fraction_full 0.938 _reflns_Friedel_fraction_max 0.938 _reflns_number_gt 3400 _reflns_number_total 3465 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1sc04491e2.cif _cod_data_source_block InOC-5 _cod_original_cell_volume 4971.04(18) _cod_database_code 1564703 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.381 _shelx_estimated_absorpt_t_min 0.251 _olex2_refinement_description ; 1. Others Fixed U13: O2(0) Cl2(0) Fixed U23: O2(0) Cl2(0) Fixed Uiso: H00D(0.032) H00E(0.038) H2(0.084) H3(0.114) H5(0.091) H6(0.085) H7A(0.108) H7B(0.108) H8A(0.045) H8B(0.045) H9A(0.037) H9B(0.037) H10A(0.037) H10B(0.037) H11A(0.041) H11B(0.041) H12A(0.03) H12B(0.03) H13A(0.051) H13B(0.051) H14A(0.046) H14B(0.046) Fixed X: O2(0.5) H00D(0.861528) H00E(0.906939) H2(0.384913) H3(0.396746) H5(0.554031) H6(0.5345) H7A(0.654183) H7B(0.717286) H8A(0.744148) H8B(0.809099) H9A(0.793261) H9B(0.827578) H10A(0.692739) H10B(0.656361) H11A(0.866187) H11B(0.922067) H12A(0.804385) H12B(0.795765) H13A(0.948018) H13B(0.856084) H14A(0.901765) H14B(0.876905) Cl2(1) Fixed Y: O2(0.5) H00D(0.552584) H00E(0.496995) H2(0.830909) H3(0.890767) H5(0.714619) H6(0.639986) H7A(0.676348) H7B(0.71009) H8A(0.597464) H8B(0.657995) H9A(0.469439) H9B(0.420842) H10A(0.371618) H10B(0.46495) H11A(0.36473) H11B(0.387813) H12A(0.403011) H12B(0.314787) H13A(0.543508) H13B(0.532316) H14A(0.651545) H14B(0.672974) Cl2(0.5) Fixed Z: H00D(0.66756) H00E(0.566029) H2(0.674084) H3(0.782238) H5(0.832356) H6(0.729815) H7A(0.712045) H7B(0.654928) H8A(0.756688) H8B(0.719102) H9A(0.75962) H9B(0.693421) H10A(0.714124) H10B(0.718626) H11A(0.550458) H11B(0.484913) H12A(0.416542) H12B(0.455294) H13A(0.46156) H13B(0.4298) H14A(0.531622) H14B(0.453761) ; _shelx_res_file ; TITL inoc-5_a.res in I-4 inoc-5_sq.res created by SHELXL-2017/1 at 21:18:14 on 24-Jan-2021 REM Old TITL InOC-5 in I-4 REM SHELXT solution in I-4 REM R1 0.093, Rweak 0.019, Alpha 0.011, Orientation as input REM Flack x = 0.075 ( 0.009 ) from Parsons' quotients REM Formula found by SHELXT: C23 N3 O6 F7 Cl2 In6 CELL 1.54178 15.9744 15.9744 19.4804 90 90 90 ZERR 2 0.0002 0.0002 0.0005 0 0 0 LATT -2 SYMM -X,-Y,+Z SYMM +Y,-X,-Z SYMM -Y,+X,-Z SFAC C H Cl F In N O UNIT 112 176 12 8 24 16 52 ISOR 0.01 0.02 Cl2 C13 ISOR 0.01 0.02 C9 ISOR 0.01 0.02 C14 C5 ISOR 0.01 0.02 C7 L.S. 10 0 49 PLAN 2 SIZE 0.05 0.06 0.08 TEMP -173.12(19) BOND $H ABIN fmap 2 53 acta SHEL 999 0.9 OMIT 0 0 4 OMIT -2 1 3 REM REM REM WGHT 0.035800 32.244904 FVAR 0.11429 IN1 5 0.544669 0.613464 0.570405 11.00000 0.01401 0.01475 = 0.00833 -0.00158 0.00060 -0.00208 IN2 5 0.735460 0.528530 0.567785 11.00000 0.01334 0.02805 = 0.01344 -0.00008 -0.00036 -0.00043 IN3 5 0.680079 0.654642 0.437320 11.00000 0.02003 0.02430 = 0.01594 0.00394 0.00456 -0.00618 CL1 3 0.759831 0.763454 0.380100 11.00000 0.04192 0.04921 = 0.04238 0.01927 0.00894 -0.02103 F3 4 0.484739 0.832569 0.882054 11.00000 0.09324 0.29722 = 0.10048 -0.13939 -0.00998 0.03516 O1 7 0.458548 0.697790 0.624655 11.00000 0.02480 0.01784 = 0.01818 -0.00739 0.00156 0.00200 O2 7 0.500000 0.500000 0.614908 10.50000 0.03721 0.01628 = 0.01801 0.00000 0.00000 -0.01265 O3 7 0.654555 0.614481 0.629045 11.00000 0.01774 0.02492 = 0.02509 -0.01098 -0.00856 0.00205 O4 7 0.681570 0.427673 0.623607 11.00000 0.03111 0.02621 = 0.01362 0.00189 -0.00871 -0.00429 O5 7 0.721490 0.402978 0.491643 11.00000 0.01641 0.02213 = 0.01710 0.00287 0.00175 0.00720 O6 7 0.777666 0.637699 0.512122 11.00000 0.01729 0.03608 = 0.02791 0.00155 -0.00289 -0.00924 O7 7 0.629187 0.553448 0.500111 11.00000 0.01096 0.01738 = 0.01161 0.00137 0.00243 -0.00316 N00D 6 0.800089 0.543764 0.674234 11.00000 0.01385 0.04982 = 0.01718 -0.00093 -0.00708 -0.00317 AFIX 13 H00D 2 0.861528 0.552584 0.667560 11.00000 -1.20000 AFIX 0 N00E 6 0.865792 0.488385 0.527992 11.00000 0.01912 0.05549 = 0.02106 -0.00722 -0.00529 0.00461 AFIX 13 H00E 2 0.906939 0.496995 0.566029 11.00000 -1.20000 AFIX 0 C1 1 0.460862 0.731269 0.690001 11.00000 0.06622 0.05531 = 0.04938 -0.01587 0.01241 0.00225 C2 1 0.419297 0.804648 0.707542 11.00000 0.05992 0.08595 = 0.06445 -0.04829 0.01868 0.00577 AFIX 43 H2 2 0.384913 0.830909 0.674084 11.00000 -1.20000 AFIX 0 C3 1 0.425938 0.840705 0.771286 11.00000 0.07023 0.10026 = 0.11507 -0.04282 -0.03832 0.00832 AFIX 43 H3 2 0.396746 0.890767 0.782238 11.00000 -1.20000 AFIX 0 C4 1 0.476480 0.801630 0.818777 11.00000 0.06693 0.12473 = 0.05646 -0.03400 -0.01699 -0.01196 C5 1 0.515172 0.736667 0.800169 11.00000 0.05311 0.12440 = 0.04986 -0.03804 -0.00863 -0.00011 AFIX 43 H5 2 0.554031 0.714619 0.832356 11.00000 -1.20000 AFIX 0 C6 1 0.508173 0.692455 0.737619 11.00000 0.04568 0.11411 = 0.05261 -0.00065 -0.01278 -0.00095 AFIX 43 H6 2 0.534500 0.639986 0.729815 11.00000 -1.20000 AFIX 0 C7 1 0.695179 0.658695 0.676789 11.00000 0.06648 0.10707 = 0.09606 -0.06668 -0.03151 0.02809 AFIX 23 H7A 2 0.654183 0.676348 0.712045 11.00000 -1.20000 H7B 2 0.717286 0.710090 0.654928 11.00000 -1.20000 AFIX 0 C8 1 0.763939 0.616667 0.711176 11.00000 0.04502 0.04220 = 0.02591 -0.00649 -0.02472 -0.00850 AFIX 23 H8A 2 0.744148 0.597464 0.756688 11.00000 -1.20000 H8B 2 0.809099 0.657995 0.719102 11.00000 -1.20000 AFIX 0 C9 1 0.785723 0.462106 0.709537 11.00000 0.03043 0.04641 = 0.01559 0.00133 -0.01472 0.00329 AFIX 23 H9A 2 0.793261 0.469439 0.759620 11.00000 -1.20000 H9B 2 0.827578 0.420842 0.693421 11.00000 -1.20000 AFIX 0 C10 1 0.698068 0.428958 0.695345 11.00000 0.03201 0.04045 = 0.02088 0.00264 -0.00516 0.00686 AFIX 23 H10A 2 0.692739 0.371618 0.714124 11.00000 -1.20000 H10B 2 0.656361 0.464950 0.718626 11.00000 -1.20000 AFIX 0 C11 1 0.868464 0.399633 0.508505 11.00000 0.01331 0.05664 = 0.03357 -0.00325 -0.00080 0.01198 AFIX 23 H11A 2 0.866187 0.364730 0.550458 11.00000 -1.20000 H11B 2 0.922067 0.387813 0.484913 11.00000 -1.20000 AFIX 0 C12 1 0.796943 0.376215 0.461958 11.00000 0.02280 0.02459 = 0.02796 0.00167 -0.00058 0.01158 AFIX 23 H12A 2 0.804385 0.403011 0.416542 11.00000 -1.20000 H12B 2 0.795765 0.314787 0.455294 11.00000 -1.20000 AFIX 0 C13 1 0.887452 0.547422 0.471843 11.00000 0.01898 0.06945 = 0.03787 0.00073 0.01285 -0.00054 AFIX 23 H13A 2 0.948018 0.543508 0.461560 11.00000 -1.20000 H13B 2 0.856084 0.532316 0.429800 11.00000 -1.20000 AFIX 0 C14 1 0.866303 0.634205 0.492444 11.00000 0.02137 0.05125 = 0.04134 0.00300 -0.00362 -0.02491 AFIX 23 H14A 2 0.901765 0.651545 0.531622 11.00000 -1.20000 H14B 2 0.876905 0.672974 0.453761 11.00000 -1.20000 AFIX 0 CL2 3 1.000000 0.500000 0.648265 10.50000 0.03077 0.36567 = 0.04580 0.00000 0.00000 0.00278 HKLF 4 REM inoc-5_a.res in I-4 REM R1 = 0.0275 for 3400 Fo > 4sig(Fo) and 0.0280 for all 3465 data REM 254 parameters refined using 36 restraints END WGHT 0.0358 32.2528 REM Highest difference peak 1.480, deepest hole -0.583, 1-sigma level 0.107 Q1 1 1.0111 0.4004 0.6248 11.00000 0.05 1.48 Q2 1 0.5029 0.8064 0.7243 11.00000 0.05 0.81 ; _shelx_res_checksum 78414 _shelx_hkl_file ; 0 0 4 372.06 8.00 0 0 -4 341.57 12.00 0 0 6 3592.84 35.60 0 0 -6 3512.05 49.20 0 0 8 4026.00 40.70 0 0 -8 3969.60 59.89 0 0 -10 515.65 22.70 0 0 10 556.04 25.40 0 0 -12 82.29 10.20 0 0 12 97.49 11.80 0 0 14 4717.73 53.09 0 0 -14 4802.42 89.19 0 0 16 5365.56 58.99 0 0 16 5196.48 103.29 0 0 18 304.57 12.30 0 0 -18 301.17 12.00 0 0 20 1036.10 22.10 0 0 -20 1053.49 22.10 0 0 22 1971.10 27.40 0 0 -22 1924.31 27.00 0 0 24 430.96 8.90 0 0 -24 413.96 8.70 0 -1 3 795.32 15.40 0 -1 3 821.52 14.00 1 0 -3 794.32 14.60 0 1 3 701.83 15.00 -1 0 -3 730.93 15.80 0 1 -3 697.83 13.90 1 0 5 486.05 12.80 0 -1 5 564.64 13.60 0 -1 5 581.44 17.40 0 1 5 551.24 8.00 1 0 -5 573.74 16.10 -1 0 -5 567.64 17.10 0 -1 -5 499.55 16.40 0 1 -5 486.35 15.00 0 -1 7 3378.26 41.70 0 1 7 3403.26 27.90 0 -1 7 3605.14 55.39 1 0 7 3524.15 40.70 1 0 -7 3396.16 50.69 0 1 -7 3501.25 51.09 0 -1 -7 3536.75 54.19 -1 0 -7 3379.86 53.09 0 -1 9 1355.66 37.40 0 -1 9 1277.77 24.40 1 0 9 1233.78 22.90 -1 0 9 1282.07 34.50 0 -1 -9 1250.57 34.50 1 0 -9 1246.48 33.10 0 1 -9 1263.57 33.00 -1 0 -9 1264.37 34.70 1 0 11 113.69 13.10 0 -1 11 106.89 11.90 -1 0 11 99.39 10.90 0 -1 -11 103.79 11.10 1 0 -11 115.69 11.40 0 1 -11 99.79 10.70 -1 0 -11 105.09 11.40 1 0 -13 1321.07 42.90 0 -1 -13 1296.77 43.40 -1 0 -13 1333.47 43.70 0 1 -13 1363.76 42.70 -1 0 13 1410.06 45.00 0 -1 13 1406.96 44.90 1 0 13 1414.26 48.30 0 1 13 1408.96 46.70 0 -1 13 1352.66 46.80 1 0 15 2644.04 37.30 -1 0 15 2548.34 37.50 0 -1 15 2622.94 38.60 0 1 -15 2480.35 64.49 -1 0 -15 2511.35 66.39 0 -1 -15 2394.36 65.29 1 0 -15 2479.35 64.79 0 -1 15 2538.25 69.79 1 0 15 2534.15 70.39 -1 0 15 2582.74 66.89 0 1 15 2627.84 68.59 0 1 17 699.83 18.40 -1 0 17 721.93 19.20 0 -1 17 728.53 19.70 1 0 17 741.43 19.40 1 0 -17 706.73 18.70 1 0 19 106.29 7.20 0 1 19 107.79 7.10 0 -1 19 104.99 7.50 -1 0 19 108.49 7.40 0 -1 -19 98.49 7.00 -1 0 -19 115.19 7.40 1 0 -19 116.49 7.50 0 1 -19 103.19 7.10 0 -1 21 779.72 18.00 -1 0 