#------------------------------------------------------------------------------ #$Date: 2021-09-27 12:00:27 +0300 (Mon, 27 Sep 2021) $ #$Revision: 269320 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/47/1564727.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564727 loop_ _publ_author_name 'Kubasov, A.S.' 'Turishev, E.S.' 'Golubev, A.V.' 'Bykov, A.Yu.' 'Zhizhin, K.Yu.' 'Kuznetsov, N.T.' _publ_section_title ; The method for synthesis of 2-sulfonium closo-decaborate anions derivatives with exo-polyhedral aminogroups ; _journal_name_full 'Inorganica Chimica Acta' _journal_page_first 119589 _journal_paper_doi 10.1016/j.ica.2020.119589 _journal_volume 507 _journal_year 2020 _chemical_formula_moiety 'C22 H20 B10 Cl9 N2 O4 S, C16 H36 N' _chemical_formula_sum 'C40 H50 B10 Cl9 N0.5 O0.5 S' _chemical_formula_weight 1005.01 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _cell_angle_alpha 80.395(2) _cell_angle_beta 89.953(2) _cell_angle_gamma 60.9440(10) _cell_formula_units_Z 2 _cell_length_a 12.3454(5) _cell_length_b 12.4756(5) _cell_length_c 22.0778(9) _cell_measurement_reflns_used 9885 _cell_measurement_temperature 296 _cell_measurement_theta_max 27.462 _cell_measurement_theta_min 2.192 _cell_volume 2918.0(2) _computing_cell_refinement 'SAINT V8.38A (?, 2016)' _computing_data_reduction 'SAINT V8.38A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 296 _diffrn_measured_fraction_theta_full 0.995 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0484 _diffrn_reflns_av_unetI/netI 0.0517 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 28 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_number 43567 _diffrn_reflns_point_group_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.499 _diffrn_reflns_theta_min 1.879 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.495 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.6290 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0843 before and 0.0576 after correction. The Ratio of minimum to maximum transmission is 0.8435. The \l/2 correction factor is Not present.' _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.144 _exptl_crystal_description plate _exptl_crystal_F_000 1033 _exptl_crystal_size_max 0.7 _exptl_crystal_size_mid 0.5 _exptl_crystal_size_min 0.05 _refine_diff_density_max 0.664 _refine_diff_density_min -0.449 _refine_diff_density_rms 0.062 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.045 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 590 _refine_ls_number_reflns 13298 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.045 _refine_ls_R_factor_all 0.0958 _refine_ls_R_factor_gt 0.0617 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1158P)^2^+0.6035P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1825 _refine_ls_wR_factor_ref 0.2068 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 8539 _reflns_number_total 13298 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file 19kbub41_0m_a.cif _cod_data_source_block 19kbub41_0m_a _cod_original_formula_sum 'C40 H50 B10 Cl9 N0.50 O0.50 S' _cod_database_code 1564727 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.976 _shelx_estimated_absorpt_t_min 0.723 _olex2_refinement_description ; 1. Others Fixed Uiso: H1A(0.085) H1B(0.085) H2A(0.092) H2B(0.092) H3A(0.107) H3B(0.107) H6(0.129) H7(0.146) H8(0.153) H9(0.131) H12A(0.089) H12B(0.089) H13A(0.094) H13B(0.094) H14A(0.114) H14B(0.114) H17(0.134) H18(0.167) H19(0.19) H20(0.173) H23A(0.092) H23B(0.092) H24A(0.117) H24B(0.117) H25A(0.129) H25B(0.129) H26A(0.202) H26B(0.202) H26C(0.202) H27A(0.087) H27B(0.087) H28A(0.1) H28B(0.1) H29A(0.134) H29B(0.134) H30A(0.222) H30B(0.222) H30C(0.222) H31A(0.084) H31B(0.084) H32A(0.104) H32B(0.104) H33A(0.108) H33B(0.108) H34A(0.166) H34B(0.166) H34C(0.166) H35A(0.09) H35B(0.09) H36A(0.111) H36B(0.111) H37A(0.149) H37B(0.149) H38A(0.266) H38B(0.266) H38C(0.266) Fixed X: H1A(0.886875) H1B(0.805177) H2A(0.781254) H2B(0.685444) H3A(0.941132) H3B(0.85374) H6(0.90069) H7(0.746377) H8(0.585618) H9(0.553936) H12A(0.723723) H12B(0.851733) H13A(0.803481) H13B(0.66816) H14A(0.73815) H14B(0.876745) H17(0.633126) H18(0.765092) H19(0.971955) H20(1.06285) H23A(0.512644) H23B(0.398634) H24A(0.61125) H24B(0.499145) H25A(0.549101) H25B(0.662833) H26A(0.766406) H26B(0.70646) H26C(0.646681) H27A(0.308748) H27B(0.401231) H28A(0.17389) H28B(0.265659) H29A(0.13854) H29B(0.235326) H30A(0.040754) H30B(0.007825) H30C(0.105392) H31A(0.464086) H31B(0.537107) H32A(0.644485) H32B(0.580573) H33A(0.74026) H33B(0.679161) H34A(0.802273) H34B(0.891294) H34C(0.840185) H35A(0.260135) H35B(0.364015) H36A(0.186904) H36B(0.294027) H37A(0.108609) H37B(0.214389) H38A(0.131346) H38B(0.029716) H38C(0.030187) Fixed Y: H1A(0.040821) H1B(0.176467) H2A(0.097384) H2B(0.229574) H3A(0.146601) H3B(0.27376) H6(0.268034) H7(0.442036) H8(0.599519) H9(0.590499) H12A(-0.130377) H12B(-0.136626) H13A(-0.096376) H13B(-0.072872) H14A(- 0.279105) H14B(-0.308186) H17(-0.225458) H18(-0.314706) H19(-0.420132) H20(- 0.444657) H23A(0.586597) H23B(0.671235) H24A(0.698805) H24B(0.775402) H25A(0.592829) H25B(0.517808) H26A(0.605586) H26B(0.580482) H26C(0.715065) H27A(0.768624) H27B(0.631531) H28A(0.78323) H28B(0.643541) H29A(0.72235) H29B(0.582908) H30A(0.61238) H30B(0.718688) H30C(0.580183) H31A(0.825373) H31B(0.814012) H32A(0.595596) H32B(0.618129) H33A(0.706515) H33B(0.72368) H34A(0.483057) H34B(0.531311) H34C(0.559279) H35A(0.877249) H35B(0.91435) H36A(0.967203) H36B(1.000019) H37A(1.098649) H37B(1.132584) H38A(1.235391) H38B(1.284762) H38C(1.193573) Fixed Z: H1A(0.360287) H1B(0.321946) H2A(0.446633) H2B(0.408647) H3A(0.43814) H3B(0.393637) H6(0.663464) H7(0.701006) H8(0.637626) H9(0.536186) H12A(0.336564) H12B(0.350118) H13A(0.44883) H13B(0.435354) H14A(0.436694) H14B(0.435228) H17(0.676102) H18(0.76671) H19(0.76387) H20(0.673123) H23A(0.186069) H23B(0.219257) H24A(0.208459) H24B(0.245033) H25A(0.315567) H25B(0.279334) H26A(0.309149) H26B(0.368648) H26C(0.328226) H27A(0.057486) H27B(0.090197) H28A(0.133896) H28B(0.164054) H29A(0.045358) H29B(0.07254) H30A(0.07976) H30B(0.117384) H30C(0.146424) H31A(0.057467) H31B(0.118128) H32A(0.124561) H32B(0.058978) H33A(0.08326) H33B(0.017776) H34A(0.056562) H34B(0.074846) H34C(0.005742) H35A(0.17684) H35B(0.170631) H36A(0.076834) H36B(0.068314) H37A(0.147018) H37B(0.137179) H38A(0.042257) H38B(0.088592) H38C(0.047452) ; _shelx_res_file ; TITL 19kbub41_0m_a.res in P-1 19kbub41_0m_a.res created by SHELXL-2016/6 at 13:36:57 on 06-Dec-2019 REM Old TITL 19kbub41_0m in P-1 REM SHELXT solution in P-1 REM R1 0.243, Rweak 0.019, Alpha 0.080, Orientation as input REM Formula found by SHELXT: C58 B2 Cl10 CELL 0.71073 12.3454 12.4756 22.0778 80.395 89.953 60.944 ZERR 2 0.0005 0.0005 0.0009 0.002 0.002 0.001 LATT 1 SFAC C H B Cl S N O UNIT 80 100 20 18 2 1 1 L.S. 4 PLAN 20 SIZE 0.05 0.5 0.7 TEMP 22.85 BOND $H LIST 6 ABIN fmap 2 ACTA OMIT -2 55 OMIT -1 0 2 OMIT -1 -1 2 OMIT -2 3 7 REM REM REM WGHT 0.115800 0.603500 FVAR 0.77180 CL1 4 0.999479 -0.060500 0.238557 11.00000 0.05428 0.10939 = 0.06096 -0.00276 0.00406 -0.03350 CL2 4 0.800771 0.290332 0.197545 11.00000 0.13448 0.10805 = 0.07626 -0.02340 0.01841 -0.09633 CL3 4 0.878280 0.041223 0.071812 11.00000 0.08719 0.08559 = 0.05494 -0.01856 0.03069 -0.04540 CL4 4 0.789995 -0.188559 0.203327 11.00000 0.10661 0.04812 = 0.07193 -0.01076 0.02225 -0.03507 CL5 4 0.607779 0.352363 0.059000 11.00000 0.11540 0.05307 = 0.04336 -0.00093 0.01188 -0.04915 CL6 4 0.599704 0.013074 0.062572 11.00000 0.11359 0.06770 = 0.04057 -0.01737 0.00712 -0.06036 CL7 4 0.489690 0.022852 0.244555 11.00000 0.07962 0.07221 = 0.06239 -0.01164 0.01633 -0.05242 CL8 4 0.498948 0.357811 0.240763 11.00000 0.10890 0.05548 = 0.06760 -0.02861 0.03184 -0.04156 CL9 4 0.347822 0.296614 0.113315 11.00000 0.06609 0.08846 = 0.06186 -0.00004 -0.00899 -0.02709 S1 5 0.693732 0.070498 0.328879 11.00000 0.07599 0.07266 = 0.03750 -0.01066 0.00656 -0.04472 O1 7 0.979037 0.134603 0.553839 11.00000 0.10301 0.09295 = 0.12040 -0.02292 -0.01928 -0.03600 O2 7 0.642867 0.451036 0.433006 11.00000 0.13501 0.11865 = 0.08903 -0.00434 -0.02485 -0.05459 O3 7 1.025864 -0.400890 0.532565 11.00000 0.10836 0.12130 = 0.09987 -0.01061 0.03467 -0.05352 O4 7 0.606868 -0.185720 0.537445 11.00000 0.09524 0.14638 = 0.10845 0.02289 -0.01127 -0.06012 N1 6 0.816687 0.275962 0.481785 11.00000 0.09054 0.08546 = 0.06310 -0.02664 0.00210 -0.04830 N2 6 0.814454 -0.287828 0.518299 11.00000 0.10125 0.09066 = 0.05481 0.00444 0.00461 -0.05770 C1 1 0.804224 0.113379 0.353897 11.00000 0.08863 0.09004 = 0.05246 -0.02004 0.00729 -0.05611 AFIX 23 H1A 2 0.886875 0.040821 0.360287 11.00000 -1.20000 H1B 2 0.805177 0.176467 0.321946 11.00000 -1.20000 AFIX 0 C2 1 0.771603 0.163616 0.413270 11.00000 0.09831 0.09258 = 0.06101 -0.02951 0.01390 -0.05897 AFIX 23 H2A 2 0.781254 0.097384 0.446633 11.00000 -1.20000 H2B 2 0.685444 0.229574 0.408647 11.00000 -1.20000 AFIX 0 C3 1 0.856081 0.214584 0.428949 11.00000 0.10482 0.12645 = 0.07157 -0.04602 0.01946 -0.07574 AFIX 23 H3A 2 0.941132 0.146601 0.438140 11.00000 -1.20000 H3B 2 0.853740 0.273760 0.393637 11.00000 -1.20000 AFIX 0 C4 1 0.883188 0.232517 0.538832 11.00000 0.08806 0.08398 = 0.07266 -0.01687 -0.00329 -0.05099 C5 1 0.811293 0.327798 0.576198 11.00000 0.10978 0.09429 = 0.05539 -0.01981 0.00893 -0.06997 C6 1 0.831358 0.331159 0.638120 11.00000 0.15406 0.12682 = 0.06734 -0.02340 0.01001 -0.08834 AFIX 43 H6 2 0.900690 0.268034 0.663464 11.00000 -1.20000 AFIX 0 C7 1 0.739230 0.436966 0.659782 11.00000 0.18741 0.15866 = 0.06900 -0.05597 0.04733 -0.11256 AFIX 43 H7 2 0.746377 0.442036 0.701006 11.00000 -1.20000 AFIX 0 C8 1 0.641809 0.530091 0.622059 11.00000 0.14800 0.14219 = 0.11209 -0.06335 0.04076 -0.07529 AFIX 43 H8 2 0.585618 0.599519 0.637626 11.00000 -1.20000 AFIX 0 C9 1 0.622469 0.526271 0.561597 11.00000 0.10950 0.10947 = 0.11243 -0.03991 0.02771 -0.05134 AFIX 43 H9 2 0.553936 0.590499 0.536186 11.00000 -1.20000 AFIX 0 C10 1 0.708978 0.423189 0.540234 11.00000 0.09172 0.08538 = 0.07349 -0.02601 0.01619 -0.05324 C11 1 0.713445 0.391459 0.478458 11.00000 0.09715 0.09411 = 0.06266 -0.01521 0.00164 -0.05727 C12 1 0.764724 -0.096075 0.357966 11.00000 0.10518 0.07359 = 0.04860 -0.00173 0.00569 -0.05033 AFIX 23 H12A 2 0.723723 -0.130377 0.336564 11.00000 -1.20000 H12B 2 0.851733 -0.136626 0.350118 11.00000 -1.20000 AFIX 0 C13 1 0.754212 -0.122003 0.427184 11.00000 0.11108 0.09142 = 0.04832 0.00006 0.00045 -0.06650 AFIX 23 H13A 2 0.803481 -0.096376 0.448830 11.00000 -1.20000 H13B 2 0.668160 -0.072872 0.435354 11.00000 -1.20000 AFIX 0 C14 1 0.798231 -0.258038 0.451279 11.00000 0.14802 0.10242 = 0.05629 -0.00069 -0.00130 -0.08258 AFIX 23 H14A 2 0.738150 -0.279105 0.436694 11.00000 -1.20000 H14B 2 0.876745 -0.308186 0.435228 11.00000 -1.20000 AFIX 0 C15 1 0.714668 -0.244977 0.555944 11.00000 0.09097 0.09991 = 0.07717 0.01407 -0.00483 -0.05743 C16 1 0.771685 -0.288270 0.619608 11.00000 0.09548 0.09224 = 0.06045 0.00329 0.01110 -0.04816 C17 1 0.718926 -0.270876 0.675062 11.00000 0.11671 0.12239 = 0.08615 -0.00187 0.02915 -0.05781 AFIX 43 H17 2 0.633126 -0.225458 0.676102 11.00000 -1.20000 AFIX 0 C18 1 0.798051 -0.323271 0.728791 11.00000 0.16011 0.18002 = 0.06264 -0.00230 0.02584 -0.07805 AFIX 43 H18 2 0.765092 -0.314706 0.766710 11.00000 -1.20000 AFIX 0 C19 1 0.921490 -0.386150 0.726840 11.00000 0.15435 0.20553 = 0.06122 0.01015 -0.00431 -0.05851 AFIX 43 H19 2 0.971955 -0.420132 0.763870 11.00000 -1.20000 AFIX 0 C20 1 0.976696 -0.402737 0.673235 11.00000 0.10660 0.19342 = 0.08006 0.02588 -0.00881 -0.04958 AFIX 43 H20 2 1.062850 -0.444657 0.673123 11.00000 -1.20000 AFIX 0 C21 1 0.898346 -0.354014 0.618117 11.00000 0.09138 0.10266 = 0.06251 0.00882 0.00498 -0.04423 C22 1 0.925005 -0.353906 0.552683 11.00000 0.09403 0.08947 = 0.06998 -0.00010 0.01951 -0.04951 B1 3 0.836940 0.027515 0.208052 11.00000 0.06616 0.06749 = 0.04434 -0.00701 0.01005 -0.03585 B2 3 0.705403 0.084330 0.242843 11.00000 0.06928 0.05773 = 0.03576 -0.00765 0.00695 -0.04058 B3 3 0.743621 0.184280 0.187135 11.00000 0.08211 0.06831 = 0.04206 -0.01306 0.01341 -0.05273 B4 3 0.776508 0.077125 0.133540 11.00000 0.07684 0.05977 = 0.04185 -0.01129 0.01660 -0.04216 B5 3 0.739284 -0.023349 0.189696 11.00000 0.07489 0.04998 = 0.04152 -0.00916 0.01383 -0.03383 B6 3 0.581978 0.230973 0.200187 11.00000 0.07550 0.04725 = 0.04368 -0.01252 0.01229 -0.03665 B7 3 0.630491 0.226883 0.122012 11.00000 0.08705 0.05005 = 0.03933 -0.00822 0.01347 -0.04236 B8 3 0.627493 0.080923 0.123253 11.00000 0.07848 0.05155 = 0.04096 -0.01184 0.00923 -0.03970 B9 3 0.579003 0.084032 0.201578 11.00000 0.06743 0.04986 = 0.04294 -0.00919 0.00681 -0.03680 B10 3 0.508919 0.208461 0.143452 11.00000 0.07289 0.05337 = 0.04522 -0.00710 0.00418 -0.03455 N3 6 0.405670 0.760630 0.134589 11.00000 0.07374 0.05247 = 0.05194 -0.01365 0.01120 -0.03695 C23 1 0.464504 0.670017 0.194891 11.00000 0.09951 0.07148 = 0.06841 -0.00898 0.00490 -0.05116 AFIX 23 H23A 2 0.512644 0.586597 0.186069 11.00000 -1.20000 H23B 2 0.398634 0.671235 0.219257 11.00000 -1.20000 AFIX 0 C24 1 0.548315 0.694596 0.233484 11.00000 0.11847 0.09732 = 0.08581 -0.00381 -0.00862 -0.06348 AFIX 23 H24A 2 0.611250 0.698805 0.208459 11.00000 -1.20000 H24B 2 0.499145 0.775402 0.245033 11.00000 -1.20000 AFIX 0 C25 1 0.611524 0.598486 0.290640 11.00000 0.15810 0.09950 = 0.07074 0.00443 -0.02381 -0.07367 AFIX 23 H25A 2 0.549101 0.592829 0.315567 11.00000 -1.20000 H25B 2 0.662833 0.517808 0.279334 11.00000 -1.20000 AFIX 0 C26 1 0.689495 0.627400 0.327332 11.00000 0.13229 0.16272 = 0.10603 0.00010 -0.02092 -0.07886 AFIX 137 H26A 2 0.766406 0.605586 0.309149 11.00000 -1.50000 H26B 2 0.706460 0.580482 0.368648 11.00000 -1.50000 H26C 2 0.646681 0.715065 0.328226 11.00000 -1.50000 AFIX 0 C27 1 0.340029 0.713240 0.097389 11.00000 0.08734 0.07516 = 0.07147 -0.02531 0.01200 -0.04883 AFIX 23 H27A 2 0.308748 0.768624 0.057486 11.00000 -1.20000 H27B 2 0.401231 0.631531 0.090197 11.00000 -1.20000 AFIX 0 C28 1 0.234805 0.702729 0.125238 11.00000 0.08260 0.08721 = 0.09558 -0.03021 0.01686 -0.05058 AFIX 23 H28A 2 0.173890 0.783230 0.133896 11.00000 -1.20000 H28B 2 0.265659 0.643541 0.164054 11.00000 -1.20000 AFIX 0 C29 1 0.172496 0.660505 0.083219 11.00000 0.10736 0.12635 = 0.13922 -0.04783 0.01413 -0.07946 AFIX 23 H29A 2 0.138540 0.722350 0.045358 11.00000 -1.20000 H29B 2 0.235326 0.582908 0.072540 11.00000 -1.20000 AFIX 0 C30 1 0.073149 0.641302 0.108884 11.00000 0.11407 0.18470 = 0.20832 -0.09567 0.04697 -0.10457 AFIX 137 H30A 2 0.040754 0.612380 0.079760 11.00000 -1.50000 H30B 2 0.007825 0.718688 0.117384 11.00000 -1.50000 H30C 2 0.105392 0.580183 0.146424 11.00000 -1.50000 AFIX 0 C31 1 0.504433 0.771966 0.097082 11.00000 0.08511 0.06390 = 0.06760 -0.01157 0.01095 -0.04296 AFIX 23 H31A 2 0.464086 0.825373 0.057467 11.00000 -1.20000 H31B 2 0.537107 0.814012 0.118128 11.00000 -1.20000 AFIX 0 C32 1 0.611065 0.654078 0.085609 11.00000 0.08188 0.07080 = 0.10876 -0.02485 0.02329 -0.03650 AFIX 23 H32A 2 0.644485 0.595596 0.124561 11.00000 -1.20000 H32B 2 0.580573 0.618129 0.058978 11.00000 -1.20000 AFIX 0 C33 1 0.712120 0.667503 0.057396 11.00000 0.08670 0.09123 = 0.09370 -0.02512 0.01561 -0.04259 AFIX 23 H33A 2 0.740260 0.706515 0.083260 11.00000 -1.20000 H33B 2 0.679161 0.723680 0.017776 11.00000 -1.20000 AFIX 0 C34 1 0.821040 0.549958 0.047793 11.00000 0.08801 0.09990 = 0.14248 -0.03905 0.03373 -0.04043 AFIX 137 H34A 2 0.802273 0.483057 0.056562 11.00000 -1.50000 H34B 2 0.891294 0.531311 0.074846 11.00000 -1.50000 H34C 2 0.840185 0.559279 0.005742 11.00000 -1.50000 AFIX 0 C35 1 0.316002 0.887832 0.148646 11.00000 0.08813 0.06431 = 0.07793 -0.02140 0.01583 -0.03975 AFIX 23 H35A 2 0.260135 0.877249 0.176840 11.00000 -1.20000 H35B 2 0.364015 0.914350 0.170631 11.00000 -1.20000 AFIX 0 C36 1 0.239722 0.989884 0.097710 11.00000 0.08266 0.06890 = 0.11166 -0.00972 0.00858 -0.02822 AFIX 23 H36A 2 0.186904 0.967203 0.076834 11.00000 -1.20000 H36B 2 0.294027 1.000019 0.068314 11.00000 -1.20000 AFIX 0 C37 1 0.160455 1.110732 0.116660 11.00000 0.10207 0.06332 = 0.18623 -0.02139 0.00539 -0.02610 AFIX 23 H37A 2 0.108609 1.098649 0.147018 11.00000 -1.20000 H37B 2 0.214389 1.132584 0.137179 11.00000 -1.20000 AFIX 0 C38 1 0.081520 1.214539 0.069950 11.00000 0.11543 0.08191 = 0.28965 0.02015 0.00040 -0.03104 AFIX 137 H38A 2 0.131346 1.235391 0.042257 11.00000 -1.50000 H38B 2 0.029716 1.284762 0.088592 11.00000 -1.50000 H38C 2 0.030187 1.193573 0.047452 11.00000 -1.50000 AFIX 0 HKLF 4 REM 19kbub41_0m_a.res in P-1 REM R1 = 0.0617 for 8539 Fo > 4sig(Fo) and 0.0958 for all 13298 data REM 590 parameters refined using 0 restraints END WGHT 0.1158 0.6035 REM Highest difference peak 0.664, deepest hole -0.449, 1-sigma level 0.062 Q1 1 1.0152 -0.0471 0.2483 11.00000 0.05 0.66 Q2 1 0.3820 0.3288 0.1198 11.00000 0.05 0.59 Q3 1 1.0099 -0.1032 0.2440 11.00000 0.05 0.52 Q4 1 0.6289 0.3206 0.0549 11.00000 0.05 0.49 Q5 1 0.5018 0.6624 0.0990 11.00000 0.05 0.48 Q6 1 0.4722 0.7597 0.1920 11.00000 0.05 0.48 Q7 1 0.3818 0.2447 