#------------------------------------------------------------------------------ #$Date: 2021-09-24 01:23:15 +0300 (Fri, 24 Sep 2021) $ #$Revision: 269266 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/47/1564716.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564716 loop_ _publ_author_name 'Aldridge, Simon' 'McManus, Caitil\'in' 'Hicks, Jamie' 'Goicoechea, Jose M.' 'Cui, Xianlu' 'Zhao, Lili' 'Frenking, Gernot' _publ_section_title ; Coinage metal aluminyl complexes: probing regiochemistry and mechanism in the insertion and reduction of carbon dioxide ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC04676D _journal_year 2021 _chemical_formula_moiety 'C72 H111 Al Cu N4 O P, C6 H6' _chemical_formula_sum 'C78 H117 Al Cu N4 O P' _chemical_formula_weight 1248.24 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2019-08-26 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-05-24 deposited with the CCDC. 2021-09-16 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 98.787(4) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.6572(4) _cell_length_b 19.3809(6) _cell_length_c 30.2695(12) _cell_measurement_reflns_used 6251 _cell_measurement_temperature 150.0(2) _cell_measurement_theta_max 75.8600 _cell_measurement_theta_min 3.6120 _cell_volume 7338.2(4) _computing_cell_refinement 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_data_collection 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 150.0(2) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.4102 _diffrn_detector_type Atlas _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.985 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -65.00 36.00 1.00 25.00 -- -42.66 19.00 60.00 101 2 \w -128.00 -84.00 1.00 25.00 -- -42.66 178.00-120.00 44 3 \w -36.00 -10.00 1.00 25.00 -- -42.66 38.00-180.00 26 4 \w -43.00 30.00 1.00 25.00 -- -42.66 38.00 120.00 73 5 \w 56.00 93.00 1.00 55.00 -- 111.00 -61.00 -30.00 37 6 \w 32.00 57.00 1.00 55.00 -- 111.00 -15.00 -90.00 25 7 \w 47.00 90.00 1.00 55.00 -- 111.00 -30.00 -30.00 43 8 \w 34.00 110.00 1.00 55.00 -- 111.00 -95.00 150.00 76 9 \w 50.00 118.00 1.00 55.00 -- 111.00-125.00 -30.00 68 10 \w 92.00 143.00 1.00 55.00 -- 111.00 45.00 90.00 51 11 \w 41.00 70.00 1.00 55.00 -- 111.00 -45.00-180.00 29 12 \w 98.00 135.00 1.00 55.00 -- 111.00 -61.00 -30.00 37 13 \w 142.00 172.00 1.00 55.00 -- 111.00 30.00 -30.00 30 14 \w 92.00 153.00 1.00 55.00 -- 111.00 45.00 120.00 61 15 \w 94.00 121.00 1.00 55.00 -- 111.00-133.00 -60.00 27 16 \w 80.00 135.00 1.00 55.00 -- 111.00 -15.00 -90.00 55 17 \w 38.00 75.00 1.00 55.00 -- 111.00 -30.00 120.00 37 18 \w 40.00 138.00 1.00 55.00 -- 111.00 -77.00 150.00 98 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, Atlas' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0720484000 _diffrn_orient_matrix_UB_12 -0.0015465000 _diffrn_orient_matrix_UB_13 -0.0458523000 _diffrn_orient_matrix_UB_21 -0.0996761000 _diffrn_orient_matrix_UB_22 -0.0039270000 _diffrn_orient_matrix_UB_23 0.0234499000 _diffrn_orient_matrix_UB_31 -0.0062236000 _diffrn_orient_matrix_UB_32 0.0793735000 _diffrn_orient_matrix_UB_33 0.0002621000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0779 _diffrn_reflns_av_unetI/netI 0.0921 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.985 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 24 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 37 _diffrn_reflns_limit_l_min -37 _diffrn_reflns_number 41242 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.985 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 76.407 _diffrn_reflns_theta_min 3.616 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 1.071 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.86629 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.130 _exptl_crystal_description plank _exptl_crystal_F_000 2712 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.04 _exptl_crystal_size_min 0.02 _refine_diff_density_max 0.802 _refine_diff_density_min -0.425 _refine_diff_density_rms 0.066 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.031 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 949 _refine_ls_number_reflns 15157 _refine_ls_number_restraints 372 _refine_ls_restrained_S_all 1.024 _refine_ls_R_factor_all 0.1236 _refine_ls_R_factor_gt 0.0790 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0657P)^2^+9.9856P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1856 _refine_ls_wR_factor_ref 0.2153 _reflns_Friedel_coverage 0.000 _reflns_number_gt 9591 _reflns_number_total 15157 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1sc04676d2.cif _cod_data_source_block 5-Cu _cod_database_code 1564716 _publcif_datablock.id {8611d99c-9c01-4445-b9e7-6b3c1792dddd} _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C50 H40 N2 O2 Cu1 P1 Al1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.979 _shelx_estimated_absorpt_t_min 0.814 _reflns_odcompleteness_completeness 99.66 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 74.33 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances C68A-C65A = C67A-C65A = C66A-C65A = C63A-C61A = C64A-C61A = C62A-C61A = C72A- C69A = C71A-C69A = C70A-C69A 1.53 with sigma of 0.008 C61-C63 1.53 with sigma of 0.008 C61-C64 1.53 with sigma of 0.008 C62-C61 1.53 with sigma of 0.008 C66-C65 = C67-C65 = C68-C65 1.53 with sigma of 0.008 C68A-C66A 2.5 with sigma of 0.008 C66A-C67A 2.5 with sigma of 0.008 C67A-C68A 2.5 with sigma of 0.008 C64A-C63A 2.5 with sigma of 0.008 C63A-C62A 2.5 with sigma of 0.008 C62A-C64A 2.5 with sigma of 0.008 C72A-C71A 2.5 with sigma of 0.008 C71A-C70A 2.5 with sigma of 0.008 C70A-C72A 2.5 with sigma of 0.008 C63-C62 2.5 with sigma of 0.008 C62-C64 2.5 with sigma of 0.008 C64-C63 2.5 with sigma of 0.008 C66-C67 2.5 with sigma of 0.008 C67-C68 2.5 with sigma of 0.008 C68-C66 2.5 with sigma of 0.008 3. Uiso/Uaniso restraints and constraints C23A \\sim C21A \\sim C22A: within 2A with sigma of 0.005 and sigma for terminal atoms of 0.01 C63A \\sim C61A \\sim C64A \\sim C62A \\sim C69A \\sim C72A \\sim C70A \\sim C71A \\sim C66A \\sim C65A \\sim C68A \\sim C67A: within 4A with sigma of 0.005 and sigma for terminal atoms of 0.01 C21 \\sim C20 \\sim C22 \\sim C23: within 2A with sigma of 0.005 and sigma for terminal atoms of 0.01 C69 \\sim C70 \\sim C71 \\sim C72: within 2A with sigma of 0.005 and sigma for terminal atoms of 0.01 C68 \\sim C65 \\sim C66 \\sim C67: within 2A with sigma of 0.005 and sigma for terminal atoms of 0.01 C20 \\sim C23A \\sim C21A \\sim C22A: within 3A with sigma of 0.005 and sigma for terminal atoms of 0.01 4. Others Sof(C63A)=Sof(H63D)=Sof(H63E)=Sof(H63F)=Sof(C61A)=Sof(C64A)=Sof(H64D)= Sof(H64E)=Sof(H64F)=Sof(C62A)=Sof(H62D)=Sof(H62E)=Sof(H62F)=Sof(C69A)= Sof(C72A)=Sof(H72D)=Sof(H72E)=Sof(H72F)=Sof(C70A)=Sof(H70D)=Sof(H70E)= Sof(H70F)=Sof(C71A)=Sof(H71D)=Sof(H71E)=Sof(H71F)=Sof(C66A)=Sof(H66D)= Sof(H66E)=Sof(H66F)=Sof(C65A)=Sof(C68A)=Sof(H68D)=Sof(H68E)=Sof(H68F)= Sof(C67A)=Sof(H67D)=Sof(H67E)=Sof(H67F)=1-FVAR(1) Sof(C64)=Sof(H64A)=Sof(H64B)=Sof(H64C)=Sof(C62)=Sof(H62A)=Sof(H62B)=Sof(H62C)= Sof(C61)=Sof(C67)=Sof(H67A)=Sof(H67B)=Sof(H67C)=Sof(C68)=Sof(H68A)=Sof(H68B)= Sof(H68C)=Sof(C71)=Sof(H71A)=Sof(H71B)=Sof(H71C)=Sof(C70)=Sof(H70A)=Sof(H70B)= Sof(H70C)=Sof(C69)=Sof(C72)=Sof(H72A)=Sof(H72B)=Sof(H72C)=Sof(C66)=Sof(H66A)= Sof(H66B)=Sof(H66C)=Sof(C65)=Sof(C63)=Sof(H63A)=Sof(H63B)=Sof(H63C)=FVAR(1) Sof(C22A)=Sof(H22D)=Sof(H22E)=Sof(H22F)=Sof(C23A)=Sof(H23D)=Sof(H23E)= Sof(H23F)=Sof(C21A)=Sof(H21D)=Sof(H21E)=Sof(H21F)=1-FVAR(2) Sof(C22)=Sof(H22A)=Sof(H22B)=Sof(H22C)=Sof(C21)=Sof(H21A)=Sof(H21B)=Sof(H21C)= Sof(C23)=Sof(H23A)=Sof(H23B)=Sof(H23C)=FVAR(2) 5.a Ternary CH refined with riding coordinates: C55(H55), C49(H49), C30(H30), C33(H33), C42(H42), C45(H45) 5.b Secondary CH2 refined with riding coordinates: C56(H56A,H56B), C60(H60A,H60B), C58(H58A,H58B), C59(H59A,H59B), C57(H57A, H57B), C54(H54A,H54B), C52(H52A,H52B), C50(H50A,H50B), C51(H51A,H51B), C53(H53A,H53B) 5.c Aromatic/amide H refined with riding coordinates: C17(H17), C3(H3), C5(H5), C19(H19), C26(H26), C28(H28), C27(H27), C38(H38), C40(H40), C39(H39), C202(H202), C201(H201), C203(H203), C200(H200), C204(H204), C205(H205) 5.d Idealised Me refined as rotating group: C12(H12A,H12B,H12C), C13(H13A,H13B,H13C), C31(H31A,H31B,H31C), C32(H32A,H32B, H32C), C47(H47A,H47B,H47C), C44(H44A,H44B,H44C), C43(H43A,H43B,H43C), C35(H35A, H35B,H35C), C8(H8A,H8B,H8C), C64(H64A,H64B,H64C), C62(H62A,H62B,H62C), C46(H46A,H46B,H46C), C34(H34A,H34B,H34C), C10(H10A,H10B,H10C), C67(H67A,H67B, H67C), C22(H22A,H22B,H22C), C9(H9A,H9B,H9C), C68(H68A,H68B,H68C), C71(H71A, H71B,H71C), C21(H21A,H21B,H21C), C23(H23A,H23B,H23C), C70(H70A,H70B,H70C), C72(H72A,H72B,H72C), C66(H66A,H66B,H66C), C63(H63A,H63B,H63C), C22A(H22D,H22E, H22F), C23A(H23D,H23E,H23F), C21A(H21D,H21E,H21F), C63A(H63D,H63E,H63F), C64A(H64D,H64E,H64F), C62A(H62D,H62E,H62F), C72A(H72D,H72E,H72F), C70A(H70D, H70E,H70F), C71A(H71D,H71E,H71F), C66A(H66D,H66E,H66F), C68A(H68D,H68E,H68F), C67A(H67D,H67E,H67F) ; _shelx_res_file ; TITL 025cmcm19_a.res in P2(1)/n 025cmcm19.res created by SHELXL-2018/3 at 16:33:35 on 26-Aug-2019 REM Old TITL 025cmcm19 in P2(1)/n REM SHELXT solution in P2(1)/n: R1 0.227, Rweak 0.058, Alpha 0.053 REM 0.589 for 470 systematic absences, Orientation as input REM Formula found by SHELXT: C74 N3 O5 P2 Cu CELL 1.54184 12.6572 19.3809 30.2695 90 98.787 90 ZERR 4 0.0004 0.0006 0.0012 0 0.004 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Al Cu N O P UNIT 312 468 4 4 16 4 4 DFIX 1.53 0.008 C68A C65A C67A C65A C66A C65A C63A C61A C64A C61A C62A C61A = C72A C69A C71A C69A C70A C69A DFIX 1.53 0.008 C61 C63 DFIX 1.53 0.008 C61 C64 DFIX 1.53 0.008 C62 C61 DFIX 1.53 0.008 C66 C65 C67 C65 C68 C65 DANG 2.5 0.008 C68A C66A DANG 2.5 0.008 C66A C67A DANG 2.5 0.008 C67A C68A DANG 2.5 0.008 C64A C63A DANG 2.5 0.008 C63A C62A DANG 2.5 0.008 C62A C64A DANG 2.5 0.008 C72A C71A DANG 2.5 0.008 C71A C70A DANG 2.5 0.008 C70A C72A DANG 2.5 0.008 C63 C62 DANG 2.5 0.008 C62 C64 DANG 2.5 0.008 C64 C63 DANG 2.5 0.008 C66 C67 DANG 2.5 0.008 C67 C68 DANG 2.5 0.008 C68 C66 SIMU 0.005 0.01 2 C23A C21A C22A SIMU 0.005 0.01 4 C63A C61A C64A C62A C69A C72A C70A C71A C66A C65A C68A C67A SIMU 0.005 0.01 2 C21 C20 C22 C23 SIMU 0.005 0.01 2 C69 C70 C71 C72 SIMU 0.005 0.01 2 C68 C65 C66 C67 SIMU 0.005 0.01 3 C20 C23A C21A C22A L.S. 30 PLAN 20 SIZE 0.04 0.02 0.2 BOND list 4 fmap 2 53 ACTA OMIT 2 12 3 REM REM REM WGHT 0.065700 9.985600 FVAR 0.26863 0.60880 0.70828 CU1 4 0.541603 0.328310 0.160254 11.00000 0.03978 0.04898 = 0.04158 0.00411 0.01984 -0.00124 AL1 3 0.485366 0.312055 0.296740 11.00000 0.02886 0.02417 = 0.03766 0.00144 0.01354 0.00075 P1 7 0.574204 0.338723 0.090675 11.00000 0.04689 0.08256 = 0.04207 0.00995 0.02337 0.00191 O1 6 0.356459 0.277344 0.321421 11.00000 0.02794 0.02132 = 0.03442 0.00225 0.01247 0.00337 N1 5 0.544919 0.229602 0.326850 11.00000 0.02323 0.02530 = 0.04463 0.00168 0.01190 0.00083 N2 5 0.443735 0.395515 0.324411 11.00000 0.03272 0.01974 = 0.03993 -0.00085 0.01243 -0.00095 N4 5 0.584638 0.336898 0.257937 11.00000 0.03409 0.03025 = 0.04203 0.00388 0.01431 0.00276 N3 5 0.424286 0.298740 0.235247 11.00000 0.03180 0.03082 = 0.03384 -0.00008 0.01041 -0.00226 C1 1 0.371232 0.215273 0.344589 11.00000 0.02789 0.02042 = 0.03220 0.00315 0.00683 0.00023 C15 1 0.303987 0.326719 0.343617 11.00000 0.02592 0.02578 = 0.02821 -0.00011 0.00712 0.00737 C16 1 0.351083 0.391895 0.343692 11.00000 0.02856 0.02909 = 0.03252 0.00041 0.00830 0.00440 C6 1 0.291309 0.188440 0.365088 11.00000 0.02525 0.02670 = 0.03379 0.00305 0.00730 -0.00272 C2 1 0.473792 0.188527 0.345679 11.00000 0.02456 0.02440 = 0.04056 0.00207 0.01035 0.00062 C14 1 0.220446 0.307708 0.364665 11.00000 0.02357 0.03522 = 0.03059 -0.00222 0.00847 0.00324 C17 1 0.298006 0.444011 0.363932 11.00000 0.04053 0.02570 = 0.03680 -0.00298 0.00902 0.00342 AFIX 43 H17 2 0.321901 0.489326 0.363301 11.00000 -1.20000 AFIX 0 C24 1 0.491601 0.462877 0.323989 11.00000 0.03150 0.02804 = 0.04812 -0.00547 0.01466 0.00029 C11 1 0.188781 0.230934 0.363681 11.00000 0.02152 0.03655 = 0.03785 0.00185 0.00808 -0.00309 C48 1 0.513975 0.320643 0.221766 11.00000 0.03647 0.02980 = 0.03893 0.00673 0.01938 0.00240 C3 1 0.491262 0.124331 0.367252 11.00000 0.02239 0.03205 = 0.05292 0.00602 0.00386 0.00332 AFIX 43 H3 2 0.557346 0.102842 0.368494 11.00000 -1.20000 AFIX 0 C5 1 0.312694 0.124359 0.386334 11.00000 0.02777 0.03593 = 0.04098 0.01035 0.00728 -0.00614 AFIX 43 H5 2 0.260486 0.103221 0.400184 11.00000 -1.20000 AFIX 0 C18 1 0.210331 0.429011 0.384900 11.00000 0.03580 0.04293 = 0.03117 -0.00393 0.00776 0.01117 C25 1 0.468409 0.504308 0.285407 11.00000 0.03371 0.02283 = 0.05314 -0.00054 0.01447 0.00121 C55 1 0.330562 0.280441 0.203887 11.00000 0.04183 0.03131 = 0.03424 0.00150 0.01250 -0.00206 AFIX 13 H55 2 0.347202 0.288290 0.173715 11.00000 -1.20000 AFIX 0 C29 1 0.561356 0.487282 0.361070 11.00000 0.03838 0.03457 = 0.05794 -0.00757 0.00988 0.00138 C19 1 0.172247 0.361131 0.385971 11.00000 0.02821 0.04209 = 0.03527 -0.00119 0.01194 0.00719 AFIX 43 H19 2 0.114881 0.351401 0.400831 11.00000 -1.20000 AFIX 0 C4 1 0.411011 0.092300 0.386848 11.00000 0.03519 0.02879 = 0.04455 0.01082 0.00254 -0.00370 C56 1 0.298623 0.204235 0.207008 11.00000 0.04747 0.02566 = 0.04962 -0.00172 0.00558 0.00324 AFIX 23 H56A 2 0.357306 0.175329 0.200944 11.00000 -1.20000 H56B 2 0.286092 0.194504 0.237212 11.00000 -1.20000 AFIX 0 C49 1 0.689805 0.364259 0.254913 11.00000 0.03530 0.03675 = 0.04970 0.00646 0.01660 0.00162 AFIX 13 H49 2 0.681973 0.399460 0.231397 11.00000 -1.20000 AFIX 0 C36 1 0.645663 0.196289 0.324019 11.00000 0.02543 0.02808 = 0.05992 0.00485 0.01866 0.00212 C30 1 0.388624 0.481800 0.245403 11.00000 0.04426 0.02415 = 0.05051 0.00458 0.00988 -0.00088 AFIX 13 H30 2 0.376273 0.432283 0.248734 11.00000 -1.20000 AFIX 0 C12 1 0.115272 0.215487 0.319362 11.00000 0.02805 0.03785 = 0.05101 0.00031 0.00308 -0.00134 AFIX 137 H12A 2 0.151511 0.227196 0.294745 11.00000 -1.50000 H12B 2 0.051050 0.242330 0.317736 11.00000 -1.50000 H12C 2 0.097448 0.167309 0.317991 11.00000 -1.50000 AFIX 0 C13 1 0.130652 0.212311 0.402821 11.00000 0.03133 0.05044 = 0.05313 0.00240 0.01950 -0.00256 AFIX 137 H13A 2 0.108389 0.164940 0.400273 11.00000 -1.50000 H13B 2 0.069112 0.241427 0.402293 11.00000 -1.50000 H13C 2 0.177987 0.218883 0.430452 11.00000 -1.50000 AFIX 0 C60 1 0.235167 0.326215 0.209661 11.00000 0.04137 0.03003 = 0.04853 0.00143 0.00672 0.00218 AFIX 23 H60A 2 0.253388 0.373942 0.204793 11.00000 -1.20000 H60B 2 0.220960 0.322122 0.240148 11.00000 -1.20000 AFIX 0 C58 1 0.105827 0.231885 0.181024 11.00000 0.04491 0.04456 = 0.04302 0.00090 0.00014 -0.00999 AFIX 23 H58A 2 0.045029 0.220879 0.158539 11.00000 -1.20000 H58B 2 0.085734 0.223008 0.210165 11.00000 -1.20000 AFIX 0 C59 1 0.133668 0.307452 0.177510 11.00000 0.04095 0.03830 = 0.05449 0.00372 0.00453 -0.00197 AFIX 23 H59A 2 0.074657 0.335431 0.184291 11.00000 -1.20000 H59B 2 0.144183 0.317651 0.147111 11.00000 -1.20000 AFIX 0 C37 1 0.652626 0.148554 0.289917 11.00000 0.03535 0.02802 = 0.07308 0.00062 0.02200 0.00383 C41 1 0.734854 0.209604 0.356737 11.00000 0.02330 0.03956 = 0.07085 0.00791 0.01430 0.00153 C31 1 0.281020 0.518360 0.245379 11.00000 0.04522 0.04829 = 0.05796 -0.00560 0.00633 0.00665 AFIX 137 H31A 2 0.256063 0.510047 0.273301 11.00000 -1.50000 H31B 2 0.229797 0.500831 0.221327 11.00000 -1.50000 H31C 2 0.289910 0.567066 0.241496 11.00000 -1.50000 AFIX 0 C33 1 0.589569 0.445321 0.404033 11.00000 0.06223 0.04141 = 0.06105 -0.00913 -0.00595 -0.00080 AFIX 13 H33 2 0.571701 0.397011 0.396818 11.00000 -1.20000 AFIX 0 C42 1 0.559682 0.135024 0.253148 11.00000 0.04490 0.03668 = 0.06665 -0.01417 0.01548 0.01023 AFIX 13 H42 2 0.506945 0.171630 0.254670 11.00000 -1.20000 AFIX 0 C26 1 0.517897 0.568868 0.284423 11.00000 0.04731 0.02506 = 0.06393 0.00023 0.01606 -0.00262 AFIX 43 H26 2 0.503761 0.596079 0.258897 11.00000 -1.20000 AFIX 0 C20 1 0.156517 0.487873 0.407875 11.00000 0.05221 0.04784 = 0.04786 -0.00838 0.01775 0.01728 C57 1 0.199268 0.186057 0.174560 11.00000 0.05835 0.03342 = 0.05127 -0.00128 0.00525 -0.00912 AFIX 23 H57A 2 0.180538 0.138257 0.178869 11.00000 -1.20000 H57B 2 0.213986 0.191024 0.144198 11.00000 -1.20000 AFIX 0 C45 1 0.731403 0.261440 0.394317 11.00000 0.02883 0.05298 = 0.06492 0.00295 0.00457 0.00396 AFIX 13 H45 2 0.685454 0.299582 0.381831 11.00000 -1.20000 AFIX 0 C28 1 0.607369 0.552327 0.358533 11.00000 0.03808 0.03829 = 0.07365 -0.01469 0.00393 -0.00236 AFIX 43 H28 2 0.653191 0.569132 0.383131 11.00000 -1.20000 AFIX 0 C27 1 0.586702 0.592320 0.320539 11.00000 0.04176 0.02389 = 0.09270 -0.00570 0.01605 -0.00676 AFIX 43 H27 2 0.619453 0.635116 0.319475 11.00000 -1.20000 AFIX 0 C38 1 0.747758 0.113481 0.289162 11.00000 0.03801 0.04437 = 0.09642 -0.01212 0.02472 0.00556 AFIX 43 H38 2 0.752944 0.081965 0.266424 11.00000 -1.20000 AFIX 0 C32 1 0.428754 0.491922 0.200741 11.00000 0.05920 0.04148 = 0.05257 0.00499 0.01421 0.00200 AFIX 137 H32A 2 0.428456 0.540198 0.193622 11.00000 -1.50000 H32B 2 0.382808 0.467653 0.177708 11.00000 -1.50000 H32C 2 0.500213 0.474275 0.202826 11.00000 -1.50000 AFIX 0 C7 1 0.436049 0.021313 0.409269 11.00000 0.05065 0.03601 = 0.06131 0.01995 -0.00497 -0.00635 C54 1 0.737093 0.398792 0.298692 11.00000 0.03629 0.04518 = 0.07631 -0.00662 0.01398 -0.00730 AFIX 23 H54A 2 0.740613 0.365482 0.322790 11.00000 -1.20000 H54B 2 0.690488 0.436073 0.305000 11.00000 -1.20000 AFIX 0 C47 1 0.840541 0.292496 0.412621 11.00000 0.04020 0.05618 = 0.06837 0.00622 0.00327 -0.00143 AFIX 137 H47A 2 0.887663 0.256635 0.425603 11.00000 -1.50000 H47B 2 0.832201 0.326290 0.435019 11.00000 -1.50000 H47C 2 0.870198 0.314039 0.388721 11.00000 -1.50000 AFIX 0 C52 1 0.923709 0.372712 0.284330 11.00000 0.03160 0.06599 = 0.10003 0.00944 0.01334 -0.00481 AFIX 23 H52A 2 0.991856 0.393601 0.281270 11.00000 -1.20000 H52B 2 0.936244 0.338496 0.307937 11.00000 -1.20000 AFIX 0 C40 1 0.828792 0.173218 0.354482 11.00000 0.02742 0.04763 = 0.10289 0.00018 0.01088 0.00513 AFIX 43 H40 2 0.888804 0.181860 0.375587 11.00000 -1.20000 AFIX 0 C50 1 0.767217 0.309073 0.242752 11.00000 0.03911 0.05929 = 0.07926 -0.00971 0.02810 -0.00158 AFIX 23 H50A 2 0.772026 0.272099 0.264565 11.00000 -1.20000 H50B 2 0.739206 0.289748 0.213763 11.00000 -1.20000 AFIX 0 C39 1 0.834774 0.124752 0.321709 11.00000 0.02784 0.05257 = 0.14053 -0.01167 0.02406 0.01578 AFIX 43 H39 2 0.897358 0.099683 0.321529 11.00000 -1.20000 AFIX 0 C44 1 0.504770 0.066450 0.259407 11.00000 0.05236 0.05795 = 0.07287 -0.01791 0.02912 -0.01169 AFIX 137 H44A 2 0.556846 0.030066 0.262539 11.00000 -1.50000 H44B 2 0.451627 0.057533 0.233855 11.00000 -1.50000 H44C 2 0.471268 0.068582 0.285768 11.00000 -1.50000 AFIX 0 C51 1 0.878769 0.337919 0.241327 11.00000 0.03727 0.08130 = 0.09051 -0.00206 0.03179 0.00059 AFIX 23 H51A 2 0.925922 0.300648 0.235520 11.00000 -1.20000 H51B 2 0.875499 0.370813 0.217004 11.00000 -1.20000 AFIX 0 C43 1 0.593093 0.138512 0.207234 11.00000 0.07751 0.04794 = 0.07273 -0.00845 0.02466 -0.00754 AFIX 137 H43A 2 0.625397 0.182500 0.203432 11.00000 -1.50000 H43B 2 0.531405 0.132771 0.184787 11.00000 -1.50000 H43C 2 0.643651 0.102476 0.204384 11.00000 -1.50000 AFIX 0 C202 1 0.507360 0.211456 0.516679 11.00000 0.08305 0.07787 = 0.06953 -0.00812 0.01654 0.01230 AFIX 43 H202 2 0.535453 0.167049 0.517597 11.00000 -1.20000 AFIX 0 C35 1 0.708523 0.448596 0.422455 11.00000 0.06962 0.08669 = 0.06625 -0.01081 -0.00532 0.02237 AFIX 137 H35A 2 0.749295 0.438066 0.399050 11.00000 -1.50000 H35B 2 0.724814 0.415669 0.446212 11.00000 -1.50000 H35C 2 0.726347 0.494116 0.433700 11.00000 -1.50000 AFIX 0 C53 1 0.849204 0.427576 0.297172 11.00000 0.03276 0.05432 = 0.12166 -0.00645 0.01660 -0.01131 AFIX 23 H53A 2 0.844516 0.465002 0.275684 11.00000 -1.20000 H53B 2 0.878135 0.446106 0.326282 11.00000 -1.20000 AFIX 0 C8 1 0.536874 0.026887 0.443689 11.00000 0.05528 0.05756 = 0.08500 0.03512 0.00030 -0.00302 AFIX 137 H8A 2 0.594609 0.043741 0.429484 11.00000 -1.50000 H8B 2 0.555020 -0.017770 0.456340 11.00000 -1.50000 H8C 2 0.524548 0.058205 0.466940 11.00000 -1.50000 AFIX 0 PART 1 C64 1 0.357200 0.364606 0.070580 21.00000 0.04144 0.06792 = 0.06426 0.00987 0.00449 0.01536 AFIX 137 H64A 2 0.358837 0.350343 0.101049 21.00000 -1.50000 H64B 2 0.289889 0.351877 0.053407 21.00000 -1.50000 H64C 2 0.365916 0.413751 0.069478 21.00000 -1.50000 AFIX 0 PART 0 C201 1 0.440819 0.233811 0.478705 11.00000 0.06411 0.11566 = 0.05698 -0.03086 0.01470 -0.01664 AFIX 43 H201 2 0.423935 0.204886 0.454125 11.00000 -1.20000 AFIX 0 PART 1 C62 1 0.448977 0.356084 0.003274 21.00000 0.07629 0.08099 = 0.04412 -0.00318 -0.00186 -0.01156 AFIX 137 H62A 2 0.472038 0.403327 0.004525 21.00000 -1.50000 H62B 2 0.378073 0.353053 -0.013237 21.00000 -1.50000 H62C 2 0.496876 0.328832 -0.011262 21.00000 -1.50000 AFIX 0 PART 0 C46 1 0.681097 0.231021 0.432270 11.00000 0.04744 0.10335 = 0.06423 -0.00369 0.01368 -0.01982 AFIX 137 H46A 2 0.607107 0.221154 0.421970 11.00000 -1.50000 H46B 2 0.686726 0.263457 0.456486 11.00000 -1.50000 H46C 2 0.717588 0.189181 0.442398 11.00000 -1.50000 AFIX 0 C203 1 0.531754 0.253475 0.552301 11.00000 0.09623 0.10498 = 0.04644 0.00563 0.00020 0.01361 AFIX 43 H203 2 0.577676 0.238209 0.577332 11.00000 -1.20000 AFIX 0 C34 1 0.526991 0.467283 0.440259 11.00000 0.06874 0.11291 = 0.05198 0.00215 0.00412 -0.00237 AFIX 137 H34A 2 0.534456 0.516154 0.444880 11.00000 -1.50000 H34B 2 0.553820 0.443558 0.467511 11.00000 -1.50000 H34C 2 0.452880 0.456109 0.431436 11.00000 -1.50000 AFIX 0 C200 1 0.401081 0.298502 0.478202 11.00000 0.07147 0.11643 = 0.06233 0.00413 -0.01236 -0.00662 AFIX 43 H200 2 0.358096 0.314747 0.452647 11.00000 -1.20000 AFIX 0 C204 1 0.488989 0.318888 0.551794 11.00000 0.10820 0.08425 = 0.05978 -0.01482 -0.00830 -0.01505 AFIX 43 H204 2 0.504813 0.347905 0.576385 11.00000 -1.20000 AFIX 0 C10 1 0.346915 -0.004394 0.431767 11.00000 0.05791 0.10079 = 0.20938 0.11638 0.01046 -0.00418 AFIX 137 H10A 2 0.333510 0.028016 0.454245 11.00000 -1.50000 H10B 2 0.366163 -0.048211 0.445465 11.00000 -1.50000 H10C 2 0.283635 -0.009553 0.410086 11.00000 -1.50000 AFIX 0 PART 1 C61 1 0.448888 0.328945 0.050950 21.00000 0.05033 0.05724 = 0.04254 -0.00532 0.00879 -0.00575 C67 1 0.660514 0.211819 0.099541 21.00000 0.10091 0.10379 = 0.07158 0.00888 0.03149 0.06157 AFIX 137 H67A 2 0.665773 0.214770 0.131461 21.00000 -1.50000 H67B 2 0.711017 0.178534 0.091990 21.00000 -1.50000 H67C 2 0.589502 0.197875 0.086942 21.00000 -1.50000 AFIX 0 PART 0 C205 1 0.423010 0.340100 0.514461 11.00000 0.10547 0.07942 = 0.08624 -0.00167 -0.01719 0.00345 AFIX 43 H205 2 0.392512 0.383814 0.513829 11.00000 -1.20000 AFIX 0 PART 1 C22 1 0.106702 0.537168 0.371339 31.00000 0.05460 0.04543 = 0.06232 -0.00312 0.01673 0.01766 AFIX 137 H22A 2 0.162121 0.558395 0.357656 31.00000 -1.50000 H22B 2 0.067055 0.572147 0.384162 31.00000 -1.50000 H22C 2 0.059536 0.512027 0.349173 31.00000 -1.50000 AFIX 0 PART 0 C9 1 0.462992 -0.029750 0.373501 11.00000 0.12989 0.03095 = 0.09956 0.01130 -0.02117 0.00124 AFIX 137 H9A 2 0.399580 -0.039418 0.352692 11.00000 -1.50000 H9B 2 0.490095 -0.071820 0.387675 11.00000 -1.50000 H9C 2 0.516066 -0.009783 0.357881 11.00000 -1.50000 AFIX 0 PART 1 C68 1 0.792838 0.307204 0.106884 21.00000 0.04990 0.15212 = 0.07058 0.01822 0.02156 0.02376 AFIX 137 H68A 2 0.810227 0.351874 0.096326 21.00000 -1.50000 H68B 2 0.847862 0.274946 0.102511 21.00000 -1.50000 H68C 2 0.787465 0.309897 0.138131 21.00000 -1.50000 AFIX 0 C71 1 0.695106 0.460072 0.127094 21.00000 0.07539 0.07659 = 0.07768 -0.00369 0.01983 -0.02825 AFIX 137 H71A 2 0.655724 0.460104 0.151800 21.00000 -1.50000 H71B 2 0.722922 0.505441 0.123405 21.00000 -1.50000 H71C 2 0.753147 0.427821 0.132840 21.00000 -1.50000 AFIX 0 C21 1 0.064766 0.462219 0.431789 31.00000 0.07311 0.06107 = 0.07394 -0.00315 0.03924 0.02402 AFIX 137 H21A 2 0.010836 0.440731 0.410459 31.00000 -1.50000 H21B 2 0.034220 0.500607 0.445406 31.00000 -1.50000 H21C 2 0.092108 0.429343 0.454395 31.00000 -1.50000 AFIX 0 C23 1 0.237441 0.524847 0.441077 31.00000 0.07545 0.07517 = 0.06519 -0.03572 -0.00134 0.02789 AFIX 137 H23A 2 0.267591 0.493195 0.463977 31.00000 -1.50000 H23B 2 0.203272 0.562077 0.454330 31.00000 -1.50000 H23C 2 0.293158 0.542890 0.426136 31.00000 -1.50000 AFIX 0 C70 1 0.673920 0.452668 0.043705 21.00000 0.06518 0.09316 = 0.05850 0.01466 0.01708 -0.02493 AFIX 137 H70A 2 0.739045 0.426648 0.045857 21.00000 -1.50000 H70B 2 0.689594 0.500964 0.041937 21.00000 -1.50000 H70C 2 0.626369 0.438905 0.017385 21.00000 -1.50000 AFIX 0 C69 1 0.621416 0.439222 0.084663 21.00000 0.06752 0.07903 = 0.04851 0.00643 0.01802 -0.02982 C72 1 0.527707 0.487633 0.083868 21.00000 0.08574 0.06238 = 0.05745 0.00740 0.01676 -0.01036 AFIX 137 H72A 2 0.484624 0.486322 0.054883 21.00000 -1.50000 H72B 2 0.553438 0.533738 0.090132 21.00000 -1.50000 H72C 2 0.485467 0.473624 0.106084 21.00000 -1.50000 AFIX 0 C66 1 0.695134 0.274848 0.031129 21.00000 0.08494 0.12634 = 0.06608 0.00637 0.03515 0.03675 AFIX 137 H66A 2 0.633001 0.251721 0.015876 21.00000 -1.50000 H66B 2 0.757727 0.248193 0.028379 21.00000 -1.50000 H66C 2 0.701026 0.319576 0.018098 21.00000 -1.50000 AFIX 0 C65 1 0.685000 0.282908 0.080641 21.00000 0.07050 0.12139 = 0.05919 0.01196 0.03081 0.03930 C63 1 0.424823 0.251175 0.048585 21.00000 0.09225 0.05954 = 0.07546 -0.01356 0.00901 -0.01518 AFIX 137 H63A 2 0.477884 0.227949 0.034542 21.00000 -1.50000 H63B 2 0.355465 0.243605 0.031471 21.00000 -1.50000 H63C 2 0.426090 0.233404 0.078265 21.00000 -1.50000 AFIX 0 PART 0 PART 2 C22A 1 0.198989 0.562249 0.397967 -31.00000 0.06682 0.04859 = 0.06147 -0.01441 0.02140 0.01851 AFIX 137 H22D 2 0.267817 0.569491 0.415606 -31.00000 -1.50000 H22E 2 0.149838 0.596475 0.405461 -31.00000 -1.50000 H22F 2 0.205067 0.565885 0.366826 -31.00000 -1.50000 AFIX 0 C23A 1 0.177473 0.474861 0.458391 -31.00000 0.06788 0.05608 = 0.05596 -0.01528 0.01980 0.01944 AFIX 137 H23D 2 0.151971 0.429780 0.464611 -31.00000 -1.50000 H23E 2 0.140733 0.508989 0.473303 -31.00000 -1.50000 H23F 2 0.252845 0.477664 0.468908 -31.00000 -1.50000 AFIX 0 C21A 1 0.036283 0.490996 0.391051 -31.00000 0.06459 0.05475 = 0.05996 -0.01205 0.02018 0.01807 AFIX 137 H21D 2 0.024253 0.491899 0.358965 -31.00000 -1.50000 H21E 2 0.006964 0.531936 0.402292 -31.00000 -1.50000 H21F 2 0.002210 0.451113 0.401344 -31.00000 -1.50000 AFIX 0 C63A 1 0.449986 0.372224 0.004017 -21.00000 0.09239 0.05973 = 0.07142 0.00373 0.03820 -0.00036 AFIX 137 H63D 2 0.520019 0.378668 -0.003809 -21.00000 -1.50000 H63E 2 0.402283 0.406380 -0.010819 -21.00000 -1.50000 H63F 2 0.424261 0.327034 -0.005085 -21.00000 -1.50000 AFIX 0 C61A 1 0.455407 0.379557 0.054748 -21.00000 0.09085 0.05685 = 0.07164 0.00216 0.04020 -0.00222 C64A 1 0.462753 0.456883 0.066750 -21.00000 0.09597 0.06115 = 0.07864 0.00430 0.03562 0.00012 AFIX 137 H64D 2 0.470497 0.462147 0.098617 -21.00000 -1.50000 H64E 2 0.398848 0.479879 0.053093 -21.00000 -1.50000 H64F 2 0.523487 0.476781 0.056013 -21.00000 -1.50000 AFIX 0 C62A 1 0.352348 0.350460 0.068521 -21.00000 0.08972 0.05838 = 0.07178 0.00432 0.03551 0.00218 AFIX 137 H62D 2 0.346479 0.302280 0.061194 -21.00000 -1.50000 H62E 2 0.291796 0.374665 0.052841 -21.00000 -1.50000 H62F 2 0.354359 0.356250 0.100136 -21.00000 -1.50000 AFIX 0 C69A 1 0.705160 0.374369 0.085971 -21.00000 0.09061 0.06001 = 0.07241 0.00236 0.04272 -0.00668 C72A 1 0.713478 0.433355 0.120280 -21.00000 0.09268 0.06479 = 0.07787 0.00040 0.04152 -0.01547 AFIX 137 H72D 2 0.667361 0.470507 0.108571 -21.00000 -1.50000 H72E 2 0.785949 0.449539 0.126170 -21.00000 -1.50000 H72F 2 0.692320 0.416855 0.147526 -21.00000 -1.50000 AFIX 0 C70A 1 0.714655 0.404725 0.039863 -21.00000 0.09134 0.06408 = 0.07465 0.00246 0.04218 -0.01055 AFIX 137 H70D 2 0.758795 0.375250 0.024878 -21.00000 -1.50000 H70E 2 0.746247 0.449796 0.043499 -21.00000 -1.50000 H70F 2 0.644856 0.408098 0.022396 -21.00000 -1.50000 AFIX 0 C71A 1 0.799511 0.325050 0.099897 -21.00000 0.09021 0.06783 = 0.07676 0.00103 0.03792 -0.00911 AFIX 137 H71D 2 0.805588 0.315451 0.131298 -21.00000 -1.50000 H71E 2 0.864334 0.346123 0.093731 -21.00000 -1.50000 H71F 2 0.787526 0.282779 0.083358 -21.00000 -1.50000 AFIX 0 C66A 1 0.621277 0.236343 0.018953 -21.00000 0.08971 0.05918 = 0.06922 -0.00212 0.04130 0.00001 AFIX 137 H66D 2 0.586695 0.270405 -0.001310 -21.00000 -1.50000 H66E 2 0.609825 0.191391 0.005771 -21.00000 -1.50000 H66F 2 0.696576 0.245734 0.024966 -21.00000 -1.50000 AFIX 0 C65A 1 0.574546 0.238739 0.062761 -21.00000 0.08833 0.05648 = 0.06973 0.00272 0.04152 -0.00205 C68A 1 0.643963 0.194672 0.098084 -21.00000 0.09616 0.06390 = 0.07488 0.00413 0.03672 0.00574 AFIX 137 H68D 2 0.717352 0.208540 0.100079 -21.00000 -1.50000 H68E 2 0.637162 0.146923 0.089694 -21.00000 -1.50000 H68F 2 0.620778 0.201000 0.126563 -21.00000 -1.50000 AFIX 0 C67A 1 0.461658 0.207527 0.054539 -21.00000 0.08831 0.05236 = 0.07322 0.00273 0.03748 -0.00329 AFIX 137 H67D 2 0.428991 0.212554 0.080970 -21.00000 -1.50000 H67E 2 0.466120 0.159451 0.047414 -21.00000 -1.50000 H67F 2 0.419331 0.231076 0.030097 -21.00000 -1.50000 AFIX 0 HKLF 4 REM 025cmcm19_a.res in P2(1)/n REM wR2 = 0.2153, GooF = S = 1.031, Restrained GooF = 1.024 for all data REM R1 = 0.0790 for 9591 Fo > 4sig(Fo) and 0.1236 for all 15157 data REM 949 parameters refined using 372 restraints END WGHT 0.0655 9.9953 REM Highest difference peak 0.802, deepest hole -0.425, 1-sigma level 0.066 Q1 1 0.5420 0.3071 0.3194 11.00000 0.05 0.80 Q2 1 0.5458 0.3232 0.1991 11.00000 0.05 0.67 Q3 1 0.5376 0.3271 0.1213 11.00000 0.05 0.63 Q4 1 0.3397 -0.0359 0.3775 11.00000 0.05 0.60 Q5 1 0.6610 0.3342 0.3382 11.00000 0.05 0.49 Q6 1 0.3878 0.0275 0.4601 11.00000 0.05 0.40 Q7 1 0.4759 0.3561 0.1800 11.00000 0.05 0.36 Q8 1 0.5351 -0.0089 0.4148 11.00000 0.05 0.34 Q9 1 0.4456 0.3027 0.2548 11.00000 0.05 0.33 Q10 1 0.4791 0.3016 0.1837 11.00000 0.05 0.32 Q11 1 0.5612 0.3364 0.2772 11.00000 0.05 0.32 Q12 1 0.5711 0.3374 0.0603 11.00000 0.05 0.31 Q13 1 0.5129 0.3411 0.0755 11.00000 0.05 0.30 Q14 1 0.5994 0.3554 0.1398 11.00000 0.05 0.29 Q15 1 0.6484 0.1546 0.3192 11.00000 0.05 0.29 Q16 1 0.1895 0.4648 0.3971 11.00000 0.05 0.29 Q17 1 0.5047 0.3364 0.5195 11.00000 0.05 0.29 Q18 1 0.4047 0.3016 0.1955 11.00000 0.05 0.28 Q19 1 0.1358 0.2194 0.3698 11.00000 0.05 0.28 Q20 1 0.6049 0.3001 0.1395 11.00000 0.05 0.28 ; _shelx_res_checksum 1113 _shelx_hkl_file ; 0 0 -3 38.98 8.44 0 0 -4 3553.96 41.04 0 0 -5 5.30 3.19 0 0 -6 473.02 19.31 0 0 -7 2.70 3.92 0 0 -8 682.36 27.68 0 0 -9 1.49 4.21 0 0 -10 53.59 9.65 0 0 -11 1.94 5.02 0 0 -12 528.61 31.83 0 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5.80 0 5 -21 5.47 5.58 0 5 -21 0.26 4.08 0 -5 -22 2.07 3.58 0 5 -22 -2.42 5.31 0 5 -22 3.10 4.28 0 5 -23 14.33 11.38 0 -5 -23 22.48 6.01 0 5 -23 9.99 6.99 0 5 -24 46.92 10.58 0 5 -24 38.13 12.65 0 -5 -24 38.98 7.88 0 -5 -25 28.62 7.07 0 5 -25 34.71 9.56 0 5 -25 28.25 14.30 0 5 -26 3.54 5.04 0 -5 -26 12.24 5.03 0 -5 -27 -4.84 2.69 0 -5 -27 1.70 4.27 0 5 -27 7.36 7.70 0 5 -28 12.04 7.05 0 -5 -28 1.58 3.51 0 -5 -28 6.79 4.33 0 -5 -29 19.79 6.12 0 -5 -29 20.74 5.95 0 5 -29 19.08 7.23 0 5 -30 25.26 8.30 0 5 -30 42.11 10.27 0 -5 -30 35.92 7.35 0 5 -31 7.83 5.95 0 -5 -31 1.46 3.80 0 5 -32 2.75 4.85 0 -5 -32 12.73 5.11 0 5 33 0.29 3.95 0 5 -33 4.81 4.35 0 5 -34 -2.50 3.89 0 5 34 -1.54 3.36 0 5 35 18.10 4.43 0 5 -35 22.34 5.98 0 5 -36 14.30 4.49 0 6 0 5811.79 97.24 0 6 1 393.69 16.42 0 6 1 403.43 26.43 0 6 1 412.68 13.43 0 6 -1 387.48 26.17 0 6 -1 394.18 11.04 0 6 2 972.12 40.44 0 6 -2 1016.09 41.70 0 6 -2 1038.94 21.96 0 6 2 1054.80 28.53 0 6 2 1038.89 21.86 0 6 -3 12.53 3.43 0 6 3 7.81 5.49 0 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-28 138.16 18.56 0 6 28 125.74 17.49 0 6 -29 -1.84 6.00 0 6 -29 3.24 5.59 0 -6 -29 -1.21 3.09 0 -6 -30 2.10 2.91 0 6 -30 -0.63 4.87 0 6 -31 27.08 8.65 0 6 -32 45.94 9.82 0 6 32 49.40 9.00 0 6 33 15.32 4.80 0 6 -33 12.65 5.39 0 6 -34 3.34 3.90 0 6 34 2.04 2.36 0 6 35 0.05 2.06 0 6 35 2.96 2.28 0 6 -35 0.71 2.68 0 6 -36 -0.95 2.61 0 7 0 8.51 12.35 0 7 -1 368.60 27.66 0 7 1 357.70 27.25 0 7 2 1415.45 53.81 0 7 2 1505.03 36.15 0 7 2 1482.36 25.56 0 7 -2 1540.51 56.61 0 7 -2 1472.65 25.95 0 7 3 100.47 15.61 0 7 3 111.33 7.43 0 7 -3 111.63 16.29 0 7 3 112.88 11.06 0 7 -3 123.84 8.90 0 7 -4 898.48 27.26 0 7 4 964.37 23.81 0 7 -4 906.30 45.02 0 7 4 898.50 33.42 0 7 -5 97.51 10.10 0 7 5 97.95 8.61 0 7 -6 116.90 11.83 0 7 6 112.72 9.98 0 7 -7 417.26 23.34 0 7 7 447.47 21.16 0 7 -8 8.13 4.23 0 7 8 13.80 4.72 0 7 -9 2.16 3.98 0 7 9 9.20 4.75 0 7 -10 9.81 5.94 0 7 -11 789.01 45.90 0 7 -12 5.65 4.47 0 7 -13 44.24 11.87 0 7 -14 360.92 31.96 0 7 -15 51.81 13.10 0 7 -16 288.95 30.56 0 7 -17 28.00 10.44 0 7 -18 -4.41 8.25 0 7 -19 31.04 12.29 0 7 -20 147.66 25.52 0 7 -20 150.95 16.16 0 7 -21 2.90 4.85 0 7 -21 1.73 7.58 0 7 -22 47.66 10.40 0 7 -22 46.37 15.22 0 7 -23 40.65 14.93 0 7 -23 31.19 8.17 0 7 -24 1.26 5.07 0 7 -24 1.30 5.11 0 7 -25 3.32 5.13 0 7 -26 20.17 6.49 0 7 26 14.54 6.09 0 7 27 11.75 6.53 0 7 -27 21.98 7.35 0 7 -28 5.12 7.51 0 7 28 10.10 5.12 0 7 -28 7.60 6.94 0 7 -29 -2.56 4.54 0 7 29 -2.60 3.98 0 7 -30 17.64 7.38 0 7 30 21.72 7.01 0 7 31 18.96 6.33 0 7 -31 12.89 5.63 0 7 32 3.39 2.82 0 7 -32 -3.26 4.04 0 7 33 2.34 2.90 0 7 -33 -0.50 3.96 0 7 -34 1.69 3.21 0 7 -35 2.18 2.67 0 7 35 4.28 2.09 0 7 36 0.87 1.74 0 8 0 1541.28 61.06 0 8 1 2102.40 71.16 0 8 -1 2083.26 71.12 0 8 2 446.86 32.45 0 8 -2 497.20 35.27 0 8 2 523.60 22.45 0 8 3 639.90 40.26 0 8 3 719.57 17.15 0 8 -3 739.00 42.94 0 8 -3 730.20 20.80 0 8 3 718.37 28.38 0 8 -4 467.67 34.52 0 8 4 458.49 14.80 0 8 4 439.51 24.16 0 8 -4 449.27 18.84 0 8 -5 428.95 20.52 0 8 5 432.35 25.27 0 8 5 432.29 15.77 0 8 -5 418.99 34.03 0 8 6 364.25 25.21 0 8 -6 376.19 21.34 0 8 6 380.12 16.44 0 8 -7 40.81 8.12 0 8 7 42.31 6.26 0 8 8 39.89 6.88 0 8 -8 37.73 7.80 0 8 -9 -3.69 4.80 0 8 9 0.22 2.80 0 8 -10 165.24 17.96 0 8 10 161.11 14.91 0 8 -11 530.83 33.79 0 8 -12 29.30 8.39 0 8 -13 129.98 18.58 0 8 -14 49.04 11.77 0 8 -15 3.55 4.60 0 8 -16 268.07 30.06 0 8 -17 73.97 16.70 0 8 -18 13.70 8.39 0 8 -19 4.50 6.92 0 8 -19 2.99 4.47 0 8 -20 16.12 10.26 0 8 -20 15.41 5.70 0 8 -21 1.77 3.43 0 8 -21 8.92 9.13 0 8 -22 3.39 4.81 0 8 -22 4.77 4.18 0 8 -23 0.41 3.77 0 8 23 5.92 10.08 0 8 -23 13.23 7.03 0 8 24 18.69 7.57 0 8 -24 8.01 5.22 0 8 25 2.85 4.30 0 8 -25 2.81 6.53 0 8 26 7.17 6.05 0 8 -26 -2.43 5.31 0 8 -27 -2.87 5.44 0 8 27 1.88 4.59 0 8 -28 61.51 13.07 0 8 28 55.53 11.47 0 8 28 56.47 10.00 0 8 -29 5.39 5.11 0 8 29 15.16 5.85 0 8 29 10.38 5.27 0 8 -30 13.41 6.12 0 8 30 15.46 4.88 0 8 30 16.74 5.40 0 8 31 11.10 4.26 0 8 -31 10.63 6.39 0 8 -32 -3.49 4.44 0 8 -33 33.45 7.10 0 8 -34 -1.88 2.62 0 8 34 4.33 2.95 0 8 35 1.09 1.86 0 9 0 -5.13 7.70 0 9 -1 49.61 12.25 0 9 1 44.69 13.08 0 9 2 6.14 7.70 0 9 -2 20.98 15.13 0 9 3 180.75 14.55 0 9 -3 169.02 22.65 0 9 3 153.46 21.54 0 9 -4 2.07 1.93 0 9 4 8.30 3.54 0 9 -4 4.45 7.31 0 9 -5 70.78 8.64 0 9 -5 80.47 17.90 0 9 5 68.80 10.39 0 9 6 51.26 10.02 0 9 -6 49.92 7.85 0 9 -6 43.73 12.58 0 9 -7 2.48 7.72 0 9 7 7.90 6.12 0 9 -7 5.10 2.69 0 9 8 66.65 12.68 0 9 -8 71.46 11.03 0 9 -9 208.91 19.46 0 9 9 229.21 25.04 0 9 -10 7.82 4.64 0 9 -11 36.97 8.91 0 9 -12 3.39 4.59 0 9 -13 104.99 17.15 0 9 -14 189.87 23.80 0 9 -15 413.52 36.71 0 9 -16 323.85 33.00 0 9 -17 6.55 6.37 0 9 -18 32.98 12.09 0 9 -18 29.76 6.55 0 9 -19 106.24 20.31 0 9 -19 99.50 13.81 0 9 -20 6.11 6.93 0 9 20 -0.35 6.65 0 9 -20 -2.57 3.26 0 9 21 0.58 5.47 0 9 -21 3.36 3.93 0 9 -21 5.00 5.93 0 9 22 11.70 7.36 0 9 -22 6.18 5.42 0 9 -22 1.67 4.86 0 9 -23 23.50 8.74 0 9 23 32.93 10.80 0 9 24 2.15 5.02 0 9 25 2.73 4.78 0 9 -26 9.26 5.24 0 9 26 7.82 6.43 0 9 -27 15.17 5.09 0 9 27 0.05 3.60 0 9 28 3.41 5.16 0 9 -28 -0.12 4.98 0 9 29 58.76 10.46 0 9 -29 73.86 12.72 0 9 -30 4.00 4.22 0 9 30 6.95 4.00 0 9 -31 17.00 5.63 0 9 -32 6.10 3.88 0 9 -33 13.86 3.91 0 9 33 8.85 3.66 0 9 34 2.00 2.02 0 9 34 0.52 2.03 0 10 0 228.22 27.09 0 10 -1 1015.94 58.13 0 10 1 941.78 54.12 0 10 2 716.31 48.57 0 10 -2 735.78 48.50 0 10 -3 3.46 7.95 0 10 3 -1.62 9.04 0 10 -4 -0.96 8.39 0 10 5 144.74 15.28 0 10 -5 148.24 23.53 0 10 6 359.91 25.36 0 10 -6 357.27 36.28 0 10 -7 44.85 12.15 0 10 7 59.18 10.87 0 10 8 83.73 14.19 0 10 -8 83.14 19.26 0 10 -8 81.34 11.19 0 10 -9 -1.05 3.51 0 10 9 4.53 5.77 0 10 -9 -1.71 6.12 0 10 -10 46.28 9.62 0 10 10 55.30 12.40 0 10 11 72.85 15.18 0 10 -11 52.21 11.27 0 10 12 42.81 12.21 0 10 -12 33.02 8.72 0 10 -13 -14.81 6.88 0 10 13 -0.77 4.05 0 10 14 -0.78 5.44 0 10 -14 0.34 3.70 0 10 15 63.61 15.69 0 10 -15 57.79 13.29 0 10 -16 12.54 6.81 0 10 16 11.27 5.42 0 10 16 2.85 4.61 0 10 17 87.52 20.28 0 10 17 87.83 14.80 0 10 -17 65.14 14.76 0 10 18 7.01 6.05 0 10 18 5.81 8.79 0 10 -18 -2.22 5.71 0 10 -19 10.93 5.64 0 10 19 4.69 4.60 0 10 19 1.59 5.03 0 10 20 -0.72 4.86 0 10 -20 -1.58 6.22 0 10 20 13.55 8.38 0 10 21 90.44 17.28 0 10 21 82.13 19.28 0 10 -21 71.90 16.28 0 10 22 -0.92 3.99 0 10 23 33.83 10.61 0 10 24 12.90 7.14 0 10 -24 4.84 5.93 0 10 25 12.83 7.89 0 10 -25 22.78 7.30 0 10 26 -0.62 4.54 0 10 -26 5.50 5.89 0 10 27 14.17 6.26 0 10 -27 14.54 5.98 0 10 28 5.10 4.33 0 10 -28 0.93 4.78 0 10 29 49.12 9.72 0 10 -29 47.40 9.48 0 10 30 0.59 2.78 0 10 -30 -1.18 3.89 0 10 -31 9.53 4.57 0 10 -32 20.34 4.84 0 10 32 18.55 6.09 0 10 33 6.03 2.95 0 10 33 3.72 2.94 0 11 0 -0.53 9.22 0 11 1 3.46 7.47 0 11 -1 -1.18 7.39 0 11 2 1042.39 61.74 0 11 -2 1087.15 63.39 0 11 -3 90.25 18.41 0 11 3 68.93 17.30 0 11 -4 34.60 10.74 0 11 -5 125.72 22.78 0 11 -6 -3.44 7.28 0 11 -7 41.97 16.21 0 11 8 202.95 21.77 0 11 -8 200.01 30.37 0 11 9 28.54 9.31 0 11 -9 27.49 13.40 0 11 -10 255.45 35.60 0 11 10 259.90 26.56 0 11 11 1.30 4.06 0 11 -11 1.16 5.84 0 11 -12 1.15 6.19 0 11 12 -2.22 5.72 0 11 13 137.58 21.75 0 11 14 112.23 20.04 0 11 14 129.18 18.47 0 11 15 215.04 28.74 0 11 15 190.95 21.84 0 11 -16 -3.80 6.03 0 11 16 1.38 3.94 0 11 16 10.79 7.46 0 11 -17 28.23 9.11 0 11 17 14.23 8.26 0 11 17 36.81 10.61 0 11 18 120.27 22.63 0 11 18 119.98 18.88 0 11 19 -8.26 6.34 0 11 19 3.11 5.65 0 11 20 -0.45 4.45 0 11 20 16.58 9.02 0 11 21 7.22 6.74 0 11 -22 6.23 4.52 0 11 22 3.57 4.65 0 11 23 5.90 5.82 0 11 -23 5.77 3.96 0 11 -24 56.62 10.34 0 11 24 60.86 13.83 0 11 25 -1.91 4.23 0 11 -25 6.10 4.57 0 11 -26 8.49 5.30 0 11 26 7.47 4.93 0 11 -27 15.28 5.96 0 11 27 17.28 6.68 0 11 28 -8.70 5.00 0 11 -28 -1.89 3.73 0 11 -29 10.57 4.05 0 11 29 14.35 5.82 0 11 -30 36.30 6.41 0 11 30 23.88 5.50 0 11 30 34.45 9.02 0 11 -31 -1.36 2.19 0 11 31 3.87 4.65 0 11 32 -3.41 3.34 0 11 32 1.96 2.23 0 11 33 0.79 2.09 0 12 0 -0.96 7.97 0 12 1 487.67 43.35 0 12 -1 514.12 45.66 0 12 -2 8.45 7.70 0 12 2 4.56 6.82 0 12 -3 347.09 38.60 0 12 -4 10.38 7.28 0 12 -5 31.17 13.23 0 12 -6 9.60 8.53 0 12 -7 210.56 31.36 0 12 -8 5.82 9.46 0 12 -9 6.39 10.63 0 12 -10 32.15 12.13 0 12 -11 1.05 5.76 0 12 -12 42.24 15.63 0 12 12 51.22 11.04 0 12 13 32.68 10.15 0 12 -13 26.14 6.77 0 12 -13 29.92 14.67 0 12 14 1.33 4.42 0 12 -14 -10.48 13.35 0 12 -14 4.19 3.17 0 12 15 62.05 14.06 0 12 -15 84.70 22.11 0 12 -15 77.06 11.49 0 12 15 85.84 15.82 0 12 16 194.68 28.13 0 12 -16 197.20 18.14 0 12 -16 207.16 38.16 0 12 16 180.74 22.56 0 12 17 9.08 5.76 0 12 -17 5.67 3.96 0 12 -17 -1.39 10.32 0 12 17 7.10 7.18 0 12 -18 7.85 10.46 0 12 18 28.19 9.06 0 12 19 -8.84 7.29 0 12 20 65.16 13.85 0 12 21 20.50 9.12 0 12 22 47.93 12.20 0 12 23 24.57 8.73 0 12 24 8.70 7.30 0 12 25 -2.14 4.12 0 12 26 16.61 7.12 0 12 27 -5.40 5.14 0 12 28 32.53 9.61 0 12 28 48.84 9.57 0 12 29 -0.13 4.30 0 12 29 16.12 5.15 0 12 30 1.66 2.49 0 12 30 -1.70 2.38 0 12 30 6.47 4.73 0 12 31 0.65 2.11 0 12 31 7.19 3.90 0 12 32 14.95 4.23 0 13 0 -2.08 7.34 0 13 1 19.77 11.09 0 13 -1 22.97 11.71 0 13 -2 250.62 33.56 0 13 -3 -6.08 7.73 0 13 -4 45.60 17.22 0 13 -5 -5.36 10.79 0 13 -6 -0.06 5.35 0 13 -7 43.27 14.74 0 13 -8 64.82 18.53 0 13 -9 36.99 16.14 0 13 9 32.19 8.57 0 13 9 25.91 7.42 0 13 -9 40.28 8.92 0 13 10 62.11 11.62 0 13 10 59.34 12.67 0 13 -10 55.75 17.20 0 13 -10 51.77 10.86 0 13 -11 50.78 10.57 0 13 11 60.67 13.16 0 13 -11 65.71 19.93 0 13 -12 3.24 4.90 0 13 12 5.56 6.28 0 13 -12 15.69 10.64 0 13 -13 6.30 8.47 0 13 13 4.42 4.94 0 13 -13 6.40 4.67 0 13 -14 103.05 24.99 0 13 -14 101.90 14.28 0 13 14 85.49 15.07 0 13 -15 51.07 10.07 0 13 15 43.58 12.71 0 13 -15 35.29 15.16 0 13 -16 81.30 13.48 0 13 -16 98.79 23.76 0 13 16 86.35 17.18 0 13 17 119.36 19.18 0 13 -17 128.67 26.53 0 13 -17 123.68 15.23 0 13 -18 -1.78 3.17 0 13 18 6.42 6.57 0 13 19 2.64 4.62 0 13 20 2.32 6.20 0 13 21 4.65 6.67 0 13 22 3.63 4.30 0 13 23 9.80 7.77 0 13 24 -2.34 5.62 0 13 25 4.75 4.64 0 13 26 -0.87 4.29 0 13 26 7.60 6.59 0 13 27 54.76 10.17 0 13 27 62.05 12.34 0 13 28 4.14 4.12 0 13 28 7.68 3.76 0 13 28 8.54 5.25 0 13 29 19.60 6.57 0 13 29 12.02 4.06 0 13 29 18.88 4.69 0 13 30 12.43 3.09 0 13 30 7.56 2.42 0 13 30 5.87 3.90 0 13 31 19.99 5.33 0 14 0 91.57 23.95 0 14 1 63.35 18.42 0 14 -1 63.32 17.00 0 14 -2 1.07 4.79 0 14 -2 0.63 7.18 0 14 -3 -9.29 13.95 0 14 -3 -5.59 5.59 0 14 -4 147.54 27.21 0 14 4 124.46 16.47 0 14 -4 101.83 14.76 0 14 4 112.18 15.14 0 14 -5 117.16 16.33 0 14 5 117.29 16.01 0 14 5 116.79 15.27 0 14 -5 143.07 26.70 0 14 6 254.57 22.39 0 14 6 258.70 25.36 0 14 6 263.65 22.92 0 14 -6 275.20 23.58 0 14 -6 294.38 38.55 0 14 -7 -0.52 4.24 0 14 7 9.49 4.67 0 14 7 7.54 4.39 0 14 -7 9.74 8.33 0 14 7 5.86 5.40 0 14 8 76.45 13.41 0 14 -8 103.42 24.39 0 14 8 88.62 13.42 0 14 8 89.44 15.90 0 14 -8 84.74 14.16 0 14 -9 1.65 7.80 0 14 9 -3.31 7.19 0 14 9 5.73 4.97 0 14 -9 8.38 4.47 0 14 9 15.51 8.34 0 14 10 213.96 20.24 0 14 10 226.62 23.84 0 14 10 225.93 19.79 0 14 -10 282.89 38.89 0 14 10 232.44 25.44 0 14 -10 251.33 23.29 0 14 -11 63.40 20.78 0 14 -11 59.42 11.96 0 14 11 60.92 13.64 0 14 11 61.33 11.46 0 14 -11 42.86 7.16 0 14 11 38.84 6.28 0 14 11 53.12 11.83 0 14 12 2.30 4.54 0 14 12 1.81 5.59 0 14 -12 15.59 13.92 0 14 -12 8.87 5.29 0 14 -12 -5.02 6.42 0 14 13 30.43 11.46 0 14 -13 21.57 10.15 0 14 13 26.76 9.52 0 14 -13 28.86 8.53 0 14 -14 4.70 5.37 0 14 -14 11.03 5.45 0 14 14 4.52 5.33 0 14 14 11.72 6.20 0 14 -15 10.40 5.98 0 14 15 7.54 5.56 0 14 -15 1.77 8.57 0 14 15 3.24 5.46 0 14 16 11.71 8.59 0 14 -16 -1.21 4.64 0 14 17 40.15 12.82 0 14 -17 59.77 10.79 0 14 18 45.93 12.72 0 14 -18 36.77 8.76 0 14 19 24.25 9.24 0 14 20 1.82 5.71 0 14 20 1.12 5.72 0 14 21 -3.45 5.83 0 14 21 -8.97 9.08 0 14 22 -0.38 5.09 0 14 22 5.64 7.00 0 14 23 15.28 8.00 0 14 23 11.30 7.80 0 14 24 2.70 6.03 0 14 24 6.83 5.87 0 14 25 7.76 5.44 0 14 25 4.65 4.51 0 14 26 -5.01 5.32 0 14 26 2.52 5.31 0 14 27 14.76 6.89 0 14 27 5.63 4.10 0 14 28 35.89 8.43 0 14 