21 774.52 17.70 1 0 21 816.72 17.90 0 1 21 774.92 17.50 0 -1 -21 803.52 18.00 1 0 -21 756.82 17.60 0 1 -21 777.92 17.70 -1 0 -21 787.72 17.70 0 1 23 451.75 10.70 1 0 23 461.05 10.90 -1 0 23 453.05 10.80 0 -1 23 466.95 11.00 0 -1 -23 447.06 10.90 -1 0 -23 440.96 10.70 0 1 -23 434.56 10.50 1 0 -23 444.56 10.90 1 -1 0 2144.99 14.80 -1 -1 0 1907.31 14.50 1 -1 2 1026.80 17.50 -1 -1 2 1110.49 14.10 1 -1 2 1120.29 15.70 1 1 -2 1056.29 12.40 -1 -1 -2 1019.30 17.70 -1 1 -2 1004.00 15.60 1 -1 4 660.53 16.00 -1 -1 4 827.12 16.50 -1 -1 4 817.22 15.20 1 -1 4 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259.47 7.90 2 -7 21 272.67 9.00 3 -7 0 2534.75 40.90 3 -7 0 2547.84 48.50 7 3 0 2567.94 45.30 -7 -3 0 2568.14 42.40 3 -7 2 964.20 25.10 3 -7 2 880.81 30.30 3 -7 -2 888.41 25.30 3 -7 2 872.41 29.90 7 3 2 859.31 27.30 7 3 -2 921.21 25.70 -7 -3 -2 914.71 27.20 -7 -3 2 920.41 21.90 3 -7 4 249.88 17.40 3 -7 -4 217.88 11.00 3 -7 4 209.28 12.90 3 -7 4 194.68 14.80 7 3 4 198.98 14.20 7 3 -4 219.38 13.00 -7 -3 -4 213.38 14.50 -3 7 -4 216.28 12.70 3 -7 6 1802.82 50.49 3 -7 6 1683.03 46.80 3 -7 6 1663.43 43.00 7 3 -6 1718.93 40.30 7 3 6 1599.64 43.00 -3 7 -6 1683.73 39.00 -7 -3 -6 1772.82 47.00 3 -7 8 2132.39 58.59 3 -7 8 2031.10 55.59 3 -7 8 1987.10 54.39 7 3 -8 1951.80 47.00 7 3 8 2023.40 50.69 -7 -3 -8 2151.58 56.59 -3 7 -8 2213.88 49.30 3 -7 10 742.23 36.10 3 -7 10 694.23 34.60 3 -7 10 701.93 36.50 7 3 10 688.33 31.60 -7 -3 -10 770.42 36.30 3 -7 12 159.58 9.40 3 -7 12 139.29 16.20 3 -7 12 142.49 16.30 3 -7 12 139.69 18.30 3 -7 -12 169.48 8.30 7 3 -12 159.48 8.30 -7 -3 -12 172.38 18.60 -7 -3 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147.49 12.90 7 4 7 147.59 13.80 -7 -4 -7 160.18 15.10 -4 7 -7 148.09 12.80 4 -7 9 185.38 18.30 4 -7 9 148.89 15.40 4 -7 9 149.79 16.50 7 4 -9 154.38 14.30 7 4 9 150.48 14.50 -7 -4 -9 177.38 17.20 -4 7 -9 148.99 14.00 4 -7 11 8.30 2.20 4 -7 11 5.10 4.60 4 -7 11 5.70 4.50 4 -7 11 3.00 4.40 4 -7 -11 17.80 2.90 7 4 11 9.10 4.40 7 4 -11 6.00 2.00 7 4 -11 8.40 4.70 -7 -4 -11 8.00 4.90 -7 -4 11 4.00 2.10 4 -7 13 65.89 6.20 4 -7 13 59.39 13.00 4 -7 -13 87.39 6.30 7 4 -13 61.39 10.80 -7 -4 -13 74.79 12.50 7 4 -13 62.99 5.40 -7 -4 13 82.19 6.90 7 4 15 49.90 4.10 7 4 -15 31.60 4.00 4 -7 -15 43.30 4.60 4 -7 15 31.90 4.60 -7 -4 15 47.80 5.10 -4 7 15 38.60 4.60 7 4 17 24.20 2.80 7 4 -17 38.00 4.20 4 -7 -17 22.30 3.40 -4 7 17 43.50 4.50 4 -7 17 36.60 4.50 -4 7 19 50.69 4.00 7 4 19 41.80 3.20 4 -7 -19 42.60 3.90 7 4 -19 50.79 4.20 -4 7 19 51.49 4.10 -4 7 21 88.19 4.10 -7 -4 -21 83.79 4.20 4 -7 -21 79.69 4.10 -4 7 21 77.79 3.70 5 -7 0 1112.49 25.70 5 -7 0 1023.50 33.70 7 5 0 1055.59 31.00 -7 -5 2 615.04 24.40 5 -7 -2 524.35 21.60 5 -7 2 553.54 27.30 5 -7 2 558.74 19.70 7 5 2 533.75 23.20 7 5 -2 573.04 22.70 -7 -5 -2 630.44 25.20 5 -7 -4 4.20 2.10 5 -7 4 2.80 4.20 5 -7 4 4.80 3.80 -7 -5 4 13.10 5.20 5 -7 4 5.70 2.90 7 5 4 4.60 3.60 7 5 -4 5.40 3.40 -5 7 -4 4.50 3.00 -7 -5 -4 5.70 3.70 5 -7 6 652.93 34.20 5 -7 6 611.04 26.80 5 -7 6 620.44 28.90 7 5 6 653.53 28.50 7 5 -6 676.63 27.40 -7 -5 -6 717.93 31.90 -5 7 -6 662.13 27.50 -7 -5 8 1242.88 55.79 5 -7 8 992.60 39.00 5 -7 8 960.30 43.10 5 -7 8 916.21 38.40 7 5 -8 997.20 36.60 7 5 8 1116.89 39.00 -5 7 -8 1158.18 39.20 -7 -5 -8 1080.49 41.50 -7 -5 10 417.96 34.60 5 -7 10 321.17 25.50 5 -7 10 318.47 23.10 5 -7 10 288.67 24.60 7 5 -10 296.97 21.80 7 5 10 377.86 24.00 -7 -5 -10 348.07 25.10 5 -7 10 303.37 11.40 -5 7 -10 388.36 24.50 -7 -5 10 345.17 13.60 -7 -5 12 90.79 17.80 5 -7 12 72.19 12.50 5 -7 12 75.19 14.30 -7 -5 -12 80.99 13.00 7 5 -12 67.09 11.30 5 -7 -12 79.79 6.10 5 -7 12 64.19 5.70 -7 -5 12 72.19 6.50 5 -7 -14 372.86 13.30 5 -7 14 386.56 14.30 -5 7 14 408.36 14.00 7 5 16 612.04 14.10 5 -7 -16 630.74 17.00 -5 7 16 618.94 16.90 5 -7 16 621.14 17.70 -5 7 18 106.89 5.80 7 5 18 96.49 5.00 5 -7 -18 90.59 5.90 -5 7 18 105.19 6.30 5 -7 18 114.89 6.80 -5 7 20 23.60 2.40 5 -7 -20 17.40 2.30 5 -7 20 23.80 2.60 -5 7 20 18.80 2.30 6 -7 1 1238.78 28.30 6 -7 -1 1134.99 36.10 6 -7 1 1179.88 40.90 -7 -6 1 1266.07 32.30 7 6 1 1173.88 35.10 7 6 -1 1173.08 34.50 6 -7 -3 1812.42 41.30 6 -7 3 1761.02 38.30 6 -7 3 1872.31 56.89 7 6 3 1919.11 48.20 7 6 -3 1906.71 45.60 -7 -6 5 831.12 38.40 6 -7 5 871.11 41.10 6 -7 5 724.73 28.10 7 6 5 788.22 32.00 7 6 -5 847.02 31.60 -6 7 -5 769.72 30.40 -7 -6 -5 915.61 35.30 -7 -6 7 715.83 40.30 6 -7 7 566.44 34.40 6 -7 7 559.84 28.90 6 -7 7 527.95 27.60 7 6 -7 596.54 27.90 7 6 7 661.73 30.50 -7 -6 -7 641.34 32.30 -6 7 -7 648.54 29.50 -7 -6 9 810.82 47.70 6 -7 9 732.53 39.70 6 -7 9 672.13 33.10 6 -7 9 600.04 34.00 7 6 -9 680.53 32.70 7 6 9 745.33 33.30 -7 -6 -9 734.03 36.40 -7 -6 9 679.73 18.80 -6 7 -9 757.42 34.70 -7 -6 11 734.33 48.80 6 -7 11 645.54 37.60 6 -7 11 533.35 35.80 7 6 -11 582.34 33.30 -7 -6 -11 615.24 34.70 7 6 11 670.23 34.30 6 -7 -11 650.93 17.10 -7 -6 11 579.44 18.40 -6 7 11 612.14 17.10 6 -7 11 625.94 16.70 -6 7 -11 640.84 34.20 6 -7 -13 511.75 15.70 -6 7 13 539.05 16.30 6 -7 13 555.94 16.30 6 -7 15 481.55 15.00 -6 7 15 486.15 15.30 7 6 17 654.23 13.60 -6 7 17 641.74 14.50 6 -7 -17 664.63 16.60 6 -7 17 690.23 16.60 -7 -6 17 694.83 16.30 -6 7 17 685.83 17.00 7 6 19 412.96 9.10 -6 7 19 418.16 9.70 6 -7 -19 421.56 11.30 6 -7 19 462.05 11.30 -6 7 19 449.16 11.70 -7 -6 -21 70.89 3.10 6 -7 -21 63.29 3.10 -6 7 21 73.29 3.30 7 -7 0 26.00 6.60 7 7 0 21.50 5.40 7 -7 -2 2171.78 51.69 7 -7 2 2180.78 63.49 -7 -7 2 2517.45 52.09 7 7 2 2395.46 55.19 7 7 -2 2317.87 52.49 7 -7 4 3246.78 57.19 7 -7 4 3450.95 86.69 -7 -7 4 3799.72 76.59 7 7 -4 3558.94 68.89 7 7 4 3551.84 71.79 -7 7 -4 3840.42 73.89 -7 -7 6 402.96 28.50 7 -7 6 397.96 30.10 7 -7 6 335.87 20.60 7 7 6 393.06 23.70 7 7 -6 396.46 23.40 -7 7 -6 402.36 24.10 -7 -7 8 289.97 27.80 7 -7 8 269.07 25.00 7 -7 8 210.78 19.00 -7 -7 -8 278.47 22.20 7 7 -8 254.67 20.00 7 7 8 278.47 20.60 -7 7 -8 278.47 21.30 -7 7 8 249.58 10.30 -7 -7 8 249.68 11.20 -7 -7 10 1487.65 68.49 7 -7 10 1394.96 57.29 7 -7 10 1072.29 48.70 7 7 10 1328.07 47.90 -7 -7 -10 1274.87 49.70 7 -7 -10 1331.07 24.80 7 7 -10 1191.08 47.00 -7 7 10 1272.77 25.10 -7 7 -10 1328.37 49.60 -7 -7 10 1145.39 26.20 7 -7 -12 1610.44 28.90 -7 7 12 1709.43 30.40 7 -7 -14 338.07 12.70 -7 7 14 359.26 13.30 -7 -7 14 344.27 12.30 7 -7 -16 319.47 11.70 -7 -7 16 314.87 11.20 7 7 18 979.90 15.30 7 -7 -18 1036.20 19.20 7 -7 -20 400.96 9.00 -7 7 20 430.86 9.70 8 -7 -1 499.45 27.60 8 -7 1 504.85 30.80 7 8 1 543.65 26.40 7 8 -1 529.55 25.60 8 -7 3 933.11 45.60 8 -7 -3 958.60 33.70 -7 -8 3 1085.39 37.60 7 8 -3 991.10 35.80 7 8 3 1014.70 38.00 -8 7 -3 1127.19 40.80 8 -7 5 659.13 18.20 8 -7 5 682.33 40.80 -7 -8 5 742.13 36.20 7 8 -5 668.23 31.10 7 8 5 731.63 33.20 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10.40 -9 -8 5 15.40 2.50 -9 -8 -5 12.30 3.20 9 8 5 19.20 6.70 9 8 -5 9.70 4.70 -9 -8 5 18.50 3.30 -8 9 -5 19.50 7.10 8 -9 7 121.79 8.20 8 -9 7 126.19 19.40 -9 -8 -7 123.79 8.20 -9 -8 7 108.39 16.30 9 8 -7 107.79 14.40 9 8 7 94.99 13.20 -9 -8 7 91.59 7.40 -8 9 7 111.99 7.00 -8 9 -7 96.19 14.00 -9 -8 -9 53.59 5.20 -9 -8 9 39.60 5.20 -8 9 9 51.79 5.10 -9 -8 -11 145.99 7.60 -9 -8 11 147.99 9.60 -8 9 11 136.79 8.30 -9 -8 13 158.68 9.00 -8 9 13 142.69 8.10 -8 9 15 61.79 5.00 -8 9 17 5.70 1.90 -8 9 19 48.70 3.00 9 -9 0 69.09 6.50 9 -9 0 50.29 10.40 -9 -9 0 61.09 5.70 9 9 0 53.29 10.00 -9 -9 0 57.59 5.50 9 -9 2 198.88 10.80 9 -9 -2 200.58 10.90 -9 -9 2 177.38 8.90 -9 -9 -2 191.18 10.60 9 -9 2 162.48 20.60 9 9 -2 186.18 18.10 9 9 2 178.38 18.20 -9 9 -2 166.48 18.10 -9 -9 2 189.48 9.80 9 -9 4 767.42 21.10 9 -9 -4 819.42 21.70 -9 -9 4 679.33 16.90 -9 -9 -4 729.03 21.10 9 -9 4 717.23 46.20 9 9 -4 743.53 36.60 9 9 4 754.92 37.70 -9 -9 4 700.23 19.50 -9 9 -4 851.61 41.00 9 -9 6 262.17 28.90 -9 -9 -6 225.48 11.40 9 9 -6 244.78 21.90 9 9 6 234.78 21.30 -9 -9 6 229.28 11.50 -9 9 6 226.68 9.50 -9 9 -6 251.77 23.00 -9 -9 -8 43.90 5.00 -9 -9 8 41.40 5.30 -9 9 8 43.50 4.70 -9 -9 -10 444.96 13.70 -9 -9 10 403.06 15.90 -9 9 10 415.46 14.20 -9 -9 -12 578.04 13.70 -9 -9 12 551.54 17.30 -9 9 12 565.54 16.20 -9 9 14 146.59 7.70 -9 9 16 44.70 3.80 -9 9 18 173.78 6.00 10 -9 -1 476.15 17.70 10 -9 1 480.35 17.70 -9 -10 1 422.16 14.90 10 -9 1 451.95 33.40 -9 -10 -1 463.65 16.40 9 10 1 491.55 31.00 9 10 -1 504.45 31.00 -10 9 -1 468.35 30.60 10 -9 3 944.91 24.80 -9 -10 3 915.31 21.00 10 -9 -3 1102.79 26.30 -9 -10 -3 909.41 24.20 10 -9 3 929.71 52.19 9 10 -3 1020.70 44.50 9 10 3 1039.40 45.60 -10 9 -3 1044.40 46.40 -9 -10 3 978.10 24.30 -9 -10 -5 581.24 18.90 -9 -10 5 563.04 15.20 -9 -10 5 613.74 19.40 -9 -10 -7 420.76 15.20 -10 9 7 396.96 13.00 -9 -10 -9 485.95 14.80 -10 9 9 453.25 14.60 -9 -10 9 436.56 16.90 -9 -10 -11 559.14 14.10 -9 -10 11 566.74 18.00 -10 9 11 573.54 16.40 -10 9 13 604.34 15.70 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8 16.50 6.60 -2 -10 8 21.10 8.10 -2 -10 8 36.70 8.80 10 -2 -8 24.60 3.30 2 10 -8 19.80 6.00 -10 2 8 22.50 3.40 -10 2 -8 16.80 5.80 -2 -10 8 20.00 3.20 -2 -10 -10 133.79 7.40 -2 -10 10 129.89 16.30 10 -2 10 143.29 16.90 -2 -10 10 110.19 17.80 10 -2 10 118.99 15.50 2 10 -10 100.49 14.00 10 -2 -10 133.89 8.20 -2 -10 10 128.49 8.50 -10 2 -10 125.39 15.50 -10 2 10 132.09 8.20 10 -2 -12 286.37 12.50 -2 -10 12 276.77 13.50 -10 2 12 279.97 12.50 10 -2 -14 145.89 9.10 -2 -10 14 141.99 10.20 -10 2 14 141.89 9.00 -2 -10 16 2.80 3.00 10 -2 -16 6.00 2.80 -10 2 16 6.00 2.70 10 -2 -18 47.30 4.40 -10 2 18 34.00 3.60 -2 -10 18 43.10 4.80 2 10 20 66.69 3.40 10 -2 -20 68.99 4.10 -10 2 20 75.99 3.70 -2 -10 20 70.29 4.30 -1 -10 1 755.42 32.00 1 10 1 810.92 28.00 1 10 -1 737.23 25.90 -10 1 -1 767.02 28.90 -1 -10 3 240.18 19.00 1 10 -3 247.58 15.40 1 10 3 246.08 15.60 -10 1 -3 247.78 17.20 -1 -10 5 115.59 13.30 -1 -10 5 98.99 13.30 1 10 -5 88.39 9.90 -10 1 -5 102.69 11.80 -1 -10 7 608.94 30.60 10 -1 7 616.34 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52.59 0 -10 4 2318.57 61.39 0 -10 4 2221.48 60.69 0 10 -4 2246.18 47.00 10 0 4 2400.26 53.09 -10 0 -4 2262.57 54.19 0 -10 6 763.62 37.00 0 -10 6 732.83 32.10 0 -10 6 734.13 37.00 10 0 6 803.02 32.10 0 10 -6 689.13 27.50 -10 0 -6 731.73 32.10 0 -10 8 320.17 11.10 0 -10 -8 343.07 11.70 0 -10 8 312.57 23.30 0 -10 8 328.07 27.10 0 10 -8 295.67 20.00 10 0 8 380.06 23.70 10 0 -8 346.97 12.20 -10 0 -8 344.07 23.70 -10 0 8 357.86 12.80 0 -10 8 345.17 12.70 0 -10 10 645.34 16.40 0 -10 10 679.33 37.70 10 0 10 660.33 35.90 0 -10 10 641.14 40.60 10 0 10 734.63 37.60 10 0 -10 671.83 18.20 0 -10 10 639.04 19.40 -10 0 -10 673.53 35.90 -10 0 10 625.84 18.30 10 0 -12 987.60 23.30 -10 0 12 1038.30 24.60 10 0 -14 427.46 15.20 0 -10 14 399.56 17.00 -10 0 14 410.56 15.30 10 0 -16 425.36 14.20 -10 0 16 436.96 14.60 0 -10 16 422.56 16.50 10 0 -18 561.04 14.50 -10 0 18 540.25 14.10 0 10 18 543.75 12.70 0 -10 18 575.14 16.30 0 10 20 261.57 7.00 10 0 -20 263.67 7.90 0 10 20 192.38 5.40 -10 0 20 202.88 5.80 0 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1197.48 29.40 1 -10 15 25.20 5.00 10 1 -15 24.30 4.00 -10 -1 15 31.30 4.50 10 1 -17 909.71 19.70 1 -10 17 901.01 22.30 -10 -1 17 923.61 20.30 -1 10 17 944.51 18.50 -1 10 19 1167.28 17.80 -10 -1 19 1188.98 18.20 -1 10 21 209.18 5.30 -10 -1 -21 205.48 5.40 1 -10 21 216.18 5.90 2 -10 0 864.81 32.90 10 2 0 874.01 31.60 -10 -2 0 935.51 30.90 2 -10 -2 1017.80 33.10 2 -10 2 1039.90 38.80 2 -10 2 1001.70 38.90 10 2 -2 1048.80 32.60 10 2 2 1006.50 35.70 -10 -2 -2 1124.19 36.10 -10 -2 2 1076.59 31.60 2 -10 4 1975.60 49.70 2 -10 4 2060.69 59.29 2 -10 4 1972.80 57.59 10 2 -4 1933.11 45.20 10 2 4 1994.90 52.49 -10 -2 -4 2095.49 52.89 2 -10 6 478.05 30.10 2 -10 6 477.25 26.20 2 -10 6 494.15 30.20 10 2 -6 461.25 22.40 10 2 6 541.45 27.60 -10 -2 -6 503.55 27.20 2 -10 8 161.18 8.00 2 -10 8 145.49 17.60 2 -10 8 134.09 15.50 2 -10 8 158.68 18.60 10 2 8 145.39 15.30 10 2 -8 135.89 13.20 10 2 -8 152.18 8.00 -10 -2 -8 166.48 17.00 -10 -2 8 136.59 8.00 2 -10 8 139.49 8.10 2 -10 10 615.44 37.50 2 -10 10 597.64 36.20 2 -10 10 580.84 37.50 10 2 -10 624.54 17.10 10 2 -10 521.95 28.00 2 -10 10 551.14 17.80 -10 -2 -10 676.63 36.20 -10 -2 10 608.54 18.20 10 2 -12 702.43 19.00 2 -10 12 700.33 21.40 10 2 -14 76.29 6.30 2 -10 14 77.79 7.50 -10 -2 14 85.69 7.20 10 2 -16 356.76 12.50 2 -10 16 367.16 14.40 10 2 -18 687.63 15.50 -10 -2 18 694.03 15.10 -2 10 18 721.93 14.90 2 -10 18 715.33 17.30 -2 10 20 288.87 7.20 10 2 -20 276.27 7.50 -2 10 20 265.47 6.70 2 -10 20 289.17 8.30 3 -10 -1 79.39 9.90 3 -10 1 77.19 10.60 10 3 1 87.49 10.50 10 3 -1 79.19 9.40 -10 -3 -1 88.19 9.90 3 -10 3 10.70 4.70 3 -10 -3 21.70 5.30 3 -10 3 27.60 6.40 3 -10 3 5.20 4.30 10 3 3 21.50 5.90 10 3 -3 13.70 4.10 -10 -3 -3 16.50 4.90 3 -10 5 18.70 6.60 3 -10 5 15.60 5.00 3 -10 5 20.90 7.30 10 3 5 21.80 6.00 10 3 -5 22.60 5.40 -10 -3 -5 20.10 5.80 3 -10 7 9.70 2.00 3 -10 7 7.90 2.10 3 -10 -7 9.80 2.40 3 -10 7 7.00 5.00 3 -10 7 8.50 4.30 3 -10 7 10.60 2.40 3 -10 7 2.50 4.60 10 3 -7 10.90 2.30 10 3 7 12.00 4.70 10 3 -7 7.00 3.50 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10 4 -6 36.20 7.30 10 4 -6 41.50 4.10 10 4 6 45.10 8.70 -10 -4 6 42.70 4.40 4 -10 6 43.60 4.20 -10 -4 -6 44.20 8.90 4 -10 8 5.00 1.90 4 -10 8 8.60 2.30 4 -10 8 3.10 3.40 4 -10 8 0.00 4.40 4 -10 8 7.70 5.80 10 4 -8 10.90 2.40 10 4 8 10.10 5.00 10 4 -8 9.70 4.50 -10 -4 8 6.20 2.20 -10 -4 -8 4.50 3.50 4 -10 10 24.20 8.00 4 -10 10 29.60 8.80 4 -10 10 25.50 8.80 10 4 10 23.00 6.90 10 4 -10 29.70 3.80 10 4 -10 15.50 5.80 -10 -4 10 24.10 4.00 -10 -4 -10 31.70 8.20 4 -10 10 29.20 4.10 10 4 -12 176.38 9.00 4 -10 12 180.68 10.20 10 4 -14 48.80 4.80 -10 -4 14 60.89 5.90 4 -10 14 47.80 5.50 10 4 -16 41.60 4.10 -10 -4 16 31.10 3.80 -4 10 16 38.70 4.10 4 -10 16 37.50 4.30 10 4 -18 15.50 2.20 -4 10 18 16.40 2.50 4 -10 18 19.60 2.70 -4 10 20 27.40 2.10 5 -10 -1 90.99 11.40 5 -10 1 98.79 12.90 10 5 1 101.09 12.00 10 5 -1 93.29 11.00 5 -10 3 325.07 12.20 5 -10 3 346.87 11.60 5 -10 3 333.57 20.00 5 -10 3 364.66 26.80 10 5 -3 328.77 20.40 10 5 3 366.86 23.50 -10 -5 3 345.57 11.60 -5 10 -3 370.36 22.40 5 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411.06 28.50 10 6 -2 407.86 23.80 10 6 2 384.56 24.40 -10 -6 2 368.36 12.20 -10 -6 -2 407.66 12.60 6 -10 -4 758.62 19.00 6 -10 4 891.31 20.10 6 -10 4 788.12 31.60 6 -10 4 901.61 46.20 10 6 -4 849.52 35.20 10 6 4 787.02 36.30 -10 -6 4 778.02 18.90 -6 10 -4 769.92 34.30 6 -10 -6 202.18 9.40 6 -10 6 246.78 10.60 -10 -6 6 245.68 23.20 6 -10 6 204.28 17.80 6 -10 6 254.67 26.30 10 6 -6 225.18 18.90 10 6 6 201.58 19.00 -10 -6 6 196.68 9.90 6 -10 8 26.70 3.80 6 -10 8 28.30 9.80 -10 -6 8 30.30 10.00 6 -10 8 12.60 5.60 10 6 8 26.70 7.30 10 6 -8 28.20 7.50 -10 -6 8 29.00 4.40 6 -10 8 34.70 3.90 -10 -6 10 238.28 12.00 6 -10 10 190.38 9.10 -6 10 12 408.86 13.80 6 -10 12 430.76 14.00 -6 10 14 126.29 7.40 6 -10 14 143.09 7.70 -10 -6 16 44.40 3.90 -6 10 16 41.60 4.00 6 -10 16 44.60 3.90 -6 10 18 245.38 7.90 7 -10 1 172.78 9.20 7 -10 -1 153.38 8.70 -10 -7 1 147.99 8.20 7 -10 -1 141.99 15.10 7 -10 1 149.39 17.40 10 7 1 157.68 16.10 10 7 -1 162.88 15.90 -10 -7 1 138.29 7.70 -10 -7 -1 167.28 8.40 7 -10 3 253.97 11.10 7 -10 -3 188.98 9.80 7 -10 3 251.87 24.60 -10 -7 3 179.68 8.50 10 7 -3 257.37 20.10 10 7 3 179.08 17.90 -10 -7 3 181.48 9.00 -7 10 -3 131.09 15.00 7 -10 -5 351.66 13.20 7 -10 5 446.26 14.90 7 -10 5 463.85 35.90 10 7 -5 435.26 27.20 10 7 5 343.47 24.90 -10 -7 5 332.27 12.90 -7 10 -5 324.77 24.00 7 -10 7 74.29 6.30 7 -10 7 72.49 15.40 10 7 -7 77.59 12.00 10 7 7 67.49 11.40 -10 -7 7 73.19 6.50 -7 10 7 78.29 6.00 -10 -7 9 85.29 7.40 -7 10 9 66.59 5.80 -10 -7 -11 293.07 10.70 -7 10 11 287.17 11.60 -10 -7 -13 209.08 7.90 -7 10 13 201.88 9.40 -10 -7 15 43.90 4.10 -7 10 15 34.30 3.80 -7 10 17 40.60 3.50 -7 10 19 48.40 2.90 8 -10 0 63.59 6.10 8 -10 0 55.49 10.80 -10 -8 0 56.59 5.50 10 8 0 52.89 10.10 -10 -8 0 57.09 5.30 8 -10 -2 289.87 12.80 8 -10 2 284.47 12.50 -10 -8 -2 291.07 13.10 8 -10 2 265.87 25.50 -10 -8 2 260.37 10.90 10 8 -2 281.27 22.10 10 8 2 284.57 22.80 -10 -8 2 268.37 11.30 8 -10 4 140.59 8.90 8 -10 -4 149.19 9.10 -10 -8 4 128.39 7.10 8 -10 4 137.59 20.10 -10 -8 -4 146.39 9.50 10 8 -4 113.99 14.40 10 8 4 142.49 16.50 -10 -8 4 139.59 8.50 -8 10 -4 91.79 13.40 8 -10 6 120.09 8.10 -10 -8 -6 136.49 9.00 8 -10 6 118.99 19.80 10 8 -6 127.49 15.60 10 8 6 90.29 13.40 -10 -8 6 96.89 7.50 -8 10 6 111.79 6.80 -10 -8 -8 14.60 3.20 -8 10 8 7.80 2.20 -10 -8 8 7.80 2.90 -10 -8 -10 80.59 6.00 -10 -8 10 87.59 7.60 -8 10 10 73.89 6.00 -10 -8 -12 111.19 6.10 -10 -8 12 100.79 7.60 -8 10 12 100.79 6.80 -10 -8 14 85.49 5.90 -8 10 14 73.79 5.30 -8 10 16 16.80 2.50 -8 10 18 86.39 4.10 9 -10 1 112.09 8.50 9 -10 -1 139.99 9.40 -10 -9 1 130.39 8.20 9 -10 1 114.99 16.50 -10 -9 -1 123.99 8.60 10 9 1 137.09 16.50 10 9 -1 115.29 15.10 -10 -9 1 127.89 8.40 9 -10 3 288.97 13.30 9 -10 -3 364.26 14.90 -10 -9 3 316.57 11.90 9 -10 3 282.17 28.50 -10 -9 -3 316.87 14.30 10 9 -3 308.17 24.20 10 9 3 344.97 26.10 -10 -9 3 339.27 13.50 -10 -9 -5 158.28 10.00 -10 -9 5 146.89 7.50 9 -10 -5 180.08 10.00 9 -10 5 156.58 9.70 -10 -9 5 140.69 9.10 -10 -9 -7 29.50 4.40 -10 -9 7 32.80 4.90 -9 10 7 25.80 3.50 -10 -9 -9 220.58 10.10 -10 -9 9 190.28 11.10 -9 10 9 199.58 9.60 -10 -9 -11 273.97 9.90 -10 -9 11 277.17 12.70 -9 10 11 261.27 10.80 -9 10 13 105.69 6.50 -10 -9 13 98.99 6.60 -10 -9 -15 15.00 1.80 -9 10 15 14.90 2.40 -9 10 17 115.19 4.90 -10 -10 0 281.17 12.60 10 -10 0 290.37 14.00 -10 -10 2 155.08 8.90 -10 -10 -2 178.78 10.60 10 -10 2 176.08 10.80 10 -10 -2 163.68 10.50 -10 -10 2 163.48 9.80 -10 -10 -4 221.58 12.00 10 -10 -4 246.68 12.20 -10 -10 4 207.58 9.60 -10 -10 4 234.58 12.00 -10 -10 -6 212.48 11.10 -10 -10 6 186.58 11.00 -10 -10 -8 315.97 12.40 -10 -10 8 292.87 13.90 -10 10 8 301.27 11.40 -10 -10 -10 272.47 10.20 -10 10 10 274.47 11.00 -10 -10 10 276.97 13.00 -10 -10 -12 143.59 