#------------------------------------------------------------------------------ #$Date: 2021-09-24 01:23:15 +0300 (Fri, 24 Sep 2021) $ #$Revision: 269266 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/47/1564717.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564717 loop_ _publ_author_name 'Aldridge, Simon' 'McManus, Caitil\'in' 'Hicks, Jamie' 'Goicoechea, Jose M.' 'Cui, Xianlu' 'Zhao, Lili' 'Frenking, Gernot' _publ_section_title ; Coinage metal aluminyl complexes: probing regiochemistry and mechanism in the insertion and reduction of carbon dioxide ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC04676D _journal_year 2021 _chemical_formula_moiety 'C66 H103 Ag Al N4 O2 P' _chemical_formula_sum 'C66 H103 Ag Al N4 O2 P' _chemical_formula_weight 1150.34 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2021-02-07 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-05-24 deposited with the CCDC. 2021-09-16 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 102.038(5) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 14.3910(8) _cell_length_b 19.5868(6) _cell_length_c 26.9617(9) _cell_measurement_reflns_used 11593 _cell_measurement_temperature 150.01(10) _cell_measurement_theta_max 75.2330 _cell_measurement_theta_min 4.0020 _cell_volume 7432.7(6) _computing_cell_refinement 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_data_collection 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 150.01(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.5035 _diffrn_detector_type Atlas _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.985 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -114.00 -28.00 1.00 15.00 -- -41.40 -37.00 0.00 86 2 \w 2.00 33.00 1.00 15.00 -- -41.40 19.00-180.00 31 3 \w -44.00 11.00 1.00 15.00 -- -41.40 57.00 -60.00 55 4 \w 1.00 36.00 1.00 15.00 -- -41.40 19.00 150.00 35 5 \w 35.00 89.00 1.00 15.00 -- 41.40-125.00-180.00 54 6 \w 66.00 115.00 1.00 60.00 -- 111.00 15.00 -30.00 49 7 \w 55.00 109.00 1.00 60.00 -- 111.00-111.00 90.00 54 8 \w 40.00 70.00 1.00 60.00 -- 111.00 -45.00-150.00 30 9 \w 111.00 146.00 1.00 60.00 -- 111.00 111.00 150.00 35 10 \w 37.00 109.00 1.00 60.00 -- 111.00-111.00-180.00 72 11 \w 57.00 86.00 1.00 60.00 -- 111.00 -61.00 60.00 29 12 \w 42.00 71.00 1.00 60.00 -- 111.00 -45.00-180.00 29 13 \w 89.00 178.00 1.00 60.00 -- 111.00 30.00 30.00 89 14 \w 148.00 175.00 1.00 60.00 -- 111.00 15.00 -30.00 27 15 \w 39.00 64.00 1.00 60.00 -- 111.00 -94.00 90.00 25 16 \w 36.00 84.00 1.00 60.00 -- 111.00 -94.00 -30.00 48 17 \w 71.00 108.00 1.00 60.00 -- 111.00-111.00 60.00 37 18 \w 74.00 107.00 1.00 60.00 -- 111.00 -94.00 90.00 33 19 \w 129.00 170.00 1.00 60.00 -- 111.00 77.00-180.00 41 20 \w 87.00 170.00 1.00 60.00 -- 111.00 45.00 -60.00 83 21 \w 43.00 71.00 1.00 60.00 -- 111.00 -45.00 60.00 28 22 \w 54.00 91.00 1.00 60.00 -- 111.00 -61.00 150.00 37 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, Atlas' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.1057592000 _diffrn_orient_matrix_UB_12 0.0039380000 _diffrn_orient_matrix_UB_13 -0.0025939000 _diffrn_orient_matrix_UB_21 -0.0280530000 _diffrn_orient_matrix_UB_22 0.0081699000 _diffrn_orient_matrix_UB_23 -0.0580214000 _diffrn_orient_matrix_UB_31 -0.0023523000 _diffrn_orient_matrix_UB_32 0.0781712000 _diffrn_orient_matrix_UB_33 0.0062179000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0510 _diffrn_reflns_av_unetI/netI 0.0508 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.985 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 24 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 32 _diffrn_reflns_limit_l_min -33 _diffrn_reflns_number 44027 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.985 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 76.146 _diffrn_reflns_theta_min 3.867 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 2.777 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.70561 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.028 _exptl_crystal_description plate _exptl_crystal_F_000 2472 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.05 _refine_diff_density_max 0.868 _refine_diff_density_min -2.430 _refine_diff_density_rms 0.103 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.028 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 705 _refine_ls_number_reflns 15310 _refine_ls_number_restraints 18 _refine_ls_restrained_S_all 1.030 _refine_ls_R_factor_all 0.1053 _refine_ls_R_factor_gt 0.0920 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1557P)^2^+15.7728P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2628 _refine_ls_wR_factor_ref 0.2760 _reflns_Friedel_coverage 0.000 _reflns_number_gt 12164 _reflns_number_total 15310 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1sc04676d2.cif _cod_data_source_block 7-Ag _cod_original_cell_volume 7432.7(5) _cod_database_code 1564717 _publcif_datablock.id {7ebd7094-9205-45bf-ae11-f6ffff973fb5} _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C50 H60 Al1 Ag1 P1 N4 O2' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.874 _shelx_estimated_absorpt_t_min 0.607 _reflns_odcompleteness_completeness 99.59 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 74.33 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2. Uiso/Uaniso restraints and constraints C19 \\sim C18 \\sim C16 \\sim C17: within 2A with sigma of 0.005 and sigma for terminal atoms of 0.01 3.a Ternary CH refined with riding coordinates: C45(H45), C52(H52), C49(H49), C30(H30), C33(H33), C42(H42) 3.b Aromatic/amide H refined with riding coordinates: C5(H5), C39(H39), C3(H3), C13(H13), C11(H11), C41(H41), C40(H40), C28(H28), C27(H27), C26(H26) 3.c Idealised Me refined as rotating group: C50(H50A,H50B,H50C), C9(H9A,H9B,H9C), C8(H8A,H8B,H8C), C48(H48A,H48B,H48C), C21(H21A,H21B,H21C), C46(H46A,H46B,H46C), C54(H54A,H54B,H54C), C31(H31A,H31B, H31C), C66(H66A,H66B,H66C), C47(H47A,H47B,H47C), C53(H53A,H53B,H53C), C32(H32A, H32B,H32C), C62(H62A,H62B,H62C), C58(H58A,H58B,H58C), C57(H57A,H57B,H57C), C60(H60A,H60B,H60C), C64(H64A,H64B,H64C), C61(H61A,H61B,H61C), C22(H22A,H22B, H22C), C65(H65A,H65B,H65C), C23(H23A,H23B,H23C), C35(H35A,H35B,H35C), C34(H34A, H34B,H34C), C56(H56A,H56B,H56C), C44(H44A,H44B,H44C), C43(H43A,H43B,H43C), C17(H17A,H17B,H17C), C19(H19A,H19B,H19C), C18(H18A,H18B,H18C) ; _shelx_res_file ; TITL 87cmcm20_a.res in P2(1)/c 87cmcm20.res created by SHELXL-2018/3 at 16:58:37 on 07-Feb-2021 REM Old TITL 87cmcm20 in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.190, Rweak 0.071, Alpha 0.074 REM 0.848 for 474 systematic absences, Orientation as input REM Formula found by SHELXT: C63 N3 O6 P2 Ag CELL 1.54184 14.391 19.5868 26.9617 90 102.038 90 ZERR 4 0.0008 0.0006 0.0009 0 0.005 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Ag Al N O P UNIT 264 412 4 4 16 8 4 SIMU 0.005 0.01 2 C19 C18 C16 C17 L.S. 20 0 0 PLAN 20 SIZE 0.2 0.1 0.05 list 4 ABIN fmap 2 53 acta REM REM REM WGHT 0.155700 15.772799 FVAR 0.23128 AG1 3 0.242070 0.639968 0.575893 11.00000 0.06010 0.05818 = 0.04399 0.00117 0.00205 -0.00342 P1 7 0.130481 0.698989 0.514358 11.00000 0.05389 0.04855 = 0.03756 -0.00217 0.00466 0.00012 AL1 4 0.556997 0.607049 0.713255 11.00000 0.04090 0.03589 = 0.02667 0.00046 0.00626 -0.00140 O1 6 0.448068 0.554972 0.701709 11.00000 0.04714 0.03391 = 0.02760 -0.00110 0.00545 -0.00366 O2 6 0.616076 0.553020 0.775116 11.00000 0.04456 0.03925 = 0.02328 0.00076 0.00669 0.00242 N1 5 0.324525 0.578252 0.633846 11.00000 0.04792 0.04126 = 0.03115 0.01076 -0.00308 -0.00083 N4 5 0.557333 0.674179 0.764271 11.00000 0.04641 0.03123 = 0.03613 -0.00080 0.00057 -0.00307 N3 5 0.657704 0.563855 0.689877 11.00000 0.04522 0.04779 = 0.02618 0.00963 0.01029 0.00529 N2 5 0.470685 0.640400 0.653960 11.00000 0.04582 0.04042 = 0.02798 0.00683 0.00823 -0.00161 C51 1 0.408864 0.591895 0.660648 11.00000 0.03547 0.03771 = 0.02809 -0.00069 0.00364 -0.00143 C5 1 0.826106 0.443970 0.803651 11.00000 0.05282 0.05532 = 0.03437 0.00788 0.00581 0.01361 AFIX 43 H5 2 0.864459 0.420372 0.830171 11.00000 -1.20000 AFIX 0 C2 1 0.715950 0.518855 0.722879 11.00000 0.04896 0.04719 = 0.02812 0.00669 0.00903 0.00254 C1 1 0.696032 0.514957 0.771442 11.00000 0.04197 0.03930 = 0.02675 0.00345 0.00830 0.00298 C10 1 0.670574 0.558304 0.865660 11.00000 0.05722 0.05245 = 0.02755 -0.00429 0.00191 0.01062 C37 1 0.533750 0.745577 0.759365 11.00000 0.05500 0.03175 = 0.03506 -0.00062 0.00032 0.00042 C38 1 0.438966 0.766410 0.752341 11.00000 0.06160 0.04099 = 0.03174 0.00130 0.00581 -0.00223 C15 1 0.624004 0.586779 0.821117 11.00000 0.05074 0.03802 = 0.03004 -0.00384 0.00568 0.00219 C6 1 0.748508 0.481969 0.812963 11.00000 0.05064 0.04324 = 0.03122 0.00369 0.00713 0.00349 C4 1 0.846505 0.441094 0.755256 11.00000 0.04930 0.05919 = 0.03804 0.00840 0.01178 0.00920 C39 1 0.420373 0.837304 0.751159 11.00000 0.07073 0.04643 = 0.04520 0.00403 0.00762 0.00700 AFIX 43 H39 2 0.357677 0.852046 0.746167 11.00000 -1.20000 AFIX 0 C14 1 0.586374 0.652499 0.814250 11.00000 0.05445 0.04291 = 0.03175 -0.00456 -0.00141 0.00496 C45 1 0.357693 0.715677 0.747294 11.00000 0.04939 0.04804 = 0.04952 -0.00728 0.00836 0.00151 AFIX 13 H45 2 0.381707 0.670990 0.739473 11.00000 -1.20000 AFIX 0 C3 1 0.792484 0.479163 0.715777 11.00000 0.05206 0.06257 = 0.03327 0.01254 0.01564 0.00794 AFIX 43 H3 2 0.807934 0.478012 0.683970 11.00000 -1.20000 AFIX 0 C13 1 0.585216 0.688189 0.859121 11.00000 0.08463 0.05062 = 0.04352 -0.01908 -0.00619 0.01958 AFIX 43 H13 2 0.556843 0.731024 0.857403 11.00000 -1.20000 AFIX 0 C7 1 0.719898 0.488869 0.863844 11.00000 0.06796 0.05206 = 0.02367 0.00563 0.00770 0.01832 C50 1 0.464890 0.653980 0.561851 11.00000 0.06396 0.07638 = 0.03493 0.01789 0.01518 0.00854 AFIX 137 H50A 2 0.530391 0.642097 0.564230 11.00000 -1.50000 H50B 2 0.445184 0.685209 0.534216 11.00000 -1.50000 H50C 2 0.426567 0.613489 0.556054 11.00000 -1.50000 AFIX 0 C24 1 0.669517 0.559713 0.637578 11.00000 0.05179 0.07329 = 0.03255 0.01900 0.01828 0.02335 C11 1 0.670979 0.596742 0.909487 11.00000 0.08430 0.05960 = 0.03182 -0.00467 0.00163 0.02608 AFIX 43 H11 2 0.701390 0.579793 0.940911 11.00000 -1.20000 AFIX 0 C9 1 0.808525 0.485740 0.908056 11.00000 0.08454 0.08769 = 0.02878 0.00216 -0.00143 0.03551 AFIX 137 H9A 2 0.848030 0.524841 0.906481 11.00000 -1.50000 H9B 2 0.843811 0.444870 0.905133 11.00000 -1.50000 H9C 2 0.788458 0.485579 0.939852 11.00000 -1.50000 AFIX 0 C52 1 0.273012 0.520494 0.650430 11.00000 0.05522 0.04690 = 0.05582 0.01077 -0.00566 -0.01518 AFIX 13 H52 2 0.320704 0.486583 0.665458 11.00000 -1.20000 AFIX 0 C36 1 0.607664 0.794387 0.765681 11.00000 0.06275 0.03626 = 0.05875 -0.00618 0.00177 -0.01267 C41 1 0.581981 0.863722 0.764047 11.00000 0.08559 0.05053 = 0.05308 -0.00549 0.00139 -0.01960 AFIX 43 H41 2 0.629739 0.896478 0.767942 11.00000 -1.20000 AFIX 0 C20 1 0.931530 0.399201 0.745160 11.00000 0.05650 0.08511 = 0.05632 0.02191 0.02612 0.02406 C29 1 0.625557 0.506370 0.606864 11.00000 0.07855 0.08063 = 0.02386 0.00567 0.01477 0.02940 C49 1 0.452951 0.687759 0.611463 11.00000 0.04691 0.04950 = 0.03552 0.01158 0.00643 -0.00096 AFIX 13 H49 2 0.386609 0.702508 0.606724 11.00000 -1.20000 AFIX 0 C8 1 0.650819 0.431645 0.869495 11.00000 0.09519 0.04748 = 0.04914 0.00611 0.03391 0.00697 AFIX 137 H8A 2 0.638199 0.432712 0.903073 11.00000 -1.50000 H8B 2 0.678320 0.388414 0.863876 11.00000 -1.50000 H8C 2 0.592502 0.437827 0.845091 11.00000 -1.50000 AFIX 0 C48 1 0.514698 0.751056 0.623964 11.00000 0.06936 0.05759 = 0.05505 0.02470 0.00639 -0.01289 AFIX 137 H48A 2 0.501036 0.772746 0.653566 11.00000 -1.50000 H48B 2 0.501545 0.782216 0.595887 11.00000 -1.50000 H48C 2 0.580470 0.738140 0.630325 11.00000 -1.50000 AFIX 0 C21 1 0.979723 0.355957 0.790808 11.00000 0.05918 0.10515 = 0.06963 0.02773 0.01726 0.03165 AFIX 137 H21A 2 1.006800 0.385465 0.818490 11.00000 -1.50000 H21B 2 1.028988 0.328755 0.781598 11.00000 -1.50000 H21C 2 0.933518 0.326611 0.800880 11.00000 -1.50000 AFIX 0 C30 1 0.567874 0.451928 0.625233 11.00000 0.08345 0.06342 = 0.03530 -0.01553 0.00182 0.02063 AFIX 13 H30 2 0.563434 0.463381 0.660046 11.00000 -1.20000 AFIX 0 C40 1 0.490750 0.884710 0.757048 11.00000 0.09616 0.03401 = 0.04835 0.00238 0.01218 0.00017 AFIX 43 H40 2 0.476297 0.931027 0.756271 11.00000 -1.20000 AFIX 0 C12 1 0.625988 0.660520 0.906449 11.00000 0.10089 0.06602 = 0.03583 -0.01490 -0.00538 0.02573 C46 1 0.274626 0.734431 0.703946 11.00000 0.05173 0.07897 = 0.05737 -0.01162 0.00155 0.00872 AFIX 137 H46A 2 0.250302 0.778456 0.710385 11.00000 -1.50000 H46B 2 0.225282 0.700889 0.701695 11.00000 -1.50000 H46C 2 0.296244 0.735701 0.672595 11.00000 -1.50000 AFIX 0 C59 1 0.048831 0.745703 0.549716 11.00000 0.06919 0.07499 = 0.06276 -0.00358 0.02283 -0.00194 C54 1 0.221429 0.540171 0.690051 11.00000 0.07519 0.08143 = 0.07532 0.01561 0.02175 -0.02589 AFIX 137 H54A 2 0.265588 0.557651 0.718949 11.00000 -1.50000 H54B 2 0.189627 0.500946 0.699936 11.00000 -1.50000 H54C 2 0.175466 0.574733 0.677081 11.00000 -1.50000 AFIX 0 C31 1 0.613415 0.381185 0.626141 11.00000 0.10135 0.06174 = 0.05561 -0.00990 0.00673 0.02440 AFIX 137 H31A 2 0.613889 0.367095 0.592092 11.00000 -1.50000 H31B 2 0.577493 0.349047 0.641406 11.00000 -1.50000 H31C 2 0.677422 0.383048 0.645495 11.00000 -1.50000 AFIX 0 C55 1 0.187799 0.763393 0.477844 11.00000 0.08854 0.05891 = 0.04800 0.00718 0.01436 -0.00114 C66 1 0.001669 0.665879 0.420340 11.00000 0.08068 0.07126 = 0.06460 -0.00997 -0.02232 0.00040 AFIX 137 H66A 2 -0.041856 0.699389 0.428102 11.00000 -1.50000 H66B 2 -0.033199 0.630179 0.400214 11.00000 -1.50000 H66C 2 0.044056 0.687014 0.401768 11.00000 -1.50000 AFIX 0 C47 1 0.324466 0.709099 0.797907 11.00000 0.07046 0.07468 = 0.05239 -0.00005 0.01320 -0.00910 AFIX 137 H47A 2 0.375670 0.691927 0.823549 11.00000 -1.50000 H47B 2 0.271641 0.678184 0.793747 11.00000 -1.50000 H47C 2 0.305408 0.753094 0.807923 11.00000 -1.50000 AFIX 0 C53 1 0.209273 0.486903 0.605163 11.00000 0.07661 0.05604 = 0.08306 0.00351 -0.01902 -0.02233 AFIX 137 H53A 2 0.159157 0.517755 0.590582 11.00000 -1.50000 H53B 2 0.182411 0.446011 0.615909 11.00000 -1.50000 H53C 2 0.245877 0.475666 0.580323 11.00000 -1.50000 AFIX 0 C28 1 0.639995 0.504945 0.556784 11.00000 0.10541 0.10466 = 0.03156 0.00795 0.01670 0.04560 AFIX 43 H28 2 0.611928 0.470251 0.535224 11.00000 -1.20000 AFIX 0 C32 1 0.466595 0.448421 0.593235 11.00000 0.08989 0.06413 = 0.06587 -0.02532 -0.00227 0.01878 AFIX 137 H32A 2 0.440506 0.493635 0.588483 11.00000 -1.50000 H32B 2 0.427916 0.420845 0.610349 11.00000 -1.50000 H32C 2 0.467924 0.428586 0.560830 11.00000 -1.50000 AFIX 0 C25 1 0.726672 0.608911 0.620340 11.00000 0.05266 0.10958 = 0.05722 0.05013 0.02552 0.02360 C33 1 0.775368 0.665813 0.652794 11.00000 0.06239 0.11817 = 0.08622 0.05863 0.01904 -0.01103 AFIX 13 H33 2 0.735642 0.677551 0.676979 11.00000 -1.20000 AFIX 0 C63 1 0.059211 0.635601 0.469782 11.00000 0.07634 0.05246 = 0.05480 -0.00165 -0.01095 0.00254 C27 1 0.693470 0.552449 0.538835 11.00000 0.10388 0.17788 = 0.04318 0.04327 0.03605 0.07250 AFIX 43 H27 2 0.700381 0.550261 0.505337 11.00000 -1.20000 AFIX 0 C62 1 0.099274 0.810599 0.575467 11.00000 0.09693 0.08206 = 0.07253 -0.02666 0.02661 -0.00050 AFIX 137 H62A 2 0.160544 0.798400 0.595182 11.00000 -1.50000 H62B 2 0.061585 0.830448 0.597210 11.00000 -1.50000 H62C 2 0.106857 0.843044 0.549918 11.00000 -1.50000 AFIX 0 C58 1 0.270125 0.800297 0.514974 11.00000 0.09406 0.06923 = 0.06738 0.00466 0.02054 -0.01793 AFIX 137 H58A 2 0.244490 0.826081 0.539283 11.00000 -1.50000 H58B 2 0.302412 0.830523 0.496172 11.00000 -1.50000 H58C 2 0.314135 0.766998 0.532314 11.00000 -1.50000 AFIX 0 C57 1 0.239103 0.724392 0.441184 11.00000 0.09100 0.11235 = 0.05548 -0.00475 0.02412 -0.00143 AFIX 137 H57A 2 0.283303 0.692413 0.460094 11.00000 -1.50000 H57B 2 0.272647 0.756320 0.424347 11.00000 -1.50000 H57C 2 0.193083 0.700324 0.416440 11.00000 -1.50000 AFIX 0 C60 1 0.030717 0.699805 0.592420 11.00000 0.07414 0.10678 = 0.07362 0.00401 0.02912 0.00222 AFIX 137 H60A 2 -0.007956 0.661777 0.578264 11.00000 -1.50000 H60B 2 -0.001504 0.725362 0.614135 11.00000 -1.50000 H60C 2 0.090210 0.683392 0.611736 11.00000 -1.50000 AFIX 0 C64 1 0.127988 0.582889 0.456087 11.00000 0.10569 0.06552 = 0.07648 -0.02429 -0.01428 0.02083 AFIX 137 H64A 2 0.176648 0.605775 0.442899 11.00000 -1.50000 H64B 2 0.094016 0.552244 0.430912 11.00000 -1.50000 H64C 2 0.156515 0.557528 0.485844 11.00000 -1.50000 AFIX 0 C61 1 -0.047387 0.770245 0.518372 11.00000 0.07591 0.08694 = 0.07972 0.01002 0.02136 0.01519 AFIX 137 H61A 2 -0.036687 0.802245 0.493178 11.00000 -1.50000 H61B 2 -0.082977 0.791936 0.540378 11.00000 -1.50000 H61C 2 -0.082440 0.731843 0.502033 11.00000 -1.50000 AFIX 0 C26 1 0.736002 0.602090 0.568954 11.00000 0.07835 0.17850 = 0.06318 0.07217 0.04524 0.05524 AFIX 43 H26 2 0.773191 0.633495 0.555994 11.00000 -1.20000 AFIX 0 C42 1 0.711132 0.775017 0.772296 11.00000 0.05405 0.06060 = 0.11599 -0.00917 -0.00509 -0.01254 AFIX 13 H42 2 0.714743 0.726041 0.765506 11.00000 -1.20000 AFIX 0 C22 1 0.894472 0.346293 0.702633 11.00000 0.08864 0.10594 = 0.06880 -0.00194 0.02429 0.04015 AFIX 137 H22A 2 0.850678 0.315750 0.713657 11.00000 -1.50000 H22B 2 0.947020 0.320729 0.695427 11.00000 -1.50000 H22C 2 0.862841 0.369738 0.672558 11.00000 -1.50000 AFIX 0 C65 1 -0.009594 0.596036 0.496774 11.00000 0.09563 0.06880 = 0.06899 0.00331 -0.00806 -0.02343 AFIX 137 H65A 2 0.026468 0.570664 0.524740 11.00000 -1.50000 H65B 2 -0.047461 0.565181 0.473203 11.00000 -1.50000 H65C 2 -0.050329 0.627800 0.509066 11.00000 -1.50000 AFIX 0 C23 1 1.000703 0.444343 0.727466 11.00000 0.05144 0.13075 = 0.14744 0.06296 0.04922 0.02731 AFIX 137 H23A 2 0.968874 0.469695 0.698378 11.00000 -1.50000 H23B 2 1.050173 0.417140 0.718470 11.00000 -1.50000 H23C 2 1.027849 0.475423 0.754092 11.00000 -1.50000 AFIX 0 C35 1 0.789099 0.732387 0.623283 11.00000 0.07040 0.12846 = 0.12955 0.08144 0.03551 0.00615 AFIX 137 H35A 2 0.837067 0.724988 0.603886 11.00000 -1.50000 H35B 2 0.808387 0.768901 0.646942 11.00000 -1.50000 H35C 2 0.730286 0.744203 0.600876 11.00000 -1.50000 AFIX 0 C34 1 0.871445 0.642867 0.683520 11.00000 0.07279 0.13538 = 0.13629 0.08762 -0.01851 -0.02091 AFIX 137 H34A 2 0.862641 0.604903 0.704586 11.00000 -1.50000 H34B 2 0.900681 0.679885 0.704430 11.00000 -1.50000 H34C 2 0.911540 0.629360 0.660901 11.00000 -1.50000 AFIX 0 C16 1 0.616832 0.700536 0.954152 11.00000 0.20980 0.11906 = 0.04205 -0.03736 -0.02672 0.09074 C56 1 0.121160 0.816960 0.447766 11.00000 0.11972 0.06850 = 0.07896 0.01991 0.03062 0.00234 AFIX 137 H56A 2 0.072603 0.794481 0.423424 11.00000 -1.50000 H56B 2 0.156863 0.846727 0.430461 11.00000 -1.50000 H56C 2 0.092316 0.843192 0.470592 11.00000 -1.50000 AFIX 0 C44 1 0.757619 0.813154 0.735337 11.00000 0.08031 0.10883 = 0.18876 0.01285 0.03711 -0.03256 AFIX 137 H44A 2 0.718491 0.809924 0.701910 11.00000 -1.50000 H44B 2 0.818778 0.793541 0.735400 11.00000 -1.50000 H44C 2 0.765164 0.860261 0.745184 11.00000 -1.50000 AFIX 0 C43 1 0.764885 0.788671 0.827235 11.00000 0.07604 0.10755 = 0.14134 -0.00850 -0.03869 -0.01279 AFIX 137 H43A 2 0.765081 0.836795 0.834004 11.00000 -1.50000 H43B 2 0.829112 0.772687 0.831410 11.00000 -1.50000 H43C 2 0.733868 0.765016 0.850434 11.00000 -1.50000 AFIX 0 C17 1 0.663581 0.663397 1.002634 11.00000 0.21385 0.12454 = 0.04035 -0.03072 -0.02819 0.08305 AFIX 137 H17A 2 0.635026 0.619210 1.003354 11.00000 -1.50000 H17B 2 0.654903 0.689403 1.031506 11.00000 -1.50000 H17C 2 0.730257 0.658186 1.003574 11.00000 -1.50000 AFIX 0 C19 1 0.658295 0.769773 0.953726 11.00000 0.23780 0.10625 = 0.07151 -0.04652 -0.04166 0.06328 AFIX 137 H19A 2 0.722845 0.766129 0.949717 11.00000 -1.50000 H19B 2 0.656833 0.792441 0.985123 11.00000 -1.50000 H19C 2 0.622053 0.795580 0.926061 11.00000 -1.50000 AFIX 0 C18 1 0.510925 0.708496 0.953948 11.00000 0.21621 0.16679 = 0.04900 -0.03283 0.00394 0.10237 AFIX 137 H18A 2 0.479978 0.731140 0.923370 11.00000 -1.50000 H18B 2 0.503345 0.735093 0.982749 11.00000 -1.50000 H18C 2 0.483040 0.664248 0.955597 11.00000 -1.50000 AFIX 0 HKLF 4 REM 87cmcm20_a.res in P2(1)/c REM wR2 = 0.2760, GooF = S = 1.028, Restrained GooF = 1.030 for all data REM R1 = 0.0920 for 12164 Fo > 4sig(Fo) and 0.1053 for all 15310 data REM 705 parameters refined using 18 restraints END WGHT 0.1557 15.7797 REM Highest difference peak 0.868, deepest hole -2.430, 1-sigma level 0.103 Q1 1 0.2376 0.6843 