28 33.55 6.32 0 14 29 -1.23 3.38 0 14 29 3.97 2.46 0 14 30 5.57 3.87 0 15 0 5.01 5.53 0 15 0 0.24 8.18 0 15 0 0.83 4.55 0 15 -1 67.11 13.29 0 15 1 76.61 13.51 0 15 -1 65.17 11.77 0 15 -1 80.32 21.22 0 15 1 60.81 12.46 0 15 2 -1.12 5.65 0 15 2 1.37 3.07 0 15 2 -1.06 5.30 0 15 -2 3.21 5.55 0 15 -2 -6.89 7.17 0 15 -2 2.68 5.24 0 15 3 72.67 13.18 0 15 -3 75.91 18.83 0 15 3 70.66 12.52 0 15 -3 65.64 11.05 0 15 3 63.12 11.09 0 15 -3 74.99 12.82 0 15 4 26.31 7.99 0 15 4 12.14 4.63 0 15 -4 17.93 7.21 0 15 -4 11.93 3.14 0 15 -4 11.64 5.28 0 15 4 25.10 7.91 0 15 5 15.81 6.40 0 15 -5 7.69 4.62 0 15 5 23.83 8.78 0 15 -5 0.66 5.79 0 15 -5 24.75 10.50 0 15 5 23.60 8.98 0 15 -6 -2.24 5.05 0 15 6 7.88 6.15 0 15 -6 13.55 7.25 0 15 -6 14.49 6.37 0 15 6 13.09 5.72 0 15 6 18.99 8.59 0 15 7 18.73 9.60 0 15 -7 5.27 4.93 0 15 7 3.69 5.02 0 15 7 3.74 4.65 0 15 -7 12.12 10.11 0 15 8 58.52 10.29 0 15 -8 66.13 19.04 0 15 8 61.04 13.72 0 15 -8 56.51 11.90 0 15 8 64.62 13.35 0 15 -9 111.39 24.77 0 15 -9 80.09 14.87 0 15 9 77.87 12.31 0 15 9 78.37 14.12 0 15 9 78.35 15.52 0 15 9 67.35 11.72 0 15 10 14.45 7.35 0 15 -10 6.41 4.39 0 15 10 25.35 8.36 0 15 -10 15.36 6.18 0 15 10 20.17 8.91 0 15 10 1.29 7.74 0 15 -10 18.33 8.97 0 15 -11 45.75 9.85 0 15 -11 33.20 7.74 0 15 11 39.88 11.68 0 15 -11 48.85 16.73 0 15 11 38.89 10.36 0 15 11 56.65 11.32 0 15 11 40.39 7.62 0 15 12 30.38 9.39 0 15 -12 13.67 8.04 0 15 -12 1.10 6.52 0 15 12 4.68 4.43 0 15 -12 1.34 5.49 0 15 12 24.34 8.94 0 15 13 -0.64 5.10 0 15 -13 -0.24 5.25 0 15 13 1.99 6.60 0 15 -14 38.73 9.27 0 15 14 19.91 9.05 0 15 14 34.91 9.70 0 15 15 -0.57 5.19 0 15 -15 2.40 3.67 0 15 15 3.36 4.96 0 15 -16 149.60 18.55 0 15 16 140.00 21.04 0 15 16 145.85 21.97 0 15 17 209.07 25.66 0 15 17 200.02 25.15 0 15 -17 203.30 20.16 0 15 18 2.22 4.90 0 15 -18 4.52 4.25 0 15 18 6.80 7.58 0 15 -19 117.82 14.37 0 15 19 118.22 18.66 0 15 19 100.83 18.00 0 15 20 4.13 4.86 0 15 20 0.21 4.88 0 15 21 26.40 10.03 0 15 21 31.70 10.31 0 15 22 4.80 5.34 0 15 22 -0.11 4.85 0 15 23 10.11 6.48 0 15 23 4.82 5.93 0 15 24 13.10 6.05 0 15 24 11.54 6.45 0 15 25 14.25 5.65 0 15 25 14.97 5.99 0 15 26 8.65 5.26 0 15 26 0.99 3.09 0 15 27 18.80 6.81 0 15 27 11.51 4.22 0 15 28 16.24 3.88 0 15 28 11.58 4.42 0 15 29 3.82 2.47 0 16 0 60.89 12.74 0 16 0 56.74 13.12 0 16 -1 165.86 21.66 0 16 1 154.22 20.22 0 16 -1 160.26 19.63 0 16 1 158.27 20.53 0 16 -2 86.17 13.89 0 16 -2 104.04 24.40 0 16 2 66.76 14.11 0 16 -2 75.95 14.49 0 16 2 79.38 15.04 0 16 2 58.88 11.04 0 16 -3 -0.31 5.84 0 16 3 7.20 5.30 0 16 -3 3.65 8.35 0 16 3 1.07 4.83 0 16 3 7.73 5.62 0 16 -3 10.71 4.44 0 16 -4 10.66 8.60 0 16 -4 -5.50 7.74 0 16 4 10.42 6.87 0 16 -4 1.73 4.56 0 16 4 11.57 4.52 0 16 4 -3.09 4.97 0 16 -5 24.23 7.18 0 16 5 38.71 10.68 0 16 5 44.09 9.91 0 16 -5 50.46 11.79 0 16 -5 41.20 9.78 0 16 5 38.69 11.37 0 16 -6 3.91 4.60 0 16 6 -3.87 5.81 0 16 -6 -3.31 7.73 0 16 6 2.05 3.57 0 16 6 5.21 8.34 0 16 6 -16.25 10.56 0 16 -6 0.18 3.83 0 16 -7 88.36 12.75 0 16 -7 80.27 19.72 0 16 -7 74.27 12.07 0 16 -7 72.00 13.30 0 16 7 87.25 16.30 0 16 7 85.34 14.00 0 16 7 67.86 12.13 0 16 7 72.30 12.84 0 16 -8 -2.46 7.11 0 16 8 -1.89 8.84 0 16 8 4.24 7.93 0 16 -8 11.78 4.74 0 16 8 17.22 6.99 0 16 8 20.24 9.07 0 16 -8 12.35 6.21 0 16 9 16.62 7.76 0 16 9 8.38 5.12 0 16 9 -4.70 6.92 0 16 -9 8.97 7.07 0 16 -9 18.56 10.08 0 16 9 18.67 8.99 0 16 -9 -4.42 9.32 0 16 10 -2.44 8.90 0 16 -10 2.78 5.75 0 16 10 -1.39 5.54 0 16 10 2.00 4.48 0 16 10 -1.01 6.00 0 16 11 100.02 15.69 0 16 -11 86.54 14.58 0 16 11 89.45 17.60 0 16 11 90.88 16.68 0 16 -11 86.08 12.88 0 16 11 92.59 12.56 0 16 12 127.15 14.60 0 16 -12 156.11 19.23 0 16 12 158.57 22.02 0 16 -12 139.92 16.40 0 16 12 187.10 20.56 0 16 12 124.21 19.09 0 16 13 14.53 8.22 0 16 13 12.90 8.24 0 16 -13 2.06 3.83 0 16 -13 15.64 7.43 0 16 14 94.46 17.20 0 16 -14 106.36 15.69 0 16 14 91.37 16.87 0 16 15 28.45 9.86 0 16 -15 35.84 9.58 0 16 15 37.34 12.17 0 16 16 6.67 6.20 0 16 -16 8.92 5.61 0 16 16 9.24 5.70 0 16 17 221.58 25.85 0 16 -17 223.22 21.50 0 16 17 199.69 24.14 0 16 18 -3.40 6.53 0 16 -18 9.69 5.79 0 16 18 11.32 9.12 0 16 19 -2.81 5.19 0 16 19 3.25 5.08 0 16 -19 -3.84 4.41 0 16 20 8.52 5.72 0 16 20 14.03 6.45 0 16 21 45.66 11.61 0 16 21 39.68 9.81 0 16 22 7.69 5.65 0 16 22 13.73 6.78 0 16 23 27.27 7.31 0 16 23 22.42 7.77 0 16 24 -0.81 3.60 0 16 24 -5.69 4.94 0 16 25 4.73 4.65 0 16 25 -1.41 4.09 0 16 26 0.09 2.44 0 16 26 -2.42 3.47 0 16 27 -1.10 2.58 0 16 27 4.77 2.82 0 16 28 -2.94 2.78 0 17 0 7.06 6.46 0 17 0 -7.03 8.66 0 17 1 3.57 6.11 0 17 1 7.42 6.24 0 17 -1 -7.79 6.48 0 17 -1 -8.56 8.50 0 17 -2 13.87 6.79 0 17 2 -3.68 8.60 0 17 2 27.88 9.89 0 17 2 24.72 10.44 0 17 -2 11.07 4.21 0 17 3 -6.88 12.00 0 17 3 7.18 6.90 0 17 3 -0.56 4.45 0 17 -3 7.96 6.35 0 17 3 5.91 5.36 0 17 -3 -1.75 7.82 0 17 4 16.83 7.79 0 17 4 9.30 8.16 0 17 -4 6.49 5.11 0 17 4 5.68 3.67 0 17 -4 6.97 5.29 0 17 -4 -8.82 10.28 0 17 5 6.43 4.56 0 17 5 -30.63 10.09 0 17 -5 12.28 5.99 0 17 -5 9.38 6.16 0 17 5 11.17 8.05 0 17 -5 -32.09 10.30 0 17 5 9.38 3.51 0 17 6 37.17 6.40 0 17 6 32.51 7.83 0 17 -6 50.33 12.17 0 17 6 46.79 10.67 0 17 -6 52.01 10.44 0 17 6 46.32 11.08 0 17 -6 30.73 8.27 0 17 7 4.55 6.34 0 17 7 -15.24 10.71 0 17 -7 -0.47 4.76 0 17 7 -27.17 9.40 0 17 -7 -1.33 7.13 0 17 7 3.42 5.42 0 17 -7 -31.33 9.92 0 17 -8 -31.06 9.80 0 17 8 10.83 5.03 0 17 8 -21.24 8.48 0 17 -8 0.06 6.29 0 17 8 3.56 5.69 0 17 8 -4.35 6.05 0 17 -9 43.69 9.90 0 17 -9 26.40 7.67 0 17 9 41.64 10.34 0 17 9 38.57 11.13 0 17 9 21.36 6.08 0 17 9 36.23 10.18 0 17 -10 62.21 13.08 0 17 10 70.72 14.29 0 17 10 87.12 15.44 0 17 10 60.35 9.76 0 17 10 71.29 13.75 0 17 -10 53.76 10.82 0 17 11 -4.46 7.14 0 17 -11 -3.27 7.66 0 17 11 5.91 4.88 0 17 -11 -3.98 5.76 0 17 11 -18.62 9.40 0 17 12 8.92 8.26 0 17 -12 -1.87 5.07 0 17 12 6.21 5.73 0 17 12 -0.90 5.54 0 17 13 7.26 6.87 0 17 -13 -3.78 5.20 0 17 -13 -1.06 5.40 0 17 13 9.15 6.36 0 17 14 19.86 9.00 0 17 -14 11.03 5.32 0 17 14 16.52 6.87 0 17 15 -0.70 4.40 0 17 15 0.48 4.98 0 17 -15 -2.32 6.13 0 17 16 66.32 13.52 0 17 -16 54.18 11.09 0 17 16 54.20 12.77 0 17 -17 -9.17 6.10 0 17 17 8.06 6.38 0 17 17 -0.46 4.82 0 17 18 30.90 9.67 0 17 18 26.69 8.80 0 17 -18 22.58 7.01 0 17 19 -8.58 5.86 0 17 -19 0.96 3.07 0 17 19 0.87 4.38 0 17 20 -7.66 6.23 0 17 20 7.05 5.40 0 17 21 27.26 8.29 0 17 21 27.25 8.76 0 17 22 1.66 4.64 0 17 22 4.10 3.84 0 17 23 -7.63 4.97 0 17 23 1.25 3.59 0 17 24 0.46 3.14 0 17 24 6.12 3.81 0 17 25 6.21 3.02 0 17 25 8.05 4.20 0 17 26 22.99 5.27 0 17 26 23.73 4.28 0 17 27 0.67 1.74 0 18 0 18.97 8.44 0 18 0 17.63 4.92 0 18 -1 4.43 9.97 0 18 -1 3.91 7.83 0 18 -1 11.63 7.44 0 18 1 20.39 8.49 0 18 1 25.14 9.83 0 18 1 -3.12 9.30 0 18 -2 -8.59 8.64 0 18 2 15.95 7.96 0 18 2 0.29 4.29 0 18 -2 0.96 6.08 0 18 3 6.47 6.97 0 18 3 -33.86 13.45 0 18 -3 2.94 6.62 0 18 -3 -9.04 7.29 0 18 3 2.90 6.99 0 18 3 4.87 5.15 0 18 -3 -30.23 10.45 0 18 -4 55.14 10.51 0 18 4 20.15 8.87 0 18 -4 61.48 12.29 0 18 4 58.14 13.26 0 18 4 50.32 10.51 0 18 -4 63.62 14.20 0 18 4 53.08 12.21 0 18 -5 -2.01 7.79 0 18 -5 14.53 8.49 0 18 5 6.55 6.23 0 18 5 -3.04 8.16 0 18 -5 21.48 6.75 0 18 5 18.32 6.39 0 18 5 11.30 7.58 0 18 6 73.75 12.78 0 18 6 49.49 12.97 0 18 -6 38.14 11.88 0 18 -6 82.12 13.45 0 18 -6 94.31 16.85 0 18 6 69.83 12.98 0 18 6 79.31 14.97 0 18 7 2.15 5.67 0 18 -7 0.33 5.80 0 18 7 -1.88 4.02 0 18 7 5.31 5.01 0 18 7 -32.68 10.14 0 18 -7 -29.61 9.83 0 18 8 7.15 4.06 0 18 -8 14.70 6.96 0 18 8 10.50 7.56 0 18 8 3.81 4.60 0 18 8 -5.17 6.86 0 18 9 9.42 7.29 0 18 -9 6.19 5.09 0 18 9 12.94 9.30 0 18 -9 -8.94 9.27 0 18 9 4.18 5.91 0 18 10 32.43 12.43 0 18 -10 13.95 8.03 0 18 -10 -27.42 8.79 0 18 10 5.12 4.29 0 18 10 -3.38 6.35 0 18 10 -0.08 6.59 0 18 -11 3.11 4.01 0 18 11 9.81 5.97 0 18 11 18.66 6.45 0 18 11 16.80 6.96 0 18 -11 24.56 9.26 0 18 12 62.80 10.89 0 18 12 75.41 14.47 0 18 12 76.26 14.94 0 18 -12 57.75 12.27 0 18 -12 67.80 11.81 0 18 -13 28.63 7.93 0 18 -13 20.03 6.77 0 18 13 22.16 8.35 0 18 13 18.44 7.84 0 18 14 10.00 6.26 0 18 -14 7.90 6.12 0 18 14 14.31 7.29 0 18 15 31.29 9.68 0 18 -15 25.98 7.78 0 18 15 20.32 8.09 0 18 -16 161.32 17.72 0 18 16 115.39 16.72 0 18 16 136.50 19.07 0 18 17 8.69 6.28 0 18 17 13.60 6.17 0 18 -17 6.30 4.71 0 18 -18 9.77 4.74 0 18 18 4.49 4.96 0 18 18 4.14 3.71 0 18 19 21.48 7.56 0 18 -19 31.52 6.52 0 18 19 13.56 6.11 0 18 20 0.33 4.55 0 18 20 4.35 4.76 0 18 21 53.89 9.77 0 18 21 58.11 10.38 0 18 22 1.13 3.44 0 18 22 4.14 3.87 0 18 23 23.09 6.12 0 18 23 24.46 5.98 0 18 24 6.32 3.23 0 18 24 2.76 2.50 0 18 25 1.79 2.03 0 19 0 11.82 8.85 0 19 0 -9.55 8.12 0 19 -1 -0.33 5.80 0 19 -1 8.05 7.14 0 19 1 -14.14 8.23 0 19 1 -26.28 9.99 0 19 1 12.56 8.35 0 19 -1 -27.63 10.13 0 19 2 -21.10 10.43 0 19 2 2.23 6.98 0 19 -2 -3.90 4.51 0 19 -2 -1.93 6.53 0 19 2 -22.55 9.86 0 19 -3 -33.00 12.05 0 19 -3 3.37 7.40 0 19 -3 7.91 5.27 0 19 3 8.17 6.72 0 19 3 -12.31 10.51 0 19 3 -37.56 11.28 0 19 4 -6.27 7.82 0 19 -4 5.94 4.02 0 19 4 -4.53 9.03 0 19 -4 1.36 5.78 0 19 4 16.56 8.58 0 19 -4 -3.21 8.16 0 19 -5 16.94 6.36 0 19 -5 23.68 9.96 0 19 5 26.85 9.90 0 19 5 18.97 6.72 0 19 5 3.20 7.11 0 19 5 11.70 6.50 0 19 6 10.25 5.42 0 19 6 26.27 9.86 0 19 -6 30.34 10.01 0 19 6 24.69 7.05 0 19 6 32.72 10.09 0 19 -6 8.48 6.91 0 19 7 44.40 10.08 0 19 -7 58.83 13.62 0 19 7 68.39 13.85 0 19 7 39.38 9.91 0 19 7 63.78 13.60 0 19 -7 51.81 10.01 0 19 8 -4.13 6.37 0 19 8 6.11 3.83 0 19 -8 -9.11 7.46 0 19 -8 -6.17 6.27 0 19 8 4.59 5.07 0 19 8 15.12 8.17 0 19 9 1.00 5.06 0 19 9 -1.04 5.82 0 19 -9 -1.08 5.81 0 19 9 -7.30 6.74 0 19 -9 6.75 6.28 0 19 10 -4.02 5.88 0 19 -10 -4.98 5.91 0 19 10 -2.88 5.21 0 19 10 5.13 5.16 0 19 -10 1.79 5.50 0 19 -11 14.89 6.38 0 19 -11 34.01 9.88 0 19 11 14.53 7.01 0 19 11 12.45 6.78 0 19 11 23.05 7.44 0 19 12 2.07 3.98 0 19 12 9.19 8.54 0 19 -12 11.10 6.36 0 19 -12 -3.56 5.98 0 19 13 29.73 8.54 0 19 13 35.68 10.22 0 19 -13 30.87 9.24 0 19 14 1.75 4.45 0 19 14 -2.77 5.95 0 19 -14 1.10 4.18 0 19 15 -1.56 3.33 0 19 -15 7.92 5.58 0 19 15 0.07 4.96 0 19 16 8.51 6.83 0 19 16 14.79 6.75 0 19 -16 8.59 5.42 0 19 17 11.08 6.05 0 19 -17 13.98 6.02 0 19 17 2.24 3.79 0 19 18 64.13 10.40 0 19 -18 70.11 9.11 0 19 18 45.23 9.54 0 19 19 14.89 5.38 0 19 19 22.36 7.00 0 19 20 53.55 8.97 0 19 20 47.24 7.73 0 19 21 -3.63 3.10 0 19 21 1.58 2.94 0 19 22 5.25 3.22 0 19 22 5.70 3.22 0 19 23 14.09 3.54 0 19 23 9.51 2.94 0 20 0 57.29 12.19 0 20 0 61.68 12.84 0 20 0 58.49 11.63 0 20 -1 0.72 5.06 0 20 -1 10.60 7.27 0 20 1 -8.49 9.98 0 20 -1 -14.76 9.21 0 20 1 -10.53 9.19 0 20 1 -5.88 6.93 0 20 2 -10.89 7.39 0 20 2 -4.93 8.36 0 20 -2 -12.54 8.91 0 20 -2 10.66 6.18 0 20 -2 8.02 7.20 0 20 2 -3.90 9.05 0 20 3 10.85 5.62 0 20 3 15.16 4.00 0 20 3 13.79 5.42 0 20 -3 43.45 11.97 0 20 -3 4.62 6.92 0 20 -3 34.24 8.77 0 20 4 -17.83 8.20 0 20 4 -1.30 6.66 0 20 -4 21.47 9.62 0 20 -4 -10.31 7.92 0 20 4 11.18 7.63 0 20 -4 0.64 4.74 0 20 -5 20.73 9.65 0 20 -5 26.22 7.92 0 20 -5 -2.51 7.28 0 20 5 0.05 4.88 0 20 5 -3.55 7.72 0 20 5 11.12 6.13 0 20 -6 20.92 8.77 0 20 6 24.70 8.50 0 20 6 -0.36 5.30 0 20 -6 2.44 4.90 0 20 6 23.29 9.02 0 20 6 11.58 5.30 0 20 7 3.26 4.05 0 20 7 13.44 9.70 0 20 7 2.34 3.30 0 20 -7 3.68 7.02 0 20 7 2.65 6.08 0 20 -7 -0.98 5.54 0 20 -8 -6.48 7.94 0 20 8 -1.77 4.44 0 20 8 -1.83 3.32 0 20 8 -0.22 4.88 0 20 -8 -3.83 4.99 0 20 9 8.10 5.97 0 20 -9 0.41 4.11 0 20 9 5.76 4.56 0 20 9 4.97 4.26 0 20 -9 6.23 6.63 0 20 -10 31.76 8.94 0 20 10 18.11 6.50 0 20 10 21.98 6.66 0 20 -10 24.59 8.43 0 20 10 34.55 9.49 0 20 11 37.88 9.67 0 20 11 47.86 9.16 0 20 11 85.47 11.83 0 20 -11 78.11 11.76 0 20 -11 63.38 12.47 0 20 12 13.37 8.03 0 20 -12 18.35 7.69 0 20 12 11.33 6.07 0 20 13 30.37 8.33 0 20 -13 50.13 10.42 0 20 13 27.33 6.91 0 20 14 4.96 5.44 0 20 14 4.51 3.31 0 20 -14 14.03 5.93 0 20 15 2.65 3.57 0 20 -15 5.74 5.28 0 20 15 -0.50 2.88 0 20 16 -0.75 3.30 0 20 16 -1.81 4.10 0 20 -16 -4.55 4.12 0 20 17 3.97 3.31 0 20 17 10.23 5.00 0 20 18 12.37 5.05 0 20 18 4.17 2.62 0 20 19 3.75 3.01 0 20 19 2.44 2.19 0 20 20 2.58 2.44 0 20 20 -0.99 2.29 0 20 21 5.17 2.79 0 21 0 1.36 3.58 0 21 0 8.61 6.91 0 21 -1 44.97 9.93 0 21 -1 49.37 9.83 0 21 1 35.27 9.46 0 21 1 46.77 11.10 0 21 1 55.11 10.19 0 21 -1 58.06 11.58 0 21 2 16.11 7.56 0 21 -2 -1.56 6.91 0 21 2 -0.32 5.77 0 21 2 2.20 3.69 0 21 -2 15.55 8.78 0 21 -3 89.00 13.36 0 21 -3 49.83 14.02 0 21 -3 94.31 12.71 0 21 3 95.74 15.41 0 21 3 92.98 14.14 0 21 3 74.25 11.54 0 21 4 -8.59 5.81 0 21 -4 11.51 7.16 0 21 4 15.82 8.59 0 21 -4 -9.03 8.92 0 21 4 2.73 6.16 0 21 -4 20.32 6.29 0 21 5 1.92 6.02 0 21 -5 16.84 7.38 0 21 5 -1.63 6.82 0 21 -5 5.28 6.03 0 21 5 22.59 9.78 0 21 6 -1.23 5.62 0 21 -6 11.65 5.59 0 21 6 3.93 6.71 0 21 -6 9.73 6.25 0 21 -7 8.13 6.46 0 21 -7 16.34 6.70 0 21 7 16.14 7.73 0 21 -8 23.05 8.11 0 21 -8 9.20 7.82 0 21 8 24.99 8.05 0 21 9 -9.86 6.73 0 21 -9 0.01 4.08 0 21 9 -1.31 2.57 0 21 10 -7.36 5.31 0 21 10 79.66 11.14 0 21 -10 59.42 10.77 0 21 10 -2.43 3.30 0 21 -10 19.82 9.41 0 21 11 3.51 2.86 0 21 -11 8.85 4.94 0 21 12 1.36 4.05 0 21 12 4.81 3.07 0 21 -12 -4.47 4.18 0 21 13 -0.88 1.99 0 21 -13 -7.77 3.66 0 21 13 -4.37 4.77 0 21 14 5.09 4.02 0 21 14 4.70 3.12 0 21 -14 -0.59 5.01 0 21 -15 -10.05 4.79 0 21 15 -6.42 4.48 0 21 15 -3.19 2.56 0 21 16 -2.17 1.94 0 21 16 -2.78 3.87 0 21 17 4.63 2.70 0 21 17 9.53 2.66 0 21 18 0.56 2.85 0 21 19 -6.46 3.33 0 22 0 27.81 6.49 0 22 0 37.79 10.88 0 22 0 33.29 9.08 0 22 -1 1.14 4.98 0 22 1 7.09 6.89 0 22 -1 11.02 7.84 0 22 -1 13.53 4.87 0 22 1 5.84 4.59 0 22 1 18.79 7.42 0 22 -2 22.31 6.07 0 22 -2 4.95 4.71 0 22 2 42.19 9.80 0 22 2 31.62 9.15 0 22 2 12.05 4.63 0 22 -2 21.49 8.17 0 22 3 -0.87 3.05 0 22 -3 22.05 8.20 0 22 -3 2.85 5.28 0 22 3 22.84 9.45 0 22 3 17.03 8.91 0 22 4 9.34 4.11 0 22 4 52.90 11.94 0 22 -4 1.68 5.74 0 22 4 42.75 9.57 0 22 -4 25.88 9.62 0 22 -5 -2.07 4.54 0 22 5 -7.31 4.81 0 22 6 35.58 6.97 0 22 -6 66.01 12.49 0 22 -6 49.65 9.41 0 22 6 81.88 11.91 0 22 7 20.33 5.76 0 22 -7 19.34 6.66 0 22 -8 86.11 11.76 0 22 8 105.79 12.34 0 22 9 -6.89 4.28 0 22 -9 -10.64 6.09 0 22 -10 -10.84 6.00 0 22 10 -8.24 5.52 0 22 11 2.06 2.75 0 22 -11 10.75 3.66 0 22 12 -9.23 4.88 0 22 -12 -3.07 4.42 0 22 -13 -2.75 3.15 0 22 13 -12.75 4.98 0 22 14 -6.39 3.99 0 22 -14 0.40 2.04 0 22 15 -4.95 3.12 0 22 16 -2.09 2.29 0 23 0 62.86 11.03 0 23 0 34.77 8.53 0 23 1 77.64 11.56 0 23 -1 43.54 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13.03 4 10 -17 57.70 13.42 -4 10 17 49.85 9.66 -4 10 16 2.78 4.08 4 10 -16 8.68 6.87 -4 10 15 16.15 5.74 4 10 -15 13.26 7.22 -4 10 15 7.93 6.11 -4 10 14 54.25 13.57 4 10 -14 87.08 13.79 4 10 -13 538.82 43.27 -4 10 13 525.20 43.00 -4 10 12 206.95 27.22 4 10 -12 202.09 26.75 4 10 -11 11.81 8.12 -4 10 11 11.09 4.52 4 10 -10 89.29 18.16 -4 10 10 101.26 19.11 4 10 -9 84.06 16.83 -4 10 9 100.59 18.36 4 10 -8 43.08 12.21 -4 10 8 39.67 10.88 -4 10 7 13.84 8.68 4 10 -7 15.28 6.92 -4 10 6 5.75 4.74 4 10 -6 10.39 7.16 -4 10 5 50.94 13.25 4 10 -5 54.72 11.41 4 10 -4 57.63 11.18 -4 10 4 44.12 12.29 4 10 -3 38.23 9.09 -4 10 3 43.85 13.88 -4 10 3 43.59 10.90 -4 10 2 154.95 20.28 4 10 -2 150.01 18.07 -4 10 2 145.48 23.87 -4 10 1 22.35 9.83 -4 10 1 -1.27 7.78 -4 10 0 81.66 19.58 -4 10 0 113.03 19.40 -4 10 -1 731.16 53.81 -4 10 -2 10.31 8.29 -4 10 -3 169.47 27.07 -4 10 -4 175.46 26.53 -4 10 -5 49.89 16.03 -4 10 -6 50.75 14.79 -4 10 -7 72.52 19.19 -4 10 -8 0.23 8.07 -4 10 -8 0.92 3.64 -4 10 -9 24.57 7.70 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14 9.29 5.24 4 11 -14 15.47 10.36 4 11 -14 19.01 8.64 4 11 -13 986.76 59.55 -4 11 13 1013.92 39.34 4 11 -13 1081.30 47.12 4 11 -12 724.95 49.94 4 11 -12 728.66 37.80 4 11 -11 164.27 23.57 4 11 -10 108.57 19.28 -4 11 9 -1.43 5.86 4 11 -9 7.50 5.76 -4 11 8 3.78 5.76 4 11 -8 1.50 3.65 4 11 -7 38.08 11.26 -4 11 7 31.48 9.83 -4 11 6 27.55 9.28 4 11 -6 35.32 10.95 -4 11 5 203.47 23.66 4 11 -5 213.11 23.07 -4 11 4 75.48 15.24 4 11 -4 78.40 13.71 4 11 -3 24.24 6.96 -4 11 3 14.18 8.26 -4 11 2 116.11 18.36 -4 11 2 78.63 19.56 4 11 -2 105.74 15.76 -4 11 1 93.64 20.08 -4 11 0 314.90 36.38 -4 11 -1 171.63 26.80 -4 11 -2 64.56 16.32 -4 11 -3 12.72 8.83 -4 11 -4 360.30 39.97 -4 11 -5 -2.80 9.42 -4 11 -6 17.06 10.35 -4 11 -7 11.21 9.84 -4 11 -8 14.33 10.14 -4 11 -9 99.92 23.57 4 11 9 104.72 17.18 4 11 10 18.56 6.66 4 11 10 22.92 9.46 -4 11 -10 44.73 19.63 4 11 10 18.50 7.06 -4 11 -11 145.01 28.75 4 11 11 136.61 15.72 4 11 11 164.59 19.86 4 11 11 155.35 17.54 4 11 12 164.96 18.35 -4 11 -12 88.19 23.30 4 11 12 139.54 19.64 4 11 12 139.95 21.32 4 11 13 24.86 7.96 4 11 13 36.97 10.76 4 11 13 27.36 8.36 -4 11 -13 37.63 16.74 4 11 14 115.20 16.02 4 11 14 97.01 16.98 -4 11 -14 112.29 25.84 4 11 14 120.43 15.94 4 11 15 4.46 5.67 -4 11 -15 -5.74 13.20 4 11 15 3.22 5.24 4 11 15 -4.40 5.85 4 11 16 25.87 7.20 4 11 16 25.76 7.68 4 11 16 10.08 3.80 -4 11 -16 13.63 9.86 4 11 16 3.67 3.94 4 11 17 69.87 11.66 4 11 17 70.49 11.88 4 11 17 73.25 14.44 4 11 17 63.34 12.42 4 11 18 26.92 7.03 4 11 18 30.62 8.58 4 11 18 40.77 11.92 4 11 18 30.71 9.02 4 11 19 6.26 3.35 4 11 19 7.99 4.71 4 11 19 0.70 4.15 4 11 20 32.99 8.67 4 11 20 18.39 7.50 4 11 20 15.72 6.77 4 11 21 39.65 9.90 4 11 21 33.08 9.68 4 11 21 27.53 8.47 4 11 22 8.47 4.86 4 11 22 1.78 3.89 4 11 22 1.71 4.27 4 11 23 15.15 5.86 4 11 23 7.48 5.59 4 11 23 5.00 3.83 4 11 24 -0.54 3.41 4 11 24 5.63 5.51 4 11 24 2.88 4.31 4 11 25 21.67 5.67 4 11 25 14.45 5.87 4 11 25 22.61 8.00 4 11 26 2.39 4.28 4 11 26 3.60 3.85 4 11 27 7.73 5.04 4 11 27 4.59 3.07 4 11 28 39.30 7.60 4 11 28 52.54 6.67 4 11 29 33.17 6.15 4 11 30 17.02 3.97 -4 12 32 16.64 4.45 -4 12 32 15.80 4.24 -4 12 31 0.05 2.97 -4 12 30 65.61 10.69 -4 12 29 17.78 7.21 -4 12 28 6.40 6.13 -4 12 27 12.06 6.98 -4 12 26 33.84 10.03 4 12 -26 29.11 6.73 4 12 -25 33.86 8.42 -4 12 25 43.00 11.41 4 12 -24 6.21 3.79 -4 12 24 8.33 6.93 4 12 -23 58.04 11.74 -4 12 23 70.59 16.19 4 12 -22 11.88 6.65 -4 12 22 14.44 8.95 4 12 -21 1.32 3.73 4 12 -21 0.01 4.43 -4 12 20 4.54 6.79 4 12 -20 7.20 5.41 4 12 -20 18.63 9.07 4 12 -19 3.44 5.90 4 12 -19 -0.67 3.79 4 12 -18 46.01 11.71 -4 12 17 4.62 4.11 4 12 -17 4.13 6.14 -4 12 16 332.24 23.16 4 12 -16 349.77 30.94 -4 12 15 28.05 6.96 4 12 -15 43.52 11.83 -4 12 14 64.00 12.79 -4 12 14 60.15 9.43 4 12 -14 81.07 15.07 -4 12 13 -0.65 5.23 -4 12 13 10.08 5.62 4 12 -13 -3.72 6.18 4 12 -13 -0.34 4.15 4 12 -12 19.67 10.17 -4 12 12 14.90 5.44 4 12 -12 24.87 7.94 -4 12 12 23.81 8.33 4 12 -11 103.88 14.68 -4 12 11 101.01 14.93 4 12 -11 107.26 18.45 -4 12 10 63.59 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4 13 -23 7.18 4.95 4 13 -22 2.19 3.49 -4 13 22 -4.33 7.34 -4 13 21 -0.85 5.57 4 13 -21 2.46 3.97 4 13 -21 8.93 6.47 -4 13 20 9.11 7.68 4 13 -20 11.64 5.95 4 13 -20 -2.50 5.52 -4 13 19 86.50 17.22 4 13 -19 90.89 15.41 4 13 -19 77.95 15.11 -4 13 18 67.95 15.00 4 13 -18 78.70 14.70 4 13 -18 73.24 14.94 4 13 -17 94.75 17.33 -4 13 17 78.85 16.41 4 13 -17 73.86 14.91 -4 13 16 58.36 13.99 4 13 -16 63.18 13.63 4 13 -16 50.48 11.92 -4 13 15 17.01 8.32 4 13 -15 17.28 8.18 4 13 -15 17.88 8.62 -4 13 14 37.73 10.95 4 13 -14 28.78 9.48 4 13 -14 43.03 11.55 -4 13 13 78.88 14.96 4 13 -13 93.83 16.02 4 13 -13 76.57 14.14 4 13 -12 497.82 34.97 4 13 -12 456.61 33.17 -4 13 12 433.30 34.05 4 13 -11 302.70 27.69 4 13 -11 336.95 27.75 -4 13 11 267.84 25.85 4 13 -10 421.56 31.72 -4 13 10 385.26 29.40 4 13 -10 421.80 30.60 4 13 -10 438.21 33.01 -4 13 10 398.69 27.77 4 13 -9 88.54 13.87 4 13 -9 89.63 14.68 -4 13 9 77.44 13.19 4 13 -9 89.44 15.26 -4 13 9 117.05 16.20 -4 13 8 28.82 12.65 4 13 -8 5.40 4.74 -4 13 8 0.01 3.86 4 13 -8 7.65 4.79 4 13 -8 -1.38 6.67 -4 13 8 0.14 3.75 4 13 -8 9.60 6.24 -4 13 8 28.54 10.43 -4 13 7 37.51 10.53 -4 13 7 32.25 12.07 4 13 -7 17.69 5.65 -4 13 7 14.52 4.94 4 13 -7 19.75 6.46 4 13 -7 19.60 6.96 4 13 -7 16.54 5.13 4 13 -6 125.43 13.17 4 13 -6 138.32 17.94 -4 13 6 137.46 18.26 -4 13 6 109.11 14.08 4 13 -6 142.32 17.13 -4 13 6 148.97 17.39 4 13 -6 135.93 16.75 4 13 -5 225.92 21.71 -4 13 5 194.05 19.42 4 13 -5 238.17 22.67 -4 13 5 194.16 21.18 4 13 -5 214.82 20.28 -4 13 4 92.76 14.43 4 13 -4 116.81 15.10 4 13 -4 106.88 15.06 4 13 -4 103.79 14.75 -4 13 4 91.82 14.14 -4 13 3 60.51 10.62 -4 13 3 35.81 7.85 4 13 -3 52.42 9.93 4 13 -3 73.15 13.35 4 13 -3 50.60 9.70 -4 13 2 8.32 5.92 4 13 -2 3.77 4.25 -4 13 2 0.75 4.54 4 13 -2 -2.82 5.62 4 13 -2 3.43 3.84 -4 13 1 54.03 10.76 -4 13 1 61.38 16.55 4 13 -1 63.19 11.33 4 13 -1 41.79 8.41 4 13 -1 62.17 10.27 -4 13 1 40.32 7.61 4 13 0 62.05 12.12 -4 13 0 47.62 9.81 -4 13 0 42.24 8.48 -4 13 0 41.42 9.17 -4 13 0 46.57 17.16 4 13 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7.55 4 13 12 19.50 6.80 4 13 12 11.60 6.15 4 13 13 12.63 7.38 4 13 13 5.97 4.83 4 13 13 13.47 7.89 4 13 14 46.99 11.68 4 13 14 62.88 12.05 4 13 14 61.10 13.94 4 13 15 8.16 5.59 4 13 15 12.40 6.50 4 13 15 12.19 6.30 4 13 16 19.71 8.22 4 13 16 24.81 8.23 4 13 16 26.31 9.32 4 13 17 -0.47 4.14 4 13 17 -2.40 5.29 4 13 17 1.26 5.92 4 13 18 17.51 6.16 4 13 18 9.21 5.06 4 13 18 -0.59 4.51 4 13 19 2.06 3.83 4 13 19 -3.81 5.24 4 13 19 0.48 6.50 4 13 20 5.31 3.10 4 13 20 -3.51 3.72 4 13 20 -8.80 6.25 4 13 21 -1.81 3.49 4 13 21 3.90 4.33 4 13 22 18.20 6.50 4 13 22 16.08 5.46 4 13 23 1.20 3.07 4 13 23 0.53 3.72 4 13 24 -0.31 3.77 4 13 24 3.56 3.40 4 13 25 -0.18 4.08 4 13 25 1.35 3.44 4 13 26 26.18 5.84 4 13 26 22.32 5.65 4 13 27 0.47 2.04 4 13 27 -2.23 2.70 4 13 28 3.08 1.74 -4 14 30 -0.06 2.62 -4 14 30 -2.06 2.23 -4 14 29 15.56 4.85 -4 14 