6.20 -10 10 12 141.69 7.50 -10 -10 12 132.29 7.90 -10 -10 -14 82.39 4.30 -10 10 14 78.19 5.00 -10 10 16 131.29 5.40 -10 -11 -1 1111.59 26.30 -10 -11 1 998.80 23.80 -10 -11 -3 141.19 9.70 -10 -11 3 116.29 7.50 -10 -11 -5 303.17 13.50 -10 -11 5 218.58 9.40 -10 -11 -7 1033.10 23.40 -10 -11 7 942.41 25.70 -10 -11 -9 614.54 15.90 -11 10 9 586.24 15.50 -10 -11 -11 47.80 3.80 -11 10 11 41.20 4.10 -10 -11 -13 199.48 7.00 -11 10 13 205.78 7.90 -11 10 15 380.06 9.10 -9 -11 0 1326.37 28.30 -9 -11 -2 576.14 18.90 -9 -11 2 537.95 15.90 -9 -11 2 542.05 16.70 -9 -11 -4 123.29 8.90 -9 -11 4 104.59 6.80 -9 -11 -6 1236.78 27.00 -9 -11 6 1229.38 29.40 -9 -11 -8 1335.67 26.00 -11 9 8 1274.77 24.20 -9 -11 8 1273.77 30.00 -9 -11 -10 373.76 11.80 -11 9 10 369.66 12.80 -9 -11 -12 76.19 5.20 -11 9 12 71.99 5.50 -9 -11 -14 627.54 12.10 -11 9 14 660.33 14.70 -11 9 16 447.26 9.90 -8 -11 1 61.99 5.80 -8 -11 -1 54.59 5.90 11 -8 1 61.29 13.20 8 11 -1 62.49 11.40 8 11 1 68.89 11.70 -11 8 -1 65.39 11.70 11 -8 3 7.30 7.00 -8 -11 3 5.10 2.00 -8 -11 -3 1.80 2.50 -8 -11 3 6.90 1.90 -8 -11 -5 84.49 7.20 -8 -11 5 90.29 6.20 -8 -11 7 264.37 10.00 -8 -11 -7 265.27 11.80 11 -8 -7 282.37 11.20 -11 8 7 265.87 10.60 -8 -11 7 245.58 12.90 -8 -11 -9 131.69 7.60 11 -8 -9 118.29 7.30 -11 8 9 118.49 7.50 -8 -11 9 112.89 8.60 -8 -11 -11 19.20 2.70 -11 8 11 18.40 3.30 -8 -11 -13 217.28 8.30 11 -8 -13 201.58 8.50 -11 8 13 212.88 9.40 11 -8 -15 117.19 5.60 -11 8 15 135.29 6.60 -11 8 17 9.30 1.60 -7 -11 0 44.50 4.90 11 -7 0 43.60 10.50 7 11 0 59.19 10.90 -11 7 0 61.99 11.00 -7 -11 2 35.00 4.00 -7 -11 2 37.80 4.40 11 -7 2 59.49 13.50 -7 -11 -2 49.00 5.40 7 11 -2 47.10 9.60 11 -7 -2 38.20 4.10 7 11 2 40.20 9.20 -11 7 -2 44.10 9.50 -7 -11 4 104.49 6.80 -7 -11 -4 103.99 7.80 11 -7 4 119.89 19.10 7 11 -4 122.79 15.30 11 -7 -4 119.49 7.20 7 11 4 115.09 14.80 -11 7 -4 130.09 16.50 -7 -11 6 7.40 2.10 -7 -11 -6 5.80 2.30 11 -7 -6 7.20 2.20 -11 7 6 3.70 1.50 -7 -11 -8 21.40 3.50 11 -7 -8 28.10 3.80 -11 7 8 20.20 3.30 -7 -11 8 25.40 4.50 -7 -11 -10 76.69 5.50 11 -7 -10 74.79 6.00 -11 7 10 73.89 6.20 -7 -11 -12 109.79 6.60 11 -7 -12 116.09 7.30 -11 7 12 101.09 7.00 -7 -11 -14 15.50 2.20 11 -7 -14 15.70 2.70 -11 7 14 16.60 3.00 11 -7 -16 24.20 2.70 -11 7 16 26.90 3.10 -11 7 18 126.29 4.80 -6 -11 1 9.50 2.40 11 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214.88 16.50 -2 -11 3 82.49 5.70 -2 -11 -3 76.99 5.90 -2 -11 3 77.89 11.80 11 -2 3 82.59 5.90 2 11 -3 79.79 9.80 11 -2 -3 85.59 5.70 -11 2 -3 80.79 10.80 -2 -11 5 143.69 7.60 -2 -11 -5 125.29 7.00 -2 -11 -5 115.99 7.40 -2 -11 5 125.19 15.70 2 11 -5 120.09 12.70 11 -2 -5 147.59 7.60 -2 -11 5 142.99 7.50 -11 2 5 124.29 6.80 -11 2 -5 148.59 15.20 -2 -11 -7 106.39 6.30 -2 -11 -7 115.69 7.30 -2 -11 7 98.59 6.30 -2 -11 7 105.89 16.20 11 -2 -7 97.69 6.60 2 11 -7 87.19 11.90 -11 2 -7 108.49 13.70 -2 -11 7 98.89 6.60 -11 2 7 108.99 6.90 -2 -11 9 32.20 3.70 -2 -11 -9 33.00 4.00 11 -2 9 36.00 9.10 -2 -11 9 26.20 9.90 -2 -11 9 49.00 11.10 11 -2 -9 30.60 4.10 2 11 -9 26.80 7.60 -2 -11 9 30.60 4.40 -11 2 9 34.90 4.50 -11 2 -9 33.60 8.40 -2 -11 -11 17.30 2.90 -2 -11 11 8.80 3.10 11 -2 -11 11.90 3.10 -11 2 11 16.80 3.50 11 -2 -13 83.69 6.90 -11 2 13 94.79 7.40 -2 -11 13 83.39 7.60 11 -2 -15 147.79 8.70 -2 -11 15 133.09 9.30 -2 -11 17 7.00 2.70 11 -2 -17 6.20 2.10 -11 2 17 6.70 2.10 11 -2 -19 28.50 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3.40 -11 -2 -7 28.00 7.40 -11 -2 7 15.90 2.90 2 -11 9 217.18 10.10 2 -11 -9 203.08 8.80 2 -11 9 258.97 25.40 2 -11 9 214.48 21.70 2 -11 9 229.98 24.00 11 2 9 200.08 18.70 11 2 -9 209.38 9.90 -11 -2 9 199.28 10.30 -11 -2 -9 207.38 20.10 2 -11 9 194.38 10.30 11 2 -11 498.15 15.90 2 -11 11 480.45 17.30 11 2 -13 96.09 7.00 2 -11 13 94.99 8.00 2 -11 15 14.40 3.40 11 2 -15 17.80 3.30 11 2 -17 288.97 10.10 -11 -2 17 286.07 10.20 2 -11 17 294.57 11.20 -2 11 19 266.77 7.10 11 2 -19 259.17 7.50 -2 11 19 258.27 7.20 2 -11 19 278.67 8.40 3 -11 0 54.29 4.70 3 -11 0 56.49 9.40 11 3 0 56.49 9.00 3 -11 2 355.86 11.70 3 -11 -2 348.17 12.10 3 -11 2 341.27 12.20 3 -11 -2 376.56 21.80 3 -11 2 358.26 24.80 11 3 -2 338.97 20.60 11 3 2 352.56 22.80 -11 -3 2 357.36 11.30 3 -11 4 219.58 9.10 3 -11 -4 240.08 10.20 3 -11 4 208.48 9.60 3 -11 4 228.88 18.10 3 -11 4 210.58 20.40 3 -11 4 225.28 20.70 11 3 -4 205.28 15.90 11 3 -4 240.18 9.90 11 3 4 255.17 19.80 -11 -3 4 251.17 10.00 -11 -3 -4 247.58 19.40 3 -11 6 55.49 4.70 3 -11 -6 94.49 6.40 3 -11 6 65.69 5.50 3 -11 6 43.90 10.00 3 -11 6 61.29 10.50 3 -11 6 50.29 11.10 11 3 -6 56.89 8.80 11 3 -6 62.39 5.20 11 3 6 100.29 12.90 3 -11 6 63.19 5.40 -11 -3 6 103.29 6.80 -11 -3 -6 73.99 11.30 3 -11 8 32.20 3.80 3 -11 8 34.00 4.20 3 -11 -8 26.50 3.40 3 -11 8 20.80 7.40 3 -11 8 24.50 7.40 3 -11 8 30.30 9.60 11 3 8 27.40 7.50 11 3 -8 32.00 4.00 11 3 -8 33.60 7.30 -11 -3 8 25.40 3.80 3 -11 8 27.20 3.90 -11 -3 -8 35.10 8.40 11 3 -10 32.70 4.20 3 -11 10 30.30 4.50 -11 -3 10 25.90 4.20 11 3 -12 172.68 9.20 -11 -3 12 138.29 9.10 3 -11 12 159.28 9.80 11 3 -14 185.28 9.20 -11 -3 14 196.78 10.40 3 -11 14 180.18 10.20 3 -11 16 20.20 3.40 11 3 -16 22.30 3.20 -3 11 16 27.00 3.40 -11 -3 16 18.90 3.00 11 3 -18 98.99 5.00 -11 -3 18 96.89 4.90 -3 11 18 103.69 5.20 3 -11 18 99.79 5.50 4 -11 1 197.98 9.00 4 -11 -1 206.48 9.30 4 -11 1 191.78 9.50 4 -11 -1 211.48 9.90 4 -11 -1 190.98 16.60 4 -11 1 184.38 17.70 11 4 -1 184.18 15.80 11 4 1 211.08 9.20 11 4 -1 196.58 8.80 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287.37 12.50 11 4 -15 53.49 4.60 -11 -4 15 53.89 5.10 -4 11 15 57.79 5.00 4 -11 15 56.69 5.30 11 4 -17 115.69 5.70 -11 -4 17 112.79 5.90 -4 11 17 120.99 6.00 4 -11 17 117.49 6.30 -4 11 19 142.19 4.40 -4 11 19 172.68 5.70 5 -11 0 997.10 21.40 5 -11 0 999.70 23.00 5 -11 0 964.90 39.90 11 5 0 996.00 39.10 11 5 0 960.00 20.30 -11 -5 0 973.20 19.70 5 -11 2 563.64 15.90 5 -11 -2 563.34 16.20 5 -11 2 550.54 16.80 5 -11 -2 570.34 16.80 5 -11 -2 534.85 26.60 5 -11 2 598.14 34.80 11 5 -2 551.14 27.90 11 5 -2 541.65 14.90 11 5 2 580.14 30.70 -11 -5 2 571.54 15.30 -11 -5 -2 552.74 14.60 5 -11 4 10.40 2.50 5 -11 -4 24.60 3.60 5 -11 4 15.10 6.50 5 -11 4 9.10 2.70 5 -11 4 6.70 5.90 11 5 -4 7.50 2.10 11 5 4 21.80 6.60 11 5 -4 13.10 4.60 -11 -5 4 18.60 3.10 5 -11 6 584.24 16.50 5 -11 -6 640.24 17.10 5 -11 6 497.15 29.00 5 -11 6 618.34 41.00 11 5 -6 536.55 29.10 11 5 -6 594.44 16.20 11 5 6 639.74 33.90 -11 -5 6 613.04 17.50 5 -11 8 724.23 18.80 5 -11 8 750.42 46.40 5 -11 8 641.84 36.40 11 5 -8 633.04 32.80 11 5 -8 729.63 18.20 11 5 8 748.03 36.60 5 -11 8 663.63 17.40 -11 -5 8 730.43 20.40 5 -11 10 124.89 7.70 11 5 -10 122.39 7.40 -11 -5 10 115.49 8.40 5 -11 10 120.09 7.80 11 5 -12 233.98 10.10 -11 -5 12 236.18 11.70 5 -11 12 235.18 10.80 -11 -5 -14 468.75 11.30 11 5 -14 482.85 13.60 -11 -5 14 492.95 15.80 5 -11 14 471.05 14.50 -5 11 14 501.45 14.20 -11 -5 16 247.58 9.30 -5 11 16 260.67 9.20 5 -11 16 256.37 9.30 -5 11 18 21.70 1.80 -5 11 18 26.20 2.60 6 -11 -1 649.43 17.80 6 -11 1 648.74 17.60 6 -11 -1 626.64 31.70 6 -11 1 634.34 35.70 11 6 -1 614.74 31.30 11 6 1 650.83 33.00 -11 -6 1 619.14 16.30 -11 -6 -1 648.44 16.40 6 -11 3 722.93 18.60 6 -11 -3 765.92 19.70 6 -11 3 700.53 40.90 -11 -6 3 711.23 17.30 11 6 -3 698.33 33.10 11 6 3 760.62 36.80 -11 -6 3 715.53 18.20 -11 -6 -3 690.83 17.40 6 -11 -5 683.73 18.40 6 -11 5 619.44 17.60 6 -11 5 615.04 41.70 11 6 -5 577.74 30.90 11 6 5 655.93 34.30 -11 -6 5 673.43 18.50 6 -11 -7 968.40 21.00 6 -11 7 882.61 21.30 6 -11 7 1008.60 54.89 11 6 -7 868.81 39.30 11 6 7 876.21 39.90 -11 -6 7 879.81 22.50 6 -11 9 534.35 16.30 -11 -6 9 596.44 18.80 6 -11 11 677.63 17.50 -11 -6 11 625.34 19.50 -6 11 11 674.83 17.60 -11 -6 -13 588.24 13.40 -11 -6 13 619.94 18.40 6 -11 13 570.34 15.40 -6 11 13 592.84 15.70 6 -11 15 401.16 11.40 -11 -6 15 397.76 12.50 -6 11 15 398.36 11.80 -6 11 17 183.58 6.80 -6 11 19 253.17 6.10 7 -11 0 18.80 3.50 -11 -7 0 22.90 3.80 7 -11 0 7.00 4.20 11 7 0 22.40 7.00 -11 -7 0 21.50 3.30 7 -11 -2 302.87 12.80 7 -11 2 279.07 12.20 7 -11 2 291.97 26.30 -11 -7 2 292.47 11.50 11 7 -2 279.67 21.80 11 7 2 283.57 22.80 -11 -7 2 274.37 11.20 -11 -7 -2 276.67 11.20 7 -11 -4 485.35 16.10 7 -11 4 473.85 15.80 7 -11 4 495.75 37.40 -11 -7 4 454.65 13.30 11 7 -4 471.15 28.50 11 7 4 484.55 29.90 -11 -7 4 476.65 15.50 7 -11 -6 239.08 10.80 7 -11 6 232.98 11.10 -11 -7 6 212.48 10.90 -7 11 6 230.38 9.90 7 -11 8 34.40 4.80 -11 -7 8 33.20 4.70 -7 11 8 41.90 4.60 -11 -7 10 361.06 14.90 -7 11 10 375.36 13.20 -11 -7 -12 328.97 10.50 -7 11 12 316.17 11.60 -11 -7 14 99.99 6.60 -7 11 14 91.29 5.80 -7 11 16 21.00 2.60 -7 11 18 125.89 4.70 8 -11 1 36.00 4.90 8 -11 -1 57.39 6.10 8 -11 1 38.10 10.10 -11 -8 1 47.90 5.20 -11 -8 -1 50.49 5.80 11 8 -1 46.10 9.80 11 8 1 58.09 10.80 -11 -8 -1 36.70 4.40 -11 -8 1 51.49 5.20 8 -11 3 73.69 14.70 -11 -8 3 72.79 5.70 -11 -8 -3 77.89 7.10 8 -11 3 61.99 6.20 8 -11 -3 79.29 7.00 -11 -8 3 69.09 