0.5633 11.00000 0.05 0.87 Q2 1 0.2228 0.6617 0.5412 11.00000 0.05 0.86 Q3 1 0.2405 0.6963 0.5776 11.00000 0.05 0.80 Q4 1 0.5655 0.6228 0.7119 11.00000 0.05 0.69 Q5 1 0.7205 0.7782 0.9403 11.00000 0.05 0.54 Q6 1 0.6501 0.5578 0.7794 11.00000 0.05 0.47 Q7 1 0.6082 0.5611 0.7647 11.00000 0.05 0.45 Q8 1 0.6659 0.5689 0.6632 11.00000 0.05 0.45 Q9 1 0.3061 0.5978 0.6253 11.00000 0.05 0.44 Q10 1 0.4447 0.5341 0.6974 11.00000 0.05 0.43 Q11 1 0.5463 0.7147 0.7600 11.00000 0.05 0.43 Q12 1 0.4627 0.6576 0.6395 11.00000 0.05 0.42 Q13 1 0.5851 0.6700 0.8374 11.00000 0.05 0.42 Q14 1 0.6685 0.5838 0.8756 11.00000 0.05 0.42 Q15 1 0.4393 0.5756 0.6855 11.00000 0.05 0.42 Q16 1 0.2486 0.5943 0.5550 11.00000 0.05 0.42 Q17 1 0.6010 0.8244 0.7598 11.00000 0.05 0.42 Q18 1 0.6638 0.5987 0.6952 11.00000 0.05 0.41 Q19 1 0.4085 0.8239 0.7539 11.00000 0.05 0.40 Q20 1 0.5516 0.7832 0.7609 11.00000 0.05 0.40 ; _shelx_res_checksum 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180.74 9.54 0 4 20 205.23 10.34 0 4 21 55.57 9.84 0 4 21 45.87 5.43 0 4 21 47.74 5.67 0 -4 21 44.50 5.15 0 4 22 90.07 12.24 0 4 22 103.97 6.87 0 4 22 88.85 7.53 0 -4 22 92.74 7.31 0 4 23 2.71 2.28 0 -4 23 2.61 2.17 0 4 23 4.03 2.40 0 4 24 114.86 7.55 0 -4 24 136.03 8.24 0 4 -24 128.03 7.52 0 4 25 0.37 2.00 0 4 -25 3.53 2.09 0 4 -26 96.38 6.29 0 4 26 79.40 5.73 0 -4 -26 95.08 6.46 0 4 -27 23.86 3.32 0 -4 -27 20.85 3.24 0 4 27 18.06 2.90 0 4 28 92.82 5.84 0 4 -28 106.81 6.25 0 -4 -28 104.02 6.36 0 -4 -29 11.37 2.36 0 4 -29 12.10 2.39 0 4 29 9.19 2.05 0 4 30 1.62 1.30 0 4 -30 0.57 1.47 0 -4 -30 2.59 2.18 0 -4 -30 1.95 1.45 0 -4 -31 0.27 1.77 0 4 -31 3.87 1.37 0 -4 -31 4.02 1.52 0 -4 -32 5.94 1.37 0 -4 -32 3.36 1.58 0 5 0 8.18 1.61 0 5 1 1079.91 17.05 0 5 2 64.02 4.65 0 -5 -2 59.02 2.68 0 5 -2 66.31 5.22 0 5 -3 6.61 2.25 0 5 3 7.16 2.07 0 5 -4 1687.16 25.44 0 5 4 1633.23 26.32 0 5 5 84.10 6.41 0 5 6 161.01 9.61 0 5 7 52.74 5.82 0 5 8 223.24 12.31 0 5 9 20.84 4.38 0 5 10 475.37 19.45 0 5 11 402.99 18.72 0 -5 11 384.11 13.89 0 -5 12 1048.90 24.38 0 5 12 1110.80 32.43 0 -5 13 98.57 7.92 0 5 13 104.35 10.67 0 5 14 515.08 23.92 0 5 15 168.72 14.14 0 5 16 105.78 11.65 0 5 17 37.84 7.32 0 5 18 127.73 13.84 0 5 19 45.51 4.94 0 5 19 40.61 7.77 0 5 19 42.97 5.00 0 5 20 171.70 9.68 0 5 20 167.23 16.65 0 5 20 162.34 9.38 0 5 21 1.49 2.40 0 -5 21 0.57 1.94 0 5 21 4.51 2.95 0 5 21 -2.71 3.80 0 5 22 200.22 11.02 0 -5 22 196.46 9.64 0 5 22 218.18 9.92 0 5 -23 24.81 3.64 0 -5 23 22.88 3.60 0 5 23 18.83 3.39 0 5 -24 36.11 4.28 0 5 24 37.60 4.48 0 -5 24 29.42 4.18 0 5 25 52.15 5.06 0 -5 -25 62.79 5.42 0 5 -25 55.55 5.06 0 -5 -26 37.43 4.20 0 5 26 36.66 4.25 0 5 -26 36.26 4.15 0 5 -27 8.71 2.48 0 -5 -27 8.62 2.56 0 5 27 9.20 2.29 0 -5 -28 55.95 4.68 0 5 28 52.86 4.30 0 5 -28 51.74 4.20 0 5 29 17.14 2.59 0 5 -29 21.11 2.63 0 -5 -29 20.47 2.88 0 5 -30 38.05 3.11 0 5 30 38.02 3.07 0 -5 -30 42.44 3.56 0 5 -31 -0.57 1.00 0 -5 -31 1.58 1.84 0 -5 -31 0.94 1.16 0 -5 -32 2.12 1.01 0 -5 -32 2.20 1.42 0 6 1 85.56 5.29 0 6 -1 88.40 6.44 0 6 -2 338.73 12.33 0 -6 -2 302.56 6.67 0 6 2 332.55 11.02 0 6 -3 1339.02 24.36 0 6 3 1321.03 24.05 0 6 3 1285.99 23.02 0 6 4 110.89 7.51 0 6 4 109.30 7.23 0 6 -4 112.64 7.28 0 6 -5 150.07 8.74 0 6 5 154.33 8.94 0 6 -6 649.23 18.28 0 6 6 631.22 19.19 0 6 7 66.85 6.73 0 6 8 438.33 17.80 0 6 9 1812.71 37.38 0 6 10 104.84 9.41 0 6 11 1064.53 31.31 0 6 12 710.87 26.56 0 6 13 12.14 4.35 0 6 14 138.29 12.73 0 6 15 182.07 15.09 0 6 16 34.53 7.01 0 6 17 60.47 9.65 0 6 18 6.98 3.93 0 6 18 5.15 2.67 0 6 18 4.64 2.42 0 6 19 42.25 5.00 0 6 19 48.17 9.29 0 6 19 46.77 5.37 0 6 20 32.45 4.67 0 6 20 33.69 4.81 0 6 20 35.77 7.98 0 6 21 81.18 12.14 0 6 21 86.31 6.98 0 6 21 90.00 7.12 0 6 21 72.91 6.14 0 6 -22 4.47 2.05 0 6 22 3.24 2.03 0 6 -23 190.13 8.99 0 6 23 208.51 9.87 0 -6 -24 54.75 5.21 0 6 -24 46.59 4.63 0 6 24 46.17 5.10 0 -6 -25 14.91 2.98 0 6 25 17.54 3.22 0 6 -25 17.68 3.07 0 6 -26 94.41 5.81 0 -6 -26 99.57 6.25 0 6 26 94.68 6.34 0 6 27 9.84 2.50 0 -6 -27 9.84 2.41 0 6 -27 7.40 1.94 0 6 -28 16.14 2.56 0 6 28 15.42 2.62 0 -6 -28 14.39 2.81 0 6 -29 37.23 3.17 0 6 29 33.71 3.21 0 -6 -29 36.50 3.42 0 6 30 0.08 1.12 0 -6 -30 1.32 1.98 0 -6 -30 0.77 1.40 0 -6 -31 2.97 1.81 0 -6 -31 3.72 1.24 0 7 0 7.38 3.05 0 7 1 301.28 12.55 0 7 1 304.09 10.70 0 7 -1 307.50 12.77 0 7 -2 55.65 5.78 0 7 2 55.54 5.58 0 -7 -2 46.20 2.88 0 7 2 55.94 4.89 0 -7 -3 22.95 1.31 0 7 3 27.86 4.05 0 7 3 29.96 4.01 0 7 -3 27.88 4.20 0 7 4 31.48 4.41 0 7 4 31.22 4.42 0 7 -4 30.94 4.68 0 7 -5 838.43 21.67 0 7 5 824.20 21.76 0 7 -6 72.72 6.86 0 7 6 71.04 6.96 0 7 7 643.58 21.28 0 7 -7 629.15 19.88 0 7 8 128.67 9.98 0 7 -8 130.00 9.35 0 7 9 360.98 17.41 0 7 -9 368.05 15.92 0 7 10 95.44 9.43 0 7 11 28.16 5.54 0 7 12 291.78 17.87 0 7 13 710.51 28.38 0 7 14 39.17 6.99 0 7 15 70.56 9.81 0 7 16 2.51 2.51 0 7 17 59.63 5.70 0 7 17 66.42 10.26 0 7 18 39.78 5.00 0 7 18 44.71 5.10 0 7 18 46.86 8.85 0 7 19 118.47 14.32 0 7 19 133.14 8.52 0 7 19 127.90 8.45 0 7 20 28.27 7.37 0 7 20 25.26 3.49 0 7 20 29.77 4.60 0 7 21 251.47 11.06 0 7 21 231.19 12.12 0 7 22 160.05 8.75 0 7 -23 7.51 2.54 0 -7 -23 6.20 2.29 0 7 23 9.47 2.95 0 -7 -24 10.34 2.53 0 7 -24 11.37 2.53 0 7 24 11.34 3.08 0 -7 -25 55.02 4.96 0 7 25 47.54 4.72 0 7 -25 56.70 4.79 0 7 26 1.80 1.79 0 -7 -26 2.81 2.11 0 7 -26 0.03 1.66 0 7 27 113.41 6.41 0 -7 -27 112.13 6.33 0 7 28 0.82 1.56 0 -7 -28 1.42 1.72 0 -7 -29 13.76 2.24 0 7 29 14.50 2.30 0 -7 -30 2.27 1.44 0 -7 -30 0.31 1.88 0 7 30 2.20 1.27 0 -7 -31 17.18 2.42 0 -7 -31 19.37 1.87 0 8 0 33.46 5.18 0 -8 -1 17.01 2.45 0 8 1 18.09 3.67 0 8 -1 19.75 3.84 0 8 2 32.74 4.02 0 -8 -2 27.75 2.50 0 8 2 30.21 4.29 0 8 -2 33.80 5.03 0 8 3 154.14 9.87 0 8 -3 146.80 9.78 0 8 3 152.02 9.07 0 8 -4 123.65 8.86 0 8 4 129.37 8.93 0 8 4 128.51 8.73 0 8 5 201.94 11.49 0 8 -5 194.57 11.41 0 8 5 207.17 11.29 0 8 -6 494.77 18.49 0 8 6 490.28 18.65 0 8 7 10.76 3.59 0 8 -7 4.22 2.54 0 8 8 205.56 13.01 0 8 -8 193.05 12.19 0 8 9 27.88 5.73 0 8 -9 24.75 5.14 0 8 10 39.59 6.36 0 8 -10 35.82 5.97 0 8 11 870.57 30.40 0 8 -11 842.62 26.97 0 8 -12 126.31 10.54 0 8 12 117.83 11.69 0 8 13 19.60 5.55 0 8 -13 18.46 5.04 0 8 14 92.19 11.30 0 8 -14 81.13 9.09 0 8 15 12.19 4.47 0 8 16 8.15 4.17 0 8 17 48.47 9.33 0 8 17 52.94 5.36 0 8 -17 47.75 5.45 0 8 17 54.48 5.54 0 8 -18 3.55 2.38 0 8 18 2.20 3.55 0 8 18 3.24 2.07 0 8 -19 14.34 3.47 0 8 19 31.24 7.77 0 8 19 22.01 4.04 0 8 19 25.04 3.94 0 8 20 125.45 8.64 0 8 20 112.44 7.52 0 8 21 60.04 5.66 0 8 22 70.11 5.98 0 -8 -22 64.24 5.34 0 -8 -23 4.96 2.12 0 8 23 8.28 2.74 0 -8 -24 21.65 3.15 0 8 24 19.64 3.22 0 8 25 166.32 8.37 0 -8 -25 148.37 7.55 0 8 26 16.37 2.93 0 -8 -26 13.32 2.67 0 8 27 15.41 2.66 0 -8 -27 17.05 2.61 0 -8 -28 46.54 3.74 0 8 28 52.10 4.10 0 -8 -29 1.32 1.17 0 8 29 1.08 1.14 0 -8 -29 1.26 2.25 0 -8 -30 10.56 2.38 0 -8 -30 9.24 1.49 0 -8 -31 7.07 1.80 0 9 0 10.05 3.33 0 -9 -1 41.33 3.60 0 9 -1 37.67 5.52 0 9 1 42.24 5.71 0 9 2 504.25 18.18 0 9 -2 487.01 18.60 0 9 -3 20.46 4.57 0 9 3 18.35 3.60 0 9 3 18.85 3.95 0 9 -4 391.72 17.03 0 9 4 401.10 16.43 0 9 4 402.15 16.37 0 9 -5 54.01 6.93 0 9 5 69.21 7.32 0 9 -6 76.49 8.13 0 9 6 81.26 8.18 0 9 -7 66.41 7.32 0 9 7 56.45 6.96 0 9 8 76.20 8.40 0 9 -8 73.78 8.17 0 9 -9 411.00 18.96 0 9 9 432.20 20.68 0 9 -10 1036.50 30.61 0 9 10 1030.25 33.10 0 9 -11 262.03 15.96 0 9 11 281.20 18.20 0 9 -12 347.06 18.69 0 9 12 397.55 22.37 0 9 13 91.06 11.00 0 9 -13 84.28 9.38 0 9 -14 28.70 5.59 0 9 14 37.50 7.21 0 9 15 29.22 6.90 0 9 16 108.09 7.57 0 9 16 94.98 12.22 0 9 -16 121.41 8.60 0 9 17 118.18 14.25 0 9 17 111.27 7.16 0 9 17 119.33 8.18 0 9 -17 98.34 8.16 0 9 18 22.36 7.01 0 9 18 22.19 4.07 0 9 -18 13.95 3.58 0 9 18 24.42 3.91 0 9 19 61.95 6.02 0 9 19 55.99 10.27 0 9 19 64.40 5.74 0 9 20 48.14 5.04 0 9 20 61.27 5.81 0 -9 -21 6.10 2.20 0 9 21 8.91 2.75 0 9 22 73.71 6.23 0 -9 -22 69.64 5.18 0 -9 -23 0.19 1.63 0 9 23 3.19 1.87 0 9 24 57.66 5.18 0 -9 -24 50.38 4.38 0 -9 -25 3.24 1.75 0 9 25 5.94 2.17 0 9 26 17.73 2.92 0 -9 -26 14.55 2.47 0 9 27 1.44 1.48 0 -9 -27 1.45 1.32 0 9 -27 -1.08 1.54 0 9 28 35.36 3.40 0 -9 -28 35.25 2.83 0 9 29 4.18 1.42 0 -9 -29 2.96 1.24 0 -9 -29 0.28 1.94 0 -9 -30 22.89 2.68 0 10 0 242.86 13.87 0 10 1 52.92 6.87 0 10 -1 51.84 6.72 0 10 -2 35.44 5.76 0 10 2 35.29 5.47 0 10 3 45.70 5.91 0 10 -3 40.59 6.14 0 10 -4 54.50 6.96 0 10 4 55.75 6.49 0 10 4 54.14 6.82 0 10 5 106.44 9.07 0 10 -5 99.26 9.41 0 10 -6 244.06 14.85 0 10 6 255.32 14.90 0 10 7 24.18 5.14 0 10 -7 17.65 4.58 0 10 -8 309.84 17.17 0 10 8 327.59 18.14 0 10 9 158.77 13.01 0 10 -9 160.44 12.63 0 10 10 41.47 7.24 0 10 -10 42.66 7.16 0 10 11 48.19 8.16 0 10 -11 43.33 6.91 0 10 12 26.70 6.21 0 10 -12 22.46 5.31 0 10 13 18.86 5.67 0 10 -13 13.37 3.82 0 10 14 74.41 10.59 0 10 15 131.44 8.35 0 10 -15 133.31 8.91 0 10 15 124.46 14.32 0 10 15 125.67 7.54 0 10 16 72.83 6.21 0 10 16 72.23 11.10 0 10 16 76.07 6.52 0 10 -16 71.97 7.17 0 10 17 23.02 4.13 0 10 17 18.33 3.72 0 10 -17 30.49 4.93 0 10 17 17.05 6.19 0 10 18 332.39 12.68 0 10 18 328.88 24.39 0 10 18 366.68 14.13 0 10 19 34.96 5.24 0 10 19 38.04 4.51 0 10 20 69.93 6.14 0 10 21 3.30 2.16 0 10 22 14.73 3.39 0 10 23 106.68 7.00 0 10 24 12.78 2.73 0 10 25 5.60 2.16 0 10 -26 101.62 5.94 0 10 26 121.82 6.40 0 10 27 9.12 2.13 0 10 -27 12.77 2.28 0 10 28 4.85 1.55 0 10 -28 1.03 1.23 0 -10 -29 20.83 2.85 0 10 -30 6.68 1.54 0 -10 -30 7.69 1.81 0 11 0 2.36 2.74 0 11 1 452.20 19.46 0 11 -1 450.39 19.82 0 11 2 39.76 6.30 0 11 -2 39.25 6.33 0 11 -3 39.09 6.36 0 11 3 31.58 5.53 0 11 4 6.97 3.06 0 11 -4 8.81 4.02 0 11 5 176.69 12.22 0 11 -5 174.56 13.15 0 11 6 18.09 4.39 0 11 -6 14.46 4.00 0 11 7 465.74 21.81 0 11 -7 467.07 21.94 0 11 -8 8.19 3.36 0 11 8 6.72 2.94 0 11 -9 193.00 14.65 0 11 9 203.41 15.61 0 11 -10 69.80 9.26 0 11 10 76.48 10.27 0 11 -11 33.44 6.46 0 11 11 32.20 6.95 0 11 -12 95.18 10.85 0 11 12 108.08 12.70 0 11 13 171.23 16.25 0 11 -13 180.26 10.62 0 11 -14 148.54 10.37 0 11 14 149.48 8.71 0 11 14 145.24 7.23 0 11 14 143.64 15.40 0 11 14 172.01 9.72 0 11 14 139.27 7.81 0 11 15 58.70 5.94 0 11 -15 63.49 7.14 0 11 15 53.58 9.74 0 11 15 54.04 5.10 0 11 -16 5.57 3.00 0 11 16 7.42 2.39 0 11 16 8.96 5.31 0 11 16 10.07 2.96 0 11 17 6.11 4.50 0 11 17 4.59 2.25 0 11 17 6.25 2.35 0 11 18 5.36 2.48 0 11 19 271.60 11.19 0 11 20 30.33 4.35 0 11 21 5.13 2.30 0 11 22 4.26 2.08 0 11 23 2.70 1.93 0 11 24 38.03 4.36 0 11 25 77.00 5.23 0 11 -25 80.43 5.78 0 11 26 6.24 1.88 0 11 -26 9.60 2.40 0 11 27 27.92 2.91 0 11 -27 17.71 2.49 0 -11 -28 3.03 1.90 0 -11 -29 4.05 1.44 0 12 0 39.43 6.08 0 12 -1 17.47 4.66 0 12 1 14.86 4.61 0 12 2 6.42 2.71 0 12 -2 9.96 3.81 0 12 -3 286.75 17.08 0 12 3 275.87 16.51 0 12 -4 79.01 9.07 0 12 -5 20.16 5.18 0 12 -6 14.76 4.95 0 12 -7 5.75 3.26 0 12 7 9.42 3.86 0 12 8 14.31 4.46 0 12 -8 17.06 4.91 0 12 -9 366.91 20.98 0 12 9 375.25 21.78 0 12 10 58.74 9.18 0 12 -10 50.56 8.52 0 12 -11 206.18 15.98 0 12 11 214.84 17.75 0 12 -11 237.80 12.06 0 12 -12 8.05 2.91 0 12 12 5.84 2.50 0 12 12 5.29 3.30 0 12 12 7.89 2.36 0 12 -12 9.43 3.32 0 12 13 4.20 2.17 0 12 13 6.56 5.04 0 12 13 4.26 1.98 0 12 -13 2.79 2.89 0 12 13 1.12 2.41 0 12 13 5.74 2.44 0 12 14 65.95 5.55 0 12 14 79.75 6.54 0 12 14 69.74 11.55 0 12 14 69.74 5.43 0 12 15 8.63 2.94 0 12 15 7.71 2.51 0 12 15 16.37 6.20 0 12 16 2.67 1.84 0 12 16 1.82 2.21 0 12 17 307.12 11.98 0 12 18 25.79 3.92 0 12 19 9.59 2.69 0 12 20 39.29 4.60 0 12 21 57.58 5.29 0 12 22 19.59 3.25 0 12 23 29.39 3.70 0 12 -23 20.30 3.63 0 12 -24 3.20 2.48 0 12 24 0.78 1.70 0 12 25 49.18 4.17 0 12 -25 32.50 3.53 0 12 26 8.28 1.87 0 12 -26 7.83 2.11 0 12 -27 4.78 1.50 0 -12 -27 5.02 1.96 0 -12 -28 1.52 1.53 0 13 0 9.16 4.08 0 13 1 24.21 5.56 0 13 -1 25.02 5.17 0 13 2 61.30 8.08 0 13 -2 68.65 8.84 0 13 -3 10.89 4.35 0 13 3 9.19 4.07 0 13 -4 163.21 14.07 0 13 -5 125.16 12.20 0 13 -6 40.55 7.52 0 13 -7 106.29 11.60 0 13 -8 40.51 7.44 0 13 9 212.01 8.32 0 13 -9 204.79 9.67 0 13 -9 204.89 16.64 0 13 10 202.25 17.00 0 13 10 244.72 9.04 0 13 -10 213.88 16.79 0 13 11 19.01 2.92 0 13 -11 16.73 5.23 0 13 11 16.58 5.48 0 13 11 23.50 4.11 0 13 12 11.20 2.66 0 13 12 7.49 2.65 0 13 12 8.66 2.65 0 13 12 3.47 3.19 0 13 12 10.71 2.44 0 13 13 19.46 6.03 0 13 13 23.64 3.28 0 13 13 26.17 3.98 0 13 13 29.35 3.74 0 13 14 38.16 8.35 0 13 14 43.11 4.61 0 13 15 22.25 3.69 0 13 16 141.05 8.04 0 13 17 2.77 2.15 0 13 18 90.74 6.53 0 13 19 4.41 2.14 0 13 -20 25.80 3.30 0 13 20 18.97 3.27 0 13 -20 26.04 4.19 0 13 -21 6.42 1.83 0 13 21 5.16 2.04 0 13 -21 2.72 2.28 0 13 22 2.29 1.70 0 13 -22 2.38 2.37 0 13 23 12.35 2.40 0 13 -23 4.36 2.52 0 13 -24 52.22 4.76 0 13 24 48.72 4.13 0 13 25 14.40 2.28 0 13 -25 9.36 2.27 0 13 -26 9.67 1.96 0 -13 -26 8.44 2.26 0 -13 -27 14.82 2.23 0 13 -27 18.21 2.01 0 13 -28 5.27 1.49 0 14 0 252.24 17.02 0 14 1 0.26 2.72 0 14 -1 0.16 3.20 0 14 2 118.01 11.92 0 14 -2 121.09 12.08 0 14 -3 21.44 5.70 0 14 -4 63.38 9.42 0 14 -5 21.26 5.58 0 14 -6 43.07 4.97 0 14 -6 38.90 7.50 0 14 6 42.42 4.11 0 14 -6 43.94 4.60 0 14 -7 18.65 4.97 0 14 7 23.44 3.07 0 14 7 22.17 3.21 0 14 -7 18.69 3.32 0 14 -7 19.68 3.93 0 14 -8 143.71 14.25 0 14 -8 157.05 8.98 0 14 8 168.78 7.35 0 14 -8 137.92 7.56 0 14 8 162.56 7.47 0 14 8 119.68 7.40 0 14 9 10.81 2.61 0 14 -9 11.72 5.32 0 14 9 4.78 2.23 0 14 9 8.43 2.42 0 14 -9 11.63 3.23 0 14 -9 6.26 2.58 0 14 -10 7.35 2.58 0 14 -10 4.13 3.22 0 14 10 -2.44 3.42 0 14 10 4.38 2.09 0 14 10 4.90 2.18 0 14 11 15.10 3.15 0 14 -11 10.42 2.56 0 14 -11 17.88 3.97 0 14 -12 115.92 8.55 0 14 12 106.51 6.70 0 14 -12 111.49 6.31 0 14 13 10.00 2.57 0 14 -13 9.01 3.00 0 14 13 7.98 2.29 0 14 -13 7.76 2.49 0 14 -14 46.30 6.11 0 14 14 61.19 5.52 0 14 15 15.00 3.01 0 14 -15 17.08 3.75 0 14 -16 16.41 3.61 0 14 16 21.87 3.25 0 14 -17 36.18 4.27 0 14 -17 42.64 5.64 0 14 18 74.97 5.71 0 14 -18 76.51 5.69 0 14 -18 81.65 6.79 0 14 -19 -0.98 2.09 0 14 19 1.19 1.81 0 14 -19 -1.77 2.69 0 14 -20 34.24 3.73 0 14 -20 36.48 4.68 0 14 20 32.11 3.74 0 14 21 6.80 2.22 0 14 -21 2.86 1.82 0 14 -21 5.80 2.47 0 14 22 4.41 1.81 0 14 -22 4.53 2.45 0 14 23 2.75 1.68 0 14 -23 0.59 1.84 0 14 -24 5.50 2.21 0 14 -25 6.71 1.82 0 -14 -25 7.06 1.94 0 -14 -26 13.38 2.00 0 14 -26 20.16 2.21 0 14 -26 18.39 2.39 0 14 -27 0.14 1.19 0 15 0 -2.29 3.12 0 15 0 0.70 1.95 0 15 0 0.64 1.77 0 15 0 1.46 3.45 0 15 0 0.16 1.77 0 15 1 158.17 8.49 0 15 -1 135.45 6.93 0 15 -1 151.81 7.52 0 15 1 160.58 7.54 0 15 1 160.29 7.89 0 15 -1 158.68 7.63 0 15 -1 150.38 13.91 0 15 1 146.96 7.19 0 15 -1 144.74 8.85 0 15 1 138.92 13.37 0 15 2 39.99 4.69 0 15 2 50.44 4.38 0 15 -2 44.58 4.51 0 15 2 49.83 4.34 0 15 2 44.73 4.28 0 15 -2 50.18 4.38 0 15 -2 51.95 4.95 0 15 -2 49.59 5.11 0 15 -2 47.83 7.82 0 15 -2 53.84 5.20 0 15 -3 60.07 5.02 0 15 -3 58.61 4.69 0 15 3 67.87 5.04 0 15 3 66.65 4.89 0 15 3 58.87 5.14 0 15 3 65.69 5.09 0 15 -3 69.41 5.95 0 15 -3 68.13 5.63 0 15 -3 59.76 9.10 0 15 3 73.96 4.99 0 15 4 122.68 6.78 0 15 4 120.55 6.59 0 15 -4 112.10 12.63 0 15 4 89.42 5.85 0 15 -4 105.57 6.71 0 15 4 80.23 6.37 0 15 4 93.05 5.70 0 15 -4 107.19 5.94 0 15 -4 95.74 6.09 0 15 -4 95.47 7.07 0 15 -5 43.36 4.82 0 15 5 61.39 4.79 0 15 -5 37.91 7.56 0 15 -5 66.51 5.22 0 15 5 45.89 5.41 0 15 -5 66.72 5.86 0 15 5 47.80 4.36 0 15 5 57.51 4.65 0 15 6 56.83 5.56 0 15 -6 59.69 9.43 0 15 -6 79.28 6.45 0 15 6 75.68 5.39 0 15 -6 76.09 5.75 0 15 6 70.13 5.17 0 15 6 72.64 5.23 0 15 7 8.12 2.19 0 15 7 5.93 2.22 0 15 7 11.50 2.66 0 15 -7 14.32 5.41 0 15 -7 10.96 3.49 0 15 7 11.40 2.63 0 15 -7 9.09 2.49 0 15 -7 6.98 2.60 0 15 -8 4.37 2.59 0 15 8 1.78 2.13 0 15 8 1.05 2.12 0 15 -8 4.59 3.87 0 15 -8 -0.37 2.06 0 15 8 4.00 2.08 0 15 8 1.34 1.88 0 15 -8 2.32 2.17 0 15 9 6.84 2.28 0 15 9 3.60 2.11 0 15 -9 8.71 2.69 0 15 9 4.45 2.80 0 15 -9 6.28 2.58 0 15 -9 6.18 2.83 0 15 -10 14.98 4.21 0 15 -10 9.10 2.60 0 15 -10 19.24 3.61 0 15 10 21.94 3.25 0 15 10 22.11 3.49 0 15 10 11.94 2.98 0 15 -11 108.13 6.47 0 15 11 130.26 7.13 0 15 -11 129.38 7.58 0 15 -11 130.46 8.68 0 15 12 120.79 6.84 0 15 -12 103.50 8.40 0 15 -12 104.80 6.20 0 15 -12 103.53 7.32 0 15 -13 65.95 5.10 0 15 -13 70.22 6.54 0 15 -13 62.96 5.52 0 15 13 61.29 5.08 0 15 -14 55.32 5.37 0 15 -14 54.10 6.26 0 15 -14 47.38 4.07 0 15 -15 4.52 2.57 0 15 15 0.43 1.66 0 15 -15 6.36 3.34 0 15 16 23.70 3.47 0 15 -16 22.19 4.24 0 15 -16 21.74 3.70 0 15 -17 1.08 2.47 0 15 -17 3.92 2.44 0 15 17 0.72 1.80 0 15 -18 32.94 3.93 0 15 -18 29.70 4.48 0 15 -19 104.83 6.17 0 15 19 103.91 6.25 0 15 -20 10.80 2.29 0 15 -20 13.11 3.22 0 15 20 14.22 2.55 0 15 -21 0.73 1.42 0 15 21 2.37 1.57 0 15 -21 0.06 1.99 0 15 -22 2.55 1.94 0 15 -23 12.40 2.49 0 15 -24 4.47 1.62 0 15 -25 0.80 1.48 0 15 -25 -0.38 1.22 0 15 -26 0.56 0.93 0 16 0 38.47 5.01 0 16 0 39.06 4.19 0 16 0 31.81 3.88 0 16 0 38.35 4.00 0 16 -1 5.07 1.79 0 16 1 12.42 2.54 0 16 -1 6.53 2.60 0 16 -1 12.37 4.75 0 16 1 6.50 2.71 0 16 1 6.45 2.99 0 16 1 7.81 2.62 0 16 -1 6.37 3.47 0 16 -1 10.17 2.85 0 16 2 8.84 3.47 0 16 -2 5.39 3.53 0 16 2 6.77 2.35 0 16 -2 11.80 3.09 0 16 2 8.85 2.74 0 16 2 4.25 1.81 0 16 -2 8.13 2.53 0 16 -2 7.19 2.03 0 16 2 8.65 2.22 0 16 -3 235.16 9.22 0 16 -3 261.78 10.11 0 16 -3 255.45 10.10 0 16 -3 266.44 11.69 0 16 3 255.64 10.19 0 16 3 247.81 9.75 0 16 -3 228.10 18.23 0 16 3 215.65 10.55 0 16 3 261.00 9.99 0 16 3 247.61 9.58 0 16 -4 5.81 2.96 0 16 4 7.53 2.42 0 16 -4 4.15 1.78 0 16 -4 3.62 2.24 0 16 4 6.20 2.49 0 16 -4 7.09 2.66 0 16 4 5.36 2.47 0 16 4 7.70 2.37 0 16 4 7.31 2.95 0 16 -4 6.88 2.41 0 16 5 21.62 3.35 0 16 5 26.99 3.65 0 16 -5 23.75 3.93 0 16 5 21.61 4.15 0 16 5 28.49 3.59 0 16 -5 20.36 4.37 0 16 -5 23.35 3.60 0 16 -5 27.53 7.49 0 16 -5 23.16 3.13 0 16 5 24.60 3.59 0 16 -6 7.98 4.96 0 16 6 5.18 2.06 0 16 -6 2.75 2.21 0 16 -6 5.35 2.72 0 16 6 3.96 2.32 0 16 6 4.03 1.74 0 16 6 4.38 2.25 0 16 -6 8.07 2.93 0 16 -7 1.05 2.13 0 16 7 3.11 2.28 0 16 -7 5.50 2.85 0 16 -7 0.75 3.11 0 16 7 4.85 2.29 0 16 7 5.04 2.21 0 16 -7 3.73 2.41 0 16 7 6.93 2.35 0 16 8 48.86 4.32 0 16 8 56.81 4.74 0 16 -8 47.18 5.55 0 16 -8 50.94 4.68 0 16 -8 47.11 5.01 0 16 8 32.65 4.61 0 16 8 51.70 4.61 0 16 -9 18.39 4.27 0 16 -9 12.35 3.24 0 16 9 15.33 3.31 0 16 9 14.28 2.86 0 16 9 13.71 3.10 0 16 -9 11.23 2.88 0 16 10 2.97 1.99 0 16 10 3.40 2.68 0 16 -10 3.39 2.38 0 16 -10 1.06 2.19 0 16 -10 4.60 2.74 0 16 10 7.69 2.96 0 16 -11 247.41 11.96 0 16 -11 230.78 9.58 0 16 11 252.30 9.46 0 16 -11 220.17 10.27 0 16 -12 47.83 5.31 0 16 12 58.06 5.22 0 16 -12 33.97 5.38 0 16 -12 28.87 3.86 0 16 -13 47.89 5.85 0 16 -13 50.03 4.89 0 16 -13 42.97 4.18 0 16 -14 1.99 2.63 0 16 -14 0.91 2.27 0 16 -14 -0.48 1.78 0 16 -15 18.98 3.24 0 16 -15 20.58 4.04 0 16 -16 8.60 3.05 0 16 -16 4.69 2.39 0 16 -17 159.20 7.67 0 16 -17 140.16 9.07 0 16 -18 13.46 3.79 0 16 -18 12.94 2.70 0 16 -19 12.66 2.66 0 16 -19 5.55 2.80 0 16 -20 5.83 2.68 0 16 -20 5.41 1.76 0 16 -21 -0.27 1.91 0 16 -21 -0.39 1.41 0 16 -22 0.52 1.65 0 16 -22 0.39 1.79 0 16 -23 9.97 2.14 0 16 -23 13.80 2.37 0 16 -24 0.58 1.22 0 16 -24 3.04 1.44 0 16 -25 2.88 1.08 0 17 0 0.12 2.45 0 17 0 0.57 2.20 0 17 0 -1.95 2.50 0 17 -1 82.48 5.96 0 17 -1 97.26 6.63 0 17 1 80.92 5.96 0 17 -1 99.78 6.89 0 17 1 108.34 6.79 0 17 1 110.93 6.61 0 17 1 70.30 6.56 0 17 1 74.68 5.80 0 17 -2 152.60 7.78 0 17 2 134.47 7.40 0 17 2 151.62 7.70 0 17 2 152.55 7.72 0 17 -2 130.71 7.38 0 17 -2 145.14 8.01 0 17 2 145.27 8.79 0 17 2 150.23 7.42 0 17 -3 26.82 3.84 0 17 -3 27.23 3.32 0 17 -3 29.68 3.94 0 17 3 32.68 4.10 0 17 3 16.92 3.80 0 17 3 20.86 3.05 0 17 3 23.45 3.55 0 17 3 25.44 3.48 0 17 -4 85.89 6.32 0 17 4 87.72 5.84 0 17 4 90.03 6.06 0 17 4 97.80 6.09 0 17 -4 94.92 6.60 0 17 4 76.32 6.21 0 17 4 84.59 5.81 0 17 -4 69.14 5.55 0 17 5 13.06 3.01 0 17 5 16.52 2.99 0 17 5 15.75 3.09 0 17 -5 18.09 3.33 0 17 -5 14.29 3.36 0 17 5 21.93 3.59 0 17 5 13.65 2.74 0 17 -5 16.92 3.82 0 17 -5 19.43 2.81 0 17 6 16.49 3.09 0 17 -6 16.37 3.82 0 17 -6 16.22 3.47 0 17 6 19.11 3.22 0 17 -6 15.00 3.11 0 17 6 21.23 3.48 0 17 6 15.08 3.49 0 17 7 5.04 2.41 0 17 -7 1.69 2.09 0 17 -7 0.61 2.20 0 17 7 2.71 2.20 0 17 7 3.76 2.41 0 17 -7 2.37 2.50 0 17 7 5.28 2.29 0 17 8 8.63 2.60 0 17 -8 3.06 2.19 0 17 8 3.14 2.32 0 17 -8 8.67 3.25 0 17 8 8.86 2.53 0 17 8 8.13 2.66 0 17 -8 6.55 2.91 0 17 -9 2.07 2.31 0 17 9 3.63 2.06 0 17 -9 2.84 2.30 0 17 -9 -0.21 2.42 0 17 9 0.29 2.26 0 17 9 4.05 2.03 0 17 9 4.90 2.17 0 17 -10 51.57 5.94 0 17 -10 46.96 5.09 0 17 10 45.09 4.68 0 17 -10 53.69 4.94 0 17 -11 2.57 2.48 0 17 -11 1.55 2.67 0 17 11 0.90 1.83 0 17 -11 1.79 2.40 0 17 -12 -1.21 2.49 0 17 -12 6.88 3.17 0 17 -12 1.87 2.28 0 17 -13 159.46 8.42 0 17 -13 158.44 7.43 0 17 -13 159.05 9.95 0 17 -14 20.29 3.01 0 17 -14 18.50 3.57 0 17 -14 14.56 3.79 0 17 -15 5.07 2.22 0 17 -15 0.03 2.50 0 17 -16 45.94 5.54 0 17 -16 38.59 4.17 0 17 -17 2.31 2.35 0 17 -17 -1.33 2.06 0 17 -17 4.94 2.11 0 17 -18 61.90 4.51 0 17 -18 60.89 5.50 0 17 -19 32.79 3.21 0 17 -19 31.57 4.25 0 17 -20 9.35 2.24 0 17 -20 7.77 2.31 0 17 -20 9.83 1.78 0 17 -21 8.87 2.35 0 17 -21 6.99 1.36 0 17 -21 6.35 2.02 0 17 -22 3.11 1.63 0 17 -22 1.83 1.45 0 17 -23 3.31 1.27 0 18 0 40.14 4.43 0 18 0 46.76 5.02 0 18 0 41.97 4.41 0 18 0 34.87 4.18 0 18 1 11.55 3.05 0 18 -1 5.09 2.06 0 18 -1 8.67 3.03 0 18 1 8.48 2.66 0 18 -1 8.98 2.82 0 18 1 3.00 1.96 0 18 1 4.89 2.36 0 18 2 227.04 9.31 0 18 2 229.64 9.44 0 18 2 248.37 9.70 0 18 2 215.42 8.87 0 18 -2 210.65 9.00 0 18 -2 223.68 9.88 0 18 -2 232.48 9.82 0 18 -3 14.97 3.39 0 18 3 8.86 2.52 0 18 3 14.67 3.22 0 18 3 12.19 2.70 0 18 -3 18.24 3.10 0 18 3 12.37 3.73 0 18 -3 7.13 2.72 0 18 3 4.77 2.31 0 18 4 34.67 3.93 0 18 -4 38.93 4.56 0 18 -4 27.32 3.62 0 18 4 26.85 3.58 0 18 4 35.39 4.15 0 18 -4 35.16 4.20 0 18 4 29.15 4.55 0 18 4 35.83 4.14 0 18 -5 5.42 2.78 0 18 -5 1.64 1.61 0 18 5 -2.21 2.57 0 18 5 2.09 2.73 0 18 5 0.84 1.90 0 18 5 2.19 2.27 0 18 -5 1.75 2.25 0 18 5 -0.16 2.00 0 18 6 -0.22 2.33 0 18 6 0.56 2.47 0 18 -6 3.27 2.42 0 18 -6 2.59 2.15 0 18 6 -0.68 2.37 0 18 6 -2.90 2.40 0 18 7 6.47 2.34 0 18 7 0.74 2.39 0 18 -7 4.34 2.34 0 18 7 5.48 2.39 0 18 7 5.86 2.37 0 18 -7 4.26 2.45 0 18 8 39.86 4.30 0 18 8 38.52 3.86 0 18 8 28.56 3.95 0 18 8 34.85 3.96 0 18 -8 34.13 4.57 0 18 -8 40.07 4.42 0 18 -8 37.87 5.01 0 18 9 16.47 3.23 0 18 9 13.67 2.61 0 18 -9 11.38 3.09 0 18 9 12.87 3.34 0 18 -9 12.81 3.44 0 18 -9 13.28 3.17 0 18 -10 7.58 2.92 0 18 -10 6.56 2.47 0 18 10 8.75 2.43 0 18 -10 8.02 2.80 0 18 -11 5.24 2.94 0 18 -11 6.53 2.53 0 18 -11 2.20 2.16 0 18 -12 93.84 6.42 0 18 -12 104.58 6.16 0 18 -12 96.80 7.54 0 18 -13 2.12 1.79 0 18 -13 3.17 2.22 0 18 -13 -0.38 2.38 0 18 -14 17.18 3.09 0 18 -14 19.16 2.86 0 18 -14 18.81 3.81 0 18 -15 4.10 2.39 0 18 -15 1.36 2.52 0 18 -16 2.11 1.95 0 18 -16 3.58 2.35 0 18 -17 1.52 2.06 0 18 -17 6.08 2.11 0 18 -18 13.62 2.23 0 18 -18 17.96 3.35 0 18 -19 3.80 1.92 0 18 -19 1.78 1.31 0 18 -20 45.53 2.77 0 18 -20 35.72 3.15 0 18 -21 0.47 1.20 0 18 -22 1.76 1.11 0 19 0 0.75 2.23 0 19 0 5.49 2.47 0 19 0 1.65 2.04 0 19 0 5.17 2.15 0 19 -1 6.81 2.23 0 19 1 15.16 3.13 0 19 1 7.47 2.68 0 19 -1 13.78 2.88 0 19 1 13.07 2.61 0 19 -1 12.66 3.12 0 19 -1 9.53 2.85 0 19 1 6.56 2.31 0 19 2 31.06 4.19 0 19 -2 25.15 3.77 0 19 -2 22.78 3.25 0 19 2 31.49 3.83 0 19 2 25.30 3.71 0 19 -2 25.30 3.72 0 19 -2 27.29 4.03 0 19 2 22.88 3.53 0 19 -3 1.44 1.81 0 19 3 -2.17 2.38 0 19 -3 5.12 2.70 0 19 3 2.15 1.93 0 19 -3 2.53 2.60 0 19 3 2.41 1.89 0 19 3 4.40 2.36 0 19 4 80.48 5.34 0 19 4 96.11 6.34 0 19 -4 89.53 5.53 0 19 4 113.16 6.40 0 19 -4 98.43 6.60 0 19 -4 84.47 6.33 0 19 4 100.01 6.33 0 19 5 28.17 3.77 0 19 5 35.23 3.80 0 19 5 42.73 4.26 0 19 -5 33.93 4.10 0 19 -5 35.87 4.20 0 19 6 4.40 2.06 0 19 6 2.69 2.01 0 19 -6 6.78 2.81 0 19 -6 4.65 2.20 0 19 6 2.02 1.99 0 19 -7 1.98 2.20 0 19 7 6.42 2.18 0 19 7 6.44 2.16 0 19 7 1.13 2.14 0 19 7 1.37 1.71 0 19 -7 -1.17 2.51 0 19 -8 6.29 2.73 0 19 8 8.29 2.32 0 19 -8 6.22 2.38 0 19 8 9.83 2.14 0 19 8 6.99 2.62 0 19 8 10.00 2.49 0 19 -9 5.70 1.91 0 19 -9 9.98 2.88 0 19 9 9.21 2.29 0 19 -9 10.73 2.85 0 19 -10 7.44 2.63 0 19 -10 12.30 2.88 0 19 -10 11.51 2.43 0 19 -11 -1.15 2.09 0 19 -11 1.35 1.62 0 19 -11 3.47 2.03 0 19 -12 9.98 2.23 0 19 -12 9.22 2.52 0 19 -12 5.67 2.16 0 19 -13 6.14 2.07 0 19 -13 9.19 2.37 0 19 -14 38.01 3.34 0 19 -14 30.62 3.23 0 19 -15 -1.14 1.72 0 19 -15 -1.11 1.71 0 19 -16 23.80 2.82 0 19 -16 14.55 2.31 0 19 -17 0.94 1.38 0 19 -17 1.94 1.71 0 19 -18 20.93 2.23 0 19 -18 19.65 2.37 0 19 -19 9.18 1.54 0 19 -19 7.25 1.60 0 19 -20 12.06 1.71 0 20 0 74.02 5.31 0 20 0 87.22 5.65 0 20 0 88.28 6.15 0 20 1 9.95 2.41 0 20 -1 16.77 2.99 0 20 -1 11.46 2.62 0 20 -1 16.92 3.17 0 20 1 15.65 2.96 0 20 1 12.22 2.57 0 20 -1 13.23 2.97 0 20 1 16.08 2.99 0 20 -2 8.35 2.11 0 20 2 0.74 2.06 0 20 -2 2.20 2.35 0 20 2 5.86 2.05 0 20 -2 6.91 2.50 0 20 2 8.70 2.31 0 20 2 3.51 2.13 0 20 -2 4.57 2.48 0 20 3 115.81 6.30 0 20 3 96.10 6.15 0 20 -3 91.93 5.57 0 20 3 105.27 6.53 0 20 -3 86.41 6.19 0 20 -3 106.79 6.54 0 20 3 92.86 5.42 0 20 -3 114.61 6.57 0 20 -4 -0.75 2.16 0 20 -4 3.34 2.13 0 20 4 6.23 2.32 0 20 -4 0.68 1.55 0 20 -4 5.93 2.65 0 20 4 -0.24 2.02 0 20 4 4.16 2.32 0 20 5 1.96 2.02 0 20 5 2.92 1.99 0 20 -5 1.21 2.21 0 20 -5 0.43 2.21 0 20 5 1.59 1.91 0 20 6 2.49 2.14 0 20 6 2.72 1.90 0 20 6 -0.19 2.03 0 20 -6 2.36 2.26 0 20 -6 -0.64 2.52 0 20 7 3.93 2.01 0 20 -7 1.39 2.15 0 20 -7 4.62 2.22 0 20 7 0.28 1.78 0 20 -8 2.90 2.09 0 20 -8 -0.27 2.13 0 20 -9 16.71 2.81 0 20 -9 11.83 2.53 0 20 -10 34.52 3.79 0 20 -10 30.96 3.61 0 20 -11 53.15 4.41 0 20 -11 57.54 4.64 0 20 -12 2.01 1.86 0 20 -12 6.59 2.29 0 20 -12 5.40 1.81 0 20 -13 9.86 1.93 0 20 -13 8.95 2.22 0 20 -13 6.07 1.69 0 20 -14 9.06 1.90 0 20 -14 10.14 2.20 0 20 -14 9.76 1.94 0 20 -15 5.40 1.70 0 20 -15 5.24 1.61 0 20 -16 -1.40 1.38 0 20 -16 -0.30 1.27 0 20 -17 30.51 2.45 0 20 -17 36.36 2.65 0 20 -18 0.57 0.96 0 20 -18 0.56 0.98 0 21 0 -3.93 2.23 0 21 0 -4.60 2.34 0 21 0 -2.47 2.57 0 21 0 -0.32 1.72 0 21 -1 41.44 4.31 0 21 1 46.74 4.41 0 21 1 35.01 3.75 0 21 -1 33.77 3.48 0 21 -1 39.98 4.00 0 21 1 33.01 3.62 0 21 -1 34.05 3.34 0 21 1 32.18 3.35 0 21 -2 2.95 2.03 0 21 -2 5.31 1.85 0 21 2 0.22 1.87 0 21 2 4.03 2.22 0 21 -2 2.80 1.98 0 21 -2 3.72 2.31 0 21 2 5.55 2.06 0 21 2 6.07 2.27 0 21 3 5.44 2.05 0 21 -3 5.22 2.17 0 21 -3 6.35 2.48 0 21 3 1.88 2.10 0 21 -3 1.95 1.48 0 21 -3 2.13 2.33 0 21 3 5.97 2.02 0 21 -4 9.16 2.62 0 21 -4 3.87 1.96 0 21 4 4.82 2.02 0 21 4 5.43 2.03 0 21 4 8.14 2.18 0 21 -4 10.54 2.76 0 21 -5 11.82 2.63 0 21 -5 15.93 2.96 0 21 5 18.49 2.73 0 21 5 17.50 2.76 0 21 5 10.67 2.45 0 21 -5 17.64 3.00 0 21 6 22.21 2.94 0 21 -6 15.62 2.84 0 21 -6 18.57 3.21 0 21 -6 15.80 3.09 0 21 -7 15.34 2.89 0 21 -7 16.25 2.90 0 21 -7 10.76 2.51 0 21 -8 1.12 2.04 0 21 -8 3.38 1.82 0 21 -8 4.17 2.17 0 21 -9 5.51 1.94 0 21 -9 6.35 2.30 0 21 -9 2.02 1.82 0 21 -10 24.54 2.97 0 21 -10 28.07 3.13 0 21 -11 20.01 2.71 0 21 -11 24.46 3.01 0 21 -12 5.68 1.75 0 21 -12 7.94 1.97 0 21 -13 10.70 1.96 0 21 -13 7.55 1.88 0 21 -14 4.52 1.53 0 21 -15 4.78 1.48 0 21 -16 2.47 1.17 0 21 -16 1.32 1.35 0 21 -17 -1.24 1.26 0 22 0 3.61 1.61 0 22 0 0.94 1.90 0 22 0 0.81 1.94 0 22 0 2.45 1.53 0 22 -1 11.87 2.64 0 22 1 18.62 2.90 0 22 1 13.86 2.14 0 22 -1 15.81 2.73 0 22 -1 13.50 2.21 0 22 1 15.61 2.49 0 22 1 13.15 2.26 0 22 -1 7.28 1.78 0 22 -2 22.95 3.26 0 22 -2 16.88 2.58 0 22 2 25.95 3.21 0 22 2 23.08 2.90 0 22 -2 25.18 2.64 0 22 -2 22.07 2.91 0 22 3 8.88 2.06 0 22 -3 1.91 1.63 0 22 -3 6.40 2.37 0 22 3 9.39 2.49 0 22 -3 9.99 2.38 0 22 -4 21.19 3.16 0 22 4 18.78 2.82 0 22 -4 15.96 2.65 0 22 -4 15.75 2.57 0 22 4 15.27 2.43 0 22 -5 8.26 2.20 0 22 -5 4.57 1.97 0 22 -5 7.12 2.24 0 22 -6 14.69 2.55 0 22 -6 13.99 2.54 0 22 -6 16.72 2.87 0 22 -7 1.02 1.71 0 22 -7 0.73 1.60 0 22 -7 5.05 2.11 0 22 -8 21.41 2.94 0 22 -8 23.93 2.98 0 22 -8 21.89 2.97 0 22 -9 8.41 1.97 0 22 -9 4.68 1.81 0 22 -9 7.00 2.00 0 22 -10 2.21 1.69 0 22 -10 0.68 1.51 0 22 -11 3.32 1.49 0 22 -11 4.65 1.78 0 22 -11 -0.05 1.41 0 22 -12 16.88 2.12 0 22 -12 13.09 2.09 0 22 -13 3.34 1.38 0 22 -13 3.56 1.30 0 22 -14 3.76 1.15 0 22 -14 2.90 1.26 0 23 0 -1.15 1.87 0 23 0 -1.84 1.62 0 23 -1 6.06 2.14 0 23 1 2.44 1.65 0 23 1 2.58 1.99 0 23 -1 2.03 1.43 0 23 -2 20.03 2.54 0 23 -2 21.23 2.81 0 23 -3 -0.13 1.27 0 23 -3 1.09 1.74 0 23 -3 0.08 1.52 0 23 -4 2.23 1.49 0 23 -4 2.25 1.41 0 23 -4 6.12 1.93 0 23 -5 12.32 2.14 0 23 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3.15 1 13 16 18.01 3.59 -1 13 -16 9.86 3.93 -1 13 -17 6.34 2.78 -1 13 -17 0.36 2.21 1 13 17 8.85 2.49 -1 13 -18 17.87 3.66 1 13 18 12.09 3.08 -1 13 -18 15.51 2.68 -1 13 -19 13.79 2.73 -1 13 -19 10.39 3.38 1 13 20 5.51 2.20 -1 13 -20 12.96 3.31 -1 13 -21 13.13 3.49 1 13 21 8.50 2.42 -1 13 -22 104.96 6.74 1 13 22 95.12 5.99 1 13 23 125.59 6.69 -1 13 -23 88.89 5.93 -1 13 -24 44.78 3.95 -1 13 -25 7.58 1.84 -1 -13 -25 3.96 1.81 -1 13 -26 28.42 2.39 -1 -13 -26 24.17 2.73 -1 13 -26 24.62 3.10 -1 13 -27 0.77 1.38 -1 13 -27 -1.09 0.98 1 14 -27 1.25 1.08 1 14 -27 2.68 1.34 1 14 -26 3.77 1.63 1 -14 -26 2.09 1.59 -1 14 25 16.06 2.22 1 14 -25 15.00 2.49 1 14 -24 3.06 1.97 -1 14 24 1.92 1.39 1 14 -23 13.03 2.96 1 14 -23 10.94 1.99 -1 14 23 18.31 2.60 -1 14 22 124.82 6.71 1 14 -22 120.69 7.80 1 14 -22 120.44 5.95 -1 14 21 19.02 2.89 1 14 -21 25.43 3.25 1 14 -21 24.76 3.79 1 14 -20 12.42 3.47 -1 14 20 5.46 1.94 1 14 -19 64.52 6.23 -1 14 19 42.91 4.25 -1 14 18 105.43 6.69 1 14 -18 95.24 7.53 -1 14 17 3.85 2.11 -1 14 16 40.61 4.41 -1 14 15 1.87 2.03 -1 14 14 43.99 4.57 -1 14 14 43.49 4.65 -1 14 14 34.02 4.14 -1 14 14 41.11 5.08 -1 14 13 31.82 5.11 -1 -14 13 42.48 9.24 -1 14 13 56.97 4.75 1 14 -12 194.13 10.58 -1 -14 12 178.34 17.18 -1 14 12 201.06 8.44 -1 14 12 198.64 10.94 1 14 -11 4.20 2.58 -1 -14 11 7.46 4.73 -1 14 11 9.52 2.57 -1 14 11 5.67 2.36 -1 14 10 4.63 2.49 1 14 -10 4.38 2.67 -1 14 10 4.93 2.60 -1 14 10 6.46 2.23 1 14 -9 21.44 4.04 -1 14 9 18.35 3.13 -1 14 9 24.06 3.42 1 14 -9 14.83 4.93 -1 14 9 19.87 3.03 -1 14 8 23.69 3.00 1 14 -8 18.33 4.32 1 14 -8 27.89 4.19 -1 14 8 27.03 3.38 -1 14 8 24.62 3.36 1 14 -7 7.26 2.73 -1 14 7 11.97 2.40 1 14 -7 7.96 3.79 -1 14 7 9.56 2.44 1 14 -6 7.15 2.80 1 14 -6 4.99 3.48 -1 14 6 7.33 2.00 1 14 -6 2.85 1.99 1 14 -5 12.01 4.31 -1 14 4 224.55 16.31 1 14 -4 203.67 15.74 1 14 -3 3.42 2.52 -1 14 3 -1.97 3.32 -1 14 2 152.92 13.72 1 14 -2 139.31 12.97 -1 14 1 11.23 4.49 1 14 -1 11.49 4.03 -1 14 0 24.18 6.25 -1 14 -1 60.04 9.05 -1 14 -2 379.14 22.28 -1 14 -3 82.73 10.85 -1 14 -4 43.43 8.15 -1 14 -5 5.48 2.28 -1 14 -5 8.13 3.82 1 14 5 6.51 2.04 -1 14 -5 6.88 2.68 -1 14 -5 9.03 2.44 1 14 6 34.54 3.67 -1 14 -6 30.66 7.17 -1 14 -6 27.01 3.28 -1 14 -6 33.70 3.75 -1 14 -6 36.82 4.90 1 14 7 4.19 1.85 -1 14 -7 4.33 1.85 -1 14 -7 9.06 5.39 -1 14 -7 4.79 2.14 1 14 7 4.87 2.65 -1 14 -7 3.59 2.59 -1 14 -8 141.94 14.86 1 14 8 151.43 7.54 -1 14 -8 146.54 7.68 1 14 8 117.12 7.88 -1 14 -8 147.08 7.09 -1 14 -8 150.32 9.04 1 14 9 10.09 2.59 -1 14 -9 6.63 2.84 -1 14 -9 7.79 2.83 -1 14 -9 6.44 2.45 1 14 9 5.50 2.70 -1 14 -9 11.71 5.56 -1 14 -10 122.20 7.16 -1 14 -10 117.79 8.40 1 14 10 101.34 7.31 1 14 10 138.54 7.05 -1 14 -10 106.80 6.56 -1 14 -10 108.29 13.23 1 14 11 4.86 2.25 -1 14 -11 1.62 1.98 -1 14 -11 4.81 2.91 -1 14 -11 1.44 2.19 1 14 11 0.20 2.36 -1 14 -11 7.62 4.52 1 14 12 48.18 4.67 -1 14 -12 29.55 3.71 1 14 12 20.23 3.35 1 14 12 38.76 4.38 -1 14 -12 32.30 4.42 -1 14 -12 27.89 4.78 1 14 13 54.25 5.47 1 14 13 48.04 4.66 -1 14 -13 56.58 5.21 -1 14 -14 13.97 2.98 -1 14 -14 17.39 4.09 1 14 14 14.07 2.86 1 14 14 10.95 3.11 -1 14 -15 19.19 4.02 1 14 15 13.02 2.96 -1 14 -15 13.58 3.22 1 14 16 206.03 9.58 -1 14 -16 213.35 8.92 -1 14 -16 204.80 11.09 -1 14 -17 -2.23 2.26 1 14 17 -1.25 1.80 -1 14 -17 2.01 2.45 -1 14 -18 72.25 7.00 1 14 18 88.32 6.28 -1 14 -18 74.10 5.30 -1 14 -19 7.92 2.91 -1 14 -19 7.97 2.24 -1 14 -20 9.80 3.34 1 14 20 12.90 2.75 -1 14 -21 16.23 3.24 1 14 21 9.75 2.14 -1 14 -22 38.05 4.15 -1 -14 -23 4.41 2.16 -1 14 -23 3.92 1.96 -1 14 -24 34.67 3.28 -1 -14 -24 29.93 2.92 -1 14 -25 1.41 1.65 -1 -14 -25 1.72 1.49 -1 14 -25 1.68 1.37 -1 14 -26 3.62 1.52 -1 14 -26 4.26 1.23 1 15 -26 4.22 1.38 1 15 -26 4.53 1.37 1 15 -25 16.34 2.29 1 15 -24 8.62 2.11 1 15 -23 9.13 2.62 1 15 -23 11.95 1.91 -1 15 23 7.79 1.80 -1 15 22 3.46 1.76 1 15 -22 5.28 2.27 1 15 -22 4.95 1.68 1 15 -21 47.96 5.21 1 15 -21 46.61 4.00 1 15 -20 36.30 4.96 1 15 -20 42.50 4.23 1 15 -19 46.35 5.31 1 15 -19 50.36 4.71 -1 15 19 50.87 4.35 1 15 -18 15.82 3.90 1 15 -18 23.80 3.72 -1 15 18 23.26 3.31 1 15 -17 13.73 3.15 -1 15 17 11.96 2.44 1 15 -17 14.81 3.87 1 15 -16 6.74 3.44 -1 15 16 4.60 1.84 1 15 -15 61.09 6.55 1 15 -15 63.99 4.74 1 15 -14 132.15 9.30 1 15 -14 126.82 6.87 -1 15 13 4.58 2.27 1 15 -13 2.60 3.11 1 15 -13 3.09 2.20 -1 15 13 5.55 3.26 1 15 -12 8.17 3.24 -1 15 12 7.61 2.84 -1 15 12 3.22 1.98 1 15 -11 72.34 6.66 -1 15 11 81.29 5.43 -1 15 11 67.31 6.47 1 15 -10 1.92 2.65 -1 15 10 4.23 2.31 -1 15 10 4.50 2.31 1 15 -10 7.10 2.74 -1 15 9 66.68 4.95 -1 15 9 67.60 5.28 1 15 -9 69.38 6.45 1 15 -9 70.52 5.87 -1 15 9 69.94 5.29 -1 15 9 82.85 5.78 -1 15 8 11.23 2.49 -1 15 8 7.25 2.51 1 15 -8 7.77 2.79 -1 15 8 5.70 2.54 1 15 -8 5.08 3.51 -1 15 8 9.57 2.51 1 15 -8 6.05 2.65 1 15 -7 28.59 4.21 -1 15 7 22.46 3.17 -1 15 7 26.95 3.62 1 15 -7 20.08 3.60 -1 15 7 19.53 2.97 -1 15 7 19.88 3.27 1 15 -6 82.46 11.06 -1 15 6 55.61 5.10 1 15 -6 75.92 6.29 -1 15 6 70.61 5.50 1 15 -6 87.60 6.35 -1 15 6 98.56 6.12 -1 15 6 100.25 6.13 -1 15 6 65.21 5.12 -1 15 5 231.45 9.04 1 15 -5 227.47 10.58 1 15 -5 230.17 9.62 -1 15 5 233.54 8.80 -1 15 5 231.40 8.94 -1 15 5 241.48 9.27 1 15 -5 196.69 16.27 1 15 -4 -1.07 4.20 1 15 -4 3.02 2.32 -1 15 4 3.43 1.69 -1 15 4 1.41 2.07 -1 15 4 4.68 2.31 -1 15 4 2.47 2.37 1 15 -4 3.56 2.60 -1 15 4 4.79 2.08 1 15 -4 1.94 2.44 -1 15 3 135.47 6.97 -1 15 3 139.43 7.23 1 15 -3 145.63 8.16 -1 15 3 149.87 7.27 -1 15 3 145.78 6.97 1 15 -3 118.82 12.53 1 15 -3 137.28 7.48 -1 15 3 116.86 7.44 1 15 -3 117.96 6.23 -1 15 3 120.36 12.45 1 15 -3 151.34 8.84 1 15 -2 17.22 3.11 -1 15 2 14.88 2.91 1 15 -2 11.93 3.45 1 15 -2 18.07 3.08 -1 15 2 12.07 2.16 -1 15 2 9.68 2.61 -1 15 2 11.50 2.97 1 15 -2 9.98 2.62 -1 15 2 20.09 5.92 1 15 -2 12.48 4.57 -1 15 1 69.51 5.77 -1 15 1 76.33 5.37 1 15 -1 72.48 6.37 -1 15 1 66.84 5.22 -1 15 1 62.12 9.32 1 15 -1 73.39 5.33 1 15 -1 68.71 4.95 -1 15 1 74.14 5.27 1 15 0 118.87 6.53 -1 15 0 111.47 6.58 -1 15 0 111.21 12.53 -1 15 0 86.88 5.91 1 15 0 116.83 6.41 -1 15 0 92.77 7.03 -1 15 0 120.88 6.48 1 15 0 103.84 7.22 1 15 1 16.19 2.88 1 15 1 13.98 2.72 -1 15 -1 15.66 5.36 1 15 1 21.55 3.32 1 15 1 16.02 3.53 -1 15 -1 12.73 2.97 -1 15 -1 14.32 2.96 -1 15 -1 18.71 3.21 -1 15 -2 5.29 2.33 -1 15 -2 3.32 1.80 1 15 2 3.74 1.87 -1 15 -2 1.62 2.04 1 15 2 4.00 2.31 -1 15 -2 2.59 3.05 -1 15 -2 3.13 2.01 1 15 2 -0.03 2.16 1 15 2 1.64 2.30 1 15 3 13.61 2.75 -1 15 -3 14.34 3.03 -1 15 -3 15.15 3.19 1 15 3 10.54 2.92 -1 15 -3 8.75 2.40 1 15 3 16.79 3.39 -1 15 -3 12.73 4.05 1 15 3 18.85 3.06 -1 15 -3 13.57 2.79 -1 15 -4 72.61 5.49 1 15 4 66.57 5.95 -1 15 -4 78.33 6.63 -1 15 -4 78.67 5.49 -1 15 -4 70.21 10.85 1 15 4 75.07 5.27 -1 15 -4 61.35 4.99 1 15 4 75.99 5.17 1 15 4 66.81 5.01 1 15 5 27.67 4.46 -1 15 -5 28.02 3.43 1 15 5 31.99 3.63 -1 15 -5 28.13 6.82 -1 15 -5 32.63 4.87 1 15 5 35.04 3.71 -1 15 -5 33.32 4.18 -1 15 -5 32.68 3.98 1 15 5 34.95 3.66 1 15 6 5.34 1.81 -1 15 -6 5.64 2.75 1 15 6 9.90 2.31 1 15 6 5.50 2.64 -1 15 -6 6.28 2.18 -1 15 -6 5.08 2.40 1 15 6 8.31 2.53 -1 15 -6 8.75 2.62 -1 15 -6 5.34 4.66 -1 15 -7 65.44 5.28 1 15 7 58.20 6.08 1 15 7 71.73 4.95 -1 15 -7 70.11 6.32 -1 15 -7 68.46 5.45 1 15 7 77.87 5.22 1 15 7 74.02 5.36 -1 15 -7 75.93 11.39 -1 15 -8 50.41 5.75 1 15 8 55.93 4.82 1 15 8 54.40 4.32 -1 15 -8 51.62 9.05 -1 15 -8 45.16 4.56 -1 15 -8 41.26 4.45 1 15 8 39.51 5.18 1 15 9 109.23 6.49 -1 15 -9 113.21 6.44 1 15 9 95.06 7.40 -1 15 -9 111.20 7.04 -1 15 -9 92.20 12.50 -1 15 -9 111.26 8.40 -1 15 -10 22.98 3.97 -1 15 -10 26.81 7.69 -1 15 -10 30.17 4.68 -1 15 -10 27.73 3.63 1 15 10 24.06 3.84 1 15 10 33.73 4.37 1 15 11 14.89 3.30 -1 15 -11 18.43 3.44 -1 15 -11 17.61 2.98 1 15 11 22.04 3.15 -1 15 -11 23.37 4.32 -1 15 -12 75.74 7.14 -1 15 -12 66.47 5.13 1 15 12 55.64 5.67 -1 15 -12 78.15 6.16 -1 15 -13 21.27 3.05 -1 15 -13 22.92 3.89 1 15 13 15.11 3.20 -1 15 -13 22.31 3.93 -1 15 -14 30.58 5.14 -1 15 -14 31.44 4.25 1 15 14 20.51 3.72 1 15 14 38.39 4.11 -1 15 -15 64.46 5.29 -1 15 -15 71.13 6.38 -1 15 -16 6.73 3.20 1 15 16 6.14 2.24 -1 15 -16 4.67 2.13 1 15 17 91.98 6.20 -1 15 -17 104.10 6.02 -1 15 -17 106.45 7.73 -1 15 -18 58.40 6.04 1 15 18 63.82 5.16 -1 15 -18 55.35 4.53 -1 15 -19 13.95 2.39 -1 15 -19 6.39 2.73 -1 15 -20 3.23 2.16 -1 15 -21 22.78 3.48 -1 15 -22 5.05 2.02 -1 15 -23 58.36 4.38 -1 15 -23 42.12 4.11 -1 15 -24 19.14 2.37 -1 15 -24 18.37 2.69 -1 15 -25 -0.52 1.44 -1 15 -25 3.11 1.28 1 16 -25 12.68 1.79 1 16 -24 3.56 1.60 1 16 -24 5.17 1.69 1 16 -23 2.32 1.17 1 16 -23 -0.10 1.62 1 16 -22 6.69 2.36 1 16 -22 2.24 1.40 1 16 -21 67.71 5.50 1 16 -21 71.32 4.35 1 16 -20 3.80 1.64 1 16 -20 2.14 2.54 1 16 -19 93.51 7.06 -1 16 19 90.10 5.28 1 16 -19 100.12 5.95 1 16 -18 9.28 3.16 -1 16 18 4.65 1.74 1 16 -18 3.72 2.13 1 16 -17 21.03 3.97 1 16 -17 26.74 4.00 1 16 -16 9.51 2.64 1 16 -16 7.24 2.98 1 16 -15 3.71 2.86 1 16 -15 7.97 2.84 1 16 -15 5.13 1.77 1 16 -14 1.69 2.84 1 16 -14 1.49 2.30 1 16 -14 2.74 2.11 1 16 -13 123.92 8.73 1 16 -13 111.92 7.60 1 16 -13 119.54 6.95 -1 16 12 16.47 2.91 1 16 -12 16.55 3.58 1 16 -12 9.11 2.49 1 16 -12 10.10 3.71 1 16 -11 3.87 2.50 -1 16 11 8.54 2.50 1 16 -11 8.41 3.23 1 16 -11 4.21 2.41 1 16 -10 18.84 3.77 1 16 -10 20.82 3.49 -1 16 10 22.30 3.49 -1 16 10 16.47 2.71 1 16 -10 17.01 3.67 -1 16 10 24.35 3.56 -1 16 9 7.86 2.71 -1 16 9 9.63 2.51 1 16 -9 12.75 3.36 -1 16 9 8.15 2.47 1 16 -9 5.18 2.87 1 16 -8 49.10 5.25 1 16 -8 43.68 5.43 -1 16 8 48.65 4.44 -1 16 8 53.96 4.80 -1 16 8 44.66 4.42 -1 16 8 48.00 4.34 1 16 -7 10.49 4.20 -1 16 7 28.54 3.88 -1 16 7 20.03 3.30 -1 16 7 32.26 3.85 1 16 -7 27.82 4.37 1 16 -7 19.88 4.11 -1 16 7 23.97 3.57 -1 16 6 3.61 2.11 1 16 -6 4.11 2.70 -1 16 6 3.11 2.13 -1 16 6 0.20 2.32 -1 16 6 2.37 2.09 1 16 -6 0.85 3.21 -1 16 6 2.37 2.25 1 16 -6 0.87 2.36 -1 16 5 91.49 7.02 1 16 -5 97.40 11.99 -1 16 5 110.86 6.53 -1 16 5 123.72 6.81 -1 16 5 112.95 6.79 -1 16 5 115.14 6.74 1 16 -5 114.15 7.69 1 16 -5 108.87 7.15 -1 16 4 37.30 4.22 1 16 -4 31.21 4.39 1 16 -4 33.20 4.15 -1 16 4 37.26 4.23 -1 16 4 29.62 4.40 -1 16 4 31.09 4.19 -1 16 4 41.85 4.46 1 16 -4 29.76 6.70 1 16 -3 131.50 8.19 1 16 -3 139.78 7.68 -1 16 3 140.20 7.39 -1 16 3 114.22 7.65 -1 16 3 155.35 7.54 1 16 -3 129.95 6.71 -1 16 3 153.69 7.46 -1 16 3 136.47 7.22 1 16 -3 160.45 9.20 1 16 -2 8.15 2.53 -1 16 2 9.83 2.83 1 16 -2 8.33 2.67 -1 16 2 4.00 2.15 1 16 -2 8.65 3.35 -1 16 2 10.19 2.61 -1 16 2 11.65 2.87 -1 16 2 6.71 2.79 1 16 -2 11.50 2.68 -1 16 1 90.19 11.46 1 16 -1 94.94 6.06 -1 16 1 80.40 6.11 1 16 -1 82.62 6.99 1 16 -1 86.10 6.12 -1 16 1 103.66 6.41 -1 16 1 108.88 6.60 1 16 -1 106.65 6.49 -1 16 0 -1.10 4.79 1 16 0 3.55 1.95 -1 16 0 4.09 1.95 -1 16 0 1.36 2.41 1 16 0 3.82 2.52 1 16 0 5.32 2.79 -1 16 0 3.88 2.13 1 16 0 4.11 2.06 1 16 1 229.85 9.56 -1 16 -1 229.26 9.73 -1 16 -1 217.92 17.94 1 16 1 237.29 11.15 1 16 1 229.79 8.97 1 16 1 245.70 9.40 -1 16 -1 245.80 9.46 -1 16 -1 232.65 9.20 1 16 2 24.18 3.48 1 16 2 12.66 3.01 -1 16 -2 16.68 3.34 -1 16 -2 19.88 6.13 -1 16 -2 25.92 3.63 -1 16 -2 14.16 3.18 1 16 2 23.14 3.49 1 16 2 11.14 3.46 1 16 3 -0.12 1.99 1 16 3 5.18 2.29 -1 16 -3 0.56 1.79 1 16 3 -1.03 2.73 1 16 3 1.76 1.91 -1 16 -3 2.76 2.29 -1 16 -3 3.53 2.36 -1 16 -3 3.23 3.04 -1 16 -4 1.88 1.77 -1 16 -4 -2.49 5.20 -1 16 -4 4.15 2.45 1 16 4 0.54 2.10 -1 16 -4 2.62 2.31 -1 16 -4 4.53 2.60 1 16 4 3.07 2.17 1 16 4 1.48 2.24 1 16 4 2.27 2.40 1 16 5 1.81 2.79 1 16 5 3.82 2.01 -1 16 -5 2.88 2.31 1 16 5 3.11 2.10 -1 16 -5 2.05 2.08 -1 16 -5 5.61 5.11 -1 16 -5 1.88 1.80 1 16 5 4.14 2.25 -1 16 -5 4.79 2.62 -1 16 -6 2.09 1.75 -1 16 -6 -3.08 4.71 1 16 6 -0.28 2.74 1 16 6 3.20 2.15 1 16 6 3.45 2.25 -1 16 -6 1.73 2.43 -1 16 -6 3.10 2.39 1 16 6 2.50 2.22 -1 16 -6 -1.48 2.83 -1 16 -7 63.98 5.68 1 16 7 52.08 5.45 1 16 7 65.31 5.44 -1 16 -7 69.75 5.80 -1 16 -7 53.07 9.74 -1 16 -7 65.57 6.54 1 16 7 65.50 5.02 1 16 7 76.16 5.14 -1 16 -8 9.01 3.26 -1 16 -8 7.91 3.16 1 16 8 5.45 2.34 1 16 8 12.58 2.94 1 16 8 11.04 2.41 -1 16 -8 10.19 2.87 1 16 9 60.88 5.89 -1 16 -9 74.08 5.72 1 16 9 79.34 5.75 -1 16 -9 71.38 6.01 -1 16 -9 79.44 7.05 1 16 10 21.35 3.99 -1 16 -10 24.59 4.17 -1 16 -10 19.99 3.34 -1 16 -10 34.17 4.31 -1 16 -11 62.18 5.46 -1 16 -11 72.29 5.36 1 16 11 55.06 5.73 -1 16 -11 64.22 6.88 -1 16 -12 20.96 3.26 -1 16 -12 27.45 3.51 -1 16 -12 28.80 4.76 1 16 12 20.26 3.49 -1 16 -13 74.77 5.71 1 16 13 53.71 5.18 -1 16 -13 64.03 4.80 -1 16 -13 58.72 6.67 -1 16 -14 -3.20 2.38 -1 16 -14 1.94 3.00 -1 16 -15 139.08 8.92 -1 16 -15 135.62 7.25 -1 16 -16 36.88 5.25 -1 16 -16 42.55 4.15 -1 16 -17 6.49 2.65 -1 16 -17 7.69 2.20 -1 16 -18 -0.51 1.50 -1 16 -18 -0.67 2.30 -1 16 -19 4.01 2.45 -1 16 -19 2.42 1.45 -1 16 -20 7.36 2.61 -1 16 -20 4.32 2.45 -1 16 -21 54.28 4.60 -1 16 -21 45.88 4.14 -1 16 -22 -0.81 1.58 -1 16 -22 3.41 1.94 -1 16 -23 4.99 1.38 -1 16 -23 4.41 1.85 -1 16 -24 1.45 1.26 -1 16 -24 2.01 1.19 1 17 -24 0.52 1.00 1 17 -23 9.76 1.96 1 17 -22 1.60 1.70 1 17 -22 1.90 1.10 1 17 -22 -1.77 1.46 1 17 -21 0.57 1.77 1 17 -21 1.73 1.46 1 17 -21 0.99 1.49 1 17 -20 52.77 4.95 1 17 -20 39.51 3.46 1 17 -20 52.50 3.73 1 17 -19 10.62 2.80 1 17 -19 9.83 2.26 1 17 -18 24.50 3.28 1 17 -18 18.74 3.84 1 17 -17 47.19 4.49 1 17 -17 39.21 5.02 1 17 -16 10.79 2.62 1 17 -16 11.29 3.35 1 17 -15 60.88 5.73 1 17 -15 57.22 6.00 1 17 -15 72.16 4.96 1 17 -14 30.47 4.26 1 17 -14 38.91 5.14 1 17 -14 42.20 4.22 1 17 -13 46.01 4.55 -1 17 13 59.51 4.86 1 17 -13 51.07 5.09 1 17 -13 49.12 5.81 1 17 -12 38.96 4.79 -1 17 12 41.06 4.14 1 17 -12 33.82 4.11 -1 17 11 3.58 2.14 1 17 -11 -1.81 2.78 1 17 -11 2.09 2.29 1 17 -11 -1.00 2.38 1 17 -10 11.39 3.31 -1 17 10 9.21 2.56 -1 17 10 5.02 2.05 1 17 -10 7.36 2.50 1 17 -10 10.69 3.31 1 17 -9 4.63 2.39 1 17 -9 6.63 2.83 -1 17 9 6.49 2.43 -1 17 9 12.96 3.04 1 17 -9 6.26 3.06 -1 17 9 5.66 2.47 -1 17 8 7.05 2.55 1 17 -8 2.88 2.37 -1 17 8 12.16 2.72 -1 17 8 8.90 2.69 1 17 -8 6.40 2.40 -1 17 8 6.04 2.13 1 17 -8 8.19 2.90 1 17 -7 44.14 4.71 -1 17 7 49.65 4.67 -1 17 7 47.16 4.37 1 17 -7 37.77 5.63 -1 17 7 54.48 4.65 -1 17 7 57.83 5.10 1 17 -7 41.77 5.19 -1 17 6 81.98 6.34 -1 17 6 83.42 5.75 1 17 -6 81.93 6.26 -1 17 6 97.23 6.21 -1 17 6 98.60 6.17 1 17 -6 99.35 6.71 1 17 -6 82.18 7.15 -1 17 6 94.01 6.25 -1 17 5 39.94 4.45 1 17 -5 50.37 4.97 1 17 -5 38.14 4.65 -1 17 5 36.62 4.71 -1 17 5 59.92 5.04 -1 17 5 38.87 4.20 -1 17 5 57.22 5.14 1 17 -5 37.85 4.87 -1 17 4 3.90 2.33 1 17 -4 10.31 2.96 -1 17 4 5.69 2.87 -1 17 4 7.63 2.55 -1 17 4 4.69 2.20 1 17 -4 6.11 1.96 1 17 -4 8.36 2.79 -1 17 4 3.65 2.65 1 17 -3 84.12 5.84 1 17 -3 94.73 6.37 -1 17 3 58.78 5.39 -1 17 3 61.06 5.37 1 17 -3 53.83 5.49 -1 17 3 101.44 6.53 -1 17 3 97.00 6.70 -1 17 2 107.82 6.50 1 17 -2 98.02 6.39 -1 17 2 93.56 6.35 1 17 -2 80.60 5.74 -1 17 2 93.56 6.19 -1 17 2 96.91 6.50 1 17 -2 91.77 6.60 1 17 -1 189.10 10.47 1 17 -1 196.36 9.27 -1 17 1 185.84 8.66 1 17 -1 193.57 8.49 -1 17 1 223.80 9.17 1 17 -1 228.89 9.37 -1 17 1 200.58 9.01 -1 17 1 226.90 9.32 1 17 0 174.89 8.41 -1 17 0 160.27 8.04 1 17 0 151.24 7.69 1 17 0 182.66 10.18 1 17 0 176.01 8.83 -1 17 0 184.69 8.73 -1 17 0 174.52 8.13 1 17 1 17.84 3.29 -1 17 -1 15.05 3.13 -1 17 -1 16.41 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8 41.32 4.42 -1 17 -9 4.00 3.14 1 17 9 8.76 2.70 -1 17 -9 8.35 2.58 -1 17 -9 6.14 2.63 1 17 9 5.12 3.04 -1 17 -10 8.54 2.54 -1 17 -10 4.08 2.78 -1 17 -10 6.31 2.59 1 17 10 4.29 2.28 -1 17 -11 141.64 9.83 -1 17 -11 157.67 7.62 -1 17 -11 142.90 8.06 1 17 12 10.27 2.74 -1 17 -12 12.57 2.79 -1 17 -12 9.01 2.94 -1 17 -12 9.24 2.66 -1 17 -13 33.62 4.13 -1 17 -13 35.14 3.54 1 17 13 22.72 3.43 -1 17 -13 39.17 5.00 -1 17 -13 25.56 3.85 -1 17 -14 95.31 6.05 -1 17 -14 107.00 7.81 -1 17 -15 5.62 2.79 -1 17 -15 7.45 2.32 -1 17 -15 2.90 2.05 -1 17 -16 0.51 2.24 -1 17 -16 4.45 2.76 -1 17 -16 4.86 2.20 -1 17 -17 107.29 7.33 -1 17 -17 113.01 5.73 -1 17 -18 23.79 3.63 -1 17 -18 16.82 2.96 -1 17 -18 17.07 2.37 -1 17 -19 2.53 1.36 -1 17 -19 2.85 2.04 -1 17 -19 1.25 1.80 -1 17 -20 9.29 2.28 -1 17 -20 6.74 2.07 -1 17 -21 2.54 1.51 -1 17 -21 1.42 1.51 -1 17 -22 0.71 1.29 -1 17 -22 0.05 1.34 -1 17 -23 14.08 1.79 1 18 -22 12.77 1.72 1 18 -21 4.87 1.86 1 18 -21 3.58 1.22 1 18 -20 5.61 2.18 1 18 -20 2.63 1.33 1 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130.48 6.94 1 18 2 133.47 7.44 1 18 2 130.25 7.04 -1 18 -2 121.53 7.00 -1 18 -2 135.59 7.78 -1 18 -2 125.64 7.34 1 18 3 1.23 2.63 1 18 3 3.02 2.34 1 18 3 2.61 1.95 1 18 3 1.68 1.93 -1 18 -3 2.16 2.39 -1 18 -3 -0.87 1.79 -1 18 -3 4.22 2.54 1 18 4 4.72 2.14 1 18 4 5.93 2.27 -1 18 -4 6.27 2.37 1 18 4 1.98 2.31 -1 18 -4 5.14 2.71 -1 18 -4 9.06 3.20 1 18 4 5.16 2.16 -1 18 -5 0.82 2.41 1 18 5 2.00 2.39 -1 18 -5 2.05 2.28 1 18 5 3.48 1.99 1 18 5 4.75 2.15 -1 18 -5 1.83 2.15 1 18 5 1.72 1.95 -1 18 -6 12.61 2.52 -1 18 -6 16.35 3.35 1 18 6 18.06 3.01 -1 18 -6 12.06 2.33 -1 18 -6 11.53 2.87 1 18 6 13.83 3.01 1 18 6 16.81 2.94 1 18 6 8.65 3.06 -1 18 -7 4.64 2.54 1 18 7 4.09 2.04 1 18 7 1.49 2.00 1 18 7 4.91 2.63 1 18 7 6.58 2.38 -1 18 -7 6.16 2.11 -1 18 -7 2.47 2.21 -1 18 -8 0.96 2.07 1 18 8 3.23 2.21 -1 18 -8 3.16 2.25 1 18 8 3.45 2.61 1 18 8 2.52 1.89 1 18 8 1.06 1.86 -1 18 -8 2.02 2.18 -1 18 -9 4.13 2.55 -1 18 -9 0.68 2.04 1 18 9 2.10 2.48 -1 18 -9 2.00 2.31 -1 18 -9 1.52 2.37 -1 18 -10 163.29 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24 15.94 3.35 -2 8 24 14.77 3.17 -2 8 23 42.41 5.26 2 8 -23 36.91 4.74 -2 8 22 20.71 3.75 2 8 -22 19.96 3.80 -2 8 22 19.80 3.82 -2 8 21 109.17 7.73 2 8 -21 94.72 7.98 -2 8 21 110.97 8.14 2 8 -20 197.93 11.63 -2 8 20 206.59 10.40 -2 -8 20 194.54 18.76 -2 8 20 165.68 17.03 -2 8 20 211.88 10.96 2 8 -19 9.17 3.44 -2 8 19 14.63 3.59 -2 8 19 10.05 3.28 -2 8 19 16.58 4.19 -2 8 19 19.30 6.28 -2 8 18 10.20 3.00 -2 8 18 10.79 2.93 2 8 -18 13.42 3.58 -2 8 18 10.58 3.43 -2 8 18 10.63 5.31 2 8 -17 3.48 2.65 -2 8 17 3.44 1.96 -2 8 17 8.06 4.17 -2 8 17 1.89 3.03 -2 8 16 44.38 8.50 -2 8 15 176.85 15.62 -2 8 14 379.67 21.76 -2 8 13 88.42 10.35 -2 8 12 461.78 22.88 -2 8 11 91.87 10.07 2 8 -11 79.16 7.34 -2 8 10 26.45 5.43 2 8 -10 29.63 4.56 -2 8 9 643.32 24.26 2 8 -9 614.81 19.13 -2 8 8 14.03 4.26 2 8 -8 11.28 2.93 -2 8 7 76.79 7.19 2 8 -7 68.00 6.47 -2 8 7 79.48 8.13 -2 8 6 330.70 14.45 -2 8 6 312.27 15.29 2 8 -6 299.13 13.10 -2 -8 5 15.93 3.89 -2 8 5 19.19 4.32 2 8 -5 14.62 3.47 -2 -8 4 777.54 21.48 2 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13 107.96 12.05 -2 10 12 286.26 19.51 -2 10 11 95.78 11.22 2 10 -10 132.55 10.52 -2 10 10 127.07 12.29 2 10 -9 13.32 3.31 -2 10 9 15.42 5.03 2 10 -8 331.77 16.02 2 10 -7 282.20 14.78 -2 -10 7 306.48 17.21 -2 10 7 315.64 16.07 2 10 -6 34.76 5.47 -2 -10 6 35.13 5.77 -2 10 6 38.59 5.72 -2 -10 5 415.76 18.39 2 10 -5 376.79 16.84 -2 10 5 429.29 18.58 -2 10 4 26.36 4.83 -2 -10 4 20.08 4.31 2 10 -4 21.02 4.40 -2 -10 3 7.73 3.07 -2 10 3 5.74 3.19 2 10 -3 6.54 2.88 -2 -10 2 247.33 12.22 2 10 -2 233.57 13.21 -2 10 1 272.58 15.53 -2 -10 1 261.41 12.02 2 10 -1 237.91 13.45 2 10 0 17.03 4.27 -2 -10 0 15.63 2.86 -2 10 0 19.63 4.57 -2 10 -1 2.82 3.31 2 10 2 94.06 7.43 -2 10 -2 96.86 10.00 2 10 3 32.52 4.86 -2 10 -3 34.77 6.31 -2 10 -4 7.39 3.54 2 10 4 7.00 3.22 2 10 5 101.44 9.18 -2 10 -5 104.27 10.70 2 10 6 328.57 17.47 -2 10 -6 336.07 19.21 2 10 7 9.12 3.52 -2 10 -7 7.84 3.89 2 10 8 41.18 7.31 -2 10 -8 36.72 7.38 2 10 9 18.66 5.31 -2 10 -9 20.22 5.58 2 10 10 36.73 7.48 -2 10 -10 30.87 6.62 -2 10 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2.61 -2 11 20 7.74 2.74 2 11 -20 8.77 3.38 -2 11 19 111.06 7.95 -2 11 19 107.61 7.59 2 11 -19 106.20 8.95 2 11 -18 35.45 5.54 -2 11 18 29.41 4.92 -2 11 18 30.27 4.42 2 11 -17 38.73 5.98 -2 -11 17 23.83 7.05 -2 11 17 32.65 5.14 -2 11 17 27.18 4.42 -2 11 17 23.28 7.00 -2 11 16 57.91 4.57 -2 11 16 42.63 5.62 -2 11 16 50.21 5.54 2 11 -16 50.06 6.34 -2 -11 16 56.64 10.06 -2 11 16 54.45 9.65 -2 -11 15 82.59 12.82 -2 11 15 75.38 11.26 -2 11 15 84.73 7.39 2 11 -15 85.15 8.24 -2 11 15 79.40 5.32 -2 11 15 84.41 6.96 -2 11 14 19.38 3.56 -2 -11 14 18.29 6.13 2 11 -14 26.53 5.17 -2 11 14 22.72 4.12 -2 11 14 18.94 5.92 -2 11 14 16.14 2.59 -2 -11 13 245.83 19.52 -2 11 13 216.06 17.88 2 11 -13 259.71 12.95 -2 -11 12 16.58 5.89 -2 -11 11 248.61 18.53 2 11 -10 29.01 5.46 -2 -11 10 39.51 7.35 -2 -11 9 44.27 7.98 2 11 -9 35.71 6.44 -2 -11 8 343.15 19.63 2 11 -8 306.51 16.48 -2 11 7 306.61 16.71 -2 -11 7 305.36 17.65 2 11 -7 273.53 15.59 -2 -11 6 60.71 7.65 2 11 -6 50.60 6.72 -2 11 6 63.69 7.72 -2 -11 5 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16 -1.12 4.64 -2 12 16 1.96 1.97 -2 12 15 67.63 6.60 -2 12 15 67.41 5.01 -2 12 15 67.04 6.40 -2 -12 15 73.77 11.90 2 12 -15 72.82 7.64 -2 12 14 5.73 3.10 -2 12 14 4.73 2.62 -2 12 14 2.19 1.79 -2 -12 14 -1.00 3.48 2 12 -14 2.56 3.02 2 12 -13 20.12 4.57 -2 -12 13 15.53 5.81 -2 12 13 16.56 2.91 -2 12 13 13.54 3.14 -2 12 13 14.13 3.16 -2 12 12 8.11 2.85 -2 12 12 7.16 1.99 -2 -12 12 5.33 4.06 2 12 -12 6.23 3.11 2 12 -11 12.01 3.55 -2 -12 11 12.20 5.91 -2 -12 10 25.23 6.05 -2 -12 9 434.62 23.68 2 12 -9 394.84 19.47 -2 -12 8 129.85 12.10 2 12 -8 101.69 9.76 -2 -12 7 10.09 4.39 2 12 -7 8.05 3.05 2 12 -6 49.75 7.21 -2 12 6 58.73 7.60 -2 -12 6 50.43 7.32 2 12 -5 31.38 5.61 -2 -12 5 29.35 5.29 -2 12 5 35.66 6.16 -2 -12 4 57.10 7.05 -2 12 4 61.39 8.03 2 12 -4 50.29 7.07 -2 12 3 337.55 18.86 2 12 -3 300.06 16.91 2 12 -2 27.25 5.28 -2 12 2 30.43 5.71 -2 12 1 230.25 15.62 -2 12 0 41.22 7.22 -2 12 -1 145.03 12.78 -2 12 -2 146.86 12.93 -2 12 -3 194.05 15.28 -2 12 -4 -0.90 3.66 -2 12 -5 535.92 26.70 2 12 6 79.10 8.93 -2 12 -6 80.53 10.19 -2 12 -7 46.43 8.30 2 12 7 41.03 7.06 2 12 8 4.47 2.58 -2 12 -8 -0.53 4.04 -2 12 -9 12.74 5.39 2 12 9 0.84 2.20 -2 12 -10 3.23 3.55 -2 12 -10 1.71 2.37 2 12 10 0.88 1.77 2 12 10 0.46 2.43 2 12 11 5.69 3.06 2 12 11 5.92 3.93 2 12 11 6.34 2.01 -2 12 -11 4.96 2.06 -2 12 -11 7.68 2.96 -2 12 -11 6.10 4.04 2 12 12 174.35 16.72 -2 12 -12 161.42 7.23 -2 12 -12 175.28 17.08 2 12 12 175.99 8.66 2 12 12 158.86 9.33 -2 12 -12 206.53 10.02 2 12 13 4.93 2.17 2 12 13 2.79 2.45 -2 12 -13 5.37 3.62 -2 12 -13 3.21 1.79 2 12 13 -3.41 2.70 -2 12 -13 4.25 2.37 2 12 14 13.73 3.24 2 12 14 9.98 3.02 -2 12 -14 10.83 2.46 2 12 14 10.49 4.69 -2 12 -14 17.05 6.26 -2 12 -14 18.48 3.53 2 12 15 150.54 9.22 -2 12 -15 140.79 7.05 2 12 15 158.45 8.97 2 12 16 122.22 7.66 -2 12 -16 111.78 8.11 -2 12 -17 60.67 6.26 2 12 17 58.31 5.91 2 12 18 5.30 2.45 -2 12 -18 2.62 2.49 2 12 18 3.54 2.60 2 12 19 16.74 3.26 -2 12 -19 10.62 3.51 2 12 20 32.31 4.15 2 12 20 31.88 4.03 -2 12 -21 114.34 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4.16 -2 13 14 29.24 4.29 -2 13 14 26.28 3.77 -2 -13 14 31.00 8.37 2 13 -13 11.22 3.83 -2 13 13 8.22 2.46 -2 13 13 12.59 3.69 -2 13 13 8.97 2.52 -2 -13 13 0.25 5.25 -2 13 12 13.28 2.91 -2 13 12 7.96 2.32 -2 -13 12 14.24 4.70 2 13 -12 13.91 4.04 -2 13 12 12.06 3.63 -2 13 11 55.29 4.60 -2 13 11 67.34 5.60 -2 13 11 47.38 5.61 2 13 -11 49.64 6.28 -2 13 11 50.02 4.95 -2 -13 11 61.27 10.13 -2 13 10 97.15 7.47 -2 -13 10 84.22 11.51 2 13 -10 105.85 8.51 -2 13 10 94.13 5.73 -2 13 10 107.93 6.35 -2 -13 9 140.85 13.64 -2 13 9 148.22 6.90 2 13 -9 173.61 10.69 2 13 -8 58.64 8.06 -2 -13 8 65.69 9.39 -2 -13 7 56.33 8.36 2 13 -7 47.21 7.59 2 13 -6 79.35 9.20 -2 13 6 93.04 10.20 -2 13 5 3.51 2.71 2 13 -5 1.35 2.31 2 13 -4 339.56 18.60 -2 13 4 402.61 21.01 -2 13 3 8.26 4.23 2 13 -3 5.70 3.34 -2 13 2 121.93 11.82 -2 13 1 92.44 10.59 -2 13 0 9.99 4.35 -2 13 -1 36.54 6.83 -2 13 -2 47.91 8.38 -2 13 -3 15.14 4.51 -2 13 -4 252.29 18.50 -2 13 -5 3.51 3.47 -2 13 -6 0.45 3.01 -2 13 -7 251.86 19.61 -2 13 -8 168.96 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111.23 7.86 2 15 -2 96.53 6.41 -2 15 2 121.95 6.71 -2 15 2 99.16 6.12 -2 15 2 101.22 6.49 -2 15 2 118.67 13.18 -2 15 2 116.56 6.94 2 15 -2 97.11 6.19 2 15 -2 124.61 6.90 2 15 -1 104.10 6.41 -2 15 1 97.54 11.86 2 15 -1 142.06 8.45 -2 15 1 117.52 6.62 2 15 -1 95.81 6.17 -2 15 1 132.59 6.92 -2 15 1 110.61 6.58 -2 15 0 19.31 3.09 2 15 0 18.03 3.48 -2 15 0 20.57 3.26 -2 15 0 19.29 3.21 2 15 0 17.21 3.14 2 15 0 28.28 3.79 -2 15 0 18.24 5.41 2 15 1 9.54 3.25 -2 15 -1 11.65 2.88 2 15 1 11.59 2.36 -2 15 -1 9.35 2.55 2 15 1 11.00 2.55 -2 15 -1 11.26 2.67 -2 15 -1 10.73 5.11 -2 15 -2 9.00 2.55 2 15 2 10.51 2.43 -2 15 -2 8.11 2.71 -2 15 -2 7.23 4.60 2 15 2 8.81 3.10 2 15 2 8.19 2.26 -2 15 -2 12.11 3.06 -2 15 -3 128.96 6.49 -2 15 -3 136.82 15.05 2 15 3 148.52 7.04 -2 15 -3 161.80 8.98 -2 15 -3 140.90 7.36 2 15 3 142.95 8.98 2 15 3 142.60 7.35 -2 15 -3 153.52 7.49 2 15 3 136.98 7.25 -2 15 -3 141.56 7.49 2 15 4 58.40 4.61 2 15 4 38.33 3.97 -2 15 -4 48.88 4.90 -2 15 -4 38.79 4.19 2 15 4 36.63 5.39 -2 15 -4 51.54 4.88 2 15 4 55.21 5.01 -2 15 -4 63.76 10.78 -2 15 -4 44.12 5.18 -2 15 -5 148.93 9.07 2 15 5 132.31 6.61 2 15 5 122.79 7.15 -2 15 -5 148.41 7.39 -2 15 -5 133.57 6.99 -2 15 -5 135.80 7.16 2 15 5 138.81 7.08 -2 15 -5 119.26 13.79 2 15 5 137.00 8.61 -2 15 -6 0.74 1.88 -2 15 -6 2.57 1.93 2 15 6 5.08 2.34 2 15 6 6.44 2.38 -2 15 -6 4.88 2.16 -2 15 -6 3.20 2.46 2 15 6 0.68 2.58 -2 15 -6 3.91 4.07 -2 15 -7 30.29 4.63 -2 15 -7 23.50 3.90 2 15 7 22.34 4.31 2 15 7 24.73 3.46 -2 15 -7 24.13 3.28 -2 15 -7 22.49 6.52 -2 15 -7 29.35 3.64 -2 15 -8 2.84 2.15 -2 15 -8 0.68 2.42 -2 15 -8 5.28 2.44 -2 15 -8 4.95 4.77 2 15 8 3.28 1.98 2 15 8 5.07 3.17 -2 15 -8 0.28 2.01 2 15 9 4.21 2.30 -2 15 -9 5.45 4.48 -2 15 -9 4.24 2.41 -2 15 -9 3.71 2.70 -2 15 -9 2.09 1.94 2 15 9 2.46 2.78 -2 15 -10 105.38 6.85 -2 15 -10 93.12 6.11 -2 15 -10 104.44 8.40 -2 15 -11 89.90 6.23 -2 15 -11 105.70 7.81 -2 15 -11 101.94 6.03 2 15 11 82.29 6.65 2 15 12 0.05 2.68 -2 15 -12 1.58 2.51 -2 15 -12 2.76 2.13 -2 15 -12 -0.46 2.04 2 15 13 35.45 4.98 -2 15 -13 46.65 4.40 -2 15 -13 48.90 6.00 2 15 14 0.51 2.51 -2 15 -14 4.25 3.19 -2 15 -14 3.99 2.12 2 15 15 58.51 5.42 -2 15 -15 79.50 7.05 -2 15 -15 75.14 5.22 -2 15 -16 56.44 4.56 -2 15 -16 58.18 5.81 2 15 16 45.50 4.91 -2 15 -17 -0.95 2.55 -2 15 -17 3.14 1.83 2 15 17 1.92 2.00 -2 15 -18 5.00 2.79 -2 15 -19 -0.23 2.03 -2 15 -20 0.40 1.77 -2 15 -21 19.79 3.24 -2 15 -21 17.26 2.89 -2 15 -22 20.96 2.82 -2 15 -22 16.27 2.98 -2 15 -23 33.77 3.02 -2 15 -23 39.85 3.56 -2 15 -24 1.33 1.64 -2 15 -24 0.98 1.31 -2 15 -25 4.82 1.49 2 16 -25 3.80 1.45 2 16 -24 1.50 0.95 2 16 -24 2.39 1.75 2 16 -24 -1.16 1.32 2 16 -23 68.87 4.88 2 16 -23 66.23 3.72 2 16 -22 6.47 1.86 2 16 -22 9.34 2.33 -2 16 21 14.12 2.16 2 16 -21 17.10 3.32 2 16 -21 17.18 2.80 2 16 -20 6.55 2.18 -2 16 20 4.29 1.56 2 16 -20 5.18 2.60 2 16 -19 2.66 2.53 2 16 -19 -1.50 2.21 2 16 -18 14.10 3.37 2 16 -18 13.32 2.65 2 16 -17 24.86 4.22 2 16 -17 22.27 3.87 2 16 -16 0.51 2.34 2 16 -16 -2.32 2.51 2 16 -16 2.30 2.02 2 16 -15 73.48 6.41 2 16 -15 78.62 7.19 2 16 -15 85.16 5.52 -2 16 14 10.95 3.39 -2 16 14 11.58 2.71 2 16 -14 12.13 3.47 2 16 -14 7.55 2.53 2 16 -14 14.34 3.45 -2 16 13 23.86 4.28 2 16 -13 22.48 4.75 2 16 -13 26.13 4.14 -2 16 13 31.45 3.78 -2 16 12 3.94 2.49 2 16 -12 0.11 2.45 2 16 -12 3.12 2.71 -2 16 12 6.36 2.23 2 16 -11 41.64 4.92 2 16 -11 32.54 5.07 -2 16 11 46.86 4.45 -2 16 11 37.15 4.97 -2 16 10 29.17 4.02 -2 16 10 31.63 4.13 2 16 -10 29.53 4.44 -2 16 10 31.78 3.79 -2 16 10 37.05 4.58 2 16 -10 27.90 4.81 2 16 -9 12.07 3.73 -2 16 9 23.54 3.51 -2 16 9 22.68 3.11 -2 16 9 25.50 3.71 2 16 -9 24.42 4.08 -2 16 9 29.69 3.98 -2 16 8 9.19 2.51 2 16 -8 8.75 3.24 -2 16 8 11.39 3.10 -2 16 8 7.17 2.52 -2 16 8 7.67 2.63 2 16 -8 4.17 2.95 2 16 -7 7.35 3.05 -2 16 7 4.63 2.30 2 16 -7 5.25 2.75 -2 16 7 5.25 2.44 -2 16 7 6.38 2.78 -2 16 7 2.83 2.12 -2 16 6 7.30 2.32 2 16 -6 10.84 2.90 2 16 -6 8.21 2.75 -2 16 6 9.49 2.82 -2 16 6 10.68 2.92 -2 16 6 10.55 2.92 -2 16 5 234.72 9.67 2 16 -5 205.34 10.00 2 16 -5 215.71 10.02 -2 16 5 218.30 9.09 -2 16 5 222.57 9.63 2 16 -4 1.60 2.78 -2 16 4 0.72 2.25 -2 16 4 -0.56 2.35 2 16 -4 2.98 2.57 -2 16 4 0.13 2.43 -2 16 4 -0.11 2.32 2 16 -4 1.95 2.14 2 16 -3 61.74 5.58 2 16 -3 69.45 6.40 -2 16 3 60.38 5.25 -2 16 3 58.82 5.05 2 16 -3 62.34 5.44 -2 16 3 65.37 9.67 -2 16 3 64.83 5.69 -2 16 3 61.32 5.19 2 16 -2 1.25 3.00 -2 16 2 2.81 2.01 -2 16 2 1.98 2.50 -2 16 2 -1.65 2.32 2 16 -2 0.89 2.28 -2 16 2 -2.63 5.02 2 16 -2 -0.76 2.02 -2 16 2 -0.48 2.33 -2 16 1 152.33 8.07 2 16 -1 149.36 9.00 -2 16 1 141.49 7.99 2 16 -1 138.93 6.96 -2 16 1 139.60 15.24 2 16 -1 152.41 7.80 -2 16 1 126.95 7.47 -2 16 1 135.62 7.52 -2 16 0 7.87 2.63 2 16 0 4.85 1.75 2 16 0 5.52 3.06 2 16 0 8.85 2.29 -2 16 0 9.01 5.40 -2 16 0 6.62 2.27 -2 16 0 3.93 2.21 2 16 1 4.63 2.73 2 16 1 3.74 2.07 -2 16 -1 4.36 2.13 -2 16 -1 7.45 2.50 2 16 1 4.10 1.99 -2 16 -1 4.04 3.36 2 16 1 3.69 2.16 -2 16 -1 6.39 2.56 2 16 2 33.24 3.57 -2 16 -2 37.74 4.26 2 16 2 39.41 5.19 -2 16 -2 28.75 7.61 -2 16 -2 32.42 3.91 2 16 2 34.40 4.02 2 16 2 32.48 3.88 -2 16 -2 34.39 3.92 2 16 3 2.79 2.53 -2 16 -3 1.22 2.17 2 16 3 3.84 1.97 -2 16 -3 5.48 2.23 -2 16 -3 5.23 3.89 -2 16 -3 4.15 1.92 2 16 3 2.78 1.92 2 16 3 2.59 2.31 -2 16 -3 3.66 2.56 -2 16 -4 2.83 3.48 2 16 4 3.45 2.16 -2 16 -4 1.28 1.68 2 16 4 4.16 2.15 -2 16 -4 1.05 1.99 -2 16 -4 1.56 2.44 2 16 4 7.73 2.93 2 16 4 1.82 1.98 -2 16 -4 2.05 1.87 -2 16 -5 53.63 4.55 2 16 5 60.97 5.44 -2 16 -5 49.04 8.94 2 16 5 58.47 5.98 2 16 5 60.96 4.50 2 16 5 61.14 4.98 -2 16 -5 61.59 5.13 -2 16 -5 55.03 5.02 -2 16 -5 69.52 6.54 -2 16 -5 60.94 5.53 -2 16 -6 27.21 3.88 -2 16 -6 17.71 3.62 -2 16 -6 28.54 4.01 2 16 6 30.20 3.74 2 16 6 14.66 3.97 -2 16 -6 22.94 3.58 2 16 6 22.91 3.20 2 16 7 10.34 2.68 -2 16 -7 8.96 2.84 2 16 7 6.32 2.36 -2 16 -7 9.69 3.27 -2 16 -7 9.21 2.75 -2 16 -7 12.11 3.04 2 16 8 4.92 2.88 -2 16 -8 8.13 3.13 -2 16 -8 8.31 2.48 2 16 8 11.67 3.17 -2 16 -8 5.46 2.33 -2 16 -8 4.48 2.21 2 16 9 193.91 10.25 -2 16 -9 200.45 9.28 -2 16 -9 236.80 9.27 -2 16 -9 249.96 12.00 -2 16 -10 22.30 4.44 2 16 10 14.31 3.21 -2 16 -10 14.42 3.12 -2 16 -10 19.79 3.52 -2 16 -10 14.42 3.01 2 16 11 11.94 3.39 -2 16 -11 20.31 4.44 -2 16 -11 10.70 3.09 -2 16 -11 24.72 3.74 -2 16 -11 19.84 3.39 -2 16 -12 24.79 3.69 -2 16 -12 29.48 3.49 -2 16 -12 20.28 3.79 2 16 12 25.68 4.13 -2 16 -12 20.71 4.05 2 16 13 55.64 5.47 -2 16 -13 51.37 5.04 -2 16 -13 59.76 5.54 -2 16 -14 17.87 3.31 -2 16 -14 11.60 2.53 -2 16 -14 14.78 3.94 2 16 14 13.68 3.28 -2 16 -15 73.72 6.02 -2 16 -15 84.91 5.32 -2 16 -15 84.44 7.12 2 16 15 69.55 5.72 2 16 16 2.17 2.03 -2 16 -16 -1.37 1.90 -2 16 -16 3.37 2.31 -2 16 -16 0.77 2.12 -2 16 -17 1.60 1.70 -2 16 -17 -0.42 2.30 -2 16 -17 5.51 2.74 -2 16 -18 -3.44 2.41 -2 16 -18 2.34 2.22 -2 16 -19 44.34 4.45 -2 16 -19 41.52 4.15 -2 16 -20 8.02 2.41 -2 16 -20 2.54 1.98 -2 16 -21 15.70 2.56 -2 16 -21 18.59 2.96 -2 16 -22 4.70 1.87 -2 16 -22 2.09 1.38 -2 16 -23 3.54 1.67 -2 16 -23 3.60 1.29 -2 16 -24 0.02 0.97 2 17 -24 1.90 1.32 2 17 -23 0.78 1.43 2 17 -23 2.85 1.09 2 17 -22 41.29 3.77 2 17 -22 41.57 2.93 2 17 -21 24.75 3.30 2 17 -21 28.84 2.92 2 17 -20 3.25 1.94 2 17 -20 2.08 1.92 2 17 -19 15.55 3.23 2 17 -19 20.52 3.16 2 17 -18 4.18 2.47 2 17 -18 -1.51 2.17 2 17 -17 30.30 3.90 2 17 -17 24.23 4.16 2 17 -16 78.80 7.13 2 17 -16 92.36 6.25 2 17 -16 97.65 5.42 2 17 -15 10.91 2.81 2 17 -15 11.96 3.39 2 17 -15 12.76 3.03 2 17 -14 3.15 2.56 2 17 -14 -1.68 2.37 -2 17 14 0.92 1.69 2 17 -14 2.72 2.00 -2 17 13 2.66 1.84 2 17 -13 -0.05 2.36 2 17 -13 2.51 2.54 2 17 -13 -0.50 2.64 -2 17 12 -0.14 2.88 2 17 -12 0.73 2.66 2 17 -12 7.80 2.98 -2 17 12 4.39 1.93 2 17 -12 4.70 2.58 2 17 -11 7.27 3.15 -2 17 11 9.83 2.73 2 17 -11 1.41 2.36 2 17 -11 7.49 2.91 2 17 -10 51.97 5.33 2 17 -10 50.30 5.58 -2 17 10 51.56 4.70 -2 17 10 53.21 4.92 2 17 -9 36.08 4.94 -2 17 9 38.87 4.15 -2 17 9 36.59 4.05 -2 17 9 36.78 4.10 -2 17 9 32.74 3.74 2 17 -9 33.16 4.26 -2 17 8 15.29 3.23 2 17 -8 10.28 3.19 -2 17 8 10.92 2.68 -2 17 8 19.62 3.88 2 17 -8 12.37 3.55 -2 17 8 17.94 3.46 2 17 -7 182.80 9.92 -2 17 7 242.02 9.59 -2 17 7 194.68 8.82 -2 17 7 184.67 8.36 2 17 -7 187.89 9.70 -2 17 7 227.34 9.42 -2 17 6 41.81 4.31 -2 17 6 45.29 4.39 -2 17 6 50.12 4.92 -2 17 6 36.73 3.94 2 17 -6 40.54 5.02 2 17 -6 38.49 4.54 -2 17 5 23.09 3.66 2 17 -5 23.91 3.89 -2 17 5 26.72 3.81 -2 17 5 22.73 3.45 -2 17 5 30.22 3.77 2 17 -5 21.77 3.74 2 17 -4 57.71 5.28 -2 17 4 70.28 5.46 -2 17 4 64.59 5.44 -2 17 4 64.93 5.28 -2 17 4 73.95 5.74 -2 17 3 11.63 3.16 -2 17 3 11.23 2.49 -2 17 3 13.87 3.18 2 17 -3 9.07 3.57 -2 17 3 8.00 2.63 2 17 -3 8.13 2.63 2 17 -2 146.54 9.08 -2 17 2 131.30 7.66 -2 17 2 119.64 7.12 2 17 -2 115.65 6.85 2 17 -2 136.92 7.87 -2 17 2 135.69 7.92 2 17 -2 103.49 6.31 -2 17 2 112.95 7.13 2 17 -1 160.75 7.72 -2 17 1 193.54 8.68 2 17 -1 174.42 10.16 2 17 -1 159.86 8.28 -2 17 1 168.57 8.39 -2 17 1 170.68 8.51 -2 17 1 189.51 8.76 2 17 -1 183.53 8.36 -2 17 0 13.21 3.07 -2 17 0 8.96 2.79 2 17 0 10.37 3.18 2 17 0 14.34 3.14 2 17 0 8.68 2.74 2 17 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17 -8 34.36 5.12 -2 17 -8 32.31 4.03 2 17 8 23.32 4.17 -2 17 -8 36.67 4.17 2 17 9 22.19 3.95 -2 17 -9 29.12 4.04 -2 17 -9 30.68 4.86 -2 17 -9 30.93 4.16 -2 17 -10 1.77 2.85 2 17 10 4.49 2.41 -2 17 -10 1.44 1.99 -2 17 -10 4.04 2.39 -2 17 -11 21.50 4.09 -2 17 -11 20.95 3.56 2 17 11 17.04 3.50 -2 17 -11 23.38 3.20 -2 17 -11 18.34 3.21 -2 17 -12 71.00 6.68 -2 17 -12 69.65 4.97 2 17 12 54.98 5.25 -2 17 -12 64.74 5.14 -2 17 -12 62.57 5.44 -2 17 -13 73.47 5.47 -2 17 -13 40.88 4.80 -2 17 -13 64.72 6.25 2 17 13 43.66 4.99 -2 17 -14 20.28 2.89 -2 17 -14 21.77 4.01 -2 17 -14 19.06 3.42 2 17 14 16.72 3.02 -2 17 -15 27.63 4.43 2 17 15 27.62 3.51 -2 17 -15 24.55 3.84 -2 17 -16 25.42 3.85 -2 17 -16 32.99 3.25 -2 17 -17 1.35 2.09 -2 17 -17 3.42 1.49 -2 17 -17 0.39 1.99 -2 17 -18 15.29 2.95 -2 17 -18 14.29 2.51 -2 17 -18 11.77 2.58 -2 17 -19 10.16 2.39 -2 17 -19 3.28 1.90 -2 17 -20 1.61 1.40 -2 17 -20 1.18 1.67 -2 17 -21 1.60 1.47 -2 17 -21 8.23 1.82 -2 17 -22 1.42 1.26 -2 17 -22 1.43 1.16 2 18 -22 12.34 2.08 2 18 -22 13.88 1.54 2 18 -21 0.90 1.40 2 18 -21 2.94 1.33 2 18 -20 58.88 3.70 2 18 -20 45.30 4.19 2 18 -19 2.68 1.95 2 18 -19 4.22 1.73 2 18 -18 55.36 4.10 2 18 -18 47.59 4.87 2 18 -17 2.52 2.38 2 18 -17 2.72 1.76 2 18 -16 13.69 3.16 2 18 -16 15.36 2.95 2 18 -16 10.97 2.14 2 18 -15 4.69 2.02 2 18 -15 2.39 2.32 2 18 -15 1.69 2.07 2 18 -14 24.68 3.94 2 18 -14 32.27 3.70 2 18 -14 29.74 3.85 2 18 -13 12.67 3.21 2 18 -13 11.05 2.92 -2 18 13 16.55 2.89 2 18 -13 9.69 2.60 2 18 -12 29.20 4.28 -2 18 12 30.46 3.81 2 18 -12 23.32 4.03 2 18 -12 26.34 3.74 2 18 -11 -0.31 2.48 2 18 -11 9.64 3.17 -2 18 11 9.45 2.47 2 18 -11 4.91 2.83 2 18 -10 14.52 3.58 2 18 -10 12.36 3.37 -2 18 10 17.07 3.03 2 18 -10 17.86 3.31 2 18 -9 7.61 2.78 2 18 -9 6.32 2.49 -2 18 9 6.96 2.35 2 18 -9 11.44 3.02 -2 18 9 10.25 2.66 2 18 -8 32.30 4.67 -2 18 8 49.58 4.53 -2 18 8 46.82 4.57 2 18 -8 35.36 4.62 -2 18 8 30.03 3.84 -2 18 8 29.98 3.67 2 18 -8 32.43 4.26 -2 18 7 16.78 3.22 -2 18 7 13.52 3.08 -2 18 7 14.54 2.91 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2.67 2 18 1 9.15 2.82 2 18 1 -2.39 3.20 -2 18 -1 5.61 2.55 2 18 1 5.93 2.39 -2 18 -1 3.05 2.13 -2 18 -1 2.24 2.41 2 18 2 3.77 2.23 2 18 2 2.49 1.99 -2 18 -2 4.57 2.22 2 18 2 -1.83 2.75 2 18 2 4.18 2.14 -2 18 -2 3.78 2.40 -2 18 -2 1.57 2.33 2 18 3 0.50 2.11 2 18 3 2.17 1.78 -2 18 -3 5.42 2.53 -2 18 -3 1.37 2.42 -2 18 -3 1.78 1.90 2 18 3 -0.87 2.56 2 18 3 2.51 2.00 -2 18 -4 31.64 4.20 2 18 4 25.94 3.80 2 18 4 31.84 3.35 -2 18 -4 24.79 3.57 2 18 4 30.72 4.71 -2 18 -4 27.68 4.04 2 18 4 29.72 3.47 2 18 5 14.04 2.99 2 18 5 10.68 2.42 -2 18 -5 7.71 2.43 -2 18 -5 8.53 2.75 -2 18 -5 11.01 2.93 -2 18 -5 11.15 2.61 2 18 5 10.80 2.71 2 18 5 10.97 3.77 -2 18 -6 64.00 5.73 -2 18 -6 69.60 5.81 -2 18 -6 70.16 5.16 2 18 6 79.78 5.87 2 18 6 79.36 5.01 -2 18 -6 66.59 5.01 2 18 6 81.49 5.26 2 18 6 73.71 6.50 2 18 7 -0.05 2.46 -2 18 -7 4.62 1.82 -2 18 -7 7.79 2.94 2 18 7 5.00 1.83 -2 18 -7 5.30 2.24 -2 18 -7 5.63 2.46 -2 18 -8 73.82 5.54 -2 18 -8 62.50 4.88 2 18 8 56.49 5.92 -2 18 -8 73.68 5.67 -2 18 -9 27.52 3.55 -2 18 -9 31.58 3.96 -2 18 -9 23.70 3.52 2 18 9 27.43 4.32 -2 18 -10 23.56 3.36 -2 18 -10 22.17 3.46 2 18 10 18.39 3.56 -2 18 -10 16.85 3.15 -2 18 -11 3.91 1.87 -2 18 -11 4.65 2.19 2 18 11 1.36 2.17 -2 18 -11 3.35 1.90 -2 18 -12 43.50 3.99 -2 18 -12 44.12 4.27 -2 18 -12 44.90 4.39 2 18 12 36.17 4.30 2 18 13 -2.24 2.33 -2 18 -13 2.90 1.91 -2 18 -13 1.70 1.95 -2 18 -14 107.73 6.34 2 18 14 111.61 6.11 -2 18 -15 4.02 2.06 -2 18 -15 5.65 1.70 -2 18 -15 6.01 2.28 -2 18 -16 4.15 1.53 -2 18 -16 4.49 1.88 -2 18 -16 4.97 2.03 -2 18 -17 1.05 1.60 -2 18 -17 -0.36 1.73 -2 18 -17 -1.12 1.34 -2 18 -18 2.51 1.65 -2 18 -18 4.95 1.78 -2 18 -19 -0.27 1.41 -2 18 -19 1.17 1.44 -2 18 -20 8.35 1.64 -2 18 -20 16.68 2.07 -2 18 -21 -0.07 0.97 2 19 -20 3.09 1.29 2 19 -20 4.31 1.13 2 19 -19 0.78 1.35 2 19 -19 2.80 1.39 2 19 -18 3.12 2.02 2 19 -18 0.74 1.44 2 19 -17 30.51 3.65 2 19 -17 33.92 3.20 2 19 -16 41.94 4.50 2 19 -16 49.11 3.47 2 19 -16 56.41 4.29 2 19 -15 38.06 4.33 2 19 -15 41.13 4.22 2 19 -15 48.49 3.70 2 19 -14 9.70 2.62 2 19 -14 7.80 2.08 2 19 -14 8.17 2.67 2 19 -13 10.45 2.42 2 19 -13 9.48 2.89 2 19 -13 12.08 2.94 2 19 -12 1.13 1.96 -2 19 12 0.86 1.74 2 19 -12 2.76 2.22 2 19 -12 1.73 2.13 2 19 -11 8.45 3.01 2 19 -11 8.27 2.91 -2 19 11 6.06 2.29 2 19 -11 7.80 2.44 2 19 -10 14.72 3.46 2 19 -10 15.99 3.41 2 19 -10 16.51 2.98 -2 19 10 21.31 3.08 2 19 -9 3.12 2.29 -2 19 9 8.33 2.46 2 19 -9 3.89 2.61 2 19 -8 5.87 2.76 -2 19 8 8.26 2.55 2 19 -8 13.15 3.08 -2 19 7 58.07 4.89 -2 19 7 69.40 5.29 2 19 -7 60.36 5.56 -2 19 7 63.10 4.91 2 19 -7 60.37 5.07 -2 19 7 74.44 5.54 -2 19 6 39.33 4.15 2 19 -6 37.98 4.33 2 19 -6 24.66 4.19 -2 19 6 25.38 3.63 -2 19 6 27.71 3.75 -2 19 6 37.58 4.17 -2 19 5 2.29 2.09 2 19 -5 2.68 2.45 -2 19 5 1.37 2.19 -2 19 5 1.75 2.24 2 19 -5 4.64 2.70 -2 19 5 0.38 2.12 2 19 -4 88.92 6.23 -2 19 4 87.15 6.18 -2 19 4 88.29 6.12 -2 19 4 79.94 5.67 -2 19 4 91.78 6.09 2 19 -4 75.31 6.04 2 19 -3 5.08 2.29 -2 19 3 0.48 2.30 -2 19 3 1.11 1.94 -2 19 3 2.13 2.37 2 19 -3 1.80 2.48 -2 19 3 4.49 2.27 2 19 -2 44.35 4.29 2 19 -2 33.28 4.33 2 19 -2 28.48 3.47 -2 19 2 39.25 4.46 2 19 -2 43.62 3.96 -2 19 2 32.37 4.22 -2 19 2 42.34 4.48 -2 19 2 47.08 4.46 -2 19 1 58.71 5.64 2 19 -1 63.11 4.77 2 19 -1 51.72 4.45 -2 19 1 58.76 5.24 -2 19 1 57.72 5.23 2 19 -1 63.41 5.51 -2 19 1 61.47 5.25 -2 19 0 13.83 3.15 -2 19 0 14.85 3.06 2 19 0 12.80 2.60 -2 19 0 18.75 3.69 2 19 0 14.05 3.16 2 19 0 12.83 2.47 -2 19 0 20.82 3.73 -2 19 -1 12.38 3.13 2 19 1 12.88 3.60 -2 19 -1 14.54 3.21 2 19 1 17.21 3.18 2 19 1 13.51 2.61 2 19 1 14.92 2.61 -2 19 -1 15.05 3.05 -2 19 -1 15.92 3.22 2 19 2 1.79 2.05 -2 19 -2 3.32 2.13 2 19 2 3.64 2.98 -2 19 -2 3.30 2.35 -2 19 -2 6.76 2.31 2 19 2 5.00 2.02 2 19 2 5.92 2.41 -2 19 -2 6.29 2.68 2 19 3 20.71 3.08 2 19 3 20.71 3.92 2 19 3 27.74 3.41 -2 19 -3 28.85 4.11 2 19 3 27.87 3.48 -2 19 -3 22.31 3.71 -2 19 -3 25.78 4.19 -2 19 -3 28.68 3.64 -2 19 -4 23.13 3.77 -2 19 -4 24.28 3.20 2 19 4 23.62 3.36 2 19 4 26.41 3.17 -2 19 -4 30.35 4.19 2 19 4 30.86 3.56 2 19 4 25.40 4.39 -2 19 -5 1.64 2.05 2 19 5 0.85 1.60 -2 19 -5 -1.07 1.84 2 19 5 0.58 2.37 2 19 5 -0.30 1.93 -2 19 -5 3.80 2.22 -2 19 -6 7.90 2.60 2 19 6 11.53 3.27 -2 19 -6 17.95 2.94 -2 19 -6 11.00 2.36 -2 19 -6 5.86 2.74 2 19 6 14.15 2.66 -2 19 -7 45.89 4.13 -2 19 -7 41.52 3.96 -2 19 -7 46.45 4.62 -2 19 -7 58.13 5.17 2 19 7 47.98 5.39 -2 19 -8 35.86 3.78 2 19 8 26.96 4.21 -2 19 -8 37.47 4.35 2 19 9 3.16 2.14 -2 19 -9 2.10 1.72 -2 19 -9 3.20 1.98 -2 19 -9 2.96 2.08 -2 19 -10 20.88 3.23 2 19 10 19.88 3.42 -2 19 -10 23.74 3.21 -2 19 -10 18.79 3.01 2 19 11 9.63 2.74 -2 19 -11 10.07 2.57 -2 19 -11 12.73 2.61 -2 19 -11 7.68 2.38 -2 19 -12 18.69 2.85 -2 19 -12 20.14 3.20 -2 19 -12 17.30 2.81 2 19 12 12.59 2.85 2 19 13 35.35 3.59 -2 19 -13 41.42 3.75 -2 19 -13 45.20 3.91 -2 19 -14 10.70 2.40 -2 19 -14 10.26 2.08 -2 19 -15 9.07 1.84 -2 19 -15 5.65 1.90 -2 19 -16 5.94 1.50 -2 19 -16 4.31 1.70 -2 19 -17 -0.88 1.39 -2 19 -18 34.96 2.94 -2 19 -19 8.94 1.53 -2 19 -19 9.59 1.68 2 20 -19 1.22 1.07 2 20 -18 17.43 1.99 2 20 -17 35.41 2.86 2 20 -17 15.98 1.72 2 20 -16 -0.31 1.24 2 20 -16 0.92 1.50 2 20 -15 14.10 1.91 2 20 -15 16.34 2.62 2 20 -14 4.76 1.95 2 20 -14 4.74 1.79 2 20 -13 3.01 1.83 2 20 -13 3.51 1.94 2 20 -12 8.02 2.18 2 20 -12 5.16 2.17 2 20 -11 1.78 1.77 -2 20 11 2.08 1.77 2 20 -11 0.63 1.97 2 20 -10 15.09 2.92 -2 20 10 15.69 2.71 2 20 -10 15.19 2.94 2 20 -9 53.71 5.01 2 20 -9 65.20 5.12 2 20 -8 6.29 2.62 2 20 -8 7.98 2.75 -2 20 8 15.53 2.87 2 20 -7 -0.27 2.07 -2 20 7 3.42 2.04 -2 20 7 5.96 2.20 2 20 -7 4.67 2.37 -2 20 6 15.67 2.91 2 20 -6 6.42 2.37 -2 20 6 14.05 2.79 -2 20 6 9.10 2.80 2 20 -6 8.92 2.61 2 20 -5 13.23 2.83 2 20 -5 8.04 2.56 -2 20 5 14.23 3.02 -2 20 5 16.62 3.13 -2 20 5 16.84 2.93 2 20 -5 10.28 2.69 -2 20 5 16.29 3.26 -2 20 4 11.98 2.85 2 20 -4 8.77 2.60 2 20 -4 5.17 2.35 -2 20 4 9.17 2.54 2 20 -4 -0.35 2.09 -2 20 4 2.70 2.18 -2 20 4 5.46 2.57 -2 20 3 93.35 6.11 2 20 -3 107.08 6.62 2 20 -3 97.54 5.92 2 20 -3 80.23 4.96 -2 20 3 95.51 6.07 -2 20 3 92.15 5.87 -2 20 3 110.69 6.78 -2 20 2 16.33 3.06 -2 20 2 18.31 3.08 -2 20 2 11.16 3.06 2 20 -2 9.37 2.56 2 20 -2 8.39 2.76 -2 20 2 9.37 2.68 2 20 -1 9.54 2.62 -2 20 1 9.72 2.91 -2 20 1 12.41 2.99 -2 20 1 10.99 2.74 -2 20 1 10.56 2.71 2 20 -1 8.27 2.13 2 20 -1 10.15 2.82 -2 20 0 22.53 3.45 -2 20 0 13.98 2.71 -2 20 0 16.83 3.02 2 20 0 12.46 2.46 2 20 0 21.32 3.40 -2 20 0 21.04 3.54 -2 20 -1 27.73 3.61 2 20 1 34.24 3.65 -2 20 -1 22.70 3.58 -2 20 -1 21.75 3.76 -2 20 -1 32.38 3.82 2 20 1 24.04 3.48 -2 20 -2 38.37 4.18 2 20 2 32.71 3.69 2 20 2 29.68 3.14 -2 20 -2 36.95 4.42 -2 20 -2 31.05 3.92 -2 20 -2 29.88 3.79 -2 20 -3 4.71 2.46 -2 20 -3 7.16 2.54 -2 20 -3 8.33 2.93 2 20 3 4.67 2.20 -2 20 -3 4.05 1.80 2 20 3 4.45 1.83 -2 20 -4 2.08 1.61 2 20 4 -1.71 2.11 2 20 4 0.20 2.41 2 20 4 0.04 1.60 -2 20 -4 4.40 2.55 -2 20 -4 0.66 2.29 -2 20 -4 3.12 2.22 -2 20 -5 41.03 4.25 2 20 5 28.29 4.33 -2 20 -5 41.16 4.32 -2 20 -5 33.61 3.53 2 20 5 36.86 3.32 -2 20 -5 36.41 4.39 2 20 5 46.17 4.03 -2 20 -6 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4.93 -4 -12 11 53.64 9.35 -4 -12 10 6.08 4.38 4 12 -10 4.49 2.52 -4 12 10 2.40 2.47 -4 -12 9 50.49 8.43 -4 -12 8 245.95 17.75 -4 12 8 256.34 16.86 -4 -12 7 77.24 9.85 -4 12 7 80.89 9.74 -4 12 6 53.44 8.05 -4 -12 6 46.59 7.42 -4 -12 5 129.91 11.88 -4 12 5 162.08 13.93 -4 12 4 39.00 6.92 -4 -12 4 37.71 6.40 -4 12 3 124.81 12.36 -4 12 2 2.89 2.66 -4 12 1 60.40 8.96 -4 12 0 14.73 4.88 -4 12 -1 32.87 7.05 -4 12 -2 32.26 6.90 -4 12 -3 578.60 28.82 -4 12 -4 64.48 10.20 -4 12 -5 50.63 9.19 -4 12 -6 9.17 5.07 4 12 7 146.18 8.80 -4 12 -7 145.58 16.13 -4 12 -8 92.39 6.71 4 12 8 94.56 7.40 -4 12 -8 76.52 5.65 -4 12 -8 75.06 11.77 4 12 9 28.44 4.87 -4 12 -9 35.63 4.55 -4 12 -9 40.51 9.41 -4 12 -9 37.63 4.43 -4 12 -10 11.28 2.86 -4 12 -10 10.03 4.07 4 12 10 7.30 3.22 -4 12 -10 9.14 2.40 4 12 10 11.35 3.90 -4 12 -11 66.48 5.85 -4 12 -11 60.33 10.63 4 12 11 59.17 10.08 -4 12 -11 72.55 5.82 -4 12 -12 17.26 3.12 -4 12 -12 11.52 5.97 4 12 12 7.69 2.85 -4 12 -12 8.51 2.23 -4 12 -13 -0.92 2.36 -4 12 -14 4.17 2.14 -4 12 -15 32.65 4.58 -4 12 -16 10.32 2.90 -4 12 -17 172.27 8.80 4 12 17 183.62 10.08 -4 -12 -17 172.42 8.88 4 12 18 13.91 3.40 -4 12 -18 18.60 3.43 -4 -12 -18 21.66 3.81 4 12 19 5.94 2.66 -4 12 -19 4.80 2.09 -4 -12 -19 0.39 2.48 -4 -12 -20 7.53 2.87 4 12 20 8.41 2.74 -4 12 -21 0.90 2.25 -4 -12 -21 0.77 2.02 4 12 21 2.62 2.04 4 12 22 4.91 1.90 -4 -12 -22 3.86 2.21 -4 12 -22 3.15 2.35 -4 12 -22 4.06 1.79 4 12 23 44.24 3.37 -4 -12 -23 42.38 3.81 -4 12 -23 42.27 3.36 -4 12 -23 48.06 4.49 -4 12 -24 4.90 2.00 -4 12 -24 3.97 1.36 -4 -12 -24 1.20 1.60 -4 12 -25 1.32 0.89 -4 12 -25 0.09 1.49 -4 -12 -25 3.71 1.47 -4 12 -26 5.06 1.65 -4 13 28 7.58 1.35 4 13 -28 9.23 1.69 -4 13 27 7.41 1.61 4 13 -27 3.99 1.81 4 13 -27 3.84 1.25 4 13 -26 2.48 1.79 -4 13 26 0.64 1.23 -4 13 25 2.33 1.50 -4 13 24 44.70 4.03 -4 13 23 1.54 1.88 -4 13 23 2.91 2.16 -4 13 22 64.10 5.21 4 13 -22 66.59 6.60 -4 13 22 66.05 5.66 -4 13 21 23.46 3.50 -4 13 21 26.15 3.93 4 13 -21 14.04 3.98 -4 13 20 7.34 2.40 4 13 -20 5.91 3.27 -4 13 20 9.76 2.67 -4 13 20 8.50 3.47 -4 13 19 33.59 4.27 -4 13 19 38.24 4.71 -4 13 19 49.58 6.22 4 13 -19 54.87 6.72 4 13 -18 10.35 3.62 -4 13 18 11.34 3.20 -4 13 18 14.28 3.91 -4 13 17 16.34 3.20 -4 13 17 28.88 4.97 -4 13 17 17.95 2.62 4 13 -17 29.55 5.65 -4 13 16 154.89 10.06 -4 13 16 161.09 7.39 -4 13 16 159.53 9.56 4 13 -16 147.76 11.64 -4 13 15 13.86 3.92 4 13 -15 11.05 3.78 -4 13 15 12.08 3.03 -4 13 15 11.33 2.54 -4 13 14 154.49 7.64 -4 -13 14 144.12 15.88 -4 13 14 150.32 9.31 -4 13 14 197.10 11.44 4 13 -14 218.54 13.51 4 13 -13 190.51 12.33 -4 13 13 228.75 9.10 -4 -13 13 214.58 19.45 -4 13 13 210.48 10.84 -4 13 13 182.77 10.91 4 13 -12 290.10 15.31 -4 13 12 259.92 11.79 -4 13 12 288.56 13.53 -4 -13 12 237.73 19.67 -4 13 12 258.73 9.54 4 13 -11 39.87 6.45 -4 13 11 38.37 5.28 -4 13 11 36.98 3.97 -4 13 11 40.90 4.64 -4 -13 11 31.74 7.48 -4 13 10 153.84 7.69 4 13 -10 143.16 8.55 4 13 -10 132.46 10.06 -4 13 10 133.44 6.87 -4 13 10 127.05 8.81 -4 -13 10 133.65 13.94 -4 13 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21 18.74 2.94 -4 13 -21 17.69 3.37 -4 13 -21 21.84 2.90 -4 -13 -21 18.17 2.84 -4 13 -22 22.89 3.33 -4 13 -22 24.09 2.66 -4 -13 -22 19.94 2.68 4 13 22 20.49 2.58 -4 13 -23 -0.25 1.23 -4 -13 -23 -1.61 1.59 -4 13 -23 1.92 1.82 -4 13 -24 64.24 3.20 -4 13 -24 53.34 4.19 -4 13 -25 0.38 1.31 -4 14 27 2.50 0.88 4 14 -27 2.86 1.46 4 14 -26 24.71 2.91 4 14 -26 24.08 2.24 -4 14 26 25.35 2.35 4 14 -25 1.47 1.79 -4 14 25 -1.44 1.39 4 14 -25 -3.84 1.62 4 14 -24 4.88 2.17 -4 14 24 3.55 1.48 -4 14 23 19.18 2.78 -4 14 22 4.53 1.79 -4 14 21 16.73 3.04 -4 14 21 24.31 3.55 -4 14 20 119.97 6.94 -4 14 20 139.69 8.13 4 14 -20 147.41 10.16 -4 14 19 12.89 2.70 -4 14 19 10.44 3.43 -4 14 19 14.63 3.25 4 14 -19 4.67 3.23 -4 14 18 4.59 2.30 -4 14 18 3.41 1.60 -4 14 18 5.22 2.92 4 14 -18 5.04 3.39 -4 14 17 -1.01 2.80 -4 14 17 1.34 1.64 -4 14 17 -0.18 1.99 -4 14 17 1.62 1.93 4 14 -17 1.85 3.01 -4 14 16 62.01 6.69 -4 14 16 54.85 4.59 -4 14 16 58.42 5.78 4 14 -16 67.07 7.65 -4 14 15 11.37 3.94 -4 14 15 6.43 2.69 -4 14 15 9.20 2.68 4 14 -15 11.37 4.45 -4 14 14 141.07 9.80 -4 14 14 134.21 8.49 4 14 -14 145.44 10.94 -4 14 14 152.66 7.36 -4 14 13 2.22 1.85 -4 14 13 -1.85 3.07 4 14 -13 2.52 2.92 -4 14 13 4.11 2.08 -4 14 12 21.30 4.10 -4 -14 12 23.73 6.99 4 14 -12 23.78 5.40 -4 14 12 22.69 3.25 -4 -14 11 10.84 5.97 -4 14 11 14.22 3.45 -4 14 11 10.28 4.07 4 14 -11 14.14 4.56 -4 14 11 10.48 2.59 -4 14 10 3.65 2.71 -4 14 10 7.95 3.11 4 14 -10 8.97 3.91 -4 14 10 8.65 2.58 4 14 -9 51.57 5.12 -4 14 9 52.83 6.31 -4 14 9 46.13 4.58 -4 14 9 58.28 5.14 4 14 -9 57.24 7.00 -4 14 9 58.69 5.62 4 14 -8 50.16 5.18 -4 14 8 80.06 5.56 -4 14 8 40.78 5.47 -4 14 8 72.40 5.25 -4 14 8 54.97 5.05 -4 14 8 58.69 5.45 4 14 -8 53.47 6.32 4 14 -7 1.74 2.66 -4 14 7 6.89 4.45 4 14 -7 1.78 2.32 4 14 -7 6.56 2.67 -4 14 7 5.66 2.33 -4 14 7 5.63 2.69 -4 14 7 -3.92 3.07 -4 14 7 2.56 1.83 -4 14 7 8.18 2.50 -4 14 6 313.37 10.84 4 14 -6 318.04 12.47 -4 14 6 316.35 11.39 4 14 -6 289.70 13.44 -4 14 6 280.01 19.34 -4 14 6 293.64 10.28 -4 14 6 310.29 10.62 -4 14 6 271.18 12.42 4 14 -5 27.68 4.23 -4 14 5 33.30 4.17 4 14 -5 27.23 4.58 -4 14 5 39.10 3.96 -4 14 5 33.11 7.24 -4 14 5 28.27 3.97 -4 14 5 21.11 3.76 -4 14 4 44.80 4.42 4 14 -4 41.16 4.07 -4 14 4 48.21 8.52 -4 14 4 42.55 4.33 4 14 -4 32.43 4.67 -4 14 4 31.57 4.37 -4 14 4 29.13 3.73 4 14 -3 31.70 4.26 -4 14 3 26.20 3.54 4 14 -3 23.04 3.30 -4 14 3 24.86 6.60 -4 14 3 26.89 3.46 -4 14 3 32.73 3.88 -4 14 3 23.84 3.40 4 14 -2 43.97 5.08 -4 14 2 44.64 4.52 4 14 -2 38.22 4.09 -4 14 2 49.21 4.66 -4 14 2 41.53 8.26 -4 14 2 41.80 4.62 -4 14 2 37.59 4.44 4 14 -1 34.97 4.52 -4 14 1 41.11 4.15 -4 14 1 36.48 7.89 -4 14 1 38.07 4.09 -4 14 1 33.71 4.13 -4 14 0 13.38 5.54 -4 14 0 10.16 2.55 -4 14 0 8.47 2.19 4 14 0 10.38 3.08 -4 14 0 12.04 2.84 -4 14 0 10.11 2.51 4 14 1 11.50 3.39 -4 14 -1 2.40 3.14 -4 14 -1 7.60 2.41 4 14 1 7.95 2.58 -4 14 -1 4.73 1.86 -4 14 -1 8.37 2.40 -4 14 -1 7.24 2.26 -4 14 -2 237.08 9.13 4 14 2 263.66 9.85 4 14 2 276.24 11.95 -4 14 -2 267.61 10.45 -4 14 -2 247.89 9.55 -4 14 -2 259.36 20.78 -4 14 -2 234.77 8.78 -4 14 -3 47.22 9.38 -4 14 -3 55.23 4.65 -4 14 -3 43.76 4.34 4 14 3 72.38 6.35 -4 14 -3 71.47 5.26 -4 14 -3 46.51 4.88 4 14 3 50.39 4.48 -4 14 -4 84.48 12.41 -4 14 -4 68.35 5.25 4 14 4 58.94 6.21 -4 14 -4 54.11 4.72 -4 14 -4 66.51 5.00 -4 14 -4 73.78 5.77 -4 14 -4 58.36 5.19 4 14 5 4.44 3.12 -4 14 -5 13.03 5.48 -4 14 -5 3.65 2.25 -4 14 -5 5.36 2.17 -4 14 -5 5.05 2.15 -4 14 -5 2.27 1.86 -4 14 -5 3.03 2.00 4 14 6 5.01 3.14 -4 14 -6 7.23 4.62 -4 14 -6 3.78 2.05 -4 14 -6 4.13 2.83 -4 14 -6 4.15 2.03 -4 14 -6 7.29 2.79 -4 14 -6 3.82 2.10 -4 14 -7 45.90 4.67 -4 14 -7 33.82 4.54 4 14 7 39.85 5.20 -4 14 -7 40.71 4.89 -4 14 -7 56.82 11.10 -4 14 -7 44.00 4.26 -4 14 -7 45.50 4.14 -4 14 -8 214.93 10.71 4 14 8 183.68 10.50 -4 14 -8 186.36 8.39 -4 14 -8 212.09 9.38 -4 14 -8 180.26 9.12 -4 14 -8 207.99 8.46 -4 14 -8 196.58 20.57 -4 14 -9 155.12 9.06 -4 14 -9 148.02 6.83 4 14 9 147.12 9.52 -4 14 -9 137.04 7.54 -4 14 -9 148.02 8.54 -4 14 -9 144.87 6.83 -4 14 -9 143.67 17.11 4 14 10 17.64 4.16 -4 14 -10 13.95 2.48 -4 14 -10 15.70 3.55 -4 14 -10 12.33 2.69 -4 14 -10 12.01 3.30 4 14 11 35.33 5.05 -4 14 -11 34.42 4.96 -4 14 -11 34.66 3.50 -4 14 -11 41.08 5.02 -4 14 -11 25.22 3.48 4 14 12 49.18 5.88 -4 14 -12 54.28 5.59 -4 14 -12 48.07 5.34 -4 14 -12 47.90 4.42 4 14 13 4.66 3.00 -4 14 -13 3.92 2.57 -4 14 -13 3.76 2.83 4 14 14 88.93 7.23 -4 14 -14 98.90 7.40 -4 14 -14 98.96 7.53 4 14 15 20.44 4.42 -4 14 -15 20.50 3.87 -4 14 -15 20.96 4.28 4 14 16 5.16 2.78 -4 14 -16 7.88 2.87 -4 14 -16 9.01 3.25 4 14 17 24.48 3.88 -4 14 -17 27.73 3.83 -4 14 -17 24.16 3.86 4 14 18 42.72 4.79 -4 14 -18 45.99 4.59 -4 14 -18 46.18 5.15 4 14 19 2.16 1.83 -4 14 -19 4.37 2.65 -4 14 -19 3.74 1.95 4 14 20 4.60 1.84 -4 14 -20 8.71 2.68 -4 14 -20 9.90 2.41 4 14 21 2.89 1.60 -4 14 -21 6.06 2.42 -4 14 -21 6.72 2.00 -4 14 -22 19.99 3.24 -4 14 -22 23.02 2.66 -4 14 -23 10.85 1.68 -4 14 -23 16.15 2.49 -4 14 -24 3.03 1.54 4 15 -26 1.44 1.28 4 15 -25 18.11 2.48 4 15 -25 23.89 2.27 -4 15 25 17.29 1.80 -4 15 24 11.57 1.74 4 15 -24 7.72 2.28 4 15 -24 10.94 2.08 -4 15 23 4.75 1.37 4 15 -23 10.17 2.16 4 15 -23 8.42 2.62 4 15 -22 5.08 2.23 -4 15 22 4.08 1.68 -4 15 21 26.48 3.06 4 15 -21 15.92 3.22 -4 15 20 38.44 3.65 4 15 -20 30.73 4.36 -4 15 19 26.07 3.26 -4 15 19 30.21 3.79 4 15 -19 38.54 4.79 -4 15 18 92.57 7.82 -4 15 18 95.04 6.58 4 15 -18 84.72 8.22 -4 15 17 11.15 3.37 -4 15 17 24.53 3.49 4 15 -17 17.77 4.55 -4 15 16 -0.38 2.04 -4 15 16 3.09 2.49 -4 15 16 3.89 1.77 4 15 -16 7.34 3.64 -4 15 15 4.71 3.14 -4 15 15 5.14 2.19 4 15 -15 1.55 3.12 -4 15 15 4.46 2.11 -4 15 14 115.84 6.58 -4 15 14 96.55 8.11 4 15 -14 87.86 8.84 4 15 -13 89.15 7.30 -4 15 13 89.81 5.96 -4 15 13 98.66 8.19 4 15 -13 102.76 9.59 4 15 -12 12.85 3.59 4 15 -12 17.41 4.46 -4 15 12 15.61 4.06 -4 15 12 13.85 2.84 4 15 -11 8.93 3.26 4 15 -11 11.12 3.95 -4 15 11 6.47 2.84 -4 15 11 16.60 2.97 -4 15 11 8.35 3.31 4 15 -10 174.94 9.55 -4 15 10 175.15 10.56 -4 15 10 221.12 9.11 4 15 -10 180.87 11.77 -4 15 10 210.10 9.63 -4 15 9 92.82 7.73 4 15 -9 88.78 6.87 4 15 -9 91.46 8.64 -4 15 9 107.58 6.78 -4 15 9 91.40 6.15 -4 15 9 108.30 7.25 4 15 -8 26.48 4.17 -4 15 8 40.40 4.86 -4 15 8 41.20 4.26 -4 15 8 31.48 4.49 4 15 -8 27.19 5.12 -4 15 8 34.97 4.75 -4 15 8 33.32 4.90 4 15 -7 79.74 6.92 4 15 -7 56.03 5.47 -4 15 7 49.36 5.77 -4 15 7 77.60 5.75 -4 15 7 67.35 5.57 -4 15 7 62.04 5.10 -4 15 7 71.18 5.93 4 15 -7 59.57 6.81 4 15 -6 6.21 2.53 -4 15 6 5.50 3.80 -4 15 6 6.89 2.27 -4 15 6 4.61 2.23 -4 15 6 3.14 2.40 4 15 -6 6.96 2.64 4 15 -6 7.70 3.62 -4 15 6 10.00 2.90 -4 15 6 4.97 2.34 4 15 -5 297.36 12.58 -4 15 5 250.56 10.14 -4 15 5 250.00 10.12 4 15 -5 237.71 9.64 -4 15 5 225.96 18.00 -4 15 5 239.60 10.04 4 15 -5 277.96 12.99 -4 15 5 289.19 11.21 4 15 -4 96.57 7.19 4 15 -4 108.77 6.55 -4 15 4 86.24 6.20 -4 15 4 92.22 6.56 -4 15 4 104.08 6.74 -4 15 4 110.31 6.76 -4 15 4 100.47 12.21 4 15 -3 12.89 3.49 -4 15 3 7.70 2.78 -4 15 3 6.60 2.49 -4 15 3 7.51 2.27 4 15 -3 9.35 3.06 -4 15 3 5.06 3.67 -4 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2.51 -4 15 -14 2.41 2.24 -4 15 -14 3.85 2.72 -4 15 -15 16.11 3.49 4 15 15 12.40 3.47 -4 15 -15 20.00 4.08 4 15 16 57.45 5.64 -4 15 -16 69.95 5.87 -4 15 -16 55.88 5.72 -4 15 -17 3.69 1.91 -4 15 -17 5.24 2.81 4 15 17 5.70 2.39 -4 15 -18 3.28 2.19 -4 15 -18 1.71 1.77 4 15 18 1.10 1.78 4 15 19 8.91 2.21 -4 15 -19 13.94 2.45 -4 15 -19 10.53 2.94 4 15 20 3.27 1.44 -4 15 -20 5.02 1.90 -4 15 -20 5.36 2.44 -4 15 -21 7.86 1.87 -4 15 -21 5.78 2.30 -4 15 -22 0.46 1.19 -4 15 -22 2.25 1.80 -4 15 -23 -0.40 1.29 -4 15 -23 -0.20 1.07 4 16 -25 30.08 2.59 4 16 -24 6.38 1.79 4 16 -24 7.37 1.53 4 16 -23 10.32 2.33 4 16 -23 13.06 2.19 4 16 -22 1.09 1.99 4 16 -22 3.65 1.82 4 16 -21 119.99 7.02 4 16 -21 142.23 6.78 4 16 -20 6.80 2.59 4 16 -20 10.27 3.04 4 16 -19 12.34 3.25 4 16 -18 1.40 2.44 4 16 -18 -0.13 1.64 4 16 -17 10.98 3.06 -4 16 17 12.76 2.77 -4 16 17 13.92 3.55 4 16 -16 2.77 2.31 -4 16 16 1.02 2.44 -4 16 16 2.93 1.86 -4 16 15 151.93 7.27 -4 16 15 139.41 9.00 4 16 -14 12.12 3.51 -4 16 14 13.41 3.28 -4 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4.38 1.87 -5 10 26 8.20 2.40 5 10 -26 6.36 2.58 -5 10 25 -1.82 2.03 5 10 -25 4.08 2.79 -5 10 24 21.16 3.72 5 10 -24 19.10 3.97 5 10 -23 -1.83 2.60 -5 10 23 -0.83 1.96 -5 10 23 0.86 1.98 -5 10 22 19.79 3.74 -5 10 22 21.27 4.31 5 10 -22 18.69 4.53 -5 10 21 19.08 3.98 5 10 -21 18.39 4.72 -5 10 21 19.38 4.60 -5 10 20 6.91 3.44 -5 10 20 4.28 2.56 5 10 -20 3.69 3.44 -5 10 19 6.42 2.81 -5 10 19 8.62 3.44 5 10 -19 0.92 3.44 -5 10 18 2.76 2.21 -5 10 18 5.13 2.89 5 10 -18 3.20 3.48 -5 -10 17 139.35 16.25 -5 10 17 151.16 10.47 5 10 -17 169.93 11.97 -5 -10 16 319.72 23.76 -5 10 16 279.57 13.64 5 10 -16 278.88 15.13 5 10 -16 272.33 10.96 -5 10 15 10.04 3.34 -5 -10 15 10.23 4.37 5 10 -15 18.06 5.24 5 10 -15 13.74 2.87 -5 -10 14 184.92 17.24 -5 10 14 170.27 10.86 5 10 -14 182.82 12.32 5 10 -14 160.56 8.42 -5 -10 13 56.67 10.09 -5 10 13 78.97 7.33 5 10 -13 76.27 7.91 -5 -10 12 5.62 4.55 -5 -10 11 31.91 6.79 -5 -10 10 153.12 14.34 -5 10 10 154.70 12.27 -5 10 9 161.49 12.63 -5 -10 9 174.24 14.94 -5 -10 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12 -14 24.72 4.23 -5 -12 13 20.51 6.49 5 12 -13 23.29 5.21 -5 12 13 28.19 3.56 -5 12 13 21.32 4.49 5 12 -13 25.50 4.03 -5 -12 12 44.95 8.61 -5 12 12 49.97 4.41 -5 12 12 46.04 6.02 5 12 -12 42.31 6.13 5 12 -12 51.42 5.46 -5 -12 11 19.43 6.69 -5 12 11 14.11 4.16 5 12 -11 11.43 3.66 -5 12 11 12.49 2.62 5 12 -11 15.30 3.72 -5 12 11 15.09 3.27 -5 12 10 167.29 10.30 -5 12 10 160.57 7.32 -5 -12 10 162.57 15.67 5 12 -10 162.64 11.11 -5 12 10 178.32 9.02 5 12 -10 177.26 9.47 -5 -12 9 3.53 2.92 -5 12 9 10.20 3.10 -5 12 9 14.63 3.65 -5 12 9 7.80 3.70 5 12 -9 10.23 3.30 5 12 -9 11.95 3.30 -5 12 8 20.44 5.06 -5 -12 8 15.88 4.58 -5 -12 7 149.24 13.81 -5 12 7 144.97 13.38 -5 -12 6 102.31 11.14 -5 12 6 109.19 11.56 -5 12 5 23.24 5.93 -5 -12 5 16.79 4.66 -5 12 4 1.60 2.82 -5 12 3 43.41 8.23 -5 12 2 15.53 5.65 -5 12 1 414.08 24.13 -5 12 0 1.42 3.41 -5 12 -1 487.05 26.88 -5 12 -2 118.20 13.58 -5 12 -3 23.69 6.19 -5 12 -4 14.52 5.52 5 12 5 106.52 7.84 -5 12 -5 108.97 7.12 -5 12 -5 101.20 5.74 -5 12 -5 100.33 6.61 -5 12 -5 104.60 14.11 5 12 6 5.31 3.11 -5 12 -6 4.50 2.56 -5 12 -6 13.49 5.95 -5 12 -6 8.77 3.13 -5 12 -6 9.80 2.95 -5 12 -7 297.70 24.19 5 12 7 278.40 12.91 -5 12 -7 293.53 11.89 -5 12 -7 277.78 11.65 -5 12 -7 298.80 11.55 5 12 8 22.55 4.04 -5 12 -8 27.74 3.67 -5 12 -8 31.39 7.79 -5 12 -8 28.50 4.32 -5 12 -8 21.10 3.55 5 12 9 41.89 5.54 -5 12 -9 51.69 5.37 -5 12 -9 53.97 10.72 -5 12 -9 52.15 5.33 -5 12 -9 48.78 5.44 5 12 10 110.50 8.10 -5 12 -10 106.77 7.38 -5 12 -10 84.88 6.14 -5 12 -10 119.65 8.00 -5 12 -10 88.90 13.29 -5 12 -11 82.10 13.32 -5 12 -11 86.92 6.62 -5 12 -11 93.52 6.80 -5 12 -11 79.88 6.02 -5 12 -12 29.25 4.10 -5 12 -12 22.31 3.59 -5 12 -13 65.39 5.68 -5 12 -13 51.01 4.89 -5 12 -14 2.75 1.89 -5 12 -14 0.87 1.76 -5 12 -15 191.03 8.98 -5 12 -16 17.76 3.06 -5 12 -16 23.75 4.12 5 12 17 29.80 4.54 -5 12 -17 27.85 4.50 -5 -12 -17 31.45 4.08 5 12 18 -1.66 2.84 -5 -12 -18 -1.27 2.34 5 12 19 2.31 2.32 -5 12 -19 2.48 2.62 -5 -12 -19 8.83 2.80 -5 12 -19 5.03 2.02 5 12 20 1.24 2.17 -5 12 -20 -0.20 2.16 -5 -12 -20 -3.47 2.65 -5 12 -20 -0.45 1.69 5 12 21 71.76 5.19 -5 12 -21 54.48 5.10 -5 12 -21 75.21 4.47 -5 -12 -21 55.37 4.66 5 12 22 37.28 3.61 -5 12 -22 42.40 4.34 -5 12 -22 44.05 3.15 -5 -12 -22 36.57 3.36 5 12 23 3.21 1.42 -5 12 -23 1.79 1.23 -5 12 -23 0.35 1.74 -5 -12 -23 0.83 1.55 -5 12 -24 5.52 1.86 -5 -12 -24 2.46 1.24 -5 12 -25 1.92 1.27 -5 13 28 13.58 1.52 5 13 -28 9.34 1.64 5 13 -27 2.79 1.68 -5 13 27 3.18 1.18 5 13 -27 1.77 1.16 -5 13 26 54.01 3.69 -5 13 25 4.74 1.65 -5 13 24 13.34 2.39 -5 13 24 17.59 2.96 -5 13 23 11.71 2.51 -5 13 23 13.23 2.66 5 13 -23 12.30 3.32 -5 13 22 0.82 1.58 -5 13 22 2.81 2.04 5 13 -22 -0.17 2.80 -5 13 21 -1.81 1.99 -5 13 21 3.41 2.07 5 13 -21 6.30 3.71 -5 13 21 6.35 3.30 -5 13 20 101.69 8.43 -5 13 20 89.18 6.85 5 13 -20 94.73 8.46 -5 13 19 16.37 3.63 5 13 -19 14.53 4.42 -5 13 19 16.36 3.40 5 13 -18 11.98 4.31 -5 13 18 12.45 3.81 -5 13 18 7.33 2.86 -5 13 17 17.21 4.04 -5 13 17 25.48 4.29 5 13 -17 12.51 3.91 -5 13 16 51.04 4.37 -5 13 16 53.70 6.44 -5 13 16 48.29 5.49 5 13 -16 57.31 7.45 -5 13 15 82.51 7.19 -5 13 15 59.70 6.74 -5 13 15 85.95 5.65 5 13 -15 52.33 7.48 5 13 -14 534.07 20.75 -5 13 14 531.25 18.78 -5 13 14 473.07 16.51 -5 13 14 469.91 12.75 -5 -13 13 15.81 5.97 -5 13 13 17.69 3.47 -5 13 13 30.80 4.90 -5 13 13 19.76 3.21 5 13 -13 30.28 6.07 5 13 -13 23.10 3.94 -5 -13 12 9.76 5.11 -5 13 12 11.53 2.96 -5 13 12 13.40 4.03 -5 13 12 10.24 2.44 5 13 -12 11.01 3.90 5 13 -12 9.29 2.87 -5 -13 11 1.69 3.61 -5 13 11 4.05 2.41 -5 13 11 1.34 2.66 -5 13 11 3.01 1.91 5 13 -11 1.77 3.01 5 13 -11 2.19 2.65 -5 -13 10 19.64 5.93 -5 13 10 18.44 4.28 -5 13 10 16.48 2.92 5 13 -10 16.16 4.81 -5 13 10 17.94 3.51 5 13 -10 15.43 3.62 -5 13 9 26.94 3.98 -5 13 9 32.96 4.45 5 13 -9 25.75 5.21 -5 -13 9 27.49 7.18 -5 13 9 33.19 3.82 -5 13 9 22.09 4.40 5 13 -9 28.95 4.52 5 13 -8 53.87 5.37 -5 13 8 39.20 4.26 -5 13 8 34.49 7.04 -5 13 8 45.48 4.40 -5 -13 8 30.43 6.87 5 13 -8 42.71 6.15 -5 13 8 60.09 5.54 5 13 -8 46.28 5.10 5 13 -7 65.25 5.81 -5 13 7 68.20 5.29 5 13 -7 57.10 6.25 -5 13 7 56.45 4.82 -5 -13 7 61.41 8.86 -5 13 7 64.63 5.42 -5 13 7 61.20 9.03 5 13 -7 60.75 5.60 -5 13 6 72.12 5.62 -5 13 6 76.24 5.28 5 13 -6 64.48 6.81 5 13 -6 75.16 6.18 -5 13 6 77.63 5.75 -5 13 6 81.72 6.09 -5 13 6 77.09 10.26 5 13 -6 77.87 6.61 5 13 -5 4.82 2.57 -5 13 5 2.90 3.22 -5 13 5 6.07 2.33 -5 13 5 2.45 1.96 -5 13 5 1.16 2.28 -5 13 5 3.17 2.48 5 13 -5 3.34 2.43 5 13 -4 39.17 4.68 -5 13 4 35.61 7.45 -5 13 4 33.78 3.66 -5 13 4 38.97 3.90 -5 13 4 40.31 4.48 -5 13 4 35.80 4.50 5 13 -4 38.69 4.81 5 13 -3 106.54 7.15 -5 13 3 107.11 6.55 -5 13 3 122.00 6.86 -5 13 3 114.36 6.76 -5 13 3 112.25 13.16 -5 13 3 113.69 6.67 5 13 -3 116.62 7.50 5 13 -2 7.54 2.74 -5 13 2 9.65 4.31 -5 13 2 6.79 2.31 -5 13 2 6.87 2.28 -5 13 2 4.22 2.25 -5 13 2 2.51 2.10 5 13 -2 6.87 2.67 -5 13 1 23.99 6.82 -5 13 1 30.15 3.73 -5 13 1 40.58 4.37 5 13 -1 28.91 4.29 -5 13 1 29.49 3.57 5 13 -1 33.96 4.49 -5 13 1 21.99 3.62 5 13 0 239.18 10.81 -5 13 0 218.82 9.20 -5 13 0 205.82 8.01 -5 13 0 237.01 9.08 -5 13 0 232.74 19.14 5 13 1 7.33 2.98 -5 13 -1 11.48 5.41 -5 13 -1 10.27 2.45 -5 13 -1 12.51 2.78 -5 13 -1 11.61 2.76 -5 13 -1 10.58 3.15 -5 13 -2 44.21 8.83 -5 13 -2 32.99 3.92 -5 13 -2 35.64 3.57 5 13 2 43.70 4.97 -5 13 -2 38.86 4.30 -5 13 -2 37.66 4.43 5 13 3 3.80 2.35 -5 13 -3 7.65 3.99 -5 13 -3 7.31 1.96 -5 13 -3 11.91 2.82 -5 13 -3 3.10 2.16 -5 13 -3 8.33 3.03 -5 13 -3 8.03 2.55 5 13 4 3.59 2.70 -5 13 -4 3.82 3.67 -5 13 -4 2.58 2.42 -5 13 -4 3.45 2.26 -5 13 -4 3.21 2.06 -5 13 -4 1.92 1.90 -5 13 -4 12.99 3.05 5 13 5 70.75 6.60 -5 13 -5 84.10 5.72 -5 13 -5 75.83 5.17 -5 13 -5 85.11 6.38 -5 13 -5 64.69 5.86 -5 13 -5 75.57 5.75 -5 13 -5 81.13 12.44 -5 13 -6 118.17 5.97 5 13 6 124.89 8.61 -5 13 -6 124.47 6.64 -5 13 -6 120.90 7.61 -5 13 -6 123.45 7.46 -5 13 -6 144.29 6.80 -5 13 -6 126.87 15.75 5 13 7 2.50 2.88 -5 13 -7 4.39 2.47 -5 13 -7 0.39 2.53 -5 13 -7 -1.16 2.01 -5 13 -7 0.82 2.01 -5 13 -7 1.20 1.94 -5 13 -7 3.95 4.94 -5 13 -7 -2.50 2.42 5 13 8 125.29 8.77 -5 13 -8 130.59 8.10 -5 13 -8 125.06 7.79 -5 13 -8 105.10 15.01 -5 13 -8 123.50 7.45 5 13 9 41.00 5.73 -5 13 -9 47.07 5.30 -5 13 -9 42.55 5.06 -5 13 -9 54.08 5.44 5 13 10 14.48 4.32 -5 13 -10 10.60 2.99 -5 13 -10 11.63 3.26 -5 13 -10 9.81 2.98 5 13 11 7.06 3.21 -5 13 -11 7.89 2.72 -5 13 -11 7.59 2.94 -5 13 -11 6.86 2.69 5 13 12 3.63 2.96 -5 13 -12 7.22 2.51 -5 13 -12 5.62 2.11 -5 13 -12 9.00 3.57 5 13 13 19.55 4.51 -5 13 -13 23.76 3.97 -5 13 -13 28.97 4.52 -5 13 -13 18.31 3.64 -5 13 -14 67.86 5.68 5 13 14 63.87 6.68 -5 13 -14 49.75 4.29 5 13 15 94.02 7.61 -5 13 -15 88.36 6.44 -5 13 -15 94.62 7.53 5 13 16 17.96 4.12 -5 13 -16 11.98 2.99 -5 13 -16 13.39 3.73 5 13 17 1.37 2.46 -5 13 -17 0.43 2.33 -5 13 -17 1.55 1.77 5 13 18 5.10 2.38 -5 13 -18 10.17 2.85 -5 13 -18 8.05 2.21 5 13 19 19.95 3.58 -5 13 -19 24.56 3.25 -5 13 -19 19.69 3.91 -5 13 -20 57.40 4.10 -5 13 -20 65.19 5.39 5 13 20 52.18 4.55 5 13 21 1.01 1.51 -5 13 -21 0.27 1.90 -5 13 -21 2.07 1.49 5 13 22 14.78 2.11 -5 13 -22 16.80 2.13 -5 13 -22 11.82 2.78 -5 13 -23 2.34 1.10 -5 13 -23 -0.51 1.84 -5 13 -24 1.48 1.30 5 14 -27 14.37 1.99 -5 14 26 1.13 0.91 5 14 -26 4.10 1.61 5 14 -26 4.11 1.50 5 14 -25 16.88 2.62 -5 14 25 16.36 2.12 -5 14 24 26.95 2.84 5 14 -24 14.52 2.93 -5 14 23 1.58 1.37 -5 14 22 72.79 5.06 -5 14 22 83.90 5.97 -5 14 21 7.58 2.22 -5 14 21 6.88 2.41 5 14 -21 2.63 2.84 -5 14 20 6.84 2.33 -5 14 20 9.07 3.02 -5 14 20 3.31 1.78 5 14 -20 7.28 3.61 -5 14 19 6.53 2.92 -5 14 19 3.44 1.85 -5 14 19 3.41 2.18 5 14 -19 2.15 2.85 -5 14 18 5.02 2.29 -5 14 18 0.30 2.82 -5 14 18 5.51 2.47 5 14 -18 3.32 3.35 -5 14 17 1.37 2.45 -5 14 17 5.15 2.30 -5 14 17 3.23 1.95 5 14 -17 2.55 2.71 -5 14 16 166.25 10.47 -5 14 16 149.42 9.06 -5 14 16 153.15 7.25 5 14 -16 175.98 11.88 -5 14 15 6.96 2.35 -5 14 15 9.18 3.41 -5 14 15 5.23 2.49 5 14 -15 12.93 4.47 -5 14 14 0.25 1.93 -5 14 14 2.64 2.31 -5 14 14 -2.34 3.32 5 14 -14 1.95 3.27 -5 14 13 3.65 2.13 -5 14 13 0.65 2.70 -5 14 13 -3.23 2.86 5 14 -13 1.16 3.31 5 14 -12 6.05 3.82 -5 14 12 3.53 2.92 -5 14 12 2.95 1.92 -5 14 11 27.18 3.38 5 14 -11 31.29 5.87 -5 14 11 28.61 4.82 -5 14 11 37.45 4.88 -5 14 10 72.64 7.30 -5 14 10 96.02 6.09 5 14 -10 72.36 7.82 -5 14 10 93.93 6.70 5 14 -9 5.74 2.38 -5 14 9 6.52 2.28 5 14 -9 1.72 3.02 -5 14 9 5.82 2.90 -5 14 9 -0.01 2.54 5 14 -9 10.50 3.19 5 14 -8 173.59 9.45 -5 14 8 188.50 9.05 -5 14 8 176.04 8.24 5 14 -8 151.24 10.33 -5 14 8 177.42 8.97 -5 14 8 180.36 15.84 5 14 -8 181.87 10.17 -5 14 8 151.76 10.06 -5 14 7 2.92 4.25 5 14 -7 3.31 2.45 -5 14 7 6.20 2.94 5 14 -7 5.08 3.19 -5 14 7 5.29 2.74 -5 14 7 7.83 2.70 5 14 -7 7.09 3.10 5 14 -6 10.16 3.22 -5 14 6 9.41 2.85 -5 14 6 13.31 5.32 -5 14 6 16.42 3.09 5 14 -6 1.82 2.54 -5 14 6 8.05 2.96 -5 14 6 11.84 3.33 5 14 -6 8.99 3.08 -5 14 5 81.96 5.78 -5 14 5 82.20 5.86 5 14 -5 99.69 7.10 -5 14 5 90.99 6.48 -5 14 5 79.26 10.94 -5 14 5 84.33 6.24 5 14 -5 83.22 6.96 5 14 -4 13.04 3.29 -5 14 4 11.71 5.02 -5 14 4 14.03 3.23 -5 14 4 14.51 2.60 5 14 -4 11.12 2.60 -5 14 4 15.63 2.59 -5 14 4 18.46 3.40 -5 14 4 8.49 2.79 5 14 -4 15.19 3.54 5 14 -3 69.83 6.28 -5 14 3 57.73 4.80 5 14 -3 58.12 4.65 -5 14 3 62.20 5.05 -5 14 3 53.15 9.40 -5 14 3 54.97 5.01 -5 14 3 61.54 5.39 -5 14 3 47.34 4.89 -5 14 2 164.31 8.12 -5 14 2 154.81 7.65 5 14 -2 160.16 8.86 -5 14 2 155.26 8.07 -5 14 2 137.27 7.45 -5 14 2 148.84 15.47 -5 14 2 145.17 7.30 -5 14 1 14.85 6.27 -5 14 1 7.76 2.50 5 14 -1 8.46 3.06 -5 14 1 8.12 2.48 -5 14 1 12.24 2.83 -5 14 1 6.78 2.55 -5 14 1 3.53 2.63 5 14 0 7.89 3.08 -5 14 0 5.42 2.21 -5 14 0 9.40 2.77 -5 14 0 5.66 2.20 -5 14 0 6.37 2.23 -5 14 0 0.82 2.13 5 14 1 13.71 3.43 -5 14 -1 16.67 6.45 -5 14 -1 8.92 2.62 -5 14 -1 9.70 2.59 -5 14 -1 9.74 2.94 -5 14 -1 11.16 3.07 5 14 2 117.29 7.87 -5 14 -2 134.82 6.80 -5 14 -2 129.42 7.50 -5 14 -2 95.22 6.62 -5 14 -2 116.96 6.71 -5 14 -2 112.15 6.93 -5 14 -2 123.80 14.91 5 14 3 83.06 6.89 -5 14 -3 69.11 5.66 -5 14 -3 73.72 5.18 -5 14 -3 68.36 5.17 -5 14 -3 73.28 5.81 -5 14 -3 70.03 5.38 -5 14 -3 70.79 11.59 -5 14 -4 14.92 3.27 5 14 4 18.29 3.92 -5 14 -4 12.56 6.13 -5 14 -4 16.87 3.38 -5 14 -4 13.49 2.68 -5 14 -4 16.40 2.93 -5 14 -4 18.66 3.07 -5 14 -5 6.21 2.73 5 14 5 10.43 3.76 -5 14 -5 3.44 3.89 -5 14 -5 3.88 1.82 -5 14 -5 2.27 2.17 -5 14 -5 3.79 2.55 -5 14 -5 3.95 2.42 5 14 6 175.04 10.82 -5 14 -6 206.97 9.43 -5 14 -6 181.57 8.20 -5 14 -6 174.03 9.32 -5 14 -6 235.06 10.47 -5 14 -6 215.28 8.70 -5 14 -6 210.84 21.09 -5 14 -7 157.56 7.02 -5 14 -7 148.34 8.17 -5 14 -7 170.71 7.67 -5 14 -7 160.85 8.24 5 14 7 174.45 10.47 5 14 8 71.08 6.89 -5 14 -8 70.61 5.81 -5 14 -8 68.03 4.88 -5 14 -8 74.54 5.42 -5 14 -8 66.32 6.06 -5 14 -8 60.01 4.93 5 14 9 17.36 3.68 -5 14 -9 20.92 4.04 -5 14 -9 15.03 3.08 -5 14 -9 14.55 3.03 5 14 10 118.21 8.76 -5 14 -10 116.11 8.13 -5 14 -10 126.07 7.47 -5 14 -10 107.57 7.04 5 14 11 -0.67 2.59 -5 14 -11 -2.22 1.99 -5 14 -11 0.65 2.55 -5 14 -11 -1.68 2.36 -5 14 -12 62.76 6.37 -5 14 -12 72.74 5.75 -5 14 -12 55.10 4.91 5 14 12 64.23 6.66 -5 14 -13 15.63 2.93 5 14 13 13.91 3.60 -5 14 -13 11.89 3.50 -5 14 -13 10.34 2.59 5 14 14 20.09 4.04 -5 14 -14 27.03 4.47 -5 14 -14 19.65 3.34 5 14 15 31.83 4.57 -5 14 -15 38.61 4.87 -5 14 -15 30.09 3.86 5 14 16 50.04 5.32 -5 14 -16 49.60 4.63 -5 14 -16 42.21 5.18 5 14 17 18.70 3.59 -5 14 -17 22.67 3.19 -5 14 -17 17.96 3.41 5 14 18 5.33 2.30 -5 14 -18 5.39 2.66 -5 14 -18 5.47 2.26 5 14 19 4.31 2.05 -5 14 -19 5.09 2.44 -5 14 -19 6.92 1.96 5 14 20 16.27 2.64 -5 14 -20 11.46 2.90 -5 14 -20 12.53 2.26 5 14 21 0.57 1.31 -5 14 -21 2.93 1.79 -5 14 -21 0.48 1.51 5 14 22 25.19 2.17 -5 14 -22 22.27 2.18 -5 14 -22 21.60 3.10 -5 14 -23 0.10 1.40 5 15 -26 0.01 1.24 5 15 -26 1.91 0.93 5 15 -25 7.66 1.82 5 15 -25 9.31 1.74 -5 15 24 15.04 1.84 5 15 -24 12.56 2.51 5 15 -24 15.48 2.25 -5 15 23 54.19 3.46 5 15 -23 59.81 4.75 5 15 -22 3.21 2.21 -5 15 22 0.94 1.21 5 15 -21 4.46 2.21 -5 15 21 8.67 2.00 -5 15 21 10.99 2.59 5 15 -20 18.61 3.56 -5 15 20 24.94 3.39 -5 15 19 12.67 3.53 -5 15 19 18.14 3.13 5 15 -19 18.21 4.26 -5 15 18 10.11 2.57 5 15 -18 6.42 3.76 -5 15 18 6.20 3.04 -5 15 17 25.66 3.12 5 15 -17 26.80 5.48 -5 15 17 24.81 3.57 -5 15 17 24.44 4.27 5 15 -16 8.31 3.78 -5 15 16 5.85 2.91 -5 15 16 0.64 1.96 -5 15 16 4.42 2.11 -5 15 15 0.91 2.64 -5 15 15 3.32 2.17 -5 15 15 1.39 1.92 5 15 -15 -0.94 3.41 -5 15 14 29.29 5.26 -5 15 14 32.20 3.70 5 15 -14 21.86 5.20 5 15 -13 16.14 3.55 -5 15 13 14.59 3.81 5 15 -13 18.97 4.77 -5 15 13 23.32 3.29 -5 15 12 75.51 7.02 5 15 -12 64.31 6.13 -5 15 12 78.03 5.70 5 15 -12 67.30 7.86 5 15 -11 76.16 6.72 -5 15 11 83.53 7.52 -5 15 11 85.42 6.07 5 15 -11 83.87 8.43 5 15 -10 2.95 2.32 -5 15 10 4.36 2.72 -5 15 10 1.94 2.70 -5 15 10 5.20 2.07 5 15 -10 4.82 3.06 5 15 -9 29.12 4.08 -5 15 9 24.81 4.65 -5 15 9 32.00 3.97 5 15 -9 27.28 5.06 -5 15 9 38.05 4.69 -5 15 8 11.37 3.09 -5 15 8 14.34 3.74 5 15 -8 12.37 3.70 -5 15 8 12.80 2.82 -5 15 8 11.84 3.35 -5 15 7 194.83 9.78 -5 15 7 179.36 8.74 5 15 -7 213.59 10.48 -5 15 7 208.01 9.26 -5 15 7 183.84 11.01 5 15 -7 178.12 11.01 5 15 -6 46.90 5.57 5 15 -6 28.79 4.77 -5 15 6 47.23 8.65 -5 15 6 52.57 5.05 5 15 -6 61.00 5.13 -5 15 6 33.79 4.85 -5 15 6 59.95 5.27 -5 15 6 42.76 5.19 5 15 -5 15.03 3.48 -5 15 5 15.69 3.29 5 15 -5 15.30 3.17 -5 15 5 22.65 3.82 -5 15 5 18.21 3.21 -5 15 5 10.13 4.26 -5 15 5 23.27 4.04 5 15 -4 23.54 4.37 -5 15 4 20.92 3.68 -5 15 4 21.04 3.75 5 15 -4 14.23 3.32 -5 15 4 25.53 6.91 -5 15 4 17.77 3.84 -5 15 4 21.71 4.02 5 15 -3 6.40 2.79 -5 15 3 5.69 3.88 -5 15 3 7.46 2.55 5 15 -3 3.71 2.12 -5 15 3 5.01 2.59 -5 15 3 5.68 2.36 -5 15 3 5.61 2.18 -5 15 3 9.53 2.80 5 15 -2 3.50 2.93 -5 15 2 1.74 1.87 -5 15 2 0.12 4.01 -5 15 2 2.12 2.27 5 15 -2 2.44 1.67 -5 15 2 3.71 2.01 -5 15 2 7.24 3.02 -5 15 2 6.23 3.10 -5 15 1 128.50 7.47 -5 15 1 136.81 8.03 -5 15 1 145.69 7.49 5 15 -1 177.10 9.70 -5 15 1 128.40 14.79 -5 15 1 165.71 8.46 -5 15 1 168.21 8.21 5 15 0 113.81 8.34 -5 15 0 108.58 7.11 -5 15 0 113.69 7.05 -5 15 0 119.67 7.14 -5 15 0 132.14 16.19 -5 15 0 118.70 7.29 5 15 1 214.98 10.84 -5 15 -1 200.43 9.79 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15 -9 78.08 6.63 -5 15 -9 68.04 5.47 -5 15 -9 63.90 4.76 -5 15 -10 2.12 2.32 5 15 10 1.93 2.94 -5 15 -10 3.57 2.79 -5 15 -10 0.97 1.72 -5 15 -11 63.27 5.54 -5 15 -11 60.42 5.03 -5 15 -11 62.39 6.15 5 15 11 63.91 6.37 5 15 12 25.41 4.56 -5 15 -12 23.30 4.03 -5 15 -12 18.02 3.00 -5 15 -12 26.08 3.72 5 15 13 10.85 3.44 -5 15 -13 10.51 2.21 -5 15 -13 19.34 3.87 -5 15 -13 12.57 3.07 5 15 14 28.52 4.40 -5 15 -14 37.35 4.27 -5 15 -14 24.92 4.47 5 15 15 7.07 2.75 -5 15 -15 4.07 2.59 -5 15 -15 4.34 2.22 5 15 16 2.08 2.26 -5 15 -16 0.06 2.31 -5 15 -16 -1.05 1.84 5 15 17 0.45 1.90 -5 15 -17 1.15 1.75 5 15 18 2.76 1.84 -5 15 -18 -2.57 2.18 -5 15 -18 1.75 1.74 5 15 19 3.23 1.55 -5 15 -19 4.09 1.76 -5 15 -19 4.17 2.31 5 15 20 2.82 1.43 -5 15 -20 5.03 1.98 -5 15 -20 2.14 1.42 5 15 21 7.05 1.44 -5 15 -21 7.20 2.11 -5 15 -21 3.22 1.39 -5 15 -22 9.77 1.84 -5 15 -22 11.60 1.55 5 16 -25 5.09 1.34 5 16 -25 6.99 1.34 5 16 -24 2.17 1.36 5 16 -24 0.44 1.17 5 16 -23 36.95 3.41 5 16 -23 50.63 3.49 5 16 -22 4.23 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16 7 158.79 10.07 5 16 -7 171.56 8.82 -5 16 7 190.03 8.93 5 16 -7 165.73 10.47 -5 16 7 192.68 9.34 5 16 -6 2.28 2.95 -5 16 6 -2.24 2.89 -5 16 6 1.17 2.29 5 16 -6 1.84 2.30 -5 16 6 1.95 2.04 -5 16 6 2.19 2.66 5 16 -5 72.53 6.70 -5 16 5 65.91 5.68 -5 16 5 76.15 6.03 5 16 -5 72.99 5.69 -5 16 5 81.08 6.10 5 16 -4 2.68 3.11 -5 16 4 2.80 2.56 -5 16 4 0.73 2.88 5 16 -4 0.17 1.88 -5 16 4 2.04 2.19 -5 16 4 -3.01 2.87 5 16 -3 108.86 7.79 -5 16 3 104.82 6.68 5 16 -3 94.18 6.12 -5 16 3 103.76 6.89 -5 16 3 107.39 7.08 -5 16 3 104.15 7.08 -5 16 2 20.75 3.43 -5 16 2 19.82 3.64 5 16 -2 19.37 2.72 5 16 -2 19.14 3.97 -5 16 2 21.62 3.56 -5 16 2 19.70 3.76 -5 16 2 18.58 4.05 5 16 -1 158.50 9.32 -5 16 1 153.53 7.91 -5 16 1 171.53 8.69 -5 16 1 141.73 8.24 -5 16 1 148.68 8.24 -5 16 1 139.20 7.33 5 16 0 14.33 3.91 -5 16 0 12.22 2.90 -5 16 0 8.34 2.65 -5 16 0 12.80 2.78 -5 16 0 17.48 3.40 -5 16 0 14.33 3.64 -5 16 -1 -0.17 2.23 5 16 1 4.59 3.04 -5 16 -1 3.30 2.26 -5 16 -1 0.60 1.99 -5 16 -1 0.56 2.53 -5 16 -1 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8.72 3.63 -7 12 20 5.80 2.58 -7 12 20 4.50 2.91 7 12 -20 5.38 3.70 -7 12 19 190.30 11.61 -7 12 19 183.26 10.52 7 12 -19 182.16 12.03 -7 12 18 3.80 2.41 -7 12 18 4.86 3.01 7 12 -18 4.67 3.66 7 12 -18 -0.44 2.03 -7 12 17 2.22 2.70 7 12 -17 4.36 3.89 7 12 -17 4.54 2.67 -7 12 16 13.50 4.16 7 12 -16 11.42 3.98 7 12 -16 9.79 3.12 -7 12 15 18.72 4.39 7 12 -15 19.49 4.71 7 12 -15 20.09 3.78 -7 12 14 9.42 3.60 7 12 -14 13.16 4.53 7 12 -14 15.42 3.50 -7 12 13 34.29 6.00 -7 12 13 46.58 4.24 7 12 -13 27.02 6.10 7 12 -13 48.03 6.02 7 12 -12 11.85 3.78 -7 12 12 14.10 4.14 7 12 -12 10.79 4.46 -7 -12 12 3.41 3.66 -7 12 12 13.38 2.78 -7 12 11 122.99 6.73 7 12 -11 109.86 9.99 -7 -12 11 107.97 14.14 7 12 -11 126.11 8.67 7 12 -10 13.73 3.30 -7 12 10 8.18 2.67 -7 -12 10 10.82 4.31 7 12 -10 14.45 4.20 -7 12 10 19.31 3.88 7 12 -9 21.43 4.14 7 12 -9 19.70 3.45 -7 12 9 26.19 4.02 -7 -12 9 16.15 4.73 7 12 -9 17.49 4.52 -7 12 9 20.40 3.18 7 12 -8 59.57 5.33 -7 12 8 44.21 7.93 -7 -12 8 49.30 9.30 -7 12 8 54.07 4.65 7 12 -8 48.65 6.18 -7 12 8 67.36 5.93 7 12 -8 59.66 6.20 7 12 -7 40.84 4.90 -7 -12 7 46.27 8.93 7 12 -7 31.77 5.80 -7 12 7 47.52 4.66 -7 12 7 47.77 4.93 -7 12 7 49.89 8.48 7 12 -7 47.10 5.73 7 12 -6 11.09 3.66 7 12 -6 10.28 2.67 -7 12 6 9.03 5.21 -7 -12 6 10.29 4.37 -7 12 6 10.55 2.64 -7 12 6 6.67 2.70 7 12 -5 318.13 12.03 -7 12 5 378.72 11.71 -7 12 5 340.76 11.54 -7 12 5 375.46 12.31 -7 12 5 338.25 21.96 7 12 -5 338.09 13.86 7 12 -4 68.94 5.72 -7 12 4 50.46 8.98 -7 12 4 61.78 5.03 -7 12 4 50.69 4.95 -7 12 4 65.23 5.64 7 12 -4 59.00 6.07 7 12 -3 12.80 3.24 7 12 -3 13.51 3.38 -7 12 3 19.30 6.19 -7 12 3 15.08 3.07 -7 12 3 15.04 2.90 -7 12 3 17.53 3.20 -7 12 3 18.34 3.43 7 12 -2 5.30 2.85 7 12 -2 0.79 2.41 -7 12 2 2.75 3.51 -7 12 2 4.64 2.26 -7 12 2 5.28 2.34 -7 12 2 4.14 2.37 -7 12 2 3.14 2.62 7 12 -1 55.02 5.28 -7 12 1 49.69 9.43 -7 12 1 43.79 4.07 -7 12 1 54.41 4.87 -7 12 1 49.52 4.91 -7 12 1 51.78 4.92 7 12 -1 45.64 5.29 7 12 0 19.49 3.82 -7 12 0 20.71 6.99 -7 12 0 18.27 2.90 -7 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6.10 3.14 8 7 -22 3.02 3.39 -8 7 21 1.85 2.00 -8 -7 21 1.14 2.46 -8 7 21 2.41 3.02 8 7 -21 6.22 3.81 -8 7 20 3.74 2.15 -8 7 20 12.35 3.92 -8 -7 20 8.31 3.32 8 7 -20 8.28 3.81 -8 7 19 135.40 8.48 -8 -7 19 152.28 10.13 -8 7 19 158.63 10.99 8 7 -19 156.94 12.27 8 7 -19 141.04 8.25 -8 7 18 34.72 5.79 8 7 -18 29.12 4.31 -8 7 18 28.08 4.14 -8 -7 18 33.86 5.01 8 7 -17 24.56 4.17 -8 -7 17 18.43 6.72 -8 -7 17 21.66 4.30 -8 7 17 25.70 5.49 8 7 -16 2.57 2.65 -8 -7 16 4.91 4.75 -8 -7 16 5.29 2.90 -8 7 16 5.86 3.34 8 7 -15 7.66 3.07 -8 -7 15 -1.54 3.27 -8 -7 15 2.39 2.82 -8 7 15 5.00 3.65 8 7 -14 8.93 3.29 -8 -7 14 9.79 4.91 -8 -7 14 16.98 3.70 -8 -7 13 123.67 8.83 -8 -7 13 124.94 14.49 -8 -7 12 53.39 9.07 -8 -7 11 41.06 8.23 -8 -7 10 88.79 11.62 -8 -7 9 14.23 4.98 -8 -7 8 21.85 6.20 -8 -7 7 294.92 19.61 -8 7 6 -1.42 2.66 -8 -7 6 1.31 3.91 -8 7 5 336.81 21.99 -8 -7 5 330.44 20.51 -8 7 5 280.87 16.78 -8 -7 4 37.22 6.90 -8 7 4 34.72 6.43 -8 7 4 44.82 8.65 -8 7 3 373.90 20.32 -8 7 3 422.01 24.90 -8 -7 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1.85 -8 -7 -24 5.84 1.76 -8 8 30 7.73 1.57 -8 8 29 4.11 1.60 -8 8 29 6.05 1.83 8 8 -29 3.37 1.45 -8 -8 28 0.26 1.21 -8 8 28 1.08 1.57 8 8 -28 1.07 1.64 -8 8 27 -1.26 1.37 -8 -8 27 -0.07 1.50 -8 8 27 1.26 1.81 8 8 -27 1.08 1.92 -8 8 26 41.66 4.03 -8 -8 26 41.64 4.04 8 8 -26 49.65 5.30 -8 8 25 1.86 1.77 -8 -8 25 3.66 1.99 -8 8 25 3.18 2.19 8 8 -25 8.97 3.73 -8 8 24 31.59 3.98 -8 -8 24 27.83 4.09 -8 8 24 35.40 4.81 -8 8 24 33.94 5.00 8 8 -24 36.25 5.11 -8 8 23 24.26 3.66 -8 -8 23 31.19 4.43 -8 8 23 35.76 4.92 -8 8 23 22.45 4.74 8 8 -23 25.39 5.33 -8 8 22 30.65 4.27 -8 -8 22 35.93 4.85 -8 8 22 36.36 5.54 8 8 -22 30.88 5.57 -8 8 21 78.81 6.44 -8 -8 21 92.15 7.62 -8 8 21 103.63 8.79 8 8 -21 102.42 9.81 -8 -8 20 5.13 2.81 -8 8 20 4.91 3.91 8 8 -20 2.01 3.39 8 8 -19 4.17 2.61 -8 -8 19 9.65 3.29 -8 8 19 7.70 3.68 8 8 -19 8.28 3.91 -8 -8 18 138.58 9.26 -8 8 18 124.08 10.31 8 8 -18 137.80 11.52 8 8 -18 130.98 8.13 8 8 -17 24.84 4.05 -8 -8 17 23.70 4.57 -8 8 17 29.35 5.42 8 8 -17 34.03 6.55 -8 -8 16 96.64 7.76 -8 8 16 84.63 8.47 8 8 -16 69.97 8.94 -8 -8 16 92.99 14.10 8 8 -16 78.82 7.18 -8 -8 15 258.44 12.25 -8 8 15 258.58 14.13 -8 -8 15 225.11 20.27 8 8 -15 255.02 11.48 8 8 -14 7.57 2.87 -8 -8 14 11.04 3.09 -8 -8 14 13.62 6.68 8 8 -13 21.24 4.23 -8 -8 13 23.17 4.43 -8 -8 13 17.49 6.98 8 8 -12 11.27 3.56 -8 -8 12 8.38 2.98 -8 -8 12 4.72 4.01 8 8 -11 3.06 2.85 -8 -8 11 5.46 4.03 -8 -8 10 28.13 7.10 -8 -8 9 132.44 14.37 -8 -8 8 89.22 11.45 -8 -8 7 92.72 11.64 -8 -8 6 63.87 9.77 -8 8 6 75.24 10.45 -8 8 6 58.91 8.57 -8 8 5 30.28 5.99 -8 8 5 42.68 7.89 -8 -8 5 34.09 6.70 -8 8 4 585.22 29.38 -8 -8 4 585.85 27.53 -8 8 4 524.74 24.98 -8 8 3 92.44 11.87 -8 -8 3 89.38 11.33 -8 8 3 71.63 9.48 -8 8 2 5.59 3.08 -8 8 2 8.77 4.32 -8 -8 2 6.26 3.81 -8 8 1 116.14 12.30 -8 8 1 128.32 14.47 -8 -8 1 118.99 13.02 -8 8 0 20.72 5.75 -8 8 0 32.18 7.36 -8 -8 0 17.02 5.65 -8 8 -1 5.23 3.25 -8 8 -1 11.05 5.49 -8 -8 -1 3.52 2.99 -8 8 -1 3.44 3.71 -8 -8 -2 18.00 5.38 -8 8 -2 13.85 5.16 -8 8 -2 13.09 5.33 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3.61 -8 -9 8 238.55 19.44 8 9 -8 224.34 11.23 -8 -9 7 41.60 8.83 -8 9 6 5.01 3.08 -8 -9 6 8.82 4.18 -8 9 5 17.17 5.81 -8 -9 5 15.47 6.24 -8 -9 4 70.49 10.28 -8 9 4 77.59 9.88 -8 9 3 4.11 3.95 -8 -9 3 6.33 4.67 -8 9 2 239.97 18.97 -8 -9 2 246.54 18.71 -8 9 2 259.53 18.79 -8 9 1 114.65 13.11 -8 9 1 106.23 12.73 -8 -9 1 107.23 12.76 -8 -9 0 31.48 7.25 -8 9 0 26.82 7.11 -8 9 0 22.58 5.52 -8 9 -1 2.88 3.91 -8 9 -1 5.12 4.52 -8 -9 -1 -0.52 3.03 -8 9 -2 230.32 19.64 -8 9 -2 254.73 9.55 -8 9 -2 256.45 10.81 -8 9 -3 54.89 9.84 -8 9 -3 51.38 4.66 -8 9 -3 46.96 5.09 -8 9 -4 5.47 4.32 -8 9 -4 6.49 4.74 -8 9 -4 11.89 3.46 -8 9 -4 9.47 3.34 -8 9 -4 9.37 2.28 -8 9 -5 138.42 15.50 -8 9 -5 161.15 8.97 -8 9 -5 141.10 9.20 -8 9 -5 156.59 7.49 -8 9 -6 44.61 4.54 -8 9 -6 43.88 5.46 -8 9 -6 55.24 5.61 -8 9 -7 8.13 4.76 -8 9 -7 7.18 3.01 -8 9 -7 10.46 3.01 -8 9 -7 10.14 4.08 -8 9 -8 0.04 3.77 -8 9 -8 3.48 2.54 -8 9 -8 2.14 2.16 8 9 8 3.81 3.78 -8 9 -8 -0.28 3.06 8 9 9 11.63 5.24 -8 9 -9 8.15 5.72 -8 9 -9 0.52 2.47 -8 9 -9 9.40 2.78 -8 9 -9 7.45 3.43 -8 9 -10 184.66 8.34 -8 9 -10 189.86 9.85 -8 9 -11 -1.10 2.33 -8 9 -11 -0.84 2.28 -8 9 -11 0.47 2.79 -8 9 -12 167.09 8.18 -8 9 -12 162.08 10.04 -8 9 -12 192.30 10.14 -8 -9 -12 193.63 9.84 -8 9 -13 -1.52 2.31 -8 9 -13 4.86 1.96 -8 9 -13 -5.32 3.52 -8 -9 -13 -3.27 2.87 -8 -9 -14 22.87 3.83 -8 9 -14 16.41 3.44 -8 9 -14 16.65 3.09 -8 9 -14 21.11 4.39 -8 -9 -14 19.16 3.84 -8 9 -15 -1.19 2.42 -8 9 -15 -0.42 1.74 -8 -9 -15 6.09 2.89 -8 -9 -15 6.17 2.47 -8 9 -16 38.75 3.57 -8 -9 -16 34.08 3.78 -8 -9 -16 39.62 4.94 -8 9 -17 5.95 1.94 -8 9 -17 5.99 2.52 -8 -9 -17 7.56 2.91 -8 9 -18 17.64 3.46 -8 -9 -18 18.31 3.40 -8 -9 -19 -1.09 2.01 -8 9 -19 -0.80 1.93 -8 9 -20 3.32 1.87 -8 -9 -20 -0.13 2.11 -8 9 -21 2.19 1.76 -8 -9 -21 -0.12 1.86 8 9 22 32.98 3.18 -8 9 -22 24.18 2.61 -8 -9 -22 27.00 2.98 8 9 23 0.66 1.27 -8 -9 -23 0.90 1.27 -8 10 29 3.09 1.17 -8 10 28 23.72 2.56 -8 10 28 28.67 2.99 -8 10 27 6.17 1.96 8 10 -27 6.33 2.31 -8 10 26 11.37 2.56 8 10 -26 8.53 2.79 -8 10 25 2.81 2.11 8 10 -25 -0.42 2.22 -8 10 24 24.14 3.78 8 10 -24 19.85 3.96 -8 10 23 20.06 4.54 -8 10 23 13.98 3.45 8 10 -23 17.48 4.15 -8 10 22 3.55 2.32 -8 10 22 4.45 2.99 8 10 -22 0.69 2.74 -8 10 21 3.54 3.22 -8 10 21 6.65 2.52 8 10 -21 5.89 3.48 -8 -10 20 64.37 5.71 -8 10 20 78.59 7.81 8 10 -20 67.54 7.78 8 10 -20 59.44 5.29 -8 -10 19 14.50 3.26 -8 10 19 12.91 3.88 8 10 -19 16.77 4.90 8 10 -19 15.61 3.36 8 10 -18 2.53 2.68 -8 -10 18 5.55 2.37 -8 10 18 1.80 2.92 8 10 -18 -1.01 3.39 -8 -10 17 38.14 4.84 -8 10 17 38.66 6.20 8 10 -17 41.66 6.74 8 10 -17 50.54 5.33 -8 -10 16 148.67 8.95 -8 10 16 168.03 11.22 8 10 -16 147.55 12.45 8 10 -16 161.68 9.05 8 10 -15 30.42 4.73 -8 -10 15 24.33 3.84 -8 10 15 34.19 6.34 8 10 -15 32.74 6.53 -8 -10 14 45.44 5.40 -8 -10 14 50.78 9.91 -8 10 14 41.74 6.37 8 10 -14 39.37 6.82 8 10 -14 44.83 5.71 8 10 -13 30.03 4.61 -8 -10 13 21.84 3.76 -8 -10 13 30.81 8.44 8 10 -13 29.07 6.12 -8 -10 12 84.93 6.94 8 10 -12 57.13 8.05 -8 -10 12 84.78 12.79 8 10 -12 79.88 7.34 -8 -10 11 78.15 6.39 8 10 -11 76.19 8.45 -8 -10 11 76.00 11.84 8 10 -11 74.29 6.90 -8 -10 10 51.19 5.34 8 10 -10 48.98 6.89 -8 -10 10 38.36 8.68 8 10 -10 47.08 5.82 8 10 -9 24.26 4.61 -8 -10 9 21.08 6.40 -8 -10 9 15.29 3.23 8 10 -9 18.57 5.17 -8 10 9 16.33 3.02 -8 10 9 23.98 4.09 -8 10 8 94.80 6.04 8 10 -8 94.04 9.14 -8 10 8 120.57 7.55 8 10 -8 104.04 7.83 -8 -10 8 111.48 13.45 -8 10 7 60.45 5.04 -8 -10 7 47.36 8.51 8 10 -7 56.08 6.90 -8 10 7 66.86 5.43 8 10 -7 67.45 6.15 -8 10 6 339.89 11.07 -8 10 6 328.36 11.67 -8 10 6 357.23 21.19 8 10 -6 338.73 13.38 -8 10 5 32.05 6.86 -8 10 5 39.13 4.00 -8 10 5 47.20 4.81 8 10 -5 36.65 5.45 -8 -10 5 36.18 7.19 -8 -10 4 127.53 13.68 -8 10 4 114.31 6.92 8 10 -4 132.40 8.09 -8 10 4 113.92 12.86 -8 10 3 41.28 8.15 -8 -10 3 38.58 8.03 -8 10 3 41.42 4.35 8 10 -3 45.98 5.45 -8 -10 2 90.50 11.52 -8 10 2 102.40 6.52 -8 10 2 98.90 6.58 8 10 -2 90.18 6.96 -8 10 2 93.15 12.09 -8 10 1 36.28 7.97 -8 -10 1 33.13 7.29 -8 10 1 40.17 4.38 8 10 -1 30.23 4.44 -8 10 1 41.84 4.30 -8 10 0 14.32 3.10 8 10 0 12.04 3.11 8 10 0 8.60 2.79 -8 10 0 12.29 5.86 -8 10 0 11.42 3.12 8 10 1 16.77 3.43 -8 10 -1 11.80 4.42 -8 10 -1 18.16 3.67 -8 10 -1 21.69 3.23 -8 10 -1 19.51 4.37 8 10 2 5.63 2.59 -8 10 -2 7.82 5.00 -8 10 -2 2.74 2.42 -8 10 -2 4.26 2.32 -8 10 -2 4.19 2.73 8 10 3 130.49 8.41 -8 10 -3 139.51 8.43 -8 10 -3 127.62 8.84 -8 10 -3 136.17 7.33 8 10 4 3.38 2.80 -8 10 -4 5.86 4.11 -8 10 -4 -1.21 2.37 -8 10 -4 6.95 2.74 -8 10 -4 0.99 2.82 -8 10 -5 9.50 4.94 -8 10 -5 5.49 2.69 -8 10 -5 5.34 2.62 -8 10 -5 3.93 2.73 -8 10 -6 191.67 20.36 -8 10 -6 216.95 9.56 -8 10 -6 209.13 10.63 -8 10 -6 196.87 11.04 -8 10 -7 0.63 4.98 -8 10 -7 8.57 3.74 -8 10 -7 3.32 2.59 -8 10 -7 2.06 3.83 -8 10 -8 46.21 5.42 -8 10 -8 41.38 5.61 -8 10 -8 47.97 4.62 -8 10 -9 2.02 2.59 -8 10 -9 1.63 2.05 -8 10 -9 5.64 3.51 -8 10 -10 7.32 2.78 -8 10 -10 9.57 2.67 -8 10 -11 37.29 4.11 -8 10 -11 39.96 5.18 -8 10 -12 5.48 2.94 -8 10 -12 1.31 1.87 -8 10 -13 28.70 4.66 -8 10 -13 21.21 3.33 -8 10 -14 201.74 8.55 -8 10 -14 218.18 10.63 -8 10 -15 8.47 3.03 -8 10 -15 4.83 1.92 -8 -10 -15 9.59 3.28 -8 10 -16 3.90 2.48 -8 10 -16 1.94 1.62 -8 -10 -16 7.91 2.58 -8 10 -17 23.97 3.90 -8 10 -17 19.76 2.87 -8 -10 -17 30.13 3.88 -8 10 -18 2.24 2.26 -8 10 -18 -0.55 1.43 -8 -10 -18 0.38 2.02 -8 10 -18 1.25 1.56 -8 10 -19 7.43 2.44 -8 -10 -19 2.84 1.77 -8 10 -19 3.04 1.36 8 10 20 21.89 3.07 -8 10 -20 17.83 2.92 -8 -10 -20 17.63 2.67 8 10 21 5.63 1.93 -8 -10 -21 1.74 1.43 8 10 22 3.36 1.45 -8 10 -22 1.16 1.29 8 10 23 10.42 1.44 -8 11 28 2.94 1.22 -8 11 27 5.04 1.55 -8 11 27 2.66 1.50 8 11 -27 0.46 1.52 -8 11 26 1.67 1.39 -8 11 26 6.06 2.05 8 11 -26 2.94 1.82 -8 11 25 7.17 2.27 8 11 -25 6.59 2.31 -8 11 24 5.10 2.17 8 11 -24 -0.63 2.47 -8 11 23 18.59 3.42 -8 11 23 22.96 4.19 8 11 -23 20.02 4.20 -8 11 22 41.27 4.97 -8 11 22 39.23 5.31 8 11 -22 29.73 5.00 -8 11 21 48.71 5.52 -8 11 21 49.06 6.32 8 11 -21 47.82 6.05 -8 11 20 3.89 3.07 -8 11 20 1.49 2.10 8 11 -20 4.33 3.01 8 11 -20 5.78 2.21 -8 11 19 20.38 4.47 8 11 -19 25.98 5.17 8 11 -19 30.28 4.02 -8 11 18 -4.37 3.30 8 11 -18 -3.45 3.79 8 11 -18 1.36 2.07 -8 11 17 15.53 4.36 8 11 -17 18.85 4.97 8 11 -17 15.27 3.53 8 11 -16 18.16 3.79 -8 11 16 15.47 4.45 8 11 -16 15.01 4.37 8 11 -15 5.27 2.98 -8 11 15 0.42 2.96 8 11 -15 5.01 3.97 8 11 -14 5.19 2.74 8 11 -14 -2.70 3.60 -8 11 14 2.22 2.88 8 11 -13 10.71 3.32 -8 11 13 7.33 3.22 8 11 -13 6.52 3.50 8 11 -12 35.71 5.19 -8 -11 12 33.14 7.93 8 11 -12 38.63 6.28 -8 11 11 143.22 7.30 8 11 -11 122.43 10.68 -8 -11 11 142.38 16.65 8 11 -11 143.34 9.48 8 11 -10 6.24 3.56 -8 -11 10 5.35 4.56 -8 11 10 2.50 2.05 8 11 -10 5.18 2.98 8 11 -9 4.90 2.82 -8 -11 9 0.33 4.17 8 11 -9 1.45 2.81 -8 11 9 4.43 1.78 -8 11 9 3.89 2.80 -8 11 8 67.85 5.47 8 11 -8 45.70 6.85 -8 11 8 80.26 6.37 8 11 -8 55.16 6.62 -8 -11 8 63.15 11.75 -8 -11 7 107.87 13.25 -8 11 7 117.58 6.97 8 11 -7 115.52 9.75 -8 11 7 142.46 8.27 8 11 -7 141.82 9.41 8 11 -6 4.16 2.63 8 11 -6 0.50 2.07 -8 11 6 1.44 3.02 -8 11 6 1.42 1.82 -8 11 6 -3.10 2.64 -8 -11 6 -6.50 4.92 8 11 -5 70.43 5.68 -8 -11 5 65.72 10.60 -8 11 5 72.09 5.62 -8 11 5 80.18 5.98 -8 11 5 66.92 10.16 8 11 -5 80.16 6.92 8 11 -4 16.51 4.01 8 11 -4 12.99 2.79 -8 11 4 12.52 5.32 -8 -11 4 25.45 7.34 -8 11 4 18.74 3.20 -8 11 4 13.25 3.18 8 11 -3 41.20 4.34 8 11 -3 32.48 4.66 -8 11 3 35.33 7.71 -8 11 3 33.16 3.90 -8 11 3 39.75 4.30 8 11 -2 35.17 4.30 -8 11 2 54.27 4.59 -8 11 2 47.22 4.96 -8 11 2 39.43 5.15 -8 11 2 46.26 5.04 -8 11 2 46.05 4.74 8 11 -2 39.47 5.21 -8 11 2 56.29 10.27 8 11 -1 23.44 3.95 8 11 -1 25.18 3.66 -8 11 1 23.76 6.59 -8 11 1 22.17 3.31 -8 11 1 20.70 3.92 -8 11 1 27.20 3.72 -8 11 1 19.28 3.10 8 11 0 2.91 2.36 8 11 0 -1.27 2.40 -8 11 0 -1.93 3.54 -8 11 0 1.72 2.50 -8 11 0 -1.49 2.18 -8 11 0 -0.25 2.28 -8 11 0 3.58 2.22 8 11 1 95.81 7.31 -8 11 -1 92.26 7.19 -8 11 -1 94.07 7.38 -8 11 -1 116.49 7.95 -8 11 -1 101.07 6.44 -8 11 -1 105.43 7.12 8 11 1 91.47 6.70 -8 11 -1 107.67 14.10 8 11 2 85.58 6.61 -8 11 -2 92.66 7.16 -8 11 -2 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12 -14 37.12 6.19 8 12 -14 45.02 5.47 8 12 -13 37.78 5.17 -8 12 13 34.24 5.86 8 12 -13 31.40 5.72 -8 12 12 54.64 4.68 8 12 -12 66.60 7.98 8 12 -12 68.73 6.68 -8 12 11 50.94 4.57 8 12 -11 38.12 6.39 8 12 -11 45.88 5.90 8 12 -10 2.37 2.77 -8 12 10 1.24 1.71 8 12 -10 0.12 2.95 -8 12 9 174.55 8.22 8 12 -9 154.54 11.21 -8 12 9 196.83 10.05 8 12 -9 183.50 10.60 -8 -12 9 153.34 16.77 8 12 -8 -0.49 2.46 8 12 -8 2.29 2.53 -8 12 8 2.25 2.87 -8 -12 8 -1.54 3.78 8 12 -8 0.84 2.78 -8 12 8 3.65 2.26 8 12 -7 126.48 7.41 -8 -12 7 118.60 14.12 -8 12 7 132.66 7.43 8 12 -7 97.00 8.64 -8 12 7 154.40 8.55 8 12 -7 123.84 9.13 8 12 -6 20.65 4.41 8 12 -6 26.59 3.70 -8 12 6 17.85 5.80 -8 12 6 20.23 3.35 -8 12 6 26.62 4.31 8 12 -5 43.46 5.11 -8 12 5 42.12 8.27 -8 12 5 50.52 4.74 -8 12 5 63.42 5.65 8 12 -5 48.69 6.05 8 12 -4 30.93 4.66 8 12 -4 31.54 3.97 -8 12 4 33.16 4.50 -8 12 4 23.76 3.62 8 12 -3 2.55 2.47 8 12 -3 8.34 2.91 -8 12 3 0.56 3.03 -8 12 3 2.22 2.03 -8 12 3 1.77 2.33 8 12 -2 2.07 2.50 8 12 -2 4.20 2.24 -8 12 2 -4.46 5.00 -8 12 2 2.07 2.64 -8 12 2 3.08 2.13 -8 12 2 -1.32 2.31 -8 12 2 1.25 2.60 8 12 -1 187.60 9.62 -8 12 1 192.76 8.41 -8 12 1 227.88 9.95 -8 12 1 226.04 10.25 -8 12 1 186.45 9.10 8 12 -1 203.38 10.39 -8 12 1 195.88 18.78 8 12 0 83.24 6.52 -8 12 0 91.51 6.30 -8 12 0 79.48 6.73 -8 12 0 74.96 6.27 -8 12 0 85.67 5.90 8 12 0 68.25 6.09 -8 12 0 67.59 11.45 8 12 1 12.48 3.32 -8 12 -1 19.35 6.92 -8 12 -1 11.04 2.64 -8 12 -1 12.67 3.36 -8 12 -1 15.26 3.79 8 12 1 17.50 3.41 8 12 2 18.71 3.66 -8 12 -2 16.52 6.02 -8 12 -2 15.64 3.32 -8 12 -2 17.47 3.48 -8 12 -2 18.48 3.33 -8 12 -2 22.92 4.23 8 12 2 17.20 3.20 8 12 3 3.55 2.75 -8 12 -3 2.41 4.03 -8 12 -3 1.71 2.42 -8 12 -3 4.38 2.58 -8 12 -3 -0.16 1.90 -8 12 -3 0.69 2.16 8 12 4 14.36 3.76 -8 12 -4 8.53 3.46 -8 12 -4 10.66 3.07 -8 12 -4 6.04 2.43 -8 12 -4 5.27 3.09 8 12 5 145.05 9.25 -8 12 -5 145.83 8.75 -8 12 -5 125.14 8.80 -8 12 -5 155.59 8.08 -8 12 -5 133.79 6.94 8 12 6 62.40 6.38 -8 12 -6 57.94 5.11 -8 12 -6 76.85 6.74 -8 12 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136.59 7.39 8 13 -10 118.57 9.74 8 13 -9 1.65 2.64 -8 13 9 2.37 2.04 -8 13 9 1.28 2.97 8 13 -9 4.39 2.95 8 13 -8 17.59 3.47 8 13 -8 17.62 4.15 -8 13 8 17.12 3.29 -8 13 8 22.78 4.12 8 13 -8 22.09 4.40 8 13 -7 110.24 7.07 -8 13 7 100.14 6.57 -8 13 7 127.37 7.79 8 13 -7 106.07 8.23 8 13 -6 3.02 2.34 -8 13 6 2.63 2.06 -8 13 6 1.06 2.56 8 13 -6 4.34 2.77 8 13 -5 7.87 2.55 -8 13 5 6.54 4.60 -8 13 5 13.56 2.83 -8 13 5 8.64 2.96 8 13 -5 10.48 3.40 8 13 -4 83.79 6.38 -8 13 4 81.10 6.36 -8 13 4 79.62 6.10 -8 13 4 72.53 11.63 8 13 -4 67.77 6.52 8 13 -3 6.37 2.67 -8 13 3 -3.77 4.00 -8 13 3 1.22 2.12 -8 13 3 3.85 2.62 8 13 -3 0.89 2.26 8 13 -2 39.04 4.75 -8 13 2 25.14 3.77 -8 13 2 38.27 4.70 -8 13 2 36.12 4.43 8 13 -2 29.12 4.58 8 13 -1 4.98 2.71 -8 13 1 1.89 2.17 -8 13 1 5.87 2.28 -8 13 1 3.65 2.44 -8 13 1 -0.22 2.39 8 13 -1 2.89 2.45 8 13 0 48.11 5.49 -8 13 0 35.89 4.22 -8 13 0 52.34 5.42 -8 13 0 55.13 5.52 -8 13 0 46.26 4.85 8 13 0 44.63 5.00 8 13 1 1.47 2.40 -8 13 -1 10.88 3.22 -8 13 -1 7.14 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-17 -8 8 11.60 1.83 -17 -8 7 0.87 1.14 -17 -8 6 -2.65 1.28 -17 -8 5 6.96 1.55 -17 -8 4 -0.31 1.05 0 0 0 0.00 0.00 TITL 87cmcm20 in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 1.54184 14.391003 19.586834 26.961671 90.0000 102.0377 90.0000 ZERR 7.00 0.000804 0.000614 0.000910 0.0000 0.0046 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O Al P Ag UNIT 350.00 420.00 28.00 14.00 7.00 7.00 7.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 93343 _shelx_fab_file ; -17 0 2 1.5609 -0.8899 -17 0 4 0.4931 -0.1810 -17 0 6 0.7920 0.1099 -17 0 8 -1.2046 -0.0497 -17 0 10 0.0790 -0.0280 -17 0 12 0.0875 -0.4437 -17 0 14 -0.4159 -0.2608 -17 0 16 0.7932 -0.1189 -17 1 1 -0.8380 0.2249 -17 1 2 -1.6661 -0.2105 -17 1 3 -1.0876 0.4837 -17 1 4 0.6488 0.1885 -17 1 5 -1.1674 0.0116 -17 1 6 0.4779 0.0029 -17 1 7 0.1687 0.1570 -17 1 8 -1.4347 -0.2080 -17 1 9 0.7092 -0.0049 -17 1 10 0.4084 -0.1267 -17 1 11 -0.4589 0.0086 -17 1 12 0.5232 0.1568 -17 1 13 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15 2 11 -0.1677 -0.1953 15 2 12 -0.6710 -0.0790 15 3 0 -0.1824 -0.0848 15 3 1 0.6454 0.4094 15 3 2 0.4780 0.0087 15 3 3 2.0350 0.2137 15 3 4 0.3076 0.2458 15 3 5 1.9267 -0.0662 15 3 6 2.7019 0.1140 15 3 7 0.6199 -0.2319 15 3 8 0.3184 -0.0862 15 3 9 -3.9206 -0.0554 15 3 10 -1.1186 -0.2941 15 3 11 0.0836 -0.4190 15 3 12 0.4582 0.0422 15 4 0 0.4916 -0.0357 15 4 1 1.4923 0.0740 15 4 2 -1.9930 -0.0420 15 4 3 -1.5001 -0.1959 15 4 4 -2.0021 -0.0462 15 4 5 0.1096 -0.2310 15 4 6 -2.2597 -0.0702 15 4 7 -1.7135 0.0601 15 4 8 1.9569 -0.2286 15 4 9 0.0313 0.2361 15 4 10 1.5716 0.2104 15 4 11 0.2872 0.0894 15 5 0 -2.5025 -0.1658 15 5 1 -0.3191 -0.1782 15 5 2 0.1439 0.0708 15 5 3 3.2519 -0.1155 15 5 4 0.8593 -0.1529 15 5 5 1.1611 0.1808 15 5 6 -0.9016 -0.0579 15 5 7 0.2491 0.3629 15 5 8 1.5065 -0.1144 15 5 9 -1.3251 0.0621 15 5 10 -0.3101 0.1791 15 5 11 -0.3890 -0.4484 15 6 0 1.2133 0.0629 15 6 1 1.6934 0.0527 15 6 2 -1.4137 0.1450 15 6 3 -0.8370 0.2102 15 6 4 -2.2915 -0.0315 15 6 5 1.1328 0.3240 15 6 6 0.6873 -0.0653 15 6 7 -0.1478 0.0560 15 6 8 0.5725 -0.1739 15 6 9 -0.3636 -0.2409 15 6 10 -0.3231 0.2603 15 7 0 -2.5092 0.0028 15 7 1 0.1821 0.0264 15 7 2 -0.2491 -0.0773 15 7 3 1.8791 0.0372 15 7 4 -0.2931 -0.1655 15 7 5 0.1175 -0.2252 15 7 6 -0.9200 -0.1132 15 7 7 -2.6157 -0.1894 15 7 8 -0.3453 0.0527 15 7 9 1.3005 0.0766 15 7 10 1.4688 0.1735 15 8 0 0.2929 -0.0872 15 8 1 1.6821 -0.0427 15 8 2 -2.0587 -0.1242 15 8 3 -0.2356 -0.1145 15 8 4 -0.7747 0.1357 15 8 5 1.0055 -0.1540 15 8 6 2.9516 0.3216 15 8 7 0.2735 0.2123 15 8 8 0.8466 0.1149 15 8 9 0.2920 0.0323 15 9 0 -2.3465 0.0082 15 9 1 1.2699 0.0687 15 9 2 0.4155 0.1815 15 9 3 1.8041 0.0988 15 9 4 -1.4428 0.3201 15 9 5 -1.5746 -0.0616 15 9 6 0.8300 -0.0302 15 9 7 -2.2892 -0.1187 15 9 8 -0.9577 -0.2293 15 10 0 -0.1095 0.0589 15 10 1 0.1978 -0.1027 15 10 2 -2.0729 -0.0956 15 10 3 0.5377 -0.2345 15 10 4 0.1887 -0.2328 15 10 5 -0.0095 -0.0486 15 10 6 1.5871 -0.1449 15 11 0 -0.2638 0.1377 15 11 1 1.4941 0.0473 15 11 2 0.8299 0.1488 15 11 3 1.1097 0.0838 15 11 4 -0.2119 0.0584 15 12 0 -0.2089 -0.1598 15 12 1 -0.2513 -0.1546 16 0 0 -1.4463 -0.3435 16 0 2 2.0569 -0.2580 16 0 4 -2.6295 -0.5768 16 0 6 -1.8884 -0.4906 16 0 8 -0.9412 0.2929 16 1 0 -0.6962 -0.2707 16 1 1 -0.3295 0.2923 16 1 2 0.4725 -0.4939 16 1 3 -0.2344 0.2115 16 1 4 -0.6968 -0.2723 16 1 5 2.9440 0.2358 16 1 6 0.4042 0.1201 16 1 7 1.6119 0.0030 16 1 8 -0.0280 0.4036 16 1 9 0.4279 0.1932 16 2 0 -1.1069 -0.6712 16 2 1 -0.5551 0.4947 16 2 2 0.4704 0.0553 16 2 3 1.0665 0.2024 16 2 4 -1.2678 0.0841 16 2 5 0.4389 0.2092 16 2 6 -2.6634 0.3022 16 2 7 -0.6667 -0.3409 16 2 8 -1.6628 -0.3837 16 3 0 -0.1921 0.0191 16 3 1 -0.0925 0.1677 16 3 2 0.0258 -0.0836 16 3 3 0.5103 -0.2622 16 3 4 -2.2277 0.0160 16 3 5 1.7892 -0.1029 16 3 6 0.6219 -0.2431 16 3 7 2.5703 -0.0919 16 3 8 0.3528 -0.2225 16 4 0 -0.3654 -0.0275 16 4 1 0.5228 -0.2742 16 4 2 0.3925 0.1680 16 4 3 1.1517 -0.0285 16 4 4 -1.6613 -0.1999 16 4 5 1.2504 0.0527 16 4 6 -1.8121 0.0501 16 4 7 -0.8181 0.4408 16 4 8 -1.1589 -0.3886 16 5 0 -1.5527 0.0456 16 5 1 -1.2199 -0.1429 16 5 2 -1.0098 0.1491 16 5 3 1.6263 0.1575 16 5 4 -1.1683 -0.0700 16 5 5 1.3121 0.2033 16 5 6 0.2384 0.0498 16 6 0 1.1924 0.0735 16 6 1 1.4105 0.0556 16 6 2 0.0536 -0.0131 16 6 3 1.3064 -0.0044 16 6 4 -2.4093 -0.0653 16 6 5 -0.0771 -0.2187 16 6 6 -1.4219 0.1355 16 7 0 0.0837 -0.0438 16 7 1 -2.0359 0.0507 16 7 2 -1.9877 -0.0622 16 7 3 2.4318 -0.1014 16 7 4 0.4856 0.2272 16 7 5 2.0828 -0.2297 16 8 0 1.5994 -0.1277 16 8 1 2.2714 -0.0426 16 8 2 -0.4583 0.0726 16 8 3 -0.3337 -0.0674 16 8 4 -3.0918 0.0789 16 9 0 -0.6191 0.0759 16 9 1 -1.0414 0.0197 16 9 2 -1.8150 0.0793 16 9 3 1.8060 0.1198 16 10 0 1.3254 0.1163 16 10 1 2.6863 -0.0461 17 0 0 -1.3885 -0.3479 17 0 2 0.5709 -0.6097 17 0 4 2.4256 0.0601 17 1 0 -0.9484 -0.5723 17 1 1 2.1104 0.4105 17 1 2 0.8716 -0.0394 17 1 3 -2.8643 0.0594 17 1 4 -0.1309 0.0531 17 2 0 -1.2424 0.1246 17 2 1 0.2468 0.2458 17 2 2 0.1580 0.1951 17 2 3 -1.3836 -0.0819 17 2 4 1.8634 0.2013 17 3 0 -0.0845 0.0572 17 3 1 0.3725 -0.2130 17 3 2 1.5565 -0.0238 17 3 3 -1.2778 -0.4532 17 4 0 -0.1248 -0.0447 17 4 1 -0.9393 -0.2265 17 4 2 1.6293 0.1310 17 5 0 0.6715 0.0114 17 5 1 -1.0311 0.1960 17 6 0 0.5806 0.0357 0 0 0 0.0 0.0 ; _shelx_fab_checksum 99421 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.690 _oxdiff_exptl_absorpt_empirical_full_min 0.660 _publcif_funding_html ; ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ag1 Ag 0.24207(3) 0.63997(2) 0.57589(2) 0.05537(16) Uani 1 1 d . . . . . P1 P 0.13048(10) 0.69899(7) 0.51436(5) 0.0474(3) Uani 1 1 d . . . . . Al1 Al 0.55700(10) 0.60705(7) 0.71325(5) 0.0346(3) Uani 1 1 d . . . . . O1 O 0.4481(2) 0.55497(15) 0.70171(11) 0.0366(6) Uani 1 1 d . . . . . O2 O 0.6161(2) 0.55302(16) 0.77512(11) 0.0358(6) Uani 1 1 d . . . . . N1 N 0.3245(3) 0.5783(2) 0.63385(14) 0.0418(9) Uani 1 1 d . . . . . N4 N 0.5573(3) 0.67418(19) 0.76427(15) 0.0391(8) Uani 1 1 d . . . . . N3 N 0.6577(3) 0.5639(2) 0.68988(14) 0.0393(8) Uani 1 1 d . . . . . N2 N 0.4707(3) 0.64040(19) 0.65396(14) 0.0380(8) Uani 1 1 d . . . . . C51 C 0.4089(3) 0.5919(2) 0.66065(16) 0.0342(8) Uani 1 1 d . . . . . C5 C 0.8261(4) 0.4440(3) 0.80365(19) 0.0480(11) Uani 1 1 d . . . . . H5 H 0.864459 0.420372 0.830171 0.058 Uiso 1 1 calc R . . . . C2 C 0.7159(4) 0.5189(3) 0.72288(17) 0.0413(10) Uani 1 1 d . . . . . C1 C 0.6960(3) 0.5150(2) 0.77144(16) 0.0358(9) Uani 1 1 d . . . . . C10 C 0.6706(4) 0.5583(3) 0.86566(18) 0.0468(11) Uani 1 1 d . . . . . C37 C 0.5338(4) 0.7456(2) 0.75937(18) 0.0419(10) Uani 1 1 d . . . . . C38 C 0.4390(4) 0.7664(3) 0.75234(18) 0.0453(11) Uani 1 1 d . . . . . C15 C 0.6240(4) 0.5868(2) 0.82112(17) 0.0400(10) Uani 1 1 d . . . . . C6 C 0.7485(4) 0.4820(2) 0.81296(17) 0.0419(10) Uani 1 1 d . . . . . C4 C 0.8465(4) 0.4411(3) 0.75526(19) 0.0485(12) Uani 1 1 d . . . . . C39 C 0.4204(5) 0.8373(3) 0.7512(2) 0.0548(13) Uani 1 1 d . . . . . H39 H 0.357677 0.852046 0.746167 0.066 Uiso 1 1 calc R . . . . C14 C 0.5864(4) 0.6525(3) 0.81425(18) 0.0445(11) Uani 1 1 d . . . . . C45 C 0.3577(4) 0.7157(3) 0.7473(2) 0.0493(12) Uani 1 1 d . . . . . H45 H 0.381707 0.670990 0.739473 0.059 Uiso 1 1 calc R . . . . C3 C 0.7925(4) 0.4792(3) 0.71578(19) 0.0483(12) Uani 1 1 d . . . . . H3 H 0.807934 0.478012 0.683970 0.058 Uiso 1 1 calc R . . . . C13 C 0.5852(5) 0.6882(3) 0.8591(2) 0.0624(17) Uani 1 1 d . . . . . H13 H 0.556843 0.731024 0.857403 0.075 Uiso 1 1 calc R . . . . C7 C 0.7199(4) 0.4889(3) 0.86384(17) 0.0482(12) Uani 1 1 d . . . . . C50 C 0.4649(5) 0.6540(3) 0.5619(2) 0.0577(14) Uani 1 1 d . . . . . H50A H 0.530391 0.642097 0.564230 0.087 Uiso 1 1 calc GR . . . . H50B H 0.445184 0.685209 0.534216 0.087 Uiso 1 1 calc GR . . . . H50C H 0.426567 0.613489 0.556054 0.087 Uiso 1 1 calc GR . . . . C24 C 0.6695(4) 0.5597(3) 0.63758(19) 0.0512(13) Uani 1 1 d . . . . . C11 C 0.6710(5) 0.5967(3) 0.9095(2) 0.0601(16) Uani 1 1 d . . . . . H11 H 0.701390 0.579793 0.940911 0.072 Uiso 1 1 calc R . . . . C9 C 0.8085(5) 0.4857(4) 0.9081(2) 0.0689(19) Uani 1 1 d . . . . . H9A H 0.848030 0.524841 0.906481 0.103 Uiso 1 1 calc GR . . . . H9B H 0.843811 0.444870 0.905133 0.103 Uiso 1 1 calc GR . . . . H9C H 0.788458 0.485579 0.939852 0.103 Uiso 1 1 calc GR . . . . C52 C 0.2730(4) 0.5205(3) 0.6504(2) 0.0552(14) Uani 1 1 d . . . . . H52 H 0.320704 0.486583 0.665458 0.066 Uiso 1 1 calc R . . . . C36 C 0.6077(5) 0.7944(3) 0.7657(2) 0.0542(13) Uani 1 1 d . . . . . C41 C 0.5820(6) 0.8637(3) 0.7640(2) 0.0650(17) Uani 1 1 d . . . . . H41 H 0.629739 0.896478 0.767942 0.078 Uiso 1 1 calc R . . . . C20 C 0.9315(5) 0.3992(4) 0.7452(2) 0.0639(17) Uani 1 1 d . . . . . C29 C 0.6256(5) 0.5064(4) 0.60686(19) 0.0604(16) Uani 1 1 d . . . . . C49 C 0.4530(4) 0.6878(3) 0.61146(18) 0.0443(11) Uani 1 1 d . . . . . H49 H 0.386609 0.702508 0.606724 0.053 Uiso 1 1 calc R . . . . C8 C 0.6508(5) 0.4316(3) 0.8695(2) 0.0612(16) Uani 1 1 d . . . . . H8A H 0.638199 0.432712 0.903073 0.092 Uiso 1 1 calc GR . . . . H8B H 0.678320 0.388414 0.863876 0.092 Uiso 1 1 calc GR . . . . H8C H 0.592502 0.437827 0.845091 0.092 Uiso 1 1 calc GR . . . . C48 C 0.5147(5) 0.7511(3) 0.6240(2) 0.0616(15) Uani 1 1 d . . . . . H48A H 0.501036 0.772746 0.653566 0.092 Uiso 1 1 calc GR . . . . H48B H 0.501545 0.782216 0.595887 0.092 Uiso 1 1 calc GR . . . . H48C H 0.580470 0.738140 0.630325 0.092 Uiso 1 1 calc GR . . . . C21 C 0.9797(5) 0.3560(4) 0.7908(3) 0.077(2) Uani 1 1 d . . . . . H21A H 1.006800 0.385465 0.818490 0.116 Uiso 1 1 calc GR . . . . H21B H 1.028988 0.328755 0.781598 0.116 Uiso 1 1 calc GR . . . . H21C H 0.933518 0.326611 0.800880 0.116 Uiso 1 1 calc GR . . . . C30 C 0.5679(5) 0.4519(3) 0.6252(2) 0.0623(16) Uani 1 1 d . . . . . H30 H 0.563434 0.463381 0.660046 0.075 Uiso 1 1 calc R . . . . C40 C 0.4907(5) 0.8847(3) 0.7570(2) 0.0599(16) Uani 1 1 d . . . . . H40 H 0.476297 0.931027 0.756271 0.072 Uiso 1 1 calc R . . . . C12 C 0.6260(6) 0.6605(4) 0.9064(2) 0.070(2) Uani 1 1 d . . . . . C46 C 0.2746(5) 0.7344(4) 0.7039(3) 0.0641(16) Uani 1 1 d . . . . . H46A H 0.250302 0.778456 0.710385 0.096 Uiso 1 1 calc GR . . . . H46B H 0.225282 0.700889 0.701695 0.096 Uiso 1 1 calc GR . . . . H46C H 0.296244 0.735701 0.672595 0.096 Uiso 1 1 calc GR . . . . C59 C 0.0488(5) 0.7457(4) 0.5497(3) 0.0677(16) Uani 1 1 d . . . . . C54 C 0.2214(6) 0.5402(4) 0.6901(3) 0.076(2) Uani 1 1 d . . . . . H54A H 0.265588 0.557651 0.718949 0.115 Uiso 1 1 calc GR . . . . H54B H 0.189627 0.500946 0.699936 0.115 Uiso 1 1 calc GR . . . . H54C H 0.175466 0.574733 0.677081 0.115 Uiso 1 1 calc GR . . . . C31 C 0.6134(6) 0.3812(4) 0.6261(3) 0.074(2) Uani 1 1 d . . . . . H31A H 0.613889 0.367095 0.592092 0.111 Uiso 1 1 calc GR . . . . H31B H 0.577493 0.349047 0.641406 0.111 Uiso 1 1 calc GR . . . . H31C H 0.677422 0.383048 0.645495 0.111 Uiso 1 1 calc GR . . . . C55 C 0.1878(6) 0.7634(3) 0.4778(2) 0.0651(16) Uani 1 1 d . . . . . C66 C 0.0017(6) 0.6659(4) 0.4203(3) 0.078(2) Uani 1 1 d . . . . . H66A H -0.041856 0.699389 0.428102 0.116 Uiso 1 1 calc GR . . . . H66B H -0.033199 0.630179 0.400214 0.116 Uiso 1 1 calc GR . . . . H66C H 0.044056 0.687014 0.401768 0.116 Uiso 1 1 calc GR . . . . C47 C 0.3245(5) 0.7091(4) 0.7979(2) 0.0658(16) Uani 1 1 d . . . . . H47A H 0.375670 0.691927 0.823549 0.099 Uiso 1 1 calc GR . . . . H47B H 0.271641 0.678184 0.793747 0.099 Uiso 1 1 calc GR . . . . H47C H 0.305408 0.753094 0.807923 0.099 Uiso 1 1 calc GR . . . . C53 C 0.2093(6) 0.4869(4) 0.6052(3) 0.077(2) Uani 1 1 d . . . . . H53A H 0.159157 0.517755 0.590582 0.116 Uiso 1 1 calc GR . . . . H53B H 0.182411 0.446011 0.615909 0.116 Uiso 1 1 calc GR . . . . H53C H 0.245877 0.475666 0.580323 0.116 Uiso 1 1 calc GR . . . . C28 C 0.6400(6) 0.5049(5) 0.5568(2) 0.080(2) Uani 1 1 d . . . . . H28 H 0.611928 0.470251 0.535224 0.096 Uiso 1 1 calc R . . . . C32 C 0.4666(6) 0.4484(4) 0.5932(3) 0.076(2) Uani 1 1 d . . . . . H32A H 0.440506 0.493635 0.588483 0.114 Uiso 1 1 calc GR . . . . H32B H 0.427916 0.420845 0.610349 0.114 Uiso 1 1 calc GR . . . . H32C H 0.467924 0.428586 0.560830 0.114 Uiso 1 1 calc GR . . . . C25 C 0.7267(5) 0.6089(4) 0.6203(3) 0.071(2) Uani 1 1 d . . . . . C33 C 0.7754(6) 0.6658(5) 0.6528(3) 0.088(3) Uani 1 1 d . . . . . H33 H 0.735642 0.677551 0.676979 0.106 Uiso 1 1 calc R . . . . C63 C 0.0592(5) 0.6356(3) 0.4698(3) 0.0648(17) Uani 1 1 d . . . . . C27 C 0.6935(7) 0.5524(7) 0.5388(3) 0.105(4) Uani 1 1 d . . . . . H27 H 0.700381 0.550261 0.505337 0.126 Uiso 1 1 calc R . . . . C62 C 0.0993(7) 0.8106(4) 0.5755(3) 0.083(2) Uani 1 1 d . . . . . H62A H 0.160544 0.798400 0.595182 0.124 Uiso 1 1 calc GR . . . . H62B H 0.061585 0.830448 0.597210 0.124 Uiso 1 1 calc GR . . . . H62C H 0.106857 0.843044 0.549918 0.124 Uiso 1 1 calc GR . . . . C58 C 0.2701(6) 0.8003(4) 0.5150(3) 0.076(2) Uani 1 1 d . . . . . H58A H 0.244490 0.826081 0.539283 0.115 Uiso 1 1 calc GR . . . . H58B H 0.302412 0.830523 0.496172 0.115 Uiso 1 1 calc GR . . . . H58C H 0.314135 0.766998 0.532314 0.115 Uiso 1 1 calc GR . . . . C57 C 0.2391(7) 0.7244(5) 0.4412(3) 0.085(2) Uani 1 1 d . . . . . H57A H 0.283303 0.692413 0.460094 0.127 Uiso 1 1 calc GR . . . . H57B H 0.272647 0.756320 0.424347 0.127 Uiso 1 1 calc GR . . . . H57C H 0.193083 0.700324 0.416440 0.127 Uiso 1 1 calc GR . . . . C60 C 0.0307(6) 0.6998(5) 0.5924(3) 0.083(2) Uani 1 1 d . . . . . H60A H -0.007956 0.661777 0.578264 0.124 Uiso 1 1 calc GR . . . . H60B H -0.001504 0.725362 0.614135 0.124 Uiso 1 1 calc GR . . . . H60C H 0.090210 0.683392 0.611736 0.124 Uiso 1 1 calc GR . . . . C64 C 0.1280(7) 0.5829(4) 0.4561(3) 0.087(3) Uani 1 1 d . . . . . H64A H 0.176648 0.605775 0.442899 0.131 Uiso 1 1 calc GR . . . . H64B H 0.094016 0.552244 0.430912 0.131 Uiso 1 1 calc GR . . . . H64C H 0.156515 0.557528 0.485844 0.131 Uiso 1 1 calc GR . . . . C61 C -0.0474(6) 0.7702(4) 0.5184(3) 0.080(2) Uani 1 1 d . . . . . H61A H -0.036687 0.802245 0.493178 0.120 Uiso 1 1 calc GR . . . . H61B H -0.082977 0.791936 0.540378 0.120 Uiso 1 1 calc GR . . . . H61C H -0.082440 0.731843 0.502033 0.120 Uiso 1 1 calc GR . . . . C26 C 0.7360(6) 0.6021(7) 0.5690(3) 0.102(4) Uani 1 1 d . . . . . H26 H 0.773191 0.633495 0.555994 0.123 Uiso 1 1 calc R . . . . C42 C 0.7111(5) 0.7750(4) 0.7723(4) 0.080(2) Uani 1 1 d . . . . . H42 H 0.714743 0.726041 0.765506 0.096 Uiso 1 1 calc R . . . . C22 C 0.8945(7) 0.3463(5) 0.7026(3) 0.087(2) Uani 1 1 d . . . . . H22A H 0.850678 0.315750 0.713657 0.130 Uiso 1 1 calc GR . . . . H22B H 0.947020 0.320729 0.695427 0.130 Uiso 1 1 calc GR . . . . H22C H 0.862841 0.369738 0.672558 0.130 Uiso 1 1 calc GR . . . . C65 C -0.0096(6) 0.5960(4) 0.4968(3) 0.081(2) Uani 1 1 d . . . . . H65A H 0.026468 0.570664 0.524740 0.122 Uiso 1 1 calc GR . . . . H65B H -0.047461 0.565181 0.473203 0.122 Uiso 1 1 calc GR . . . . H65C H -0.050329 0.627800 0.509066 0.122 Uiso 1 1 calc GR . . . . C23 C 1.0007(6) 0.4443(5) 0.7275(4) 0.106(4) Uani 1 1 d . . . . . H23A H 0.968874 0.469695 0.698378 0.159 Uiso 1 1 calc GR . . . . H23B H 1.050173 0.417140 0.718470 0.159 Uiso 1 1 calc GR . . . . H23C H 1.027849 0.475423 0.754092 0.159 Uiso 1 1 calc GR . . . . C35 C 0.7891(6) 0.7324(5) 0.6233(4) 0.107(4) Uani 1 1 d . . . . . H35A H 0.837067 0.724988 0.603886 0.161 Uiso 1 1 calc GR . . . . H35B H 0.808387 0.768901 0.646942 0.161 Uiso 1 1 calc GR . . . . H35C H 0.730286 0.744203 0.600876 0.161 Uiso 1 1 calc GR . . . . C34 C 0.8714(7) 0.6429(6) 0.6835(5) 0.121(5) Uani 1 1 d . . . . . H34A H 0.862641 0.604903 0.704586 0.181 Uiso 1 1 calc GR . . . . H34B H 0.900681 0.679885 0.704430 0.181 Uiso 1 1 calc GR . . . . H34C H 0.911540 0.629360 0.660901 0.181 Uiso 1 1 calc GR . . . . C16 C 0.6168(10) 0.7005(6) 0.9542(3) 0.131(3) Uani 1 1 d . U . . . C56 C 0.1212(7) 0.8170(4) 0.4478(3) 0.088(2) Uani 1 1 d . . . . . H56A H 0.072603 0.794481 0.423424 0.131 Uiso 1 1 calc GR . . . . H56B H 0.156863 0.846727 0.430461 0.131 Uiso 1 1 calc GR . . . . H56C H 0.092316 0.843192 0.470592 0.131 Uiso 1 1 calc GR . . . . C44 C 0.7576(8) 0.8132(6) 0.7353(6) 0.125(4) Uani 1 1 d . . . . . H44A H 0.718491 0.809924 0.701910 0.187 Uiso 1 1 calc GR . . . . H44B H 0.818778 0.793541 0.735400 0.187 Uiso 1 1 calc GR . . . . H44C H 0.765164 0.860261 0.745184 0.187 Uiso 1 1 calc GR . . . . C43 C 0.7649(7) 0.7887(6) 0.8272(5) 0.117(4) Uani 1 1 d . . . . . H43A H 0.765081 0.836795 0.834004 0.176 Uiso 1 1 calc GR . . . . H43B H 0.829112 0.772687 0.831410 0.176 Uiso 1 1 calc GR . . . . H43C H 0.733868 0.765016 0.850434 0.176 Uiso 1 1 calc GR . . . . C17 C 0.6636(10) 0.6634(6) 1.0026(3) 0.134(4) Uani 1 1 d . U . . . H17A H 0.635026 0.619210 1.003354 0.201 Uiso 1 1 calc GR . . . . H17B H 0.654903 0.689403 1.031506 0.201 Uiso 1 1 calc GR . . . . H17C H 0.730257 0.658186 1.003574 0.201 Uiso 1 1 calc GR . . . . C19 C 0.6583(11) 0.7698(6) 0.9537(4) 0.149(4) Uani 1 1 d . U . . . H19A H 0.722845 0.766129 0.949717 0.224 Uiso 1 1 calc GR . . . . H19B H 0.656833 0.792441 0.985123 0.224 Uiso 1 1 calc GR . . . . H19C H 0.622053 0.795580 0.926061 0.224 Uiso 1 1 calc GR . . . . C18 C 0.5109(11) 0.7085(7) 0.9539(3) 0.147(4) Uani 1 1 d . U . . . H18A H 0.479978 0.731140 0.923370 0.221 Uiso 1 1 calc GR . . . . H18B H 0.503345 0.735093 0.982749 0.221 Uiso 1 1 calc GR . . . . H18C H 0.483040 0.664248 0.955597 0.221 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ag1 0.0601(3) 0.0582(3) 0.0440(2) 0.00117(16) 0.00205(17) -0.00342(18) P1 0.0539(8) 0.0485(7) 0.0376(6) -0.0022(5) 0.0047(5) 0.0001(6) Al1 0.0409(7) 0.0359(6) 0.0267(6) 0.0005(5) 0.0063(5) -0.0014(5) O1 0.0471(18) 0.0339(14) 0.0276(14) -0.0011(11) 0.0054(12) -0.0037(13) O2 0.0446(17) 0.0392(15) 0.0233(13) 0.0008(11) 0.0067(12) 0.0024(13) N1 0.048(2) 0.041(2) 0.0311(18) 0.0108(15) -0.0031(16) -0.0008(17) N4 0.046(2) 0.0312(17) 0.0361(19) -0.0008(15) 0.0006(16) -0.0031(15) N3 0.045(2) 0.048(2) 0.0262(17) 0.0096(15) 0.0103(15) 0.0053(17) N2 0.046(2) 0.0404(19) 0.0280(17) 0.0068(14) 0.0082(15) -0.0016(16) C51 0.035(2) 0.038(2) 0.0281(19) -0.0007(16) 0.0036(16) -0.0014(17) C5 0.053(3) 0.055(3) 0.034(2) 0.008(2) 0.006(2) 0.014(2) C2 0.049(3) 0.047(2) 0.028(2) 0.0067(18) 0.0090(18) 0.003(2) C1 0.042(2) 0.039(2) 0.0268(19) 0.0034(16) 0.0083(17) 0.0030(18) C10 0.057(3) 0.052(3) 0.028(2) -0.0043(19) 0.0019(19) 0.011(2) C37 0.055(3) 0.032(2) 0.035(2) -0.0006(17) 0.0003(19) 0.0004(19) C38 0.062(3) 0.041(2) 0.032(2) 0.0013(18) 0.006(2) -0.002(2) C15 0.051(3) 0.038(2) 0.030(2) -0.0038(17) 0.0057(18) 0.0022(19) C6 0.051(3) 0.043(2) 0.031(2) 0.0037(18) 0.0071(19) 0.003(2) C4 0.049(3) 0.059(3) 0.038(2) 0.008(2) 0.012(2) 0.009(2) C39 0.071(4) 0.046(3) 0.045(3) 0.004(2) 0.008(2) 0.007(3) C14 0.054(3) 0.043(2) 0.032(2) -0.0046(19) -0.0014(19) 0.005(2) C45 0.049(3) 0.048(3) 0.050(3) -0.007(2) 0.008(2) 0.002(2) C3 0.052(3) 0.063(3) 0.033(2) 0.013(2) 0.016(2) 0.008(2) C13 0.085(4) 0.051(3) 0.044(3) -0.019(2) -0.006(3) 0.020(3) C7 0.068(3) 0.052(3) 0.024(2) 0.0056(19) 0.008(2) 0.018(2) C50 0.064(4) 0.076(4) 0.035(3) 0.018(2) 0.015(2) 0.009(3) C24 0.052(3) 0.073(3) 0.033(2) 0.019(2) 0.018(2) 0.023(3) C11 0.084(4) 0.060(3) 0.032(2) -0.005(2) 0.002(2) 0.026(3) C9 0.085(5) 0.088(4) 0.029(2) 0.002(3) -0.001(3) 0.036(4) C52 0.055(3) 0.047(3) 0.056(3) 0.011(2) -0.006(2) -0.015(2) C36 0.063(3) 0.036(2) 0.059(3) -0.006(2) 0.002(3) -0.013(2) C41 0.086(5) 0.051(3) 0.053(3) -0.005(3) 0.001(3) -0.020(3) C20 0.057(3) 0.085(4) 0.056(3) 0.022(3) 0.026(3) 0.024(3) C29 0.079(4) 0.081(4) 0.024(2) 0.006(2) 0.015(2) 0.029(3) C49 0.047(3) 0.049(3) 0.036(2) 0.012(2) 0.0064(19) -0.001(2) C8 0.095(5) 0.047(3) 0.049(3) 0.006(2) 0.034(3) 0.007(3) C48 0.069(4) 0.058(3) 0.055(3) 0.025(3) 0.006(3) -0.013(3) C21 0.059(4) 0.105(6) 0.070(4) 0.028(4) 0.017(3) 0.032(4) C30 0.083(4) 0.063(3) 0.035(3) -0.016(2) 0.002(3) 0.021(3) C40 0.096(5) 0.034(2) 0.048(3) 0.002(2) 0.012(3) 0.000(3) C12 0.101(5) 0.066(4) 0.036(3) -0.015(3) -0.005(3) 0.026(4) C46 0.052(3) 0.079(4) 0.057(3) -0.012(3) 0.002(3) 0.009(3) C59 0.069(4) 0.075(4) 0.063(4) -0.004(3) 0.023(3) -0.002(3) C54 0.075(5) 0.081(5) 0.075(4) 0.016(4) 0.022(4) -0.026(4) C31 0.101(6) 0.062(4) 0.056(4) -0.010(3) 0.007(3) 0.024(4) C55 0.089(5) 0.059(3) 0.048(3) 0.007(3) 0.014(3) -0.001(3) C66 0.081(5) 0.071(4) 0.065(4) -0.010(3) -0.022(3) 0.000(4) C47 0.070(4) 0.075(4) 0.052(3) 0.000(3) 0.013(3) -0.009(3) C53 0.077(5) 0.056(3) 0.083(5) 0.004(3) -0.019(4) -0.022(3) C28 0.105(6) 0.105(6) 0.032(3) 0.008(3) 0.017(3) 0.046(5) C32 0.090(5) 0.064(4) 0.066(4) -0.025(3) -0.002(4) 0.019(4) C25 0.053(3) 0.110(5) 0.057(3) 0.050(4) 0.026(3) 0.024(4) C33 0.062(4) 0.118(7) 0.086(5) 0.059(5) 0.019(4) -0.011(4) C63 0.076(4) 0.052(3) 0.055(3) -0.002(3) -0.011(3) 0.003(3) C27 0.104(7) 0.178(11) 0.043(4) 0.043(6) 0.036(4) 0.072(7) C62 0.097(6) 0.082(5) 0.073(5) -0.027(4) 0.027(4) 0.000(4) C58 0.094(5) 0.069(4) 0.067(4) 0.005(3) 0.021(4) -0.018(4) C57 0.091(6) 0.112(6) 0.055(4) -0.005(4) 0.024(4) -0.001(5) C60 0.074(5) 0.107(6) 0.074(5) 0.004(4) 0.029(4) 0.002(4) C64 0.106(6) 0.066(4) 0.076(5) -0.024(4) -0.014(4) 0.021(4) C61 0.076(5) 0.087(5) 0.080(5) 0.010(4) 0.021(4) 0.015(4) C26 0.078(5) 0.178(11) 0.063(5) 0.072(6) 0.045(4) 0.055(6) C42 0.054(4) 0.061(4) 0.116(6) -0.009(4) -0.005(4) -0.013(3) C22 0.089(6) 0.106(6) 0.069(4) -0.002(4) 0.024(4) 0.040(5) C65 0.096(6) 0.069(4) 0.069(4) 0.003(3) -0.008(4) -0.023(4) C23 0.051(4) 0.131(8) 0.147(9) 0.063(7) 0.049(5) 0.027(4) C35 0.070(5) 0.128(8) 0.130(8) 0.081(7) 0.036(5) 0.006(5) C34 0.073(5) 0.135(9) 0.136(9) 0.088(7) -0.019(5) -0.021(5) C16 0.210(8) 0.119(5) 0.042(3) -0.037(3) -0.027(4) 0.091(5) C56 0.120(7) 0.069(4) 0.079(5) 0.020(4) 0.031(5) 0.002(4) C44 0.080(6) 0.109(8) 0.189(13) 0.013(8) 0.037(7) -0.033(6) C43 0.076(6) 0.108(7) 0.141(9) -0.008(7) -0.039(6) -0.013(5) C17 0.214(9) 0.125(6) 0.040(3) -0.031(4) -0.028(5) 0.083(7) C19 0.238(10) 0.106(6) 0.072(5) -0.047(5) -0.042(6) 0.063(7) C18 0.216(10) 0.167(8) 0.049(4) -0.033(5) 0.004(5) 0.102(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.2130 0.2455 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Ag1 P1 171.15(12) . . ? C59 P1 Ag1 106.6(2) . . ? C55 P1 Ag1 112.7(2) . . ? C55 P1 C59 108.8(3) . . ? C63 P1 Ag1 109.1(2) . . ? C63 P1 C59 109.1(3) . . ? C63 P1 C55 110.3(3) . . ? O1 Al1 O2 92.67(14) . . ? O1 Al1 N4 112.26(17) . . ? O1 Al1 N3 112.30(18) . . ? O1 Al1 N2 70.62(16) . . ? O1 Al1 C51 35.37(14) . . ? O2 Al1 C51 128.04(16) . . ? N4 Al1 O2 80.03(15) . . ? N4 Al1 N2 105.68(18) . . ? N4 Al1 C51 113.20(18) . . ? N3 Al1 O2 79.65(15) . . ? N3 Al1 N4 131.46(19) . . ? N3 Al1 N2 106.33(17) . . ? N3 Al1 C51 114.10(17) . . ? N2 Al1 O2 163.28(17) . . ? N2 Al1 C51 35.25(16) . . ? C51 O1 Al1 92.1(3) . . ? C1 O2 Al1 115.9(2) . . ? C15 O2 Al1 115.6(3) . . ? C15 O2 C1 113.8(4) . . ? C51 N1 Ag1 127.0(3) . . ? C51 N1 C52 117.3(4) . . ? C52 N1 Ag1 114.8(3) . . ? C37 N4 Al1 129.8(3) . . ? C14 N4 Al1 116.4(3) . . ? C14 N4 C37 113.8(4) . . ? C2 N3 Al1 117.9(3) . . ? C2 N3 C24 113.9(4) . . ? C24 N3 Al1 126.7(3) . . ? C51 N2 Al1 88.8(3) . . ? C51 N2 C49 123.1(4) . . ? C49 N2 Al1 148.0(3) . . ? O1 C51 Al1 52.5(2) . . ? N1 C51 Al1 174.4(3) . . ? N1 C51 O1 121.9(4) . . ? N1 C51 N2 129.7(4) . . ? N2 C51 Al1 55.9(2) . . ? N2 C51 O1 108.4(4) . . ? C4 C5 C6 121.1(5) . . ? C1 C2 N3 114.6(4) . . ? C3 C2 N3 130.5(4) . . ? C3 C2 C1 114.8(4) . . ? O2 C1 C2 111.8(4) . . ? C6 C1 O2 121.1(4) . . ? C6 C1 C2 127.1(4) . . ? C15 C10 C7 118.5(4) . . ? C15 C10 C11 115.9(5) . . ? C11 C10 C7 125.5(4) . . ? C38 C37 N4 120.1(4) . . ? C38 C37 C36 120.5(5) . . ? C36 C37 N4 119.3(5) . . ? C37 C38 C39 117.7(5) . . ? C37 C38 C45 122.2(5) . . ? C39 C38 C45 120.1(5) . . ? O2 C15 C14 111.3(4) . . ? C10 C15 O2 121.6(4) . . ? C10 C15 C14 126.8(4) . . ? C5 C6 C7 125.7(4) . . ? C1 C6 C5 115.2(4) . . ? C1 C6 C7 119.2(4) . . ? C5 C4 C20 121.0(5) . . ? C3 C4 C5 119.9(5) . . ? C3 C4 C20 119.0(5) . . ? C40 C39 C38 122.4(6) . . ? N4 C14 C15 116.1(4) . . ? N4 C14 C13 129.0(5) . . ? C15 C14 C13 114.9(5) . . ? C38 C45 C46 112.0(5) . . ? C38 C45 C47 110.5(5) . . ? C46 C45 C47 111.0(5) . . ? C2 C3 C4 121.6(4) . . ? C12 C13 C14 121.1(5) . . ? C10 C7 C9 108.7(5) . . ? C6 C7 C10 108.7(4) . . ? C6 C7 C9 110.8(5) . . ? C6 C7 C8 109.3(4) . . ? C8 C7 C10 109.3(5) . . ? C8 C7 C9 110.0(5) . . ? C29 C24 N3 119.0(5) . . ? C29 C24 C25 122.6(5) . . ? C25 C24 N3 118.4(6) . . ? C10 C11 C12 120.6(5) . . ? N1 C52 C54 112.4(5) . . ? N1 C52 C53 110.3(5) . . ? C54 C52 C53 112.7(6) . . ? C37 C36 C42 122.9(5) . . ? C41 C36 C37 117.6(6) . . ? C41 C36 C42 119.5(6) . . ? C40 C41 C36 122.7(6) . . ? C4 C20 C22 108.8(6) . . ? C21 C20 C4 113.2(5) . . ? C21 C20 C22 104.6(6) . . ? C23 C20 C4 110.5(6) . . ? C23 C20 C21 111.4(7) . . ? C23 C20 C22 108.1(7) . . ? C24 C29 C30 123.3(4) . . ? C24 C29 C28 116.3(7) . . ? C28 C29 C30 120.4(7) . . ? N2 C49 C50 112.3(4) . . ? N2 C49 C48 110.3(4) . . ? C48 C49 C50 112.2(5) . . ? C29 C30 C31 112.6(6) . . ? C29 C30 C32 111.9(6) . . ? C31 C30 C32 108.8(6) . . ? C41 C40 C39 119.2(5) . . ? C13 C12 C11 120.0(5) . . ? C13 C12 C16 118.3(6) . . ? C11 C12 C16 121.7(6) . . ? C62 C59 P1 109.8(5) . . ? C60 C59 P1 108.5(5) . . ? C60 C59 C62 106.4(7) . . ? C60 C59 C61 108.8(6) . . ? C61 C59 P1 117.1(5) . . ? C61 C59 C62 105.8(7) . . ? C58 C55 P1 109.3(4) . . ? C57 C55 P1 108.7(5) . . ? C57 C55 C58 103.8(7) . . ? C56 C55 P1 116.0(6) . . ? C56 C55 C58 109.2(6) . . ? C56 C55 C57 109.1(6) . . ? C27 C28 C29 122.4(9) . . ? C24 C25 C33 123.4(6) . . ? C24 C25 C26 115.9(9) . . ? C26 C25 C33 120.7(8) . . ? C25 C33 C35 114.7(7) . . ? C25 C33 C34 111.0(9) . . ? C34 C33 C35 109.1(7) . . ? C66 C63 P1 115.1(5) . . ? C66 C63 C65 108.6(6) . . ? C64 C63 P1 107.9(5) . . ? C64 C63 C66 108.1(6) . . ? C64 C63 C65 106.5(6) . . ? C65 C63 P1 110.3(5) . . ? C26 C27 C28 120.3(7) . . ? C27 C26 C25 122.5(9) . . ? C36 C42 C43 110.7(8) . . ? C44 C42 C36 111.1(8) . . ? C44 C42 C43 110.2(8) . . ? C17 C16 C12 112.0(7) . . ? C17 C16 C18 108.2(12) . . ? C19 C16 C12 110.8(11) . . ? C19 C16 C17 109.7(10) . . ? C19 C16 C18 108.0(9) . . ? C18 C16 C12 108.0(8) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ag1 P1 2.3572(14) . ? Ag1 N1 2.130(4) . ? P1 C59 1.896(7) . ? P1 C55 1.892(7) . ? P1 C63 1.877(6) . ? Al1 O1 1.842(3) . ? Al1 O2 2.008(3) . ? Al1 N4 1.902(4) . ? Al1 N3 1.896(4) . ? Al1 N2 1.923(4) . ? Al1 C51 2.320(5) . ? O1 C51 1.344(5) . ? O2 C1 1.392(6) . ? O2 C15 1.389(5) . ? N1 C51 1.304(6) . ? N1 C52 1.472(7) . ? N4 C37 1.439(6) . ? N4 C14 1.391(6) . ? N3 C2 1.400(6) . ? N3 C24 1.457(6) . ? N2 C51 1.339(6) . ? N2 C49 1.455(6) . ? C5 C6 1.407(7) . ? C5 C4 1.397(7) . ? C2 C1 1.400(6) . ? C2 C3 1.394(7) . ? C1 C6 1.374(6) . ? C10 C15 1.366(7) . ? C10 C7 1.540(7) . ? C10 C11 1.400(7) . ? C37 C38 1.398(8) . ? C37 C36 1.414(7) . ? C38 C39 1.413(7) . ? C38 C45 1.519(8) . ? C15 C14 1.394(7) . ? C6 C7 1.518(6) . ? C4 C3 1.396(7) . ? C4 C20 1.544(8) . ? C39 C40 1.359(9) . ? C14 C13 1.400(7) . ? C45 C46 1.532(8) . ? C45 C47 1.543(8) . ? C13 C12 1.398(8) . ? C7 C9 1.555(8) . ? C7 C8 1.527(9) . ? C50 C49 1.534(8) . ? C24 C29 1.400(10) . ? C24 C25 1.407(9) . ? C11 C12 1.402(8) . ? C52 C54 1.474(10) . ? C52 C53 1.516(8) . ? C36 C41 1.406(8) . ? C36 C42 1.511(10) . ? C41 C40 1.351(10) . ? C20 C21 1.535(9) . ? C20 C22 1.555(12) . ? C20 C23 1.483(10) . ? C29 C30 1.498(10) . ? C29 C28 1.409(7) . ? C49 C48 1.522(8) . ? C30 C31 1.531(8) . ? C30 C32 1.533(10) . ? C12 C16 1.535(9) . ? C59 C62 1.554(11) . ? C59 C60 1.525(10) . ? C59 C61 1.541(11) . ? C55 C58 1.560(10) . ? C55 C57 1.552(10) . ? C55 C56 1.534(11) . ? C66 C63 1.534(9) . ? C28 C27 1.359(15) . ? C25 C33 1.498(13) . ? C25 C26 1.426(11) . ? C33 C35 1.561(10) . ? C33 C34 1.524(11) . ? C63 C64 1.528(10) . ? C63 C65 1.553(11) . ? C27 C26 1.331(17) . ? C42 C44 1.509(14) . ? C42 C43 1.545(13) . ? C16 C17 1.524(11) . ? C16 C19 1.483(19) . ? C16 C18 1.531(19) . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.006 -0.040 0.120 17.7 0.0 ? 2 -0.971 0.000 0.500 867.3 116.3 ? 3 -0.006 0.040 0.880 17.7 0.0 ? 4 -0.359 0.500 0.000 867.3 116.3 ? 5 -0.006 0.460 0.380 17.7 0.0 ? 6 0.006 0.540 0.620 17.7 0.0 ? loop_ _publcif_info_exptl_table_extra_item sin_theta_over_lambda_max loop_ _publcif_info_exptl_table_header_item ?