29 14.89 5.20 -4 14 28 12.61 5.49 -4 14 28 8.34 5.05 -4 14 27 30.34 7.19 -4 14 27 33.98 8.57 4 14 -26 5.10 3.61 -4 14 26 -4.22 5.00 -4 14 25 28.04 9.14 4 14 -25 22.43 6.05 -4 14 24 -6.24 6.57 4 14 -24 4.27 4.10 4 14 -23 16.51 6.31 -4 14 23 11.70 8.13 -4 14 22 24.34 10.51 4 14 -22 21.59 8.28 4 14 -21 -3.51 4.26 -4 14 21 3.28 6.85 4 14 -21 -10.94 6.55 -4 14 20 4.14 7.05 4 14 -20 6.55 4.84 4 14 -20 0.15 4.89 -4 14 19 1.41 7.23 4 14 -19 3.64 5.30 4 14 -19 1.03 5.02 -4 14 18 9.12 6.92 4 14 -18 0.93 4.67 4 14 -18 3.73 6.03 -4 14 17 18.03 7.72 4 14 -17 18.18 7.09 4 14 -17 16.48 7.40 4 14 -16 30.54 9.92 4 14 -16 29.21 9.97 -4 14 16 28.06 9.95 4 14 -15 158.21 20.91 -4 14 15 150.55 21.64 4 14 -15 167.68 21.12 4 14 -14 102.58 16.69 4 14 -14 129.03 19.01 -4 14 14 101.96 18.17 4 14 -13 30.16 9.54 -4 14 13 41.73 11.79 4 14 -13 52.86 12.46 -4 14 12 0.15 4.87 4 14 -12 0.75 4.65 4 14 -12 2.06 4.61 4 14 -11 76.72 14.60 4 14 -11 76.69 14.70 -4 14 11 68.01 14.38 -4 14 10 2.93 4.00 4 14 -10 15.80 7.25 4 14 -10 13.36 6.65 4 14 -10 22.14 10.93 4 14 -9 97.32 15.05 -4 14 9 130.15 23.23 -4 14 9 79.17 13.20 4 14 -9 85.99 15.97 4 14 -9 87.66 14.56 -4 14 9 134.18 18.49 4 14 -8 81.12 13.72 -4 14 8 111.01 20.04 4 14 -8 85.91 14.21 -4 14 8 124.17 18.48 -4 14 8 61.35 11.42 4 14 -8 85.81 15.54 -4 14 7 16.10 10.96 4 14 -7 4.33 4.34 4 14 -7 -0.41 2.19 -4 14 7 0.48 4.96 4 14 -7 -4.96 7.68 4 14 -7 11.03 6.95 -4 14 7 19.18 10.79 -4 14 6 58.32 13.01 4 14 -6 19.85 5.53 -4 14 6 32.79 11.98 4 14 -6 28.24 6.84 -4 14 6 23.25 6.89 4 14 -6 35.57 10.12 4 14 -6 24.29 7.51 -4 14 5 60.77 14.41 4 14 -5 38.28 7.62 4 14 -5 54.73 11.05 -4 14 5 36.20 8.18 4 14 -5 46.21 10.10 4 14 -5 46.97 11.71 -4 14 5 41.57 12.37 -4 14 4 71.42 14.40 4 14 -4 72.18 12.50 -4 14 4 72.21 13.20 4 14 -4 57.89 11.23 4 14 -4 72.33 13.15 -4 14 4 42.93 9.23 -4 14 3 67.13 12.75 4 14 -3 107.88 16.39 -4 14 3 75.53 12.14 4 14 -3 79.81 12.60 4 14 -3 97.88 14.89 -4 14 3 95.54 15.45 4 14 -2 51.46 10.24 -4 14 2 60.76 11.31 -4 14 2 61.45 11.79 4 14 -2 51.96 11.93 4 14 -2 63.88 11.09 -4 14 2 29.61 8.39 -4 14 1 53.23 12.55 4 14 -1 24.70 8.71 -4 14 1 30.35 8.41 4 14 -1 32.48 8.51 -4 14 1 24.49 8.54 4 14 -1 21.61 5.32 4 14 0 463.05 29.05 4 14 0 473.76 34.38 -4 14 0 367.94 28.94 -4 14 0 415.45 28.56 -4 14 0 443.29 48.90 4 14 0 457.71 32.94 -4 14 0 379.24 28.78 4 14 1 17.01 10.33 -4 14 -1 17.88 9.52 -4 14 -1 -10.44 8.91 4 14 1 11.86 6.12 4 14 1 0.23 3.54 -4 14 -1 1.43 5.91 -4 14 -1 5.77 5.12 -4 14 -2 126.07 25.95 -4 14 -2 125.20 16.16 -4 14 -2 135.86 17.39 4 14 2 150.03 20.07 4 14 2 148.79 15.76 4 14 2 146.59 19.43 -4 14 -2 146.59 18.81 -4 14 -3 47.17 12.33 4 14 3 26.61 10.02 -4 14 -3 20.34 10.45 -4 14 -3 19.83 7.84 4 14 3 34.80 11.68 4 14 3 22.97 6.80 -4 14 -3 24.23 8.57 4 14 4 13.83 6.64 -4 14 -4 3.92 6.66 4 14 4 -0.13 5.37 -4 14 -4 8.85 5.67 -4 14 -4 11.99 3.93 -4 14 -5 52.52 18.94 4 14 5 46.56 11.08 -4 14 -5 42.87 10.51 4 14 5 44.27 11.21 -4 14 -5 76.75 14.23 -4 14 -6 23.93 12.14 4 14 6 25.11 9.20 -4 14 -6 26.81 9.67 4 14 6 24.79 9.20 4 14 7 14.13 6.64 -4 14 -7 14.41 7.94 4 14 7 12.67 6.93 -4 14 -7 8.57 6.61 -4 14 -8 265.31 39.06 4 14 8 245.95 26.02 4 14 8 255.61 27.83 -4 14 -8 268.58 23.83 -4 14 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6.00 -4 15 27 14.90 4.69 -4 15 26 33.27 8.73 -4 15 26 33.26 7.05 4 15 -26 17.38 3.84 -4 15 25 -0.81 4.02 4 15 -25 -4.83 3.19 -4 15 25 1.51 3.87 -4 15 24 4.33 4.20 4 15 -24 2.15 3.60 -4 15 24 3.80 3.89 -4 15 23 17.80 7.68 -4 15 23 22.83 7.52 4 15 -23 19.80 6.51 4 15 -22 16.78 6.68 -4 15 22 17.32 6.27 -4 15 22 3.12 5.03 -4 15 21 3.35 4.93 4 15 -21 2.94 3.95 -4 15 21 5.39 6.06 -4 15 20 -3.37 6.49 -4 15 20 -1.48 6.00 4 15 -20 -4.13 4.11 4 15 -20 0.45 4.13 4 15 -19 0.97 5.72 4 15 -19 -4.16 5.29 -4 15 19 0.35 6.50 -4 15 19 -7.11 7.18 -4 15 18 2.39 5.02 4 15 -18 -3.38 4.60 -4 15 18 3.36 4.37 4 15 -18 -0.40 5.44 4 15 -17 8.10 6.59 4 15 -17 3.29 5.54 -4 15 17 -2.64 5.91 -4 15 17 -5.66 5.36 -4 15 16 13.72 7.88 4 15 -16 9.16 6.41 -4 15 16 6.24 4.56 4 15 -16 21.83 8.43 4 15 -15 26.53 9.27 -4 15 15 16.40 9.14 4 15 -15 25.96 8.37 4 15 -14 44.27 11.65 -4 15 14 40.76 11.24 4 15 -14 54.99 12.61 4 15 -13 23.30 9.75 4 15 -13 28.70 10.12 -4 15 13 12.09 7.44 4 15 -12 98.87 16.86 -4 15 12 130.95 20.88 4 15 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31.92 -4 15 1 312.19 28.72 -4 15 1 387.31 27.62 -4 15 1 355.63 29.35 4 15 0 8.45 5.97 -4 15 0 7.27 5.59 4 15 0 13.99 7.96 -4 15 0 12.94 6.45 4 15 0 20.04 7.30 4 15 1 172.69 21.14 4 15 1 173.72 21.48 -4 15 -1 184.33 19.97 -4 15 -1 194.52 33.26 4 15 1 196.93 20.06 -4 15 -1 168.13 20.16 -4 15 -1 178.14 22.29 -4 15 -2 60.18 18.75 -4 15 -2 54.92 10.39 -4 15 -2 57.47 10.42 4 15 2 71.39 14.37 4 15 2 76.05 12.19 -4 15 -2 110.43 18.13 4 15 2 83.49 14.98 -4 15 -3 46.79 14.75 4 15 3 90.91 12.96 4 15 3 90.07 16.36 -4 15 -3 77.83 13.41 4 15 3 89.84 16.23 -4 15 -3 44.39 8.98 -4 15 -3 93.34 17.13 4 15 4 13.37 7.61 -4 15 -4 18.14 6.73 -4 15 -4 -6.06 9.45 -4 15 -4 19.61 7.28 4 15 4 1.10 4.30 4 15 5 89.40 16.05 -4 15 -5 71.23 18.84 4 15 5 79.51 15.49 -4 15 -5 96.04 15.49 -4 15 -5 50.71 9.82 4 15 6 6.43 6.66 -4 15 -6 -0.85 4.79 4 15 6 -7.00 6.69 4 15 7 26.73 9.93 4 15 7 19.76 7.70 4 15 8 91.64 16.54 4 15 8 89.93 17.20 -4 15 -8 72.74 12.61 4 15 9 54.99 12.08 4 15 9 67.77 15.32 -4 15 -9 58.05 9.60 4 15 10 19.94 8.32 -4 15 -10 5.57 4.05 4 15 10 21.25 9.58 4 15 11 5.95 5.95 4 15 11 -1.15 6.04 4 15 12 -4.49 5.40 4 15 12 0.26 5.74 4 15 13 -0.80 4.25 4 15 13 -1.84 5.64 4 15 14 2.85 5.10 4 15 14 6.22 5.51 4 15 15 6.24 5.76 4 15 15 8.60 7.60 4 15 16 52.68 10.36 4 15 16 50.84 12.57 4 15 17 5.44 3.46 4 15 17 12.28 5.02 4 15 17 3.52 5.24 4 15 18 7.75 4.86 4 15 18 4.21 4.84 4 15 18 6.36 3.33 4 15 19 3.56 3.50 4 15 19 0.39 4.45 4 15 19 7.22 3.96 4 15 20 0.43 3.01 4 15 20 7.12 5.79 4 15 20 -1.42 3.36 4 15 21 86.40 13.39 4 15 21 78.06 9.49 4 15 21 87.71 9.70 4 15 22 -1.89 2.86 4 15 22 -2.64 3.96 4 15 23 70.57 10.20 4 15 23 49.91 6.31 4 15 24 -0.37 3.65 4 15 24 4.77 2.18 4 15 25 -1.87 2.92 -4 15 -26 121.59 10.68 -4 16 28 4.73 2.57 -4 16 27 1.72 3.15 -4 16 26 2.38 3.11 -4 16 26 2.10 1.97 -4 16 25 17.23 4.18 4 16 -25 9.92 2.78 4 16 -24 -4.19 3.15 -4 16 24 -5.11 5.18 -4 16 24 -4.23 3.81 -4 16 23 16.67 7.20 4 16 -23 14.04 5.24 -4 16 23 14.47 5.28 -4 16 22 1.69 4.12 4 16 -22 7.02 4.57 -4 16 22 3.77 5.02 -4 16 21 15.31 6.52 -4 16 21 7.41 3.43 4 16 -21 15.18 6.51 -4 16 20 27.17 8.97 4 16 -20 25.77 7.54 -4 16 20 27.22 7.27 -4 16 19 9.67 6.61 4 16 -19 7.05 5.59 4 16 -19 -6.64 5.01 -4 16 19 -1.34 3.34 -4 16 18 3.53 5.70 4 16 -18 6.64 6.22 -4 16 18 -1.49 4.37 4 16 -18 -4.19 5.30 4 16 -17 13.14 5.65 -4 16 17 12.83 5.16 4 16 -17 0.83 4.26 -4 16 17 18.95 8.92 -4 16 16 6.44 4.42 4 16 -16 11.31 6.81 4 16 -16 18.66 8.05 -4 16 15 65.05 13.78 4 16 -15 53.67 12.46 4 16 -15 70.67 14.04 -4 16 14 11.30 7.06 4 16 -14 8.00 6.01 4 16 -14 11.27 6.72 4 16 -13 74.06 14.19 -4 16 13 49.65 11.57 4 16 -13 56.88 12.31 -4 16 12 63.28 13.68 4 16 -12 58.42 12.54 4 16 -12 57.88 12.63 -4 16 11 82.62 14.81 4 16 -11 79.82 14.15 4 16 -11 85.54 14.87 -4 16 10 3.62 4.87 4 16 -10 16.91 8.33 4 16 -10 7.81 4.96 -4 16 9 28.14 8.51 4 16 -9 20.18 7.85 4 16 -9 24.43 7.07 4 16 -9 50.41 13.95 -4 16 8 12.27 6.12 -4 16 8 108.58 23.05 4 16 -8 8.42 6.73 4 16 -8 15.27 10.59 -4 16 8 123.85 20.84 -4 16 7 -5.19 5.51 -4 16 7 58.57 19.55 4 16 -7 -6.66 7.03 4 16 -7 -3.08 5.15 4 16 -7 9.74 7.49 -4 16 7 80.05 17.98 4 16 -6 12.78 6.22 -4 16 6 35.20 14.85 4 16 -6 12.95 6.34 4 16 -6 15.51 8.95 4 16 -5 57.87 12.73 -4 16 5 75.51 17.46 4 16 -5 58.41 12.35 4 16 -5 60.46 12.64 -4 16 5 102.50 19.18 -4 16 4 27.19 14.02 4 16 -4 14.35 8.01 4 16 -4 10.44 6.02 4 16 -4 7.50 5.62 -4 16 3 164.25 22.75 4 16 -3 124.78 17.63 4 16 -3 120.77 17.89 -4 16 3 125.65 20.36 4 16 -3 127.17 19.47 4 16 -2 256.34 25.97 4 16 -2 241.40 25.26 -4 16 2 233.33 21.08 4 16 -2 274.21 25.85 -4 16 2 233.53 25.62 -4 16 2 265.02 26.80 4 16 -1 53.27 11.97 -4 16 1 44.71 12.97 4 16 -1 29.98 9.87 4 16 -1 42.63 11.99 -4 16 1 40.46 9.91 -4 16 1 81.30 18.04 4 16 0 332.88 30.22 4 16 0 342.57 28.03 -4 16 0 263.47 26.88 -4 16 0 287.93 24.24 4 16 0 291.69 27.89 -4 16 0 313.16 28.80 -4 16 -1 97.41 16.17 -4 16 -1 117.43 16.13 4 16 1 128.03 19.39 4 16 1 130.73 17.31 4 16 1 106.53 16.87 -4 16 -1 131.63 20.44 -4 16 -2 26.90 8.53 4 16 2 26.61 7.41 4 16 2 45.92 12.13 -4 16 -2 44.79 10.23 4 16 2 42.78 9.76 -4 16 -3 137.52 17.88 -4 16 -3 106.92 16.37 4 16 3 133.64 16.45 4 16 3 127.29 19.68 4 16 3 114.02 16.94 4 16 4 5.44 5.59 4 16 4 -3.43 5.74 -4 16 -4 -3.87 8.41 4 16 4 -4.51 6.67 -4 16 -4 1.07 4.23 4 16 5 41.55 12.33 -4 16 -5 46.51 10.67 4 16 5 45.78 12.54 -4 16 -5 38.35 9.49 4 16 6 27.96 10.58 -4 16 -6 26.15 9.16 -4 16 -6 9.23 7.34 4 16 6 29.33 10.26 4 16 7 9.99 6.24 -4 16 -7 -3.57 8.13 4 16 7 3.82 4.70 -4 16 -7 -4.42 6.79 4 16 8 5.95 5.69 -4 16 -8 -1.81 3.77 4 16 8 -4.01 7.91 -4 16 -8 -3.38 9.22 4 16 9 2.13 4.52 -4 16 -9 -7.08 6.98 4 16 9 -2.15 6.84 4 16 10 3.83 4.69 -4 16 -10 0.77 5.66 4 16 10 10.30 6.92 4 16 11 4.20 5.02 4 16 11 0.80 5.10 -4 16 -11 1.30 6.35 4 16 12 8.29 6.86 4 16 12 7.82 7.55 4 16 13 9.39 5.93 4 16 13 11.88 6.55 4 16 14 2.05 4.51 4 16 14 5.39 5.69 4 16 15 1.11 4.24 4 16 15 6.09 5.53 4 16 16 -2.59 4.72 4 16 16 3.90 5.28 4 16 17 0.45 3.45 4 16 17 5.37 5.74 4 16 18 16.43 5.32 4 16 18 8.23 5.17 4 16 19 -2.41 3.46 4 16 19 4.38 5.02 4 16 20 -0.43 3.60 4 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8 42.66 9.08 5 11 8 53.22 11.00 5 11 8 54.38 10.04 -5 11 -8 65.77 17.83 5 11 9 118.94 15.08 -5 11 -9 117.36 24.99 5 11 9 124.34 17.69 5 11 9 114.77 14.10 5 11 10 73.42 12.61 5 11 10 86.31 13.31 5 11 10 71.63 13.66 -5 11 -10 102.56 23.11 5 11 11 153.76 16.24 5 11 11 181.79 21.42 5 11 11 162.50 19.14 -5 11 -11 152.00 28.33 5 11 12 17.72 6.81 5 11 12 20.04 8.39 5 11 12 13.25 4.99 -5 11 -12 25.84 13.58 5 11 13 159.29 17.56 -5 11 -13 157.53 28.08 5 11 13 177.49 20.53 5 11 13 163.12 17.60 5 11 13 186.29 22.30 5 11 14 17.92 5.44 5 11 14 27.57 9.74 5 11 14 30.60 9.01 -5 11 -14 26.53 12.67 5 11 15 -1.49 3.81 5 11 15 -0.97 3.91 5 11 15 -0.27 4.98 5 11 16 3.63 4.57 5 11 16 2.56 4.21 5 11 16 1.68 5.33 5 11 17 -2.29 5.70 5 11 17 -3.97 4.30 5 11 17 7.02 6.04 5 11 18 24.89 7.58 5 11 18 29.33 8.06 5 11 18 31.84 10.49 5 11 19 61.29 11.55 5 11 19 77.22 14.04 5 11 19 71.01 13.61 5 11 20 6.07 3.41 5 11 20 -1.40 4.71 5 11 20 9.02 5.87 5 11 21 -4.08 5.87 5 11 21 -4.64 5.31 5 11 21 6.73 4.28 5 11 22 5.12 5.46 5 11 22 1.77 4.41 5 11 22 0.86 3.99 5 11 23 15.49 6.77 5 11 23 11.78 5.10 5 11 24 2.73 3.64 5 11 24 2.20 3.60 5 11 25 5.68 3.93 5 11 25 4.90 5.11 5 11 26 -0.70 3.24 5 11 26 0.72 2.09 5 11 27 -1.22 2.76 5 11 28 6.81 3.54 5 11 29 11.05 3.15 -5 12 32 -2.03 2.47 -5 12 32 2.86 2.06 -5 12 31 -2.43 3.32 -5 12 30 2.37 3.75 -5 12 29 25.79 7.82 5 12 -28 16.12 4.47 -5 12 28 18.23 7.00 -5 12 27 50.93 11.83 5 12 -27 33.14 6.85 -5 12 26 72.73 15.45 5 12 -26 56.62 10.14 5 12 -25 -8.66 5.89 -5 12 25 8.13 6.46 -5 12 24 75.98 15.12 5 12 -24 64.69 11.88 -5 12 23 0.63 5.41 5 12 -23 11.72 5.67 -5 12 22 2.33 3.38 5 12 -22 1.23 3.94 -5 12 22 -3.09 5.80 5 12 -22 1.26 7.11 -5 12 21 2.71 4.66 5 12 -21 1.85 5.42 -5 12 21 2.64 6.30 -5 12 20 82.16 12.74 5 12 -20 80.82 14.86 -5 12 19 8.69 5.16 5 12 -19 15.97 7.03 -5 12 18 5.36 5.46 5 12 -18 12.95 6.79 5 12 -17 63.14 15.28 -5 12 17 48.17 10.22 -5 12 16 28.43 8.26 5 12 -16 45.76 13.09 5 12 -15 8.81 7.01 -5 12 15 6.95 5.66 -5 12 14 24.21 8.12 5 12 -14 29.34 10.59 -5 12 13 108.88 14.50 5 12 -13 116.54 18.59 -5 12 13 106.93 16.51 -5 12 12 454.34 29.43 5 12 -12 471.82 35.16 -5 12 12 423.20 31.58 5 12 -11 353.20 29.56 -5 12 11 319.51 25.92 -5 12 10 89.94 12.63 5 12 -10 112.72 14.78 5 12 -10 133.22 17.86 5 12 -10 135.84 19.42 5 12 -9 1.96 3.48 5 12 -9 -0.91 4.76 -5 12 9 0.95 3.57 5 12 -8 82.47 12.95 5 12 -8 92.43 12.35 -5 12 8 73.48 12.81 5 12 -8 102.98 16.23 5 12 -7 87.17 11.80 -5 12 7 90.28 13.84 -5 12 7 126.86 20.77 5 12 -7 76.76 12.50 5 12 -7 89.11 15.18 -5 12 6 354.54 32.46 5 12 -6 360.68 23.55 -5 12 6 321.79 27.67 -5 12 6 323.43 25.16 5 12 -6 357.76 27.86 5 12 -6 355.74 27.83 -5 12 5 41.21 12.35 -5 12 5 19.95 8.10 5 12 -5 29.93 6.94 5 12 -5 33.73 9.11 -5 12 5 33.94 8.74 5 12 -5 28.26 6.95 5 12 -5 36.14 8.59 -5 12 4 92.92 16.80 -5 12 4 86.37 13.80 5 12 -4 111.46 13.79 -5 12 4 101.59 14.18 5 12 -4 98.15 14.09 5 12 -4 118.48 15.27 -5 12 4 144.23 18.20 -5 12 3 13.80 6.67 -5 12 3 18.54 7.41 5 12 -3 17.92 7.53 -5 12 3 19.98 6.79 5 12 -3 12.51 4.94 5 12 -2 39.87 10.52 -5 12 2 21.57 7.58 -5 12 2 18.78 5.85 5 12 -2 30.87 8.31 -5 12 1 10.44 7.73 -5 12 1 31.08 7.84 5 12 -1 27.05 8.01 -5 12 1 28.62 7.92 5 12 -1 25.82 7.60 -5 12 0 55.38 17.17 -5 12 0 62.87 11.27 5 12 0 66.58 11.21 5 12 0 60.26 12.35 -5 12 -1 2.96 5.23 5 12 1 6.42 6.39 -5 12 -1 13.77 4.68 5 12 2 9.09 7.82 -5 12 -2 3.05 10.43 -5 12 -2 8.54 6.48 5 12 2 3.04 6.75 -5 12 -2 3.41 5.15 5 12 3 178.40 20.78 -5 12 -3 191.12 30.60 5 12 3 188.89 19.79 -5 12 -3 143.55 15.64 5 12 4 5.96 5.75 -5 12 -4 10.82 10.68 5 12 4 -3.19 6.40 -5 12 -4 2.36 4.87 -5 12 -5 32.91 14.45 5 12 5 43.45 9.49 -5 12 -5 28.50 6.57 5 12 5 49.70 11.37 5 12 6 52.43 10.49 5 12 6 36.21 7.17 5 12 6 43.84 10.39 -5 12 -6 48.59 16.82 5 12 7 49.60 10.86 5 12 7 27.61 6.51 5 12 7 45.22 12.45 -5 12 -7 57.99 18.89 5 12 8 300.92 23.07 -5 12 -8 328.79 41.64 5 12 8 333.60 26.30 5 12 8 322.31 29.28 5 12 9 1.80 3.15 5 12 9 0.02 4.80 5 12 9 5.20 4.06 -5 12 -9 2.86 7.68 5 12 10 126.58 16.57 5 12 10 133.52 18.75 5 12 10 115.49 15.42 -5 12 -10 109.00 23.98 5 12 11 50.81 10.88 5 12 11 41.99 9.99 5 12 11 42.56 12.09 -5 12 -11 61.24 17.26 5 12 12 23.56 6.83 5 12 12 28.59 8.25 5 12 12 22.31 8.33 -5 12 -12 19.18 13.26 5 12 13 38.67 9.07 5 12 13 49.43 12.77 5 12 13 45.30 10.70 5 12 14 11.30 5.19 5 12 14 10.33 8.52 5 12 14 19.02 8.64 5 12 15 35.24 8.32 5 12 15 29.51 9.29 5 12 15 33.48 10.41 5 12 16 9.05 5.28 5 12 16 8.27 5.37 5 12 17 92.91 16.61 5 12 17 82.34 14.52 5 12 18 4.76 5.69 5 12 18 5.80 5.79 5 12 19 36.62 9.44 5 12 19 49.79 11.75 5 12 20 4.18 4.03 5 12 20 4.14 5.09 5 12 21 0.75 4.62 5 12 21 -2.03 5.52 5 12 22 -3.83 5.04 5 12 22 0.62 4.09 5 12 23 4.78 3.82 5 12 23 2.15 4.21 5 12 24 89.98 11.48 5 12 24 78.57 11.60 5 12 25 1.17 2.84 5 12 25 4.62 3.95 5 12 26 0.69 2.61 5 12 26 -2.42 2.49 5 12 27 4.15 2.59 5 12 28 -3.72 2.19 -5 13 31 6.83 2.73 -5 13 30 10.45 4.95 -5 13 30 12.01 3.64 -5 13 29 1.18 3.51 -5 13 28 8.79 4.44 -5 13 27 12.78 6.51 5 13 -27 5.38 2.61 -5 13 26 11.99 7.10 5 13 -26 6.65 3.53 -5 13 25 71.85 14.75 5 13 -25 63.70 10.65 -5 13 24 4.61 5.80 5 13 -24 11.62 6.04 -5 13 23 -0.61 5.06 5 13 -23 -0.02 3.64 -5 13 22 2.80 4.98 5 13 -22 9.52 8.42 -5 13 21 13.96 8.13 -5 13 21 9.59 3.62 5 13 -21 12.46 4.49 5 13 -21 7.59 6.06 -5 13 20 0.74 5.47 -5 13 20 -1.77 3.50 5 13 -20 1.45 5.46 5 13 -20 4.51 5.41 -5 13 19 11.91 8.48 -5 13 19 12.62 5.19 5 13 -19 -0.14 6.54 5 13 -19 3.85 5.73 5 13 -18 15.38 8.49 -5 13 18 3.67 4.03 5 13 -18 16.35 8.47 -5 13 18 3.97 6.21 -5 13 17 54.67 12.75 -5 13 17 41.49 9.42 5 13 -17 61.49 14.18 5 13 -17 55.69 13.56 -5 13 16 10.20 5.16 -5 13 16 10.60 5.57 5 13 -16 23.28 9.23 5 13 -16 25.06 9.27 -5 13 15 382.72 27.06 5 13 -15 457.62 36.36 -5 13 15 407.58 34.82 -5 13 14 82.32 12.87 5 13 -14 110.87 18.37 -5 13 14 97.24 16.67 -5 13 13 137.66 16.77 5 13 -13 122.80 19.15 -5 13 13 116.88 17.91 -5 13 12 67.49 11.39 5 13 -12 80.06 15.12 -5 13 12 56.90 12.23 -5 13 11 53.05 11.86 5 13 -11 61.01 13.32 5 13 -11 61.91 12.91 5 13 -10 175.32 21.17 -5 13 10 167.37 19.14 5 13 -10 194.65 22.03 -5 13 9 15.97 8.14 5 13 -9 12.06 6.10 5 13 -9 6.78 4.52 5 13 -9 17.30 8.07 5 13 -9 30.29 11.94 -5 13 9 32.84 10.90 5 13 -8 352.38 28.37 5 13 -8 319.88 24.15 5 13 -8 345.68 29.30 -5 13 8 280.67 24.88 5 13 -8 339.01 29.78 5 13 -7 7.54 5.45 5 13 -7 -5.12 4.51 5 13 -7 -8.52 7.97 5 13 -7 -5.47 5.36 -5 13 7 3.47 4.70 5 13 -6 16.27 5.24 -5 13 6 66.69 15.62 -5 13 6 64.03 18.73 5 13 -6 34.36 8.44 5 13 -6 23.01 7.43 5 13 -6 22.31 7.85 5 13 -5 11.41 4.85 5 13 -5 5.61 5.51 -5 13 5 5.38 5.00 5 13 -5 2.74 4.33 5 13 -5 5.89 4.69 5 13 -4 0.37 3.35 5 13 -4 -1.18 3.44 -5 13 4 17.27 11.32 5 13 -4 3.89 5.73 -5 13 4 5.14 4.29 5 13 -4 -0.97 4.98 5 13 -3 80.43 10.91 5 13 -3 90.31 13.28 5 13 -3 94.34 15.08 -5 13 3 74.68 12.97 -5 13 3 78.32 14.39 5 13 -3 80.31 13.46 -5 13 3 137.06 20.15 5 13 -2 29.11 7.40 5 13 -2 32.37 7.48 5 13 -2 49.19 11.48 -5 13 2 47.20 11.15 -5 13 2 44.58 10.95 5 13 -2 43.94 10.46 5 13 -1 141.87 17.61 5 13 -1 150.98 15.37 5 13 -1 178.69 20.86 5 13 -1 162.23 16.47 -5 13 1 160.64 18.69 -5 13 1 128.12 16.72 -5 13 1 200.02 22.30 -5 13 0 25.24 13.59 -5 13 0 42.80 9.27 5 13 0 40.77 9.76 5 13 0 37.40 7.80 5 13 0 44.45 8.54 5 13 0 40.00 9.02 -5 13 0 39.99 9.83 -5 13 -1 9.08 7.08 -5 13 -1 2.65 4.27 -5 13 -1 22.09 7.29 5 13 1 10.60 6.34 5 13 1 11.67 4.19 -5 13 -2 -1.92 8.75 -5 13 -2 -0.36 4.35 5 13 2 0.27 4.96 -5 13 -2 10.19 7.29 5 13 2 -7.73 8.28 -5 13 -3 137.02 15.91 -5 13 -3 128.17 26.46 5 13 3 170.92 20.52 -5 13 -3 171.21 20.36 5 13 3 167.85 20.19 5 13 4 14.45 8.03 -5 13 -4 18.71 11.88 -5 13 -4 14.57 5.88 5 13 4 18.01 7.25 5 13 5 24.08 8.63 -5 13 -5 23.55 10.96 -5 13 -5 13.74 5.77 5 13 5 13.64 4.80 -5 13 -6 17.46 12.40 5 13 6 12.67 6.60 -5 13 -6 8.08 4.98 5 13 6 19.93 7.09 5 13 7 357.67 31.49 -5 13 -7 336.55 41.11 5 13 7 330.33 28.07 5 13 8 65.42 10.60 5 13 8 74.34 14.80 5 13 8 84.75 14.54 -5 13 -8 75.01 21.40 5 13 9 105.76 17.65 5 13 9 98.89 13.60 5 13 9 99.09 16.37 -5 13 -9 104.31 24.17 5 13 10 15.74 7.24 5 13 10 13.54 4.45 5 13 10 23.87 9.11 -5 13 -10 29.21 12.41 5 13 11 31.46 9.61 5 13 11 40.61 9.50 5 13 11 38.57 11.69 5 13 12 -0.22 3.26 5 13 12 10.72 7.72 5 13 12 5.85 6.71 5 13 13 91.47 13.93 5 13 13 88.09 15.89 5 13 13 91.42 14.78 5 13 14 15.90 6.03 5 13 14 10.59 6.70 5 13 14 4.04 6.62 5 13 15 40.70 10.53 5 13 15 31.82 9.16 5 13 15 33.23 12.39 5 13 16 -4.83 4.49 5 13 16 3.81 4.48 5 13 16 3.63 4.01 5 13 17 14.38 5.58 5 13 17 20.46 8.87 5 13 17 26.88 9.35 5 13 18 3.00 4.54 5 13 18 1.93 4.48 5 13 19 19.64 6.60 5 13 19 27.16 6.93 5 13 20 2.10 3.72 5 13 20 -1.24 3.73 5 13 21 3.07 3.62 5 13 21 3.00 3.96 5 13 22 2.50 4.35 5 13 22 1.66 3.86 5 13 23 4.95 4.04 5 13 23 6.24 4.36 5 13 24 -0.13 2.48 5 13 24 -0.95 3.10 5 13 25 -0.51 2.29 5 13 25 -0.06 2.61 5 13 26 -2.40 2.65 5 13 27 17.02 3.38 -5 14 30 4.00 2.68 -5 14 29 6.14 3.62 -5 14 29 6.18 2.50 -5 14 28 4.12 4.06 -5 14 28 4.75 3.05 5 14 -27 80.97 7.77 -5 14 27 86.11 10.63 -5 14 27 94.75 13.06 -5 14 26 9.93 5.67 5 14 -26 2.90 2.70 -5 14 26 8.62 4.73 -5 14 25 19.01 7.87 5 14 -25 16.06 5.59 5 14 -24 79.09 11.92 -5 14 24 83.92 15.08 -5 14 23 15.64 8.06 5 14 -23 14.94 6.48 -5 14 22 0.46 4.87 5 14 -22 8.72 6.19 -5 14 21 31.62 9.60 5 14 -21 23.63 7.55 5 14 -21 40.75 11.10 -5 14 20 14.61 7.88 5 14 -20 5.06 5.71 5 14 -20 4.44 4.97 -5 14 19 7.84 6.89 5 14 -19 8.35 4.96 5 14 -18 8.08 6.09 5 14 -18 4.66 6.88 -5 14 18 6.22 7.62 -5 14 17 48.36 13.23 -5 14 17 30.04 8.21 5 14 -17 28.60 10.10 5 14 -17 37.09 12.01 5 14 -16 104.14 17.59 -5 14 16 80.84 12.34 -5 14 16 100.07 17.65 5 14 -16 108.98 16.85 -5 14 15 4.60 6.05 5 14 -15 -0.02 4.68 -5 14 15 -2.42 4.85 5 14 -15 -6.41 5.89 -5 14 14 9.60 4.63 5 14 -14 14.74 8.22 -5 14 14 15.78 8.17 5 14 -14 10.65 7.55 -5 14 13 51.17 12.11 -5 14 13 37.20 8.52 5 14 -13 48.46 12.55 5 14 -13 45.36 12.20 -5 14 12 67.33 13.51 5 14 -12 57.75 13.43 -5 14 12 60.42 10.95 5 14 -12 78.50 14.90 5 14 -11 4.20 5.06 -5 14 11 0.40 4.62 -5 14 11 8.53 5.95 5 14 -11 15.98 7.49 -5 14 10 7.42 5.04 5 14 -10 3.34 4.69 5 14 -10 -0.55 5.12 5 14 -9 18.30 8.27 5 14 -9 21.37 7.96 -5 14 9 7.09 3.77 5 14 -8 18.32 7.53 5 14 -8 17.94 7.06 5 14 -8 23.24 6.97 -5 14 8 26.02 7.62 5 14 -8 29.90 12.11 5 14 -7 -1.22 6.45 5 14 -7 5.84 5.36 5 14 -7 4.26 4.67 -5 14 7 5.87 6.37 5 14 -7 6.39 7.37 5 14 -6 368.77 29.76 5 14 -6 372.80 25.39 -5 14 6 340.59 27.82 -5 14 6 396.62 34.55 5 14 -6 377.60 31.11 5 14 -6 376.71 31.62 5 14 -5 8.76 6.18 5 14 -5 21.82 6.16 5 14 -5 17.43 9.25 -5 14 5 5.04 6.37 5 14 -5 15.53 10.11 -5 14 4 20.70 13.13 5 14 -4 3.56 4.95 5 14 -4 4.50 3.99 -5 14 4 7.15 6.87 5 14 -4 6.15 5.14 5 14 -4 15.45 7.59 -5 14 3 -2.42 5.71 -5 14 3 12.35 10.05 5 14 -3 -1.22 3.97 5 14 -3 1.99 4.38 5 14 -3 7.25 7.00 5 14 -3 -7.41 7.19 -5 14 2 36.43 12.67 5 14 -2 36.81 7.36 5 14 -2 38.58 10.26 -5 14 2 31.98 9.14 5 14 -2 42.79 9.47 5 14 -2 39.50 9.64 5 14 -1 33.46 7.07 -5 14 1 40.17 11.51 5 14 -1 48.75 11.92 -5 14 1 35.18 10.89 5 14 -1 37.14 8.78 5 14 -1 27.71 4.45 5 14 0 161.46 17.14 5 14 0 165.53 16.50 -5 14 0 153.12 19.64 5 14 0 181.43 21.71 5 14 0 163.76 19.66 -5 14 0 148.50 19.35 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4.53 5 14 14 3.28 5.14 5 14 14 2.09 4.25 5 14 15 61.46 10.91 5 14 15 42.81 9.05 5 14 15 45.03 11.58 5 14 16 4.78 4.27 5 14 16 2.73 3.85 5 14 16 3.59 6.86 5 14 17 48.48 9.49 5 14 17 43.41 11.70 5 14 17 41.33 8.63 5 14 18 15.84 5.48 5 14 18 29.35 7.82 5 14 18 16.27 7.22 5 14 19 11.38 4.92 5 14 19 17.82 6.99 5 14 20 30.48 7.15 5 14 20 35.97 8.30 5 14 21 0.74 3.38 5 14 21 1.30 3.21 5 14 22 3.34 3.61 5 14 22 2.48 2.81 5 14 23 18.88 4.81 5 14 23 18.13 4.90 5 14 24 2.69 3.34 5 14 24 1.93 1.93 5 14 25 9.76 3.09 5 14 25 8.12 2.44 -5 14 -26 4.30 2.77 -5 15 29 -3.54 2.41 -5 15 28 3.12 2.74 -5 15 27 0.85 3.25 -5 15 27 1.80 1.91 -5 15 26 44.35 9.00 -5 15 26 34.31 5.83 5 15 -26 30.04 4.89 5 15 -25 6.95 3.71 -5 15 25 3.06 2.39 -5 15 25 6.93 5.27 -5 15 24 1.65 4.02 -5 15 24 -1.67 3.19 5 15 -24 5.05 4.04 -5 15 23 16.98 6.74 5 15 -23 9.58 4.92 -5 15 23 10.62 4.66 -5 15 22 34.56 10.54 5 15 -22 44.53 9.89 -5 15 22 39.82 7.94 -5 15 21 4.47 4.55 5 15 -21 0.79 4.23 -5 15 21 11.26 5.49 5 15 -20 2.47 4.18 -5 15 20 13.10 5.43 -5 15 20 14.91 7.20 5 15 -20 5.16 5.60 -5 15 19 6.89 5.39 5 15 -19 0.29 4.45 5 15 -19 3.64 6.75 5 15 -18 4.38 4.46 -5 15 18 -4.40 5.18 5 15 -18 0.96 5.08 -5 15 17 1.32 6.28 5 15 -17 -7.96 5.60 5 15 -17 3.74 5.84 -5 15 16 26.34 8.16 5 15 -16 26.68 9.73 5 15 -16 20.95 9.68 5 15 -15 47.71 12.41 -5 15 15 39.46 10.86 5 15 -15 51.17 12.22 -5 15 14 76.33 14.68 5 15 -14 87.51 16.58 5 15 -14 93.59 16.01 -5 15 13 72.41 13.44 -5 15 13 53.84 9.85 5 15 -13 67.77 12.85 5 15 -13 79.62 15.79 -5 15 12 12.48 7.77 5 15 -12 10.72 8.03 -5 15 11 18.62 7.91 -5 15 11 -0.30 4.90 5 15 -11 7.08 4.92 5 15 -11 11.88 5.67 -5 15 10 157.46 17.05 5 15 -10 183.64 22.29 5 15 -10 199.12 22.66 -5 15 10 157.49 19.29 5 15 -9 212.73 23.93 5 15 -9 205.97 22.71 5 15 -9 222.62 25.67 -5 15 9 176.63 19.00 5 15 -8 272.57 28.22 5 15 -8 265.04 26.02 5 15 -8 256.45 26.38 5 15 -7 238.00 20.64 5 15 -7 234.06 25.96 -5 15 7 216.40 21.96 5 15 -7 246.18 25.42 5 15 -7 229.13 24.33 5 15 -6 0.76 3.34 -5 15 6 -4.89 5.74 5 15 -6 -2.48 5.05 5 15 -6 -1.70 7.02 5 15 -6 6.08 4.56 5 15 -5 72.68 11.15 5 15 -5 73.50 14.09 -5 15 5 69.46 13.12 5 15 -5 63.62 13.24 5 15 -5 69.46 15.43 5 15 -4 280.11 25.66 5 15 -4 273.37 21.19 5 15 -4 284.99 27.39 -5 15 4 270.35 25.28 -5 15 4 289.85 30.43 5 15 -4 267.07 27.35 5 15 -3 115.19 13.52 5 15 -3 95.29 15.11 -5 15 3 104.12 16.48 -5 15 3 104.12 20.65 5 15 -3 115.60 17.97 5 15 -3 97.96 17.01 5 15 -2 46.70 8.89 -5 15 2 62.42 16.22 -5 15 2 39.79 9.71 5 15 -2 40.59 10.44 5 15 -2 39.55 9.63 5 15 -2 47.55 11.42 5 15 -1 34.94 8.84 5 15 -1 54.73 9.71 -5 15 1 74.67 17.13 5 15 -1 51.20 12.15 5 15 -1 62.72 11.62 -5 15 1 48.01 12.00 -5 15 0 64.80 15.01 5 15 0 56.28 10.64 5 15 0 58.30 14.45 5 15 0 53.07 10.70 -5 15 0 75.46 15.19 5 15 0 46.95 11.53 5 15 1 265.21 20.73 -5 15 -1 225.37 23.51 -5 15 -1 238.93 24.68 5 15 1 250.13 26.71 5 15 1 259.36 21.87 5 15 1 233.54 24.64 -5 15 -2 9.09 7.38 -5 15 -2 4.12 4.70 5 15 2 -4.11 4.97 5 15 2 3.99 5.26 -5 15 -2 7.42 9.39 5 15 2 -6.59 8.72 5 15 3 140.68 15.72 -5 15 -3 154.57 20.25 -5 15 -3 128.84 17.37 5 15 3 151.06 21.15 5 15 3 109.45 16.86 5 15 4 16.43 9.49 -5 15 -4 22.99 9.10 -5 15 -4 17.89 8.22 5 15 4 8.52 4.90 5 15 4 0.32 5.89 -5 15 -5 7.75 6.41 -5 15 -5 -3.94 7.12 5 15 5 3.19 6.62 5 15 5 -17.76 10.84 -5 15 -6 6.82 5.34 5 15 6 2.28 5.66 -5 15 -6 3.16 5.75 5 15 6 6.65 4.62 5 15 7 18.09 8.11 5 15 7 5.01 5.38 -5 15 -7 13.81 7.47 -5 15 -7 16.07 8.74 5 15 8 12.22 5.83 -5 15 -8 1.88 4.71 5 15 8 -5.24 7.60 5 15 9 5.70 5.17 5 15 9 9.52 6.94 5 15 10 4.28 5.38 5 15 10 1.69 5.90 5 15 11 3.11 4.10 5 15 11 1.74 5.23 5 15 12 1.70 3.66 5 15 12 0.96 4.72 5 15 13 4.56 3.57 5 15 13 5.84 4.15 5 15 13 2.44 5.29 5 15 14 26.10 7.42 5 15 14 30.83 9.09 5 15 14 20.69 5.87 5 15 15 10.49 4.59 5 15 15 -1.08 4.37 5 15 15 9.28 5.81 5 15 16 15.08 5.85 5 15 16 13.56 4.63 5 15 16 8.14 4.05 5 15 17 6.46 5.23 5 15 17 8.39 4.72 5 15 17 0.02 2.91 5 15 18 -2.11 5.75 5 15 18 7.68 3.89 5 15 18 -5.37 4.20 5 15 19 7.63 4.64 5 15 19 14.28 4.83 5 15 20 -6.25 4.66 5 15 20 0.01 3.04 5 15 21 12.03 4.06 5 15 21 8.06 2.86 5 15 22 -0.52 2.84 5 15 22 1.42 2.21 5 15 23 8.67 3.33 5 15 23 5.70 2.03 5 15 24 4.39 2.28 -5 15 -24 5.71 3.75 -5 15 -25 1.00 2.15 -5 16 27 5.12 2.56 -5 16 26 2.00 2.53 5 16 -25 53.91 6.60 -5 16 25 65.52 9.76 -5 16 24 11.01 5.54 5 16 -24 -3.52 4.04 -5 16 23 4.49 4.11 5 16 -23 8.61 4.75 -5 16 22 72.79 12.24 5 16 -22 55.74 9.44 -5 16 21 5.96 5.61 5 16 -21 -2.97 4.75 5 16 -20 22.39 8.11 -5 16 20 10.98 6.76 5 16 -20 9.45 4.72 -5 16 19 9.93 6.20 5 16 -19 6.83 5.61 5 16 -19 5.58 3.79 5 16 -18 4.52 5.04 5 16 -18 1.66 4.01 -5 16 18 0.94 4.80 -5 16 17 5.66 4.98 5 16 -17 6.75 6.00 5 16 -17 -4.08 5.16 -5 16 16 -3.20 6.25 5 16 -16 5.35 4.26 5 16 -16 5.00 4.81 5 16 -15 12.70 7.20 5 16 -15 26.30 9.24 -5 16 15 38.00 10.28 -5 16 14 1.87 4.05 5 16 -14 7.38 7.95 5 16 -14 0.82 5.33 -5 16 13 -0.59 6.18 5 16 -13 10.61 7.50 5 16 -13 -7.33 6.13 -5 16 12 73.61 13.30 5 16 -12 68.90 14.83 5 16 -12 78.28 15.39 -5 16 11 10.64 6.68 5 16 -11 24.03 9.35 5 16 -11 11.49 8.07 -5 16 10 43.23 10.25 5 16 -10 36.89 10.14 5 16 -10 45.86 11.57 5 16 -9 -10.59 7.09 -5 16 9 -0.63 3.17 5 16 -9 0.46 4.89 5 16 -8 18.93 7.00 5 16 -8 21.08 7.04 5 16 -8 36.68 13.28 5 16 -7 20.80 8.49 5 16 -7 40.63 13.24 5 16 -7 28.16 9.26 5 16 -6 1.48 4.40 5 16 -6 -5.51 7.03 5 16 -6 13.01 8.94 -5 16 6 2.80 5.20 5 16 -5 -0.25 2.63 -5 16 5 2.96 3.47 5 16 -5 4.90 4.56 5 16 -5 -3.17 7.11 5 16 -5 1.65 5.58 5 16 -4 7.31 4.22 5 16 -4 2.45 6.63 -5 16 4 12.03 6.84 5 16 -4 4.69 6.22 5 16 -4 8.21 6.65 5 16 -3 73.72 10.60 -5 16 3 112.28 20.82 -5 16 3 54.55 11.40 5 16 -3 74.66 14.05 5 16 -3 74.54 13.06 5 16 -3 76.21 15.25 -5 16 2 15.03 9.37 5 16 -2 14.59 9.66 5 16 -2 -2.31 4.12 5 16 -2 1.31 4.91 -5 16 1 157.76 19.76 -5 16 1 184.11 23.59 5 16 -1 180.31 22.51 5 16 -1 170.13 19.06 5 16 -1 173.21 21.92 5 16 0 13.26 5.48 5 16 0 26.85 9.90 -5 16 0 13.54 5.54 5 16 0 13.15 4.86 -5 16 -1 23.27 11.42 5 16 1 12.43 5.62 5 16 1 22.89 10.07 -5 16 -1 21.64 8.72 5 16 1 17.07 6.73 5 16 2 55.14 10.02 -5 16 -2 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18.99 -6 12 11 -1.57 5.32 6 12 -11 11.24 8.27 6 12 -11 9.97 6.92 6 12 -10 224.54 22.92 6 12 -10 266.77 26.74 6 12 -9 103.00 14.81 -6 12 9 102.50 16.67 6 12 -9 88.79 16.12 -6 12 8 76.77 16.34 6 12 -8 91.30 14.14 -6 12 8 101.93 16.57 6 12 -8 99.00 16.36 6 12 -8 96.99 17.47 -6 12 7 5.24 3.85 6 12 -7 -4.69 4.91 -6 12 7 -1.20 5.16 6 12 -7 -5.12 7.75 6 12 -7 5.83 7.02 -6 12 6 22.66 8.36 6 12 -6 30.39 8.08 -6 12 6 29.29 9.86 6 12 -6 31.10 8.68 6 12 -6 26.65 8.95 -6 12 5 9.94 7.03 6 12 -5 2.73 4.02 6 12 -5 6.58 5.06 -6 12 5 1.95 4.49 6 12 -5 0.54 3.34 6 12 -5 3.19 5.36 -6 12 4 12.59 7.01 6 12 -4 9.34 5.99 -6 12 4 9.01 5.40 6 12 -4 6.52 4.32 6 12 -4 9.67 5.60 6 12 -4 3.91 5.34 -6 12 3 -4.34 6.59 6 12 -3 1.05 4.06 6 12 -3 2.03 3.49 -6 12 3 6.58 5.87 6 12 -3 -5.05 5.03 6 12 -3 6.42 4.51 6 12 -2 36.57 9.34 6 12 -2 29.77 7.88 -6 12 2 51.91 14.70 -6 12 2 27.08 7.70 6 12 -2 23.19 6.76 6 12 -2 33.99 8.47 6 12 -1 7.20 3.96 -6 12 1 14.94 7.03 6 12 -1 4.23 4.00 -6 12 0 107.26 16.34 -6 12 0 117.71 17.88 6 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34.56 9.66 6 12 13 6.26 4.60 6 12 13 4.74 4.03 6 12 14 4.68 5.36 6 12 14 11.76 5.79 6 12 15 17.13 6.13 6 12 15 16.00 7.71 6 12 16 2.53 4.94 6 12 16 -0.44 5.12 6 12 17 16.61 8.26 6 12 17 16.68 7.03 6 12 18 35.47 9.19 6 12 18 41.91 10.41 6 12 19 10.49 5.92 6 12 19 11.19 6.06 6 12 20 23.73 7.35 6 12 20 20.07 7.42 6 12 21 2.78 4.01 6 12 21 -0.56 3.62 6 12 22 -8.60 4.23 6 12 22 1.49 3.48 6 12 23 10.08 4.32 6 12 23 8.99 3.07 6 12 24 -1.06 3.23 6 12 25 25.93 5.43 6 12 26 2.77 1.79 6 12 27 0.98 1.52 -6 12 -27 -0.42 1.64 -6 13 30 -2.05 3.09 -6 13 29 25.03 6.01 -6 13 29 31.99 4.89 -6 13 28 16.99 5.82 6 13 -28 10.25 3.05 -6 13 28 6.97 3.30 -6 13 27 3.67 4.30 6 13 -27 4.49 2.73 -6 13 26 2.01 4.46 6 13 -26 4.48 3.42 -6 13 25 31.32 8.86 6 13 -25 42.94 8.81 6 13 -24 26.53 7.21 -6 13 24 32.08 9.37 -6 13 23 53.52 12.06 6 13 -23 45.27 9.66 -6 13 22 2.34 6.00 -6 13 22 5.58 4.06 6 13 -22 -11.90 7.80 6 13 -22 3.05 5.39 -6 13 21 8.98 5.42 -6 13 21 3.22 3.70 6 13 -21 -1.07 6.99 6 13 -21 6.15 6.39 -6 13 20 12.09 6.53 -6 13 20 14.13 6.01 6 13 -20 9.11 6.52 6 13 -20 18.18 8.22 -6 13 19 -7.78 7.67 -6 13 19 5.03 5.39 6 13 -19 1.42 5.63 6 13 -19 3.40 4.56 -6 13 18 -2.35 5.13 -6 13 18 3.55 4.33 6 13 -18 0.21 6.99 6 13 -18 -2.30 4.88 -6 13 17 3.70 5.20 6 13 -17 1.32 6.02 -6 13 16 -6.68 7.71 -6 13 16 8.01 6.53 6 13 -16 1.66 5.55 -6 13 15 4.68 6.76 -6 13 15 -4.81 4.96 6 13 -15 1.34 6.40 -6 13 14 22.57 12.23 6 13 -14 4.36 6.26 -6 13 13 77.32 13.92 6 13 -13 103.72 18.48 -6 13 13 75.95 13.40 -6 13 12 10.24 6.81 6 13 -12 3.89 6.17 -6 13 12 -1.92 5.59 -6 13 11 3.03 5.96 6 13 -11 3.30 5.76 6 13 -10 33.35 9.25 6 13 -10 35.71 10.63 6 13 -9 24.75 8.38 6 13 -9 25.41 8.27 -6 13 9 15.65 8.46 6 13 -9 9.72 5.45 6 13 -8 12.50 5.49 6 13 -8 17.53 7.42 -6 13 8 9.70 5.68 6 13 -8 11.00 6.53 6 13 -8 18.31 11.23 6 13 -7 6.63 4.54 6 13 -7 3.85 4.83 6 13 -7 16.60 6.54 6 13 -7 25.82 10.24 -6 13 7 12.04 6.84 6 13 -6 57.17 11.57 -6 13 6 56.96 13.32 6 13 -6 45.43 10.42 6 13 -6 46.60 10.89 6 13 -6 51.21 12.62 6 13 -5 142.17 17.25 6 13 -5 132.57 17.20 -6 13 5 124.48 18.46 6 13 -5 139.37 18.82 6 13 -5 153.64 19.62 6 13 -4 -4.66 5.38 6 13 -4 1.48 3.05 -6 13 4 1.40 4.36 6 13 -4 0.02 3.98 6 13 -4 -7.38 5.20 6 13 -3 6.21 4.05 6 13 -3 9.03 4.46 6 13 -3 14.52 6.59 6 13 -3 12.14 6.62 6 13 -2 41.25 8.67 6 13 -2 36.50 10.45 -6 13 2 40.88 10.63 6 13 -2 34.90 7.30 6 13 -2 43.72 9.91 6 13 -1 2.82 4.13 6 13 -1 2.52 4.38 6 13 -1 4.47 4.13 -6 13 1 7.52 7.19 6 13 -1 0.92 4.12 6 13 0 127.83 16.54 -6 13 0 138.76 19.85 6 13 0 139.25 18.54 6 13 0 125.28 16.64 -6 13 0 150.59 20.65 -6 13 -1 39.91 12.24 -6 13 -1 40.88 12.28 6 13 1 38.16 12.27 6 13 1 36.40 12.75 -6 13 -2 39.04 14.41 -6 13 -2 48.80 13.16 6 13 2 28.09 8.48 -6 13 -2 36.96 10.00 6 13 2 27.95 7.74 -6 13 -3 4.90 5.29 -6 13 -3 41.39 10.96 6 13 3 26.47 9.63 -6 13 -3 28.40 9.51 6 13 3 17.37 5.28 -6 13 -4 4.58 4.26 -6 13 -4 -0.62 4.59 6 13 4 -0.58 2.69 6 13 4 0.39 3.93 -6 13 -4 14.79 9.64 6 13 4 -1.12 6.41 -6 13 -5 6.73 6.32 6 13 5 14.53 7.22 6 13 5 19.03 5.98 6 13 5 15.67 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6.49 2.84 -6 14 26 60.89 10.51 6 14 -26 52.51 7.95 -6 14 26 54.06 6.99 -6 14 25 37.55 8.97 6 14 -25 29.13 6.90 -6 14 25 35.03 6.27 -6 14 24 45.37 10.26 6 14 -24 49.04 9.51 -6 14 24 43.87 7.62 -6 14 23 7.67 5.23 6 14 -23 9.84 4.96 -6 14 22 4.20 5.60 6 14 -22 1.86 4.32 6 14 -21 0.22 4.35 -6 14 21 5.85 6.11 -6 14 21 5.01 3.16 6 14 -21 7.01 5.60 -6 14 20 60.32 13.17 -6 14 20 49.93 8.90 6 14 -20 45.60 10.90 6 14 -20 55.47 12.19 -6 14 19 119.44 14.40 6 14 -19 120.49 18.10 6 14 -19 133.72 18.72 -6 14 19 131.91 18.66 -6 14 18 17.35 8.03 -6 14 18 11.53 6.29 6 14 -18 5.21 7.00 6 14 -18 15.46 5.94 -6 14 17 68.57 13.51 -6 14 17 66.63 11.47 6 14 -17 70.57 15.27 6 14 -17 68.77 14.39 -6 14 16 2.97 5.24 -6 14 16 6.47 4.34 6 14 -16 2.04 8.00 6 14 -16 9.84 7.27 -6 14 15 12.09 6.59 -6 14 15 4.82 4.64 6 14 -15 12.74 8.19 6 14 -15 1.39 5.11 -6 14 14 46.77 10.69 -6 14 14 57.24 12.04 6 14 -14 40.45 11.91 6 14 -14 50.75 13.63 -6 14 13 4.51 3.98 -6 14 13 6.92 5.73 6 14 -13 3.15 5.29 6 14 -13 7.50 9.00 -6 14 12 10.69 4.96 -6 14 12 24.78 7.50 6 14 -12 40.46 10.88 6 14 -12 27.94 8.65 -6 14 11 9.93 7.09 6 14 -11 6.93 4.44 6 14 -11 5.17 4.49 6 14 -10 92.56 16.47 6 14 -10 82.12 15.13 6 14 -9 116.45 17.29 6 14 -9 113.95 15.84 6 14 -9 109.17 17.65 6 14 -8 143.15 19.92 6 14 -8 135.55 17.17 -6 14 8 124.95 18.73 6 14 -8 144.02 21.46 6 14 -8 113.69 17.03 6 14 -7 32.31 9.74 6 14 -7 41.24 9.81 -6 14 7 38.88 10.47 6 14 -7 35.47 8.62 6 14 -7 62.46 14.96 -6 14 6 28.60 10.09 6 14 -6 29.73 8.35 6 14 -6 45.10 13.69 6 14 -6 25.03 8.07 6 14 -6 31.46 9.22 6 14 -5 -2.68 4.51 6 14 -5 0.89 4.45 6 14 -5 -3.44 6.24 6 14 -5 13.15 7.83 6 14 -4 260.88 24.21 6 14 -4 249.46 22.35 -6 14 4 265.74 27.33 6 14 -4 262.12 26.36 6 14 -4 266.20 26.14 6 14 -3 143.95 17.50 -6 14 3 162.13 21.83 6 14 -3 137.06 19.70 6 14 -3 141.12 17.21 6 14 -3 127.35 18.00 6 14 -2 154.27 18.20 -6 14 2 134.49 19.03 6 14 -2 162.67 21.57 6 14 -2 134.20 18.83 6 14 -2 145.08 17.01 6 14 -1 71.19 14.56 6 14 -1 70.92 12.64 6 14 -1 63.81 11.50 -6 14 1 83.46 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3.90 5.15 6 14 13 115.05 17.28 6 14 13 127.85 16.01 6 14 13 102.81 13.23 6 14 14 1.44 4.22 6 14 14 9.25 5.51 6 14 14 1.08 3.04 6 14 15 79.30 13.61 6 14 15 81.67 12.48 6 14 16 -5.29 5.88 6 14 16 1.43 3.43 6 14 17 14.93 5.94 6 14 17 27.16 8.17 6 14 18 -1.04 3.86 6 14 18 -1.75 3.81 6 14 19 5.62 4.50 6 14 19 1.95 2.76 6 14 20 3.95 3.55 6 14 20 1.66 3.26 6 14 21 15.29 4.89 6 14 21 10.53 3.89 6 14 22 3.61 2.65 6 14 22 5.43 2.64 6 14 23 5.28 2.27 6 14 23 7.68 3.07 -6 14 -23 8.16 3.62 6 14 24 1.03 1.57 -6 14 -24 0.63 2.41 -6 14 -25 0.46 1.58 -6 15 28 27.93 5.12 -6 15 27 7.56 3.72 -6 15 26 8.65 4.46 6 15 -26 16.11 4.04 -6 15 25 1.41 3.42 6 15 -25 -0.64 2.52 -6 15 24 38.40 8.98 6 15 -24 33.60 7.29 -6 15 23 61.08 10.35 6 15 -23 51.59 9.28 -6 15 22 2.92 4.06 6 15 -22 5.45 4.44 -6 15 21 30.70 8.68 6 15 -21 17.31 7.29 6 15 -21 18.38 6.69 6 15 -20 5.87 6.56 6 15 -20 -8.84 7.38 -6 15 19 -2.03 4.35 -6 15 19 -0.08 2.78 6 15 -19 6.76 5.89 6 15 -19 1.79 4.59 -6 15 18 22.61 7.98 -6 15 18 10.02 4.74 6 15 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8.56 7 10 13 41.46 11.08 7 10 14 0.67 3.22 7 10 14 4.26 5.63 7 10 15 -5.89 5.43 7 10 15 3.88 5.65 7 10 16 39.42 8.79 7 10 16 54.40 12.94 7 10 17 -5.00 5.27 7 10 17 2.74 4.70 7 10 18 109.87 16.92 7 10 19 -2.09 4.90 7 10 20 4.36 7.04 7 10 21 18.76 6.74 7 10 22 0.59 4.11 7 10 23 -3.35 4.22 7 10 24 0.10 3.24 -7 10 -24 1.94 2.36 7 10 25 0.18 2.74 -7 10 -25 1.93 2.05 7 10 26 4.12 2.51 -7 10 -26 -0.94 2.02 7 10 27 0.12 1.78 -7 11 31 3.32 2.54 -7 11 30 -3.17 3.96 7 -11 -29 9.39 2.65 -7 11 29 9.76 4.59 7 11 -29 13.11 3.72 7 -11 -28 2.90 2.43 7 11 -28 9.04 4.10 -7 11 28 14.06 6.20 7 -11 -27 3.02 3.16 -7 11 27 4.82 3.97 7 11 -27 -2.01 3.48 7 -11 -26 32.80 6.95 -7 11 26 43.78 10.88 7 11 -26 29.30 7.75 7 -11 -25 19.66 5.93 7 -11 -24 7.53 4.77 7 -11 -23 6.73 5.01 -7 11 23 6.25 5.37 7 -11 -22 7.01 5.20 -7 11 22 2.49 4.19 7 11 -22 -1.35 6.36 -7 11 21 3.44 4.75 7 11 -21 -6.70 6.63 -7 11 20 138.64 18.12 7 11 -20 132.42 20.37 -7 11 19 -7.07 7.63 7 11 -19 -4.39 6.72 -7 11 18 83.60 14.47 7 11 -18 100.25 18.13 -7 11 17 1.30 5.07 7 11 -17 4.49 7.76 -7 11 16 -0.06 5.30 7 11 -16 5.09 6.57 -7 11 15 34.63 9.79 7 11 -15 48.17 12.04 -7 11 14 209.30 23.20 7 11 -14 216.84 26.12 -7 11 13 35.62 12.17 -7 11 13 29.83 9.25 7 11 -13 51.78 14.41 -7 11 12 213.82 30.76 7 11 -12 280.48 25.30 7 11 -12 274.56 28.17 -7 11 11 23.07 6.58 -7 11 11 46.35 15.68 7 11 -11 31.59 9.88 7 11 -11 30.01 10.39 -7 11 10 16.88 5.79 -7 11 10 14.01 10.52 7 11 -10 17.68 7.94 7 11 -10 10.89 7.03 -7 11 9 22.96 5.83 -7 11 9 23.17 9.48 -7 11 9 39.28 12.19 7 11 -9 35.43 10.31 7 11 -9 29.72 8.70 -7 11 8 167.62 27.56 -7 11 8 163.41 15.10 7 11 -8 173.29 19.48 -7 11 8 173.59 22.47 7 11 -8 179.24 21.57 -7 11 7 37.02 7.48 -7 11 7 38.38 12.86 7 11 -7 48.88 10.73 -7 11 7 39.89 11.57 7 11 -7 35.88 10.12 -7 11 6 26.48 6.12 -7 11 6 31.73 12.54 7 11 -6 34.64 8.65 -7 11 6 29.86 9.03 7 11 -6 26.86 8.05 7 11 -6 42.29 12.26 -7 11 5 -2.32 3.69 -7 11 5 6.63 7.13 7 11 -5 -0.94 3.25 7 11 -5 3.14 4.11 -7 11 5 2.45 5.58 7 11 -5 10.25 8.73 -7 11 4 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44.78 10.36 -7 12 23 40.76 8.41 7 12 -23 50.29 10.57 7 -12 -22 2.20 3.45 -7 12 22 -0.32 4.95 -7 12 22 7.41 5.28 7 12 -22 -0.51 5.32 -7 12 21 3.73 5.80 -7 12 21 2.93 5.32 7 12 -21 2.19 6.70 -7 12 20 2.67 4.15 -7 12 20 3.44 4.52 7 12 -20 3.84 6.35 -7 12 19 -13.03 6.82 -7 12 19 -5.18 5.80 7 12 -19 -0.68 8.70 -7 12 18 0.65 5.23 -7 12 18 -10.03 5.84 7 12 -18 -2.92 6.71 -7 12 17 8.92 5.58 -7 12 17 5.04 5.22 7 12 -17 15.56 10.02 -7 12 16 31.53 9.94 -7 12 16 22.40 7.08 7 12 -16 33.41 11.58 -7 12 15 81.95 13.61 -7 12 15 87.17 14.93 7 12 -15 96.16 20.16 -7 12 14 40.55 10.05 -7 12 14 39.72 9.97 7 12 -14 59.32 14.69 -7 12 13 20.38 9.24 7 12 -13 16.81 9.82 -7 12 12 12.68 7.12 7 12 -12 11.12 8.75 7 12 -11 21.01 8.37 7 12 -11 26.49 9.17 7 12 -10 27.24 10.14 7 12 -10 24.55 11.29 -7 12 9 6.63 5.30 7 12 -9 9.77 6.13 -7 12 9 11.73 7.68 7 12 -9 10.42 4.67 -7 12 8 17.06 8.90 -7 12 8 18.89 8.39 7 12 -8 24.92 8.25 7 12 -8 18.36 7.36 -7 12 7 46.64 13.37 7 12 -7 88.96 14.52 7 12 -7 81.15 15.12 -7 12 7 82.15 16.09 -7 12 6 2.72 7.76 7 12 -6 17.41 6.31 -7 12 6 8.62 5.56 7 12 -6 14.99 4.90 7 12 -6 26.00 11.00 -7 12 5 9.45 8.68 7 12 -5 8.72 4.83 -7 12 5 9.25 8.04 7 12 -5 -4.44 6.11 7 12 -5 -1.12 3.14 7 12 -5 17.66 9.67 -7 12 4 64.36 16.49 7 12 -4 69.07 12.48 7 12 -4 68.36 13.07 -7 12 4 79.69 15.68 7 12 -4 57.87 10.33 7 12 -4 71.44 14.16 7 12 -3 18.24 6.71 7 12 -3 35.70 11.64 -7 12 3 15.33 8.44 7 12 -3 18.48 6.19 7 12 -3 8.49 5.10 7 12 -2 0.77 4.17 7 12 -2 8.37 7.10 -7 12 2 16.34 8.13 7 12 -2 5.64 4.85 -7 12 1 20.29 5.58 7 12 -1 28.88 8.31 7 12 -1 27.33 7.98 -7 12 1 35.89 11.36 7 12 -1 17.08 6.94 -7 12 0 51.72 8.44 7 12 0 65.56 12.95 -7 12 0 63.35 13.27 7 12 0 56.64 11.27 -7 12 -1 57.77 9.32 7 12 1 52.10 12.59 -7 12 -1 50.40 12.73 7 12 1 48.40 10.47 -7 12 -2 103.15 11.88 -7 12 -2 126.57 19.05 7 12 2 142.90 18.63 7 12 2 126.36 16.26 -7 12 -3 32.53 6.79 7 12 3 44.87 11.50 -7 12 -3 33.22 10.62 7 12 3 45.22 9.82 7 12 3 36.88 9.06 7 12 4 2.05 4.01 -7 12 -4 10.05 7.07 7 12 4 1.59 3.81 -7 12 -4 9.27 9.12 7 12 4 -2.21 6.18 7 12 5 409.08 30.05 7 12 5 402.62 32.30 -7 12 -5 405.21 34.41 7 12 5 391.53 27.52 7 12 6 4.53 5.48 7 12 6 0.82 4.07 -7 12 -6 0.53 6.85 7 12 6 0.01 3.98 7 12 7 -1.67 6.01 7 12 7 0.51 3.29 -7 12 -7 -0.16 6.71 7 12 7 -8.15 6.05 7 12 8 19.80 7.42 7 12 8 13.45 3.71 7 12 8 13.08 6.19 7 12 9 -1.38 3.84 7 12 9 6.73 5.88 7 12 10 11.48 5.15 7 12 10 2.10 3.73 7 12 11 6.48 3.91 7 12 11 8.37 5.52 7 12 12 87.52 15.05 7 12 12 87.71 14.80 7 12 13 20.62 7.79 7 12 13 16.45 7.18 7 12 14 -3.67 5.58 7 12 14 -1.60 4.52 7 12 15 15.17 6.01 7 12 15 27.97 8.96 7 12 16 70.27 11.67 7 12 16 75.92 13.64 7 12 17 24.21 6.66 7 12 17 33.22 8.94 7 12 18 45.42 8.42 7 12 18 38.37 8.94 7 12 19 8.41 4.28 7 12 19 8.71 5.35 7 12 20 5.57 3.11 7 12 20 6.07 4.16 7 12 21 13.30 4.92 7 12 22 1.32 3.55 -7 12 -23 3.91 3.74 7 12 23 12.08 4.02 -7 12 -24 12.22 4.75 7 12 24 3.22 2.52 -7 12 -25 -1.12 2.04 7 12 25 -0.99 2.17 -7 13 29 2.51 2.40 -7 13 28 11.78 4.52 7 13 -28 16.66 3.53 -7 13 27 6.19 3.22 7 13 -27 5.37 2.51 -7 13 26 3.43 4.32 7 13 -26 7.62 4.27 -7 13 25 59.30 10.66 7 13 -25 65.06 10.23 -7 13 24 26.30 7.34 7 13 -24 18.45 6.04 7 -13 -23 10.74 3.78 -7 13 23 5.43 5.17 7 13 -23 5.89 5.41 7 -13 -22 4.75 3.63 -7 13 22 -1.24 4.58 -7 13 22 -5.31 5.47 7 13 -22 -6.70 5.04 7 -13 -21 9.20 4.35 -7 13 21 9.75 6.76 -7 13 21 11.09 5.82 7 13 -21 12.89 5.67 7 13 -21 8.45 6.27 -7 13 20 36.28 10.04 -7 13 20 30.41 8.73 7 13 -20 24.42 9.27 7 13 -20 20.81 9.58 -7 13 19 55.49 13.01 -7 13 19 71.06 12.51 7 13 -19 44.48 12.06 7 13 -19 55.65 11.95 -7 13 18 63.76 13.28 -7 13 18 64.06 11.94 7 13 -18 58.36 14.72 -7 13 17 79.80 13.90 7 13 -17 73.86 16.42 -7 13 16 -1.38 5.18 -7 13 16 4.30 5.46 7 13 -16 6.00 7.49 -7 13 15 27.77 8.78 -7 13 15 23.80 8.48 7 13 -15 28.05 11.46 -7 13 14 21.50 9.57 7 13 -14 20.93 10.09 -7 13 13 62.84 13.62 7 13 -13 88.77 17.05 -7 13 12 2.21 4.09 7 13 -12 9.67 8.86 7 13 -11 8.54 8.73 7 13 -10 14.52 9.37 7 13 -10 19.60 8.35 7 13 -9 75.96 14.20 7 13 -9 58.10 14.16 7 13 -9 61.86 13.48 7 13 -8 30.28 8.63 -7 13 8 14.05 8.91 7 13 -8 13.54 8.60 7 13 -8 6.86 5.40 7 13 -7 -2.19 7.43 7 13 -7 3.64 5.11 -7 13 7 -1.11 4.74 7 13 -7 5.82 4.59 7 13 -6 1.23 4.34 -7 13 6 3.09 5.89 7 13 -6 -3.56 7.38 7 13 -6 0.20 5.52 7 13 -6 15.33 10.01 7 13 -5 39.19 9.80 -7 13 5 27.40 9.03 7 13 -5 38.16 9.66 7 13 -5 32.76 8.92 7 13 -5 50.34 12.79 7 13 -4 5.55 3.94 7 13 -4 4.00 6.35 -7 13 4 10.75 7.97 7 13 -4 3.69 3.50 7 13 -4 13.54 7.70 7 13 -3 21.49 6.71 7 13 -3 22.73 8.36 -7 13 3 29.00 10.73 7 13 -3 14.35 4.70 7 13 -3 26.87 10.14 7 13 -2 28.71 8.57 7 13 -2 42.11 11.02 -7 13 2 38.09 12.49 7 13 -2 36.31 8.42 7 13 -2 32.72 9.98 7 13 -1 29.90 7.95 7 13 -1 36.62 10.29 -7 13 1 44.26 12.92 7 13 -1 36.51 10.26 7 13 0 73.34 13.33 -7 13 0 80.55 16.00 7 13 0 86.13 15.21 7 13 0 76.13 13.58 7 13 1 33.73 9.41 7 13 1 23.84 9.19 -7 13 -1 22.56 8.48 7 13 1 18.78 7.07 7 13 2 -1.77 5.48 7 13 2 2.06 4.76 -7 13 -3 344.57 33.04 7 13 3 360.26 30.53 7 13 3 370.62 28.22 7 13 4 48.86 12.97 -7 13 -4 36.74 11.72 7 13 4 46.37 10.61 7 13 5 235.74 22.32 -7 13 -5 241.14 27.44 7 13 5 235.45 25.25 7 13 5 230.97 21.81 7 13 6 96.84 14.94 -7 13 -6 63.67 9.32 7 13 6 84.52 14.83 -7 13 -6 79.83 16.35 7 13 6 71.09 12.37 7 13 7 6.98 5.78 7 13 7 2.18 3.13 -7 13 -7 -0.78 5.54 7 13 7 -0.05 6.21 7 13 8 9.68 3.88 7 13 8 1.98 3.26 7 13 8 12.34 5.30 -7 13 -8 7.30 4.91 7 13 9 32.70 9.55 -7 13 -9 21.17 7.64 7 13 9 24.18 7.20 7 13 9 29.17 8.41 -7 13 -10 9.93 7.09 7 13 10 4.42 4.72 7 13 10 9.68 6.06 7 13 11 47.89 11.10 7 13 11 53.72 11.36 7 13 12 43.23 10.90 7 13 12 39.77 10.46 7 13 13 44.67 10.38 7 13 13 39.35 9.73 7 13 14 72.36 12.50 7 13 14 73.42 12.82 7 13 15 14.73 6.53 7 13 15 15.18 6.35 7 13 16 18.88 6.78 7 13 16 13.39 5.58 7 13 17 7.98 5.44 7 13 17 11.96 5.56 7 13 18 7.64 4.68 7 13 18 11.32 5.10 7 13 19 7.51 4.64 7 13 19 13.52 4.60 7 13 20 81.76 8.51 -7 13 -20 102.11 14.20 7 13 20 79.40 10.89 7 13 21 1.77 3.14 -7 13 -21 -3.53 3.73 7 13 22 6.14 2.97 -7 13 -22 3.98 4.26 7 13 23 2.21 1.95 -7 13 -23 4.98 3.75 -7 13 -24 -2.19 2.80 7 13 24 0.79 1.55 -7 14 28 3.98 2.28 -7 14 27 14.63 4.33 7 14 -27 18.95 3.78 -7 14 26 -0.91 3.10 7 14 -26 4.40 2.95 -7 14 25 13.93 5.19 7 14 -25 5.42 3.43 -7 14 24 28.53 7.22 7 14 -24 39.03 8.30 -7 14 23 2.15 4.64 7 14 -23 -0.06 3.70 -7 14 22 33.54 8.57 7 14 -22 27.95 7.29 -7 14 21 6.40 5.34 -7 14 21 -0.28 3.36 7 14 -21 0.15 5.76 7 14 -21 4.62 5.72 -7 14 20 1.08 3.93 -7 14 20 4.34 4.05 7 14 -20 0.26 5.60 7 14 -20 0.23 4.11 -7 14 19 9.57 5.97 -7 14 19 1.85 3.70 7 14 -19 4.15 4.81 7 14 -19 1.90 5.32 -7 14 18 4.59 5.28 -7 14 18 0.67 3.82 7 14 -18 7.69 6.22 7 14 -18 -2.88 4.74 -7 14 17 8.27 6.29 -7 14 17 5.12 4.45 7 14 -17 5.54 5.82 7 14 -17 -0.09 5.42 -7 14 16 17.26 7.48 -7 14 16 30.94 9.17 7 14 -16 20.86 9.47 7 14 -16 26.48 8.14 -7 14 15 