6.00 -11 -8 -5 8.50 3.20 8 -11 -5 4.20 2.20 8 -11 5 7.30 3.00 -11 -8 5 2.40 2.10 -11 -8 -7 27.00 4.20 8 -11 7 38.30 5.20 -11 -8 7 29.30 4.40 -8 11 7 29.40 3.70 -11 -8 -9 71.29 5.90 -11 -8 9 53.59 6.00 -8 11 9 66.69 5.60 -11 -8 -11 34.60 3.70 -11 -8 11 32.10 4.60 -8 11 11 31.50 3.90 -11 -8 -13 24.20 2.50 -11 -8 13 25.30 3.60 -8 11 13 23.50 3.20 -8 11 15 4.40 1.60 -8 11 17 32.80 2.60 -11 -9 0 22.50 3.90 9 -11 0 22.20 4.40 -11 -9 2 11.50 2.80 -11 -9 -2 9.80 3.20 9 -11 2 12.30 3.50 9 -11 -2 15.70 3.70 -11 -9 2 11.10 3.00 -11 -9 -4 24.30 4.50 -11 -9 4 20.60 3.10 9 -11 4 32.30 5.10 9 -11 -4 24.00 4.30 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38.60 3.70 -11 -11 -12 67.39 3.50 -11 -11 -12 72.29 4.40 -11 11 12 70.99 4.50 -11 -11 -14 21.80 1.80 -11 11 14 21.70 2.10 -11 -12 -1 65.19 6.60 -11 -12 1 41.00 5.10 -11 -12 1 35.60 4.20 -11 -12 -1 59.09 5.90 -11 -12 3 178.68 8.90 -11 -12 -3 209.78 11.20 -11 -12 -5 79.69 6.70 -11 -12 5 81.99 5.50 -11 -12 -7 1.10 2.10 -11 -12 -9 78.59 5.50 -11 -12 -9 75.59 4.90 -11 -12 -11 114.99 4.60 -11 -12 -11 117.59 5.50 -11 -12 -13 9.20 1.20 -10 -12 0 503.45 16.50 -10 -12 0 551.84 18.10 -10 -12 -2 520.15 17.90 -10 -12 2 475.95 15.70 -10 -12 2 474.65 14.60 -10 -12 -4 297.67 13.50 -10 -12 4 274.77 11.00 -10 -12 -6 468.35 15.60 -10 -12 6 377.96 11.90 -10 -12 -8 569.34 15.50 -10 -12 -10 310.97 9.60 -10 -12 -10 329.27 11.10 -12 10 10 302.27 10.10 -10 -12 -12 228.98 7.70 -12 10 12 229.98 8.00 -12 10 14 192.68 6.10 -9 -12 1 798.82 21.40 -9 -12 -1 914.31 23.80 -9 -12 -1 874.21 23.00 -9 -12 1 786.72 20.20 -9 -12 3 518.65 15.90 -9 -12 -3 553.04 18.60 -9 -12 -5 677.63 20.00 -9 -12 5 578.34 15.90 -9 -12 7 897.01 18.60 -9 -12 -7 1090.39 23.60 -9 -12 -9 674.43 16.40 -12 9 9 627.54 16.00 -9 -12 -11 197.48 8.40 -9 -12 -11 192.28 7.00 -12 9 11 198.48 8.70 -9 -12 -13 420.76 10.10 -12 9 13 420.16 11.40 -12 9 15 378.36 8.80 -8 -12 0 75.09 6.50 -8 -12 0 76.09 6.80 -8 -12 -2 279.47 13.10 -8 -12 2 293.67 11.70 -8 -12 2 281.47 12.10 -8 -12 4 597.84 16.80 -8 -12 -4 554.04 18.50 -8 -12 6 329.67 11.80 -8 -12 -6 341.97 13.80 12 -8 -6 343.57 12.20 -8 -12 -8 150.78 8.40 12 -8 -8 140.39 7.80 -12 8 8 137.69 7.70 -8 -12 -10 280.77 9.80 -8 -12 -10 286.37 11.40 12 -8 -10 260.37 10.40 -12 8 10 258.97 10.70 -8 -12 -12 356.76 10.90 -12 8 12 349.87 11.80 -8 -12 -14 114.49 4.80 12 -8 -14 100.19 5.10 -12 8 14 117.39 6.10 -12 8 16 18.90 2.10 -7 -12 1 63.79 6.00 -7 -12 -1 87.59 7.20 -7 -12 1 60.99 5.60 -7 -12 -1 88.59 7.20 12 -7 -1 70.19 5.70 -7 -12 3 86.29 6.50 -7 -12 3 86.79 6.20 12 -7 -3 102.69 6.80 -7 -12 -5 237.38 11.70 -7 -12 5 274.17 11.00 -7 -12 7 120.79 7.00 -7 -12 -7 119.89 7.90 12 -7 -7 137.69 8.00 -12 7 7 125.29 7.30 -7 -12 -9 128.99 7.30 -7 -12 -9 137.09 8.50 12 -7 -9 145.09 8.20 -12 7 9 122.29 7.60 -7 -12 -11 205.88 9.30 12 -7 -11 193.78 9.20 -12 7 11 199.18 9.70 -7 -12 -13 49.60 3.90 12 -7 -13 48.50 4.30 -12 7 13 55.39 4.80 12 -7 -15 63.29 4.20 -12 7 15 60.89 4.40 -12 7 17 113.39 4.60 -6 -12 0 1.50 1.90 12 -6 0 5.90 4.60 -6 -12 0 1.10 2.00 12 -6 0 1.90 1.60 6 12 0 3.50 3.40 -12 6 0 1.60 2.80 -6 -12 2 127.69 7.90 -6 -12 2 124.99 7.60 -6 -12 -2 133.79 8.80 -6 -12 -2 130.59 8.80 12 -6 2 168.88 21.80 6 12 -2 130.89 15.70 12 -6 -2 137.29 7.90 6 12 2 130.29 15.90 -12 6 -2 135.59 15.90 -6 -12 -4 264.17 12.10 -6 -12 4 237.48 9.80 -6 -12 -4 270.67 12.90 -6 -12 4 235.08 10.40 6 12 -4 242.58 21.40 12 -6 -4 255.37 10.80 6 12 4 241.98 21.60 -6 -12 -6 77.19 6.50 -6 -12 6 58.49 5.20 -6 -12 -6 77.89 7.00 12 -6 -6 81.49 6.20 -12 6 6 85.09 5.80 -6 -12 8 26.40 3.40 -6 -12 -8 24.30 3.60 -6 -12 -8 29.00 4.40 12 -6 -8 30.40 4.10 -12 6 8 29.30 3.90 -6 -12 -10 165.88 7.60 -6 -12 -10 169.18 9.00 12 -6 -10 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3 180.58 9.10 1 -12 3 166.18 18.20 12 1 -3 199.68 9.20 -12 -1 3 172.78 8.00 -12 -1 -3 182.68 16.70 1 -12 -5 63.89 5.30 1 -12 5 96.89 6.20 1 -12 -5 65.19 5.80 1 -12 5 96.59 6.70 1 -12 5 95.39 14.80 12 1 -5 98.79 6.60 -12 -1 5 68.19 5.40 -12 -1 -5 96.69 12.80 1 -12 7 17.90 2.80 1 -12 -7 6.90 2.30 1 -12 7 21.00 3.50 1 -12 7 13.30 6.80 1 -12 7 46.20 11.30 12 1 -7 16.30 3.00 1 -12 7 31.70 5.20 -12 -1 7 5.80 2.20 -12 -1 -7 22.40 7.00 1 -12 9 64.89 5.80 1 -12 -9 91.39 6.30 12 1 -9 65.99 5.90 1 -12 9 59.19 6.00 -12 -1 9 86.29 7.00 12 1 -11 40.50 4.90 1 -12 11 38.20 5.30 1 -12 13 19.90 4.20 12 1 -13 22.10 3.70 -12 -1 13 29.30 4.50 1 -12 15 34.60 4.70 12 1 -15 33.10 4.00 -12 -1 15 40.10 4.60 12 1 -17 32.20 3.40 -12 -1 17 27.00 3.20 -1 12 17 30.30 3.00 -1 12 19 4.90 1.10 12 1 -19 6.50 1.30 -1 12 19 6.80 1.20 2 -12 0 70.69 5.60 2 -12 0 60.19 5.40 12 2 0 64.09 5.30 12 2 0 64.19 9.70 -12 -2 0 61.69 4.60 2 -12 2 123.69 7.30 2 -12 -2 129.69 7.70 2 -12 2 114.29 7.30 2 -12 -2 128.19 7.70 2 -12 2 168.68 18.20 12 2 -2 127.69 7.30 12 2 2 141.99 14.40 -12 -2 2 121.39 6.70 -12 -2 -2 151.48 14.90 2 -12 4 85.69 5.90 2 -12 -4 97.09 6.80 2 -12 4 83.09 6.40 2 -12 -4 100.09 6.60 2 -12 4 109.19 16.20 2 -12 4 87.79 13.80 12 2 -4 92.09 6.40 12 2 4 100.19 12.60 -12 -2 4 101.89 6.40 -12 -2 -4 87.29 12.00 2 -12 -6 9.40 2.50 2 -12 6 16.90 2.80 2 -12 6 20.40 7.60 2 -12 6 51.49 10.90 2 -12 6 59.39 13.50 2 -12 6 17.80 3.20 12 2 -6 16.20 3.00 12 2 6 6.50 4.10 -12 -2 6 8.90 2.40 -12 -2 -6 11.20 5.00 2 -12 8 18.90 2.80 2 -12 -8 20.10 3.20 2 -12 8 30.60 9.70 2 -12 8 16.20 3.30 12 2 -8 17.40 3.30 2 -12 8 28.90 5.00 -12 -2 8 18.50 3.50 -12 -2 -8 11.10 5.70 2 -12 10 22.10 4.40 12 2 -10 23.60 3.80 -12 -2 10 18.30 3.60 12 2 -12 46.90 5.00 2 -12 12 48.00 5.90 2 -12 14 17.30 3.90 12 2 -14 20.40 3.30 -12 -2 14 16.20 3.40 12 2 -16 37.80 3.80 -12 -2 16 45.20 4.30 2 -12 16 43.10 5.00 -2 12 16 36.50 3.60 12 2 -18 88.09 4.50 -12 -2 18 86.39 4.40 -2 12 18 92.79 4.50 3 -12 1 169.58 8.60 3 -12 -1 159.18 8.50 3 -12 1 170.48 9.10 3 -12 -1 158.28 8.70 3 -12 1 181.18 18.30 12 3 -1 171.18 15.70 12 3 1 169.58 8.60 12 3 -1 175.88 8.70 12 3 1 150.88 15.30 -12 -3 -1 162.58 7.50 -12 -3 1 171.28 8.00 3 -12 3 557.04 15.50 3 -12 -3 576.74 16.50 3 -12 3 512.65 16.00 3 -12 -3 563.14 16.30 3 -12 3 543.95 33.50 12 3 -3 506.45 26.30 12 3 -3 574.84 15.90 12 3 3 597.84 30.70 -12 -3 3 586.34 15.50 -12 -3 -3 551.64 14.10 3 -12 5 399.46 13.10 3 -12 -5 460.15 14.70 3 -12 5 404.86 14.20 3 -12 5 392.36 30.70 3 -12 5 402.26 29.80 12 3 -5 422.56 13.90 12 3 5 476.25 28.10 -12 -3 5 478.95 14.70 3 -12 7 22.30 3.30 3 -12 -7 13.90 2.70 3 -12 7 21.30 3.80 3 -12 7 20.00 8.00 3 -12 7 37.50 9.80 3 -12 7 29.80 10.20 12 3 7 16.90 6.00 12 3 -7 25.30 3.70 -12 -3 7 15.70 3.00 -12 -3 -7 25.70 7.70 3 -12 -9 227.38 9.50 3 -12 9 239.28 10.20 12 3 -9 224.88 10.40 3 -12 9 206.18 10.90 -12 -3 9 213.48 10.80 12 3 -11 596.54 17.20 -12 -3 11 634.04 18.80 12 3 -13 223.68 10.10 -12 -3 13 241.98 11.40 3 -12 13 218.18 11.10 12 3 -15 25.80 3.30 3 -12 15 34.60 4.80 -3 12 15 22.70 3.20 -12 -3 15 22.80 3.40 12 3 -17 249.68 8.10 -12 -3 17 240.08 8.30 -3 12 17 262.67 8.20 -3 12 19 263.07 6.20 4 -12 0 1111.09 23.40 4 -12 0 1107.79 24.50 12 4 0 1164.08 23.30 12 4 0 1092.69 41.50 -12 -4 0 1121.69 21.40 4 -12 2 1116.09 22.90 4 -12 -2 1089.59 23.50 4 -12 2 1099.59 24.40 4 -12 -2 1114.19 24.10 4 -12 2 1040.40 46.10 12 4 -2 1111.59 40.90 12 4 -2 1123.19 22.90 12 4 2 1042.50 41.60 -12 -4 2 1129.09 22.10 -12 -4 -2 1103.99 21.00 4 -12 4 806.02 19.30 4 -12 -4 805.62 20.10 4 -12 4 791.32 20.60 4 -12 4 810.42 43.80 12 4 -4 742.93 33.00 12 4 -4 857.81 19.80 12 4 4 789.52 36.60 -12 -4 4 811.52 19.50 4 -12 6 468.75 14.80 4 -12 6 453.05 15.60 4 -12 -6 494.25 15.30 4 -12 6 415.96 27.70 4 -12 6 480.95 35.70 12 4 -6 377.36 24.10 12 4 -6 496.85 15.20 12 4 6 456.95 28.00 -12 -4 6 463.45 15.20 4 -12 -8 450.45 13.90 4 -12 8 442.06 14.50 12 4 -8 436.36 14.40 -12 -4 8 446.26 15.50 12 4 -10 426.46 14.20 4 -12 10 419.26 15.00 -12 -4 10 467.05 16.20 12 4 -12 510.45 15.10 4 -12 12 511.25 16.50 12 4 -14 310.47 10.80 4 -12 14 311.97 11.90 -12 -4 14 340.17 12.60 -4 12 14 308.47 10.80 12 4 -16 436.16 11.20 -12 -4 16 441.46 12.30 -4 12 16 440.76 11.50 -4 12 18 342.17 7.10 -4 12 18 403.76 8.90 5 -12 1 2417.26 36.70 5 -12 -1 2487.45 37.60 5 -12 1 2542.05 40.00 5 -12 -1 2515.85 39.40 5 -12 -1 2263.67 61.09 5 -12 1 2385.16 69.19 12 5 -1 2363.86 63.39 12 5 -1 2518.95 36.00 12 5 1 2373.96 64.69 -12 -5 -1 2533.85 34.60 -12 -5 1 2478.85 34.80 5 -12 3 460.25 14.90 5 -12 -3 456.35 15.30 5 -12 3 464.65 16.30 5 -12 -3 473.85 15.50 5 -12 3 470.65 33.20 -12 -5 3 465.55 13.60 12 5 -3 425.26 25.80 12 5 -3 490.45 14.80 12 5 3 446.06 27.90 -12 -5 3 458.05 14.40 -12 -5 -3 492.75 14.30 5 -12 5 246.78 10.90 5 -12 -5 254.57 11.20 5 -12 5 249.18 25.90 12 5 -5 228.38 19.10 12 5 -5 263.87 10.80 12 5 5 234.58 20.70 -12 -5 5 247.98 11.10 5 -12 -7 2137.09 32.80 5 -12 7 1864.21 32.20 12 5 -7 1894.51 31.30 -12 -5 7 2098.49 35.00 5 -12 9 1125.09 23.80 12 5 -9 1167.88 23.70 -12 -5 9 1166.18 26.10 12 5 -11 31.20 3.90 -12 -5 11 54.59 5.80 12 5 -13 718.93 16.70 -5 12 13 717.43 16.80 -12 -5 15 1120.09 21.40 -5 12 15 1148.19 