0.1122 11.00000 0.05 0.48 Q8 1 0.6616 -0.0378 0.0794 11.00000 0.05 0.48 Q9 1 0.3462 0.8867 0.0936 11.00000 0.05 0.47 Q10 1 0.5944 0.0000 0.0521 11.00000 0.05 0.43 Q11 1 0.7052 0.5840 0.0502 11.00000 0.05 0.40 Q12 1 0.5663 0.0314 0.0759 11.00000 0.05 0.39 Q13 1 0.3028 0.7267 0.1521 11.00000 0.05 0.39 Q14 1 0.1964 1.1156 0.0703 11.00000 0.05 0.38 Q15 1 0.9035 0.0707 0.0889 11.00000 0.05 0.37 Q16 1 0.9164 0.0370 0.1001 11.00000 0.05 0.36 Q17 1 0.1459 0.6729 0.1395 11.00000 0.05 0.31 Q18 1 0.8237 0.0570 0.0759 11.00000 0.05 0.30 Q19 1 0.8985 0.0335 0.0608 11.00000 0.05 0.28 Q20 1 0.8532 -0.1840 0.2211 11.00000 0.05 0.27 ; _shelx_res_checksum 22394 _shelx_hkl_file ; -3 0 0 62.89 5.70 -3 0 0 48.60 4.90 3 0 0 58.29 4.90 3 0 0 62.09 5.70 -4 0 0 248.88 14.60 -4 0 0 245.98 15.40 4 0 0 260.27 15.50 4 0 0 260.07 14.60 4 0 0 262.07 13.40 -5 0 0 1898.81 96.99 5 0 0 1861.51 95.19 5 0 0 1997.40 97.09 5 0 0 1860.91 96.29 -6 0 0 791.32 43.40 -6 0 0 764.02 42.40 6 0 0 826.02 42.60 6 0 0 825.52 41.00 6 0 0 832.32 43.50 -7 0 0 206.18 14.30 -7 0 0 239.08 16.10 7 0 0 260.37 16.40 7 0 0 216.58 14.60 7 0 0 205.78 12.30 -8 0 0 431.36 25.00 -8 0 0 394.26 23.20 8 0 0 392.66 23.50 8 0 0 408.36 25.00 8 0 0 374.76 21.00 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101.69 6.70 4 -6 4 111.69 12.00 -5 6 -4 -4.60 8.50 5 -6 4 3.40 7.40 -6 6 -4 18.30 9.60 6 -6 4 15.30 8.50 -7 6 -4 57.79 11.80 7 -6 4 28.80 9.60 -8 6 -4 -13.60 9.60 8 -6 4 2.00 9.00 -9 6 -4 -0.60 11.00 9 -6 4 -2.70 9.70 16 5 -4 12.00 9.90 16 5 -4 -13.20 9.60 15 5 -4 10.60 9.00 15 5 -4 -0.70 9.40 14 5 -4 27.40 10.30 14 5 -4 25.20 8.50 13 5 -4 -1.20 6.90 13 5 -4 10.90 7.50 13 5 -4 4.90 7.90 12 5 -4 0.50 6.70 12 5 -4 1.10 7.50 12 5 -4 1.60 5.60 12 5 -4 7.00 8.60 -12 -5 4 -3.70 6.00 11 5 -4 297.77 20.30 11 5 -4 256.27 18.30 11 5 -4 288.17 19.60 11 5 -4 269.07 19.40 -11 -5 4 245.78 18.90 10 5 -4 9.00 6.20 10 5 -4 7.10 5.20 10 5 -4 7.00 6.00 10 5 -4 4.20 5.80 -10 -5 4 6.40 5.30 9 5 -4 36.70 5.90 9 5 -4 38.10 6.30 9 5 -4 37.10 6.50 -9 -5 4 47.30 6.20 8 5 -4 118.69 9.70 8 5 -4 100.79 9.90 8 5 -4 120.59 9.90 8 5 -4 103.59 9.70 -8 -5 4 99.29 9.00 7 5 -4 239.88 15.40 7 5 -4 279.47 15.40 7 5 -4 275.07 15.50 -7 -5 4 199.48 14.40 6 5 -4 63.69 6.70 6 5 -4 59.69 6.00 6 5 -4 61.09 6.30 -6 -5 4 62.89 6.30 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11.60 9.40 15 8 -5 6.60 8.50 15 8 -5 21.40 9.50 14 8 -5 1.10 8.00 14 8 -5 -3.20 7.40 13 8 -5 98.99 11.30 13 8 -5 85.59 11.70 13 8 -5 82.89 10.60 12 8 -5 57.79 8.70 12 8 -5 54.39 9.60 12 8 -5 60.79 8.90 11 8 -5 34.60 7.30 11 8 -5 30.90 7.10 11 8 -5 37.50 8.40 -11 -8 5 34.10 7.10 10 8 -5 42.10 7.00 10 8 -5 42.80 8.30 10 8 -5 43.20 7.10 -10 -8 5 30.40 7.90 9 8 -5 35.10 7.60 9 8 -5 40.30 6.50 9 8 -5 30.70 7.30 9 8 -5 47.30 6.60 -9 -8 5 33.70 6.60 8 8 -5 108.79 10.40 8 8 -5 92.79 9.70 8 8 -5 98.69 9.80 8 8 -5 106.79 11.30 -8 -8 5 104.79 10.80 -8 -8 5 110.49 10.70 7 8 -5 238.08 17.50 7 8 -5 233.78 16.30 7 8 -5 276.07 17.60 -7 -8 5 274.67 15.80 -7 -8 5 280.87 17.60 -7 -8 5 274.67 17.40 6 8 -5 319.67 20.30 6 8 -5 321.77 19.00 6 8 -5 319.67 20.60 -6 -8 5 344.37 20.20 -6 -8 5 344.77 18.70 -6 -8 5 315.37 20.20 5 8 -5 1424.46 71.09 5 8 -5 1407.46 69.79 5 8 -5 1338.87 70.69 -5 -8 5 1385.76 70.99 -5 -8 5 1304.57 70.29 -5 -8 5 1332.67 69.69 4 8 -5 -5.70 5.10 4 8 -5 0.10 3.70 4 8 -5 -2.90 4.30 -4 -8 5 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7.30 13 7 -5 2.90 7.50 12 7 -5 23.10 8.10 12 7 -5 17.00 7.30 12 7 -5 14.00 7.20 -12 -7 5 18.80 6.80 11 7 -5 70.79 9.10 11 7 -5 74.19 9.40 11 7 -5 59.79 9.00 -11 -7 5 63.89 8.30 10 7 -5 -2.40 5.60 10 7 -5 -4.10 5.50 10 7 -5 -8.60 6.00 10 7 -5 -5.20 5.40 -10 -7 5 1.20 5.40 9 7 -5 3.80 5.50 9 7 -5 9.90 6.30 9 7 -5 25.00 5.80 9 7 -5 26.80 5.80 -9 -7 5 29.20 6.10 8 7 -5 380.46 21.60 8 7 -5 358.86 22.30 8 7 -5 359.86 22.20 -8 -7 5 390.16 22.00 7 7 -5 137.69 11.90 7 7 -5 153.38 11.90 7 7 -5 140.39 10.80 -7 -7 5 144.69 11.20 -7 -7 5 126.59 10.20 -7 -7 5 150.78 11.70 6 7 -5 32.10 5.20 6 7 -5 23.40 5.30 6 7 -5 34.10 6.10 -6 -7 5 32.10 4.70 -6 -7 5 28.40 5.70 -6 -7 5 25.10 5.20 5 7 -5 44.00 6.20 5 7 -5 54.79 6.80 5 7 -5 54.09 5.90 -5 -7 5 38.00 5.70 -5 -7 5 45.20 5.30 -5 -7 5 50.39 6.70 4 7 -5 120.59 10.40 4 7 -5 134.69 9.40 4 7 -5 125.89 10.40 -4 -7 5 128.29 10.50 -4 -7 5 124.19 9.30 -4 -7 5 117.89 10.60 3 7 -5 334.07 19.80 3 7 -5 343.67 19.10 3 7 -5 320.37 19.80 -3 -7 5 344.17 19.60 -3 -7 5 352.36 19.60 -3 -7 5 322.07 20.10 2 7 -5 4.00 3.90 2 7 -5 4.90 4.70 2 7 -5 0.00 4.00 -2 -7 5 10.40 4.50 -2 -7 5 5.20 5.10 -2 -7 5 6.70 4.00 1 7 -5 426.86 25.50 -1 -7 5 452.25 26.10 -1 -7 5 447.36 25.40 -1 -7 5 467.35 24.90 -1 -7 5 474.85 25.90 0 7 -5 37.30 6.90 0 7 -5 45.00 5.50 0 -7 5 48.00 5.50 0 -7 5 46.10 7.40 0 -7 5 50.89 6.80 0 -7 5 50.79 7.00 -1 7 -5 60.59 8.20 -1 7 -5 47.00 5.40 1 -7 5 48.30 5.30 1 -7 5 54.49 7.80 1 -7 5 58.69 7.90 1 -7 5 43.50 7.10 -2 7 -5 28.20 7.70 2 -7 5 37.20 4.60 2 -7 5 38.80 7.60 2 -7 5 47.60 7.70 2 -7 5 23.30 6.70 -3 7 -5 110.29 12.50 3 -7 5 89.59 16.50 3 -7 5 103.99 11.40 4 -7 5 11.80 7.40 -5 7 -5 5.80 8.90 5 -7 5 2.90 7.50 -6 7 -5 7.00 9.20 6 -7 5 2.00 7.90 -7 7 -5 0.70 9.90 7 -7 5 -4.80 8.50 -8 7 -5 -6.70 9.80 8 -7 5 -0.20 9.60 16 6 -5 15.30 9.50 15 6 -5 4.40 9.50 15 6 -5 11.90 8.70 14 6 -5 -3.80 7.50 14 6 -5 -7.20 8.40 13 6 -5 -3.60 7.70 12 6 -5 42.40 8.60 12 6 -5 22.30 6.90 12 6 -5 31.60 8.10 -12 -6 5 22.10 6.80 11 6 -5 349.87 22.50 11 6 -5 337.87 22.70 11 6 -5 373.76 22.70 10 6 -5 3.20 6.10 10 6 -5 10.80 6.20 10 6 -5 8.00 6.20 10 6 -5 9.30 6.40 -10 -6 5 14.10 4.30 9 6 -5 -0.20 5.10 9 6 -5 5.00 6.00 9 6 -5 -3.10 5.30 9 6 -5 2.10 4.90 -9 -6 5 1.30 2.80 8 6 -5 167.78 12.70 8 6 -5 188.38 13.30 8 6 -5 165.88 12.90 8 6 -5 189.88 12.80 7 6 -5 86.79 8.90 7 6 -5 101.89 9.00 7 6 -5 107.79 8.80 -7 -6 5 68.29 7.40 6 6 -5 31.90 5.60 6 6 -5 25.40 5.10 6 6 -5 43.80 5.50 -6 -6 5 42.80 5.10 -6 -6 5 30.10 5.50 -6 -6 5 37.70 5.60 5 6 -5 10.20 4.20 5 6 -5 5.00 4.20 5 6 -5 1.80 5.10 -5 -6 5 5.30 3.50 -5 -6 5 7.10 4.40 -5 -6 5 1.70 4.00 4 6 -5 214.38 13.80 4 6 -5 214.28 14.00 4 6 -5 228.08 15.50 -4 -6 5 230.38 14.50 -4 -6 5 224.68 14.10 -4 -6 5 227.78 13.50 3 6 -5 1466.25 74.69 3 6 -5 1521.75 74.49 3 6 -5 1499.85 74.89 -3 -6 5 1392.16 74.59 -3 -6 5 1460.65 74.99 -3 -6 5 1438.36 74.49 2 6 -5 279.27 16.60 2 6 -5 295.37 16.40 2 6 -5 269.77 16.60 -2 -6 5 263.67 17.00 -2 -6 5 281.27 16.60 -2 -6 5 267.57 16.20 1 6 -5 2688.63 138.19 -1 -6 5 2706.33 137.69 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12.00 11 5 -5 85.49 9.90 11 5 -5 87.79 9.70 10 5 -5 643.44 35.60 10 5 -5 599.84 34.30 10 5 -5 641.64 36.00 10 5 -5 617.34 35.10 9 5 -5 3.10 4.90 9 5 -5 1.60 3.20 9 5 -5 17.00 5.60 9 5 -5 12.30 5.70 -9 -5 5 -1.60 0.90 8 5 -5 219.48 14.40 8 5 -5 207.58 14.10 8 5 -5 208.68 14.40 7 5 -5 91.09 8.80 7 5 -5 94.99 8.80 7 5 -5 83.89 9.00 6 5 -5 63.99 6.60 6 5 -5 55.69 6.20 6 5 -5 67.69 7.30 -6 -5 5 68.39 7.20 5 5 -5 126.29 10.30 5 5 -5 126.69 9.80 5 5 -5 133.89 9.90 -5 -5 5 130.59 9.40 4 5 -5 9.80 4.50 4 5 -5 7.30 3.90 4 5 -5 6.80 4.20 -4 -5 5 4.30 4.00 -4 -5 5 19.00 4.10 -4 -5 5 7.90 4.30 3 5 -5 520.75 28.00 3 5 -5 516.05 27.90 3 5 -5 553.04 28.10 -3 -5 5 498.75 27.90 -3 -5 5 495.35 28.70 -3 -5 5 529.65 28.10 2 5 -5 1192.78 58.29 2 5 -5 1125.09 58.19 2 5 -5 1106.29 58.89 -2 -5 5 1063.59 57.89 -2 -5 5 1146.89 58.39 -2 -5 5 1179.28 59.29 1 5 -5 57.09 6.20 -1 -5 5 46.70 6.10 -1 -5 5 41.20 5.80 -1 -5 5 44.10 4.80 0 5 -5 120.79 8.90 0 5 -5 117.99 10.20 0 -5 5 120.59 9.90 0 -5 5 124.29 8.70 0 -5 5 118.59 10.00 0 -5 5 139.29 10.00 -1 5 -5 225.78 14.30 -1 5 -5 196.38 12.10 1 -5 5 185.58 13.20 1 -5 5 210.38 13.90 1 -5 5 207.38 11.90 1 -5 5 197.18 13.40 -2 5 -5 499.55 29.30 -2 5 -5 480.95 26.90 2 -5 5 536.45 28.50 2 -5 5 531.25 26.70 2 -5 5 526.75 29.00 2 -5 5 512.05 28.70 -3 5 -5 36.60 7.60 -3 5 -5 51.09 4.70 3 -5 5 50.79 6.80 3 -5 5 40.80 7.30 3 -5 5 44.70 6.90 -4 5 -5 71.59 10.20 4 -5 5 55.69 8.10 4 -5 5 90.09 10.00 -5 5 -5 30.40 9.20 5 -5 5 17.70 7.70 5 -5 5 34.10 7.90 -6 5 -5 13.10 9.20 6 -5 5 12.80 7.60 -7 5 -5 47.40 11.50 7 -5 5 35.80 9.90 -8 5 -5 9.90 9.50 8 -5 5 4.00 8.30 -9 5 -5 15.80 10.70 9 -5 5 -4.40 8.60 -10 5 -5 6.90 11.40 10 -5 5 -1.70 9.70 15 4 -5 -3.30 10.10 15 4 -5 -6.10 8.00 14 4 -5 8.00 9.50 14 4 -5 0.40 7.80 13 4 -5 10.30 6.40 13 4 -5 30.40 10.00 13 4 -5 19.40 8.10 12 4 -5 13.60 6.90 12 4 -5 3.90 5.50 12 4 -5 -1.70 8.10 -12 -4 5 2.50 3.20 11 4 -5 3.10 6.40 11 4 -5 0.10 7.30 11 4 -5 2.70 7.50 -11 -4 5 -0.40 1.30 10 4 -5 50.19 8.50 10 4 -5 39.90 6.30 10 4 -5 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11.00 3 14 -7 35.80 8.70 -3 -14 7 41.00 11.60 2 14 -7 -4.80 7.40 14 13 -7 10.00 6.70 14 13 -7 18.50 12.00 13 13 -7 3.50 5.20 13 13 -7 10.80 9.10 12 13 -7 12.20 5.80 12 13 -7 -10.00 8.20 11 13 -7 -1.60 8.40 11 13 -7 14.70 4.70 10 13 -7 27.20 5.90 10 13 -7 18.10 4.80 10 13 -7 29.20 9.60 9 13 -7 10.90 4.20 9 13 -7 0.40 7.60 9 13 -7 11.30 6.70 8 13 -7 7.90 4.40 8 13 -7 2.40 8.00 -8 -13 7 11.90 4.70 7 13 -7 40.90 6.00 7 13 -7 29.60 9.50 -7 -13 7 25.60 5.70 -7 -13 7 23.50 9.30 6 13 -7 10.10 9.40 6 13 -7 11.00 5.70 -6 -13 7 0.30 8.30 -6 -13 7 -1.40 5.00 5 13 -7 27.10 6.70 -5 -13 7 36.40 8.80 -5 -13 7 16.80 6.20 4 13 -7 61.19 8.70 -4 -13 7 46.90 9.70 -4 -13 7 49.99 11.40 -4 -13 7 42.40 7.60 3 13 -7 11.00 7.20 -3 -13 7 18.80 7.00 -3 -13 7 -1.10 7.90 -3 -13 7 17.00 9.10 2 13 -7 2.90 7.90 -2 -13 7 21.40 11.10 1 13 -7 12.70 8.50 -1 -13 7 2.40 9.60 0 13 -7 12.80 9.00 14 12 -7 23.10 9.90 14 12 -7 17.10 7.10 13 12 -7 42.40 10.20 13 12 -7 29.60 6.70 13 12 -7 21.60 7.10 12 12 -7 19.20 5.90 12 12 -7 17.50 6.50 12 12 -7 24.00 9.30 11 12 -7 97.79 9.90 11 12 -7 92.29 12.50 11 12 -7 93.29 10.10 10 12 -7 7.90 4.90 10 12 -7 11.40 4.90 10 12 -7 7.50 7.80 9 12 -7 49.80 9.20 9 12 -7 41.20 6.00 8 12 -7 172.68 16.10 -8 -12 7 180.48 12.50 7 12 -7 61.39 7.10 7 12 -7 52.79 9.90 -7 -12 7 56.89 7.30 -7 -12 7 47.90 9.10 6 12 -7 110.09 10.60 6 12 -7 94.59 11.90 -6 -12 7 97.69 11.10 -6 -12 7 99.69 10.20 5 12 -7 137.09 13.80 5 12 -7 154.58 12.70 -5 -12 7 132.99 12.00 -5 -12 7 127.59 12.30 4 12 -7 119.69 12.50 -4 -12 7 110.39 11.30 -4 -12 7 111.29 13.50 -4 -12 7 117.69 11.80 3 12 -7 41.30 8.30 -3 -12 7 43.50 8.40 -3 -12 7 36.30 8.40 -3 -12 7 52.29 10.60 2 12 -7 4.00 7.40 -2 -12 7 0.50 6.10 -2 -12 7 -4.10 8.20 -2 -12 7 4.30 7.30 -1 -12 7 41.80 10.00 0 12 -7 25.80 9.50 0 -12 7 25.50 15.90 -1 12 -7 -0.30 5.80 -1 12 -7 27.40 10.00 1 -12 7 8.00 9.60 -2 12 -7 1.30 9.50 15 11 -7 3.00 7.20 15 11 -7 19.50 9.70 14 11 -7 8.60 7.30 14 11 -7 -5.50 8.50 14 11 -7 28.70 6.90 13 11 -7 5.80 6.90 13 11 -7 6.00 8.70 13 11 -7 6.80 5.90 12 11 -7 91.99 9.40 12 11 -7 67.79 9.40 12 11 -7 83.39 11.50 11 11 -7 21.30 6.10 11 11 -7 24.20 6.70 11 11 -7 12.70 8.30 10 11 -7 137.49 14.80 10 11 -7 98.89 11.20 10 11 -7 130.99 10.80 9 11 -7 117.79 10.60 9 11 -7 128.79 13.80 9 11 -7 101.29 9.90 8 11 -7 2.40 4.70 8 11 -7 9.90 8.90 -8 -11 7 -1.70 4.50 7 11 -7 72.69 12.20 7 11 -7 94.59 9.60 -7 -11 7 77.19 10.20 -7 -11 7 96.99 8.70 6 11 -7 80.39 10.80 6 11 -7 73.29 8.00 -6 -11 7 63.19 7.60 -6 -11 7 53.59 8.90 5 11 -7 27.70 8.30 5 11 -7 25.10 5.90 -5 -11 7 18.10 6.00 -5 -11 7 21.00 7.50 4 11 -7 20.30 6.40 -4 -11 7 21.50 6.40 -4 -11 7 24.50 8.40 3 11 -7 38.90 7.70 -3 -11 7 20.50 8.30 -3 -11 7 37.20 7.80 -3 -11 7 30.50 7.20 2 11 -7 8.20 6.30 2 11 -7 -1.20 6.50 -2 -11 7 -5.20 6.20 -2 -11 7 1.70 7.70 1 11 -7 16.20 7.60 1 11 -7 9.10 5.50 -1 -11 7 22.30 7.30 -1 -11 7 15.40 9.00 0 11 -7 116.69 14.60 0 11 -7 115.09 11.30 0 -11 7 113.59 13.30 -1 11 -7 53.69 10.90 1 -11 7 37.30 9.50 -2 11 -7 7.70 9.10 2 -11 7 2.50 8.90 -3 11 -7 10.10 10.40 3 -11 7 1.60 9.10 15 10 -7 1.30 8.80 15 10 -7 7.30 7.90 14 10 -7 14.50 7.10 14 10 -7 -0.80 8.00 13 10 -7 2.90 6.70 13 10 -7 2.70 6.60 13 10 -7 8.60 8.10 12 10 -7 -3.50 6.10 12 10 -7 4.30 6.20 12 10 -7 2.40 7.60 11 10 -7 0.50 6.00 11 10 -7 7.80 5.80 10 10 -7 180.78 15.70 10 10 -7 149.69 12.70 10 10 -7 170.88 13.90 9 10 -7 25.50 8.20 9 10 -7 39.80 7.10 9 10 -7 28.20 5.90 -9 -10 7 43.50 8.00 8 10 -7 411.16 24.50 8 10 -7 382.56 22.90 -8 -10 7 383.26 24.30 -8 -10 7 376.06 22.30 7 10 -7 56.39 7.00 7 10 -7 39.90 8.20 -7 -10 7 45.60 6.50 -7 -10 7 42.10 7.70 -7 -10 7 41.10 8.40 6 10 -7 99.39 10.60 6 10 -7 100.49 10.10 -6 -10 7 117.79 12.10 -6 -10 7 94.29 9.60 -6 -10 7 104.69 14.70 5 10 -7 23.00 5.80 5 10 -7 23.80 7.20 -5 -10 7 23.70 7.90 -5 -10 7 21.20 6.70 -5 -10 7 20.90 5.80 4 10 -7 19.40 6.10 4 10 -7 21.40 7.50 4 10 -7 24.80 6.40 -4 -10 7 21.70 6.00 -4 -10 7 7.70 6.20 3 10 -7 14.50 5.80 3 10 -7 36.20 7.10 -3 -10 7 31.10 6.80 -3 -10 7 20.30 6.40 2 10 -7 -5.00 6.10 2 10 -7 4.30 1.70 -2 -10 7 2.00 6.10 -2 -10 7 16.80 7.90 -2 -10 7 8.30 5.90 1 10 -7 113.29 11.80 -1 -10 7 109.29 11.60 -1 -10 7 65.09 8.30 -1 -10 7 84.19 10.30 0 10 -7 5.60 7.60 0 10 -7 11.40 5.20 0 -10 7 11.10 7.70 0 -10 7 4.30 6.70 -1 10 -7 21.00 8.90 -1 10 -7 6.00 4.60 1 -10 7 16.10 8.20 -2 10 -7 55.49 11.10 -2 10 -7 33.00 5.30 2 -10 7 39.60 10.00 -3 10 -7 15.50 9.90 3 -10 7 -0.30 9.90 -4 10 -7 41.30 11.70 4 -10 7 12.10 9.70 -5 10 -7 3.10 10.60 15 9 -7 2.40 8.30 15 9 -7 14.60 9.10 14 9 -7 6.90 8.50 14 9 -7 5.70 7.70 13 9 -7 -10.30 6.50 13 9 -7 13.60 8.20 13 9 -7 6.30 7.10 12 9 -7 -4.70 10.30 12 9 -7 9.70 6.60 12 9 -7 14.40 9.40 11 9 -7 34.40 8.40 11 9 -7 36.10 7.40 11 9 -7 28.20 6.90 10 9 -7 45.60 7.30 10 9 -7 24.30 7.60 10 9 -7 39.40 7.20 -10 -9 7 19.40 6.00 9 9 -7 64.39 8.30 9 9 -7 72.09 9.50 9 9 -7 74.99 8.00 -9 -9 7 55.89 8.30 8 9 -7 213.28 15.90 8 9 -7 202.68 15.20 -8 -9 7 208.88 14.20 7 9 -7 542.85 30.50 7 9 -7 512.45 29.70 -7 -9 7 513.45 30.60 -7 -9 7 552.44 29.30 6 9 -7 184.68 14.80 6 9 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9.60 8.90 14 8 -7 5.40 8.20 14 8 -7 -2.40 7.80 13 8 -7 4.40 8.70 13 8 -7 5.70 7.40 12 8 -7 66.49 9.80 12 8 -7 73.49 9.60 12 8 -7 76.79 10.00 -12 -8 7 59.79 8.70 11 8 -7 32.00 7.80 11 8 -7 22.80 7.30 11 8 -7 30.10 7.30 -11 -8 7 11.40 5.40 10 8 -7 -2.80 5.30 10 8 -7 1.30 5.90 10 8 -7 1.20 6.40 -10 -8 7 1.70 3.10 9 8 -7 112.19 10.90 9 8 -7 98.09 9.60 9 8 -7 99.59 11.20 8 8 -7 131.29 12.00 8 8 -7 129.89 12.00 8 8 -7 126.19 11.40 -8 -8 7 126.29 10.90 7 8 -7 297.87 19.60 7 8 -7 311.27 19.60 7 8 -7 308.67 20.10 -7 -8 7 327.07 18.80 -7 -8 7 313.77 19.70 6 8 -7 13.60 5.40 6 8 -7 17.80 6.10 -6 -8 7 24.90 6.50 -6 -8 7 26.50 5.30 5 8 -7 53.99 8.30 5 8 -7 58.29 7.60 -5 -8 7 63.49 7.10 -5 -8 7 69.59 8.50 -5 -8 7 60.79 7.60 4 8 -7 477.35 27.30 4 8 -7 503.25 27.00 4 8 -7 477.45 27.40 -4 -8 7 480.05 26.90 -4 -8 7 457.35 27.50 -4 -8 7 475.55 27.00 3 8 -7 348.87 21.00 3 8 -7 334.97 21.20 3 8 -7 385.26 21.30 -3 -8 7 335.37 21.80 -3 -8 7 335.77 21.00 -3 -8 7 363.06 20.80 2 8 -7 273.67 17.60 2 8 -7 301.47 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3.90 6.60 -8 -10 8 -1.50 4.80 7 10 -8 73.99 8.10 7 10 -8 63.39 8.90 -7 -10 8 59.59 7.60 -7 -10 8 45.50 9.20 6 10 -8 22.10 6.20 6 10 -8 30.50 7.80 -6 -10 8 24.40 6.20 -6 -10 8 27.20 8.10 5 10 -8 30.00 6.60 5 10 -8 23.70 7.40 -5 -10 8 27.40 8.10 -5 -10 8 22.60 6.10 4 10 -8 26.00 6.50 4 10 -8 14.40 7.10 -4 -10 8 31.90 6.70 3 10 -8 9.00 6.30 3 10 -8 9.10 5.50 -3 -10 8 1.90 7.60 -3 -10 8 8.40 6.20 2 10 -8 7.10 3.40 2 10 -8 4.50 6.70 -2 -10 8 2.00 7.30 -2 -10 8 10.50 6.30 1 10 -8 14.10 7.70 1 10 -8 16.60 5.70 -1 -10 8 20.90 7.50 -1 -10 8 15.10 7.40 0 10 -8 24.30 8.40 0 10 -8 12.00 5.30 0 -10 8 14.90 7.60 -1 10 -8 20.60 9.30 -1 10 -8 24.90 5.30 1 -10 8 21.40 8.60 -2 10 -8 -2.50 8.50 -2 10 -8 14.60 4.50 2 -10 8 -6.20 7.80 -3 10 -8 31.60 11.10 3 -10 8 22.50 10.70 -4 10 -8 6.60 10.10 4 -10 8 19.50 10.10 15 9 -8 6.50 8.40 15 9 -8 11.90 8.70 14 9 -8 4.40 8.30 14 9 -8 -5.20 7.50 13 9 -8 12.70 7.40 13 9 -8 2.20 11.40 13 9 -8 17.50 8.00 12 9 -8 13.10 7.10 12 9 -8 2.30 6.60 12 9 -8 6.10 7.40 11 9 -8 214.38 17.10 11 9 -8 231.78 17.40 11 9 -8 243.08 16.90 -11 -9 8 211.58 16.10 10 9 -8 10.20 7.10 10 9 -8 19.90 6.40 10 9 -8 20.70 6.90 -10 -9 8 3.40 4.30 9 9 -8 -2.50 5.80 9 9 -8 7.40 6.60 8 9 -8 134.29 12.50 8 9 -8 118.19 12.40 -8 -9 8 125.79 11.20 7 9 -8 18.80 7.00 7 9 -8 33.40 6.90 -7 -9 8 15.10 7.80 -7 -9 8 32.40 6.10 6 9 -8 54.09 7.50 6 9 -8 31.30 7.20 6 9 -8 44.90 8.00 -6 -9 8 26.20 9.00 -6 -9 8 56.79 7.10 5 9 -8 68.59 7.70 5 9 -8 68.59 8.90 5 9 -8 52.09 8.10 -5 -9 8 50.19 7.20 -5 -9 8 61.19 10.70 4 9 -8 15.90 6.10 4 9 -8 28.20 6.90 4 9 -8 25.80 6.20 -4 -9 8 22.30 7.00 -4 -9 8 16.90 6.10 3 9 -8 87.29 9.30 3 9 -8 61.79 8.10 -3 -9 8 87.99 9.90 -3 -9 8 81.99 10.50 -3 -9 8 71.49 9.10 2 9 -8 88.99 9.80 -2 -9 8 79.89 9.40 -2 -9 8 68.19 9.90 -2 -9 8 70.79 9.20 1 9 -8 2.90 6.60 1 9 -8 10.20 5.10 -1 -9 8 5.60 13.00 -1 -9 8 20.50 7.80 0 9 -8 5.00 4.60 0 9 -8 4.60 7.50 0 -9 8 14.20 7.00 0 -9 8 19.20 7.40 -1 9 -8 20.70 4.90 -1 9 -8 12.40 8.20 1 -9 8 18.20 7.80 -2 9 -8 1.60 3.70 -2 9 -8 2.20 8.20 2 -9 8 -1.40 7.10 -3 9 -8 -2.20 9.40 3 -9 8 8.20 8.30 -4 9 -8 18.60 10.50 4 -9 8 20.90 9.80 -5 9 -8 2.20 10.30 5 -9 8 -13.60 9.10 -6 9 -8 2.10 10.90 15 8 -8 11.20 8.90 15 8 -8 9.60 8.80 14 8 -8 4.30 8.10 14 8 -8 8.80 8.20 12 8 -8 -7.40 6.50 12 8 -8 7.80 7.30 12 8 -8 0.00 6.70 -12 -8 8 -0.40 5.70 11 8 -8 214.08 17.30 11 8 -8 239.48 17.70 11 8 -8 262.87 17.60 -11 -8 8 223.48 16.30 10 8 -8 -3.40 6.00 