0.62 3.86 -7 14 15 0.33 4.11 7 14 -15 2.33 6.34 7 14 -15 -2.10 5.96 -7 14 14 53.84 10.38 -7 14 14 54.73 11.41 7 14 -14 69.67 16.30 7 14 -14 49.82 12.68 -7 14 13 11.56 6.68 7 14 -13 21.84 9.91 7 14 -13 10.70 6.98 -7 14 12 51.30 11.53 7 14 -12 66.76 14.64 7 14 -12 70.66 13.65 -7 14 11 13.75 6.80 7 14 -11 25.33 9.69 7 14 -11 21.11 8.87 7 14 -10 68.58 14.90 7 14 -10 66.23 13.32 7 14 -9 113.18 15.79 7 14 -9 118.57 18.24 7 14 -9 110.15 16.36 7 14 -8 2.34 4.62 -7 14 8 5.61 7.32 7 14 -8 -3.05 5.24 7 14 -8 -10.84 6.23 7 14 -7 0.83 5.01 7 14 -7 -1.07 6.36 -7 14 7 6.92 5.27 7 14 -7 -0.01 4.79 7 14 -6 -2.23 4.05 7 14 -6 -5.30 6.50 7 14 -6 -0.13 3.84 -7 14 6 4.96 4.64 7 14 -5 1.22 3.39 -7 14 5 0.52 5.75 7 14 -5 -0.17 6.48 7 14 -5 -0.66 4.37 7 14 -4 51.77 10.69 7 14 -4 44.71 10.27 -7 14 4 38.00 11.05 7 14 -4 53.47 9.97 7 14 -4 55.42 13.93 7 14 -3 6.49 5.26 7 14 -3 7.56 4.52 -7 14 3 8.93 5.88 7 14 -3 -1.93 4.44 7 14 -3 13.13 9.14 7 14 -2 -0.94 3.96 7 14 -2 8.70 7.18 -7 14 2 -0.95 6.53 7 14 -2 8.07 7.09 7 14 -1 4.01 4.98 7 14 -1 8.78 7.45 -7 14 1 -0.39 5.21 7 14 -1 0.74 6.18 7 14 0 7.44 5.66 7 14 0 11.92 6.49 -7 14 0 8.08 6.62 7 14 0 8.46 5.66 7 14 1 55.43 12.83 7 14 1 84.78 17.54 -7 14 -1 3.82 6.76 7 14 1 26.83 11.95 7 14 2 4.49 4.57 7 14 2 12.22 7.17 -7 14 -2 5.23 4.88 7 14 2 13.76 6.78 7 14 3 33.31 9.66 7 14 3 27.01 8.07 -7 14 -3 26.60 11.27 7 14 3 23.92 6.97 7 14 4 7.86 5.22 -7 14 -4 5.06 6.87 7 14 4 5.97 5.06 7 14 5 49.59 12.11 -7 14 -5 34.66 11.58 7 14 5 32.52 9.17 7 14 6 20.36 8.85 -7 14 -6 10.26 6.06 7 14 6 11.08 5.79 -7 14 -7 -4.10 7.37 7 14 7 2.42 3.92 7 14 7 0.52 2.92 7 14 7 -4.67 6.25 7 14 8 9.45 5.72 7 14 8 -4.66 6.20 -7 14 -8 5.20 4.78 7 14 8 5.19 3.45 7 14 9 6.92 4.61 7 14 9 8.31 5.82 -7 14 -9 -0.71 5.56 7 14 9 4.06 3.88 7 14 10 19.63 6.12 -7 14 -10 26.69 10.80 7 14 10 21.03 7.21 7 14 10 21.71 5.42 7 14 11 2.52 5.53 7 14 11 -1.00 4.09 -7 14 -11 -1.02 5.80 7 14 11 7.52 4.31 7 14 12 11.32 5.34 7 14 12 3.05 3.47 -7 14 -12 11.83 7.86 7 14 13 7.76 6.28 7 14 13 8.13 4.62 -7 14 -13 9.56 5.65 7 14 14 4.75 3.48 7 14 14 5.20 3.45 -7 14 -14 -0.22 6.49 7 14 15 18.94 7.11 7 14 15 15.66 5.49 -7 14 -15 19.98 7.84 7 14 16 1.81 2.92 7 14 16 -0.73 3.06 -7 14 -16 4.59 5.21 7 14 17 37.62 7.74 7 14 17 38.14 8.14 -7 14 -17 30.56 9.39 7 14 18 -2.17 3.90 7 14 18 -1.41 3.52 -7 14 -18 0.26 4.43 7 14 19 3.65 3.31 7 14 19 8.98 3.69 -7 14 -19 8.66 5.50 7 14 20 1.77 1.91 7 14 20 5.48 3.36 7 14 21 16.37 4.16 -7 14 -21 17.14 5.42 -7 14 -22 -1.22 3.26 -7 14 -23 -1.29 2.06 -7 15 26 2.25 1.97 7 15 -26 3.07 2.06 -7 15 25 -0.05 2.64 7 15 -25 0.09 2.63 -7 15 24 54.45 8.18 7 15 -24 54.71 8.30 -7 15 23 -2.90 3.66 7 15 -23 -2.70 3.45 -7 15 22 8.00 5.38 7 15 -22 -2.43 3.59 -7 15 21 39.48 8.28 7 15 -21 43.15 9.47 -7 15 20 11.08 5.49 7 15 -20 -5.91 5.93 -7 15 20 3.72 3.44 7 15 -20 -0.48 3.78 -7 15 19 131.65 13.57 7 15 -19 164.99 19.50 7 15 -19 157.18 18.01 -7 15 19 139.00 16.38 -7 15 18 -5.46 4.87 -7 15 18 4.70 4.19 7 15 -18 1.68 4.95 7 15 -18 0.83 4.33 -7 15 17 34.07 8.53 -7 15 17 26.93 8.41 7 15 -17 26.11 9.45 7 15 -17 19.10 7.73 -7 15 16 0.72 4.37 -7 15 16 0.28 3.65 7 15 -16 11.40 8.52 7 15 -16 2.09 5.23 -7 15 15 17.77 6.93 7 15 -15 12.55 8.73 -7 15 15 9.74 4.83 7 15 -15 14.62 7.00 -7 15 14 51.18 9.63 7 15 -14 78.96 15.64 7 15 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4.62 6.92 -7 15 0 9.40 6.64 7 15 0 10.13 7.28 7 15 1 113.89 15.81 -7 15 -1 116.76 18.77 7 15 1 121.28 18.67 7 15 1 124.21 17.50 7 15 2 19.58 8.06 7 15 2 33.70 10.83 -7 15 -2 31.12 10.96 7 15 2 22.61 8.83 7 15 3 127.07 16.14 -7 15 -3 114.84 18.73 7 15 3 131.75 18.48 7 15 3 112.65 15.85 7 15 4 17.53 7.55 7 15 4 15.17 8.47 -7 15 -4 22.60 10.08 7 15 4 21.05 7.04 7 15 5 63.77 12.05 7 15 5 77.46 14.85 -7 15 -5 68.81 15.26 7 15 5 78.22 13.08 -7 15 -6 6.84 5.36 7 15 6 12.10 5.88 7 15 6 11.84 7.67 7 15 6 8.44 5.07 7 15 7 10.25 6.87 -7 15 -7 14.96 8.31 7 15 7 16.51 7.29 7 15 8 75.79 14.34 -7 15 -8 67.24 15.29 7 15 8 71.08 12.07 7 15 9 18.67 7.63 -7 15 -9 15.46 7.97 7 15 9 12.77 4.12 7 15 10 3.17 5.16 7 15 10 2.08 4.19 -7 15 -10 9.04 5.60 -7 15 -11 47.65 11.80 7 15 11 29.86 8.86 7 15 11 32.69 7.66 7 15 11 30.28 7.21 7 15 12 18.97 7.50 -7 15 -12 19.17 8.27 7 15 12 17.36 5.85 7 15 13 4.07 3.66 7 15 13 2.80 4.07 -7 15 -13 1.08 4.88 7 15 14 53.16 10.56 7 15 14 50.03 8.91 -7 15 -14 53.86 11.81 7 15 15 23.90 6.62 -7 15 -15 13.14 6.65 7 15 15 17.44 5.43 7 15 16 24.12 5.95 7 15 16 25.48 7.31 -7 15 -16 24.80 8.22 7 15 17 3.07 3.77 -7 15 -17 10.68 5.60 7 15 17 5.15 3.22 7 15 18 3.67 2.62 -7 15 -18 -3.71 4.61 7 15 19 -1.77 1.88 7 15 19 5.81 2.68 -7 15 -19 11.59 4.90 -7 15 -20 27.59 6.06 -7 15 -21 2.53 2.13 -7 15 -22 -2.09 2.33 -7 16 24 -5.05 3.02 7 16 -24 0.71 2.56 -7 16 23 11.87 3.58 7 16 -23 15.18 4.54 -7 16 22 33.73 6.12 7 16 -22 38.55 7.31 -7 16 21 4.58 3.14 7 16 -21 0.57 3.18 -7 16 20 5.29 3.86 7 16 -20 0.53 3.41 7 16 -20 8.57 4.72 -7 16 19 12.41 4.88 7 16 -19 11.81 5.34 7 16 -19 17.11 6.23 -7 16 18 5.13 3.41 -7 16 18 4.98 2.54 7 16 -18 10.09 5.92 7 16 -18 7.88 5.99 -7 16 17 23.06 6.24 -7 16 17 17.93 5.58 7 16 -17 17.76 7.15 7 16 -17 22.94 7.43 -7 16 16 15.87 4.62 -7 16 16 14.04 4.77 7 16 -16 23.45 8.71 7 16 -16 16.66 6.76 -7 16 15 22.88 5.87 7 16 -15 26.76 9.03 7 16 -15 34.47 9.38 -7 16 14 12.81 5.78 7 16 -14 22.30 9.31 7 16 -14 24.82 8.15 -7 16 13 36.75 8.90 7 16 -13 43.76 11.73 7 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12.44 -8 9 13 105.85 23.72 -8 9 13 62.09 13.04 8 9 -13 6.48 6.03 8 9 -13 8.19 8.78 -8 9 12 100.63 13.82 -8 9 12 101.57 21.99 8 9 -12 112.67 16.51 8 9 -12 119.47 18.56 -8 9 11 135.86 16.16 8 9 -11 151.15 18.91 8 9 -11 130.71 19.00 -8 9 11 146.39 28.87 -8 9 10 -4.42 5.54 -8 9 10 5.34 4.31 8 9 -10 0.64 3.77 8 9 -10 3.98 4.56 -8 9 9 57.77 18.33 -8 9 9 46.31 9.45 8 9 -9 75.34 14.25 -8 9 9 54.92 12.75 8 9 -9 61.60 13.35 -8 9 8 7.87 9.33 -8 9 8 10.23 5.47 8 9 -8 4.34 3.88 -8 9 8 10.76 7.59 8 9 -8 8.62 5.28 -8 9 7 89.79 12.25 -8 9 7 83.58 21.03 8 9 -7 95.30 14.33 -8 9 7 86.98 15.94 8 9 -7 100.48 15.69 -8 9 6 40.77 17.49 -8 9 6 41.58 8.21 8 9 -6 36.41 9.13 -8 9 6 40.16 11.83 8 9 -6 39.05 9.50 -8 9 5 125.99 26.91 -8 9 5 129.61 14.90 8 9 -5 135.31 17.41 -8 9 5 131.69 20.90 8 9 -5 124.05 16.40 -8 9 4 20.40 11.36 -8 9 4 17.29 6.34 8 9 -4 36.52 9.11 8 9 -4 30.32 7.78 -8 9 4 33.58 10.01 -8 9 3 10.48 6.66 -8 9 3 10.30 3.25 8 9 -3 16.32 5.09 -8 9 3 15.59 7.79 -8 9 2 73.01 14.20 -8 9 2 59.94 23.82 -8 9 2 64.91 15.65 8 9 -2 38.93 8.66 8 9 -2 44.06 9.71 -8 9 1 -2.27 9.70 -8 9 1 5.87 3.15 8 9 -1 14.28 7.85 -8 9 1 5.28 5.35 8 9 -1 16.20 6.77 -8 9 0 8.49 6.53 8 9 0 24.23 6.72 -8 9 0 9.52 6.41 -8 9 -1 93.20 13.21 -8 9 -1 104.10 16.84 8 9 1 112.93 16.82 -8 9 -2 72.12 13.74 8 9 2 80.86 13.36 8 9 2 93.21 15.31 8 9 3 47.26 9.02 -8 9 -3 47.54 11.54 8 9 3 50.90 11.33 8 9 4 31.97 8.86 8 9 4 35.01 7.96 -8 9 -4 39.10 10.77 8 9 5 199.71 19.46 -8 9 -5 233.60 24.97 8 9 5 253.29 24.82 8 9 6 8.21 3.80 8 9 6 5.33 5.65 -8 9 -6 3.41 4.80 -8 9 -6 -0.71 3.82 8 9 7 198.12 19.01 -8 9 -7 202.81 24.31 8 9 7 227.74 23.81 -8 9 -7 185.34 17.47 8 9 8 31.29 8.19 8 9 8 40.77 10.75 -8 9 -8 31.68 7.75 8 9 9 6.70 5.55 8 9 9 8.55 4.94 -8 9 -9 8.45 4.93 8 9 10 9.35 8.49 -8 9 -10 0.23 3.79 8 9 11 43.15 11.62 8 9 12 109.38 17.79 8 9 13 8.06 5.65 8 9 14 63.90 13.42 8 9 15 -1.21 5.34 8 9 16 -2.27 4.85 8 9 17 160.18 20.31 8 9 18 3.04 4.87 8 9 19 67.41 13.24 8 9 20 17.02 7.28 -8 9 -21 10.03 5.02 8 9 21 13.41 5.76 8 9 22 -2.03 4.41 -8 9 -22 -1.09 3.79 -8 9 -22 0.83 3.64 8 9 23 -0.28 3.10 -8 9 -23 2.89 3.02 -8 9 -23 2.12 3.37 8 9 24 4.92 3.83 -8 9 -24 3.73 2.80 -8 9 -24 -0.66 2.73 8 9 25 4.08 2.71 -8 9 -25 6.03 2.79 8 9 26 -1.47 2.13 -8 10 31 -0.35 2.16 8 -10 -30 4.64 2.25 -8 10 30 0.08 2.86 8 10 -30 -0.25 1.54 8 -10 -29 -4.43 2.47 -8 10 29 1.89 2.92 8 10 -29 -0.13 2.34 8 -10 -28 12.25 4.28 -8 10 28 3.73 3.33 8 10 -28 1.87 2.70 8 -10 -27 2.47 3.45 -8 10 27 -1.70 5.26 8 -10 -26 -4.59 3.77 8 -10 -25 37.12 8.60 8 -10 -24 2.43 3.87 8 -10 -23 17.19 6.28 -8 10 23 22.30 8.46 -8 10 22 16.03 8.36 -8 10 21 4.30 5.94 8 10 -21 -0.25 9.15 -8 10 20 59.84 12.89 8 10 -20 69.00 14.89 -8 10 19 86.04 15.62 8 10 -19 106.70 18.40 -8 10 18 44.99 11.85 8 10 -18 40.76 12.21 -8 10 17 49.37 12.08 8 -10 -17 43.24 8.88 8 10 -17 56.77 14.53 -8 10 16 22.01 8.28 8 -10 -16 26.59 6.80 8 10 -16 41.53 12.79 -8 10 15 2.29 4.87 8 -10 -15 5.97 4.71 8 10 -15 7.78 8.53 -8 10 14 -1.16 4.95 8 10 -14 2.97 7.60 -8 10 13 243.85 25.47 8 10 -13 239.96 26.29 -8 10 13 217.47 32.01 -8 10 12 6.43 4.79 -8 10 12 3.25 7.29 -8 10 12 2.13 4.86 8 10 -12 9.22 6.46 8 10 -12 15.55 8.49 -8 10 11 290.49 37.27 -8 10 11 272.45 22.32 8 10 -11 321.78 27.37 8 10 -11 334.12 30.27 -8 10 10 11.10 5.19 -8 10 10 5.24 7.13 8 10 -10 11.71 6.40 8 10 -10 9.59 7.69 -8 10 9 32.39 7.99 -8 10 9 16.71 10.38 8 10 -9 35.25 9.36 -8 10 9 28.70 10.58 8 10 -9 26.58 8.83 -8 10 8 81.28 20.57 -8 10 8 59.83 9.99 8 10 -8 66.13 12.16 -8 10 8 65.94 14.46 8 10 -8 81.00 14.46 -8 10 7 -1.26 5.77 -8 10 7 6.44 5.65 8 10 -7 4.28 3.70 -8 10 7 4.25 6.89 8 10 -7 4.92 4.89 -8 10 6 47.38 16.17 -8 10 6 58.39 9.84 8 10 -6 76.67 13.75 -8 10 6 55.35 13.37 8 10 -6 73.46 14.22 -8 10 5 1.64 5.08 -8 10 5 10.23 6.56 8 10 -5 6.13 5.29 8 10 -5 6.78 4.74 -8 10 5 12.17 7.78 -8 10 4 69.00 19.92 -8 10 4 63.32 10.10 8 10 -4 84.63 14.08 8 10 -4 83.87 13.38 -8 10 4 70.20 14.38 -8 10 3 10.68 7.65 -8 10 3 5.13 5.72 8 10 -3 3.97 3.48 8 10 -3 1.10 4.94 -8 10 3 6.86 5.98 -8 10 2 37.84 14.14 -8 10 2 48.58 9.62 8 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11 -4 34.88 10.36 -8 11 4 40.02 11.13 -8 11 3 27.06 7.15 -8 11 3 16.46 7.88 8 11 -3 17.21 6.21 8 11 -3 18.97 6.11 -8 11 3 18.06 9.14 8 11 -3 31.69 11.02 -8 11 2 14.29 5.54 8 11 -2 9.25 3.58 8 11 -2 11.98 6.17 -8 11 2 10.13 5.67 8 11 -2 22.15 8.72 -8 11 1 9.02 5.23 8 11 -1 14.11 6.75 -8 11 1 17.02 7.99 8 11 -1 14.75 8.12 -8 11 0 3.46 3.87 8 11 0 11.47 6.92 -8 11 0 11.21 8.20 8 11 0 5.48 4.54 -8 11 -1 4.83 3.61 8 11 1 10.35 6.71 -8 11 -1 2.52 4.46 8 11 1 3.24 4.57 -8 11 -2 -2.19 3.55 -8 11 -2 0.33 4.82 8 11 2 3.42 6.30 8 11 2 0.69 4.33 -8 11 -3 7.88 5.56 8 11 3 17.89 6.44 -8 11 -3 14.01 9.36 8 11 3 11.82 4.96 -8 11 -4 164.95 17.75 8 11 4 182.94 21.29 -8 11 -4 187.40 23.46 8 11 4 179.90 20.30 8 11 5 21.34 9.13 8 11 5 22.16 7.28 -8 11 -5 15.61 9.02 -8 11 -6 314.28 30.37 8 11 6 271.20 25.35 8 11 6 262.36 25.96 8 11 7 5.11 4.97 8 11 7 7.24 5.48 -8 11 -7 4.89 6.38 8 11 8 2.84 3.60 -8 11 -8 8.29 5.34 8 11 8 7.44 6.60 8 11 9 13.20 5.63 8 11 9 17.75 8.04 -8 11 -9 13.72 6.67 8 11 10 16.14 7.54 8 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2.50 4.90 -8 12 23 0.02 4.63 8 12 -23 -1.37 4.06 8 -12 -22 8.02 3.59 -8 12 22 14.64 6.56 -8 12 22 10.39 5.38 -8 12 21 5.23 3.89 -8 12 21 0.60 4.43 8 12 -21 -2.29 4.98 -8 12 20 60.12 11.64 -8 12 20 47.81 11.11 8 12 -20 57.54 13.71 -8 12 19 4.74 3.80 -8 12 19 21.57 6.89 8 12 -19 18.54 7.28 -8 12 18 0.11 3.99 -8 12 18 6.79 6.07 8 12 -18 16.14 9.48 -8 12 17 15.11 5.73 -8 12 17 11.67 6.36 8 12 -17 26.86 10.47 -8 12 16 4.40 3.59 -8 12 16 17.32 8.42 8 12 -16 16.58 11.57 -8 12 15 -4.44 6.80 8 12 -15 21.54 9.85 -8 12 14 17.77 8.74 8 12 -14 8.63 6.93 -8 12 13 15.41 7.95 8 12 -13 38.42 11.40 -8 12 12 156.67 20.85 8 12 -12 155.48 21.72 8 12 -11 92.58 15.25 8 12 -11 109.18 19.05 -8 12 10 15.77 5.92 8 12 -10 34.16 9.77 8 12 -10 23.96 9.54 -8 12 9 12.76 5.74 8 12 -9 19.48 6.84 8 12 -9 25.86 10.34 -8 12 8 77.27 11.58 8 12 -8 90.03 14.53 -8 12 8 80.67 17.02 8 12 -8 84.52 15.39 -8 12 7 51.22 9.18 8 12 -7 57.10 12.06 -8 12 7 50.43 14.18 8 12 -7 51.27 12.43 -8 12 6 68.11 10.46 8 12 -6 71.93 13.47 -8 12 6 64.47 14.60 8 12 -6 71.06 13.99 8 12 -6 56.08 11.24 -8 12 5 17.24 6.95 8 12 -5 13.68 6.87 -8 12 5 27.86 11.52 8 12 -5 13.62 5.79 8 12 -5 15.05 5.54 -8 12 4 73.14 10.77 8 12 -4 74.96 13.49 8 12 -4 80.81 13.31 -8 12 4 73.77 15.80 8 12 -4 67.95 11.82 -8 12 3 2.83 4.11 8 12 -3 2.87 4.03 8 12 -3 -4.07 7.20 -8 12 3 0.59 5.87 8 12 -3 9.56 7.35 -8 12 2 5.88 4.07 8 12 -2 2.99 4.73 8 12 -2 -1.02 7.05 -8 12 2 -2.16 5.30 8 12 -2 16.64 8.20 -8 12 1 19.60 7.78 8 12 -1 1.83 4.92 -8 12 1 6.46 7.41 8 12 -1 11.34 7.14 8 12 -1 13.49 8.70 -8 12 0 88.81 12.63 8 12 0 67.76 14.24 8 12 0 85.91 14.38 -8 12 0 84.75 16.81 8 12 0 85.01 14.21 -8 12 -1 95.53 12.28 -8 12 -1 109.98 18.95 8 12 1 104.72 16.55 8 12 1 93.86 14.38 -8 12 -2 11.52 6.48 8 12 2 24.10 8.22 -8 12 -2 10.37 7.55 8 12 2 10.49 6.83 -8 12 -3 86.47 12.88 -8 12 -3 95.55 18.12 8 12 3 99.86 16.38 8 12 3 85.17 13.33 -8 12 -4 197.13 18.38 -8 12 -4 200.22 25.79 8 12 4 211.83 22.80 8 12 4 216.41 19.34 8 12 5 10.14 6.62 -8 12 -5 6.43 5.39 8 12 5 1.35 4.57 -8 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12.70 6.17 9 13 -17 16.92 7.08 9 13 -17 2.83 4.78 -9 13 16 -2.68 5.49 9 13 -16 3.61 6.68 9 13 -16 -4.39 6.36 -9 13 15 16.70 6.90 9 13 -15 15.74 7.88 9 13 -15 -2.59 6.06 -9 13 14 3.71 4.89 9 13 -14 11.18 8.85 9 13 -14 -6.49 6.17 -9 13 13 21.35 8.96 9 13 -13 24.30 10.46 9 13 -13 13.10 7.07 -9 13 12 4.18 6.07 9 13 -12 5.99 5.95 9 13 -12 -0.15 4.20 -9 13 11 90.59 15.99 9 13 -11 115.35 18.70 9 13 -11 78.32 13.58 -9 13 10 38.39 11.42 9 13 -10 43.31 11.28 9 13 -10 47.88 13.35 9 13 -10 29.45 8.18 -9 13 9 8.64 4.79 9 13 -9 26.27 9.96 9 13 -9 17.78 10.00 9 13 -9 11.17 5.43 -9 13 8 77.40 10.95 9 13 -8 81.91 14.82 9 13 -8 79.42 15.77 9 13 -8 73.15 12.71 -9 13 7 99.94 12.65 9 13 -7 115.34 16.28 9 13 -7 101.50 16.42 9 13 -7 79.67 13.05 -9 13 6 3.76 4.97 9 13 -6 6.08 6.15 -9 13 6 2.83 8.36 9 13 -6 7.34 7.04 9 13 -6 -0.74 3.15 -9 13 5 25.65 7.09 9 13 -5 21.96 7.67 -9 13 5 13.21 8.18 9 13 -5 17.21 6.84 -9 13 4 27.25 7.41 9 13 -4 26.32 7.86 -9 13 4 22.76 10.96 9 13 -4 28.53 8.12 -9 13 3 4.48 3.56 9 13 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9.08 -9 14 11 61.89 12.91 9 14 -11 75.31 15.05 9 14 -11 48.65 10.43 -9 14 10 9.41 6.56 9 14 -10 1.59 3.86 9 14 -10 17.04 10.47 9 14 -9 54.35 13.11 9 14 -9 46.06 10.34 9 14 -8 39.76 10.31 9 14 -8 28.26 9.25 9 14 -8 26.13 7.19 9 14 -7 6.65 6.54 9 14 -7 11.80 7.33 9 14 -7 6.56 3.86 9 14 -6 3.48 5.12 9 14 -6 0.85 4.68 9 14 -6 8.23 4.68 9 14 -5 14.49 6.10 -9 14 5 19.47 9.07 9 14 -5 6.73 6.00 9 14 -4 4.30 6.66 -9 14 4 17.15 8.93 9 14 -4 8.30 6.70 9 14 -3 47.28 10.54 -9 14 3 34.39 11.13 9 14 -3 34.52 9.16 9 14 -2 -4.77 4.00 9 14 -2 1.52 4.33 -9 14 1 2.56 4.13 9 14 -1 -1.51 4.57 -9 14 1 0.05 6.23 9 14 -1 -6.42 6.17 -9 14 0 15.98 5.24 9 14 0 15.44 7.98 9 14 0 14.43 6.38 -9 14 0 24.56 9.93 -9 14 -1 22.62 6.74 9 14 1 14.87 6.98 9 14 1 13.69 5.84 -9 14 -1 32.29 11.42 -9 14 -2 70.33 9.28 9 14 2 57.84 11.74 9 14 2 64.40 11.67 -9 14 -2 68.13 15.19 -9 14 -3 2.19 3.95 9 14 3 8.47 4.53 9 14 3 3.00 4.20 -9 14 -3 6.84 7.32 -9 14 -4 3.64 3.61 9 14 4 -0.38 4.10 9 14 4 -8.47 6.69 -9 14 -4 4.30 6.31 -9 14 -5 7.08 4.05 9 14 5 7.10 4.97 9 14 5 1.90 4.04 -9 14 -5 4.46 6.07 -9 14 -6 45.80 7.87 9 14 6 33.19 9.07 9 14 6 35.28 8.43 -9 14 -6 45.16 11.25 -9 14 -7 2.13 3.52 9 14 7 -1.60 3.39 9 14 7 -4.56 4.72 -9 14 -7 -1.23 4.76 -9 14 -8 61.40 8.57 9 14 8 49.95 9.67 9 14 8 49.24 9.49 -9 14 -8 55.80 12.82 -9 14 -9 5.97 2.95 9 14 9 5.54 3.98 -9 14 -9 4.37 5.70 -9 14 -10 19.00 4.87 9 14 10 10.96 4.84 -9 14 -10 13.80 6.64 -9 14 -11 19.87 4.45 9 14 11 21.82 6.07 -9 14 -11 22.24 8.04 -9 14 -12 -2.45 2.50 9 14 12 0.52 3.16 -9 14 -12 2.34 4.99 -9 14 -13 3.90 2.23 9 14 13 2.88 2.08 -9 14 -13 4.63 4.26 -9 14 -14 -1.05 2.11 -9 14 -14 -0.89 3.42 -9 14 -15 -2.29 3.31 9 14 16 2.27 2.39 -9 14 -16 -1.12 2.75 9 14 17 2.59 1.87 -9 14 -17 8.84 3.43 9 14 18 6.39 2.11 -9 14 -18 12.05 4.02 9 15 -23 11.54 3.33 9 15 -22 5.34 3.03 9 15 -21 -1.12 2.96 -9 15 20 -1.22 3.22 9 15 -20 -2.90 3.66 -9 15 19 23.58 5.59 9 15 -19 21.29 6.67 9 15 -19 30.84 6.63 9 -15 -18 0.00 1.85 -9 15 18 0.86 3.06 9 15 -18 -7.49 5.70 9 15 -18 -0.90 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16 -2 2.08 5.43 9 16 2 5.99 4.86 9 16 3 -0.73 2.76 -9 16 -3 0.72 4.23 9 16 3 -6.85 5.43 9 16 4 4.11 2.64 -9 16 -4 1.37 4.42 9 16 4 2.68 3.91 9 16 5 1.99 2.89 9 16 5 3.30 3.28 -9 16 -5 5.38 5.44 9 16 6 23.90 6.43 9 16 6 14.76 5.39 -9 16 -6 27.30 9.26 9 16 7 1.01 2.61 9 16 7 -0.84 2.80 9 16 8 8.44 3.49 9 16 8 10.36 4.89 -9 16 -8 14.29 6.47 9 16 9 2.30 2.39 9 16 9 -3.75 3.28 9 16 10 5.91 3.14 9 16 10 8.35 3.92 -9 16 -10 0.70 3.19 9 16 11 6.48 2.80 9 16 11 1.23 2.05 -9 16 -11 2.58 4.18 9 16 12 6.60 2.61 9 16 12 5.51 1.83 9 16 13 8.99 2.28 -9 16 -13 11.64 3.99 -9 16 -14 3.20 3.22 -9 16 -15 4.66 3.27 9 17 -19 -8.45 3.04 9 17 -18 23.16 4.91 9 17 -17 14.80 4.15 9 17 -17 15.90 4.21 -9 17 16 4.71 2.47 9 17 -16 3.59 3.47 -9 17 15 6.10 2.94 9 17 -15 -1.12 3.57 9 17 -15 4.34 3.56 -9 17 14 8.19 3.34 9 17 -14 12.20 5.66 9 17 -14 14.37 4.70 -9 17 13 3.07 3.04 9 17 -13 0.49 3.80 9 17 -13 1.05 3.06 -9 17 12 10.16 3.53 9 17 -12 17.68 7.18 9 17 -12 17.12 5.31 -9 17 11 8.92 4.24 9 17 -11 11.86 6.04 9 17 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15.61 8.79 10 10 -12 27.39 10.46 -10 10 11 247.03 21.92 -10 10 11 257.31 26.99 10 10 -11 277.76 25.46 10 10 -11 235.39 24.44 -10 10 10 22.50 7.95 -10 10 10 17.65 9.30 10 10 -10 23.87 9.09 10 10 -10 26.92 9.33 -10 10 9 3.01 4.81 10 10 -9 2.51 4.85 -10 10 8 45.14 10.63 10 10 -8 40.91 9.75 10 10 -8 52.38 12.66 -10 10 7 29.33 8.29 10 10 -7 22.06 8.23 10 10 -7 15.11 7.08 -10 10 6 42.42 10.56 10 10 -6 20.50 7.35 -10 10 6 33.59 12.37 10 10 -6 27.71 9.88 -10 10 5 61.38 11.51 10 10 -5 48.75 11.44 -10 10 5 43.73 12.32 10 10 -5 43.07 11.56 -10 10 4 14.68 8.12 10 10 -4 1.29 4.21 -10 10 4 9.92 8.23 10 10 -4 0.68 3.74 -10 10 3 46.27 10.40 10 10 -3 40.60 10.31 -10 10 3 50.21 13.58 10 10 -3 34.52 9.36 -10 10 2 35.22 9.14 10 10 -2 28.19 9.67 -10 10 2 21.48 9.71 10 10 -2 18.86 7.11 -10 10 1 16.09 7.68 10 10 -1 3.72 6.05 10 10 -1 7.58 4.76 -10 10 1 10.99 8.46 -10 10 0 14.78 6.65 10 10 0 17.28 7.49 10 10 0 16.21 5.63 -10 10 0 22.15 9.52 10 10 1 7.79 3.67 -10 10 -1 13.08 8.60 -10 10 -2 33.31 11.60 10 10 2 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6.33 10 11 -25 42.08 7.01 10 -11 -24 1.05 3.07 10 11 -24 -4.71 3.04 10 -11 -23 26.99 5.76 10 11 -23 24.35 6.57 10 -11 -22 56.67 8.51 -10 11 22 60.43 10.15 -10 11 21 -0.73 4.90 -10 11 20 4.47 4.95 -10 11 19 -3.62 4.67 10 11 -19 -2.41 7.56 -10 11 18 -1.80 5.41 10 -11 -18 7.29 4.46 10 11 -18 10.39 6.77 -10 11 17 13.41 6.87 10 -11 -17 11.16 4.60 10 11 -17 14.28 7.65 -10 11 16 6.02 6.03 10 -11 -16 9.23 5.54 10 11 -16 0.11 4.51 -10 11 15 3.91 5.85 10 -11 -15 -0.30 4.68 10 11 -15 6.82 6.93 -10 11 14 142.57 19.72 10 -11 -14 108.13 13.98 10 11 -14 136.83 18.99 -10 11 13 7.11 7.17 10 -11 -13 18.06 6.67 10 11 -13 22.45 9.95 -10 11 12 26.47 9.67 10 11 -12 53.00 13.65 -10 11 11 34.97 9.16 -10 11 11 26.09 9.95 10 11 -11 31.47 9.91 10 11 -11 44.74 11.65 -10 11 10 116.53 14.96 -10 11 10 106.51 18.01 10 11 -10 116.73 16.26 10 11 -10 104.08 17.06 -10 11 9 82.17 13.04 10 11 -9 89.25 14.93 10 11 -9 90.44 16.48 -10 11 8 22.93 7.74 10 11 -8 17.75 7.96 10 11 -8 29.52 10.41 -10 11 7 14.01 6.97 10 11 -7 15.08 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-7 49.15 9.29 14 -3 -6 16.91 7.15 -14 3 6 16.64 8.26 -14 3 5 51.83 8.75 14 -3 -5 51.47 9.03 -14 3 5 61.15 10.46 -14 -3 4 17.73 7.16 -14 3 4 30.47 8.79 -14 3 3 56.52 8.95 -14 -3 3 51.93 9.11 -14 3 3 57.91 10.21 -14 3 2 23.41 6.43 -14 -3 2 11.84 6.06 -14 3 2 8.70 6.16 -14 3 1 -0.34 3.05 -14 -3 1 0.25 3.26 -14 3 1 3.66 4.19 -14 3 0 -1.20 3.04 -14 -3 0 -4.23 4.07 -14 3 0 -1.53 3.79 -14 3 -1 -0.71 2.75 -14 -3 -1 0.62 3.00 -14 3 -1 -1.71 4.39 -14 3 -2 2.29 3.13 -14 -3 -2 8.16 4.59 -14 3 -2 9.05 4.77 -14 3 -3 10.59 3.78 -14 -3 -3 15.54 5.01 -14 3 -3 23.63 6.20 -14 3 -4 6.90 3.49 -14 -3 -4 0.99 2.89 -14 3 -4 5.71 3.58 -14 3 -5 14.70 4.01 -14 -3 -5 10.31 3.73 -14 3 -5 12.45 4.70 -14 3 -6 2.93 2.33 -14 -3 -6 -1.06 2.25 -14 3 -6 3.00 4.09 -14 3 -7 0.45 2.16 -14 -3 -7 0.92 2.13 -14 3 -7 -0.02 2.65 -14 3 -8 5.79 2.42 -14 -3 -8 3.74 2.73 -14 3 -8 7.46 3.77 -14 3 -9 1.64 1.85 -14 -3 -9 2.51 2.47 -14 3 -9 1.55 2.50 -14 3 -10 -2.06 1.76 -14 -3 -10 2.00 2.04 -14 3 -10 5.32 2.77 -14 3 -11 4.26 2.38 -14 3 -12 7.70 2.66 14 -4 -21 26.24 4.55 14 -4 -20 3.06 1.66 14 -4 -20 3.50 2.68 14 -4 -19 18.79 3.46 14 -4 -19 17.25 4.15 14 -4 -18 17.31 3.71 14 -4 -18 11.93 4.29 14 -4 -17 66.84 7.08 14 4 -17 52.78 5.08 14 -4 -17 60.75 8.30 14 4 -16 2.90 2.43 14 -4 -16 -3.11 3.58 14 -4 -15 42.69 7.56 14 -4 -14 12.69 4.85 14 -4 -13 35.94 7.12 14 -4 -12 8.04 5.50 14 -4 -11 3.02 4.20 14 -4 -10 15.79 6.36 14 -4 -9 58.97 9.79 -14 4 8 36.38 7.71 14 -4 -8 6.76 6.10 -14 4 7 9.77 5.52 14 -4 -7 4.86 4.20 -14 4 6 24.89 7.10 14 -4 -6 22.40 6.88 -14 4 6 19.89 7.02 -14 4 5 37.37 7.55 -14 4 5 33.88 8.24 -14 4 4 28.12 7.12 -14 4 4 23.80 7.65 -14 4 3 19.85 5.84 -14 -4 3 10.69 4.88 -14 4 3 15.32 6.06 -14 -4 2 4.35 4.14 -14 4 2 7.79 4.05 -14 -4 1 6.90 3.95 -14 4 1 6.00 4.73 -14 4 0 7.48 3.70 -14 -4 0 0.18 2.77 -14 4 0 -0.39 3.34 -14 4 -1 -0.55 2.96 -14 -4 -1 0.06 2.71 -14 4 -1 4.52 4.38 -14 4 -2 -1.72 3.02 -14 -4 -2 4.45 3.44 -14 4 -2 7.62 4.23 -14 4 -3 5.47 3.37 -14 -4 -3 3.09 3.24 -14 4 -3 -1.38 2.95 -14 4 -4 3.71 2.49 -14 -4 -4 4.76 3.26 -14 4 -4 4.75 3.76 -14 4 -5 14.20 4.20 -14 -4 -5 19.66 4.63 -14 4 -5 18.03 5.39 -14 4 -6 1.50 2.61 -14 -4 -6 -0.57 2.11 -14 4 -6 6.52 3.99 -14 4 -7 32.97 5.35 -14 -4 -7 28.69 4.72 -14 4 -7 32.00 6.11 -14 4 -8 -0.02 1.89 -14 -4 -8 -0.92 1.92 -14 4 -8 1.13 2.63 -14 4 -9 8.65 2.94 -14 -4 -9 1.91 1.30 -14 4 -9 14.42 4.67 -14 4 -10 6.37 2.27 -14 4 -10 4.67 2.35 -14 4 -11 4.91 2.35 14 -5 -21 2.41 2.28 14 -5 -20 8.38 2.03 