19.70 -5 12 17 331.47 7.10 -12 -5 17 355.56 8.50 6 -12 0 1652.93 30.70 12 6 0 1624.74 54.09 -12 -6 0 1653.53 28.20 6 -12 2 826.92 21.00 6 -12 -2 812.92 21.10 6 -12 2 781.62 42.50 -12 -6 2 848.02 19.90 12 6 -2 825.42 37.70 12 6 2 816.32 38.70 -12 -6 2 788.92 19.30 -12 -6 -2 811.92 19.30 6 -12 4 166.78 9.30 6 -12 -4 225.18 10.90 6 -12 4 153.78 21.20 12 6 -4 160.48 16.70 12 6 4 245.28 21.20 -12 -6 4 215.58 10.30 6 -12 -6 942.21 21.80 6 -12 6 890.31 21.70 -12 -6 6 912.21 22.50 6 -12 8 1367.86 27.40 -12 -6 8 1572.94 30.60 -12 -6 10 183.38 10.40 -6 12 10 154.58 8.40 -12 -6 -12 264.27 9.30 -12 -6 12 284.17 12.20 -6 12 12 256.77 10.20 -12 -6 -14 735.03 13.20 -12 -6 14 772.32 18.20 -6 12 14 779.22 16.40 -12 -6 16 469.95 11.00 -6 12 16 469.15 10.90 -6 12 18 93.39 3.80 -12 -7 1 80.79 6.50 -12 -7 -1 74.79 6.80 7 -12 1 44.20 10.50 7 -12 1 56.89 5.90 7 -12 -1 75.69 6.90 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4 -5 140.89 8.20 -13 -4 5 118.99 7.80 4 -13 -7 163.98 8.70 4 -13 7 163.78 9.00 13 4 -7 156.88 8.70 -13 -4 7 149.59 8.90 4 -13 9 239.88 10.50 13 4 -9 231.08 10.40 -13 -4 9 233.08 11.30 13 4 -11 89.39 6.30 -13 -4 11 115.69 7.90 13 4 -13 61.99 4.90 -4 13 13 63.59 4.90 13 4 -15 106.29 5.40 -13 -4 15 119.89 6.50 -4 13 15 111.19 5.70 -13 -4 17 165.98 5.50 -4 13 17 196.38 6.20 5 -13 0 777.52 20.70 5 -13 0 800.72 22.10 -13 -5 0 783.62 18.60 5 -13 2 313.97 12.60 5 -13 -2 303.87 12.90 5 -13 2 319.67 14.00 5 -13 -2 326.17 13.50 13 5 -2 305.67 12.00 -13 -5 2 292.97 11.50 -13 -5 -2 323.67 11.70 5 -13 4 42.30 4.80 5 -13 -4 42.90 5.00 13 5 -4 43.80 4.70 -13 -5 4 45.40 5.00 5 -13 -6 457.85 15.00 5 -13 6 426.66 14.90 13 5 -6 448.86 14.50 -13 -5 6 439.36 15.20 5 -13 -8 606.54 16.10 5 -13 8 544.75 16.60 13 5 -8 558.04 16.00 -13 -5 8 615.44 18.30 13 5 -10 101.59 6.60 -13 -5 10 113.49 8.00 13 5 -12 46.00 4.20 -13 -5 12 59.69 5.60 -5 13 12 48.90 4.40 -13 -5 -14 186.08 6.20 -5 13 14 198.68 7.70 -13 -5 16 255.67 7.70 -5 13 16 254.17 7.50 -13 -6 1 389.86 13.80 6 -13 1 349.07 13.90 6 -13 -1 354.06 14.00 -13 -6 1 335.47 12.60 -13 -6 -1 355.96 12.80 -13 -6 3 6.70 2.00 6 -13 -3 7.50 2.70 -13 -6 3 6.10 2.30 6 -13 -5 187.58 10.00 6 -13 5 168.48 9.50 -13 -6 5 169.18 9.30 6 -13 -7 282.97 11.40 6 -13 7 231.98 11.10 -13 -6 7 287.67 12.40 -6 13 7 251.27 10.50 -13 -6 9 93.39 7.30 -6 13 9 93.79 6.40 -6 13 11 3.80 1.90 -13 -6 11 1.60 2.30 -13 -6 -13 31.60 2.90 -13 -6 13 22.00 3.40 -6 13 13 31.70 3.50 -13 -6 15 203.28 7.50 -6 13 15 192.78 6.80 -6 13 17 111.59 4.00 -13 -7 0 142.79 8.80 7 -13 0 134.99 9.10 -13 -7 0 125.29 7.80 -13 -7 2 53.69 5.10 -13 -7 -2 59.89 6.20 7 -13 -2 55.99 6.00 7 -13 2 47.40 5.60 -13 -7 2 53.89 5.40 7 -13 -4 30.20 4.50 7 -13 4 32.70 4.70 -13 -7 4 27.80 4.10 7 -13 -6 132.19 8.20 7 -13 6 107.69 7.80 -13 -7 6 123.49 8.30 -13 -7 -8 247.98 10.70 7 -13 8 218.38 10.60 -13 -7 8 213.48 10.90 -7 13 8 225.58 9.60 -13 -7 -10 84.89 5.60 -13 -7 10 68.99 6.20 -7 13 10 84.39 5.80 -13 -7 -12 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80.59 6.70 -10 -14 -6 251.27 9.90 -10 -14 -6 252.67 10.60 -10 -14 -8 339.77 9.80 -10 -14 -8 363.96 11.30 -10 -14 -10 155.18 5.00 -10 -14 -10 186.28 6.70 -9 -14 -1 176.68 10.30 -9 -14 1 150.98 8.40 -9 -14 -1 149.49 9.00 -9 -14 1 160.78 9.40 -9 -14 -3 20.60 4.00 -9 -14 3 8.60 2.60 -9 -14 -3 15.50 3.60 -9 -14 5 34.60 4.00 -9 -14 -5 45.40 5.00 -9 -14 -5 42.70 5.20 -9 -14 -7 30.40 3.60 -9 -14 -7 31.50 4.30 -9 -14 7 19.00 2.50 -9 -14 -9 52.89 4.50 -9 -14 -9 48.30 3.60 -9 -14 -11 23.50 2.50 -8 -14 0 37.90 5.20 -8 -14 0 36.60 4.70 -8 -14 -2 42.40 5.50 -8 -14 2 28.80 3.90 -8 -14 -2 36.90 5.00 -8 -14 2 31.90 4.50 -8 -14 -4 36.70 5.00 -8 -14 4 38.30 4.50 -8 -14 -4 37.70 5.30 14 -8 -4 31.80 3.70 -8 -14 6 53.19 4.70 -8 -14 -6 87.09 6.50 -8 -14 -6 76.79 6.90 14 -8 -6 54.39 4.70 -8 -14 -8 7.30 2.60 -8 -14 -8 9.80 2.20 14 -8 -8 7.70 2.00 -8 -14 -10 52.09 3.50 -8 -14 -10 52.29 4.30 14 -8 -10 43.50 3.70 -14 8 10 49.10 3.80 -8 -14 -12 55.29 3.50 14 -8 -12 49.70 3.30 -14 8 12 53.09 3.60 -7 -14 -1 139.49 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5 13 3.82 5.45 0 7 13 -2.15 7.35 0 9 13 5.02 -0.09 1 14 13 -3.13 -1.31 1 10 13 2.00 1.02 1 8 13 -4.56 6.13 1 6 13 -3.06 1.39 1 4 13 4.30 -3.70 1 2 13 0.41 -6.73 -1 2 13 -6.47 5.25 -1 4 13 -4.25 5.63 -1 6 13 2.48 -1.32 -1 8 13 4.79 0.19 -1 12 13 0.23 -1.76 -1 14 13 1.07 -0.84 2 13 13 -4.34 0.20 2 11 13 0.76 1.45 2 9 13 -5.38 -1.58 2 7 13 -6.88 0.93 2 5 13 0.09 -3.85 2 3 13 0.24 -0.05 -2 3 13 -6.39 2.99 -2 5 13 4.83 -6.94 -2 7 13 0.21 -10.13 -2 13 13 0.12 -1.70 3 12 13 -0.08 -1.48 3 10 13 -1.85 -1.16 3 8 13 -1.36 -1.69 3 6 13 -1.79 -0.69 3 4 13 -1.56 1.12 -3 4 13 0.12 -7.12 -3 6 13 0.16 -8.85 -3 8 13 -4.18 1.70 -3 10 13 0.62 6.75 -3 12 13 -0.24 -2.71 4 13 13 -0.68 -1.20 4 11 13 -2.48 2.35 4 9 13 -1.59 -0.53 4 7 13 1.05 3.84 4 5 13 -4.21 -3.05 -4 5 13 0.65 3.97 -4 7 13 -5.04 1.41 5 12 13 -3.27 1.05 5 10 13 -0.87 5.31 5 8 13 3.12 -2.19 5 6 13 0.74 -2.58 -5 6 13 -1.90 9.48 -5 8 13 -3.27 -0.91 -5 10 13 1.68 0.75 6 11 13 -3.83 2.27 6 9 13 2.10 -3.93 6 7 13 -0.45 -7.09 -6 7 13 -1.47 2.54 -6 9 13 -1.69 -5.55 -6 11 13 -3.15 0.81 7 12 13 -2.14 -0.69 7 10 13 -0.87 -2.24 -7 8 13 -0.66 -1.86 -7 12 13 -1.15 -0.69 8 11 13 -1.79 -1.16 8 9 13 -1.43 -2.21 7 8 13 1.73 -6.59 -8 9 13 -0.54 -1.45 -8 11 13 -0.06 1.19 9 10 13 -3.07 0.03 -4 9 13 -0.82 3.32 -2 9 13 0.77 3.71 -9 10 13 0.30 2.12 -7 10 13 -2.41 0.21 -1 10 13 1.66 -0.07 -4 11 13 2.54 -2.39 -2 11 13 -2.93 -0.40 0 11 13 2.57 -1.48 -5 12 13 -0.19 -0.01 1 12 13 0.23 1.94 -4 13 13 -0.32 -0.21 0 13 13 0.66 -1.42 0 0 14 -10.25 0.13 0 2 14 0.15 2.49 0 4 14 -2.06 -6.35 0 6 14 -6.56 -4.98 0 8 14 -3.69 -2.39 0 10 14 -3.50 2.34 0 12 14 -1.96 -0.41 1 13 14 1.12 -0.22 1 11 14 -3.15 -3.59 1 9 14 -1.90 -4.82 1 7 14 1.77 -6.96 1 5 14 -3.93 -3.48 1 3 14 2.02 3.50 1 1 14 -5.65 7.32 -1 3 14 1.84 -5.51 -1 5 14 -6.77 -5.37 -1 7 14 -2.08 5.53 -1 9 14 -1.40 2.15 -1 13 14 -0.10 0.92 2 12 14 -0.55 -0.37 2 10 14 0.57 -1.44 2 8 14 5.49 -3.86 2 6 14 0.79 1.84 2 4 14 -0.23 -2.21 2 2 14 3.00 6.74 -2 4 14 1.41 1.21 -2 6 14 -0.51 9.15 -2 8 14 2.36 3.51 -2 10 14 -1.05 -4.87 -2 12 14 0.09 2.17 3 13 14 0.43 1.75 3 11 14 1.53 -0.06 3 9 14 1.66 0.20 3 7 14 0.95 -0.80 3 5 14 -4.85 -0.74 3 3 14 2.04 -7.56 -3 5 14 0.84 6.66 -3 7 14 1.54 7.30 -3 11 14 -1.96 1.31 -3 13 14 0.55 0.87 4 12 14 1.44 2.47 4 10 14 0.04 -1.38 4 8 14 -5.45 2.27 4 6 14 -3.77 2.64 4 4 14 -0.99 -0.56 -4 6 14 -0.15 -3.09 -4 8 14 -2.13 -2.40 -4 10 14 -1.45 -1.64 -4 12 14 -1.96 2.96 5 11 14 1.01 -2.76 5 9 14 -6.58 -0.78 5 7 14 -2.00 3.15 5 5 14 -0.56 6.31 -5 7 14 -0.08 -1.65 -5 9 14 -0.96 2.53 -5 11 14 -1.39 0.20 6 12 14 1.20 0.31 6 10 14 -0.28 0.66 6 8 14 -3.02 6.75 6 6 14 4.40 8.06 -6 8 14 -2.01 3.38 -6 12 14 -1.24 -0.88 7 11 14 1.45 2.34 7 7 14 1.14 1.81 -7 9 14 -1.92 3.96 -7 11 14 1.38 -1.25 8 10 14 1.09 1.68 8 8 14 -3.35 -2.57 -8 10 14 -0.39 1.04 9 9 14 -0.86 -1.94 -3 9 14 -0.84 -6.98 7 9 14 -0.75 2.14 -6 10 14 0.85 -0.58 -1 11 14 -1.03 0.11 0 1 15 2.24 -0.89 0 3 15 0.92 -0.18 0 5 15 5.67 5.72 0 7 15 7.82 -1.01 0 9 15 1.04 -1.56 0 11 15 0.68 0.78 1 12 15 1.89 3.05 1 10 15 2.50 2.26 1 8 15 1.72 5.72 1 6 15 4.49 5.13 1 4 15 -4.42 3.83 1 2 15 -0.98 -6.39 -1 2 15 4.23 2.48 -1 4 15 3.28 3.60 -1 6 15 5.11 -2.44 -1 8 15 -2.95 -4.01 -1 10 15 -0.74 0.69 -1 12 15 0.85 0.80 2 9 15 -0.09 3.49 2 7 15 -2.16 4.08 2 5 15 3.23 5.97 2 3 15 -5.46 1.87 -2 3 15 -1.72 -0.05 -2 5 15 -3.55 -1.30 -2 7 15 -4.60 -7.83 3 12 15 -0.27 -1.45 3 10 15 -1.86 1.43 3 8 15 -2.47 0.27 3 6 15 3.37 -0.97 3 4 15 -0.67 5.66 -3 4 15 -4.70 -4.96 -3 6 15 -2.79 -5.41 -3 8 15 1.96 -0.28 -3 10 15 2.42 2.44 -3 12 15 1.17 -2.07 4 11 15 -0.53 -0.32 4 9 15 6.96 0.62 4 7 15 5.64 -5.71 4 5 15 6.64 -1.12 -4 5 15 -2.30 -1.32 -4 7 15 4.43 -0.87 -4 9 15 1.44 0.36 -4 11 15 0.58 -2.45 5 10 15 3.21 1.19 5 8 15 6.12 -2.55 5 6 15 -2.21 -6.40 -5 6 15 0.31 2.59 -5 8 15 6.05 0.43 -5 10 15 -1.09 -0.60 6 11 15 1.11 -0.86 6 7 15 -2.32 -3.91 -6 9 15 2.47 -1.13 -6 11 15 1.51 0.55 7 10 15 -1.43 -0.57 -6 7 15 -0.69 1.23 -7 8 15 5.28 -2.68 -7 10 15 1.18 -0.14 8 9 15 1.52 2.81 7 8 15 -0.92 2.52 -8 9 15 3.24 -4.35 -2 9 15 -2.14 1.55 6 9 15 2.52 0.77 -2 11 15 1.99 0.42 2 11 15 0.56 2.66 0 0 16 5.35 0.53 0 2 16 -0.87 1.09 0 4 16 2.06 1.13 0 6 16 -6.43 0.96 0 8 16 -0.47 2.89 0 10 16 0.76 0.21 1 11 16 0.22 -2.65 1 9 16 -1.70 0.51 1 7 16 -4.14 -2.41 1 5 16 -0.07 -6.08 1 3 16 3.57 0.73 1 1 16 -1.55 -1.43 -1 3 16 -5.56 1.83 -1 5 16 -0.27 1.57 -1 7 16 0.40 3.64 -1 9 16 6.29 -1.20 -1 11 16 1.05 -1.26 2 10 16 -0.84 -2.20 2 8 16 1.81 -3.30 2 6 16 -1.73 -8.38 2 4 16 6.22 -5.65 2 2 16 1.01 -0.87 -2 4 16 4.27 -0.20 -2 6 16 5.23 2.47 -2 8 16 4.13 0.89 3 11 16 2.40 -0.92 3 9 16 0.53 -2.48 3 7 16 0.42 2.58 3 5 16 -1.53 -3.91 3 3 16 5.60 -0.04 -3 5 16 7.73 1.94 -3 7 16 1.77 2.15 -3 9 16 -0.20 1.49 -3 11 16 0.22 0.11 4 10 16 -1.36 -0.71 4 8 16 -4.46 2.39 4 6 16 -2.12 5.29 4 4 16 4.44 -4.19 -4 6 16 -0.48 4.78 -4 8 16 -4.81 1.27 -4 10 16 0.96 2.04 