10 8 -8 5.40 6.50 10 8 -8 1.20 6.00 -10 -8 8 13.90 5.60 9 8 -8 27.80 6.90 9 8 -8 15.70 6.50 9 8 -8 17.40 5.90 -9 -8 8 23.10 5.90 8 8 -8 3.30 5.80 8 8 -8 -3.10 5.40 -8 -8 8 -5.50 4.60 -8 -8 8 0.30 4.80 7 8 -8 143.59 11.90 7 8 -8 124.49 11.90 7 8 -8 128.49 12.20 -7 -8 8 118.29 10.90 6 8 -8 0.90 5.20 6 8 -8 13.10 5.70 6 8 -8 7.00 5.10 -6 -8 8 7.30 5.80 -6 -8 8 12.00 5.10 5 8 -8 443.76 25.40 5 8 -8 421.76 25.30 5 8 -8 432.96 25.80 -5 -8 8 447.96 25.20 -5 -8 8 453.35 25.80 4 8 -8 229.88 15.70 4 8 -8 214.58 15.30 4 8 -8 235.98 15.50 -4 -8 8 219.88 15.80 -4 -8 8 214.58 15.20 3 8 -8 45.90 6.90 3 8 -8 66.79 7.90 -3 -8 8 57.49 8.40 -3 -8 8 47.50 7.30 2 8 -8 238.88 17.10 2 8 -8 287.47 18.30 -2 -8 8 317.67 24.20 -2 -8 8 293.77 18.40 -2 -8 8 260.37 18.20 1 8 -8 122.59 12.20 1 8 -8 97.69 9.20 -1 -8 8 110.89 12.00 -1 -8 8 117.99 11.70 -1 -8 8 112.99 11.80 0 8 -8 23.30 7.30 0 8 -8 21.50 5.10 0 -8 8 18.70 8.10 0 -8 8 21.50 8.20 0 -8 8 24.70 7.40 -1 8 -8 21.10 8.20 -1 8 -8 23.50 5.00 1 -8 8 31.30 7.70 1 -8 8 20.70 7.70 -2 8 -8 1.80 3.50 -2 8 -8 -5.70 7.40 2 -8 8 -4.50 6.70 -3 8 -8 45.20 6.80 -3 8 -8 43.70 10.50 3 -8 8 34.60 8.60 -4 8 -8 13.10 9.40 4 -8 8 12.20 8.00 -5 8 -8 15.00 10.20 5 -8 8 2.00 9.40 -6 8 -8 6.20 14.80 6 -8 8 -5.70 8.90 -7 8 -8 7.20 11.10 15 7 -8 2.50 8.40 15 7 -8 2.90 8.90 14 7 -8 6.20 7.90 14 7 -8 -8.80 7.90 13 7 -8 3.00 7.80 13 7 -8 12.80 8.10 12 7 -8 0.10 7.20 12 7 -8 -7.30 4.80 12 7 -8 -5.80 6.70 -12 -7 8 -7.40 5.30 11 7 -8 143.59 13.80 11 7 -8 145.49 13.40 11 7 -8 141.69 13.80 -11 -7 8 123.59 11.80 10 7 -8 28.60 7.40 10 7 -8 18.10 6.70 10 7 -8 17.50 7.00 -10 -7 8 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12 -9 81.89 8.40 10 12 -9 62.79 8.40 9 12 -9 18.00 6.00 9 12 -9 17.30 8.40 -9 -12 9 14.00 5.50 8 12 -9 2.70 7.90 8 12 -9 8.30 5.40 -8 -12 9 3.00 5.40 7 12 -9 1.00 8.00 7 12 -9 2.60 5.50 -7 -12 9 6.20 5.50 6 12 -9 16.50 8.30 6 12 -9 15.40 6.20 -6 -12 9 3.70 5.50 5 12 -9 21.60 6.90 -5 -12 9 13.40 6.20 -5 -12 9 18.60 9.10 4 12 -9 137.29 13.90 -4 -12 9 102.19 11.40 -4 -12 9 165.28 16.30 3 12 -9 72.39 10.40 -3 -12 9 55.79 8.90 -3 -12 9 50.79 10.40 -2 -12 9 0.10 8.40 1 12 -9 49.30 10.70 -1 -12 9 55.19 14.20 0 12 -9 56.29 11.10 0 -12 9 4.70 9.50 -1 12 -9 22.70 10.30 1 -12 9 21.60 11.50 14 11 -9 5.50 8.80 13 11 -9 1.10 8.20 13 11 -9 8.10 7.50 12 11 -9 45.40 9.70 12 11 -9 32.10 8.40 11 11 -9 21.10 6.80 11 11 -9 23.30 7.50 11 11 -9 27.00 8.70 10 11 -9 19.10 6.80 10 11 -9 9.80 7.60 10 11 -9 8.90 5.50 9 11 -9 0.80 7.20 9 11 -9 1.70 5.60 -9 -11 9 2.80 4.90 8 11 -9 9.10 7.40 8 11 -9 -4.40 5.40 -8 -11 9 -0.40 5.00 7 11 -9 27.60 6.50 7 11 -9 12.20 7.90 -7 -11 9 24.10 6.10 6 11 -9 339.77 20.90 6 11 -9 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8.50 -7 7 -9 44.30 12.70 7 -7 9 26.10 10.40 15 6 -9 -12.60 9.10 15 6 -9 -1.70 8.20 14 6 -9 29.80 9.90 14 6 -9 28.40 8.90 13 6 -9 33.50 8.30 13 6 -9 52.29 10.30 -13 -6 9 37.20 7.40 12 6 -9 1.90 7.70 12 6 -9 3.90 6.90 -12 -6 9 1.50 5.80 11 6 -9 46.00 9.10 11 6 -9 50.99 9.20 11 6 -9 51.19 8.00 -11 -6 9 49.60 7.00 10 6 -9 35.50 8.00 10 6 -9 31.50 8.60 10 6 -9 31.10 6.80 -10 -6 9 37.70 6.00 9 6 -9 8.70 5.80 9 6 -9 -9.30 4.90 9 6 -9 3.80 6.50 9 6 -9 1.50 3.70 -9 -6 9 1.80 4.50 8 6 -9 66.79 7.40 8 6 -9 63.59 8.30 8 6 -9 64.29 7.80 -8 -6 9 65.99 6.90 -8 -6 9 67.69 8.20 7 6 -9 1436.66 71.19 7 6 -9 1408.66 72.19 7 6 -9 1381.86 71.89 -7 -6 9 1286.27 70.89 -7 -6 9 1422.96 71.99 6 6 -9 440.66 24.60 6 6 -9 417.96 24.90 6 6 -9 420.86 25.10 -6 -6 9 403.56 24.50 -6 -6 9 434.26 23.80 5 6 -9 269.67 17.30 5 6 -9 278.57 18.80 5 6 -9 310.67 18.10 -5 -6 9 307.37 17.80 -5 -6 9 292.17 18.20 4 6 -9 2026.20 101.59 4 6 -9 2055.19 102.19 4 6 -9 2007.30 101.19 -4 -6 9 1901.81 101.89 -4 -6 9 1993.00 101.59 3 6 -9 2429.86 128.99 3 6 -9 2666.83 129.89 -3 -6 9 2568.24 129.69 2 6 -9 97.89 10.50 2 6 -9 113.49 9.50 -2 -6 9 105.79 9.50 -2 -6 9 111.79 10.10 -2 -6 9 113.19 10.80 1 6 -9 -0.70 3.20 1 6 -9 0.10 5.30 -1 -6 9 -1.60 5.50 -1 -6 9 -0.80 4.40 -1 -6 9 0.50 4.50 0 6 -9 147.89 11.00 0 6 -9 164.58 13.30 0 -6 9 157.68 12.10 0 -6 9 172.18 13.50 0 -6 9 147.79 12.10 -1 6 -9 207.18 13.40 -1 6 -9 235.38 16.60 1 -6 9 219.78 16.30 1 -6 9 203.48 14.90 -2 6 -9 7.90 7.50 -2 6 -9 5.60 3.40 2 -6 9 14.50 6.40 2 -6 9 13.90 7.30 2 -6 9 13.70 6.40 -3 6 -9 109.69 12.30 -3 6 -9 91.09 7.70 3 -6 9 116.09 12.00 -4 6 -9 30.70 9.60 4 -6 9 39.90 8.70 -5 6 -9 -5.70 8.20 5 -6 9 -2.10 7.50 -6 6 -9 2.20 9.50 6 -6 9 -7.90 7.90 -7 6 -9 79.59 13.40 7 -6 9 65.09 11.70 -8 6 -9 5.30 11.10 8 -6 9 12.60 9.60 15 5 -9 13.00 8.80 14 5 -9 21.50 9.80 14 5 -9 0.60 7.90 13 5 -9 7.80 7.30 13 5 -9 0.60 9.00 -13 -5 9 0.80 5.60 12 5 -9 52.29 10.20 12 5 -9 69.59 8.90 -12 -5 9 36.00 8.30 11 5 -9 -9.10 7.10 11 5 -9 7.90 6.10 -11 -5 9 -1.10 4.90 10 5 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310.47 19.20 -1 5 -9 301.57 16.70 1 -5 9 266.97 18.70 1 -5 9 308.77 17.90 1 -5 9 264.97 17.90 -2 5 -9 119.49 8.40 -2 5 -9 123.09 12.30 2 -5 9 117.19 11.90 2 -5 9 118.39 10.60 2 -5 9 101.49 10.20 -3 5 -9 272.67 18.70 -3 5 -9 233.98 13.70 3 -5 9 220.98 16.50 3 -5 9 229.78 16.90 3 -5 9 273.87 18.00 -4 5 -9 259.97 18.90 -4 5 -9 204.88 11.70 4 -5 9 215.88 17.00 -5 5 -9 13.50 8.60 5 -5 9 6.90 7.50 -6 5 -9 22.90 10.30 6 -5 9 16.60 8.00 -7 5 -9 5.70 9.40 7 -5 9 0.90 8.40 -8 5 -9 3.40 10.30 8 -5 9 8.70 8.60 -9 5 -9 5.90 11.10 9 -5 9 14.00 9.30 15 4 -9 -1.20 10.00 15 4 -9 7.80 8.80 14 4 -9 0.90 7.90 14 4 -9 17.70 9.90 13 4 -9 2.10 7.10 13 4 -9 -6.30 8.70 -13 -4 9 7.30 5.50 12 4 -9 -6.80 8.30 12 4 -9 0.40 6.40 -12 -4 9 -1.80 6.20 11 4 -9 107.19 11.50 -11 -4 9 104.49 10.50 10 4 -9 38.00 8.70 10 4 -9 23.90 6.20 10 4 -9 36.10 8.30 10 4 -9 52.69 7.20 -10 -4 9 47.20 6.40 9 4 -9 576.34 32.80 9 4 -9 569.04 31.00 9 4 -9 519.55 31.30 -9 -4 9 606.14 30.80 8 4 -9 26.60 5.60 8 4 -9 14.90 6.60 8 4 -9 29.60 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77.39 8.80 -11 -6 11 82.79 8.20 10 6 -11 27.80 7.90 10 6 -11 18.80 6.00 10 6 -11 22.90 8.60 -10 -6 11 25.00 5.40 9 6 -11 193.08 16.10 9 6 -11 180.18 13.20 -9 -6 11 176.18 12.40 8 6 -11 14.30 7.20 8 6 -11 15.80 5.30 -8 -6 11 20.40 4.80 -8 -6 11 15.30 6.60 7 6 -11 57.69 7.40 7 6 -11 57.19 8.70 7 6 -11 44.30 7.30 -7 -6 11 49.80 8.30 -7 -6 11 50.79 6.20 6 6 -11 3.00 5.00 6 6 -11 3.10 5.90 -6 -6 11 4.10 4.30 -6 -6 11 3.30 5.60 5 6 -11 4.80 4.30 5 6 -11 4.10 6.10 -5 -6 11 8.10 5.60 -5 -6 11 7.80 4.70 4 6 -11 2.90 4.50 4 6 -11 -1.70 5.80 -4 -6 11 -2.90 4.30 -4 -6 11 6.00 5.60 3 6 -11 2379.26 125.39 3 6 -11 2415.66 124.49 -3 -6 11 2488.15 124.09 -3 -6 11 2590.84 125.49 -3 -6 11 2409.56 124.59 2 6 -11 130.69 12.60 2 6 -11 134.49 10.70 -2 -6 11 116.09 10.60 -2 -6 11 127.99 12.40 1 6 -11 145.99 13.10 1 6 -11 119.49 10.40 -1 -6 11 123.49 11.10 -1 -6 11 151.68 12.80 -1 -6 11 131.39 11.30 0 6 -11 871.01 47.10 0 6 -11 881.81 45.10 0 -6 11 827.32 45.50 0 -6 11 847.82 46.00 -1 6 -11 342.07 23.20 -1 6 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305.77 17.50 -7 -5 11 299.97 19.90 6 5 -11 7.20 6.30 6 5 -11 13.40 4.00 -6 -5 11 20.00 4.20 -6 -5 11 8.90 5.80 5 5 -11 120.89 11.70 5 5 -11 106.69 10.30 5 5 -11 125.39 8.80 -5 -5 11 106.19 9.00 -5 -5 11 128.79 11.20 4 5 -11 -1.80 4.20 4 5 -11 7.20 6.00 -4 -5 11 5.30 6.40 -4 -5 11 7.00 5.20 3 5 -11 1422.06 77.49 3 5 -11 1537.65 78.89 -3 -5 11 1467.75 77.79 -3 -5 11 1620.34 78.69 -3 -5 11 1540.25 77.59 2 5 -11 83.99 9.80 2 5 -11 92.69 8.80 -2 -5 11 95.69 10.10 -2 -5 11 76.19 8.50 -2 -5 11 82.79 8.10 1 5 -11 257.57 17.70 -1 -5 11 259.57 17.60 -1 -5 11 258.47 15.70 0 5 -11 -3.30 5.50 0 5 -11 8.10 3.70 0 -5 11 0.50 5.80 0 -5 11 3.20 4.50 0 -5 11 1.80 4.50 -1 5 -11 337.07 18.30 -1 5 -11 325.17 21.10 1 -5 11 315.37 22.30 1 -5 11 300.67 19.10 1 -5 11 296.87 19.40 -2 5 -11 13.90 4.10 -2 5 -11 16.90 7.70 2 -5 11 9.30 5.80 2 -5 11 15.70 6.60 2 -5 11 5.50 7.30 -3 5 -11 82.79 7.20 -3 5 -11 77.89 11.00 3 -5 11 88.49 9.80 3 -5 11 93.39 10.10 -4 5 -11 67.19 5.30 -4 5 -11 55.39 10.80 4 -5 11 68.89 10.00 -5 5 -11 79.39 12.30 5 -5 11 66.99 10.10 -6 5 -11 -0.90 9.40 6 -5 11 -0.20 8.10 -7 5 -11 41.30 12.00 7 -5 11 30.90 10.00 -8 5 -11 9.90 10.80 8 -5 11 -9.40 8.50 15 4 -11 2.70 8.30 15 4 -11 -0.40 10.70 14 4 -11 -0.10 7.60 14 4 -11 -9.00 9.80 13 4 -11 -5.70 6.60 13 4 -11 -10.40 8.50 -13 -4 11 4.30 5.10 12 4 -11 26.20 7.10 12 4 -11 18.40 9.20 -12 -4 11 23.10 5.70 11 4 -11 25.80 9.00 11 4 -11 26.80 6.60 -11 -4 11 22.60 5.50 10 4 -11 37.90 9.30 10 4 -11 18.00 5.90 -10 -4 11 29.80 5.40 9 4 -11 349.96 21.00 9 4 -11 347.77 23.80 9 4 -11 370.06 22.50 9 4 -11 387.16 24.20 -9 -4 11 385.46 20.70 8 4 -11 122.09 11.30 8 4 -11 114.49 9.30 8 4 -11 128.49 13.10 -8 -4 11 118.79 8.90 7 4 -11 214.48 14.50 7 4 -11 208.28 15.70 7 4 -11 183.28 12.50 -7 -4 11 191.08 15.20 -7 -4 11 235.18 12.50 6 4 -11 281.77 18.10 6 4 -11 301.87 16.60 6 4 -11 321.57 19.70 -6 -4 11 283.07 16.30 -6 -4 11 309.77 19.10 5 4 -11 274.77 15.40 5 4 -11 257.57 16.90 5 4 -11 274.27 18.40 -5 -4 11 286.67 18.00 -5 -4 11 291.37 15.60 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11 30.50 9.30 -9 -12 -11 -5.00 7.90 9 12 11 6.00 8.30 -10 -12 -11 32.80 8.70 10 12 11 23.80 9.70 -11 -12 -11 61.89 10.40 11 12 11 70.69 12.10 -12 -12 -11 34.30 8.90 12 12 11 18.10 10.60 -13 -12 -11 2.50 7.90 13 12 11 3.20 10.40 13 12 11 10.00 4.20 13 12 11 3.00 3.50 -14 -12 -11 5.70 8.10 14 12 11 15.40 10.50 2 -13 -11 -10.00 8.50 2 -13 -11 -5.70 9.00 2 -13 -11 0.10 9.30 1 -13 -11 0.80 8.60 1 -13 -11 12.50 9.00 1 -13 -11 11.00 10.10 0 -13 -11 -1.70 7.10 0 -13 -11 4.50 5.80 0 -13 -11 10.00 9.10 0 -13 -11 -2.60 8.40 -1 -13 -11 27.00 6.40 -1 -13 -11 17.00 6.60 -1 -13 -11 23.60 9.50 -2 -13 -11 13.10 5.30 -2 -13 -11 -3.00 4.80 -2 -13 -11 -2.30 8.10 2 13 11 -0.50 7.80 -3 -13 -11 14.90 4.30 -3 -13 -11 1.30 4.50 -3 -13 -11 21.60 9.10 3 13 11 6.10 8.10 -4 -13 -11 4.00 8.00 4 13 11 0.70 8.20 -5 -13 -11 18.20 8.50 5 13 11 14.20 9.00 -6 -13 -11 8.20 8.80 6 13 11 21.10 9.40 -7 -13 -11 64.49 10.80 7 13 11 75.79 11.90 -8 -13 -11 9.70 9.00 8 13 11 18.10 9.50 -9 -13 -11 11.20 8.70 9 13 11 13.90 9.50 -10 -13 -11 2.10 8.10 10 13 11 17.40 9.90 -11 -13 -11 3.40 8.30 11 13 11 3.40 9.10 -12 -13 -11 0.80 8.00 12 13 11 15.90 11.30 13 13 11 31.70 10.80 -14 -13 -11 -9.80 8.30 0 -14 -11 8.50 14.90 0 -14 -11 17.70 9.80 0 -14 -11 13.90 8.50 -1 -14 -11 5.20 9.30 -1 -14 -11 -14.90 13.90 -1 -14 -11 10.40 6.60 -2 -14 -11 18.50 5.90 -2 -14 -11 20.10 9.50 -2 -14 -11 43.50 7.20 2 14 11 19.80 9.60 -3 -14 -11 10.70 8.70 -3 -14 -11 9.90 4.00 -3 -14 -11 10.40 4.60 3 14 11 -1.80 9.50 -4 -14 -11 -10.90 7.90 4 14 11 0.80 8.80 -5 -14 -11 7.20 9.00 5 14 11 14.00 9.40 -6 -14 -11 -4.40 8.90 6 14 11 -6.50 8.80 -7 -14 -11 22.10 9.10 7 14 11 70.29 12.00 -8 -14 -11 20.10 9.60 8 14 11 32.30 10.40 -9 -14 -11 0.10 8.50 9 14 11 20.00 10.10 -11 -14 -11 10.70 9.20 11 14 11 18.00 11.00 -12 -14 -11 64.59 11.40 12 14 11 86.99 13.80 -13 -14 -11 8.00 9.50 -2 -15 -11 58.79 11.60 -3 -15 -11 -3.90 9.20 3 15 11 -4.70 10.20 -4 -15 -11 -6.90 8.90 4 15 11 2.00 10.00 -5 -15 -11 10.40 9.30 5 15 11 26.80 10.90 -6 -15 -11 -12.90 9.30 6 15 11 1.30 10.80 -7 -15 -11 5.00 9.60 7 15 11 22.30 12.40 -8 -15 -11 15.60 9.20 8 15 11 18.70 10.50 -9 -15 -11 33.50 10.30 9 15 11 70.89 13.90 -10 -15 -11 -6.10 9.10 10 15 11 28.70 11.70 -11 -15 -11 26.40 10.20 11 15 11 42.70 11.90 5 16 11 4.90 15.30 6 16 11 3.10 10.80 7 16 11 19.00 11.00 8 16 11 -1.40 11.20 11 13 -12 -1.00 8.60 11 13 -12 10.90 7.10 10 13 -12 -4.50 8.70 10 13 -12 15.90 7.00 9 13 -12 28.70 7.40 9 13 -12 27.40 9.80 8 13 -12 42.80 8.60 7 13 -12 15.80 7.10 -7 -13 12 -3.60 9.30 6 13 -12 20.40 8.10 -6 -13 12 23.80 9.80 5 13 -12 1.20 7.30 -5 -13 12 1.00 8.90 4 13 -12 6.90 8.40 -4 -13 12 -4.30 9.20 3 13 -12 50.59 10.90 -3 -13 12 42.60 11.00 12 12 -12 1.30 7.80 12 12 -12 -14.70 6.90 11 12 -12 15.60 8.00 11 12 -12 25.40 8.20 11 12 -12 37.40 7.40 10 12 -12 9.20 8.30 10 12 -12 0.60 7.00 -10 -12 12 5.30 6.20 9 12 -12 0.90 8.10 9 12 -12 3.90 7.40 -9 -12 12 4.10 6.20 8 12 -12 132.09 13.60 8 12 -12 146.49 14.70 -8 -12 12 113.59 12.30 7 12 -12 4.60 7.20 -7 -12 12 -6.70 6.40 6 12 -12 166.78 15.50 -6 -12 12 129.69 14.00 -6 -12 12 125.89 13.70 5 12 -12 17.60 8.10 -5 -12 12 20.60 8.50 4 12 -12 -3.90 7.70 -4 -12 12 8.20 8.60 3 12 -12 6.30 8.30 -3 -12 12 -5.50 8.50 2 12 -12 18.00 9.20 1 12 -12 56.89 12.00 -1 -12 12 82.09 13.10 13 11 -12 6.40 8.40 13 11 -12 -0.60 7.50 12 11 -12 28.30 8.20 11 11 -12 13.50 8.10 11 11 -12 11.50 7.50 11 11 -12 24.00 7.10 10 11 -12 -1.40 6.80 10 11 -12 7.50 7.50 -10 -11 12 6.30 6.30 9 11 -12 34.30 8.10 9 11 -12 10.90 7.00 -9 -11 12 2.90 6.40 8 11 -12 10.50 7.80 8 11 -12 10.10 7.10 -8 -11 12 -3.00 6.40 7 11 -12 106.59 12.00 7 11 -12 137.89 14.40 -7 -11 12 97.19 11.30 6 11 -12 199.28 16.30 -6 -11 12 142.39 14.70 -6 -11 12 207.78 17.00 5 11 -12 68.09 10.00 -5 -11 12 61.39 9.30 -5 -11 12 49.50 9.50 4 11 -12 39.70 9.20 -4 -11 12 42.10 9.50 3 11 -12 164.28 16.90 -3 -11 12 153.18 16.00 2 11 -12 40.80 10.20 -2 -11 12 52.99 10.70 1 11 -12 31.10 9.90 -1 -11 12 8.90 9.10 0 11 -12 2.80 9.30 0 -11 12 -5.70 17.20 -1 11 -12 9.10 9.80 1 -11 12 -0.50 8.90 14 10 -12 20.60 8.30 14 10 -12 2.40 8.80 13 10 -12 7.10 7.50 13 10 -12 1.20 8.30 12 10 -12 5.10 7.90 11 10 -12 25.10 7.60 11 10 -12 30.50 9.10 10 10 -12 12.70 6.70 10 10 -12 -1.10 7.20 -10 -10 12 5.30 6.00 -10 -10 12 2.70 6.70 9 10 -12 -2.20 6.10 9 10 -12 -5.80 6.70 -9 -10 12 -3.20 5.90 -9 -10 12 -1.10 6.20 8 10 -12 55.79 8.70 8 10 -12 67.49 10.00 -8 -10 12 70.59 9.40 -8 -10 12 59.39 9.30 7 10 -12 14.00 7.50 7 10 -12 23.90 7.50 -7 -10 12 3.70 6.50 -7 -10 12 20.70 7.70 6 10 -12 9.30 7.00 -6 -10 12 -0.60 6.10 5 10 -12 39.20 8.40 -5 -10 12 19.10 6.80 4 10 -12 10.40 7.40 -4 -10 12 11.90 6.90 -4 -10 12 6.40 6.70 3 10 -12 48.00 9.30 -3 -10 12 35.20 8.30 2 10 -12 12.90 8.60 -2 -10 12 16.70 8.00 1 10 -12 40.10 10.10 1 10 -12 55.59 7.90 -1 -10 12 66.89 10.90 0 10 -12 21.60 6.00 0 10 -12 34.70 10.20 0 -10 12 21.80 9.10 -1 10 -12 57.09 11.50 -1 10 -12 27.30 6.90 1 -10 12 29.50 9.80 -2 10 -12 10.50 9.80 2 -10 12 -3.50 8.40 -3 10 -12 6.40 10.50 3 -10 12 -2.70 9.70 14 9 -12 9.80 8.90 14 9 -12 14.90 7.90 13 9 -12 -0.60 7.00 13 9 -12 0.30 8.50 12 9 -12 13.10 8.60 12 9 -12 16.40 7.40 -12 -9 12 19.50 6.40 11 9 -12 5.40 6.50 11 9 -12 -4.90 7.40 -11 -9 12 -2.10 5.20 10 9 -12 61.19 8.40 10 9 -12 67.89 10.10 -10 -9 12 38.80 7.20 9 9 -12 -3.10 5.80 9 9 -12 14.30 8.00 -9 -9 12 1.20 6.30 8 9 -12 57.09 8.20 8 9 -12 52.29 10.00 -8 -9 12 84.99 10.10 7 9 -12 273.47 19.30 7 9 -12 250.17 18.00 -7 -9 12 227.88 24.70 6 9 -12 77.09 10.80 6 9 -12 91.99 9.70 -6 -9 12 113.09 11.20 5 9 -12 19.20 7.60 -5 -9 12 8.30 6.90 -5 -9 12 13.40 6.80 4 9 -12 12.80 7.40 -4 -9 12 7.80 6.40 -4 -9 12 17.70 6.80 -4 -9 12 12.20 6.70 3 9 -12 -0.30 7.00 3 9 -12 2.60 6.30 -3 -9 12 1.90 7.00 -3 -9 12 -2.80 6.20 2 9 -12 12.30 7.90 2 9 -12 5.40 4.90 -2 -9 12 15.00 8.20 -2 -9 12 7.70 7.10 1 9 -12 -4.70 8.80 1 9 -12 -5.70 5.00 -1 -9 12 -5.80 6.50 0 9 -12 90.29 10.20 0 9 -12 106.09 13.10 0 -9 12 96.79 11.40 -1 9 -12 67.79 12.10 -1 9 -12 59.39 7.30 1 -9 12 84.49 10.80 -2 9 -12 19.70 4.80 -2 9 -12 33.50 10.70 2 -9 12 36.80 9.50 -3 9 -12 6.90 10.00 -3 9 -12 13.60 4.00 -4 9 -12 29.80 11.90 4 -9 12 36.40 11.60 14 8 -12 10.70 9.30 13 8 -12 1.10 8.20 13 8 -12 3.70 6.70 -13 -8 12 -15.10 5.10 12 8 -12 4.90 8.10 -12 -8 12 -6.60 5.20 11 8 -12 19.40 6.80 -11 -8 12 16.30 5.70 10 8 -12 12.90 8.30 10 8 -12 12.70 6.10 -10 -8 12 11.10 5.10 9 8 -12 1.20 7.40 9 8 -12 5.40 5.70 -9 -8 12 3.60 4.90 -9 -8 12 0.30 6.10 8 8 -12 97.69 10.40 8 8 -12 95.19 11.60 -8 -8 12 70.69 8.60 -8 -8 12 92.09 12.00 7 8 -12 2166.98 107.49 7 8 -12 2203.28 108.99 -7 -8 12 2014.00 107.59 -7 -8 12 2051.09 108.59 6 8 -12 338.57 20.50 6 8 -12 345.07 22.50 -6 -8 12 314.27 20.70 -6 -8 12 317.07 21.60 5 8 -12 4.50 6.90 -5 -8 12 3.20 5.90 -5 -8 12 18.50 6.70 4 8 -12 4.10 6.00 4 8 -12 -0.80 6.70 -4 -8 12 -4.30 5.70 -4 -8 12 7.60 6.90 3 8 -12 -5.50 5.30 3 8 -12 5.20 6.90 -3 -8 12 1.80 6.10 -3 -8 12 7.10 6.00 -3 -8 12 2.10 6.20 2 8 -12 68.89 9.80 -2 -8 12 62.79 8.90 -2 -8 12 68.59 9.60 -2 -8 12 63.79 8.60 1 8 -12 81.29 10.80 1 8 -12 44.40 7.10 -1 -8 12 60.29 8.80 -1 -8 12 59.19 10.20 0 8 -12 6.50 4.80 0 -8 12 16.20 7.30 -1 8 -12 81.29 12.10 -1 8 -12 64.89 7.10 1 -8 12 72.79 10.00 -2 8 -12 24.60 9.60 -2 8 -12 17.50 4.60 2 -8 12 7.90 8.10 -3 8 -12 67.49 12.30 -3 8 -12 43.90 7.50 3 -8 12 50.69 10.70 -4 8 -12 37.10 11.60 4 -8 12 30.40 10.70 -5 8 -12 4.10 10.30 5 -8 12 -1.10 9.90 15 7 -12 6.80 7.60 14 7 -12 -4.80 8.50 14 7 -12 7.10 7.20 13 7 -12 -4.30 6.30 13 7 -12 -4.20 8.40 -13 -7 12 1.50 5.30 12 7 -12 53.19 10.60 12 7 -12 53.39 8.30 -12 -7 12 59.09 7.60 11 7 -12 -7.20 5.40 11 7 -12 -4.20 7.40 -11 -7 12 -8.90 4.50 10 7 -12 -1.30 7.40 10 7 -12 -0.70 5.30 10 7 -12 6.30 6.30 -10 -7 12 -3.20 4.50 9 7 -12 5.50 7.80 9 7 -12 20.40 5.80 -9 -7 12 20.30 5.30 -9 -7 12 27.10 7.30 8 7 -12 19.20 5.50 8 7 -12 14.80 7.60 -8 -7 12 9.50 7.50 -8 -7 12 13.30 5.10 7 7 -12 294.77 20.20 7 7 -12 272.07 17.20 -7 -7 12 283.87 19.40 -7 -7 12 262.07 17.20 6 7 -12 37.40 8.30 6 7 -12 44.90 11.20 6 7 -12 28.70 5.90 -6 -7 12 22.10 6.00 -6 -7 12 27.60 7.10 5 7 -12 31.40 6.80 5 7 -12 33.80 8.10 -5 -7 12 36.10 6.70 -5 -7 12 42.70 7.80 4 7 -12 10.70 5.60 4 7 -12 3.70 6.90 -4 -7 12 3.10 5.90 -4 -7 12 9.90 5.30 -4 -7 12 13.10 5.60 3 7 -12 71.99 9.90 -3 -7 12 65.19 7.70 -3 -7 12 50.59 6.70 -3 -7 12 58.69 8.50 2 7 -12 -7.60 6.30 2 7 -12 -2.20 4.50 -2 -7 12 1.80 5.20 -2 -7 12 -10.60 5.00 1 7 -12 43.60 6.40 1 7 -12 50.99 9.40 -1 -7 12 43.00 7.70 -1 -7 12 36.50 8.50 -1 -7 12 42.30 7.50 0 7 -12 56.59 7.00 0 7 -12 72.99 10.60 0 -7 12 65.49 8.90 0 -7 12 77.29 9.30 0 -7 12 57.79 9.90 -1 7 -12 3.40 4.10 -2 7 -12 0.20 8.20 -2 7 -12 0.90 3.70 2 -7 12 -11.50 6.60 -3 7 -12 16.20 9.30 -3 7 -12 6.00 5.60 3 -7 12 18.80 8.50 -4 7 -12 -14.70 8.90 4 -7 12 -1.60 8.30 -5 7 -12 10.50 10.40 5 -7 12 12.00 9.30 -6 7 -12 35.00 12.00 6 -7 12 14.20 10.10 15 6 -12 2.40 10.30 15 6 -12 13.10 7.90 14 6 -12 4.60 9.40 14 6 -12 0.50 6.90 -14 -6 12 -2.90 5.40 13 6 -12 6.00 9.00 13 6 -12 15.00 6.90 -13 -6 12 7.00 5.60 12 6 -12 11.20 9.00 12 6 -12 41.70 7.30 -12 -6 12 34.40 6.30 11 6 -12 54.49 7.60 11 6 -12 56.89 10.50 -11 -6 12 57.39 7.00 10 6 -12 35.30 9.10 10 6 -12 25.30 6.00 -10 -6 12 16.90 5.00 9 6 -12 167.68 12.60 9 6 -12 184.98 16.20 -9 -6 12 163.58 11.80 -9 -6 12 190.58 15.30 8 6 -12 68.79 7.30 8 6 -12 61.59 9.70 -8 -6 12 53.19 9.10 -8 -6 12 60.69 6.50 7 6 -12 104.29 11.60 7 6 -12 121.99 11.50 -7 -6 12 110.99 9.50 -7 -6 12 130.09 12.50 6 6 -12 16.70 5.80 6 6 -12 7.50 6.50 -6 -6 12 14.50 6.50 -6 -6 12 21.20 5.00 5 6 -12 74.79 8.20 5 6 -12 90.29 10.10 5 6 -12 82.09 8.20 -5 -6 12 70.09 9.00 -5 -6 12 82.59 8.70 4 6 -12 24.90 7.40 4 6 -12 18.40 6.50 -4 -6 12 30.20 5.60 -4 -6 12 37.10 7.10 -4 -6 12 37.00 5.70 3 6 -12 2.90 6.30 3 6 -12 1.90 4.80 -3 -6 12 1.30 4.80 -3 -6 12 6.20 4.50 -3 -6 12 6.10 5.70 2 6 -12 44.80 6.00 2 6 -12 43.90 8.40 -2 -6 12 28.30 7.00 -2 -6 12 35.00 6.00 -2 -6 12 22.00 4.80 1 6 -12 368.76 22.20 1 6 -12 405.96 24.60 -1 -6 12 402.56 22.60 -1 -6 12 373.56 25.50 -1 -6 12 367.56 22.80 0 6 -12 370.86 24.40 0 6 -12 343.47 21.50 0 -6 12 376.16 24.10 0 -6 12 392.46 22.60 0 -6 12 374.76 24.20 -1 6 -12 -1.60 3.80 -1 6 -12 -4.60 6.60 1 -6 12 2.50 6.20 1 -6 12 3.50 7.60 1 -6 12 7.00 5.80 -2 6 -12 15.20 4.10 2 -6 12 24.90 7.50 -3 6 -12 51.99 5.30 -3 6 -12 57.69 10.60 3 -6 12 72.29 10.30 -4 6 -12 65.89 12.00 -4 6 -12 49.30 5.00 4 -6 12 58.39 10.30 -5 6 -12 -1.60 9.30 5 -6 12 4.20 8.10 -6 6 -12 15.00 10.60 6 -6 12 6.00 9.40 -7 6 -12 4.90 11.00 7 -6 12 15.30 10.20 15 5 -12 14.40 8.00 15 5 -12 20.20 11.10 14 5 -12 18.10 7.90 14 5 -12 14.60 10.90 -14 -5 12 9.60 5.70 13 5 -12 4.20 6.70 13 5 -12 -5.10 9.10 12 5 -12 31.10 7.00 12 5 -12 19.50 9.20 -12 -5 12 19.90 5.50 11 5 -12 22.00 8.70 11 5 -12 31.50 6.30 -11 -5 12 20.30 5.30 10 5 -12 37.80 6.10 10 5 -12 44.40 9.30 -10 -5 12 30.10 5.40 9 5 -12 66.19 10.00 9 5 -12 79.09 7.80 -9 -5 12 87.89 7.90 8 5 -12 614.54 32.20 8 5 -12 590.44 34.80 -8 -5 12 605.24 34.70 7 5 -12 463.05 26.30 7 5 -12 430.26 24.60 7 5 -12 446.16 27.70 -7 -5 12 458.15 24.50 -7 -5 12 482.45 27.30 6 5 -12 11.90 5.30 6 5 -12 23.20 7.80 6 5 -12 18.30 4.10 -6 -5 12 25.90 6.70 -6 -5 12 17.90 4.30 5 5 -12 215.38 13.40 5 5 -12 230.08 16.70 -5 -5 12 225.08 16.10 -5 -5 12 228.18 13.90 4 5 -12 28.20 5.60 4 5 -12 29.10 7.70 -4 -5 12 43.90 7.40 -4 -5 12 33.40 4.90 3 5 -12 23.20 6.90 3 5 -12 28.80 5.50 -3 -5 12 29.90 6.90 -3 -5 12 24.00 5.00 2 5 -12 392.16 25.10 2 5 -12 418.16 23.40 -2 -5 12 438.86 25.10 -2 -5 12 396.46 23.40 -2 -5 12 420.46 23.00 1 5 -12 59.29 8.40 -1 -5 12 42.20 7.50 -1 -5 12 39.40 5.90 -1 -5 12 26.70 4.30 0 5 -12 24.40 4.80 0 5 -12 25.20 7.70 0 -5 12 19.00 7.20 0 -5 12 31.60 5.90 0 -5 12 23.40 5.70 -1 5 -12 183.18 15.20 -1 5 -12 168.28 11.40 1 -5 12 135.59 12.50 1 -5 12 163.58 14.90 1 -5 12 157.58 12.70 -2 5 -12 152.98 10.50 -2 5 -12 146.59 15.00 2 -5 12 152.68 12.50 2 -5 12 137.09 13.10 2 -5 12 133.89 14.70 -3 5 -12 22.30 3.70 3 -5 12 30.80 8.00 -4 5 -12 -1.20 8.10 -4 5 -12 -0.90 2.40 4 -5 12 3.20 7.60 -5 5 -12 13.00 9.10 5 -5 12 0.70 7.80 -6 5 -12 20.80 9.90 6 -5 12 11.30 8.50 -7 5 -12 6.60 10.00 7 -5 12 2.70 8.40 -8 5 -12 11.20 10.70 8 -5 12 4.80 9.80 14 4 -12 19.00 7.80 14 4 -12 3.90 17.00 -14 -4 12 19.00 6.10 13 4 -12 -11.70 8.60 13 4 -12 6.00 6.70 12 4 -12 32.40 7.10 12 4 -12 18.30 9.30 -12 -4 12 24.10 5.30 11 4 -12 11.90 5.70 11 4 -12 16.40 9.20 -11 -4 12 11.80 4.60 10 4 -12 101.09 9.80 10 4 -12 117.89 14.20 -10 -4 12 101.69 9.20 9 4 -12 51.29 9.70 9 4 -12 52.49 9.50 9 4 -12 47.00 6.00 8 4 -12 9.50 7.30 8 4 -12 2.00 5.20 8 4 -12 6.00 4.00 -8 -4 12 6.50 6.70 -8 -4 12 11.20 3.70 7 4 -12 16.20 7.20 7 4 -12 20.30 5.50 7 4 -12 9.80 3.60 -7 -4 12 11.90 6.60 -7 -4 12 7.90 3.30 6 4 -12 271.47 15.20 6 4 -12 289.97 19.10 -6 -4 12 264.17 15.10 -6 -4 12 274.87 18.40 5 4 -12 140.99 8.90 5 4 -12 140.89 11.00 5 4 -12 132.19 12.90 -5 -4 12 130.89 9.00 -5 -4 12 136.09 12.20 4 4 -12 1724.43 96.09 4 4 -12 2019.50 95.19 -4 -4 12 1930.71 94.09 -4 -4 12 1714.93 95.89 -4 -4 12 1939.91 94.39 3 4 -12 103.39 11.80 3 4 -12 99.39 9.20 -3 -4 12 111.19 10.80 -3 -4 12 105.89 8.50 -3 -4 12 122.39 8.00 2 4 -12 293.47 20.00 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39.20 9.30 -5 -9 13 47.90 8.30 -5 -9 13 48.40 8.40 -5 -9 13 51.89 8.80 4 9 -13 82.19 11.10 -4 -9 13 70.79 10.00 -4 -9 13 74.09 9.30 3 9 -13 33.60 9.00 -3 -9 13 41.10 12.50 2 9 -13 1.70 5.60 -2 -9 13 -3.20 6.70 1 9 -13 -2.80 5.00 1 9 -13 -1.90 8.10 -1 -9 13 0.30 7.20 0 9 -13 58.09 7.70 0 9 -13 72.29 11.50 0 -9 13 52.69 9.80 -1 9 -13 23.40 9.90 -1 9 -13 13.30 5.20 1 -9 13 11.50 9.10 -2 9 -13 59.39 12.40 -2 9 -13 50.09 6.30 2 -9 13 44.80 10.80 -3 9 -13 31.50 11.70 3 -9 13 12.60 10.50 -4 9 -13 3.40 10.80 4 -9 13 18.10 12.40 14 8 -13 3.80 9.00 14 8 -13 1.80 7.00 13 8 -13 11.40 6.80 13 8 -13 -4.80 8.70 -13 -8 13 -7.90 5.30 12 8 -13 5.50 6.20 12 8 -13 -6.40 8.30 11 8 -13 14.70 6.40 11 8 -13 10.10 8.90 -11 -8 13 2.60 5.10 10 8 -13 23.80 8.90 10 8 -13 19.60 6.30 -10 -8 13 17.00 5.50 9 8 -13 40.30 6.90 9 8 -13 48.50 9.70 -9 -8 13 40.60 8.80 -9 -8 13 41.20 6.50 8 8 -13 137.79 13.80 8 8 -13 126.29 11.20 -8 -8 13 101.59 11.80 7 8 -13 657.83 36.30 7 8 -13 646.04 38.30 -7 -8 13 673.53 36.50 -7 -8 13 676.43 38.00 6 8 -13 27.20 8.40 -6 -8 13 20.50 6.80 -6 -8 13 18.50 7.50 5 8 -13 -2.00 7.30 -5 -8 13 3.60 6.50 -5 -8 13 6.40 5.90 -5 -8 13 7.60 6.20 4 8 -13 42.30 9.00 -4 -8 13 44.90 7.10 -4 -8 13 29.40 7.60 -4 -8 13 35.90 9.00 3 8 -13 90.29 11.30 3 8 -13 67.99 8.60 -3 -8 13 92.59 9.60 -3 -8 13 82.79 10.60 2 8 -13 134.69 13.20 -2 -8 13 84.49 11.00 -2 -8 13 102.69 10.70 -2 -8 13 84.89 10.30 1 8 -13 49.99 11.20 1 8 -13 29.60 7.20 -1 -8 13 23.50 13.20 0 8 -13 142.69 15.00 0 8 -13 129.99 11.80 0 -8 13 137.49 14.30 -1 8 -13 93.59 10.00 -1 8 -13 105.19 13.30 1 -8 13 110.89 12.10 -2 8 -13 58.09 11.80 -2 8 -13 37.30 5.60 2 -8 13 32.80 9.40 -3 8 -13 29.70 4.60 -3 8 -13 32.20 10.70 3 -8 13 36.40 10.10 -4 8 -13 19.60 11.30 4 -8 13 21.40 12.50 -5 8 -13 9.40 10.90 5 -8 13 -14.50 9.00 14 7 -13 13.80 7.00 14 7 -13 18.40 10.20 13 7 -13 6.40 6.40 13 7 -13 -6.90 8.30 -13 -7 13 0.70 5.60 12 7 -13 -2.70 8.70 12 7 -13 6.20 6.10 -12 -7 13 -7.80 4.90 11 7 -13 3.20 5.60 11 7 -13 -2.10 8.40 -11 -7 13 -0.70 4.60 10 7 -13 -8.20 8.30 10 7 -13 3.30 5.30 -10 -7 13 -1.60 4.50 9 7 -13 136.39 11.30 9 7 -13 116.29 13.30 -9 -7 13 147.29 10.90 -9 -7 13 132.29 13.60 8 7 -13 60.49 9.80 8 7 -13 45.50 6.70 -8 -7 13 50.99 6.70 -8 -7 13 72.19 9.80 7 7 -13 -5.30 4.60 7 7 -13 5.40 7.60 -7 -7 13 9.30 6.90 -7 -7 13 6.40 4.90 6 7 -13 72.79 7.80 6 7 -13 70.79 10.20 -6 -7 13 85.99 8.50 5 7 -13 158.88 15.10 5 7 -13 164.88 15.10 -5 -7 13 156.08 12.10 -5 -7 13 147.19 12.50 4 7 -13 217.58 17.20 4 7 -13 190.48 15.30 -4 -7 13 209.08 14.30 -4 -7 13 203.68 14.90 3 7 -13 82.89 10.60 3 7 -13 87.99 9.30 -3 -7 13 92.99 10.10 -3 -7 13 93.79 10.40 -3 -7 13 100.79 9.90 2 7 -13 -4.00 7.10 -2 -7 13 2.50 5.60 -2 -7 13 -1.80 6.40 1 7 -13 -3.30 4.80 1 7 -13 8.20 7.40 -1 -7 13 2.30 5.70 -1 -7 13 4.80 6.10 -1 -7 13 6.80 7.40 0 7 -13 53.59 10.60 0 7 -13 54.49 6.80 0 -7 13 64.29 10.00 0 -7 13 52.79 8.40 -1 7 -13 91.39 9.60 -1 7 -13 88.39 12.30 1 -7 13 109.59 11.30 -2 7 -13 2.80 8.30 -2 7 -13 1.20 3.90 2 -7 13 1.50 7.10 -3 7 -13 10.50 10.00 3 -7 13 14.70 8.50 -4 7 -13 -2.80 9.50 4 -7 13 10.70 9.50 -5 7 -13 7.90 10.90 -6 7 -13 14.00 11.30 6 -7 13 -4.10 9.80 14 6 -13 2.20 9.90 14 6 -13 8.90 6.70 13 6 -13 21.40 9.90 13 6 -13 24.40 6.90 -13 -6 13 16.90 5.70 12 6 -13 7.60 5.80 12 6 -13 -0.70 9.10 -12 -6 13 11.20 5.10 11 6 -13 46.10 10.50 11 6 -13 56.19 7.30 -11 -6 13 55.89 6.70 10 6 -13 53.49 6.90 -10 -6 13 47.80 6.00 9 6 -13 277.37 16.90 9 6 -13 273.57 20.50 -9 -6 13 253.87 19.70 -9 -6 13 281.77 16.40 8 6 -13 17.70 8.00 -8 -6 13 19.70 4.60 -8 -6 13 17.10 7.50 7 6 -13 256.17 19.80 7 6 -13 271.47 16.80 -7 -6 13 265.97 19.00 -7 -6 13 252.17 15.80 6 6 -13 29.30 8.00 6 6 -13 3.30 5.50 -6 -6 13 12.10 7.00 -6 -6 13 11.90 4.70 5 6 -13 140.79 14.60 5 6 -13 153.88 12.90 -5 -6 13 164.48 11.70 -5 -6 13 150.98 13.60 4 6 -13 17.30 5.50 4 6 -13 13.00 7.40 -4 -6 13 19.40 6.30 -4 -6 13 26.50 5.40 -4 -6 13 20.00 5.00 3 6 -13 34.60 8.00 3 6 -13 26.50 6.70 -3 -6 13 42.90 7.60 -3 -6 13 42.40 6.60 -3 -6 13 41.10 6.10 2 6 -13 30.20 8.30 2 6 -13 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6.80 -4 -7 14 14.30 5.50 3 7 -14 -3.50 7.20 3 7 -14 -2.30 5.10 -3 -7 14 -6.30 5.10 -3 -7 14 0.50 5.40 -3 -7 14 3.90 6.70 2 7 -14 38.50 9.40 2 7 -14 47.90 7.30 -2 -7 14 53.39 7.90 -2 -7 14 49.40 9.20 1 7 -14 -4.20 7.30 1 7 -14 -1.50 5.70 -1 -7 14 -0.30 5.90 -1 -7 14 -0.30 6.30 0 7 -14 1.10 4.80 0 7 -14 5.80 7.80 0 -7 14 11.30 6.90 -1 7 -14 -3.20 8.30 -1 7 -14 6.30 4.60 1 -7 14 2.60 7.10 -2 7 -14 11.20 4.50 -2 7 -14 16.60 9.80 2 -7 14 12.80 8.40 -3 7 -14 2.20 3.60 -3 7 -14 2.80 9.20 3 -7 14 4.60 8.40 -4 7 -14 26.90 10.90 4 -7 14 7.30 9.50 -5 7 -14 9.60 11.00 5 -7 14 -4.20 9.20 -6 7 -14 -8.50 11.50 6 -7 14 -1.90 10.90 14 6 -14 26.90 7.10 13 6 -14 13.50 6.10 13 6 -14 -4.40 9.20 -13 -6 14 4.10 5.20 12 6 -14 83.29 12.40 12 6 -14 99.79 10.20 -12 -6 14 70.99 7.70 11 6 -14 41.60 10.70 11 6 -14 46.50 6.80 -11 -6 14 47.20 6.10 10 6 -14 8.90 8.40 10 6 -14 24.50 5.40 -10 -6 14 15.20 4.60 9 6 -14 67.09 11.20 -9 -6 14 72.99 7.60 8 6 -14 99.59 9.00 8 6 -14 103.29 12.30 -8 -6 14 91.79 8.40 -8 -6 14 126.89 13.60 7 6 -14 503.45 27.40 7 6 -14 495.65 30.90 -7 -6 14 517.45 30.80 -7 -6 14 511.85 27.50 6 6 -14 169.18 16.30 -6 -6 14 169.28 11.70 -6 -6 14 147.99 14.60 5 6 -14 30.50 8.50 5 6 -14 30.50 6.80 -5 -6 14 33.00 6.00 -5 -6 14 34.20 8.00 -5 -6 14 35.40 5.50 4 6 -14 143.09 15.10 4 6 -14 152.08 13.00 -4 -6 14 189.38 14.40 -4 -6 14 151.88 12.00 -4 -6 14 149.19 11.50 3 6 -14 52.59 7.40 3 6 -14 95.49 11.40 -3 -6 14 69.79 7.90 -3 -6 14 66.19 7.20 -3 -6 14 60.19 9.10 2 6 -14 47.70 7.70 2 6 -14 46.00 9.90 -2 -6 14 53.19 7.50 -2 -6 14 45.00 9.00 -2 -6 14 63.49 7.40 1 6 -14 90.19 11.60 1 6 -14 100.59 9.00 -1 -6 14 86.09 9.00 -1 -6 14 94.69 11.70 0 6 -14 71.29 10.80 0 6 -14 71.29 7.60 0 -6 14 87.09 9.40 0 -6 14 82.09 9.10 -1 6 -14 0.40 4.30 -1 6 -14 17.80 8.60 1 -6 14 12.10 6.80 1 -6 14 13.60 6.60 -2 6 -14 110.99 9.50 -2 6 -14 88.79 12.70 2 -6 14 111.69 11.50 -3 6 -14 33.00 4.80 -3 6 -14 29.80 10.30 3 -6 14 41.10 9.50 -4 6 -14 53.59 11.80 -4 6 -14 36.80 4.00 4 -6 14 51.99 10.40 -5 6 -14 25.20 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15 147.59 10.50 2 4 -15 5.80 4.50 2 4 -15 13.40 7.20 -2 -4 15 5.70 6.60 -2 -4 15 5.30 4.20 1 4 -15 1006.10 55.39 1 4 -15 1101.79 58.19 -1 -4 15 1023.00 55.19 -1 -4 15 1083.49 55.39 -1 -4 15 1130.09 57.69 0 4 -15 30.90 5.50 0 4 -15 39.70 9.50 0 -4 15 20.60 7.70 0 -4 15 37.10 6.40 0 -4 15 38.10 6.20 -1 4 -15 4.60 4.20 -1 4 -15 3.60 7.50 1 -4 15 -3.30 13.20 1 -4 15 7.70 6.10 -2 4 -15 -0.50 12.50 -2 4 -15 -2.80 3.80 2 -4 15 2.10 5.20 2 -4 15 -3.80 6.00 -3 4 -15 85.79 8.30 -3 4 -15 100.69 12.40 3 -4 15 91.29 10.60 -4 4 -15 24.40 9.70 -4 4 -15 19.30 3.80 4 -4 15 15.50 7.90 -5 4 -15 6.40 2.10 -5 4 -15 19.90 10.30 5 -4 15 14.60 8.10 -6 4 -15 58.09 12.30 6 -4 15 41.30 9.50 7 -4 15 19.30 8.90 -8 4 -15 21.50 10.80 8 -4 15 -5.10 8.40 13 3 -15 7.60 10.40 13 3 -15 20.10 6.00 12 3 -15 38.80 11.50 12 3 -15 57.79 6.80 -12 -3 15 52.19 5.80 11 3 -15 77.79 8.00 11 3 -15 91.19 12.90 -11 -3 15 72.59 7.10 10 3 -15 7.10 3.60 10 3 -15 12.60 9.10 -10 -3 15 3.50 2.90 9 3 -15 -11.60 7.70 9 3 -15 -2.50 2.80 -9 -3 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22 28.80 4.70 6 7 -22 17.70 11.00 -6 -7 22 16.70 5.00 -6 -7 22 16.90 5.30 5 7 -22 8.60 10.10 -5 -7 22 3.80 5.20 4 7 -22 -3.10 9.60 -4 -7 22 -6.60 5.80 3 7 -22 1.60 10.00 -3 -7 22 5.80 6.80 -3 -7 22 17.20 5.80 2 7 -22 4.70 18.80 -2 -7 22 4.60 8.80 1 7 -22 4.30 10.60 -1 -7 22 11.90 8.00 0 7 -22 -3.40 11.40 0 -7 22 -16.10 7.80 10 6 -22 -4.90 10.10 9 6 -22 66.89 14.30 8 6 -22 26.30 11.70 7 6 -22 195.08 20.00 6 6 -22 47.40 12.20 -6 -6 22 42.90 4.20 -6 -6 22 30.60 4.10 5 6 -22 3.20 9.80 -5 -6 22 3.50 6.40 4 6 -22 0.30 8.90 -4 -6 22 4.40 4.30 -4 -6 22 -4.70 4.90 3 6 -22 13.60 10.50 -3 -6 22 28.20 6.80 -3 -6 22 39.60 6.20 2 6 -22 35.20 11.40 -2 -6 22 23.10 7.20 -2 -6 22 46.60 7.00 1 6 -22 75.49 14.90 -1 -6 22 93.89 10.80 0 6 -22 -3.90 10.70 0 -6 22 5.00 7.50 -1 6 -22 -10.10 10.60 1 -6 22 3.50 7.90 -2 6 -22 -4.40 11.10 2 -6 22 -5.20 8.80 10 5 -22 11.40 11.30 9 5 -22 -16.00 10.30 8 5 -22 216.68 22.80 7 5 -22 82.69 14.50 6 5 -22 4.70 10.20 5 5 -22 42.90 11.10 -5 -5 22 40.10 3.90 -5 -5 22 48.40 5.30 4 5 -22 37.10 10.90 -4 -5 22 46.00 5.50 -4 -5 22 59.39 6.30 3 5 -22 9.30 9.70 -3 -5 22 2.10 4.80 -3 -5 22 13.70 4.60 2 5 -22 65.19 12.60 -2 -5 22 66.09 7.60 -2 -5 22 56.49 7.20 1 5 -22 2.70 9.70 -1 -5 22 10.30 6.50 -1 -5 22 13.40 7.50 0 5 -22 6.80 11.30 0 -5 22 15.60 6.80 0 -5 22 8.40 6.90 1 -5 22 -2.40 7.10 -2 5 -22 -3.70 9.90 -2 5 -22 -20.50 5.70 2 -5 22 6.00 7.90 -3 5 -22 -1.10 10.70 3 -5 22 5.90 8.50 10 4 -22 4.00 11.60 9 4 -22 -15.40 10.90 8 4 -22 32.00 11.40 7 4 -22 8.70 10.90 6 4 -22 17.20 10.30 5 4 -22 86.49 13.80 4 4 -22 90.19 13.50 -4 -4 22 78.69 5.80 -4 -4 22 97.89 6.00 3 4 -22 28.30 11.10 -3 -4 22 38.00 5.00 -3 -4 22 32.10 4.60 2 4 -22 86.39 13.50 -2 -4 22 105.99 9.50 -2 -4 22 112.99 9.50 1 4 -22 107.79 14.60 -1 -4 22 101.59 10.50 -1 -4 22 103.49 9.90 0 4 -22 5.20 10.00 0 -4 22 5.50 5.90 -1 4 -22 28.60 12.00 1 -4 22 39.70 8.00 1 -4 22 18.30 7.40 -2 4 -22 -8.50 4.90 -2 4 -22 -14.00 10.10 2 -4 22 5.20 7.40 -3 4 -22 -3.90 9.80 -3 4 -22 -7.60 4.90 3 -4 22 0.20 8.00 -4 4 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0 -2 22 88.29 7.80 0 -2 22 72.09 8.10 -1 2 -22 0.00 9.50 1 -2 22 -1.20 4.40 1 -2 22 5.20 5.20 -2 2 -22 268.17 22.70 2 -2 22 248.68 17.00 2 -2 22 279.37 17.80 -3 2 -22 28.90 10.70 -4 2 -22 13.30 10.50 4 -2 22 25.80 7.70 -5 2 -22 51.09 13.20 -5 2 -22 33.40 5.70 5 -2 22 44.00 9.30 -6 2 -22 -4.80 10.80 -6 2 -22 0.60 8.00 6 -2 22 1.50 8.60 10 1 -22 1.70 10.90 9 1 -22 5.50 10.50 8 1 -22 50.19 12.90 7 1 -22 42.90 12.30 6 1 -22 13.90 10.50 5 1 -22 -11.90 8.40 4 1 -22 6.40 9.80 3 1 -22 17.30 9.90 2 1 -22 -8.10 8.50 1 1 -22 29.60 10.60 -1 -1 22 49.60 4.90 -1 -1 22 42.00 4.70 0 1 -22 -4.70 8.10 0 -1 22 -1.80 5.10 0 -1 22 1.90 3.70 -1 1 -22 8.30 9.90 1 -1 22 20.60 5.50 1 -1 22 16.50 4.60 -2 1 -22 24.10 10.10 -2 1 -22 39.00 6.60 2 -1 22 38.10 6.60 -3 1 -22 6.00 10.10 -3 1 -22 8.30 5.70 3 -1 22 8.00 6.30 -4 1 -22 27.60 11.00 4 -1 22 10.10 6.90 -5 1 -22 11.40 10.70 5 -1 22 26.40 8.00 -6 1 -22 35.30 6.20 -6 1 -22 20.10 4.80 -6 1 -22 28.20 12.20 6 -1 22 33.20 9.00 -7 1 -22 3.70 4.70 -7 1 -22 5.70 11.30 7 -1 22 4.80 8.90 9 0 -22 12.50 11.50 8 0 -22 63.89 15.50 7 0 -22 1.50 10.20 6 0 -22 17.60 10.10 5 0 -22 33.10 10.80 4 0 -22 40.10 11.00 3 0 -22 3.50 9.60 2 0 -22 84.09 12.70 1 0 -22 -9.30 8.10 -1 0 22 5.90 2.60 -1 0 22 7.80 2.50 0 0 -22 285.97 24.00 0 0 22 319.87 18.00 0 0 22 350.76 18.50 -1 0 -22 233.18 14.40 -1 0 -22 195.78 19.90 1 0 22 239.68 14.80 -2 0 -22 81.49 13.80 -2 0 -22 98.79 9.50 2 0 22 111.29 10.40 -3 0 -22 0.50 5.20 -3 0 -22 -15.80 8.70 3 0 22 1.80 5.70 -4 0 -22 53.79 12.30 4 0 22 79.39 9.20 -5 0 -22 -5.50 9.10 5 0 22 -2.50 6.70 -6 0 -22 13.30 5.60 -6 0 -22 34.50 11.50 6 0 22 -2.00 7.20 -7 0 -22 -0.10 4.40 -7 0 -22 8.90 10.50 7 0 22 -14.10 7.70 -8 0 -22 -3.70 13.30 8 0 22 -2.80 10.10 9 -1 -22 12.30 10.60 8 -1 -22 -0.50 9.90 7 -1 -22 19.70 10.30 6 -1 -22 1.50 9.60 5 -1 -22 -1.10 8.90 4 -1 -22 -4.40 9.30 3 -1 -22 219.58 20.40 2 -1 -22 0.80 8.80 1 -1 -22 6.00 8.50 0 -1 -22 205.18 18.90 0 1 22 206.78 12.50 -1 -1 -22 132.89 14.80 -1 -1 -22 118.29 9.20 -2 -1 -22 131.29 14.90 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10.00 4 -4 -22 -4.80 9.20 3 -4 -22 3.60 9.90 2 -4 -22 45.30 11.10 1 -4 -22 240.38 20.70 0 -4 -22 104.09 13.90 0 -4 -22 133.79 8.70 0 4 22 142.69 8.90 -1 -4 -22 15.80 9.20 1 4 22 10.40 4.30 -2 -4 -22 0.20 8.20 -2 -4 -22 4.30 4.40 2 4 22 3.20 4.90 -3 -4 -22 4.70 4.80 -3 -4 -22 7.00 8.20 3 4 22 -1.00 5.40 -4 -4 -22 43.80 7.00 -4 -4 -22 40.90 10.50 4 4 22 63.19 8.40 -5 -4 -22 6.10 9.20 -5 -4 -22 6.90 6.00 5 4 22 -0.50 6.80 -6 -4 -22 2.50 8.70 -6 -4 -22 9.40 7.50 -7 -4 -22 16.20 10.10 -7 -4 -22 19.00 6.80 7 4 22 26.80 8.60 -8 -4 -22 1.70 6.10 -8 -4 -22 5.40 9.40 8 4 22 5.10 8.50 -9 -4 -22 12.20 6.30 -9 -4 -22 18.00 11.00 9 4 22 3.90 9.40 -10 -4 -22 -6.10 10.10 -10 -4 -22 -8.00 5.20 10 4 22 7.70 9.50 7 -5 -22 0.60 10.60 5 -5 -22 9.30 10.10 4 -5 -22 -2.00 9.30 3 -5 -22 6.60 9.40 2 -5 -22 174.08 18.90 1 -5 -22 60.79 11.70 1 -5 -22 57.49 5.10 1 -5 -22 42.70 4.70 0 -5 -22 0.60 3.60 0 -5 -22 -7.60 8.10 0 5 22 0.70 3.40 -1 -5 -22 7.50 4.50 -1 -5 -22 19.10 8.90 1 5 22 7.70 4.50 -2 -5 -22 18.80 5.20 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0.4296 0.0088 1 11 9 -0.5090 -0.0054 1 11 10 0.2722 -0.0014 1 11 11 0.4525 -0.0001 1 11 12 -0.6802 0.0097 1 11 13 0.2889 -0.0086 1 11 14 0.1222 0.0023 1 11 15 -0.1194 -0.0034 1 11 16 -0.0249 0.0026 1 11 17 -0.3345 -0.0011 1 11 18 0.6459 0.0049 1 11 19 -0.4047 -0.0066 1 11 20 0.0940 0.0059 1 11 21 0.2372 -0.0045 1 11 22 -0.1881 0.0035 1 11 23 -0.4762 -0.0063 1 11 24 0.5349 0.0025 1 12 0 -0.0216 0.0699 1 12 1 0.3007 -0.0335 1 12 2 0.3079 -0.0192 1 12 3 -0.4185 0.0338 1 12 4 -0.3019 -0.0137 1 12 5 0.2029 0.0002 1 12 6 0.5195 -0.0049 1 12 7 -0.6875 -0.0019 1 12 8 0.6083 0.0155 1 12 9 -0.6333 -0.0048 1 12 10 0.4398 -0.0101 1 12 11 0.0765 0.0053 1 12 12 -0.3400 0.0016 1 12 13 -0.2093 -0.0054 1 12 14 0.8674 0.0094 1 12 15 -0.7517 -0.0022 1 12 16 0.2103 -0.0087 1 12 17 0.0555 0.0080 1 12 18 0.1809 0.0033 1 12 19 -0.4521 -0.0163 1 12 20 0.2478 0.0157 1 12 21 0.1062 -0.0025 1 12 22 -0.2357 -0.0058 1 13 0 -0.0515 0.0247 1 13 1 0.0043 -0.0291 1 13 2 0.0785 0.0064 1 13 3 -0.0305 0.0011 1 13 4 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2 -3 13 1.4728 0.0026 2 -3 14 -1.5738 -0.0011 2 -3 15 0.8411 -0.0010 2 -3 16 -0.0428 -0.0025 2 -3 17 -0.2376 0.0074 2 -3 18 0.0305 -0.0026 2 -3 19 0.1362 -0.0036 2 -3 20 -0.0501 0.0042 2 -3 21 -0.1779 -0.0049 2 -3 22 0.1869 0.0008 2 -3 23 0.1486 0.0062 2 -3 24 -0.4737 -0.0008 2 -3 25 0.6675 -0.0092 2 -3 26 -0.4312 0.0077 2 -2 0 -0.0677 -0.2317 2 -2 1 -0.1146 0.0415 2 -2 2 2.7887 0.0780 2 -2 3 -3.4659 -0.0322 2 -2 4 1.2414 -0.0491 2 -2 5 2.2376 0.0578 2 -2 6 -4.4912 -0.0279 2 -2 7 3.1504 0.0165 2 -2 8 0.1432 -0.0085 2 -2 9 -2.5150 -0.0037 2 -2 10 3.0148 -0.0042 2 -2 11 -1.5866 0.0141 2 -2 12 -0.5673 -0.0067 2 -2 13 1.9035 0.0022 2 -2 14 -1.8480 -0.0020 2 -2 15 0.7394 -0.0031 2 -2 16 0.2260 0.0022 2 -2 17 -0.4367 0.0030 2 -2 18 0.2780 -0.0005 2 -2 19 -0.1782 -0.0055 2 -2 20 0.1816 0.0065 2 -2 21 0.2196 -0.0036 2 -2 22 -0.5786 0.0012 2 -2 23 0.0798 -0.0009 2 -2 24 0.1952 0.0042 2 -2 25 0.2805 -0.0102 2 -2 26 -0.4209 0.0109 2 -2 27 0.1328 -0.0002 2 -1 0 -9.3010 -0.1606 2 -1 1 10.8600 0.0037 2 -1 2 -6.2129 0.1039 2 -1 3 1.4336 -0.0323 2 -1 4 -1.6030 -0.0646 2 -1 5 4.3212 0.0536 2 -1 6 -4.6682 -0.0238 2 -1 7 1.8595 0.0301 2 -1 8 2.7903 -0.0189 2 -1 9 -5.9028 -0.0010 2 -1 10 4.8451 -0.0096 2 -1 11 -1.5839 0.0251 2 -1 12 -1.2280 -0.0173 2 -1 13 2.4779 0.0042 2 -1 14 -1.9979 -0.0008 2 -1 15 0.7792 -0.0029 2 -1 16 0.3032 0.0041 2 -1 17 -0.5256 0.0047 2 -1 18 -0.0442 -0.0070 2 -1 19 0.2015 -0.0019 2 -1 20 -0.0371 0.0041 2 -1 21 0.0661 -0.0022 2 -1 22 0.0040 0.0046 2 -1 23 -0.0457 -0.0013 2 -1 24 0.0493 -0.0020 2 -1 25 0.2039 -0.0078 2 -1 26 -0.6936 0.0142 2 -1 27 0.2043 0.0003 2 0 1 29.0171 0.0034 2 0 2 -12.6425 0.0609 2 0 3 0.7549 0.0044 2 0 4 1.2750 -0.0654 2 0 5 0.5717 0.0567 2 0 7 -1.7558 0.0418 2 0 8 5.9967 -0.0360 2 0 9 -7.8928 0.0128 2 0 10 6.0911 -0.0118 2 0 11 -1.3988 0.0256 2 0 12 -2.4630 -0.0189 2 0 13 3.2027 0.0057 2 0 14 -2.1782 -0.0028 2 0 15 0.7211 -0.0022 2 0 16 0.1212 0.0044 2 0 17 -0.0363 0.0048 2 0 18 -0.2730 -0.0094 2 0 19 0.5426 0.0017 2 0 20 -0.0321 0.0046 2 0 21 -0.8580 -0.0041 2 0 22 0.5661 0.0036 2 0 23 0.0363 -0.0035 2 0 24 -0.1313 0.0010 2 0 25 0.3681 -0.0033 2 0 26 -0.1747 0.0113 2 0 27 -0.6301 -0.0087 2 0 28 1.1403 -0.0117 2 1 0 -47.7546 -0.1718 2 1 1 36.6584 0.0128 2 1 2 -10.1340 0.0843 2 1 3 -9.8350 -0.0406 2 1 4 10.6681 -0.0378 2 1 5 -3.4452 0.0488 2 1 6 2.2908 -0.0304 2 1 7 -5.6358 0.0303 2 1 8 8.4803 -0.0206 2 1 9 -8.7135 -0.0002 2 1 10 5.0012 -0.0022 2 1 11 -0.0771 0.0181 2 1 12 -2.8694 -0.0202 2 1 13 3.3952 0.0124 2 1 14 -2.1714 -0.0042 2 1 15 0.9487 -0.0064 2 1 16 -0.4590 0.0110 2 1 17 0.4754 0.0004 2 1 18 -0.8414 -0.0101 2 1 19 0.3842 0.0028 2 1 20 0.5987 0.0037 2 1 21 -0.8551 -0.0018 2 1 22 0.6811 0.0064 2 1 23 0.0182 -0.0097 2 1 24 -0.6576 0.0002 2 1 25 0.1820 0.0031 2 1 26 0.2009 0.0072 2 1 27 -0.1444 -0.0062 2 1 28 0.3942 -0.0109 2 2 0 -48.8591 -0.1660 2 2 1 29.2773 0.0207 2 2 2 1.5903 0.1059 2 2 3 -18.5660 -0.0769 2 2 6 2.3245 -0.0129 2 2 7 -5.7749 0.0180 2 2 8 9.0681 -0.0136 2 2 9 -6.6948 -0.0036 2 2 10 2.2829 0.0004 2 2 11 1.3986 0.0221 2 2 12 -3.3132 -0.0277 2 2 13 2.9042 0.0132 2 2 14 -2.0996 -0.0002 2 2 15 1.6822 -0.0089 2 2 16 -1.3518 0.0100 2 2 17 1.1516 0.0037 2 2 18 -0.4441 -0.0140 2 2 19 -0.3471 0.0078 2 2 20 0.7809 0.0013 2 2 21 -0.9911 -0.0033 2 2 22 0.3087 0.0033 2 2 23 0.4372 -0.0033 2 2 24 -0.3658 -0.0001 2 2 25 0.3409 0.0051 2 2 26 -0.1936 -0.0036 2 2 27 -0.0609 -0.0046 2 2 28 -0.0826 0.0080 2 2 29 -0.0655 -0.0023 2 3 0 -31.5207 -0.0950 2 3 1 12.5750 0.0260 2 3 2 7.8934 0.0650 2 3 3 -19.3195 -0.0990 2 3 4 15.4211 0.0500 2 3 5 -4.5616 0.0068 2 3 7 -2.7129 0.0220 2 3 8 5.3564 -0.0225 2 3 9 -5.0751 0.0013 2 3 10 1.2802 0.0093 2 3 11 2.2292 0.0096 2 3 12 -2.8086 -0.0245 2 3 13 2.2297 0.0160 2 3 14 -1.7431 0.0003 2 3 15 1.7408 -0.0075 2 3 16 -1.7402 0.0040 2 3 17 0.7305 0.0045 2 3 18 0.5003 -0.0124 2 3 19 -1.2519 0.0102 2 3 20 1.3271 -0.0001 2 3 21 -0.7043 -0.0033 2 3 22 0.4170 0.0015 2 3 23 -0.1643 -0.0017 2 3 24 -0.3579 -0.0013 2 3 25 -0.0119 0.0055 2 3 26 0.4373 -0.0015 2 3 27 -0.0877 -0.0087 2 3 28 -0.0637 0.0164 2 3 29 0.1566 -0.0137 2 4 0 -13.7595 -0.0121 2 4 2 9.2474 0.0334 2 4 3 -10.6278 -0.0786 2 4 4 6.3259 0.0360 2 4 5 -1.7254 0.0185 2 4 6 -1.2729 -0.0303 2 4 7 -0.5850 0.0206 2 4 8 4.5696 -0.0106 2 4 9 -4.5357 -0.0036 2 4 10 1.5297 0.0136 2 4 11 1.0899 0.0039 2 4 12 -2.2243 -0.0272 2 4 13 1.8325 0.0183 2 4 14 -1.5028 0.0033 2 4 15 1.7087 -0.0094 2 4 16 -1.3897 0.0073 2 4 17 0.3739 -0.0008 2 4 18 0.9661 -0.0086 2 4 19 -1.6732 0.0096 2 4 20 1.4484 -0.0023 2 4 21 -1.0091 -0.0053 2 4 22 0.4002 0.0070 2 4 23 -0.1281 -0.0004 2 4 24 0.2793 -0.0067 2 4 25 0.0080 0.0076 2 4 26 0.0090 -0.0022 2 4 27 -0.2519 -0.0078 2 4 28 -0.4157 0.0126 2 4 29 0.7585 -0.0025 2 5 0 -4.0189 -0.0337 2 5 1 -1.3937 0.0421 2 5 2 3.2821 -0.0219 2 5 3 -2.6917 -0.0355 2 5 4 0.7330 0.0380 2 5 5 0.7341 0.0158 2 5 6 0.7422 -0.0222 2 5 7 -2.9548 -0.0062 2 5 8 3.6646 0.0027 2 5 9 -3.0166 0.0049 2 5 10 0.7722 0.0035 2 5 11 1.3302 0.0027 2 5 12 -1.6891 -0.0163 2 5 13 1.7299 0.0089 2 5 14 -2.0395 0.0104 2 5 15 1.8845 -0.0155 2 5 16 -1.1126 0.0083 2 5 17 -0.0270 -0.0043 2 5 18 1.0095 -0.0013 2 5 19 -1.5697 0.0087 2 5 20 1.3653 -0.0014 2 5 21 -0.5767 -0.0103 2 5 22 0.2310 0.0056 2 5 23 0.0798 0.0064 2 5 24 -0.4991 -0.0106 2 5 25 0.0320 0.0052 2 5 26 0.2334 0.0031 2 5 27 0.2383 -0.0019 2 5 28 -0.1597 -0.0082 2 5 29 0.0507 0.0149 2 6 0 -1.9179 -0.0487 2 6 1 0.6000 0.0017 2 6 2 0.7208 0.0344 2 6 3 0.1400 -0.0604 2 6 4 -0.8118 0.0511 2 6 5 -0.7352 -0.0136 2 6 6 1.9086 -0.0119 2 6 7 -1.9172 0.0072 2 6 8 1.6484 0.0017 2 6 9 -0.5933 -0.0007 2 6 10 -0.6926 0.0074 2 6 11 1.0365 -0.0082 2 6 12 -0.7799 -0.0101 2 6 13 0.9732 0.0116 2 6 14 -1.5845 0.0077 2 6 15 1.4228 -0.0127 2 6 16 -0.4640 0.0079 2 6 17 -0.3916 -0.0080 2 6 18 0.9762 0.0018 2 6 19 -1.0838 0.0062 2 6 20 0.8190 -0.0010 2 6 21 -0.3596 -0.0086 2 6 22 -0.4599 0.0054 2 6 23 0.5800 0.0059 2 6 24 0.0331 -0.0070 2 6 25 0.0160 -0.0001 2 6 26 0.0993 -0.0018 2 6 27 -0.6137 0.0150 2 6 28 0.1450 -0.0260 2 7 0 -1.0309 -0.0448 2 7 1 0.6347 -0.0194 2 7 2 -0.8245 0.0388 2 7 3 0.5982 -0.0333 2 7 4 0.4572 0.0301 2 7 5 -1.2366 -0.0032 2 7 6 0.9058 -0.0252 2 7 7 0.1043 0.0164 2 7 8 -0.3471 0.0048 2 7 9 -0.2452 -0.0123 2 7 10 0.3264 0.0086 2 7 11 0.0811 0.0049 2 7 12 -0.1778 -0.0175 2 7 13 0.0654 0.0132 2 7 14 -0.3499 0.0014 2 7 15 0.9359 -0.0091 2 7 16 -0.7551 0.0093 2 7 17 -0.0906 -0.0087 2 7 18 0.5902 0.0018 2 7 19 -0.8042 0.0073 2 7 20 0.4091 -0.0002 2 7 21 0.4365 -0.0126 2 7 22 -0.3508 0.0071 2 7 23 0.1077 0.0061 2 7 24 -0.3557 -0.0086 2 7 25 -0.2004 0.0082 2 7 26 0.6174 -0.0126 2 7 27 -0.0477 0.0156 2 7 28 -0.0891 -0.0111 2 8 0 -0.4770 -0.1341 2 8 1 0.8588 0.0706 2 8 2 -1.0052 -0.0076 2 8 3 0.2599 -0.0180 2 8 4 0.9090 0.0197 2 8 5 -1.2266 -0.0104 2 8 6 0.3813 -0.0024 2 8 7 0.5915 0.0044 2 8 8 -0.6466 0.0061 2 8 9 -0.2081 -0.0094 2 8 10 0.5850 0.0017 2 8 11 -0.0893 0.0019 2 8 12 0.0705 -0.0022 2 8 13 -0.1486 0.0043 2 8 14 -0.5329 -0.0012 2 8 15 0.8397 -0.0060 2 8 16 -0.5980 0.0091 2 8 17 0.2344 -0.0078 2 8 18 0.5298 0.0031 2 8 19 -0.7210 0.0013 2 8 20 0.1088 0.0031 2 8 21 0.2805 -0.0101 2 8 22 -0.5512 0.0054 2 8 23 0.3378 0.0036 2 8 24 0.3251 -0.0045 2 8 25 -0.1417 0.0041 2 8 26 -0.0930 -0.0017 2 8 27 -0.2525 -0.0123 2 9 0 -0.4286 -0.1133 2 9 1 0.7431 0.0455 2 9 2 -0.1856 0.0230 2 9 3 -0.3900 -0.0316 2 9 4 0.3583 0.0216 2 9 5 -0.5477 -0.0227 2 9 6 0.4864 0.0069 2 9 7 0.3927 0.0118 2 9 8 -0.7861 -0.0021 2 9 9 0.4058 -0.0131 2 9 10 0.1110 0.0118 2 9 11 -0.6640 -0.0057 2 9 12 0.6153 0.0004 2 9 13 -0.1120 0.0056 2 9 14 -0.1228 -0.0064 2 9 15 0.3336 -0.0005 2 9 16 -0.1463 0.0100 2 9 17 -0.3695 -0.0113 2 9 18 0.3104 0.0018 2 9 19 -0.2891 0.0030 2 9 20 0.1859 0.0032 2 9 21 0.5653 -0.0074 2 9 22 -0.4396 0.0076 2 9 23 -0.3265 -0.0078 2 9 24 0.2114 0.0033 2 9 25 -0.1772 0.0022 2 9 26 0.4024 0.0033 2 9 27 -0.0753 -0.0164 2 10 0 -0.4381 -0.0240 2 10 1 0.1980 0.0036 2 10 2 0.0317 -0.0142 2 10 3 -0.1005 0.0196 2 10 4 0.2912 -0.0030 2 10 5 -0.0705 -0.0009 2 10 6 -0.1880 -0.0118 2 10 7 0.0343 0.0159 2 10 8 -0.2246 -0.0051 2 10 9 0.1857 -0.0081 2 10 10 0.6088 0.0056 2 10 11 -0.9786 0.0089 2 10 12 0.8785 -0.0103 2 10 13 -0.5927 0.0037 2 10 14 -0.0651 -0.0058 2 10 15 0.1743 0.0025 2 10 16 0.0951 0.0071 2 10 17 0.1138 -0.0043 2 10 18 -0.1140 -0.0036 2 10 19 -0.0616 0.0036 2 10 20 -0.0462 0.0007 2 10 21 0.0182 -0.0053 2 10 22 -0.0024 0.0044 2 10 23 -0.1990 0.0025 2 10 24 0.6651 -0.0078 2 10 25 -0.4229 0.0124 2 10 26 0.0666 -0.0111 2 11 0 -0.1314 -0.0360 2 11 1 0.5061 0.0186 2 11 2 -0.4339 -0.0234 2 11 3 -0.2490 0.0235 2 11 4 0.0576 -0.0073 2 11 5 0.5059 -0.0078 2 11 6 -0.3490 -0.0025 2 11 7 0.2569 0.0198 2 11 8 -0.2514 -0.0101 2 11 9 -0.2440 -0.0040 2 11 10 0.7106 -0.0043 2 11 11 -0.7077 0.0079 2 11 12 0.2876 0.0013 2 11 13 -0.0220 0.0005 2 11 14 0.1293 -0.0086 2 11 15 0.1862 0.0084 2 11 16 -0.5726 -0.0018 2 11 17 0.3516 -0.0044 2 11 18 -0.2166 0.0025 2 11 19 0.0464 0.0020 2 11 20 0.3588 -0.0019 2 11 21 -0.2063 0.0056 2 11 22 0.0106 -0.0071 2 11 23 -0.2711 -0.0019 2 11 24 0.2734 0.0037 2 12 0 -0.5074 -0.0145 2 12 1 0.5429 -0.0357 2 12 2 -0.1692 0.0303 2 12 3 0.2924 -0.0041 2 12 4 -0.3824 0.0106 2 12 5 0.3876 -0.0158 2 12 6 -0.8221 -0.0081 2 12 7 0.7716 0.0181 2 12 8 -0.1086 -0.0047 2 12 9 -0.2303 -0.0016 2 12 10 0.4007 0.0024 2 12 11 -0.4652 -0.0024 2 12 12 0.1002 -0.0047 2 12 13 0.2406 0.0103 2 12 14 -0.1607 -0.0106 2 12 15 -0.0152 0.0053 2 12 16 -0.1952 0.0049 2 12 17 0.5333 -0.0053 2 12 18 -0.4180 -0.0028 2 12 19 0.0940 0.0049 2 12 20 0.2564 -0.0041 2 12 21 -0.5452 -0.0010 2 12 22 0.1481 0.0147 2 13 0 0.1002 -0.0043 2 13 1 -0.0797 -0.0238 2 13 2 -0.5443 0.0148 2 13 3 0.3513 -0.0026 2 13 4 0.0115 0.0081 2 13 5 0.4695 -0.0086 2 13 6 -0.4697 -0.0004 2 13 7 -0.1454 0.0115 2 13 8 0.0363 -0.0121 2 13 9 0.2664 -0.0012 2 13 10 0.1032 0.0014 2 13 11 -0.3929 0.0118 2 13 12 0.0095 -0.0109 2 13 13 0.3735 0.0052 2 13 14 -0.1081 -0.0043 2 13 15 -0.3512 -0.0005 2 13 16 0.2709 -0.0032 2 13 17 0.2931 0.0156 2 13 18 -0.5848 -0.0158 2 13 19 0.0958 0.0040 2 13 20 0.5301 0.0097 2 14 0 0.4058 -0.0228 2 14 1 0.0236 0.0161 2 14 2 -0.0376 0.0008 2 14 3 0.1270 -0.0083 2 14 4 -0.2197 0.0126 2 14 5 -0.4745 -0.0187 2 14 6 0.7368 0.0006 2 14 7 0.0500 0.0161 2 14 8 -0.5366 -0.0028 2 14 9 0.5958 0.0024 2 14 10 -0.5793 -0.0163 2 14 11 -0.0238 0.0049 2 14 12 0.5630 0.0085 2 14 13 -0.2541 -0.0025 2 14 14 0.1265 -0.0054 2 14 15 -0.6112 0.0147 2 14 16 0.5846 -0.0204 2 14 17 -0.0122 0.0131 2 15 0 0.2775 0.0062 2 15 1 -0.4830 -0.0057 2 15 2 -0.0903 -0.0045 2 15 3 0.3140 -0.0016 2 15 4 0.3755 0.0138 2 15 5 -0.6319 0.0002 2 15 6 0.2447 -0.0047 2 15 7 0.1857 -0.0108 2 15 8 -0.8992 0.0000 2 15 9 1.2017 0.0160 2 15 10 -0.2875 -0.0046 2 15 11 -0.6848 -0.0074 2 15 12 0.7632 0.0126 3 -12 0 -0.4023 -0.0041 3 -12 1 -0.0432 0.0065 3 -12 2 0.2397 0.0002 3 -12 3 0.1430 -0.0050 3 -12 4 -0.3621 0.0055 3 -11 0 -0.9009 -0.0072 3 -11 1 0.3973 -0.0085 3 -11 2 0.3699 0.0055 3 -11 3 -0.2492 0.0004 3 -11 4 -0.4746 0.0080 3 -11 5 0.2792 -0.0133 3 -11 6 0.4186 0.0057 3 -11 7 -0.0068 0.0020 3 -11 8 -0.9177 -0.0071 3 -11 9 0.6341 0.0073 3 -10 0 -0.3237 -0.0094 3 -10 1 -0.0812 -0.0071 3 -10 2 0.2284 0.0042 3 -10 3 0.2322 -0.0043 3 -10 4 -0.5247 0.0115 3 -10 5 0.1853 -0.0118 3 -10 6 0.2254 0.0042 3 -10 7 0.0371 0.0044 3 -10 8 -0.7433 -0.0048 3 -10 9 0.8821 0.0005 3 -10 10 -0.1708 -0.0006 3 -10 11 -0.4342 -0.0025 3 -10 12 0.2407 0.0066 3 -9 0 0.3026 -0.0035 3 -9 1 0.1940 -0.0034 3 -9 2 -0.8156 0.0180 3 -9 3 0.4722 -0.0205 3 -9 4 -0.2851 0.0175 3 -9 5 0.1304 -0.0161 3 -9 6 0.5864 0.0062 3 -9 7 -0.4967 0.0003 3 -9 8 -0.6388 0.0048 3 -9 9 0.8429 -0.0075 3 -9 10 -0.0275 0.0081 3 -9 11 -0.2489 -0.0073 3 -9 12 0.5309 0.0004 3 -9 13 -1.2718 -0.0004 3 -9 14 0.7855 0.0070 3 -9 15 0.6889 -0.0055 3 -8 0 -0.1735 0.0247 3 -8 1 0.3053 -0.0143 3 -8 2 -0.3600 0.0018 3 -8 3 0.3482 -0.0056 3 -8 4 -0.0023 0.0181 3 -8 5 -0.3429 -0.0102 3 -8 6 0.2800 -0.0050 3 -8 7 -0.0951 0.0064 3 -8 8 -0.2002 -0.0015 3 -8 9 0.6102 -0.0033 3 -8 10 -0.4491 0.0038 3 -8 11 -0.3240 0.0016 3 -8 12 0.6771 -0.0039 3 -8 13 -0.5435 0.0030 3 -8 14 0.3601 -0.0010 3 -8 15 0.7347 -0.0010 3 -8 16 -2.1533 -0.0046 3 -8 17 1.5729 0.0077 3 -7 0 -0.3690 0.0493 3 -7 1 0.1700 -0.0043 3 -7 2 -0.6945 -0.0232 3 -7 3 0.2127 0.0057 3 -7 4 0.1828 0.0120 3 -7 5 0.5227 -0.0118 3 -7 6 -0.6026 0.0018 3 -7 7 -0.2006 0.0072 3 -7 8 0.1811 -0.0038 3 -7 9 0.3213 -0.0021 3 -7 10 -0.0523 0.0031 3 -7 11 -0.2251 -0.0055 3 -7 12 -0.0165 0.0019 3 -7 13 0.0218 0.0052 3 -7 14 -0.1623 -0.0033 3 -7 15 0.8254 0.0015 3 -7 16 -1.1568 -0.0036 3 -7 17 1.0373 0.0002 3 -7 18 -0.6766 0.0046 3 -7 19 -0.0627 -0.0029 3 -6 0 -1.3402 0.0768 3 -6 1 1.2097 -0.0362 3 -6 2 -0.8682 -0.0002 3 -6 3 0.5992 -0.0101 3 -6 4 -0.2454 0.0399 3 -6 5 0.0842 -0.0359 3 -6 6 -0.2652 0.0116 3 -6 7 -0.0053 -0.0100 3 -6 8 0.6571 0.0146 3 -6 9 -0.5423 -0.0066 3 -6 10 -0.0783 0.0068 3 -6 11 0.0182 -0.0137 3 -6 12 0.1306 0.0095 3 -6 13 0.4047 0.0007 3 -6 14 -0.4638 -0.0041 3 -6 15 -0.0210 -0.0001 3 -6 16 -0.3825 0.0020 3 -6 17 0.9677 -0.0007 3 -6 18 -0.5883 0.0028 3 -6 19 0.2464 0.0011 3 -6 20 -0.2805 -0.0112 3 -6 21 -0.0546 0.0066 3 -5 0 -2.1097 0.0727 3 -5 1 1.9993 -0.0290 3 -5 2 -1.8390 -0.0065 3 -5 3 0.9406 -0.0074 3 -5 4 0.2122 0.0330 3 -5 5 -0.5885 -0.0247 3 -5 6 0.3579 0.0055 3 -5 7 -0.4074 -0.0019 3 -5 8 0.6578 0.0047 3 -5 9 -0.5460 -0.0029 3 -5 10 0.3403 0.0005 3 -5 11 -0.2446 -0.0053 3 -5 12 0.0681 0.0064 3 -5 13 0.0608 0.0049 3 -5 14 -0.2510 -0.0101 3 -5 15 0.5341 0.0044 3 -5 16 -0.4276 -0.0031 3 -5 17 0.2388 0.0054 3 -5 18 -0.5339 -0.0059 3 -5 19 0.6701 0.0059 3 -5 20 -0.2453 -0.0055 3 -5 21 -0.0405 0.0065 3 -5 22 0.0384 -0.0054 3 -4 0 -4.4148 0.0024 3 -4 1 3.8085 0.0452 3 -4 2 -2.2382 -0.0354 3 -4 3 1.2325 0.0045 3 -4 4 -0.3227 0.0124 3 -4 5 -0.9742 -0.0181 3 -4 6 1.7686 0.0077 3 -4 7 -1.2049 0.0048 3 -4 8 0.3166 0.0005 3 -4 9 -0.3740 -0.0091 3 -4 10 0.5775 0.0122 3 -4 11 -0.3142 -0.0133 3 -4 12 0.2499 0.0055 3 -4 13 -0.1876 0.0052 3 -4 14 -0.2995 -0.0062 3 -4 15 0.6584 0.0016 3 -4 16 -0.5187 0.0004 3 -4 17 0.0694 0.0001 3 -4 18 0.3058 0.0010 3 -4 19 -0.0107 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0.0128 9 9 13 -0.1019 -0.0179 9 9 14 -0.0537 0.0048 9 9 15 0.0788 0.0046 9 9 16 -0.1565 0.0012 9 9 17 0.1026 -0.0049 9 9 18 0.0526 0.0011 9 9 19 -0.0781 0.0000 9 9 20 0.0332 -0.0003 9 9 21 -0.3415 0.0008 9 9 22 0.8338 0.0048 9 9 23 -0.6945 -0.0099 9 9 24 0.2548 0.0063 9 10 0 0.4358 0.0620 9 10 1 0.3555 -0.0304 9 10 2 -0.5467 -0.0162 9 10 3 0.5540 0.0546 9 10 4 0.1052 -0.0542 9 10 5 -0.9855 0.0165 9 10 6 0.7736 0.0111 9 10 7 -0.0474 -0.0046 9 10 8 -0.3162 -0.0057 9 10 9 0.5094 0.0011 9 10 10 -0.4926 0.0014 9 10 11 0.3226 0.0002 9 10 12 -0.3069 0.0108 9 10 13 0.2810 -0.0227 9 10 14 -0.0899 0.0116 9 10 15 -0.0942 0.0068 9 10 16 0.2090 -0.0034 9 10 17 -0.2625 -0.0086 9 10 18 0.0203 0.0028 9 10 19 0.3492 0.0080 9 10 20 -0.0380 -0.0045 9 10 21 -0.7202 -0.0000 9 10 22 0.8087 -0.0015 9 10 23 -0.3907 -0.0050 9 11 0 -0.1616 0.0816 9 11 1 0.3251 -0.0825 9 11 2 -0.4989 0.0324 9 11 3 0.1289 0.0346 9 11 4 0.2682 -0.0551 9 11 5 -0.4121 0.0286 9 11 6 0.5291 0.0016 9 11 7 0.0299 -0.0083 9 11 8 -0.8216 -0.0014 9 11 9 0.6141 0.0052 9 11 10 -0.1995 -0.0003 9 11 11 0.5217 -0.0022 9 11 12 -0.7905 0.0058 9 11 13 0.5828 -0.0121 9 11 14 -0.2838 0.0088 9 11 15 -0.1306 0.0020 9 11 16 0.4774 -0.0049 9 11 17 -0.2479 -0.0001 9 11 18 -0.2037 0.0019 9 11 19 0.2019 0.0029 9 11 20 0.1410 -0.0100 9 11 21 -0.4986 0.0102 9 11 22 0.6040 -0.0006 9 11 23 -0.2641 -0.0073 9 12 0 -0.5840 0.0612 9 12 1 0.6661 -0.0353 9 12 2 0.0029 -0.0048 9 12 3 -0.1564 0.0495 9 12 4 -0.0346 -0.0608 9 12 5 -0.1751 0.0235 9 12 6 -0.0138 0.0080 9 12 7 0.6132 0.0004 9 12 8 -0.6398 -0.0119 9 12 9 0.4988 0.0070 9 12 10 -0.8901 -0.0045 9 12 11 1.1902 0.0029 9 12 12 -0.8468 0.0064 9 12 13 0.4203 -0.0121 9 12 14 -0.2996 0.0054 9 12 15 -0.0580 0.0038 9 12 16 0.7152 -0.0025 9 12 17 -0.7209 -0.0038 9 12 18 0.0134 0.0028 9 12 19 0.1684 0.0023 9 12 20 0.3647 -0.0039 9 12 21 -0.4995 0.0077 9 12 22 0.1595 -0.0121 9 13 0 -0.4350 0.0062 9 13 1 0.6620 -0.0005 9 13 2 -0.5704 -0.0060 9 13 3 -0.0343 0.0217 9 13 4 0.2089 -0.0255 9 13 5 0.3631 0.0138 9 13 6 -0.3314 -0.0004 9 13 7 -0.1315 -0.0022 9 13 8 -0.2418 -0.0070 9 13 9 0.9585 0.0085 9 13 10 -1.1576 0.0024 9 13 11 1.0085 -0.0069 9 13 12 -0.5706 0.0039 9 13 13 0.0323 -0.0049 9 13 14 0.0192 0.0080 9 13 15 0.0128 -0.0056 9 13 16 0.5984 -0.0013 9 13 17 -0.9984 0.0020 9 13 18 0.2917 0.0064 9 13 19 0.3868 -0.0074 9 13 20 0.0341 -0.0065 9 14 0 0.2695 0.0568 9 14 1 0.0847 -0.0474 9 14 2 -0.0471 0.0112 9 14 3 0.0015 0.0241 9 14 4 0.0183 -0.0289 9 14 5 -0.2936 0.0078 9 14 6 0.4396 0.0030 9 14 7 -0.2137 -0.0002 9 14 8 -0.2129 0.0025 9 14 9 0.6419 -0.0000 9 14 10 -0.7263 -0.0069 9 14 11 0.4202 0.0010 9 14 12 -0.1215 0.0079 9 14 13 0.1109 -0.0079 9 14 14 -0.3011 0.0072 9 14 15 0.1159 -0.0065 9 14 16 0.6941 0.0014 9 14 17 -1.0531 0.0039 9 14 18 0.2653 -0.0029 9 15 0 1.4137 0.0623 9 15 1 -0.9467 -0.0157 9 15 2 -0.0673 -0.0283 9 15 3 0.3842 0.0320 9 15 4 -0.2604 -0.0217 9 15 5 0.3211 0.0151 9 15 6 -0.1321 0.0029 9 15 7 -0.0800 -0.0089 9 15 8 -0.2059 -0.0120 9 15 9 0.3536 0.0154 9 15 10 0.0386 0.0030 9 15 11 -0.2307 -0.0060 9 15 12 -0.2597 0.0023 9 15 13 0.6926 -0.0074 9 15 14 -0.2138 0.0098 9 15 15 -0.5794 -0.0059 9 15 16 0.6779 -0.0026 9 16 0 0.8380 -0.0026 9 16 1 -0.2293 -0.0024 9 16 2 -0.7088 -0.0021 9 16 3 1.1555 0.0174 9 16 4 -0.8564 -0.0124 9 16 5 0.6519 0.0001 9 16 6 -0.7617 -0.0151 9 16 7 0.1959 0.0187 9 16 8 0.6609 0.0074 9 16 9 -0.5938 -0.0056 10 -6 0 -0.1518 0.0022 10 -6 1 -0.8184 0.0039 10 -6 2 0.9701 -0.0096 10 -5 0 0.4966 0.0113 10 -5 1 -1.4919 -0.0053 10 -5 2 1.0931 0.0006 10 -5 3 0.4595 0.0005 10 -5 4 -0.5281 0.0008 10 -5 5 -0.1398 -0.0025 10 -5 6 -0.2623 0.0025 10 -4 0 0.4514 0.0235 10 -4 1 -0.2457 -0.0157 10 -4 2 -0.2395 0.0020 10 -4 3 0.0475 0.0037 10 -4 4 -0.0874 -0.0041 10 -4 5 0.1822 0.0034 10 -4 6 0.2420 0.0012 10 -4 7 0.0851 -0.0022 10 -4 8 -0.7104 -0.0043 10 -4 9 0.2266 0.0084 10 -4 10 0.2743 -0.0062 10 -3 0 -1.0703 0.0111 10 -3 1 0.5028 0.0021 10 -3 2 0.5663 -0.0092 10 -3 3 -0.3224 0.0086 10 -3 4 0.0915 -0.0082 10 -3 5 -0.3141 0.0074 10 -3 6 0.0064 -0.0052 10 -3 7 -0.0351 0.0035 10 -3 8 0.2634 -0.0052 10 -3 9 0.2243 0.0074 10 -3 10 -0.1856 -0.0032 10 -3 11 -0.4365 -0.0010 10 -3 12 0.1663 -0.0015 10 -2 0 -0.2269 0.0054 10 -2 1 -0.1141 0.0008 10 -2 2 0.2145 0.0002 10 -2 3 -0.3917 -0.0042 10 -2 4 0.0481 0.0040 10 -2 5 0.3010 0.0024 10 -2 6 0.1667 -0.0060 10 -2 7 -0.3157 0.0019 10 -2 8 0.0268 0.0039 10 -2 9 -0.0255 -0.0051 10 -2 10 -0.2677 0.0011 10 -2 12 -0.1458 0.0007 10 -2 13 -0.0408 -0.0017 10 -2 14 0.1106 0.0035 10 -2 15 -0.2958 -0.0054 10 -1 0 0.2548 -0.0050 10 -1 1 -0.0605 0.0138 10 -1 2 -0.0912 0.0002 10 -1 3 0.4259 -0.0099 10 -1 4 0.0134 -0.0003 10 -1 5 -0.5835 0.0123 10 -1 6 0.2191 -0.0114 10 -1 7 -0.2349 0.0031 10 -1 8 0.6379 0.0014 10 -1 9 -0.1496 0.0018 10 -1 10 -0.4204 -0.0057 10 -1 11 0.4006 0.0052 10 -1 12 -0.1675 -0.0027 10 -1 13 -0.1835 -0.0008 10 -1 14 0.0917 0.0015 10 -1 15 0.4505 0.0025 10 -1 16 -0.6071 -0.0042 10 -1 17 0.4895 0.0013 10 0 0 0.8656 -0.0544 10 0 1 -0.0476 0.0480 10 0 2 -0.4241 -0.0104 10 0 3 -0.2752 -0.0096 10 0 4 0.6225 -0.0037 10 0 5 -0.6343 0.0198 10 0 6 1.0042 -0.0152 10 0 7 -0.6048 0.0036 10 0 8 -0.1363 -0.0007 10 0 9 0.1813 0.0020 10 0 10 -0.3187 -0.0033 10 0 11 0.2667 0.0029 10 0 12 0.1552 0.0014 10 0 13 0.3428 -0.0017 10 0 14 -1.0878 -0.0023 10 0 15 0.9032 0.0008 10 0 16 -0.4787 0.0026 10 0 17 0.0507 -0.0025 10 0 18 0.3830 0.0043 10 0 19 -0.1144 -0.0060 10 1 0 0.4739 -0.0648 10 1 1 0.2661 0.0558 10 1 2 -0.4900 -0.0052 10 1 3 0.0232 -0.0234 10 1 4 0.8225 0.0071 10 1 5 -0.9528 0.0132 10 1 6 0.3808 -0.0099 10 1 7 -0.1947 -0.0027 10 1 8 -0.3889 0.0075 10 1 9 1.1584 -0.0046 10 1 10 -0.2694 0.0023 10 1 11 -0.7537 -0.0015 10 1 12 0.1352 -0.0013 10 1 13 0.6531 0.0007 10 1 14 -0.9469 0.0037 10 1 15 0.7579 -0.0050 10 1 16 0.4084 0.0058 10 1 17 -1.2599 -0.0055 10 1 18 0.8287 -0.0007 10 1 19 -0.3258 0.0027 10 1 20 0.2792 0.0042 10 2 0 -0.2411 -0.0821 10 2 1 1.1784 0.0692 10 2 2 -1.0160 -0.0171 10 2 3 -0.6423 -0.0187 10 2 4 1.4670 0.0120 10 2 5 -1.0169 0.0119 10 2 6 0.7292 -0.0160 10 2 7 -0.2154 0.0034 10 2 8 -0.4633 0.0002 10 2 9 0.4189 0.0036 10 2 10 -0.0114 -0.0042 10 2 11 -0.5814 0.0062 10 2 12 0.6582 -0.0079 10 2 13 0.3696 0.0039 10 2 14 -0.6061 0.0013 10 2 15 -0.3841 -0.0029 10 2 16 0.7190 -0.0001 10 2 17 -0.6708 0.0043 10 2 18 1.0051 -0.0042 10 2 19 -0.8691 0.0024 10 2 20 0.2775 0.0007 10 2 21 -0.0594 -0.0080 10 3 0 -0.5344 -0.1045 10 3 1 0.1857 0.0593 10 3 2 0.1874 -0.0024 10 3 3 -0.6948 -0.0232 10 3 4 1.5803 0.0101 10 3 5 -1.5467 0.0105 10 3 6 0.4234 -0.0175 10 3 7 -0.0147 0.0136 10 3 8 -0.1386 -0.0047 10 3 9 0.7995 -0.0004 10 3 10 -0.5201 -0.0023 10 3 11 -0.1482 0.0054 10 3 12 0.0401 -0.0063 10 3 13 -0.1271 0.0040 10 3 14 0.1891 0.0036 10 3 15 0.2029 -0.0063 10 3 16 -0.0045 0.0005 10 3 17 -0.4984 0.0017 10 3 18 0.4722 0.0019 10 3 19 -0.2873 -0.0056 10 3 20 0.2805 0.0082 10 3 21 -0.2602 -0.0105 10 3 22 0.0355 0.0124 10 4 0 0.3020 -0.0780 10 4 1 -0.2004 0.0190 10 4 2 0.1376 0.0182 10 4 3 -0.2201 -0.0191 10 4 4 0.1767 0.0066 10 4 5 -0.2474 0.0077 10 4 6 0.3648 -0.0180 10 4 7 0.2182 0.0119 10 4 8 -0.7873 0.0031 10 4 9 0.7314 -0.0079 10 4 10 -0.7599 0.0012 10 4 11 0.2932 0.0079 10 4 12 0.5050 -0.0099 10 4 13 -0.1232 0.0015 10 4 14 -0.3996 0.0084 10 4 15 0.0679 -0.0108 10 4 16 0.0210 0.0046 10 4 17 0.0340 0.0026 10 4 18 0.1576 0.0007 10 4 19 -0.1228 -0.0099 10 4 20 0.0576 0.0119 10 4 21 -0.2073 -0.0098 10 4 22 0.3565 0.0075 10 5 0 0.1100 -0.1085 10 5 1 -0.3360 0.0378 10 5 2 0.1738 0.0092 10 5 3 0.2841 -0.0172 10 5 4 -0.3300 0.0102 10 5 5 0.0204 0.0017 10 5 6 0.1308 -0.0141 10 5 7 -0.1047 0.0140 10 5 8 -0.3115 0.0015 10 5 9 0.6101 -0.0105 10 5 10 0.0012 -0.0023 10 5 11 -0.1473 0.0156 10 5 12 -0.5337 -0.0106 10 5 13 0.2290 0.0007 10 5 14 0.4054 0.0030 10 5 15 -0.0975 -0.0036 10 5 16 -0.1101 0.0003 10 5 17 -0.1536 0.0053 10 5 18 0.2041 -0.0047 10 5 19 0.1428 -0.0038 10 5 20 -0.3480 0.0099 10 5 21 -0.2134 -0.0034 10 5 22 0.5803 -0.0092 10 5 23 -0.1008 0.0144 10 6 0 0.8606 -0.1069 10 6 1 -0.5965 0.0176 10 6 2 0.4481 0.0426 10 6 3 -0.2002 -0.0492 10 6 4 -0.4315 0.0286 10 6 5 0.4969 -0.0104 10 6 6 0.1423 -0.0039 10 6 7 -0.0748 0.0096 10 6 8 -0.3019 0.0029 10 6 9 -0.1325 -0.0158 10 6 10 0.1859 0.0069 10 6 11 0.4943 0.0117 10 6 12 -0.5455 -0.0152 10 6 13 -0.1145 0.0042 10 6 14 0.7834 0.0011 10 6 15 -0.7437 0.0028 10 6 16 0.0427 -0.0030 10 6 17 0.0587 -0.0001 10 6 18 0.2380 0.0007 10 6 19 0.0246 -0.0012 10 6 20 -0.2352 0.0009 10 6 21 -0.0643 0.0034 10 6 22 0.6060 -0.0083 10 6 23 -0.7686 0.0110 10 7 0 0.7108 -0.0429 10 7 1 -0.7531 -0.0194 10 7 2 0.0092 0.0447 10 7 3 0.6954 -0.0362 10 7 4 -0.7610 0.0263 10 7 5 0.4811 -0.0160 10 7 6 -0.1234 -0.0014 10 7 7 -0.3329 0.0076 10 7 8 0.3568 0.0053 10 7 9 0.0025 -0.0147 10 7 10 0.1310 0.0031 10 7 11 -0.0988 0.0153 10 7 12 -0.3775 -0.0178 10 7 13 -0.2364 0.0072 10 7 14 1.1773 0.0003 10 7 15 -0.6047 -0.0008 10 7 16 -0.2798 -0.0008 10 7 17 0.0100 0.0002 10 7 18 0.4903 0.0027 10 7 19 -0.0027 -0.0032 10 7 20 -0.5965 0.0012 10 7 21 -0.2428 -0.0002 10 7 22 1.1424 -0.0005 10 7 23 -0.4146 0.0000 10 8 0 0.4572 -0.0633 10 8 1 -0.3472 0.0136 10 8 2 -0.2890 0.0169 10 8 3 0.7398 -0.0303 10 8 4 -0.7092 0.0274 10 8 5 0.3632 -0.0167 10 8 6 0.3750 0.0055 10 8 7 -0.8702 0.0036 10 8 8 0.4878 0.0001 10 8 9 -0.0073 -0.0108 10 8 10 -0.0962 0.0042 10 8 11 0.1596 0.0138 10 8 12 -0.1179 -0.0148 10 8 13 -0.1160 0.0016 10 8 14 0.3465 0.0027 10 8 15 -0.2531 0.0011 10 8 16 -0.0455 0.0005 10 8 17 -0.0120 -0.0018 10 8 18 0.0111 -0.0017 10 8 19 0.3736 -0.0025 10 8 20 -0.3486 0.0102 10 8 21 0.0295 -0.0061 10 8 22 0.0793 -0.0007 10 8 23 -0.1074 -0.0026 10 9 0 0.5151 -0.0512 10 9 1 -0.4417 -0.0304 10 9 2 -0.1296 0.0640 10 9 3 0.6462 -0.0562 10 9 4 -0.7986 0.0393 10 9 5 0.2980 -0.0266 10 9 6 0.3798 0.0128 10 9 7 -0.6428 -0.0035 10 9 8 0.4893 0.0085 10 9 9 0.0548 -0.0168 10 9 10 -0.4264 0.0095 10 9 11 0.2314 0.0077 10 9 12 -0.1582 -0.0132 10 9 13 0.1914 0.0057 10 9 14 0.2245 -0.0004 10 9 15 -0.4266 -0.0003 10 9 16 -0.0893 0.0013 10 9 17 0.4023 -0.0007 10 9 18 -0.0328 -0.0020 10 9 19 0.0300 0.0018 10 9 20 -0.6522 0.0034 10 9 21 0.6361 -0.0073 10 9 22 -0.1324 0.0037 10 9 23 0.1404 -0.0001 10 10 0 0.4947 -0.0090 10 10 1 -0.4780 -0.0450 10 10 2 -0.0650 0.0606 10 10 3 0.7062 -0.0440 10 10 4 -0.5746 0.0296 10 10 5 0.1683 -0.0260 10 10 6 0.1488 0.0152 10 10 7 -0.6443 -0.0000 10 10 8 0.6470 0.0013 10 10 9 -0.0548 -0.0134 10 10 10 -0.1699 0.0087 10 10 11 0.0673 0.0130 10 10 12 -0.1441 -0.0206 10 10 13 0.1144 0.0074 10 10 14 0.1761 -0.0005 10 10 15 -0.2384 0.0044 10 10 16 -0.0505 -0.0005 10 10 17 0.1253 -0.0034 10 10 18 0.1311 -0.0057 10 10 19 -0.1360 0.0080 10 10 20 -0.3065 0.0032 10 10 21 0.6543 -0.0047 10 10 22 -0.3255 -0.0008 10 11 0 0.8143 -0.0652 10 11 1 -0.4803 0.0198 10 11 2 0.0733 0.0249 10 11 3 -0.0794 -0.0465 10 11 4 -0.3831 0.0397 10 11 5 0.3149 -0.0224 10 11 6 0.7804 0.0129 10 11 7 -0.9579 -0.0026 10 11 8 0.1721 -0.0041 10 11 9 -0.0408 -0.0080 10 11 10 0.2383 0.0152 10 11 11 -0.0419 0.0042 10 11 12 -0.1355 -0.0202 10 11 13 0.1545 0.0100 10 11 14 -0.1364 0.0026 10 11 15 -0.0129 0.0026 10 11 16 0.1334 -0.0093 10 11 17 -0.1516 0.0018 10 11 18 0.2184 0.0054 10 11 19 -0.0552 0.0015 10 11 20 -0.4065 -0.0077 10 11 21 0.4749 0.0016 10 11 22 -0.0649 0.0028 10 12 0 0.3198 -0.0558 10 12 1 -0.4598 0.0101 10 12 2 0.5155 0.0454 10 12 3 0.0948 -0.0589 10 12 4 -0.1776 0.0406 10 12 5 -0.3702 -0.0294 10 12 6 0.5796 0.0194 10 12 7 -0.5939 -0.0085 10 12 8 0.4156 0.0105 10 12 9 -0.0354 -0.0147 10 12 10 0.1944 0.0085 10 12 11 -0.4415 0.0031 10 12 12 -0.1210 -0.0108 10 12 13 0.6787 0.0085 10 12 14 -0.4922 -0.0039 10 12 15 0.1401 0.0057 10 12 16 0.0335 -0.0057 10 12 17 -0.0652 0.0019 10 12 18 -0.1277 -0.0031 10 12 19 0.3019 0.0037 10 12 20 -0.2656 -0.0011 10 12 21 0.2139 0.0057 10 13 0 0.5861 -0.0214 10 13 1 -0.2397 0.0130 10 13 2 -0.2145 0.0115 10 13 3 -0.0560 -0.0312 10 13 4 0.1180 0.0298 10 13 5 0.1453 -0.0198 10 13 6 0.2692 0.0213 10 13 7 -0.5445 -0.0156 10 13 8 0.1774 -0.0014 10 13 9 -0.3677 -0.0001 10 13 10 0.6957 0.0090 10 13 11 0.1724 0.0014 10 13 12 -1.2226 -0.0122 10 13 13 1.0201 0.0062 10 13 14 -0.3990 0.0003 10 13 15 0.4372 0.0044 10 13 16 -0.4698 -0.0116 10 13 17 -0.0265 0.0095 10 13 18 0.1433 -0.0023 10 13 19 0.3039 0.0023 10 14 0 0.3986 -0.0550 10 14 1 0.1921 0.0372 10 14 2 -0.4155 -0.0050 10 14 3 0.5796 -0.0184 10 14 4 -0.3627 0.0237 10 14 5 0.0158 -0.0187 10 14 6 -0.1345 0.0056 10 14 7 -0.0706 0.0008 10 14 8 0.7538 0.0049 10 14 9 -0.6319 -0.0058 10 14 10 -0.3289 0.0033 10 14 12 -1.1770 -0.0006 10 14 13 0.8831 0.0069 10 14 14 -0.5138 -0.0066 10 14 15 0.4761 0.0040 10 14 16 -0.4523 -0.0027 10 14 17 0.0102 0.0052 10 15 0 0.0915 -0.0365 10 15 1 -0.1528 0.0007 10 15 2 -0.0640 0.0285 10 15 3 0.1394 -0.0277 10 15 4 -0.0980 0.0078 10 15 5 0.0876 -0.0031 10 15 6 0.2361 0.0161 10 15 7 -0.6573 -0.0123 10 15 8 0.5239 -0.0010 10 15 9 0.0888 -0.0054 10 15 10 -0.5296 0.0106 10 15 11 0.5374 -0.0003 10 15 12 -0.4663 -0.0041 10 15 13 0.4966 0.0034 10 15 14 -0.4837 -0.0053 10 16 0 0.5155 -0.0033 10 16 1 -1.1302 -0.0169 10 16 2 0.9763 0.0120 10 16 3 -0.3749 -0.0036 10 16 4 0.1885 0.0163 10 16 5 -0.3019 -0.0199 10 16 6 0.2073 0.0036 10 16 7 -0.1537 -0.0045 11 -5 0 -1.4455 -0.0037 11 -5 1 0.4405 0.0066 11 -4 0 -0.4913 -0.0094 11 -4 1 0.2910 0.0052 11 -4 2 0.1374 -0.0066 11 -4 3 -0.2580 0.0018 11 -4 4 -0.3316 0.0034 11 -4 5 0.1413 -0.0029 11 -3 0 -0.1965 -0.0020 11 -3 1 0.1468 -0.0062 11 -3 2 -0.2626 0.0089 11 -3 3 0.5993 -0.0054 11 -3 4 -0.1606 0.0053 11 -3 5 0.0590 -0.0064 11 -3 6 -0.4892 0.0038 11 -3 7 0.2840 -0.0029 11 -3 8 -0.2173 0.0012 11 -2 0 -0.0564 0.0050 11 -2 1 1.2016 -0.0070 11 -2 2 -0.9970 0.0021 11 -2 3 0.0327 -0.0024 11 -2 4 -0.1418 0.0077 11 -2 5 0.3072 -0.0062 11 -2 6 -0.0624 -0.0014 11 -2 8 -0.2623 -0.0043 11 -2 9 -0.1880 -0.0001 11 -2 10 0.0132 0.0010 11 -2 11 0.1113 -0.0017 11 -1 0 -0.2886 0.0127 11 -1 1 0.6008 0.0053 11 -1 2 -0.5328 -0.0067 11 -1 3 0.3463 -0.0056 11 -1 4 0.0340 0.0139 11 -1 5 0.0873 -0.0101 11 -1 6 -0.4891 -0.0018 11 -1 7 0.4198 0.0073 11 -1 8 -0.3404 -0.0009 11 -1 9 0.1358 -0.0071 11 -1 11 0.4144 0.0019 11 -1 12 -0.9019 -0.0056 11 -1 13 0.4383 0.0022 11 -1 14 0.0186 -0.0009 11 0 0 0.2675 0.0234 11 0 1 -0.0319 0.0111 11 0 2 -0.4221 -0.0134 11 0 3 0.5133 -0.0091 11 0 4 -0.5661 0.0203 11 0 5 0.2153 -0.0101 11 0 6 -0.0340 0.0000 11 0 7 0.4861 0.0005 11 0 8 -0.3222 0.0024 11 0 9 -0.1078 -0.0029 11 0 10 -0.2457 -0.0008 11 0 11 0.5493 0.0022 11 0 12 -0.4594 0.0010 11 0 13 0.1215 -0.0018 11 0 14 0.4897 -0.0010 11 0 15 -0.3437 0.0037 11 0 16 -0.4489 -0.0046 11 1 0 0.6048 0.0231 11 1 1 -1.0896 0.0235 11 1 2 -0.0979 -0.0243 11 1 3 0.6818 -0.0043 11 1 4 0.0511 0.0161 11 1 5 -0.2421 -0.0051 11 1 6 0.2907 -0.0033 11 1 7 -0.9362 0.0011 11 1 8 0.4973 -0.0024 11 1 9 0.6172 0.0071 11 1 10 -0.7833 -0.0029 11 1 11 0.4589 -0.0036 11 1 12 0.2165 0.0028 11 1 13 -0.6909 0.0006 11 1 14 -0.2354 -0.0061 11 1 15 1.1592 0.0095 11 1 16 -0.8658 -0.0014 11 1 17 0.5013 -0.0079 11 2 0 1.2893 0.0398 11 2 1 -0.8822 0.0208 11 2 2 -0.1181 -0.0304 11 2 3 0.6122 0.0005 11 2 4 -0.3975 0.0127 11 2 5 -0.4095 0.0004 11 2 6 0.8514 -0.0059 11 2 7 -0.6328 -0.0000 11 2 8 0.3241 -0.0007 11 2 9 0.8017 0.0039 11 2 10 -1.7319 0.0008 11 2 11 0.3241 -0.0077 11 2 12 1.0866 0.0059 11 2 13 -0.2329 0.0030 11 2 14 -0.8623 -0.0054 11 2 15 1.1676 -0.0013 11 2 16 -1.0365 0.0070 11 2 17 0.1722 -0.0091 11 2 18 0.4149 0.0049 11 2 19 0.0018 0.0075 11 3 0 0.4439 0.0325 11 3 1 -0.0996 0.0351 11 3 2 -1.1495 -0.0442 11 3 3 1.4620 0.0185 11 3 4 -0.1602 -0.0035 11 3 5 -0.5427 0.0047 11 3 6 0.4563 -0.0056 11 3 7 -0.8222 0.0008 11 3 8 0.5828 0.0003 11 3 9 0.3221 0.0039 11 3 10 -0.5356 -0.0002 11 3 11 0.1937 -0.0077 11 3 12 0.4659 0.0042 11 3 13 -0.6380 0.0025 11 3 14 -0.4794 -0.0007 11 3 15 0.9448 -0.0025 11 3 16 0.0085 0.0021 11 3 17 -0.3763 0.0001 11 3 18 0.0856 -0.0050 11 3 19 -0.1886 0.0113 11 3 20 0.2674 -0.0152 11 4 0 -0.1063 -0.0036 11 4 1 0.3909 0.0510 11 4 2 -0.2965 -0.0479 11 4 3 0.2806 0.0225 11 4 4 -0.1305 -0.0088 11 4 5 -0.6611 0.0055 11 4 6 1.1734 0.0008 11 4 7 -1.0097 -0.0035 11 4 8 1.1023 -0.0025 11 4 9 -0.6283 0.0029 11 4 10 -0.6074 0.0049 11 4 11 0.5576 -0.0074 11 4 12 0.1811 0.0029 11 4 13 -0.0782 0.0023 11 4 14 0.0861 -0.0035 11 4 15 -0.1896 0.0001 11 4 16 -0.1105 -0.0002 11 4 17 -0.0935 0.0040 11 4 18 0.4864 -0.0050 11 4 19 -0.2116 0.0068 11 4 20 -0.1607 -0.0096 11 5 0 0.2778 0.0127 11 5 1 -0.4383 0.0285 11 5 2 0.2407 -0.0322 11 5 3 0.0171 0.0209 11 5 4 -0.0344 -0.0140 11 5 5 -0.0006 0.0059 11 5 6 0.4309 0.0029 11 5 7 -1.0651 -0.0026 11 5 8 0.6687 -0.0019 11 5 9 0.2496 0.0015 11 5 10 -0.5455 0.0031 11 5 11 0.6335 -0.0053 11 5 12 -0.3082 0.0009 11 5 13 -0.3923 0.0034 11 5 14 0.2649 -0.0006 11 5 15 0.1437 -0.0040 11 5 16 -0.0109 0.0049 11 5 17 -0.0610 -0.0027 11 5 18 0.0597 -0.0006 11 5 19 0.0232 0.0002 11 5 20 -0.3782 0.0024 11 5 21 0.4025 -0.0028 11 6 0 -0.1646 0.0051 11 6 1 0.3403 0.0423 11 6 2 0.1002 -0.0498 11 6 3 -0.1590 0.0460 11 6 4 -0.2977 -0.0395 11 6 5 0.3395 0.0211 11 6 6 0.1315 -0.0043 11 6 7 -0.3325 0.0048 11 6 8 0.1295 -0.0117 11 6 9 0.2781 0.0085 11 6 10 -0.4226 -0.0005 11 6 11 -0.0082 -0.0000 11 6 12 -0.0979 -0.0003 11 6 13 0.7252 -0.0045 11 6 14 -0.3058 0.0054 11 6 15 -0.3267 -0.0021 11 6 16 -0.1569 0.0025 11 6 17 0.5747 -0.0050 11 6 18 -0.1327 0.0059 11 6 19 -0.2395 -0.0053 11 6 20 -0.2338 0.0044 11 6 21 0.7635 -0.0049 11 7 0 -0.1186 -0.0168 11 7 1 -0.1187 0.0292 11 7 2 0.2252 -0.0431 11 7 3 -0.3706 0.0543 11 7 4 0.3042 -0.0469 11 7 5 0.1121 0.0230 11 7 6 -0.2399 -0.0023 11 7 7 0.0194 0.0003 11 7 8 -0.2524 -0.0080 11 7 9 0.4534 0.0068 11 7 10 0.0358 0.0017 11 7 11 0.0344 -0.0058 11 7 12 -0.9141 0.0053 11 7 13 1.0064 -0.0062 11 7 14 -0.1121 0.0076 11 7 15 -0.5326 -0.0036 11 7 16 0.2468 -0.0011 11 7 17 0.1943 -0.0034 11 7 18 0.2015 0.0105 11 7 19 -0.5334 -0.0086 11 7 20 0.0095 0.0013 11 7 21 0.3484 0.0037 11 7 22 -0.1461 -0.0031 11 8 0 0.0607 0.0286 11 8 1 -0.2088 -0.0230 11 8 2 0.3937 -0.0072 11 8 3 -0.2416 0.0459 11 8 4 -0.0111 -0.0546 11 8 5 0.2723 0.0230 11 8 6 -0.4080 0.0055 11 8 7 0.3195 -0.0017 11 8 8 -0.2139 -0.0091 11 8 9 0.2629 0.0054 11 8 10 -0.2636 0.0000 11 8 11 0.1228 0.0012 11 8 12 -0.3073 0.0013 11 8 13 0.4907 -0.0076 11 8 14 0.2326 0.0062 11 8 15 -1.0201 -0.0009 11 8 16 0.7683 0.0012 11 8 17 -0.2739 -0.0019 11 8 18 0.3520 0.0002 11 8 19 -0.5548 -0.0005 11 8 20 0.1678 -0.0014 11 8 21 0.4069 0.0055 11 8 22 -0.0818 -0.0028 11 9 0 -0.0512 0.0107 11 9 1 -0.1018 -0.0128 11 9 2 0.2174 -0.0100 11 9 3 -0.0561 0.0519 11 9 4 -0.1922 -0.0644 11 9 5 0.2544 0.0354 11 9 6 -0.3093 -0.0061 11 9 7 0.1402 0.0059 11 9 8 0.2410 -0.0167 11 9 9 -0.1023 0.0138 11 9 10 -0.2599 -0.0050 11 9 11 0.0986 0.0032 11 9 12 0.0821 -0.0004 11 9 13 0.0863 -0.0067 11 9 14 0.0954 0.0057 11 9 15 -0.6559 0.0027 11 9 16 0.6473 -0.0028 11 9 17 -0.1685 -0.0034 11 9 18 0.0790 -0.0014 11 9 19 -0.0812 0.0104 11 9 20 -0.1059 -0.0035 11 9 21 0.0135 -0.0075 11 10 0 0.0473 -0.0106 11 10 1 -0.3791 -0.0168 11 10 2 0.1315 0.0079 11 10 3 0.0691 0.0356 11 10 4 0.0635 -0.0551 11 10 5 0.2554 0.0308 11 10 6 -0.4433 -0.0015 11 10 7 -0.1296 -0.0008 11 10 8 0.3898 -0.0103 11 10 9 0.0233 0.0087 11 10 10 -0.2600 0.0019 11 10 11 0.1802 -0.0045 11 10 12 -0.2200 0.0043 11 10 13 0.3763 -0.0076 11 10 14 -0.2126 0.0039 11 10 15 -0.3030 0.0023 11 10 16 0.4041 0.0036 11 10 17 0.2066 -0.0094 11 10 18 -0.5179 0.0015 11 10 19 -0.0394 0.0048 11 10 20 0.3622 0.0000 11 10 21 0.1457 -0.0048 11 11 0 0.1714 0.0478 11 11 1 -0.0156 -0.0421 11 11 2 -0.0496 0.0132 11 11 3 -0.0347 0.0264 11 11 4 -0.2779 -0.0462 11 11 5 0.2341 0.0208 11 11 6 0.0205 0.0141 11 11 7 0.0799 -0.0079 11 11 8 0.1390 -0.0154 11 11 9 -0.3570 0.0108 11 11 10 -0.1824 0.0060 11 11 11 0.5073 -0.0062 11 11 12 -0.2118 0.0013 11 11 13 0.2115 -0.0083 11 11 14 -0.2959 0.0144 11 11 15 -0.0785 -0.0048 11 11 16 0.1926 -0.0023 11 11 17 0.2294 -0.0087 11 11 18 -0.2883 0.0126 11 11 19 -0.2034 0.0021 11 11 20 0.4008 -0.0062 11 12 0 -0.3896 0.0450 11 12 1 -0.0760 -0.0235 11 12 2 -0.0410 -0.0113 11 12 3 0.0998 0.0422 11 12 4 0.4047 -0.0396 11 12 5 -0.1045 0.0177 11 12 6 -0.2616 -0.0051 11 12 7 -0.6320 0.0023 11 12 8 0.8854 -0.0097 11 12 9 0.1821 0.0166 11 12 10 -0.4181 -0.0040 11 12 11 -0.1674 -0.0110 11 12 12 0.0809 0.0098 11 12 13 0.2853 -0.0087 11 12 14 -0.2261 0.0128 11 12 15 0.0186 -0.0088 11 12 16 0.1148 0.0004 11 12 17 -0.1447 0.0011 11 12 18 0.1327 0.0054 11 12 19 -0.1930 -0.0104 11 13 0 -0.1283 0.0442 11 13 1 0.2534 -0.0318 11 13 2 0.2082 -0.0010 11 13 3 -0.7739 0.0273 11 13 4 0.3428 -0.0435 11 13 5 -0.1522 0.0311 11 13 6 0.8182 0.0018 11 13 7 -0.8165 -0.0056 11 13 8 0.1341 -0.0115 11 13 9 0.0824 0.0073 11 13 10 0.1583 0.0054 11 13 11 -0.5066 -0.0052 11 13 12 0.5525 0.0039 11 13 13 -0.0003 -0.0092 11 13 14 -0.4109 0.0137 11 13 15 0.1334 -0.0077 11 13 16 0.2843 -0.0019 11 13 17 -0.3610 -0.0023 11 13 18 0.0802 0.0112 11 14 0 -0.0074 0.0671 11 14 1 -0.2197 -0.0410 11 14 2 0.4350 0.0009 11 14 3 -0.1900 0.0305 11 14 4 0.4541 -0.0340 11 14 5 -0.7061 0.0179 11 14 6 0.2572 -0.0035 11 14 7 -0.0863 -0.0037 11 14 8 0.1737 -0.0040 11 14 9 -0.0751 0.0148 11 14 10 0.6752 -0.0040 11 14 11 -1.4709 -0.0081 11 14 12 0.7777 0.0014 11 14 13 0.5504 0.0002 11 14 14 -0.5675 0.0094 11 14 15 -0.1735 -0.0111 11 14 16 0.1669 0.0053 11 15 0 0.3252 0.0180 11 15 1 -0.0668 -0.0010 11 15 2 -0.2393 -0.0078 11 15 3 0.0967 0.0170 11 15 4 -0.0782 -0.0259 11 15 5 0.1290 0.0189 11 15 6 -0.0128 -0.0048 11 15 7 0.1533 0.0103 11 15 8 -0.1347 -0.0176 11 15 9 -0.5811 0.0068 11 15 10 1.1208 -0.0008 11 15 11 -0.7724 0.0034 11 15 12 0.0590 0.0003 12 -3 0 -0.3709 -0.0060 12 -3 1 -0.2661 -0.0042 12 -3 2 0.1950 0.0055 12 -3 3 -0.0896 0.0039 12 -3 4 0.3356 -0.0066 12 -2 0 0.9749 -0.0104 12 -2 1 -0.4209 -0.0038 12 -2 2 0.3055 0.0085 12 -2 3 -0.3329 -0.0017 12 -2 4 -0.0240 -0.0067 12 -2 5 -0.1056 0.0039 12 -2 6 0.2088 0.0032 12 -2 7 0.0365 -0.0025 12 -1 0 1.0692 -0.0086 12 -1 1 -0.6743 -0.0032 12 -1 2 -0.2700 0.0067 12 -1 3 0.3745 0.0012 12 -1 4 0.1537 -0.0029 12 -1 5 -0.1978 -0.0030 12 -1 6 0.3973 0.0021 12 -1 7 -0.6732 0.0058 12 -1 8 0.2918 -0.0092 12 -1 9 -0.2268 0.0033 12 -1 10 0.6041 0.0031 12 0 0 0.4148 0.0036 12 0 1 -0.4354 -0.0086 12 0 2 -0.1169 0.0012 12 0 3 0.5110 -0.0008 12 0 4 -0.1291 0.0039 12 0 5 -0.8474 -0.0008 12 0 6 1.0980 -0.0053 12 0 7 -0.5939 0.0090 12 0 8 0.1911 -0.0056 12 0 9 -0.0461 -0.0023 12 0 10 0.5185 0.0041 12 0 11 -0.8134 0.0025 12 0 12 -0.2167 -0.0079 12 0 13 0.9924 0.0031 12 1 0 -0.6902 0.0170 12 1 1 -0.2842 -0.0126 12 1 2 -0.0564 0.0039 12 1 3 0.5450 -0.0041 12 1 4 -0.2786 0.0054 12 1 5 -0.1558 0.0034 12 1 6 0.6083 -0.0113 12 1 7 -0.4549 0.0047 12 1 8 -0.2191 0.0044 12 1 9 0.0257 -0.0032 12 1 10 0.3395 -0.0042 12 1 11 0.0928 0.0093 12 1 12 -0.3992 -0.0046 12 1 13 0.5060 -0.0064 12 1 14 -0.3881 0.0077 12 1 15 -0.3532 0.0019 12 2 0 -1.5691 0.0108 12 2 1 0.0073 -0.0043 12 2 2 0.6568 -0.0010 12 2 3 0.3261 -0.0070 12 2 4 -0.6494 0.0095 12 2 5 -0.1903 0.0040 12 2 6 0.1994 -0.0113 12 2 7 -0.1731 0.0004 12 2 8 0.9939 0.0092 12 2 9 -0.5912 -0.0013 12 2 10 -0.6299 -0.0089 12 2 11 0.7044 0.0043 12 2 12 -0.2229 0.0033 12 2 13 -0.3154 -0.0023 12 2 14 0.5198 -0.0012 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0.0058 14 2 8 0.5860 -0.0051 14 2 9 0.0721 -0.0052 14 2 10 -0.5053 0.0126 14 3 0 -0.0294 0.0022 14 3 1 0.3980 0.0063 14 3 2 0.4749 -0.0084 14 3 3 -0.9192 0.0020 14 3 4 -0.2853 0.0081 14 3 5 0.9849 -0.0100 14 3 6 -0.5216 0.0019 14 3 7 0.2769 0.0028 14 3 8 0.0063 0.0054 14 3 9 -0.1633 -0.0146 14 3 10 -0.2687 0.0092 14 3 11 0.1710 0.0018 14 4 0 0.0440 0.0045 14 4 1 -0.3847 0.0003 14 4 2 -0.0946 -0.0010 14 4 3 0.4432 -0.0067 14 4 4 0.1518 0.0118 14 4 5 -0.1973 -0.0072 14 4 6 -0.3956 -0.0008 14 4 7 0.4066 0.0008 14 4 8 -0.4508 0.0069 14 4 9 0.2868 -0.0074 14 4 10 0.6160 -0.0034 14 4 11 -0.5381 0.0102 14 4 12 -0.3008 -0.0026 14 4 13 0.0993 -0.0075 14 5 0 0.0964 0.0018 14 5 1 -0.0850 -0.0021 14 5 2 0.1109 0.0003 14 5 3 -0.2000 -0.0010 14 5 4 0.0411 0.0014 14 5 5 -0.3228 0.0029 14 5 6 0.6401 -0.0069 14 5 7 0.1911 0.0034 14 5 8 -0.7869 0.0033 14 5 9 0.1353 -0.0013 14 5 10 0.3605 -0.0093 14 5 11 -0.1645 0.0114 14 5 12 -0.4606 0.0012 14 5 13 0.8566 -0.0076 14 5 14 -0.0733 -0.0041 14 6 0 -0.6901 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-0.0614 0.0065 14 8 14 -0.7329 -0.0060 14 8 15 0.9493 0.0074 14 9 0 -0.2053 -0.0115 14 9 1 0.7005 -0.0054 14 9 2 -0.5879 0.0146 14 9 3 0.1450 -0.0170 14 9 4 0.2917 0.0107 14 9 5 -0.2470 -0.0022 14 9 6 0.2054 0.0041 14 9 7 -0.4681 -0.0125 14 9 8 0.2647 0.0128 14 9 9 0.0929 -0.0055 14 9 10 0.2151 0.0019 14 9 11 -0.5078 -0.0009 14 9 12 0.1772 -0.0032 14 9 13 0.2185 0.0055 14 9 14 -0.4239 -0.0042 14 9 15 0.5555 0.0033 14 10 0 -0.2501 -0.0208 14 10 1 0.5258 -0.0030 14 10 2 -0.1558 0.0203 14 10 3 -0.4173 -0.0229 14 10 4 0.2202 0.0104 14 10 5 -0.0805 0.0020 14 10 6 0.2357 0.0029 14 10 7 0.2433 -0.0161 14 10 8 -0.5642 0.0158 14 10 9 -0.0303 -0.0054 14 10 10 0.5045 0.0026 14 10 11 -0.5309 -0.0037 14 10 12 0.5368 -0.0029 14 10 13 -0.2116 0.0083 14 10 14 -0.2839 -0.0036 14 10 15 0.2151 -0.0001 14 11 0 0.1277 -0.0158 14 11 1 -0.1305 -0.0088 14 11 2 -0.0981 0.0218 14 11 3 0.1575 -0.0240 14 11 4 0.2234 0.0167 14 11 5 -0.0960 -0.0014 14 11 6 -0.3314 -0.0004 14 11 7 0.1404 -0.0159 14 11 8 -0.0474 0.0192 14 11 9 -0.0041 -0.0035 14 11 10 0.9213 -0.0014 14 11 11 -1.3314 -0.0048 14 11 12 0.3074 -0.0019 14 11 13 0.3378 0.0138 14 11 14 0.0303 -0.0088 14 12 0 0.1244 -0.0143 14 12 1 0.4776 0.0080 14 12 2 -0.3735 0.0210 14 12 3 -0.2626 -0.0378 14 12 4 0.2119 0.0151 14 12 5 -0.1514 0.0050 14 12 6 0.4398 0.0076 14 12 7 -0.0243 -0.0195 14 12 8 -0.3421 0.0100 14 12 9 -0.3180 0.0003 14 12 10 0.7651 0.0029 14 12 11 -0.4082 -0.0066 14 12 12 0.0423 -0.0037 14 12 13 0.1354 0.0143 14 13 0 -0.2825 -0.0331 14 13 1 0.2373 0.0134 14 13 2 0.3560 0.0156 14 13 3 -0.6259 -0.0235 14 13 4 0.6084 0.0131 14 13 5 -0.0769 0.0002 14 13 6 -0.4057 0.0045 14 13 7 -0.0554 -0.0239 14 13 8 0.1789 0.0183 14 13 9 0.5361 0.0061 14 13 10 -0.2747 -0.0038 14 13 11 -0.5924 -0.0123 14 14 0 0.4398 -0.0175 14 14 1 -0.2238 0.0133 14 14 2 0.6302 0.0055 14 14 3 -0.8869 -0.0211 14 14 4 -0.1123 0.0095 14 14 5 0.6210 -0.0055 14 14 6 0.2731 0.0265 14 14 7 -0.4209 -0.0255 14 14 8 -0.3643 0.0014 15 2 0 -0.0841 -0.0109 15 2 1 0.7892 0.0053 15 2 2 -0.6670 0.0068 15 2 3 -0.3355 -0.0059 15 2 4 0.7027 -0.0004 15 3 1 0.8259 -0.0121 15 3 2 -0.1735 0.0048 15 3 3 -0.6355 0.0007 15 3 4 0.6851 0.0008 15 3 5 -0.0320 -0.0055 15 3 6 -1.1001 0.0065 15 3 7 1.2401 0.0021 15 4 0 -0.2227 0.0269 15 4 1 -0.2247 -0.0080 15 4 2 0.1503 -0.0111 15 4 3 -0.3570 0.0109 15 4 4 0.4833 0.0012 15 4 5 0.3168 -0.0075 15 4 6 -0.5116 0.0013 15 4 7 -0.1229 0.0075 15 4 8 0.0154 -0.0061 15 4 9 0.2011 -0.0045 15 5 0 -0.4111 0.0259 15 5 1 -0.2775 -0.0032 15 5 2 0.9693 -0.0172 15 5 3 -0.1233 0.0108 15 5 4 -0.9552 0.0092 15 5 5 0.1037 -0.0114 15 5 6 0.9329 -0.0027 15 5 7 -0.5165 0.0075 15 5 8 0.0356 0.0032 15 5 10 -0.3186 0.0041 15 6 0 0.1448 0.0303 15 6 1 -0.5162 -0.0065 15 6 2 0.4722 -0.0157 15 6 3 0.0880 0.0090 15 6 4 -0.2126 0.0102 15 6 5 -0.0524 -0.0099 15 6 6 0.6381 -0.0059 15 6 7 -1.1447 0.0092 15 6 8 0.4959 0.0033 15 6 9 0.4165 -0.0084 15 6 10 -0.3507 -0.0015 15 6 11 0.0476 0.0107 15 7 0 0.8605 0.0298 15 7 1 0.4856 -0.0057 15 7 2 -0.2705 -0.0160 15 7 3 -0.6001 0.0146 15 7 4 0.3102 0.0014 15 7 5 0.0435 -0.0056 15 7 6 0.4830 -0.0049 15 7 7 -0.6045 0.0087 15 7 8 0.1375 -0.0003 15 7 9 0.2718 -0.0032 15 7 10 -0.6840 -0.0046 15 7 11 0.7622 0.0095 15 7 12 -0.3549 -0.0028 15 8 0 0.5068 0.0246 15 8 1 0.6762 -0.0071 15 8 2 -0.6129 -0.0172 15 8 3 -0.1920 0.0207 15 8 4 0.5645 -0.0080 15 8 5 -0.1552 0.0020 15 8 6 -0.4075 -0.0042 15 8 7 0.2779 0.0040 15 8 8 -0.0604 -0.0010 15 8 9 0.5137 0.0016 15 8 10 -0.8667 -0.0038 15 8 11 0.5353 0.0017 15 8 12 0.0610 0.0025 15 9 0 0.5187 0.0206 15 9 1 0.2453 -0.0097 15 9 2 -0.7739 -0.0127 15 9 3 0.2310 0.0229 15 9 5 0.3434 0.0078 15 9 6 -0.5044 -0.0075 15 9 7 0.2254 0.0030 15 9 8 -0.4068 0.0021 15 9 9 0.4933 0.0017 15 9 10 -0.1652 -0.0053 15 9 11 0.0084 0.0007 15 9 12 0.1706 0.0048 15 10 0 0.2364 0.0186 15 10 1 0.5764 -0.0070 15 10 2 -0.8672 -0.0075 15 10 3 0.4870 0.0144 15 10 4 -0.0813 -0.0114 15 10 5 -0.1294 0.0104 15 10 6 -0.1224 -0.0124 15 10 7 0.3597 0.0065 15 10 8 -0.1038 0.0026 15 10 9 0.1760 -0.0012 15 10 10 -0.5590 -0.0051 15 10 11 0.2012 0.0016 15 10 12 0.4678 0.0066 15 11 0 -0.6344 0.0130 15 11 1 0.4786 0.0020 15 11 2 -0.3944 -0.0137 15 11 3 -0.1658 0.0105 15 11 4 0.6532 -0.0050 15 11 5 -0.0789 0.0132 15 11 6 -0.3706 -0.0205 15 11 7 0.1628 0.0094 15 11 8 -0.6058 0.0035 15 11 9 1.1431 0.0008 15 11 10 -0.6178 -0.0071 15 11 11 0.0063 -0.0011 15 12 0 -0.2260 0.0116 15 12 1 -0.2885 0.0112 15 12 2 0.4788 -0.0191 15 12 3 -0.1899 0.0113 15 12 4 -0.1355 -0.0043 15 12 5 0.0632 0.0073 15 12 6 -0.3634 -0.0148 15 12 7 0.9795 0.0112 15 12 8 -0.8525 -0.0002 15 12 9 0.5137 0.0022 15 13 0 0.1992 0.0215 15 13 1 -0.2301 0.0069 15 13 2 -0.2946 -0.0240 15 13 3 0.3116 0.0041 15 13 4 0.1674 0.0101 15 13 5 0.1259 0.0131 15 13 6 -0.5372 -0.0244 15 13 7 0.1510 0.0014 16 5 0 -0.5710 0.0115 16 5 1 0.7172 -0.0248 16 5 2 0.4173 0.0115 16 5 3 -0.6298 0.0054 16 6 0 -0.8571 0.0218 16 6 1 0.7748 -0.0292 16 6 2 0.0621 0.0066 16 6 3 -0.9023 0.0130 16 6 4 0.3351 -0.0036 16 6 5 0.8159 -0.0125 16 7 0 -0.3417 0.0187 16 7 1 0.5795 -0.0294 16 7 2 0.0182 0.0067 16 7 3 -0.5470 0.0148 16 7 4 0.1282 -0.0039 16 7 5 0.1015 -0.0147 16 7 6 0.0744 0.0085 16 8 0 0.9245 0.0150 16 8 1 -0.5154 -0.0305 16 8 2 -0.4445 0.0152 16 8 3 0.1710 0.0056 16 8 4 0.7767 -0.0035 16 8 5 -0.5074 -0.0099 16 8 7 -0.2134 -0.0008 16 9 0 1.0427 0.0070 16 9 1 -0.7574 -0.0316 16 9 2 -0.1663 0.0265 16 9 3 0.1193 -0.0039 16 9 4 0.3749 -0.0028 16 9 5 -0.5155 -0.0032 16 9 6 0.3507 0.0031 16 10 0 0.7432 0.0002 16 10 1 -1.0102 -0.0205 16 10 2 0.3240 0.0216 16 10 3 0.3684 -0.0061 16 10 4 -0.0112 -0.0030 16 10 5 -0.4203 0.0011 16 10 6 -0.0396 -0.0018 16 11 0 0.5615 0.0012 16 11 1 -0.3744 -0.0087 16 11 2 -0.4451 0.0091 16 11 3 0.6048 -0.0055 16 11 4 -0.1939 0.0044 16 11 5 0.0399 -0.0045 0 0 0 0.0 0.0 ; _shelx_fab_checksum 13215 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 0.99948(8) -0.06050(10) 0.23856(4) 0.0796(3) Uani 1 1 d . . . . . Cl2 Cl 0.80077(11) 0.29033(11) 0.19754(5) 0.0896(3) Uani 1 1 d . . . . . Cl3 Cl 0.87828(9) 0.04122(9) 0.07181(4) 0.0740(2) Uani 1 1 d . . . . . Cl4 Cl 0.79000(10) -0.18856(7) 0.20333(4) 0.0770(3) Uani 1 1 d . . . . . Cl5 Cl 0.60778(9) 0.35236(7) 0.05900(3) 0.0684(2) Uani 1 1 d . . . . . Cl6 Cl 0.59970(9) 0.01307(7) 0.06257(3) 0.0662(2) Uani 1 1 d . . . . . Cl7 Cl 0.48969(8) 0.02285(8) 0.24455(4) 0.0650(2) Uani 1 1 d . . . . . Cl8 Cl 0.49895(10) 0.35781(7) 0.24076(4) 0.0746(3) Uani 1 1 d . . . . . Cl9 Cl 0.34782(8) 0.29661(9) 0.11332(4) 0.0788(3) Uani 1 1 d . . . . . S1 S 0.69373(8) 0.07050(8) 0.32888(3) 0.0585(2) Uani 1 1 d . . . . . O1 O 0.9790(3) 0.1346(3) 0.55384(17) 0.1104(10) Uani 1 1 d . . . . . O2 O 0.6429(4) 0.4510(3) 0.43301(16) 0.1197(12) Uani 1 1 d . . . . . O3 O 1.0259(3) -0.4009(3) 0.53256(16) 0.1125(11) Uani 1 1 d . . . . . O4 O 0.6069(3) -0.1857(4) 0.53744(17) 0.1226(12) Uani 1 1 d . . . . . N1 N 0.8167(3) 0.2760(3) 0.48179(14) 0.0759(8) Uani 1 1 d . . . . . N2 N 0.8145(3) -0.2878(3) 0.51830(14) 0.0801(9) Uani 1 1 d . . . . . C1 C 0.8042(4) 0.1134(4) 0.35390(15) 0.0709(9) Uani 1 1 d . . . . . H1A H 0.886875 0.040821 0.360287 0.085 Uiso 1 1 calc R . . . . H1B H 0.805177 0.176467 0.321946 0.085 Uiso 1 1 calc R . . . . C2 C 0.7716(4) 0.1636(4) 0.41327(17) 0.0768(10) Uani 1 1 d . . . . . H2A H 0.781254 0.097384 0.446633 0.092 Uiso 1 1 calc R . . . . H2B H 0.685444 0.229574 0.408647 0.092 Uiso 1 1 calc R . . . . C3 C 0.8561(4) 0.2146(5) 0.42895(19) 0.0892(12) Uani 1 1 d . . . . . H3A H 0.941132 0.146601 0.438140 0.107 Uiso 1 1 calc R . . . . H3B H 0.853740 0.273760 0.393637 0.107 Uiso 1 1 calc R . . . . C4 C 0.8832(4) 0.2325(4) 0.53883(18) 0.0776(10) Uani 1 1 d . . . . . C5 C 0.8113(4) 0.3278(4) 0.57620(17) 0.0772(10) Uani 1 1 d . . . . . C6 C 0.8314(6) 0.3312(5) 0.6381(2) 0.1071(15) Uani 1 1 d . . . . . H6 H 0.900690 0.268034 0.663464 0.129 Uiso 1 1 calc R . . . . C7 C 0.7392(7) 0.4370(7) 0.6598(2) 0.122(2) Uani 1 1 d . . . . . H7 H 0.746377 0.442036 0.701006 0.146 Uiso 1 1 calc R . . . . C8 C 0.6418(7) 0.5301(7) 0.6221(3) 0.1273(19) Uani 1 1 d . . . . . H8 H 0.585618 0.599519 0.637626 0.153 Uiso 1 1 calc R . . . . C9 C 0.6225(5) 0.5263(5) 0.5616(3) 0.1091(15) Uani 1 1 d . . . . . H9 H 0.553936 0.590499 0.536186 0.131 Uiso 1 1 calc R . . . . C10 C 0.7090(4) 0.4232(4) 0.54023(18) 0.0779(10) Uani 1 1 d . . . . . C11 C 0.7134(4) 0.3915(4) 0.47846(18) 0.0802(10) Uani 1 1 d . . . . . C12 C 0.7647(4) -0.0961(3) 0.35797(15) 0.0744(9) Uani 1 1 d . . . . . H12A H 0.723723 -0.130377 0.336564 0.089 Uiso 1 1 calc R . . . . H12B H 0.851733 -0.136626 0.350118 0.089 Uiso 1 1 calc R . . . . C13 C 0.7542(4) -0.1220(4) 0.42718(15) 0.0782(10) Uani 1 1 d . . . . . H13A H 0.803481 -0.096376 0.448830 0.094 Uiso 1 1 calc R . . . . H13B H 0.668160 -0.072872 0.435354 0.094 Uiso 1 1 calc R . . . . C14 C 0.7982(5) -0.2580(4) 0.45128(17) 0.0951(13) Uani 1 1 d . . . . . H14A H 0.738150 -0.279105 0.436694 0.114 Uiso 1 1 calc R . . . . H14B H 0.876745 -0.308186 0.435228 0.114 Uiso 1 1 calc R . . . . C15 C 0.7147(4) -0.2450(4) 0.5559(2) 0.0889(12) Uani 1 1 d . . . . . C16 C 0.7717(4) -0.2883(4) 0.61961(18) 0.0842(11) Uani 1 1 d . . . . . C17 C 0.7189(5) -0.2709(5) 0.6751(2) 0.1113(16) Uani 1 1 d . . . . . H17 H 0.633126 -0.225458 0.676102 0.134 Uiso 1 1 calc R . . . . C18 C 0.7981(7) -0.3233(7) 0.7288(2) 0.139(2) Uani 1 1 d . . . . . H18 H 0.765092 -0.314706 0.766710 0.167 Uiso 1 1 calc R . . . . C19 C 0.9215(8) -0.3862(8) 0.7268(3) 0.158(3) Uani 1 1 d . . . . . H19 H 0.971955 -0.420132 0.763870 0.190 Uiso 1 1 calc R . . . . C20 C 0.9767(6) -0.4027(7) 0.6732(3) 0.144(2) Uani 1 1 d . . . . . H20 H 1.062850 -0.444657 0.673123 0.173 Uiso 1 1 calc R . . . . C21 C 0.8983(4) -0.3540(4) 0.61812(18) 0.0903(12) Uani 1 1 d . . . . . C22 C 0.9250(4) -0.3539(4) 0.55268(19) 0.0846(11) Uani 1 1 d . . . . . B1 B 0.8369(4) 0.0275(4) 0.20805(16) 0.0585(8) Uani 1 1 d . . . . . B2 B 0.7054(3) 0.0843(3) 0.24284(14) 0.0504(7) Uani 1 1 d . . . . . B3 B 0.7436(4) 0.1843(3) 0.18713(15) 0.0570(8) Uani 1 1 d . . . . . B4 B 0.7765(4) 0.0771(3) 0.13354(15) 0.0556(8) Uani 1 1 d . . . . . B5 B 0.7393(3) -0.0233(3) 0.18970(15) 0.0541(8) Uani 1 1 d . . . . . B6 B 0.5820(3) 0.2310(3) 0.20019(15) 0.0522(7) Uani 1 1 d . . . . . B7 B 0.6305(4) 0.2269(3) 0.12201(15) 0.0551(8) Uani 1 1 d . . . . . B8 B 0.6275(4) 0.0809(3) 0.12325(15) 0.0533(8) Uani 1 1 d . . . . . B9 B 0.5790(3) 0.0840(3) 0.20158(14) 0.0499(7) Uani 1 1 d . . . . . B10 B 0.5089(4) 0.2085(3) 0.14345(15) 0.0560(8) Uani 1 1 d . . . . . N3 N 0.4057(2) 0.7606(2) 0.13459(11) 0.0564(6) Uani 1 1 d . . . . . C23 C 0.4645(4) 0.6700(4) 0.19489(17) 0.0764(10) Uani 1 1 d . . . . . H23A H 0.512644 0.586597 0.186069 0.092 Uiso 1 1 calc R . . . . H23B H 0.398634 0.671235 0.219257 0.092 Uiso 1 1 calc R . . . . C24 C 0.5483(5) 0.6946(4) 0.2335(2) 0.0978(13) Uani 1 1 d . . . . . H24A H 0.611250 0.698805 0.208459 0.117 Uiso 1 1 calc R . . . . H24B H 0.499145 0.775402 0.245033 0.117 Uiso 1 1 calc R . . . . C25 C 0.6115(5) 0.5985(5) 0.2906(2) 0.1077(16) Uani 1 1 d . . . . . H25A H 0.549101 0.592829 0.315567 0.129 Uiso 1 1 calc R . . . . H25B H 0.662833 0.517808 0.279334 0.129 Uiso 1 1 calc R . . . . C26 C 0.6895(6) 0.6274(6) 0.3273(3) 0.134(2) Uani 1 1 d . . . . . H26A H 0.766406 0.605586 0.309149 0.202 Uiso 1 1 calc GR . . . . H26B H 0.706460 0.580482 0.368648 0.202 Uiso 1 1 calc GR . . . . H26C H 0.646681 0.715065 0.328226 0.202 Uiso 1 1 calc GR . . . . C27 C 0.3400(4) 0.7132(4) 0.09739(17) 0.0727(9) Uani 1 1 d . . . . . H27A H 0.308748 0.768624 0.057486 0.087 Uiso 1 1 calc R . . . . H27B H 0.401231 0.631531 0.090197 0.087 Uiso 1 1 calc R . . . . C28 C 0.2348(4) 0.7027(4) 0.1252(2) 0.0830(11) Uani 1 1 d . . . . . H28A H 0.173890 0.783230 0.133896 0.100 Uiso 1 1 calc R . . . . H28B H 0.265659 0.643541 0.164054 0.100 Uiso 1 1 calc R . . . . C29 C 0.1725(5) 0.6605(5) 0.0832(3) 0.1118(16) Uani 1 1 d . . . . . H29A H 0.138540 0.722350 0.045358 0.134 Uiso 1 1 calc R . . . . H29B H 0.235326 0.582908 0.072540 0.134 Uiso 1 1 calc R . . . . C30 C 0.0731(5) 0.6413(7) 0.1089(3) 0.148(3) Uani 1 1 d . . . . . H30A H 0.040754 0.612380 0.079760 0.222 Uiso 1 1 calc GR . . . . H30B H 0.007825 0.718688 0.117384 0.222 Uiso 1 1 calc GR . . . . H30C H 0.105392 0.580183 0.146424 0.222 Uiso 1 1 calc GR . . . . C31 C 0.5044(3) 0.7720(3) 0.09708(17) 0.0696(9) Uani 1 1 d . . . . . H31A H 0.464086 0.825373 0.057467 0.084 Uiso 1 1 calc R . . . . H31B H 0.537107 0.814012 0.118128 0.084 Uiso 1 1 calc R . . . . C32 C 0.6111(4) 0.6541(4) 0.0856(2) 0.0866(11) Uani 1 1 d . . . . . H32A H 0.644485 0.595596 0.124561 0.104 Uiso 1 1 calc R . . . . H32B H 0.580573 0.618129 0.058978 0.104 Uiso 1 1 calc R . . . . C33 C 0.7121(4) 0.6675(4) 0.0574(2) 0.0901(11) Uani 1 1 d . . . . . H33A H 0.740260 0.706515 0.083260 0.108 Uiso 1 1 calc R . . . . H33B H 0.679161 0.723680 0.017776 0.108 Uiso 1 1 calc R . . . . C34 C 0.8210(4) 0.5500(5) 0.0478(3) 0.1106(16) Uani 1 1 d . . . . . H34A H 0.802273 0.483057 0.056562 0.166 Uiso 1 1 calc GR . . . . H34B H 0.891294 0.531311 0.074846 0.166 Uiso 1 1 calc GR . . . . H34C H 0.840185 0.559279 0.005742 0.166 Uiso 1 1 calc GR . . . . C35 C 0.3160(4) 0.8878(3) 0.14865(18) 0.0748(9) Uani 1 1 d . . . . . H35A H 0.260135 0.877249 0.176840 0.090 Uiso 1 1 calc R . . . . H35B H 0.364015 0.914350 0.170631 0.090 Uiso 1 1 calc R . . . . C36 C 0.2397(4) 0.9899(4) 0.0977(2) 0.0927(12) Uani 1 1 d . . . . . H36A H 0.186904 0.967203 0.076834 0.111 Uiso 1 1 calc R . . . . H36B H 0.294027 1.000019 0.068314 0.111 Uiso 1 1 calc R . . . . C37 C 0.1605(5) 1.1107(4) 0.1167(3) 0.1239(19) Uani 1 1 d . . . . . H37A H 0.108609 1.098649 0.147018 0.149 Uiso 1 1 calc R . . . . H37B H 0.214389 1.132584 0.137179 0.149 Uiso 1 1 calc R . . . . C38 C 0.0815(6) 1.2145(5) 0.0699(4) 0.177(4) Uani 1 1 d . . . . . H38A H 0.131346 1.235391 0.042257 0.266 Uiso 1 1 calc GR . . . . H38B H 0.029716 1.284762 0.088592 0.266 Uiso 1 1 calc GR . . . . H38C H 0.030187 1.193573 0.047452 0.266 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0543(5) 0.1094(7) 0.0610(5) -0.0028(5) 0.0041(4) -0.0335(5) Cl2 0.1345(9) 0.1081(7) 0.0763(6) -0.0234(5) 0.0184(6) -0.0963(7) Cl3 0.0872(6) 0.0856(6) 0.0549(5) -0.0186(4) 0.0307(4) -0.0454(5) Cl4 0.1066(7) 0.0481(4) 0.0719(5) -0.0108(4) 0.0223(5) -0.0351(4) Cl5 0.1154(7) 0.0531(4) 0.0434(4) -0.0009(3) 0.0119(4) -0.0491(5) Cl6 0.1136(7) 0.0677(5) 0.0406(4) -0.0174(3) 0.0071(4) -0.0604(5) Cl7 0.0796(5) 0.0722(5) 0.0624(5) -0.0116(4) 0.0163(4) -0.0524(4) Cl8 0.1089(7) 0.0555(4) 0.0676(5) -0.0286(4) 0.0318(5) -0.0416(5) Cl9 0.0661(5) 0.0885(6) 0.0619(5) 0.0000(4) -0.0090(4) -0.0271(5) S1 0.0760(5) 0.0727(5) 0.0375(4) -0.0107(3) 0.0066(3) -0.0447(4) O1 0.103(2) 0.093(2) 0.120(3) -0.0229(19) -0.019(2) -0.036(2) O2 0.135(3) 0.119(3) 0.089(2) -0.0043(19) -0.025(2) -0.055(2) O3 0.108(2) 0.121(3) 0.100(2) -0.0106(19) 0.035(2) -0.054(2) O4 0.095(2) 0.146(3) 0.108(3) 0.023(2) -0.011(2) -0.060(2) N1 0.091(2) 0.085(2) 0.0631(18) -0.0266(15) 0.0021(15) -0.0483(19) N2 0.101(2) 0.091(2) 0.0548(17) 0.0044(15) 0.0046(17) -0.058(2) C1 0.089(2) 0.090(2) 0.0525(18) -0.0200(16) 0.0073(17) -0.056(2) C2 0.098(3) 0.093(3) 0.061(2) -0.0295(18) 0.0139(19) -0.059(2) C3 0.105(3) 0.126(4) 0.072(2) -0.046(2) 0.019(2) -0.076(3) C4 0.088(3) 0.084(3) 0.073(2) -0.0169(19) -0.003(2) -0.051(2) C5 0.110(3) 0.094(3) 0.0554(19) -0.0198(18) 0.009(2) -0.070(3) C6 0.154(5) 0.127(4) 0.067(3) -0.023(3) 0.010(3) -0.088(4) C7 0.187(6) 0.159(5) 0.069(3) -0.056(3) 0.047(4) -0.113(5) C8 0.148(5) 0.142(5) 0.112(5) -0.063(4) 0.041(4) -0.075(5) C9 0.110(4) 0.109(4) 0.112(4) -0.040(3) 0.028(3) -0.051(3) C10 0.092(3) 0.085(3) 0.073(2) -0.026(2) 0.016(2) -0.053(2) C11 0.097(3) 0.094(3) 0.063(2) -0.015(2) 0.002(2) -0.057(3) C12 0.105(3) 0.074(2) 0.0486(18) -0.0017(15) 0.0057(18) -0.050(2) C13 0.111(3) 0.091(3) 0.0483(18) 0.0001(17) 0.0004(18) -0.067(2) C14 0.148(4) 0.102(3) 0.056(2) -0.001(2) -0.001(2) -0.083(3) C15 0.091(3) 0.100(3) 0.077(3) 0.014(2) -0.005(2) -0.057(3) C16 0.095(3) 0.092(3) 0.060(2) 0.0033(19) 0.011(2) -0.048(2) C17 0.117(4) 0.122(4) 0.086(3) -0.002(3) 0.029(3) -0.058(3) C18 0.160(6) 0.180(6) 0.063(3) -0.002(3) 0.026(4) -0.078(5) C19 0.154(6) 0.206(8) 0.061(3) 0.010(4) -0.004(4) -0.059(6) C20 0.107(4) 0.193(6) 0.080(4) 0.026(4) -0.009(3) -0.050(4) C21 0.091(3) 0.103(3) 0.063(2) 0.009(2) 0.005(2) -0.044(3) C22 0.094(3) 0.089(3) 0.070(2) 0.000(2) 0.020(2) -0.050(2) B1 0.066(2) 0.067(2) 0.0443(18) -0.0070(15) 0.0101(15) -0.0358(18) B2 0.069(2) 0.0577(18) 0.0358(15) -0.0077(13) 0.0069(14) -0.0406(17) B3 0.082(2) 0.068(2) 0.0421(17) -0.0131(15) 0.0134(16) -0.053(2) B4 0.077(2) 0.0598(19) 0.0418(17) -0.0113(14) 0.0166(15) -0.0422(18) B5 0.075(2) 0.0500(17) 0.0415(16) -0.0092(13) 0.0138(15) -0.0338(17) B6 0.075(2) 0.0472(16) 0.0437(16) -0.0125(13) 0.0123(15) -0.0366(16) B7 0.087(2) 0.0500(17) 0.0393(16) -0.0082(13) 0.0135(16) -0.0424(18) B8 0.078(2) 0.0515(17) 0.0410(16) -0.0118(13) 0.0092(15) -0.0397(17) B9 0.067(2) 0.0499(16) 0.0429(16) -0.0092(13) 0.0068(14) -0.0368(16) B10 0.073(2) 0.0534(18) 0.0452(17) -0.0071(14) 0.0042(15) -0.0345(17) N3 0.0737(17) 0.0525(13) 0.0519(14) -0.0137(11) 0.0112(12) -0.0370(13) C23 0.100(3) 0.071(2) 0.068(2) -0.0090(17) 0.0049(19) -0.051(2) C24 0.118(4) 0.097(3) 0.086(3) -0.004(2) -0.009(3) -0.063(3) C25 0.158(5) 0.099(3) 0.071(3) 0.004(2) -0.024(3) -0.074(3) C26 0.132(5) 0.163(6) 0.106(4) 0.000(4) -0.021(3) -0.079(4) C27 0.087(2) 0.075(2) 0.071(2) -0.0253(17) 0.0120(18) -0.049(2) C28 0.083(3) 0.087(3) 0.096(3) -0.030(2) 0.017(2) -0.051(2) C29 0.107(3) 0.126(4) 0.139(4) -0.048(3) 0.014(3) -0.079(3) C30 0.114(4) 0.185(6) 0.208(7) -0.096(6) 0.047(4) -0.105(5) C31 0.085(2) 0.0639(19) 0.068(2) -0.0116(15) 0.0110(17) -0.0430(18) C32 0.082(3) 0.071(2) 0.109(3) -0.025(2) 0.023(2) -0.036(2) C33 0.087(3) 0.091(3) 0.094(3) -0.025(2) 0.016(2) -0.043(2) C34 0.088(3) 0.100(3) 0.142(5) -0.039(3) 0.034(3) -0.040(3) C35 0.088(3) 0.064(2) 0.078(2) -0.0214(17) 0.0158(19) -0.0398(19) C36 0.083(3) 0.069(2) 0.112(3) -0.010(2) 0.009(2) -0.028(2) C37 0.102(4) 0.063(3) 0.186(6) -0.021(3) 0.005(4) -0.026(3) C38 0.115(5) 0.082(4) 0.290(11) 0.020(5) 0.000(6) -0.031(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C1 S1 C12 104.94(19) . . C1 S1 B2 102.94(15) . . C12 S1 B2 104.33(15) . . C4 N1 C3 124.8(4) . . C11 N1 C3 123.1(3) . . C11 N1 C4 111.8(3) . . C15 N2 C14 123.6(4) . . C22 N2 C14 125.1(4) . . C22 N2 C15 111.2(3) . . S1 C1 H1A 109.4 . . S1 C1 H1B 109.4 . . H1A C1 H1B 108.0 . . C2 C1 S1 111.3(3) . . C2 C1 H1A 109.4 . . C2 C1 H1B 109.4 . . C1 C2 H2A 109.6 . . C1 C2 H2B 109.6 . . C1 C2 C3 110.3(3) . . H2A C2 H2B 108.1 . . C3 C2 H2A 109.6 . . C3 C2 H2B 109.6 . . N1 C3 C2 110.8(3) . . N1 C3 H3A 109.5 . . N1 C3 H3B 109.5 . . C2 C3 H3A 109.5 . . C2 C3 H3B 109.5 . . H3A C3 H3B 108.1 . . O1 C4 N1 125.5(4) . . O1 C4 C5 128.8(4) . . N1 C4 C5 105.6(4) . . C6 C5 C4 131.0(4) . . C10 C5 C4 108.6(3) . . C10 C5 C6 120.3(4) . . C5 C6 H6 122.1 . . C5 C6 C7 115.8(5) . . C7 C6 H6 122.1 . . C6 C7 H7 119.2 . . C8 C7 C6 121.6(5) . . C8 C7 H7 119.2 . . C7 C8 H8 118.8 . . C7 C8 C9 122.4(6) . . C9 C8 H8 118.8 . . C8 C9 H9 121.6 . . C8 C9 C10 116.9(6) . . C10 C9 H9 121.6 . . C5 C10 C9 123.0(4) . . C5 C10 C11 107.3(4) . . C9 C10 C11 129.7(4) . . O2 C11 N1 124.6(4) . . O2 C11 C10 128.8(4) . . N1 C11 C10 106.6(3) . . S1 C12 H12A 109.5 . . S1 C12 H12B 109.5 . . H12A C12 H12B 108.1 . . C13 C12 S1 110.5(3) . . C13 C12 H12A 109.5 . . C13 C12 H12B 109.5 . . C12 C13 H13A 109.3 . . C12 C13 H13B 109.3 . . H13A C13 H13B 107.9 . . C14 C13 C12 111.8(3) . . C14 C13 H13A 109.3 . . C14 C13 H13B 109.3 . . N2 C14 C13 111.8(3) . . N2 C14 H14A 109.3 . . N2 C14 H14B 109.3 . . C13 C14 H14A 109.3 . . C13 C14 H14B 109.3 . . H14A C14 H14B 107.9 . . O4 C15 N2 125.1(4) . . O4 C15 C16 129.0(5) . . N2 C15 C16 105.9(4) . . C17 C16 C15 131.0(4) . . C21 C16 C15 108.0(4) . . C21 C16 C17 121.0(4) . . C16 C17 H17 121.1 . . C18 C17 C16 117.8(5) . . C18 C17 H17 121.1 . . C17 C18 H18 119.6 . . C19 C18 C17 120.7(6) . . C19 C18 H18 119.6 . . C18 C19 H19 118.4 . . C18 C19 C20 123.1(6) . . C20 C19 H19 118.5 . . C19 C20 H20 121.4 . . C19 C20 C21 117.3(6) . . C21 C20 H20 121.4 . . C16 C21 C20 120.0(4) . . C16 C21 C22 108.0(4) . . C20 C21 C22 132.0(5) . . O3 C22 N2 125.4(4) . . O3 C22 C21 127.7(4) . . N2 C22 C21 106.9(4) . . B2 B1 Cl1 131.8(2) . . B2 B1 B3 65.8(2) . . B2 B1 B4 99.6(3) . . B2 B1 B5 65.9(2) . . B3 B1 Cl1 129.2(2) . . B4 B1 Cl1 128.6(2) . . B4 B1 B3 65.4(2) . . B5 B1 Cl1 129.9(3) . . B5 B1 B3 100.8(3) . . B5 B1 B4 65.7(2) . . B1 B2 S1 126.0(2) . . B1 B2 B3 57.7(2) . . B1 B2 B5 57.5(2) . . B1 B2 B6 113.5(2) . . B1 B2 B9 113.2(2) . . B3 B2 S1 132.0(2) . . B5 B2 S1 133.8(2) . . B5 B2 B3 91.0(2) . . B6 B2 S1 112.0(2) . . B6 B2 B3 60.18(19) . . B6 B2 B5 103.5(2) . . B9 B2 S1 113.3(2) . . B9 B2 B3 103.2(2) . . B9 B2 B5 60.15(19) . . B9 B2 B6 61.35(18) . . Cl2 B3 B2 131.5(2) . . Cl2 B3 B4 132.8(2) . . Cl2 B3 B6 118.2(2) . . Cl2 B3 B7 119.3(2) . . B1 B3 Cl2 120.6(3) . . B1 B3 B2 56.41(19) . . B1 B3 B4 57.1(2) . . B1 B3 B6 111.5(2) . . B1 B3 B7 112.4(2) . . B2 B3 B4 89.1(2) . . B6 B3 B2 59.36(18) . . B6 B3 B4 102.0(2) . . B7 B3 B2 101.1(2) . . B7 B3 B4 60.36(19) . . B7 B3 B6 60.09(19) . . Cl3 B4 B3 131.7(2) . . Cl3 B4 B5 130.9(2) . . Cl3 B4 B7 119.2(2) . . Cl3 B4 B8 118.5(2) . . B1 B4 Cl3 120.3(3) . . B1 B4 B3 57.4(2) . . B1 B4 B5 57.08(19) . . B1 B4 B7 112.0(2) . . B1 B4 B8 112.2(2) . . B3 B4 B5 90.8(2) . . B3 B4 B7 59.64(19) . . B5 B4 B7 102.2(2) . . B8 B4 B3 102.1(2) . . B8 B4 B5 60.16(19) . . B8 B4 B7 60.04(19) . . Cl4 B5 B2 131.4(2) . . Cl4 B5 B4 133.0(2) . . Cl4 B5 B8 119.6(2) . . Cl4 B5 B9 118.2(2) . . B1 B5 Cl4 120.6(3) . . B1 B5 B2 56.60(19) . . B1 B5 B4 57.23(19) . . B1 B5 B8 112.1(2) . . B1 B5 B9 111.7(2) . . B2 B5 B4 89.1(2) . . B2 B5 B8 100.9(2) . . B4 B5 B8 59.85(19) . . B9 B5 B2 59.46(18) . . B9 B5 B4 101.8(2) . . B9 B5 B8 60.02(19) . . Cl8 B6 B2 118.5(2) . . Cl8 B6 B3 118.4(2) . . Cl8 B6 B7 132.3(2) . . Cl8 B6 B9 131.7(2) . . B2 B6 B3 60.46(19) . . B2 B6 B7 101.7(2) . . B2 B6 B9 59.32(17) . . B3 B6 B7 59.93(19) . . B3 B6 B9 101.9(2) . . B7 B6 B9 89.76(19) . . B10 B6 Cl8 121.1(3) . . B10 B6 B2 111.4(2) . . B10 B6 B3 112.2(2) . . B10 B6 B7 57.09(19) . . B10 B6 B9 56.81(18) . . Cl5 B7 B3 118.7(2) . . Cl5 B7 B4 119.8(2) . . Cl5 B7 B6 130.9(2) . . Cl5 B7 B8 131.9(2) . . B3 B7 B4 60.0(2) . . B3 B7 B6 59.98(19) . . B3 B7 B8 102.2(2) . . B6 B7 B4 101.7(2) . . B6 B7 B8 90.32(19) . . B8 B7 B4 59.80(19) . . B10 B7 Cl5 120.0(3) . . B10 B7 B3 112.2(2) . . B10 B7 B4 111.9(2) . . B10 B7 B6 57.09(19) . . B10 B7 B8 57.15(19) . . Cl6 B8 B4 120.1(2) . . Cl6 B8 B5 118.8(2) . . Cl6 B8 B7 132.3(2) . . Cl6 B8 B9 130.5(2) . . B4 B8 B5 59.98(19) . . B4 B8 B7 60.17(19) . . B7 B8 B5 102.2(2) . . B9 B8 B4 101.6(2) . . B9 B8 B5 59.61(18) . . B9 B8 B7 90.04(19) . . B10 B8 Cl6 119.8(2) . . B10 B8 B4 112.0(2) . . B10 B8 B5 111.9(2) . . B10 B8 B7 56.84(19) . . B10 B8 B9 57.06(18) . . Cl7 B9 B2 118.4(2) . . Cl7 B9 B5 119.1(2) . . Cl7 B9 B6 130.5(2) . . Cl7 B9 B8 133.0(2) . . B2 B9 B5 60.38(19) . . B2 B9 B6 59.33(18) . . B2 B9 B8 101.8(2) . . B5 B9 B6 102.2(2) . . B5 B9 B8 60.37(19) . . B8 B9 B6 89.87(19) . . B10 B9 Cl7 120.6(2) . . B10 B9 B2 111.3(2) . . B10 B9 B5 112.7(2) . . B10 B9 B6 56.64(18) . . B10 B9 B8 57.20(19) . . B6 B10 Cl9 129.2(2) . . B6 B10 B8 100.9(3) . . B6 B10 B9 66.5(2) . . B7 B10 Cl9 130.1(2) . . B7 B10 B6 65.8(2) . . B7 B10 B8 66.0(2) . . B7 B10 B9 100.7(3) . . B8 B10 Cl9 130.0(2) . . B9 B10 Cl9 129.2(2) . . B9 B10 B8 65.7(2) . . C23 N3 C27 109.2(2) . . C23 N3 C31 110.6(3) . . C23 N3 C35 108.4(3) . . C27 N3 C31 108.5(2) . . C35 N3 C27 111.7(3) . . C35 N3 C31 108.4(2) . . N3 C23 H23A 108.4 . . N3 C23 H23B 108.4 . . N3 C23 C24 115.6(3) . . H23A C23 H23B 107.4 . . C24 C23 H23A 108.4 . . C24 C23 H23B 108.4 . . C23 C24 H24A 108.7 . . C23 C24 H24B 108.7 . . H24A C24 H24B 107.6 . . C25 C24 C23 114.2(4) . . C25 C24 H24A 108.7 . . C25 C24 H24B 108.7 . . C24 C25 H25A 109.1 . . C24 C25 H25B 109.1 . . H25A C25 H25B 107.9 . . C26 C25 C24 112.4(4) . . C26 C25 H25A 109.1 . . C26 C25 H25B 109.1 . . C25 C26 H26A 109.5 . . C25 C26 H26B 109.5 . . C25 C26 H26C 109.5 . . H26A C26 H26B 109.5 . . H26A C26 H26C 109.5 . . H26B C26 H26C 109.5 . . N3 C27 H27A 108.2 . . N3 C27 H27B 108.2 . . H27A C27 H27B 107.3 . . C28 C27 N3 116.4(3) . . C28 C27 H27A 108.2 . . C28 C27 H27B 108.2 . . C27 C28 H28A 109.2 . . C27 C28 H28B 109.2 . . C27 C28 C29 112.1(4) . . H28A C28 H28B 107.9 . . C29 C28 H28A 109.2 . . C29 C28 H28B 109.2 . . C28 C29 H29A 108.5 . . C28 C29 H29B 108.5 . . H29A C29 H29B 107.5 . . C30 C29 C28 115.1(5) . . C30 C29 H29A 108.5 . . C30 C29 H29B 108.5 . . C29 C30 H30A 109.5 . . C29 C30 H30B 109.5 . . C29 C30 H30C 109.5 . . H30A C30 H30B 109.5 . . H30A C30 H30C 109.5 . . H30B C30 H30C 109.5 . . N3 C31 H31A 108.1 . . N3 C31 H31B 108.1 . . H31A C31 H31B 107.3 . . C32 C31 N3 116.9(3) . . C32 C31 H31A 108.1 . . C32 C31 H31B 108.1 . . C31 C32 H32A 108.5 . . C31 C32 H32B 108.5 . . H32A C32 H32B 107.5 . . C33 C32 C31 114.9(3) . . C33 C32 H32A 108.5 . . C33 C32 H32B 108.5 . . C32 C33 H33A 108.4 . . C32 C33 H33B 108.4 . . C32 C33 C34 115.4(4) . . H33A C33 H33B 107.5 . . C34 C33 H33A 108.4 . . C34 C33 H33B 108.4 . . C33 C34 H34A 109.5 . . C33 C34 H34B 109.5 . . C33 C34 H34C 109.5 . . H34A C34 H34B 109.5 . . H34A C34 H34C 109.5 . . H34B C34 H34C 109.5 . . N3 C35 H35A 107.6 . . N3 C35 H35B 107.6 . . H35A C35 H35B 107.0 . . C36 C35 N3 119.0(3) . . C36 C35 H35A 107.6 . . C36 C35 H35B 107.6 . . C35 C36 H36A 108.7 . . C35 C36 H36B 108.7 . . C35 C36 C37 114.2(4) . . H36A C36 H36B 107.6 . . C37 C36 H36A 108.7 . . C37 C36 H36B 108.7 . . C36 C37 H37A 107.9 . . C36 C37 H37B 107.9 . . H37A C37 H37B 107.2 . . C38 C37 C36 117.7(6) . . C38 C37 H37A 107.9 . . C38 C37 H37B 107.9 . . C37 C38 H38A 109.5 . . C37 C38 H38B 109.5 . . C37 C38 H38C 109.5 . . H38A C38 H38B 109.5 . . H38A C38 H38C 109.5 . . H38B C38 H38C 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Cl1 B1 1.817(4) . Cl2 B3 1.819(3) . Cl3 B4 1.814(3) . Cl4 B5 1.808(3) . Cl5 B7 1.820(3) . Cl6 B8 1.814(3) . Cl7 B9 1.809(3) . Cl8 B6 1.804(3) . Cl9 B10 1.800(4) . S1 C1 1.806(3) . S1 C12 1.813(4) . S1 B2 1.890(3) . O1 C4 1.210(5) . O2 C11 1.201(5) . O3 C22 1.212(5) . O4 C15 1.195(5) . N1 C3 1.456(5) . N1 C4 1.377(5) . N1 C11 1.374(5) . N2 C14 1.453(5) . N2 C15 1.415(6) . N2 C22 1.349(5) . C1 H1A 0.9700 . C1 H1B 0.9700 . C1 C2 1.517(5) . C2 H2A 0.9700 . C2 H2B 0.9700 . C2 C3 1.526(5) . C3 H3A 0.9700 . C3 H3B 0.9700 . C4 C5 1.477(6) . C5 C6 1.401(6) . C5 C10 1.367(6) . C6 H6 0.9300 . C6 C7 1.420(8) . C7 H7 0.9300 . C7 C8 1.346(8) . C8 H8 0.9300 . C8 C9 1.369(8) . C9 H9 0.9300 . C9 C10 1.373(6) . C10 C11 1.476(5) . C12 H12A 0.9700 . C12 H12B 0.9700 . C12 C13 1.527(5) . C13 H13A 0.9700 . C13 H13B 0.9700 . C13 C14 1.504(5) . C14 H14A 0.9700 . C14 H14B 0.9700 . C15 C16 1.463(6) . C16 C17 1.386(6) . C16 C21 1.372(6) . C17 H17 0.9300 . C17 C18 1.383(8) . C18 H18 0.9300 . C18 C19 1.338(8) . C19 H19 0.9300 . C19 C20 1.361(8) . C20 H20 0.9300 . C20 C21 1.404(7) . C21 C22 1.481(6) . B1 B2 1.671(5) . B1 B3 1.696(5) . B1 B4 1.691(5) . B1 B5 1.688(5) . B2 B3 1.830(4) . B2 B5 1.826(5) . B2 B6 1.810(5) . B2 B9 1.809(5) . B3 B4 1.831(5) . B3 B6 1.825(5) . B3 B7 1.824(5) . B4 B5 1.833(4) . B4 B7 1.837(5) . B4 B8 1.830(5) . B5 B8 1.836(5) . B5 B9 1.822(5) . B6 B7 1.827(4) . B6 B9 1.846(4) . B6 B10 1.681(5) . B7 B8 1.835(4) . B7 B10 1.681(5) . B8 B9 1.830(4) . B8 B10 1.687(5) . B9 B10 1.685(5) . N3 C23 1.510(4) . N3 C27 1.520(4) . N3 C31 1.523(4) . N3 C35 1.516(4) . C23 H23A 0.9700 . C23 H23B 0.9700 . C23 C24 1.512(6) . C24 H24A 0.9700 . C24 H24B 0.9700 . C24 C25 1.492(6) . C25 H25A 0.9700 . C25 H25B 0.9700 . C25 C26 1.466(7) . C26 H26A 0.9600 . C26 H26B 0.9600 . C26 H26C 0.9600 . C27 H27A 0.9700 . C27 H27B 0.9700 . C27 C28 1.490(5) . C28 H28A 0.9700 . C28 H28B 0.9700 . C28 C29 1.513(6) . C29 H29A 0.9700 . C29 H29B 0.9700 . C29 C30 1.457(7) . C30 H30A 0.9600 . C30 H30B 0.9600 . C30 H30C 0.9600 . C31 H31A 0.9700 . C31 H31B 0.9700 . C31 C32 1.484(5) . C32 H32A 0.9700 . C32 H32B 0.9700 . C32 C33 1.463(6) . C33 H33A 0.9700 . C33 H33B 0.9700 . C33 C34 1.480(6) . C34 H34A 0.9600 . C34 H34B 0.9600 . C34 H34C 0.9600 . C35 H35A 0.9700 . C35 H35B 0.9700 . C35 C36 1.460(6) . C36 H36A 0.9700 . C36 H36B 0.9700 . C36 C37 1.477(6) . C37 H37A 0.9700 . C37 H37B 0.9700 . C37 C38 1.421(9) . C38 H38A 0.9600 . C38 H38B 0.9600 . C38 H38C 0.9600 . loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons 1 0.288 -0.057 0.370 170.3 42.5 2 -0.288 0.057 0.630 170.3 42.4 3 0.176 0.465 0.803 13.5 0.3 4 0.824 0.535 0.197 13.5 0.3