14 -5 -20 4.20 2.39 14 -5 -19 4.97 2.37 14 -5 -19 -0.63 2.22 14 -5 -18 3.45 2.18 14 -5 -18 -2.35 2.91 14 -5 -17 1.00 2.68 14 -5 -16 1.20 3.52 14 -5 -15 7.23 4.55 14 -5 -14 -4.06 3.80 14 -5 -13 -2.40 3.87 14 -5 -12 69.04 9.90 14 -5 -11 3.88 4.68 14 -5 -10 29.17 7.80 14 -5 -9 64.67 11.26 -14 5 8 60.87 10.14 14 -5 -8 42.27 8.99 -14 5 7 63.17 9.64 14 -5 -7 68.93 11.06 -14 5 6 34.14 7.77 -14 5 5 10.59 5.41 -14 5 5 12.43 5.13 -14 5 4 27.91 7.24 -14 5 4 16.27 5.76 -14 5 3 49.46 8.83 -14 5 3 34.85 7.38 -14 5 2 41.49 8.51 -14 5 2 27.19 7.48 -14 5 1 37.18 7.07 -14 -5 1 30.04 6.15 -14 5 1 28.85 6.66 -14 5 0 10.27 5.14 -14 -5 0 7.62 3.84 -14 5 0 4.66 4.40 -14 5 -1 16.25 4.99 -14 -5 -1 19.78 5.18 -14 5 -1 16.84 5.24 -14 5 -2 9.42 4.37 -14 -5 -2 3.30 2.84 -14 5 -2 5.04 3.65 -14 5 -3 -1.37 3.18 -14 -5 -3 0.09 2.18 -14 5 -3 0.52 2.77 -14 5 -4 17.91 4.65 -14 5 -4 7.67 3.82 -14 5 -5 7.40 3.84 -14 -5 -5 0.90 1.67 -14 5 -5 4.28 2.67 -14 5 -6 11.41 3.88 -14 -5 -6 5.54 2.17 -14 5 -6 3.34 2.63 -14 5 -7 -3.39 2.78 -14 -5 -7 2.53 1.42 -14 5 -7 1.39 2.86 -14 5 -8 15.49 3.61 -14 5 -8 14.00 3.69 -14 5 -9 4.30 2.53 -14 5 -9 4.19 2.65 -14 5 -10 6.90 2.24 -14 5 -10 2.94 1.61 14 -6 -20 2.76 2.04 14 -6 -19 2.83 2.03 14 -6 -19 6.82 2.92 14 -6 -18 84.35 7.52 14 -6 -18 85.05 8.18 14 -6 -17 21.25 4.52 14 -6 -16 53.40 7.22 14 -6 -15 32.78 6.38 -14 6 14 -0.42 2.42 14 -6 -14 3.52 3.12 -14 6 13 -4.83 2.66 14 -6 -13 -0.08 3.29 -14 6 12 -5.51 2.07 14 -6 -12 5.89 4.20 -14 6 11 8.04 3.06 14 -6 -11 3.06 4.05 14 -6 -10 79.69 10.76 14 -6 -9 10.65 6.15 14 -6 -8 65.64 10.51 -14 6 7 25.64 7.16 14 -6 -7 16.99 6.88 -14 6 6 24.80 7.12 -14 6 5 36.45 7.11 -14 6 4 15.52 5.93 -14 6 4 10.54 4.77 -14 6 3 5.10 4.28 -14 6 3 9.45 4.18 -14 6 2 9.30 4.84 14 6 -2 0.91 1.84 -14 6 2 4.10 3.87 -14 6 1 12.22 4.95 14 6 -1 10.59 3.01 -14 6 1 6.85 3.65 -14 6 0 8.43 4.51 14 6 0 0.33 1.87 -14 6 0 5.86 3.15 -14 6 -1 6.53 3.47 14 6 1 9.61 2.97 -14 6 -1 6.89 3.54 -14 6 -2 4.66 3.31 14 6 2 -1.97 1.83 -14 6 -2 0.31 2.39 -14 6 -3 -3.27 2.86 14 6 3 0.05 1.55 -14 6 -3 -2.97 2.88 14 6 4 1.78 1.31 -14 6 -4 3.44 2.73 -14 6 -5 2.54 2.61 14 6 5 3.78 2.29 -14 6 -5 -4.31 3.17 -14 6 -6 61.90 7.32 -14 6 -6 47.91 6.64 -14 6 -7 2.76 1.98 -14 6 -7 1.99 2.30 -14 6 -8 4.83 2.33 -14 6 -8 6.60 2.82 -14 6 -9 0.55 1.85 -14 6 -9 1.28 1.78 14 -7 -18 0.79 1.65 14 -7 -18 -0.91 1.90 14 -7 -17 1.07 2.43 14 -7 -16 -7.31 3.45 14 -7 -15 21.66 4.96 -14 7 14 -4.74 2.37 14 -7 -14 0.11 3.24 -14 7 13 6.87 2.53 14 -7 -13 6.38 4.19 -14 7 12 7.78 3.06 14 -7 -12 7.91 3.59 -14 7 11 3.49 2.45 14 -7 -11 6.24 4.52 -14 7 10 3.03 1.98 14 -7 -10 7.13 4.23 -14 7 9 8.62 3.23 14 -7 -9 15.08 5.12 -14 7 8 73.58 7.27 14 -7 -8 83.16 10.93 -14 7 7 21.46 4.13 14 -7 -7 24.62 6.71 -14 7 6 36.86 7.07 -14 7 5 19.59 6.23 -14 7 4 18.37 5.49 -14 7 3 23.81 6.36 -14 7 2 30.05 6.74 14 7 -2 29.19 5.43 -14 7 2 28.53 5.53 -14 7 1 33.72 6.83 14 7 -1 26.86 5.07 -14 7 1 22.82 5.09 -14 7 0 7.35 4.17 14 7 0 2.87 2.46 -14 7 0 1.52 2.05 -14 7 -1 -0.15 2.55 14 7 1 1.03 1.98 -14 7 -1 -2.63 2.08 -14 7 -2 11.04 4.35 14 7 2 9.50 2.81 -14 7 -2 8.37 2.70 -14 7 -3 6.93 3.82 14 7 3 3.98 2.28 -14 7 -3 1.48 1.99 -14 7 -4 12.24 4.09 14 7 4 6.18 2.24 -14 7 -4 6.41 2.81 -14 7 -5 12.86 3.83 14 7 5 11.88 2.70 -14 7 -5 11.06 3.26 -14 7 -6 5.33 2.54 -14 7 -6 3.18 2.17 -14 7 -7 9.33 2.77 -14 7 -7 9.86 2.61 -14 7 -8 7.44 2.62 -14 7 -9 0.31 1.32 14 -8 -17 0.15 1.62 14 -8 -17 1.02 1.82 14 -8 -16 47.33 5.78 14 -8 -15 9.68 3.43 -14 8 14 35.45 4.93 14 -8 -14 38.41 6.07 -14 8 13 5.70 2.51 14 -8 -13 2.67 3.37 -14 8 12 9.90 3.14 14 -8 -12 7.87 3.64 -14 8 11 4.17 2.76 14 -8 -11 6.69 3.82 -14 8 10 41.48 5.57 14 -8 -10 46.43 7.41 -14 8 9 51.91 6.19 14 -8 -9 60.21 8.46 -14 8 8 39.57 5.64 14 -8 -8 39.65 7.02 -14 8 7 7.18 3.03 14 -8 -7 4.99 4.06 -14 8 6 1.86 3.05 -14 8 6 1.02 2.08 14 -8 -6 4.70 3.94 -14 8 5 5.13 3.22 -14 8 5 6.86 2.43 -14 8 4 8.28 3.90 -14 8 4 5.70 2.44 -14 8 3 13.28 4.72 -14 8 2 23.09 5.96 14 8 -2 15.68 4.14 -14 8 1 41.50 6.98 14 8 -1 39.16 5.94 -14 8 0 14.75 4.85 14 8 0 15.10 4.13 -14 8 -1 6.11 3.12 14 8 1 6.34 2.95 -14 8 -1 5.34 2.33 -14 8 -2 1.48 2.58 14 8 2 2.18 2.02 -14 8 -2 4.44 2.30 -14 8 -3 7.74 3.16 14 8 3 4.12 1.85 -14 8 -3 4.48 2.05 -14 8 -4 5.33 2.87 14 8 4 3.23 1.69 -14 8 -5 15.12 3.79 14 8 5 5.26 1.81 -14 8 -6 37.94 5.19 -14 8 -7 47.12 5.21 -14 8 -8 45.71 4.65 14 -9 -15 26.29 3.93 14 -9 -14 -0.38 2.15 -14 9 13 14.52 3.04 14 -9 -13 18.60 4.36 -14 9 12 1.96 1.74 14 -9 -12 -0.02 2.34 -14 9 11 3.69 2.01 14 -9 -11 6.09 2.98 -14 9 10 38.74 5.09 14 -9 -10 42.17 6.50 -14 9 9 41.59 5.36 14 -9 -9 41.03 6.57 -14 9 8 11.64 3.50 14 -9 -8 10.08 4.06 -14 9 7 39.43 5.18 14 -9 -7 36.01 6.47 -14 9 6 10.91 2.93 14 -9 -6 -0.09 3.54 -14 9 5 -1.96 2.51 -14 9 5 0.74 2.20 14 -9 -5 2.38 2.85 -14 9 4 1.20 2.61 -14 9 4 -2.30 1.63 -14 9 3 -0.58 2.53 -14 9 3 5.34 2.10 -14 9 2 8.12 3.48 -14 9 1 9.00 3.90 14 9 -1 3.86 2.49 -14 9 0 25.84 4.95 14 9 0 16.03 3.42 -14 9 -1 3.21 2.88 14 9 1 -0.19 1.41 -14 9 -2 4.87 2.75 14 9 2 4.77 2.17 -14 9 -3 -0.52 1.86 14 9 3 0.24 1.66 -14 9 -4 6.76 2.91 -14 9 -5 10.42 2.96 -14 9 -6 19.26 3.31 14 -10 -12 1.01 1.84 14 -10 -11 8.25 3.05 -14 10 10 -1.34 2.04 14 -10 -10 3.03 2.25 -14 10 9 10.72 2.69 14 -10 -9 12.89 4.02 -14 10 8 6.59 2.48 14 -10 -8 2.64 2.74 -14 10 7 -1.61 2.20 14 -10 -7 -1.20 2.87 -14 10 6 11.28 2.85 14 -10 -6 8.86 3.39 -14 10 5 0.62 1.66 14 -10 -5 1.63 2.65 14 -10 -4 0.13 3.19 -14 10 3 0.11 2.04 -14 10 2 1.06 2.17 -14 10 1 10.80 3.33 -14 10 0 7.93 2.75 -14 10 -1 4.98 2.19 -14 10 -2 6.42 2.43 -14 10 -3 1.46 1.75 14 -11 -8 4.06 2.52 14 -11 -7 17.80 3.72 14 -11 -6 3.81 2.66 14 -11 -5 2.04 2.50 14 -11 -4 0.71 2.12 14 -11 -3 -0.48 2.24 14 -11 -2 3.14 1.93 14 -11 -1 3.37 2.01 15 0 -16 1.61 1.75 15 0 -15 -4.57 2.50 15 0 -14 -0.69 1.75 15 0 -13 4.09 1.98 15 0 -12 -2.21 2.19 15 0 -11 16.03 3.34 15 0 -10 1.36 2.23 15 0 -9 6.31 2.67 15 0 -8 21.39 4.16 15 0 -7 97.94 7.27 15 0 -6 15.81 3.47 -15 0 2 12.40 5.39 -15 0 1 32.12 6.08 -15 0 0 3.23 3.09 -15 0 -1 5.44 3.30 -15 0 -2 -1.15 2.34 -15 0 -3 12.09 3.67 -15 0 -4 5.54 2.81 -15 0 -5 17.52 3.81 -15 0 -6 -0.61 1.81 15 -1 -17 53.88 5.07 15 -1 -16 -1.32 2.22 15 -1 -15 48.26 5.39 15 1 -14 1.73 1.65 15 -1 -14 -0.71 2.35 15 1 -13 6.08 2.23 15 -1 -13 16.08 3.71 15 1 -12 6.41 2.31 15 -1 -12 7.12 2.42 15 1 -11 -2.23 2.13 15 -1 -11 0.84 2.40 15 1 -10 -1.28 1.74 15 -1 -10 -0.67 2.56 15 -1 -9 0.21 2.59 15 -1 -8 1.35 2.51 15 -1 -7 5.93 2.88 15 -1 -6 8.31 3.35 15 -1 -5 -4.14 2.37 15 -1 -4 -3.71 3.13 15 -1 -3 -5.10 2.60 -15 1 2 2.04 2.68 -15 -1 1 -1.76 2.65 -15 1 1 4.53 3.02 -15 -1 0 1.36 2.19 -15 1 0 1.41 2.24 -15 -1 -1 9.43 3.35 -15 1 -1 10.99 4.05 -15 -1 -2 4.79 2.76 -15 1 -2 1.16 2.33 -15 -1 -3 2.99 2.70 -15 1 -3 3.33 2.55 -15 -1 -4 1.03 1.92 -15 1 -4 1.76 1.92 -15 -1 -5 4.75 2.45 -15 1 -5 4.21 2.57 -15 -1 -6 2.19 1.96 -15 1 -6 0.91 1.65 -15 1 -7 4.21 1.77 15 -2 -17 -1.64 1.79 15 -2 -16 2.30 1.99 15 -2 -15 10.42 3.22 15 -2 -14 4.61 2.12 15 -2 -13 -0.11 2.56 15 -2 -12 2.84 2.40 15 -2 -11 3.66 2.81 15 -2 -10 1.20 2.65 15 -2 -9 15.11 4.25 15 -2 -8 61.16 6.95 15 -2 -7 24.34 5.02 15 -2 -6 43.52 6.02 15 -2 -5 8.66 3.39 15 -2 -4 15.08 3.63 15 -2 -3 21.41 3.99 15 -2 -2 15.88 3.25 -15 2 2 16.21 4.97 -15 2 1 8.13 2.73 15 -2 -1 0.87 1.61 -15 2 1 6.59 3.36 -15 2 0 5.82 2.29 -15 -2 0 9.50 3.58 -15 2 0 5.59 3.27 -15 2 -1 4.09 1.97 -15 -2 -1 5.52 3.15 -15 2 -1 4.10 2.43 -15 2 -2 3.11 1.65 -15 -2 -2 0.31 2.05 -15 2 -2 0.45 2.42 -15 -2 -3 -1.95 2.15 -15 2 -3 1.45 2.45 -15 -2 -4 3.95 2.32 -15 2 -4 2.65 1.86 -15 -2 -5 5.33 1.91 -15 2 -5 9.26 2.92 -15 2 -6 8.32 2.62 15 -3 -17 4.01 2.31 15 -3 -16 7.93 2.45 15 -3 -15 2.47 2.08 15 -3 -14 38.18 5.49 15 -3 -13 -0.56 2.42 15 -3 -12 29.69 4.90 15 -3 -11 -2.48 3.13 15 -3 -10 10.42 3.52 15 -3 -9 1.00 2.47 15 -3 -8 21.47 4.83 15 -3 -7 22.12 4.83 15 -3 -6 13.35 4.30 15 -3 -5 3.15 2.88 15 -3 -4 7.95 3.44 15 -3 -3 2.43 2.19 -15 3 2 -1.84 2.06 15 -3 -2 1.21 1.95 -15 3 2 -0.25 2.20 -15 3 1 -1.41 2.10 15 -3 -1 3.36 2.27 -15 3 1 5.58 3.31 -15 3 0 -0.85 2.03 15 -3 0 3.63 2.20 -15 3 0 1.96 2.71 -15 3 -1 6.11 2.61 -15 3 -1 9.18 3.32 -15 3 -2 1.13 1.66 -15 3 -2 1.55 1.95 -15 3 -3 4.51 1.84 -15 3 -3 7.34 3.29 -15 3 -4 2.99 2.42 -15 3 -5 10.58 3.16 -15 3 -6 50.26 5.21 15 -4 -16 3.16 2.33 15 -4 -15 -1.05 2.07 15 -4 -14 7.73 3.03 15 -4 -13 4.16 2.30 15 -4 -12 -3.46 3.14 15 -4 -11 19.00 4.43 15 -4 -10 6.36 3.33 15 -4 -9 6.41 2.53 15 -4 -8 24.55 5.23 15 -4 -7 17.15 4.88 15 -4 -6 21.83 4.55 15 -4 -5 1.64 2.95 15 -4 -4 16.63 4.05 -15 4 3 30.83 5.38 15 -4 -3 23.90 4.54 -15 4 2 49.88 6.10 15 -4 -2 44.05 5.78 -15 4 1 16.10 3.97 15 -4 -1 12.30 3.48 -15 4 1 7.03 3.55 -15 4 0 23.95 4.26 15 -4 0 19.64 3.45 -15 4 0 24.54 4.90 -15 4 -1 9.93 2.97 15 -4 1 11.50 2.77 -15 4 -1 5.99 3.08 -15 4 -2 3.26 2.08 -15 4 -2 4.44 2.63 -15 4 -3 5.65 2.07 -15 4 -3 5.01 2.66 -15 4 -4 2.84 2.08 -15 4 -5 -0.23 1.58 15 -5 -15 32.35 4.39 15 -5 -14 21.55 3.96 15 -5 -13 0.27 2.20 15 -5 -12 16.77 3.84 15 -5 -11 13.78 3.92 15 -5 -10 3.96 3.20 15 -5 -9 19.26 4.38 15 -5 -8 19.57 4.51 15 -5 -7 17.21 4.27 15 -5 -6 10.68 3.92 15 -5 -5 26.02 5.41 15 -5 -4 18.52 4.32 -15 5 3 11.20 3.51 15 -5 -3 7.95 3.29 -15 5 2 3.90 2.47 15 -5 -2 3.92 2.70 -15 5 1 -1.63 2.13 15 -5 -1 5.05 3.29 -15 5 0 6.07 2.65 15 -5 0 5.03 2.85 -15 5 -1 -0.13 1.63 15 -5 1 1.66 1.91 -15 5 -2 8.46 2.74 -15 5 -2 5.06 2.32 -15 5 -3 21.33 3.34 -15 5 -3 17.90 3.22 15 -6 -14 -1.64 2.04 15 -6 -13 4.57 2.27 15 -6 -12 0.09 2.28 15 -6 -11 3.17 2.46 15 -6 -10 21.70 4.53 15 -6 -9 5.04 2.39 15 -6 -8 14.92 4.20 15 -6 -7 65.40 7.10 15 -6 -6 18.60 4.65 15 -6 -5 30.43 5.10 15 -6 -4 22.91 4.63 15 -6 -3 55.96 6.55 -15 6 2 72.50 7.43 15 -6 -2 61.04 6.48 -15 6 1 60.41 6.55 15 -6 -1 47.76 5.61 -15 6 0 28.25 4.22 15 -6 0 25.64 4.11 -15 6 -1 4.67 2.16 -15 6 -2 3.78 2.11 15 -7 -12 -1.71 1.98 15 -7 -11 30.92 4.36 15 -7 -10 7.99 2.85 15 -7 -9 38.93 4.87 15 -7 -8 19.98 4.00 15 -7 -7 12.14 3.70 15 -7 -6 7.22 3.03 15 -7 -5 8.51 3.10 15 -7 -4 15.01 3.74 15 -7 -3 2.92 2.12 15 -7 -2 5.33 2.44 -15 7 1 0.37 1.61 15 -7 -1 5.97 2.38 -15 7 0 -0.75 1.52 -15 7 -1 0.99 1.42 15 -8 -8 26.62 3.91 15 -8 -7 3.89 2.03 15 -8 -6 8.71 2.78 15 -8 -5 11.32 3.08 15 -8 -4 1.35 1.81 0 0 0 0.00 0.00 TITL 025cmcm19 in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 1.54184 12.657216 19.380925 30.269468 90.0000 98.7873 90.0000 ZERR 7.00 0.000400 0.000620 0.001195 0.0000 0.0037 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N O Al P Cu UNIT 350.00 280.00 14.00 14.00 7.00 7.00 7.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 71651 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.237 _oxdiff_exptl_absorpt_empirical_full_min 0.754 _publcif_funding_html ; ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.54160(5) 0.32831(3) 0.16025(2) 0.04202(17) Uani 1 1 d . . . . . Al1 Al 0.48537(8) 0.31206(5) 0.29674(4) 0.0294(2) Uani 1 1 d . . . . . P1 P 0.57420(10) 0.33872(8) 0.09068(4) 0.0554(3) Uani 1 1 d . . . . . O1 O 0.35646(18) 0.27734(12) 0.32142(8) 0.0271(5) Uani 1 1 d . . . . . N1 N 0.5449(2) 0.22960(15) 0.32685(11) 0.0304(6) Uani 1 1 d . . . . . N2 N 0.4437(2) 0.39551(15) 0.32441(11) 0.0301(6) Uani 1 1 d . . . . . N4 N 0.5846(2) 0.33690(16) 0.25794(11) 0.0346(7) Uani 1 1 d . . . . . N3 N 0.4243(2) 0.29874(16) 0.23525(11) 0.0316(6) Uani 1 1 d . . . . . C1 C 0.3712(3) 0.21527(17) 0.34459(12) 0.0266(7) Uani 1 1 d . . . . . C15 C 0.3040(3) 0.32672(18) 0.34362(11) 0.0263(7) Uani 1 1 d . . . . . C16 C 0.3511(3) 0.39189(19) 0.34369(12) 0.0297(7) Uani 1 1 d . . . . . C6 C 0.2913(3) 0.18844(18) 0.36509(12) 0.0283(7) Uani 1 1 d . . . . . C2 C 0.4738(3) 0.18853(18) 0.34568(13) 0.0293(7) Uani 1 1 d . . . . . C14 C 0.2204(3) 0.30771(19) 0.36467(12) 0.0293(7) Uani 1 1 d . . . . . C17 C 0.2980(3) 0.44401(19) 0.36393(13) 0.0340(8) Uani 1 1 d . . . . . H17 H 0.321901 0.489326 0.363301 0.041 Uiso 1 1 calc R . . . . C24 C 0.4916(3) 0.4629(2) 0.32399(14) 0.0350(8) Uani 1 1 d . . . . . C11 C 0.1888(3) 0.2309(2) 0.36368(13) 0.0316(8) Uani 1 1 d . . . . . C48 C 0.5140(3) 0.32064(19) 0.22177(13) 0.0336(8) Uani 1 1 d . . . . . C3 C 0.4913(3) 0.1243(2) 0.36725(14) 0.0360(8) Uani 1 1 d . . . . . H3 H 0.557346 0.102842 0.368494 0.043 Uiso 1 1 calc R . . . . C5 C 0.3127(3) 0.1244(2) 0.38633(13) 0.0347(8) Uani 1 1 d . . . . . H5 H 0.260486 0.103221 0.400184 0.042 Uiso 1 1 calc R . . . . C18 C 0.2103(3) 0.4290(2) 0.38490(13) 0.0364(9) Uani 1 1 d . . . . . C25 C 0.4684(3) 0.50431(19) 0.28541(14) 0.0357(8) Uani 1 1 d . . . . . C55 C 0.3306(3) 0.2804(2) 0.20389(13) 0.0351(8) Uani 1 1 d . . . . . H55 H 0.347202 0.288290 0.173715 0.042 Uiso 1 1 calc R . . . . C29 C 0.5614(3) 0.4873(2) 0.36107(16) 0.0434(10) Uani 1 1 d . . . . . C19 C 0.1722(3) 0.3611(2) 0.38597(13) 0.0345(8) Uani 1 1 d . . . . . H19 H 0.114881 0.351401 0.400831 0.041 Uiso 1 1 calc R . . . . C4 C 0.4110(3) 0.0923(2) 0.38685(14) 0.0365(8) Uani 1 1 d . . . . . C56 C 0.2986(3) 0.2042(2) 0.20701(15) 0.0411(9) Uani 1 1 d . . . . . H56A H 0.357306 0.175329 0.200944 0.049 Uiso 1 1 calc R . . . . H56B H 0.286092 0.194504 0.237212 0.049 Uiso 1 1 calc R . . . . C49 C 0.6898(3) 0.3643(2) 0.25491(15) 0.0395(9) Uani 1 1 d . . . . . H49 H 0.681973 0.399460 0.231397 0.047 Uiso 1 1 calc R . . . . C36 C 0.6457(3) 0.19629(19) 0.32402(15) 0.0365(9) Uani 1 1 d . . . . . C30 C 0.3886(3) 0.4818(2) 0.24540(15) 0.0394(9) Uani 1 1 d . . . . . H30 H 0.376273 0.432283 0.248734 0.047 Uiso 1 1 calc R . . . . C12 C 0.1153(3) 0.2155(2) 0.31936(15) 0.0393(9) Uani 1 1 d . . . . . H12A H 0.151511 0.227196 0.294745 0.059 Uiso 1 1 calc GR . . . . H12B H 0.051050 0.242330 0.317736 0.059 Uiso 1 1 calc GR . . . . H12C H 0.097448 0.167309 0.317991 0.059 Uiso 1 1 calc GR . . . . C13 C 0.1307(3) 0.2123(2) 0.40282(15) 0.0436(10) Uani 1 1 d . . . . . H13A H 0.108389 0.164940 0.400273 0.065 Uiso 1 1 calc GR . . . . H13B H 0.069112 0.241427 0.402293 0.065 Uiso 1 1 calc GR . . . . H13C H 0.177987 0.218883 0.430452 0.065 Uiso 1 1 calc GR . . . . C60 C 0.2352(3) 0.3262(2) 0.20966(15) 0.0400(9) Uani 1 1 d . . . . . H60A H 0.253388 0.373942 0.204793 0.048 Uiso 1 1 calc R . . . . H60B H 0.220960 0.322122 0.240148 0.048 Uiso 1 1 calc R . . . . C58 C 0.1058(3) 0.2319(2) 0.18102(15) 0.0448(10) Uani 1 1 d . . . . . H58A H 0.045029 0.220879 0.158539 0.054 Uiso 1 1 calc R . . . . H58B H 0.085734 0.223008 0.210165 0.054 Uiso 1 1 calc R . . . . C59 C 0.1337(3) 0.3075(2) 0.17751(16) 0.0449(10) Uani 1 1 d . . . . . H59A H 0.074657 0.335431 0.184291 0.054 Uiso 1 1 calc R . . . . H59B H 0.144183 0.317651 0.147111 0.054 Uiso 1 1 calc R . . . . C37 C 0.6526(3) 0.1486(2) 0.28992(17) 0.0441(10) Uani 1 1 d . . . . . C41 C 0.7349(3) 0.2096(2) 0.35674(17) 0.0438(10) Uani 1 1 d . . . . . C31 C 0.2810(4) 0.5184(3) 0.24538(17) 0.0507(11) Uani 1 1 d . . . . . H31A H 0.256063 0.510047 0.273301 0.076 Uiso 1 1 calc GR . . . . H31B H 0.229797 0.500831 0.221327 0.076 Uiso 1 1 calc GR . . . . H31C H 0.289910 0.567066 0.241496 0.076 Uiso 1 1 calc GR . . . . C33 C 0.5896(4) 0.4453(3) 0.40403(18) 0.0565(12) Uani 1 1 d . . . . . H33 H 0.571701 0.397011 0.396818 0.068 Uiso 1 1 calc R . . . . C42 C 0.5597(4) 0.1350(2) 0.25315(17) 0.0487(11) Uani 1 1 d . . . . . H42 H 0.506945 0.171630 0.254670 0.058 Uiso 1 1 calc R . . . . C26 C 0.5179(4) 0.5689(2) 0.28442(17) 0.0446(10) Uani 1 1 d . . . . . H26 H 0.503761 0.596079 0.258897 0.054 Uiso 1 1 calc R . . . . C20 C 0.1565(4) 0.4879(2) 0.40788(16) 0.0482(10) Uani 1 1 d . U . . . C57 C 0.1993(4) 0.1861(2) 0.17456(16) 0.0480(10) Uani 1 1 d . . . . . H57A H 0.180538 0.138257 0.178869 0.058 Uiso 1 1 calc R . . . . H57B H 0.213986 0.191024 0.144198 0.058 Uiso 1 1 calc R . . . . C45 C 0.7314(3) 0.2614(3) 0.39432(17) 0.0492(11) Uani 1 1 d . . . . . H45 H 0.685454 0.299582 0.381831 0.059 Uiso 1 1 calc R . . . . C28 C 0.6074(3) 0.5523(2) 0.35853(18) 0.0505(11) Uani 1 1 d . . . . . H28 H 0.653191 0.569132 0.383131 0.061 Uiso 1 1 calc R . . . . C27 C 0.5867(4) 0.5923(2) 0.32054(19) 0.0522(12) Uani 1 1 d . . . . . H27 H 0.619453 0.635116 0.319475 0.063 Uiso 1 1 calc R . . . . C38 C 0.7478(4) 0.1135(3) 0.2892(2) 0.0581(13) Uani 1 1 d . . . . . H38 H 0.752944 0.081965 0.266424 0.070 Uiso 1 1 calc R . . . . C32 C 0.4288(4) 0.4919(2) 0.20074(16) 0.0505(11) Uani 1 1 d . . . . . H32A H 0.428456 0.540198 0.193622 0.076 Uiso 1 1 calc GR . . . . H32B H 0.382808 0.467653 0.177708 0.076 Uiso 1 1 calc GR . . . . H32C H 0.500213 0.474275 0.202826 0.076 Uiso 1 1 calc GR . . . . C7 C 0.4360(4) 0.0213(2) 0.40927(17) 0.0507(11) Uani 1 1 d . . . . . C54 C 0.7371(3) 0.3988(3) 0.29869(18) 0.0520(12) Uani 1 1 d . . . . . H54A H 0.740613 0.365482 0.322790 0.062 Uiso 1 1 calc R . . . . H54B H 0.690488 0.436073 0.305000 0.062 Uiso 1 1 calc R . . . . C47 C 0.8405(4) 0.2925(3) 0.41262(19) 0.0554(12) Uani 1 1 d . . . . . H47A H 0.887663 0.256635 0.425603 0.083 Uiso 1 1 calc GR . . . . H47B H 0.832201 0.326290 0.435019 0.083 Uiso 1 1 calc GR . . . . H47C H 0.870198 0.314039 0.388721 0.083 Uiso 1 1 calc GR . . . . C52 C 0.9237(4) 0.3727(3) 0.2843(2) 0.0655(15) Uani 1 1 d . . . . . H52A H 0.991856 0.393601 0.281270 0.079 Uiso 1 1 calc R . . . . H52B H 0.936244 0.338496 0.307937 0.079 Uiso 1 1 calc R . . . . C40 C 0.8288(3) 0.1732(3) 0.3545(2) 0.0592(14) Uani 1 1 d . . . . . H40 H 0.888804 0.181860 0.375587 0.071 Uiso 1 1 calc R . . . . C50 C 0.7672(4) 0.3091(3) 0.2428(2) 0.0572(13) Uani 1 1 d . . . . . H50A H 0.772026 0.272099 0.264565 0.069 Uiso 1 1 calc R . . . . H50B H 0.739206 0.289748 0.213763 0.069 Uiso 1 1 calc R . . . . C39 C 0.8348(4) 0.1248(3) 0.3217(2) 0.0725(18) Uani 1 1 d . . . . . H39 H 0.897358 0.099683 0.321529 0.087 Uiso 1 1 calc R . . . . C44 C 0.5048(4) 0.0665(3) 0.25941(19) 0.0590(13) Uani 1 1 d . . . . . H44A H 0.556846 0.030066 0.262539 0.089 Uiso 1 1 calc GR . . . . H44B H 0.451627 0.057533 0.233855 0.089 Uiso 1 1 calc GR . . . . H44C H 0.471268 0.068582 0.285768 0.089 Uiso 1 1 calc GR . . . . C51 C 0.8788(4) 0.3379(3) 0.2413(2) 0.0674(15) Uani 1 1 d . . . . . H51A H 0.925922 0.300648 0.235520 0.081 Uiso 1 1 calc R . . . . H51B H 0.875499 0.370813 0.217004 0.081 Uiso 1 1 calc R . . . . C43 C 0.5931(5) 0.1385(3) 0.2072(2) 0.0647(14) Uani 1 1 d . . . . . H43A H 0.625397 0.182500 0.203432 0.097 Uiso 1 1 calc GR . . . . H43B H 0.531405 0.132771 0.184787 0.097 Uiso 1 1 calc GR . . . . H43C H 0.643651 0.102476 0.204384 0.097 Uiso 1 1 calc GR . . . . C202 C 0.5074(5) 0.2115(4) 0.5167(2) 0.0763(17) Uani 1 1 d . . . . . H202 H 0.535453 0.167049 0.517597 0.092 Uiso 1 1 calc R . . . . C35 C 0.7085(5) 0.4486(4) 0.4225(2) 0.0758(17) Uani 1 1 d . . . . . H35A H 0.749295 0.438066 0.399050 0.114 Uiso 1 1 calc GR . . . . H35B H 0.724814 0.415669 0.446212 0.114 Uiso 1 1 calc GR . . . . H35C H 0.726347 0.494116 0.433700 0.114 Uiso 1 1 calc GR . . . . C53 C 0.8492(4) 0.4276(3) 0.2972(2) 0.0691(17) Uani 1 1 d . . . . . H53A H 0.844516 0.465002 0.275684 0.083 Uiso 1 1 calc R . . . . H53B H 0.878135 0.446106 0.326282 0.083 Uiso 1 1 calc R . . . . C8 C 0.5369(4) 0.0269(3) 0.4437(2) 0.0670(16) Uani 1 1 d . . . . . H8A H 0.594609 0.043741 0.429484 0.101 Uiso 1 1 calc GR . . . . H8B H 0.555020 -0.017770 0.456340 0.101 Uiso 1 1 calc GR . . . . H8C H 0.524548 0.058205 0.466940 0.101 Uiso 1 1 calc GR . . . . C64 C 0.3572(8) 0.3646(5) 0.0706(5) 0.058(3) Uani 0.609(5) 1 d D . P A 1 H64A H 0.358837 0.350343 0.101049 0.087 Uiso 0.609(5) 1 calc GR . P A 1 H64B H 0.289889 0.351877 0.053407 0.087 Uiso 0.609(5) 1 calc GR . P A 1 H64C H 0.365916 0.413751 0.069478 0.087 Uiso 0.609(5) 1 calc GR . P A 1 C201 C 0.4408(5) 0.2338(4) 0.4787(2) 0.0784(19) Uani 1 1 d . . . . . H201 H 0.423935 0.204886 0.454125 0.094 Uiso 1 1 calc R . . . . C62 C 0.4490(15) 0.3561(5) 0.0033(3) 0.068(4) Uani 0.609(5) 1 d D . P A 1 H62A H 0.472038 0.403327 0.004525 0.102 Uiso 0.609(5) 1 calc GR . P A 1 H62B H 0.378073 0.353053 -0.013237 0.102 Uiso 0.609(5) 1 calc GR . P A 1 H62C H 0.496876 0.328832 -0.011262 0.102 Uiso 0.609(5) 1 calc GR . P A 1 C46 C 0.6811(4) 0.2310(4) 0.4323(2) 0.0711(16) Uani 1 1 d . . . . . H46A H 0.607107 0.221154 0.421970 0.107 Uiso 1 1 calc GR . . . . H46B H 0.686726 0.263457 0.456486 0.107 Uiso 1 1 calc GR . . . . H46C H 0.717588 0.189181 0.442398 0.107 Uiso 1 1 calc GR . . . . C203 C 0.5318(6) 0.2535(4) 0.5523(2) 0.084(2) Uani 1 1 d . . . . . H203 H 0.577676 0.238209 0.577332 0.100 Uiso 1 1 calc R . . . . C34 C 0.5270(5) 0.4673(4) 0.44026(19) 0.0784(18) Uani 1 1 d . . . . . H34A H 0.534456 0.516154 0.444880 0.118 Uiso 1 1 calc GR . . . . H34B H 0.553820 0.443558 0.467511 0.118 Uiso 1 1 calc GR . . . . H34C H 0.452880 0.456109 0.431436 0.118 Uiso 1 1 calc GR . . . . C200 C 0.4011(5) 0.2985(4) 0.4782(2) 0.086(2) Uani 1 1 d . . . . . H200 H 0.358096 0.314747 0.452647 0.103 Uiso 1 1 calc R . . . . C204 C 0.4890(6) 0.3189(4) 0.5518(2) 0.086(2) Uani 1 1 d . . . . . H204 H 0.504813 0.347905 0.576385 0.104 Uiso 1 1 calc R . . . . C10 C 0.3469(5) -0.0044(4) 0.4318(3) 0.124(4) Uani 1 1 d . . . . . H10A H 0.333510 0.028016 0.454245 0.186 Uiso 1 1 calc GR . . . . H10B H 0.366163 -0.048211 0.445465 0.186 Uiso 1 1 calc GR . . . . H10C H 0.283635 -0.009553 0.410086 0.186 Uiso 1 1 calc GR . . . . C61 C 0.4489(6) 0.3289(4) 0.0510(2) 0.0499(19) Uani 0.609(5) 1 d D . P A 1 C67 C 0.6605(9) 0.2118(6) 0.0995(4) 0.090(4) Uani 0.609(5) 1 d D U P A 1 H67A H 0.665773 0.214770 0.131461 0.135 Uiso 0.609(5) 1 calc GR . P A 1 H67B H 0.711017 0.178534 0.091990 0.135 Uiso 0.609(5) 1 calc GR . P A 1 H67C H 0.589502 0.197875 0.086942 0.135 Uiso 0.609(5) 1 calc GR . P A 1 C205 C 0.4230(6) 0.3401(4) 0.5145(3) 0.094(2) Uani 1 1 d . . . . . H205 H 0.392512 0.383814 0.513829 0.112 Uiso 1 1 calc R . . . . C22 C 0.1067(6) 0.5372(4) 0.3713(2) 0.0533(17) Uani 0.708(7) 1 d . U P B 1 H22A H 0.162121 0.558395 0.357656 0.080 Uiso 0.708(7) 1 calc GR . P B 1 H22B H 0.067055 0.572147 0.384162 0.080 Uiso 0.708(7) 1 calc GR . P B 1 H22C H 0.059536 0.512027 0.349173 0.080 Uiso 0.708(7) 1 calc GR . P B 1 C9 C 0.4630(6) -0.0298(3) 0.3735(2) 0.091(2) Uani 1 1 d . . . . . H9A H 0.399580 -0.039418 0.352692 0.136 Uiso 1 1 calc GR . . . . H9B H 0.490095 -0.071820 0.387675 0.136 Uiso 1 1 calc GR . . . . H9C H 0.516066 -0.009783 0.357881 0.136 Uiso 1 1 calc GR . . . . C68 C 0.7928(7) 0.3072(6) 0.1069(3) 0.090(4) Uani 0.609(5) 1 d D U P A 1 H68A H 0.810227 0.351874 0.096326 0.134 Uiso 0.609(5) 1 calc GR . P A 1 H68B H 0.847862 0.274946 0.102511 0.134 Uiso 0.609(5) 1 calc GR . P A 1 H68C H 0.787465 0.309897 0.138131 0.134 Uiso 0.609(5) 1 calc GR . P A 1 C71 C 0.6951(10) 0.4601(6) 0.1271(4) 0.076(3) Uani 0.609(5) 1 d . U P A 1 H71A H 0.655724 0.460104 0.151800 0.114 Uiso 0.609(5) 1 calc GR . P A 1 H71B H 0.722922 0.505441 0.123405 0.114 Uiso 0.609(5) 1 calc GR . P A 1 H71C H 0.753147 0.427821 0.132840 0.114 Uiso 0.609(5) 1 calc GR . P A 1 C21 C 0.0648(7) 0.4622(4) 0.4318(3) 0.066(2) Uani 0.708(7) 1 d . U P B 1 H21A H 0.010836 0.440731 0.410459 0.100 Uiso 0.708(7) 1 calc GR . P B 1 H21B H 0.034220 0.500607 0.445406 0.100 Uiso 0.708(7) 1 calc GR . P B 1 H21C H 0.092108 0.429343 0.454395 0.100 Uiso 0.708(7) 1 calc GR . P B 1 C23 C 0.2374(7) 0.5248(5) 0.4411(3) 0.073(2) Uani 0.708(7) 1 d . U P B 1 H23A H 0.267591 0.493195 0.463977 0.110 Uiso 0.708(7) 1 calc GR . P B 1 H23B H 0.203272 0.562077 0.454330 0.110 Uiso 0.708(7) 1 calc GR . P B 1 H23C H 0.293158 0.542890 0.426136 0.110 Uiso 0.708(7) 1 calc GR . P B 1 C70 C 0.6739(8) 0.4527(6) 0.0437(3) 0.071(3) Uani 0.609(5) 1 d . U P A 1 H70A H 0.739045 0.426648 0.045857 0.107 Uiso 0.609(5) 1 calc GR . P A 1 H70B H 0.689594 0.500964 0.041937 0.107 Uiso 0.609(5) 1 calc GR . P A 1 H70C H 0.626369 0.438905 0.017385 0.107 Uiso 0.609(5) 1 calc GR . P A 1 C69 C 0.6214(8) 0.4392(5) 0.0847(3) 0.064(2) Uani 0.609(5) 1 d . U P A 1 C72 C 0.5277(9) 0.4876(5) 0.0839(3) 0.068(2) Uani 0.609(5) 1 d . U P A 1 H72A H 0.484624 0.486322 0.054883 0.102 Uiso 0.609(5) 1 calc GR . P A 1 H72B H 0.553438 0.533738 0.090132 0.102 Uiso 0.609(5) 1 calc GR . P A 1 H72C H 0.485467 0.473624 0.106084 0.102 Uiso 0.609(5) 1 calc GR . P A 1 C66 C 0.6951(8) 0.2748(6) 0.0311(2) 0.090(3) Uani 0.609(5) 1 d D U P A 1 H66A H 0.633001 0.251721 0.015876 0.135 Uiso 0.609(5) 1 calc GR . P A 1 H66B H 0.757727 0.248193 0.028379 0.135 Uiso 0.609(5) 1 calc GR . P A 1 H66C H 0.701026 0.319576 0.018098 0.135 Uiso 0.609(5) 1 calc GR . P A 1 C65 C 0.6850(6) 0.2829(5) 0.0806(3) 0.082(3) Uani 0.609(5) 1 d D U P A 1 C63 C 0.4248(9) 0.2512(3) 0.0486(3) 0.076(3) Uani 0.609(5) 1 d D . P A 1 H63A H 0.477884 0.227949 0.034542 0.114 Uiso 0.609(5) 1 calc GR . P A 1 H63B H 0.355465 0.243605 0.031471 0.114 Uiso 0.609(5) 1 calc GR . P A 1 H63C H 0.426090 0.233404 0.078265 0.114 Uiso 0.609(5) 1 calc GR . P A 1 C22A C 0.1990(15) 0.5622(9) 0.3980(6) 0.058(3) Uani 0.292(7) 1 d . U P B 2 H22D H 0.267817 0.569491 0.415606 0.087 Uiso 0.292(7) 1 calc GR . P B 2 H22E H 0.149838 0.596475 0.405461 0.087 Uiso 0.292(7) 1 calc GR . P B 2 H22F H 0.205067 0.565885 0.366826 0.087 Uiso 0.292(7) 1 calc GR . P B 2 C23A C 0.1775(15) 0.4749(10) 0.4584(6) 0.059(3) Uani 0.292(7) 1 d . U P B 2 H23D H 0.151971 0.429780 0.464611 0.088 Uiso 0.292(7) 1 calc GR . P B 2 H23E H 0.140733 0.508989 0.473303 0.088 Uiso 0.292(7) 1 calc GR . P B 2 H23F H 0.252845 0.477664 0.468908 0.088 Uiso 0.292(7) 1 calc GR . P B 2 C21A C 0.0363(14) 0.4910(9) 0.3911(6) 0.059(3) Uani 0.292(7) 1 d . U P B 2 H21D H 0.024253 0.491899 0.358965 0.088 Uiso 0.292(7) 1 calc GR . P B 2 H21E H 0.006964 0.531936 0.402292 0.088 Uiso 0.292(7) 1 calc GR . P B 2 H21F H 0.002210 0.451113 0.401344 0.088 Uiso 0.292(7) 1 calc GR . P B 2 C63A C 0.450(3) 0.3722(11) 0.0040(5) 0.072(3) Uani 0.391(5) 1 d D U P A 2 H63D H 0.520019 0.378668 -0.003809 0.108 Uiso 0.391(5) 1 calc GR . P A 2 H63E H 0.402283 0.406380 -0.010819 0.108 Uiso 0.391(5) 1 calc GR . P A 2 H63F H 0.424261 0.327034 -0.005085 0.108 Uiso 0.391(5) 1 calc GR . P A 2 C61A C 0.4554(11) 0.3796(6) 0.0547(4) 0.070(2) Uani 0.391(5) 1 d D U P A 2 C64A C 0.4628(14) 0.4569(6) 0.0667(5) 0.076(3) Uani 0.391(5) 1 d D U P A 2 H64D H 0.470497 0.462147 0.098617 0.114 Uiso 0.391(5) 1 calc GR . P A 2 H64E H 0.398848 0.479879 0.053093 0.114 Uiso 0.391(5) 1 calc GR . P A 2 H64F H 0.523487 0.476781 0.056013 0.114 Uiso 0.391(5) 1 calc GR . P A 2 C62A C 0.3523(19) 0.3505(10) 0.0685(10) 0.071(3) Uani 0.391(5) 1 d D U P A 2 H62D H 0.346479 0.302280 0.061194 0.106 Uiso 0.391(5) 1 calc GR . P A 2 H62E H 0.291796 0.374665 0.052841 0.106 Uiso 0.391(5) 1 calc GR . P A 2 H62F H 0.354359 0.356250 0.100136 0.106 Uiso 0.391(5) 1 calc GR . P A 2 C69A C 0.7052(10) 0.3744(6) 0.0860(4) 0.071(2) Uani 0.391(5) 1 d D U P A 2 C72A C 0.7135(17) 0.4334(8) 0.1203(5) 0.075(3) Uani 0.391(5) 1 d D U P A 2 H72D H 0.667361 0.470507 0.108571 0.113 Uiso 0.391(5) 1 calc GR . P A 2 H72E H 0.785949 0.449539 0.126170 0.113 Uiso 0.391(5) 1 calc GR . P A 2 H72F H 0.692320 0.416855 0.147526 0.113 Uiso 0.391(5) 1 calc GR . P A 2 C70A C 0.7147(13) 0.4047(7) 0.0399(4) 0.074(2) Uani 0.391(5) 1 d D U P A 2 H70D H 0.758795 0.375250 0.024878 0.110 Uiso 0.391(5) 1 calc GR . P A 2 H70E H 0.746247 0.449796 0.043499 0.110 Uiso 0.391(5) 1 calc GR . P A 2 H70F H 0.644856 0.408098 0.022396 0.110 Uiso 0.391(5) 1 calc GR . P A 2 C71A C 0.7995(15) 0.3250(8) 0.0999(6) 0.076(3) Uani 0.391(5) 1 d D U P A 2 H71D H 0.805588 0.315451 0.131298 0.113 Uiso 0.391(5) 1 calc GR . P A 2 H71E H 0.864334 0.346123 0.093731 0.113 Uiso 0.391(5) 1 calc GR . P A 2 H71F H 0.787526 0.282779 0.083358 0.113 Uiso 0.391(5) 1 calc GR . P A 2 C66A C 0.6213(11) 0.2363(8) 0.0190(4) 0.070(2) Uani 0.391(5) 1 d D U P A 2 H66D H 0.586695 0.270405 -0.001310 0.104 Uiso 0.391(5) 1 calc GR . P A 2 H66E H 0.609825 0.191391 0.005771 0.104 Uiso 0.391(5) 1 calc GR . P A 2 H66F H 0.696576 0.245734 0.024966 0.104 Uiso 0.391(5) 1 calc GR . P A 2 C65A C 0.5745(9) 0.2387(6) 0.0628(4) 0.068(2) Uani 0.391(5) 1 d D U P A 2 C68A C 0.6440(13) 0.1947(12) 0.0981(6) 0.076(3) Uani 0.391(5) 1 d D U P A 2 H68D H 0.717352 0.208540 0.100079 0.114 Uiso 0.391(5) 1 calc GR . P A 2 H68E H 0.637162 0.146923 0.089694 0.114 Uiso 0.391(5) 1 calc GR . P A 2 H68F H 0.620778 0.201000 0.126563 0.114 Uiso 0.391(5) 1 calc GR . P A 2 C67A C 0.4617(9) 0.2075(8) 0.0545(5) 0.069(3) Uani 0.391(5) 1 d D U P A 2 H67D H 0.428991 0.212554 0.080970 0.103 Uiso 0.391(5) 1 calc GR . P A 2 H67E H 0.466120 0.159451 0.047414 0.103 Uiso 0.391(5) 1 calc GR . P A 2 H67F H 0.419331 0.231076 0.030097 0.103 Uiso 0.391(5) 1 calc GR . P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.0398(3) 0.0490(4) 0.0416(3) 0.0041(3) 0.0198(3) -0.0012(3) Al1 0.0289(5) 0.0242(5) 0.0377(6) 0.0014(4) 0.0135(4) 0.0008(4) P1 0.0469(6) 0.0826(9) 0.0421(6) 0.0100(6) 0.0234(5) 0.0019(6) O1 0.0279(11) 0.0213(12) 0.0344(13) 0.0022(10) 0.0125(10) 0.0034(9) N1 0.0232(13) 0.0253(15) 0.0446(18) 0.0017(13) 0.0119(12) 0.0008(11) N2 0.0327(15) 0.0197(14) 0.0399(17) -0.0008(12) 0.0124(13) -0.0009(11) N4 0.0341(16) 0.0303(16) 0.0420(18) 0.0039(14) 0.0143(14) 0.0028(13) N3 0.0318(15) 0.0308(16) 0.0338(16) -0.0001(13) 0.0104(12) -0.0023(12) C1 0.0279(16) 0.0204(16) 0.0322(18) 0.0031(13) 0.0068(13) 0.0002(13) C15 0.0259(15) 0.0258(17) 0.0282(17) -0.0001(14) 0.0071(13) 0.0074(13) C16 0.0286(16) 0.0291(18) 0.0325(19) 0.0004(14) 0.0083(14) 0.0044(14) C6 0.0252(15) 0.0267(17) 0.0338(18) 0.0031(14) 0.0073(13) -0.0027(13) C2 0.0246(16) 0.0244(17) 0.041(2) 0.0021(15) 0.0103(14) 0.0006(13) C14 0.0236(15) 0.0352(19) 0.0306(18) -0.0022(15) 0.0085(13) 0.0032(14) C17 0.041(2) 0.0257(18) 0.037(2) -0.0030(15) 0.0090(16) 0.0034(15) C24 0.0315(18) 0.0280(19) 0.048(2) -0.0055(16) 0.0147(16) 0.0003(14) C11 0.0215(16) 0.037(2) 0.038(2) 0.0019(16) 0.0081(14) -0.0031(14) C48 0.0365(19) 0.0298(19) 0.039(2) 0.0067(16) 0.0194(16) 0.0024(15) C3 0.0224(16) 0.032(2) 0.053(2) 0.0060(17) 0.0039(15) 0.0033(14) C5 0.0278(17) 0.036(2) 0.041(2) 0.0103(17) 0.0073(15) -0.0061(15) C18 0.0358(19) 0.043(2) 0.0312(19) -0.0039(16) 0.0078(15) 0.0112(16) C25 0.0337(18) 0.0228(18) 0.053(2) -0.0005(16) 0.0145(17) 0.0012(14) C55 0.042(2) 0.031(2) 0.034(2) 0.0015(16) 0.0125(16) -0.0021(16) C29 0.038(2) 0.035(2) 0.058(3) -0.0076(19) 0.0099(19) 0.0014(17) C19 0.0282(17) 0.042(2) 0.035(2) -0.0012(16) 0.0119(15) 0.0072(15) C4 0.0352(19) 0.0288(19) 0.045(2) 0.0108(17) 0.0025(16) -0.0037(15) C56 0.047(2) 0.0257(19) 0.050(2) -0.0017(17) 0.0056(18) 0.0032(16) C49 0.035(2) 0.037(2) 0.050(2) 0.0065(18) 0.0166(17) 0.0016(16) C36 0.0254(17) 0.0281(19) 0.060(3) 0.0049(17) 0.0187(16) 0.0021(14) C30 0.044(2) 0.0242(18) 0.051(2) 0.0046(17) 0.0099(18) -0.0009(16) C12 0.0281(18) 0.038(2) 0.051(2) 0.0003(18) 0.0031(16) -0.0013(15) C13 0.0313(19) 0.050(3) 0.053(3) 0.002(2) 0.0195(18) -0.0026(17) C60 0.041(2) 0.030(2) 0.049(2) 0.0014(17) 0.0067(17) 0.0022(16) C58 0.045(2) 0.045(2) 0.043(2) 0.0009(19) 0.0001(18) -0.0100(19) C59 0.041(2) 0.038(2) 0.054(3) 0.0037(19) 0.0045(19) -0.0020(17) C37 0.035(2) 0.028(2) 0.073(3) 0.0006(19) 0.022(2) 0.0038(16) C41 0.0233(17) 0.040(2) 0.071(3) 0.008(2) 0.0143(18) 0.0015(15) C31 0.045(2) 0.048(3) 0.058(3) -0.006(2) 0.006(2) 0.007(2) C33 0.062(3) 0.041(3) 0.061(3) -0.009(2) -0.006(2) -0.001(2) C42 0.045(2) 0.037(2) 0.067(3) -0.014(2) 0.015(2) 0.0102(18) C26 0.047(2) 0.0251(19) 0.064(3) 0.0002(19) 0.016(2) -0.0026(17) C20 0.052(2) 0.048(2) 0.048(2) -0.0084(19) 0.0177(18) 0.0173(18) C57 0.058(3) 0.033(2) 0.051(3) -0.0013(19) 0.005(2) -0.0091(19) C45 0.0288(19) 0.053(3) 0.065(3) 0.003(2) 0.0046(19) 0.0040(18) C28 0.038(2) 0.038(2) 0.074(3) -0.015(2) 0.004(2) -0.0024(18) C27 0.042(2) 0.024(2) 0.093(4) -0.006(2) 0.016(2) -0.0068(17) C38 0.038(2) 0.044(3) 0.096(4) -0.012(3) 0.025(2) 0.0056(19) C32 0.059(3) 0.041(2) 0.053(3) 0.005(2) 0.014(2) 0.002(2) C7 0.051(2) 0.036(2) 0.061(3) 0.020(2) -0.005(2) -0.0064(19) C54 0.036(2) 0.045(3) 0.076(3) -0.007(2) 0.014(2) -0.0073(19) C47 0.040(2) 0.056(3) 0.068(3) 0.006(2) 0.003(2) -0.001(2) C52 0.032(2) 0.066(3) 0.100(5) 0.009(3) 0.013(2) -0.005(2) C40 0.027(2) 0.048(3) 0.103(4) 0.000(3) 0.011(2) 0.0051(19) C50 0.039(2) 0.059(3) 0.079(4) -0.010(3) 0.028(2) -0.002(2) C39 0.028(2) 0.053(3) 0.141(6) -0.012(3) 0.024(3) 0.016(2) C44 0.052(3) 0.058(3) 0.073(3) -0.018(3) 0.029(2) -0.012(2) C51 0.037(2) 0.081(4) 0.091(4) -0.002(3) 0.032(3) 0.001(2) C43 0.078(4) 0.048(3) 0.073(4) -0.008(3) 0.025(3) -0.008(3) C202 0.083(4) 0.078(4) 0.070(4) -0.008(3) 0.017(3) 0.012(3) C35 0.070(4) 0.087(4) 0.066(4) -0.011(3) -0.005(3) 0.022(3) C53 0.033(2) 0.054(3) 0.122(5) -0.006(3) 0.017(3) -0.011(2) C8 0.055(3) 0.058(3) 0.085(4) 0.035(3) 0.000(3) -0.003(2) C64 0.041(4) 0.068(7) 0.064(6) 0.010(6) 0.004(4) 0.015(4) C201 0.064(3) 0.116(6) 0.057(3) -0.031(4) 0.015(3) -0.017(4) C62 0.076(7) 0.081(10) 0.044(5) -0.003(5) -0.002(5) -0.012(7) C46 0.047(3) 0.103(5) 0.064(3) -0.004(3) 0.014(2) -0.020(3) C203 0.096(5) 0.105(5) 0.046(3) 0.006(3) 0.000(3) 0.014(4) C34 0.069(4) 0.113(5) 0.052(3) 0.002(3) 0.004(3) -0.002(4) C200 0.071(4) 0.116(6) 0.062(4) 0.004(4) -0.012(3) -0.007(4) C204 0.108(5) 0.084(5) 0.060(4) -0.015(3) -0.008(4) -0.015(4) C10 0.058(4) 0.101(5) 0.209(10) 0.116(6) 0.010(5) -0.004(3) C61 0.050(4) 0.057(5) 0.043(4) -0.005(4) 0.009(3) -0.006(4) C67 0.101(7) 0.104(9) 0.072(6) 0.009(6) 0.031(6) 0.062(6) C205 0.105(5) 0.079(5) 0.086(5) -0.002(4) -0.017(4) 0.003(4) C22 0.055(4) 0.045(4) 0.062(4) -0.003(3) 0.017(3) 0.018(3) C9 0.130(6) 0.031(3) 0.100(5) 0.011(3) -0.021(4) 0.001(3) C68 0.050(5) 0.152(10) 0.071(6) 0.018(7) 0.022(5) 0.024(6) C71 0.075(6) 0.077(6) 0.078(6) -0.004(5) 0.020(5) -0.028(5) C21 0.073(4) 0.061(4) 0.074(5) -0.003(4) 0.039(4) 0.024(4) C23 0.075(5) 0.075(5) 0.065(4) -0.036(4) -0.001(4) 0.028(4) C70 0.065(5) 0.093(6) 0.058(5) 0.015(5) 0.017(4) -0.025(5) C69 0.068(4) 0.079(5) 0.049(4) 0.006(4) 0.018(3) -0.030(4) C72 0.086(6) 0.062(5) 0.057(5) 0.007(4) 0.017(4) -0.010(5) C66 0.085(6) 0.126(8) 0.066(6) 0.006(6) 0.035(5) 0.037(6) C65 0.071(5) 0.121(7) 0.059(4) 0.012(5) 0.031(4) 0.039(5) C63 0.092(8) 0.060(6) 0.075(7) -0.014(5) 0.009(6) -0.015(5) C22A 0.067(6) 0.049(6) 0.061(6) -0.014(5) 0.021(5) 0.019(5) C23A 0.068(6) 0.056(6) 0.056(6) -0.015(5) 0.020(5) 0.019(5) C21A 0.065(6) 0.055(6) 0.060(6) -0.012(5) 0.020(5) 0.018(5) C63A 0.092(5) 0.060(4) 0.071(5) 0.004(4) 0.038(4) 0.000(4) C61A 0.091(4) 0.057(4) 0.072(4) 0.002(3) 0.040(4) -0.002(3) C64A 0.096(5) 0.061(5) 0.079(5) 0.004(4) 0.036(4) 0.000(4) C62A 0.090(6) 0.058(5) 0.072(6) 0.004(5) 0.036(5) 0.002(5) C69A 0.091(4) 0.060(4) 0.072(4) 0.002(3) 0.043(4) -0.007(3) C72A 0.093(6) 0.065(5) 0.078(5) 0.000(5) 0.042(5) -0.015(5) C70A 0.091(5) 0.064(4) 0.075(5) 0.002(4) 0.042(4) -0.011(4) C71A 0.090(5) 0.068(5) 0.077(5) 0.001(4) 0.038(5) -0.009(4) C66A 0.090(5) 0.059(4) 0.069(4) -0.002(4) 0.041(4) 0.000(4) C65A 0.088(4) 0.056(4) 0.070(4) 0.003(3) 0.042(4) -0.002(3) C68A 0.096(6) 0.064(5) 0.075(5) 0.004(5) 0.037(5) 0.006(5) C67A 0.088(5) 0.052(5) 0.073(5) 0.003(4) 0.037(4) -0.003(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.2130 0.2455 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu -1.9646 0.5888 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C48 Cu1 P1 179.04(13) . . ? O1 Al1 C48 129.32(13) . . ? N1 Al1 O1 80.13(11) . . ? N1 Al1 C48 113.93(14) . . ? N2 Al1 O1 80.12(12) . . ? N2 Al1 N1 126.87(15) . . ? N2 Al1 C48 116.77(14) . . ? N4 Al1 O1 163.92(14) . . ? N4 Al1 N1 104.63(14) . . ? N4 Al1 N2 107.73(14) . . ? N4 Al1 N3 69.07(14) . . ? N4 Al1 C48 34.65(14) . . ? N3 Al1 O1 94.92(12) . . ? N3 Al1 N1 114.57(14) . . ? N3 Al1 N2 115.89(14) . . ? N3 Al1 C48 34.42(13) . . ? C61 P1 Cu1 110.1(2) . . ? C61 P1 C69 105.8(4) . . ? C69 P1 Cu1 105.6(3) . . ? C65 P1 Cu1 111.2(2) . . ? C65 P1 C61 115.7(4) . . ? C65 P1 C69 107.7(4) . . ? C61A P1 Cu1 109.7(3) . . ? C61A P1 C65A 101.8(5) . . ? C69A P1 Cu1 114.4(4) . . ? C69A P1 C61A 116.7(5) . . ? C69A P1 C65A 105.0(5) . . ? C65A P1 Cu1 108.0(3) . . ? C1 O1 Al1 114.99(19) . . ? C1 O1 C15 112.8(3) . . ? C15 O1 Al1 115.0(2) . . ? C2 N1 Al1 115.9(2) . . ? C2 N1 C36 113.7(3) . . ? C36 N1 Al1 128.7(2) . . ? C16 N2 Al1 116.3(2) . . ? C16 N2 C24 115.6(3) . . ? C24 N2 Al1 127.8(2) . . ? C48 N4 Al1 91.3(2) . . ? C48 N4 C49 122.6(3) . . ? C49 N4 Al1 146.0(3) . . ? C48 N3 Al1 91.1(2) . . ? C48 N3 C55 121.9(3) . . ? C55 N3 Al1 146.9(3) . . ? O1 C1 C2 112.8(3) . . ? C6 C1 O1 120.4(3) . . ? C6 C1 C2 126.8(3) . . ? O1 C15 C16 112.8(3) . . ? C14 C15 O1 120.0(3) . . ? C14 C15 C16 127.1(3) . . ? N2 C16 C15 115.6(3) . . ? N2 C16 C17 129.6(3) . . ? C15 C16 C17 114.8(3) . . ? C1 C6 C11 117.7(3) . . ? C1 C6 C5 116.1(3) . . ? C5 C6 C11 126.2(3) . . ? N1 C2 C1 115.9(3) . . ? N1 C2 C3 129.2(3) . . ? C1 C2 C3 114.8(3) . . ? C15 C14 C11 118.0(3) . . ? C15 C14 C19 115.8(3) . . ? C19 C14 C11 126.2(3) . . ? C18 C17 C16 121.1(4) . . ? C25 C24 N2 119.3(4) . . ? C29 C24 N2 120.9(4) . . ? C29 C24 C25 119.8(4) . . ? C6 C11 C14 107.6(3) . . ? C6 C11 C12 108.4(3) . . ? C14 C11 C12 109.0(3) . . ? C13 C11 C6 110.9(3) . . ? C13 C11 C14 111.6(3) . . ? C13 C11 C12 109.3(3) . . ? Cu1 C48 Al1 178.5(2) . . ? N4 C48 Cu1 124.5(3) . . ? N4 C48 Al1 54.00(18) . . ? N3 C48 Cu1 127.0(3) . . ? N3 C48 Al1 54.53(19) . . ? N3 C48 N4 108.5(3) . . ? C4 C3 C2 121.1(3) . . ? C4 C5 C6 120.7(3) . . ? C17 C18 C19 120.5(3) . . ? C17 C18 C20 119.2(4) . . ? C19 C18 C20 120.3(4) . . ? C24 C25 C30 121.7(3) . . ? C26 C25 C24 119.2(4) . . ? C26 C25 C30 119.0(4) . . ? N3 C55 C56 113.1(3) . . ? N3 C55 C60 111.4(3) . . ? C60 C55 C56 109.3(3) . . ? C24 C29 C33 122.6(4) . . ? C28 C29 C24 118.6(4) . . ? C28 C29 C33 118.8(4) . . ? C18 C19 C14 120.3(3) . . ? C3 C4 C7 117.9(4) . . ? C5 C4 C3 120.3(3) . . ? C5 C4 C7 121.8(4) . . ? C57 C56 C55 112.6(4) . . ? N4 C49 C54 110.4(3) . . ? N4 C49 C50 112.8(4) . . ? C54 C49 C50 109.6(4) . . ? C37 C36 N1 119.7(4) . . ? C37 C36 C41 120.4(4) . . ? C41 C36 N1 119.8(4) . . ? C25 C30 C31 110.5(4) . . ? C25 C30 C32 113.5(4) . . ? C32 C30 C31 110.8(4) . . ? C55 C60 C59 112.9(3) . . ? C59 C58 C57 111.3(4) . . ? C58 C59 C60 111.5(4) . . ? C36 C37 C42 121.8(3) . . ? C38 C37 C36 119.3(5) . . ? C38 C37 C42 118.8(4) . . ? C36 C41 C45 122.3(3) . . ? C40 C41 C36 118.1(5) . . ? C40 C41 C45 119.5(4) . . ? C35 C33 C29 112.2(5) . . ? C34 C33 C29 112.8(4) . . ? C34 C33 C35 108.7(5) . . ? C37 C42 C44 112.2(4) . . ? C37 C42 C43 111.9(4) . . ? C43 C42 C44 110.4(4) . . ? C27 C26 C25 120.8(4) . . ? C18 C20 C22A 113.6(7) . . ? C22 C20 C18 107.3(4) . . ? C22 C20 C21 106.6(5) . . ? C21 C20 C18 112.8(5) . . ? C23 C20 C18 110.5(4) . . ? C23 C20 C22 110.5(6) . . ? C23 C20 C21 109.0(6) . . ? C23A C20 C18 107.8(7) . . ? C23A C20 C22A 109.1(11) . . ? C21A C20 C18 111.3(7) . . ? C21A C20 C22A 104.5(10) . . ? C21A C20 C23A 110.5(10) . . ? C56 C57 C58 111.5(4) . . ? C41 C45 C47 113.7(4) . . ? C46 C45 C41 111.9(4) . . ? C46 C45 C47 109.8(4) . . ? C27 C28 C29 121.8(5) . . ? C26 C27 C28 119.8(4) . . ? C39 C38 C37 120.8(5) . . ? C8 C7 C4 109.4(4) . . ? C8 C7 C9 105.9(5) . . ? C10 C7 C4 112.3(4) . . ? C10 C7 C8 109.0(5) . . ? C10 C7 C9 111.7(6) . . ? C9 C7 C4 108.4(4) . . ? C49 C54 C53 112.1(4) . . ? C51 C52 C53 111.8(5) . . ? C39 C40 C41 121.5(5) . . ? C51 C50 C49 112.3(4) . . ? C40 C39 C38 119.8(4) . . ? C52 C51 C50 111.7(4) . . ? C203 C202 C201 120.7(7) . . ? C52 C53 C54 111.6(4) . . ? C200 C201 C202 118.5(6) . . ? C202 C203 C204 120.3(6) . . ? C201 C200 C205 120.9(7) . . ? C205 C204 C203 118.5(6) . . ? C64 C61 P1 108.9(6) . . ? C62 C61 P1 116.9(7) . . ? C62 C61 C64 108.4(6) . . ? C62 C61 C63 108.7(5) . . ? C63 C61 P1 106.0(6) . . ? C63 C61 C64 107.5(5) . . ? C200 C205 C204 121.1(8) . . ? C71 C69 P1 109.0(7) . . ? C70 C69 P1 113.9(7) . . ? C70 C69 C71 110.8(8) . . ? C72 C69 P1 110.6(6) . . ? C72 C69 C71 103.1(9) . . ? C72 C69 C70 108.8(8) . . ? C67 C65 P1 105.3(6) . . ? C67 C65 C68 107.1(6) . . ? C68 C65 P1 111.9(7) . . ? C66 C65 P1 113.8(6) . . ? C66 C65 C67 108.9(6) . . ? C66 C65 C68 109.6(6) . . ? C63A C61A P1 116.6(14) . . ? C63A C61A C64A 108.5(7) . . ? C63A C61A C62A 109.1(7) . . ? C64A C61A P1 104.9(10) . . ? C62A C61A P1 108.9(14) . . ? C62A C61A C64A 108.4(7) . . ? C72A C69A P1 101.4(10) . . ? C72A C69A C71A 107.9(7) . . ? C70A C69A P1 114.5(9) . . ? C70A C69A C72A 108.8(7) . . ? C70A C69A C71A 108.8(7) . . ? C71A C69A P1 114.9(10) . . ? C66A C65A P1 113.5(8) . . ? C66A C65A C68A 109.3(7) . . ? C66A C65A C67A 108.7(7) . . ? C68A C65A P1 105.5(11) . . ? C68A C65A C67A 108.2(7) . . ? C67A C65A P1 111.5(8) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1 P1 2.2163(13) . ? Cu1 C48 1.952(4) . ? Al1 O1 2.011(2) . ? Al1 N1 1.935(3) . ? Al1 N2 1.931(3) . ? Al1 N4 1.908(3) . ? Al1 N3 1.921(3) . ? Al1 C48 2.358(4) . ? P1 C61 1.848(7) . ? P1 C69 2.054(9) . ? P1 C65 1.833(8) . ? P1 C61A 1.890(14) . ? P1 C69A 1.821(12) . ? P1 C65A 2.114(12) . ? O1 C1 1.391(4) . ? O1 C15 1.394(4) . ? N1 C2 1.388(4) . ? N1 C36 1.443(4) . ? N2 C16 1.389(5) . ? N2 C24 1.440(5) . ? N4 C48 1.341(5) . ? N4 C49 1.449(5) . ? N3 C48 1.333(5) . ? N3 C55 1.446(5) . ? C1 C6 1.368(5) . ? C1 C2 1.393(5) . ? C15 C16 1.397(5) . ? C15 C14 1.366(5) . ? C16 C17 1.404(5) . ? C6 C11 1.532(5) . ? C6 C5 1.406(5) . ? C2 C3 1.407(5) . ? C14 C11 1.540(5) . ? C14 C19 1.407(5) . ? C17 C18 1.391(6) . ? C24 C25 1.411(6) . ? C24 C29 1.400(6) . ? C11 C12 1.541(5) . ? C11 C13 1.530(5) . ? C3 C4 1.398(5) . ? C5 C4 1.389(5) . ? C18 C19 1.403(6) . ? C18 C20 1.547(5) . ? C25 C30 1.517(6) . ? C25 C26 1.402(5) . ? C55 C56 1.538(5) . ? C55 C60 1.530(5) . ? C29 C33 1.529(7) . ? C29 C28 1.396(6) . ? C4 C7 1.545(5) . ? C56 C57 1.514(6) . ? C49 C54 1.523(7) . ? C49 C50 1.533(6) . ? C36 C37 1.399(6) . ? C36 C41 1.407(6) . ? C30 C31 1.535(6) . ? C30 C32 1.528(6) . ? C60 C59 1.532(6) . ? C58 C59 1.514(6) . ? C58 C57 1.515(6) . ? C37 C42 1.514(7) . ? C37 C38 1.386(6) . ? C41 C45 1.523(7) . ? C41 C40 1.393(6) . ? C33 C35 1.525(8) . ? C33 C34 1.509(8) . ? C42 C44 1.525(7) . ? C42 C43 1.515(7) . ? C26 C27 1.367(7) . ? C20 C22 1.523(8) . ? C20 C21 1.542(9) . ? C20 C23 1.503(9) . ? C20 C22A 1.583(19) . ? C20 C23A 1.532(19) . ? C20 C21A 1.530(19) . ? C45 C47 1.531(6) . ? C45 C46 1.515(7) . ? C28 C27 1.378(7) . ? C38 C39 1.378(8) . ? C7 C8 1.523(7) . ? C7 C10 1.490(8) . ? C7 C9 1.543(9) . ? C54 C53 1.532(6) . ? C52 C51 1.499(8) . ? C52 C53 1.511(8) . ? C40 C39 1.377(8) . ? C50 C51 1.525(6) . ? C202 C201 1.387(9) . ? C202 C203 1.349(9) . ? C64 C61 1.545(7) . ? C201 C200 1.350(10) . ? C62 C61 1.536(7) . ? C203 C204 1.378(10) . ? C200 C205 1.356(10) . ? C204 C205 1.362(9) . ? C61 C63 1.537(6) . ? C67 C65 1.541(7) . ? C68 C65 1.544(7) . ? C71 C69 1.522(15) . ? C70 C69 1.516(11) . ? C69 C72 1.510(14) . ? C66 C65 1.532(7) . ? C63A C61A 1.533(8) . ? C61A C64A 1.542(8) . ? C61A C62A 1.536(8) . ? C69A C72A 1.537(8) . ? C69A C70A 1.536(7) . ? C69A C71A 1.537(8) . ? C66A C65A 1.533(7) . ? C65A C68A 1.535(8) . ? C65A C67A 1.536(7) . ? loop_ _publcif_info_exptl_table_extra_item sin_theta_over_lambda_max loop_ _publcif_info_exptl_table_header_item ?