5 9 16 -4.33 -0.89 5 7 16 -0.18 6.15 5 5 16 0.52 -0.36 -5 7 16 -4.56 -1.48 -5 9 16 0.64 -2.12 6 10 16 -0.61 -0.57 6 6 16 1.77 0.41 -6 8 16 -5.44 -3.38 -6 10 16 -0.76 0.79 7 9 16 2.71 -4.04 7 7 16 0.09 -0.55 8 8 16 -2.08 -3.52 6 8 16 2.25 -3.91 -7 9 16 -3.87 -0.56 -2 10 16 -1.03 -0.21 0 1 17 -1.37 -1.05 0 3 17 1.28 -4.35 0 5 17 -0.69 -3.95 0 7 17 0.37 -2.37 0 9 17 -2.30 -1.20 1 8 17 -0.48 -4.41 1 6 17 2.08 4.80 1 4 17 -1.56 -0.09 1 2 17 1.63 6.01 -1 2 17 2.86 -3.28 -1 4 17 0.29 -4.19 -1 6 17 -0.44 -2.60 -1 8 17 -4.31 0.60 -1 10 17 -2.26 0.48 2 9 17 0.88 1.34 2 7 17 1.12 3.34 2 5 17 -2.17 6.86 2 3 17 -1.55 -1.39 -2 3 17 0.69 -0.86 -2 5 17 -3.78 -0.72 -2 7 17 -2.59 2.10 -2 9 17 -2.02 0.82 3 10 17 -1.67 2.26 3 8 17 0.12 0.52 3 6 17 -0.46 1.72 3 4 17 -6.94 2.21 -3 4 17 -6.75 2.50 -3 6 17 -3.61 -2.10 -3 8 17 -1.83 -3.29 -3 10 17 -1.00 -3.12 4 7 17 0.89 -5.82 4 5 17 -4.48 2.09 -4 5 17 -3.38 -4.49 -4 7 17 1.44 -2.89 -4 9 17 -0.35 -1.04 5 8 17 -0.34 -0.09 5 6 17 -0.18 -0.87 -5 6 17 2.56 -4.56 -5 8 17 1.86 3.87 6 9 17 -1.56 3.31 6 7 17 -1.20 2.35 -6 7 17 4.04 3.42 -7 8 17 3.36 3.23 7 8 17 -1.94 3.64 -6 9 17 1.89 4.18 4 9 17 1.25 0.97 1 10 17 1.17 -1.33 0 0 18 -1.99 0.36 0 2 18 -1.94 -0.54 0 4 18 -2.20 5.13 0 6 18 2.68 0.43 0 8 18 4.03 2.89 1 9 18 -0.10 3.64 1 7 18 1.54 1.29 1 5 18 0.50 0.64 1 3 18 -4.75 0.59 1 1 18 0.00 -4.18 -1 3 18 -0.36 4.41 -1 5 18 -0.64 3.92 -1 7 18 1.28 -1.61 -1 9 18 0.78 -0.70 2 8 18 -1.49 0.41 2 6 18 0.06 -3.79 2 4 18 -0.04 0.96 2 2 18 -4.04 -3.92 -2 4 18 -0.43 0.43 -2 6 18 -1.03 -0.57 -2 8 18 1.87 -1.20 3 9 18 -0.53 -2.37 3 7 18 -2.05 0.39 3 5 18 6.46 -2.57 3 3 18 2.36 2.44 -3 5 18 0.92 -1.00 -3 7 18 1.47 2.00 -3 9 18 1.72 2.23 4 8 18 0.24 0.98 4 6 18 2.07 -1.00 4 4 18 6.91 -1.22 -4 6 18 -0.24 5.22 -4 8 18 2.62 2.36 5 7 18 -0.07 -0.14 5 5 18 1.05 -4.57 -5 7 18 -2.37 0.00 6 6 18 -3.78 -2.17 0 1 19 0.94 0.07 0 3 19 1.94 -1.23 0 5 19 -0.46 -1.50 0 7 19 -4.84 0.25 1 8 19 -1.50 -2.11 1 6 19 -3.43 -0.44 1 4 19 3.81 -3.10 1 2 19 2.77 1.47 -1 2 19 -0.99 -3.17 -1 4 19 0.69 -2.62 -1 6 19 0.22 0.84 -1 8 19 -0.64 -0.16 2 7 19 0.71 -0.50 2 5 19 -2.79 -2.47 2 3 19 3.63 -0.01 -2 3 19 -0.16 -3.34 -2 5 19 3.87 0.01 -2 7 19 0.86 -0.18 3 6 19 -0.81 1.36 3 4 19 -3.08 -0.60 -3 4 19 -1.07 0.55 -3 6 19 1.95 -0.66 4 7 19 -0.57 0.28 4 5 19 -5.28 3.06 -4 5 19 -0.94 -1.71 -4 7 19 -1.74 -3.49 5 6 19 1.46 2.71 -5 6 19 1.21 -2.54 0 0 20 -0.67 -0.31 0 2 20 0.12 1.46 0 4 20 -0.91 -0.13 0 6 20 2.19 -0.84 1 5 20 1.89 2.20 1 3 20 -0.99 0.39 1 1 20 1.42 0.61 -1 3 20 2.48 1.82 -1 5 20 -0.56 -1.07 2 6 20 2.08 2.23 2 4 20 -0.13 3.03 2 2 20 0.99 -1.45 -2 4 20 0.15 1.79 -2 6 20 -2.49 -0.22 3 5 20 1.98 0.24 3 3 20 0.45 -3.00 -3 5 20 -1.90 0.12 4 4 20 1.23 -0.86 0 1 21 -0.85 -0.10 0 3 21 -0.42 -0.19 1 4 21 -1.49 -0.94 1 2 21 -1.93 -2.27 -1 2 21 -1.11 -0.55 -1 4 21 -1.27 0.47 2 3 21 -1.93 0.93 -2 3 21 -2.10 -1.18 -8 16 0 3.10 0.43 8 16 0 -1.44 0.43 0 1 1 -187.93 28.03 -11 14 1 -4.48 -2.28 11 14 1 -2.19 0.49 0 0 2 86.50 -0.35 -5 17 2 -1.49 1.17 5 17 2 0.30 -3.07 -12 13 3 -0.60 0.84 12 13 3 0.57 -2.40 0 0 4 -123.65 1.56 -9 15 4 1.17 0.57 9 15 4 1.49 1.28 -10 14 6 0.95 -2.05 10 14 6 -1.33 -1.03 -6 16 6 -1.57 -2.55 6 16 6 0.91 1.46 -7 15 8 0.16 -0.27 7 15 8 -1.08 1.47 -11 12 9 -0.81 -0.72 11 12 9 -1.88 1.80 -6 15 9 -0.50 -1.15 6 15 9 -0.88 -1.02 -3 16 9 -0.41 0.46 3 16 9 -0.95 -0.69 -9 13 10 -0.21 -0.45 9 13 10 -0.41 -0.65 -5 15 10 0.59 0.23 5 15 10 0.32 -0.28 -6 13 13 -0.49 -0.61 6 13 13 -2.37 1.20 -3 14 13 0.01 0.49 3 14 13 -1.38 -0.68 -5 12 15 3.87 0.23 5 12 15 0.57 -0.57 0 13 15 -0.17 -0.22 -5 11 16 -0.02 0.62 5 11 16 -1.29 1.55 -2 12 16 -1.66 0.14 0 12 16 -0.05 -1.50 2 12 16 -1.04 -1.08 -5 10 17 -1.29 -0.54 5 10 17 0.94 -1.14 -2 11 17 0.66 0.16 0 11 17 -0.86 1.52 2 11 17 -0.63 0.96 7 7 18 -2.30 1.02 -6 8 18 -2.31 -5.29 6 8 18 0.76 -3.32 0 10 18 0.23 -0.50 -3 8 19 -3.15 -1.41 3 8 19 2.65 -0.07 5 5 20 1.04 -1.69 -1 7 20 0.77 0.66 1 7 20 2.78 -0.66 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 281019) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.000 0.500 571 171 ' ' 2 0.000 0.500 0.167 13 1 ' ' 3 0.000 0.500 0.333 13 1 ' ' 4 0.500 0.500 1.000 571 171 ' ' 5 0.500 0.000 0.833 13 1 ' ' 6 0.500 1.000 0.667 13 1 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 0 1 1 3.578 0 0 2 4.539 0 0 4 9.108 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL inoc-5 I -4 R = 0.04 CELL 15.9744 15.9744 19.4804 90.00 90.00 90.00 SPGR I-4 # Solvent Accessible Volume = 1198 # Electrons Found in S.A.V. = 343 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.237 0.916 0.375 ! 4.13 eA-3 C102 0.613 0.681 0.111 ! 3.11 eA-3 C103 0.502 0.711 0.108 ! 2.92 eA-3 C104 0.858 0.991 0.371 ! 2.85 eA-3 C105 0.614 0.649 0.047 ! 2.41 eA-3 C106 0.561 0.595 0.123 ! 2.16 eA-3 C107 1.000 0.999 0.266 ! 2.05 eA-3 Q108 0.490 0.111 0.122 ! 1.92 eA-3 C109 0.857 0.045 0.346 ! 1.77 eA-3 C110 0.875 0.034 0.476 ! 1.73 eA-3 Q111 1.002 0.315 0.217 ! 0.96 eA-3 Q112 0.979 0.455 0.122 ! 0.89 eA-3 C113 0.500 0.500 0.000 ! 0.89 eA-3 Q114 0.337 0.295 0.019 ! 0.87 eA-3 Q115 0.333 0.376 0.156 ! 0.82 eA-3 Q116 0.111 0.793 0.077 ! 0.76 eA-3 Q117 0.715 0.670 0.206 ! 0.70 eA-3 Q118 0.472 0.090 0.183 ! 0.68 eA-3 Q119 0.684 0.293 0.343 ! 0.68 eA-3 C120 0.500 0.514 0.172 ! 0.67 eA-3 Q121 0.074 0.057 0.084 ! 0.63 eA-3 C122 0.385 0.531 0.047 ! 0.62 eA-3 Q123 0.763 0.205 0.311 ! 0.61 eA-3 Q124 0.106 0.516 0.263 ! 0.58 eA-3 C125 0.294 0.360 0.050 ! 0.58 eA-3 Q126 0.626 0.797 0.094 ! 0.57 eA-3 Q127 0.282 0.064 0.065 ! 0.55 eA-3 Q128 0.015 0.154 0.080 ! 0.54 eA-3 Q129 0.505 0.691 0.427 ! 0.54 eA-3 Q130 0.466 0.751 0.001 ! 0.53 eA-3 Q131 0.199 0.862 0.060 ! 0.52 eA-3 Q132 0.581 0.494 0.436 ! 0.51 eA-3 ) ; _shelx_fab_checksum 82786 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' 'y, -x, -z' '-y, x, -z' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group In1 In 0.54467(4) 0.61346(4) 0.57040(3) 0.01236(17) Uani 1 1 d . . . . . In2 In 0.73546(4) 0.52853(4) 0.56779(3) 0.01827(19) Uani 1 1 d . . . . . In3 In 0.68008(4) 0.65464(4) 0.43732(3) 0.02009(19) Uani 1 1 d . . . . . Cl1 Cl 0.7598(2) 0.7635(2) 0.38010(17) 0.0445(8) Uani 1 1 d . . . . . F3 F 0.4847(8) 0.8326(13) 0.8821(7) 0.164(8) Uani 1 1 d . . . . . O1 O 0.4585(4) 0.6978(4) 0.6247(3) 0.0203(15) Uani 1 1 d . . . . . O2 O 0.500000 0.500000 0.6149(5) 0.024(2) Uani 1 2 d S T P . . O3 O 0.6546(4) 0.6145(4) 0.6290(4) 0.0226(16) Uani 1 1 d . . . . . O4 O 0.6816(4) 0.4277(4) 0.6236(4) 0.0236(16) Uani 1 1 d . . . . . O5 O 0.7215(4) 0.4030(4) 0.4916(3) 0.0185(15) Uani 1 1 d . . . . . O6 O 0.7777(4) 0.6377(5) 0.5121(4) 0.0271(17) Uani 1 1 d . . . . . O7 O 0.6292(4) 0.5534(4) 0.5001(3) 0.0133(14) Uani 1 1 d . . . . . N00D N 0.8001(5) 0.5438(6) 0.6742(4) 0.027(2) Uani 1 1 d . . . . . H00D H 0.861528 0.552584 0.667560 0.032 Uiso 1 1 calc R . . . . N00E N 0.8658(5) 0.4884(7) 0.5280(5) 0.032(2) Uani 1 1 d . . . . . H00E H 0.906939 0.496995 0.566029 0.038 Uiso 1 1 calc R . . . . C1 C 0.4609(10) 0.7313(10) 0.6900(8) 0.057(4) Uani 1 1 d . . . . . C2 C 0.4193(10) 0.8046(11) 0.7075(9) 0.070(5) Uani 1 1 d . . . . . H2 H 0.384913 0.830909 0.674084 0.084 Uiso 1 1 calc R . . . . C3 C 0.4259(12) 0.8407(14) 0.7713(12) 0.095(7) Uani 1 1 d . . . . . H3 H 0.396746 0.890767 0.782238 0.114 Uiso 1 1 calc R . . . . C4 C 0.4765(12) 0.8016(15) 0.8188(9) 0.083(6) Uani 1 1 d . . . . . C5 C 0.5152(11) 0.7367(13) 0.8002(8) 0.076(5) Uani 1 1 d . U . . . H5 H 0.554031 0.714619 0.832356 0.091 Uiso 1 1 calc R . . . . C6 C 0.5082(10) 0.6925(13) 0.7376(8) 0.071(5) Uani 1 1 d . . . . . H6 H 0.534500 0.639986 0.729815 0.085 Uiso 1 1 calc R . . . . C7 C 0.6952(12) 0.6587(14) 0.6768(11) 0.090(6) Uani 1 1 d . U . . . H7A H 0.654183 0.676348 0.712045 0.108 Uiso 1 1 calc R . . . . H7B H 0.717286 0.710090 0.654928 0.108 Uiso 1 1 calc R . . . . C8 C 0.7639(8) 0.6167(8) 0.7112(6) 0.038(3) Uani 1 1 d . . . . . H8A H 0.744148 0.597464 0.756688 0.045 Uiso 1 1 calc R . . . . H8B H 0.809099 0.657995 0.719102 0.045 Uiso 1 1 calc R . . . . C9 C 0.7857(7) 0.4621(8) 0.7095(5) 0.031(3) Uani 1 1 d . U . . . H9A H 0.793261 0.469439 0.759620 0.037 Uiso 1 1 calc R . . . . H9B H 0.827578 0.420842 0.693421 0.037 Uiso 1 1 calc R . . . . C10 C 0.6981(7) 0.4290(8) 0.6953(6) 0.031(3) Uani 1 1 d . . . . . H10A H 0.692739 0.371618 0.714124 0.037 Uiso 1 1 calc R . . . . H10B H 0.656361 0.464950 0.718626 0.037 Uiso 1 1 calc R . . . . C11 C 0.8685(6) 0.3996(8) 0.5085(6) 0.035(3) Uani 1 1 d . . . . . H11A H 0.866187 0.364730 0.550458 0.041 Uiso 1 1 calc R . . . . H11B H 0.922067 0.387813 0.484913 0.041 Uiso 1 1 calc R . . . . C12 C 0.7969(6) 0.3762(7) 0.4620(6) 0.025(2) Uani 1 1 d . . . . . H12A H 0.804385 0.403011 0.416542 0.030 Uiso 1 1 calc R . . . . H12B H 0.795765 0.314787 0.455294 0.030 Uiso 1 1 calc R . . . . C13 C 0.8875(7) 0.5474(9) 0.4718(7) 0.042(3) Uani 1 1 d . U . . . H13A H 0.948018 0.543508 0.461560 0.051 Uiso 1 1 calc R . . . . H13B H 0.856084 0.532316 0.429800 0.051 Uiso 1 1 calc R . . . . C14 C 0.8663(7) 0.6342(8) 0.4924(7) 0.038(3) Uani 1 1 d . U . . . H14A H 0.901765 0.651545 0.531622 0.046 Uiso 1 1 calc R . . . . H14B H 0.876905 0.672974 0.453761 0.046 Uiso 1 1 calc R . . . . Cl2 Cl 1.000000 0.500000 0.6483(3) 0.147(5) Uani 1 2 d S TU P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 In1 0.0140(3) 0.0148(3) 0.0083(3) -0.0016(2) 0.0006(3) -0.0021(2) In2 0.0133(3) 0.0280(4) 0.0134(3) -0.0001(3) -0.0004(3) -0.0004(3) In3 0.0200(3) 0.0243(4) 0.0159(3) 0.0039(3) 0.0046(3) -0.0062(3) Cl1 0.0419(17) 0.0492(18) 0.0424(17) 0.0193(15) 0.0089(14) -0.0210(15) F3 0.093(9) 0.30(2) 0.100(9) -0.139(13) -0.010(8) 0.035(11) O1 0.025(4) 0.018(4) 0.018(3) -0.007(3) 0.002(3) 0.002(3) O2 0.037(6) 0.016(5) 0.018(5) 0.000 0.000 -0.013(5) O3 0.018(3) 0.025(4) 0.025(4) -0.011(3) -0.009(3) 0.002(3) O4 0.031(4) 0.026(4) 0.014(3) 0.002(3) -0.009(3) -0.004(3) O5 0.016(4) 0.022(4) 0.017(4) 0.003(3) 0.002(3) 0.007(3) O6 0.017(4) 0.036(4) 0.028(4) 0.002(3) -0.003(3) -0.009(3) O7 0.011(3) 0.017(3) 0.012(3) 0.001(3) 0.002(3) -0.003(3) N00D 0.014(4) 0.050(6) 0.017(4) -0.001(4) -0.007(3) -0.003(4) N00E 0.019(5) 0.055(6) 0.021(4) -0.007(5) -0.005(4) 0.005(4) C1 0.066(10) 0.055(10) 0.049(9) -0.016(8) 0.012(8) 0.002(8) C2 0.060(10) 0.086(12) 0.064(11) -0.048(10) 0.019(8) 0.006(9) C3 0.070(12) 0.100(15) 0.115(18) -0.043(14) -0.038(12) 0.008(11) C4 0.067(11) 0.125(17) 0.056(10) -0.034(11) -0.017(10) -0.012(12) C5 0.053(8) 0.124(12) 0.050(8) -0.038(9) -0.009(7) 0.000(9) C6 0.046(9) 0.114(15) 0.053(9) -0.001(10) -0.013(8) -0.001(9) C7 0.066(9) 0.107(11) 0.096(10) -0.067(9) -0.032(8) 0.028(9) C8 0.045(7) 0.042(7) 0.026(6) -0.006(5) -0.025(6) -0.008(6) C9 0.030(6) 0.046(6) 0.016(5) 0.001(5) -0.015(4) 0.003(5) C10 0.032(6) 0.040(7) 0.021(6) 0.003(5) -0.005(5) 0.007(5) C11 0.013(5) 0.057(8) 0.034(6) -0.003(6) -0.001(5) 0.012(5) C12 0.023(5) 0.025(6) 0.028(6) 0.002(5) -0.001(5) 0.012(5) C13 0.019(5) 0.069(8) 0.038(6) 0.001(6) 0.013(5) -0.001(5) C14 0.021(5) 0.051(7) 0.041(6) 0.003(6) -0.004(5) -0.025(5) Cl2 0.031(3) 0.366(15) 0.046(3) 0.000 0.000 0.003(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' In In 0.0822 5.0449 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag In2 In1 In3 173.50(2) . 4_656 ? O1 In1 In2 145.99(18) . . ? O1 In1 In3 39.99(18) . 4_656 ? O1 In1 O5 91.2(2) . 4_656 ? O2 In1 In2 88.07(2) . . ? O2 In1 In3 88.30(3) . 4_656 ? O2 In1 O1 96.7(2) . . ? O2 In1 O5 170.9(3) . 4_656 ? O2 In1 O7 95.2(2) . . ? O3 In1 In2 41.05(18) . . ? O3 In1 In3 144.69(19) . 4_656 ? O3 In1 O1 104.9(3) . . ? O3 In1 O2 93.7(3) . . ? O3 In1 O5 88.6(3) . 4_656 ? O3 In1 O7 169.0(3) . 4_656 ? O3 In1 O7 79.9(3) . . ? O5 In1 In2 87.96(17) 4_656 . ? O5 In1 In3 94.86(17) 4_656 4_656 ? O7 In1 In2 136.11(17) 4_656 . ? O7 In1 In2 40.08(16) . . ? O7 In1 In3 135.08(17) . 4_656 ? O7 In1 In3 39.23(16) 4_656 4_656 ? O7 In1 O1 166.9(2) . . ? O7 In1 O1 76.9(2) 4_656 . ? O7 In1 O2 96.8(2) 4_656 . ? O7 In1 O5 80.5(2) 4_656 4_656 ? O7 In1 O5 76.6(2) . 4_656 ? O7 In1 O7 96.1(2) 4_656 . ? In1 In2 In3 61.802(18) . . ? O3 In2 In1 38.05(17) . . ? O3 In2 In3 83.29(19) . . ? O3 In2 O5 139.3(2) . . ? O3 In2 N00D 73.5(3) . . ? O3 In2 N00E 150.6(3) . . ? O4 In2 In1 86.01(19) . . ? O4 In2 In3 137.25(18) . . ? O4 In2 O3 87.6(3) . . ? O4 In2 O5 70.1(2) . . ? O4 In2 O6 173.9(3) . . ? O4 In2 O7 97.6(3) . . ? O4 In2 N00D 78.7(3) . . ? O4 In2 N00E 109.0(3) . . ? O5 In2 In1 104.67(15) . . ? O5 In2 In3 90.50(15) . . ? O6 In2 In1 87.97(19) . . ? O6 In2 In3 38.67(19) . . ? O6 In2 O3 87.3(3) . . ? O6 In2 O5 112.1(2) . . ? O6 In2 O7 78.0(2) . . ? O6 In2 N00D 102.9(3) . . ? O6 In2 N00E 77.0(3) . . ? O7 In2 In1 39.26(15) . . ? O7 In2 In3 39.69(17) . . ? O7 In2 O3 76.2(2) . . ? O7 In2 O5 73.7(2) . . ? O7 In2 N00D 149.6(3) . . ? O7 In2 N00E 123.2(3) . . ? N00D In2 In1 110.4(2) . . ? N00D In2 In3 136.6(3) . . ? N00D In2 O5 130.6(3) . . ? N00E In2 In1 160.1(2) . . ? N00E In2 In3 98.6(2) . . ? N00E In2 O5 70.1(3) . . ? N00E In2 N00D 85.9(3) . . ? In1 In3 In2 63.218(19) 3_566 . ? Cl1 In3 In1 145.54(9) . 3_566 ? Cl1 In3 In2 129.68(9) . . ? O1 In3 In1 40.08(17) 3_566 3_566 ? O1 In3 In2 83.58(18) 3_566 . ? O1 In3 Cl1 105.67(19) 3_566 . ? O1 In3 O5 145.7(2) 3_566 4_656 ? O4 In3 In1 84.87(19) 4_656 3_566 ? O4 In3 In2 138.88(19) 4_656 . ? O4 In3 Cl1 91.4(2) 4_656 . ? O4 In3 O1 87.9(3) 4_656 3_566 ? O4 In3 O5 76.4(3) 4_656 4_656 ? O4 In3 O6 170.6(3) 4_656 . ? O4 In3 O7 99.2(3) 4_656 . ? O5 In3 In1 107.33(17) 4_656 3_566 ? O5 In3 In2 88.51(18) 4_656 . ? O5 In3 Cl1 104.98(19) 4_656 . ? O6 In3 In1 98.1(2) . 3_566 ? O6 In3 In2 38.9(2) . . ? O6 In3 Cl1 91.2(2) . . ? O6 In3 O1 100.1(3) . 3_566 ? O6 In3 O5 94.1(3) . 4_656 ? O6 In3 O7 78.3(2) . . ? O7 In3 In1 37.43(16) . 3_566 ? O7 In3 In2 39.73(16) . . ? O7 In3 Cl1 169.41(19) . . ? O7 In3 O1 75.3(2) . 3_566 ? O7 In3 O5 77.4(2) . 4_656 ? In3 O1 In1 99.9(3) 4_656 . ? C1 O1 In1 131.6(8) . . ? C1 O1 In3 125.4(8) . 4_656 ? In1 O2 In1 132.0(5) 2_665 . ? In1 O3 In2 100.9(3) . . ? C7 O3 In1 142.3(9) . . ? C7 O3 In2 114.6(9) . . ? In2 O4 In3 114.1(3) . 3_566 ? C10 O4 In2 114.6(6) . . ? C10 O4 In3 126.5(7) . 3_566 ? In1 O5 In2 95.1(2) 3_566 . ? In3 O5 In1 100.9(3) 3_566 3_566 ? In3 O5 In2 98.9(2) 3_566 . ? C12 O5 In1 123.1(6) . 3_566 ? C12 O5 In2 114.3(6) . . ? C12 O5 In3 119.6(6) . 3_566 ? In3 O6 In2 102.4(3) . . ? C14 O6 In2 113.7(7) . . ? C14 O6 In3 121.8(7) . . ? In1 O7 In1 132.5(3) 3_566 . ? In1 O7 In2 110.6(3) 3_566 . ? In1 O7 In2 100.7(2) . . ? In1 O7 In3 103.3(2) 3_566 . ? In1 O7 In3 105.1(3) . . ? In3 O7 In2 100.6(3) . . ? In2 N00D H00D 109.5 . . ? C8 N00D In2 109.9(6) . . ? C8 N00D H00D 109.5 . . ? C8 N00D C9 113.7(9) . . ? C9 N00D In2 104.5(6) . . ? C9 N00D H00D 109.5 . . ? In2 N00E H00E 107.8 . . ? C11 N00E In2 112.4(7) . . ? C11 N00E H00E 107.8 . . ? C11 N00E C13 114.6(9) . . ? C13 N00E In2 106.3(7) . . ? C13 N00E H00E 107.8 . . ? O1 C1 C2 122.7(15) . . ? C6 C1 O1 118.1(14) . . ? C6 C1 C2 119.1(16) . . ? C1 C2 H2 118.7 . . ? C3 C2 C1 122.6(19) . . ? C3 C2 H2 118.7 . . ? C2 C3 H3 121.2 . . ? C2 C3 C4 117.6(19) . . ? C4 C3 H3 121.2 . . ? F3 C4 C3 121(2) . . ? C5 C4 F3 121(2) . . ? C5 C4 C3 117.8(18) . . ? C4 C5 H5 115.8 . . ? C4 C5 C6 128.4(19) . . ? C6 C5 H5 115.8 . . ? C1 C6 C5 114.1(18) . . ? C1 C6 H6 123.0 . . ? C5 C6 H6 123.0 . . ? O3 C7 H7A 108.2 . . ? O3 C7 H7B 108.2 . . ? O3 C7 C8 116.4(15) . . ? H7A C7 H7B 107.3 . . ? C8 C7 H7A 108.2 . . ? C8 C7 H7B 108.2 . . ? N00D C8 H8A 108.4 . . ? N00D C8 H8B 108.4 . . ? C7 C8 N00D 115.7(10) . . ? C7 C8 H8A 108.4 . . ? C7 C8 H8B 108.4 . . ? H8A C8 H8B 107.4 . . ? N00D C9 H9A 109.4 . . ? N00D C9 H9B 109.4 . . ? N00D C9 C10 111.2(8) . . ? H9A C9 H9B 108.0 . . ? C10 C9 H9A 109.4 . . ? C10 C9 H9B 109.4 . . ? O4 C10 C9 110.7(9) . . ? O4 C10 H10A 109.5 . . ? O4 C10 H10B 109.5 . . ? C9 C10 H10A 109.5 . . ? C9 C10 H10B 109.5 . . ? H10A C10 H10B 108.1 . . ? N00E C11 H11A 109.2 . . ? N00E C11 H11B 109.2 . . ? N00E C11 C12 111.9(9) . . ? H11A C11 H11B 107.9 . . ? C12 C11 H11A 109.2 . . ? C12 C11 H11B 109.2 . . ? O5 C12 C11 109.1(9) . . ? O5 C12 H12A 109.9 . . ? O5 C12 H12B 109.9 . . ? C11 C12 H12A 109.9 . . ? C11 C12 H12B 109.9 . . ? H12A C12 H12B 108.3 . . ? N00E C13 H13A 109.7 . . ? N00E C13 H13B 109.7 . . ? H13A C13 H13B 108.2 . . ? C14 C13 N00E 110.0(10) . . ? C14 C13 H13A 109.7 . . ? C14 C13 H13B 109.7 . . ? O6 C14 C13 109.0(9) . . ? O6 C14 H14A 109.9 . . ? O6 C14 H14B 109.9 . . ? C13 C14 H14A 109.9 . . ? C13 C14 H14B 109.9 . . ? H14A C14 H14B 108.3 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag In1 In2 3.3365(8) . ? In1 In3 3.3603(9) 4_656 ? In1 O1 2.196(6) . ? In1 O2 2.132(4) . ? In1 O3 2.094(7) . ? In1 O5 2.267(7) 4_656 ? In1 O7 2.099(6) 4_656 ? In1 O7 2.149(6) . ? In2 In3 3.3616(9) . ? In2 O3 2.232(7) . ? In2 O4 2.126(7) . ? In2 O5 2.504(7) . ? In2 O6 2.161(7) . ? In2 O7 2.186(6) . ? In2 N00D 2.329(8) . ? In2 N00E 2.312(9) . ? In3 Cl1 2.426(3) . ? In3 O1 2.192(7) 3_566 ? In3 O4 2.135(7) 4_656 ? In3 O5 2.194(7) 4_656 ? In3 O6 2.151(7) . ? In3 O7 2.184(6) . ? F3 C4 1.335(19) . ? O1 C1 1.381(16) . ? O3 C7 1.336(18) . ? O4 C10 1.422(13) . ? O5 C12 1.404(12) . ? O6 C14 1.468(13) . ? N00D H00D 1.0000 . ? N00D C8 1.486(16) . ? N00D C9 1.492(15) . ? N00E H00E 1.0000 . ? N00E C11 1.468(16) . ? N00E C13 1.485(16) . ? C1 C2 1.39(2) . ? C1 C6 1.35(2) . ? C2 H2 0.9500 . ? C2 C3 1.37(2) . ? C3 H3 0.9500 . ? C3 C4 1.38(3) . ? C4 C5 1.26(3) . ? C5 H5 0.9500 . ? C5 C6 1.41(2) . ? C6 H6 0.9500 . ? C7 H7A 0.9900 . ? C7 H7B 0.9900 . ? C7 C8 1.45(2) . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C9 H9A 0.9900 . ? C9 H9B 0.9900 . ? C9 C10 1.522(16) . ? C10 H10A 0.9900 . ? C10 H10B 0.9900 . ? C11 H11A 0.9900 . ? C11 H11B 0.9900 . ? C11 C12 1.506(15) . ? C12 H12A 0.9900 . ? C12 H12B 0.9900 . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C13 C14 1.482(18) . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ?