#------------------------------------------------------------------------------ #$Date: 2021-09-27 12:04:59 +0300 (Mon, 27 Sep 2021) $ #$Revision: 269322 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/47/1564729.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564729 loop_ _publ_author_name 'Kubasov, A.S.' 'Turishev, E.S.' 'Golubev, A.V.' 'Bykov, A.Yu.' 'Zhizhin, K.Yu.' 'Kuznetsov, N.T.' _publ_section_title ; The method for synthesis of 2-sulfonium closo-decaborate anions derivatives with exo-polyhedral aminogroups ; _journal_name_full 'Inorganica Chimica Acta' _journal_page_first 119589 _journal_paper_doi 10.1016/j.ica.2020.119589 _journal_volume 507 _journal_year 2020 _chemical_formula_moiety 'C20 H25 B10 N2 O4 S, C16 H36 N' _chemical_formula_sum 'C36 H61 B10 N3 O4 S' _chemical_formula_weight 740.03 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _cell_angle_alpha 90 _cell_angle_beta 111.673(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 14.9294(12) _cell_length_b 17.0837(11) _cell_length_c 20.1140(15) _cell_measurement_reflns_used 2750 _cell_measurement_temperature 296 _cell_measurement_theta_max 27.80 _cell_measurement_theta_min 2.44 _cell_volume 4767.4(6) _computing_cell_refinement 'SAINT V8.38A (?, 2016)' _computing_data_reduction 'SAINT V8.38A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'olex2.solve (Bourhis et al., 2015)' _diffrn_ambient_temperature 296.0 _diffrn_detector_area_resol_mean 8 _diffrn_measured_fraction_theta_full 0.975 _diffrn_measured_fraction_theta_max 0.970 _diffrn_measurement_device_type 'Bruker SMART APEX CCD area detector' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0929 _diffrn_reflns_av_unetI/netI 0.1446 _diffrn_reflns_Laue_measured_fraction_full 0.975 _diffrn_reflns_Laue_measured_fraction_max 0.970 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_number 24187 _diffrn_reflns_point_group_measured_fraction_full 0.975 _diffrn_reflns_point_group_measured_fraction_max 0.970 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.997 _diffrn_reflns_theta_min 1.891 _diffrn_source 'sealed tube' _exptl_absorpt_coefficient_mu 0.104 _exptl_absorpt_correction_T_max 0.7458 _exptl_absorpt_correction_T_min 0.6397 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0953 before and 0.0545 after correction. The Ratio of minimum to maximum transmission is 0.8577. The \l/2 correction factor is Not present.' _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.031 _exptl_crystal_description plate _exptl_crystal_F_000 1584 _exptl_crystal_size_max 0.8 _exptl_crystal_size_mid 0.8 _exptl_crystal_size_min 0.03 _refine_diff_density_max 0.480 _refine_diff_density_min -0.471 _refine_diff_density_rms 0.078 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.966 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 495 _refine_ls_number_reflns 9086 _refine_ls_number_restraints 46 _refine_ls_restrained_S_all 1.000 _refine_ls_R_factor_all 0.2300 _refine_ls_R_factor_gt 0.1130 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1958P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2983 _refine_ls_wR_factor_ref 0.3731 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 3150 _reflns_number_total 9086 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file 19kub41_0m_a.cif _cod_data_source_block 19kub41_0m_a _cod_database_code 1564729 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.997 _shelx_estimated_absorpt_t_min 0.921 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All B(H) groups, All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances N3-C21B = N3-C33B = N3-C25B = N3-C21 = N3-C25 1.55 with sigma of 0.02 N3-C33 1.5 with sigma of 0.02 C34-C33 1.55 with sigma of 0.02 C34-C35 1.55 with sigma of 0.02 C35-C36 1.55 with sigma of 0.02 C35B-C36B 1.55 with sigma of 0.02 C27B-C26B = C27B-C28B 1.55 with sigma of 0.02 C27-C28 = C27-C26 1.55 with sigma of 0.02 C26-C25 = C26-C27 1.55 with sigma of 0.02 C26B-C27B = C26B-C25B 1.55 with sigma of 0.02 C22B-C21B 1.55 with sigma of 0.02 C23-C22B = C23-C24 1.55 with sigma of 0.02 C22B-C21B = C22B-C23 1.55 with sigma of 0.02 C22-C21 1.55 with sigma of 0.02 C23B-C24B 1.55 with sigma of 0.02 C35B-C34B = C35B-C36B 1.52 with sigma of 0.02 C29-N3 = C29-C30B 1.52 with sigma of 0.02 C30-C29 1.52 with sigma of 0.02 C29-N3 = C29-C30 1.52 with sigma of 0.02 C31-C30 1.52 with sigma of 0.02 C32-C31 1.52 with sigma of 0.02 C31B-C30B 1.52 with sigma of 0.02 C29B-N3 = C29B-C30B 1.52 with sigma of 0.02 C30B-C29B = C30B-C31B 1.52 with sigma of 0.02 C32B-C31B 1.52 with sigma of 0.02 C29-C31 2.48 with sigma of 0.02 C30-C32 2.48 with sigma of 0.02 C29B-C31B 2.48 with sigma of 0.02 C30B-C32B 2.48 with sigma of 0.02 C26-C28 2.48 with sigma of 0.02 C21-C23 2.48 with sigma of 0.02 C22-N3 2.48 with sigma of 0.02 C22-C24 2.48 with sigma of 0.02 C34-C36 2.48 with sigma of 0.02 3. Uiso/Uaniso restraints and constraints Uanis(C35) = Uanis(C35B) Uanis(C33B) = Uanis(C33) Uanis(C36B) = Uanis(C36) Uanis(C34B) = Uanis(C34) Uanis(C25B) = Uanis(C25) Uanis(C26B) = Uanis(C26) Uanis(C27B) = Uanis(C27) Uanis(C28B) = Uanis(C28) Uanis(C21) = Uanis(C21B) Uanis(C22B) = Uanis(C22) Uanis(C24) = Uanis(C23B) Uanis(C23) = Uanis(C23B) Uanis(C24) = Uanis(C24B) Uanis(C32B) = Uanis(C32) Uanis(C31) = Uanis(C31B) Uanis(C30) = Uanis(C30B) Uanis(C23) = Uanis(C27) Uanis(C23B) = Uanis(C35B) Uanis(C23) = Uanis(C35) Uanis(C32) = Uanis(C24) Uanis(C32B) = Uanis(C24B) Uanis(C31) = Uanis(C27) Uanis(C31B) = Uanis(C27B) Uanis(C30B) = Uanis(C22B) 4. Others Fixed Sof: C21B(0.666) H21A(0.666) H21B(0.666) C26B(0.6666) H26A(0.6666) H26B(0.6666) C22(0.33333) H22A(0.33333) H22B(0.33333) C27B(0.6666) H27A(0.6666) H27B(0.6666) C33B(0.66667) H33A(0.66667) H33B(0.66667) C28B(0.6666) H28A(0.6666) H28B(0.6666) H28C(0.6666) C25B(0.6666) H25A(0.6666) H25B(0.6666) C21(0.33333) H21C(0.33333) H21D(0.33333) C23B(0.66666) H23A(0.66666) H23B(0.66666) C25(0.33333) H25C(0.33333) H25D(0.33333) C34B(0.66667) H34A(0.66667) H34B(0.66667) C35B(0.66667) H35A(0.66667) H35B(0.66667) C36B(0.66667) H36A(0.66667) H36B(0.66667) H36C(0.66667) C33(0.33333) H33C(0.33333) H33D(0.33333) C34(0.33333) H34C(0.33333) H34D(0.33333) C35(0.33333) H35C(0.33333) H35D(0.33333) C36(0.33333) H36D(0.33333) H36E(0.33333) H36F(0.33333) C28(0.33333) H28D(0.33333) H28E(0.33333) H28F(0.33333) C27(0.33333) H27C(0.33333) H27D(0.33333) C26(0.33333) H26C(0.33333) H26D(0.33333) C22B(0.6666) H22C(0.6666) H22D(0.6666) C24(0.3333) H24A(0.3333) H24B(0.3333) H24C(0.3333) C23(0.3333) H23C(0.3333) H23D(0.3333) C24B(0.66666) H24D(0.66666) H24E(0.66666) H24F(0.66666) C29B(0.66666) H29A(0.66666) H29B(0.66666) C30B(0.66667) H30A(0.66667) H30B(0.66667) C31B(0.66667) H31A(0.66667) H31B(0.66667) C29(0.33333) H29C(0.33333) H29D(0.33333) C30(0.33333) H30C(0.33333) H30D(0.33333) C31(0.33333) H31C(0.33333) H31D(0.33333) C32B(0.6666) H32A(0.6666) H32B(0.6666) H32C(0.6666) C32(0.33333) H32D(0.33333) H32E(0.33333) H32F(0.33333) Fixed X: C22(0.87501) C23B(0.881961) C22B(0.853001) C24(0.83191) C23(0.90418) C24B(0.87739) Fixed Y: C22(0.57352) C23B(0.628761) C22B(0.542689) C24(0.661751) C23(0.64259) C24B(0.68773) Fixed Z: C22(0.739539) C23B(0.71885) C22B(0.703589) C24(0.631921) C23(0.709049) C24B(0.661251) 5.a Secondary CH2 refined with riding coordinates: C2(H2A,H2B), C11(H11A,H11B), C1(H1A,H1B), C12(H12A,H12B), C21B(H21A,H21B), C26B(H26A,H26B), C22(H22A,H22B), C27B(H27A,H27B), C33B(H33A,H33B), C25B(H25A, H25B), C21(H21C,H21D), C23B(H23A,H23B), C25(H25C,H25D), C34B(H34A,H34B), C35B(H35A,H35B), C33(H33C,H33D), C34(H34C,H34D), C35(H35C,H35D), C27(H27C, H27D), C26(H26C,H26D), C22B(H22C,H22D), C23(H23C,H23D), C29B(H29A,H29B), C30B(H30A,H30B), C31B(H31A,H31B), C29(H29C,H29D), C30(H30C,H30D), C31(H31C, H31D) 5.b Aromatic/amide H refined with riding coordinates: C15(H15), C5(H5A), C18(H18), C16(H16), C17(H17), C8(H8), C6(H6A), C7(H7A) 5.c Idealised Me refined as rotating group: C28B(H28A,H28B,H28C), C36B(H36A,H36B,H36C), C36(H36D,H36E,H36F), C28(H28D, H28E,H28F), C24(H24A,H24B,H24C), C24B(H24D,H24E,H24F), C32B(H32A,H32B,H32C), C32(H32D,H32E,H32F) 5.d Boron cage BH refined with riding coordinates: B9(H9), B5(H5), B6(H6), B1(H1), B7(H7), B3(H3), B8(H8A), B4(H4), B10(H10) ; _shelx_res_file ; TITL 19kub41_0m_a.res in P2(1)/c 19kub41_0m_a.res created by SHELXL-2017/1 at 15:26:36 on 19-Dec-2019 REM Old TITL 19kub41_0m in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.277, Rweak 0.052, Alpha 0.065, Orientation as input REM Formula found by SHELXT: C33 B10 N4 O6 S CELL 0.71073 14.9294 17.0837 20.114 90 111.673 90 ZERR 4 0.0012 0.0011 0.0015 0 0.003 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H B N O S UNIT 144 243.99 40 12 16 4 DFIX 1.55 N3 C21B N3 C33B N3 C25B N3 C21 N3 C25 DFIX 1.5 N3 C33 DFIX 1.55 C34 C33 DFIX 1.55 C34 C35 DFIX 1.55 C35 C36 DFIX 1.55 C35B C36B DFIX 1.55 C27B C26B C27B C28B DFIX 1.55 C27 C28 C27 C26 DFIX 1.55 C26 C25 C26 C27 DFIX 1.55 C26B C27B C26B C25B DFIX 1.55 C22B C21B DFIX 1.55 C23 C22B C23 C24 DFIX 1.55 C22B C21B C22B C23 DFIX 1.55 C22 C21 DFIX 1.55 C23B C24B DFIX 1.52 C35B C34B C35B C36B DFIX 1.52 C29 N3 C29 C30B DFIX 1.52 C30 C29 DFIX 1.52 C29 N3 C29 C30 DFIX 1.52 C31 C30 DFIX 1.52 C32 C31 DFIX 1.52 C31B C30B DFIX 1.52 C29B N3 C29B C30B DFIX 1.52 C30B C29B C30B C31B DFIX 1.52 C32B C31B DFIX 2.48 C29 C31 DFIX 2.48 C30 C32 DFIX 2.48 C29B C31B DFIX 2.48 C30B C32B DFIX 2.48 C26 C28 DFIX 2.48 C21 C23 DFIX 2.48 C22 N3 DFIX 2.48 C22 C24 DFIX 2.48 C34 C36 EADP C35 C35B EADP C33B C33 EADP C36B C36 EADP C34B C34 EADP C25B C25 EADP C26B C26 EADP C27B C27 EADP C28B C28 EADP C21 C21B EADP C22B C22 EADP C24 C23B EADP C23 C23B EADP C24 C24B EADP C32B C32 EADP C31 C31B EADP C30 C30B EADP C23 C27 EADP C23B C35B EADP C23 C35 EADP C32 C24 EADP C32B C24B EADP C31 C27 EADP C31B C27B EADP C30B C22B L.S. 50 PLAN 40 SIZE 0.03 0.8 0.8 TEMP 22.85 BOND $H LIST 6 ABIN fmap 2 acta OMIT -2 52 OMIT 2 0 0 OMIT -2 1 1 OMIT -2 2 1 OMIT -2 2 5 OMIT 1 6 0 OMIT 0 2 2 OMIT 0 0 2 REM REM REM WGHT 0.195800 FVAR 0.50421 S1 6 0.541313 0.180239 0.581324 11.00000 0.06979 0.03663 = 0.07142 -0.00361 0.02568 0.00000 N2 4 0.504422 0.356617 0.514777 11.00000 0.07795 0.04661 = 0.06118 0.00881 0.01735 0.00929 N1 4 0.347997 0.173987 0.612253 11.00000 0.07602 0.03960 = 0.08840 -0.00505 0.03473 0.00348 O3 5 0.364115 0.378955 0.418195 11.00000 0.09751 0.09454 = 0.06422 0.00521 0.00934 0.02096 O2 5 0.324252 0.284400 0.542064 11.00000 0.15641 0.06772 = 0.10775 0.02031 0.07692 0.02377 O4 5 0.630974 0.371762 0.620997 11.00000 0.10927 0.08775 = 0.08294 -0.00098 0.00315 -0.00644 O1 5 0.360850 0.089517 0.704007 11.00000 0.14168 0.06055 = 0.12393 0.02459 0.05399 0.01552 N3 4 0.884514 0.418720 0.782651 11.00000 0.09632 0.09622 = 0.09852 -0.04138 0.01768 -0.03176 C13 1 0.416439 0.393916 0.477695 11.00000 0.08490 0.05421 = 0.05988 0.00914 0.02214 0.00360 C14 1 0.406626 0.454591 0.527441 11.00000 0.10685 0.04467 = 0.07711 0.00452 0.03958 0.00684 C10 1 0.330726 0.253381 0.596958 11.00000 0.08771 0.05555 = 0.09593 0.00123 0.04340 0.00340 C3 1 0.349870 0.155267 0.680556 11.00000 0.08748 0.05790 = 0.08408 0.00358 0.03269 -0.00076 C2 1 0.358338 0.118081 0.560612 11.00000 0.07795 0.05075 = 0.10434 -0.02076 0.04027 -0.00851 AFIX 23 H2A 2 0.329448 0.139885 0.512874 11.00000 -1.20000 H2B 2 0.323753 0.070481 0.562180 11.00000 -1.20000 AFIX 0 C11 1 0.498901 0.214818 0.489922 11.00000 0.08245 0.05309 = 0.06453 -0.00717 0.02275 0.00854 AFIX 23 H11A 2 0.516337 0.177160 0.460672 11.00000 -1.20000 H11B 2 0.429155 0.218584 0.471779 11.00000 -1.20000 AFIX 0 C4 1 0.334541 0.228909 0.712675 11.00000 0.09521 0.05384 = 0.07270 0.00735 0.03030 0.00349 C9 1 0.323530 0.287478 0.663150 11.00000 0.08650 0.05793 = 0.09115 -0.01205 0.04079 -0.00214 C19 1 0.486832 0.452124 0.589062 11.00000 0.11304 0.04142 = 0.07657 -0.00734 0.03841 -0.01083 C1 1 0.463256 0.098095 0.575288 11.00000 0.07438 0.04239 = 0.09828 -0.00753 0.03400 -0.00538 AFIX 23 H1A 2 0.465546 0.063767 0.537536 11.00000 -1.20000 H1B 2 0.488517 0.069069 0.619820 11.00000 -1.20000 AFIX 0 C12 1 0.540483 0.293364 0.483542 11.00000 0.09895 0.05400 = 0.08019 0.00599 0.03849 0.01204 AFIX 23 H12A 2 0.610064 0.291013 0.506883 11.00000 -1.20000 H12B 2 0.525622 0.304681 0.433336 11.00000 -1.20000 AFIX 0 C20 1 0.552274 0.389506 0.579811 11.00000 0.09780 0.05233 = 0.06388 0.00835 0.01313 -0.00424 C15 1 0.332369 0.506724 0.519779 11.00000 0.12576 0.06279 = 0.11248 0.00788 0.05184 0.03013 AFIX 43 H15 2 0.276998 0.507938 0.478561 11.00000 -1.20000 AFIX 0 B2 3 0.658049 0.126168 0.597796 11.00000 0.06192 0.03518 = 0.07250 -0.00141 0.02150 0.00245 B9 3 0.674737 0.073063 0.527058 11.00000 0.07690 0.05693 = 0.07492 -0.00388 0.02416 0.01072 AFIX 153 H9 2 0.615156 0.063669 0.475538 11.00000 -1.20000 AFIX 0 B5 3 0.678610 0.022078 0.607117 11.00000 0.07259 0.03807 = 0.11190 0.00469 0.02618 -0.00118 AFIX 153 H5 2 0.629763 -0.027696 0.601994 11.00000 -1.20000 AFIX 0 C5 1 0.330120 0.245282 0.778728 11.00000 0.12507 0.10787 = 0.06567 -0.00384 0.03187 -0.00921 AFIX 43 H5A 2 0.337200 0.206086 0.812381 11.00000 -1.20000 AFIX 0 C18 1 0.498502 0.502977 0.646472 11.00000 0.17319 0.05602 = 0.09435 -0.01837 0.04628 -0.02020 AFIX 43 H18 2 0.553673 0.502123 0.687845 11.00000 -1.20000 AFIX 0 C16 1 0.344732 0.557133 0.576759 11.00000 0.17427 0.05196 = 0.16156 -0.00244 0.09614 0.01848 AFIX 43 H16 2 0.297366 0.594149 0.572824 11.00000 -1.20000 AFIX 0 C17 1 0.424482 0.553840 0.638370 11.00000 0.20812 0.04800 = 0.13322 -0.01674 0.09464 0.00125 AFIX 43 H17 2 0.428547 0.587190 0.675921 11.00000 -1.20000 AFIX 0 C8 1 0.306799 0.365560 0.677062 11.00000 0.16030 0.05427 = 0.14563 -0.00596 0.09117 -0.00072 AFIX 43 H8 2 0.298945 0.405313 0.643789 11.00000 -1.20000 AFIX 0 B6 3 0.747738 0.159212 0.565434 11.00000 0.06504 0.05500 = 0.08966 0.01820 0.02449 0.00238 AFIX 153 H6 2 0.744711 0.218159 0.542699 11.00000 -1.20000 AFIX 0 B1 3 0.703855 0.083165 0.679004 11.00000 0.08807 0.05789 = 0.08334 0.01005 0.03132 0.00083 AFIX 153 H1 2 0.678483 0.082139 0.723855 11.00000 -1.20000 AFIX 0 C6 1 0.314772 0.322163 0.792631 11.00000 0.17381 0.11371 = 0.09656 -0.03543 0.06194 -0.01737 AFIX 43 H6A 2 0.312613 0.334999 0.836947 11.00000 -1.20000 AFIX 0 B7 3 0.848986 0.102041 0.616985 11.00000 0.06329 0.05933 = 0.09592 0.00732 0.02625 -0.00032 AFIX 153 H7 2 0.926500 0.115150 0.635370 11.00000 -1.20000 AFIX 0 B3 3 0.778646 0.147869 0.660694 11.00000 0.08245 0.05944 = 0.08511 -0.01475 0.01739 -0.01337 AFIX 153 H3 2 0.808048 0.197032 0.697667 11.00000 -1.20000 AFIX 0 B8 3 0.780273 0.013846 0.581049 11.00000 0.07052 0.08075 = 0.11681 -0.02583 0.02563 0.01419 AFIX 153 H8A 2 0.804607 -0.044280 0.571233 11.00000 -1.20000 AFIX 0 B4 3 0.800721 0.040857 0.671106 11.00000 0.07449 0.07330 = 0.08558 0.02092 0.00951 0.00463 AFIX 153 H4 2 0.848000 0.005558 0.716135 11.00000 -1.20000 AFIX 0 C7 1 0.302806 0.379257 0.743742 11.00000 0.19203 0.07831 = 0.13693 -0.03089 0.09264 0.00158 AFIX 43 H7A 2 0.291380 0.430015 0.755347 11.00000 -1.20000 AFIX 0 B10 3 0.787118 0.086203 0.529823 11.00000 0.08717 0.10315 = 0.09465 0.01108 0.03184 0.02404 AFIX 153 H10 2 0.812434 0.085503 0.484941 11.00000 -1.20000 AFIX 0 PART 2 C21B 1 0.917924 0.506062 0.775662 10.66600 0.08769 0.09326 = 0.10723 -0.04347 0.02704 -0.03409 AFIX 23 H21A 2 0.914490 0.537492 0.814813 10.66600 -1.20000 H21B 2 0.984317 0.505729 0.778751 10.66600 -1.20000 AFIX 0 C26B 1 0.986784 0.410048 0.916260 10.66660 0.10602 0.06272 = 0.12039 -0.01706 0.03905 -0.01066 AFIX 23 H26A 2 0.927334 0.414362 0.925077 10.66660 -1.20000 H26B 2 1.015646 0.461612 0.920813 10.66660 -1.20000 AFIX 0 PART 0 PART 1 C22 1 10.875010 10.573520 10.739539 10.33333 0.18002 0.10262 = 0.10583 -0.02946 0.04649 -0.06194 AFIX 23 H22A 2 0.936519 0.566585 0.778556 10.33333 -1.20000 H22B 2 0.837101 0.602183 0.761540 10.33333 -1.20000 AFIX 0 PART 0 PART 2 C27B 1 1.057383 0.352265 0.970622 10.66660 0.17811 0.21318 = 0.17723 0.03916 0.04371 -0.04901 AFIX 23 H27A 2 1.026405 0.301858 0.968143 10.66660 -1.20000 H27B 2 1.114319 0.344762 0.958976 10.66660 -1.20000 AFIX 0 C33B 1 0.789519 0.422971 0.789603 10.66667 0.08575 0.11651 = 0.10076 -0.02968 0.04403 -0.00695 AFIX 23 H33A 2 0.741966 0.443386 0.745761 10.66667 -1.20000 H33B 2 0.793044 0.458119 0.828366 10.66667 -1.20000 AFIX 0 C28B 1 1.085635 0.385592 1.044897 10.66660 0.11829 0.12814 = 0.16729 0.00378 0.06694 0.01263 AFIX 137 H28A 2 1.112046 0.437045 1.046114 10.66660 -1.50000 H28B 2 1.133040 0.352385 1.078220 10.66660 -1.50000 H28C 2 1.029825 0.388588 1.057698 10.66660 -1.50000 AFIX 0 C25B 1 0.966654 0.377033 0.841512 10.66660 0.10410 0.07622 = 0.13491 0.00256 0.04364 -0.01101 AFIX 23 H25A 2 0.950823 0.321934 0.841217 10.66660 -1.20000 H25B 2 1.024806 0.381105 0.830905 10.66660 -1.20000 AFIX 0 PART 0 PART 1 C21 1 0.838130 0.498869 0.746291 10.33333 0.08769 0.09326 = 0.10723 -0.04347 0.02704 -0.03409 AFIX 23 H21C 2 0.800834 0.484133 0.697245 10.33333 -1.20000 H21D 2 0.790934 0.510236 0.767598 10.33333 -1.20000 AFIX 0 PART 0 PART 2 C23B 1 10.881961 10.628761 10.718850 10.66666 0.17811 0.21318 = 0.17723 0.03916 0.04371 -0.04901 AFIX 23 H23A 2 0.842891 0.649923 0.743867 10.66666 -1.20000 H23B 2 0.948001 0.628944 0.752784 10.66666 -1.20000 AFIX 0 PART 0 PART 1 C25 1 0.930048 0.432763 0.864452 10.33333 0.10410 0.07622 = 0.13491 0.00256 0.04364 -0.01101 AFIX 23 H25C 2 0.878524 0.450089 0.879416 10.33333 -1.20000 H25D 2 0.974068 0.476536 0.871882 10.33333 -1.20000 AFIX 0 PART 0 PART 2 C34B 1 0.759313 0.341348 0.804668 10.66667 0.11993 0.09274 = 0.10163 -0.03303 0.04926 -0.04108 AFIX 23 H34A 2 0.754791 0.305530 0.766140 10.66667 -1.20000 H34B 2 0.805180 0.320652 0.849112 10.66667 -1.20000 AFIX 0 C35B 1 0.663604 0.353000 0.809772 10.66667 0.17811 0.21318 = 0.17723 0.03916 0.04371 -0.04901 AFIX 23 H35A 2 0.619974 0.371164 0.763432 10.66667 -1.20000 H35B 2 0.670042 0.395248 0.843449 10.66667 -1.20000 AFIX 0 C36B 1 0.615350 0.286167 0.831400 10.66667 0.30956 0.08134 = 0.20186 -0.03371 0.14036 -0.07781 AFIX 137 H36A 2 0.658637 0.264322 0.875549 10.66667 -1.50000 H36B 2 0.598239 0.246706 0.794844 10.66667 -1.50000 H36C 2 0.558247 0.304634 0.837668 10.66667 -1.50000 AFIX 0 PART 0 PART 1 C33 1 0.811330 0.352252 0.782803 10.33333 0.08575 0.11651 = 0.10076 -0.02968 0.04403 -0.00695 AFIX 23 H33C 2 0.772111 0.340812 0.733330 10.33333 -1.20000 H33D 2 0.848647 0.305552 0.802512 10.33333 -1.20000 AFIX 0 C34 1 0.743195 0.365168 0.822415 10.33333 0.11993 0.09274 = 0.10163 -0.03303 0.04926 -0.04108 AFIX 23 H34C 2 0.777694 0.343802 0.869689 10.33333 -1.20000 H34D 2 0.743502 0.421446 0.828889 10.33333 -1.20000 AFIX 0 C35 1 0.638970 0.341789 0.806130 10.33333 0.17811 0.21318 = 0.17723 0.03916 0.04371 -0.04901 AFIX 23 H35C 2 0.616917 0.364029 0.841768 10.33333 -1.20000 H35D 2 0.598516 0.361993 0.759650 10.33333 -1.20000 AFIX 0 C36 1 0.631016 0.253867 0.806528 10.33333 0.30956 0.08134 = 0.20186 -0.03371 0.14036 -0.07781 AFIX 137 H36D 2 0.639537 0.232783 0.765015 10.33333 -1.50000 H36E 2 0.568575 0.239471 0.805949 10.33333 -1.50000 H36F 2 0.679869 0.233336 0.848875 10.33333 -1.50000 AFIX 0 C28 1 1.097203 0.337128 1.041043 10.33333 0.11829 0.12814 = 0.16729 0.00378 0.06694 0.01263 AFIX 137 H28D 2 1.136376 0.315562 1.016963 10.33333 -1.50000 H28E 2 1.058604 0.296423 1.049797 10.33333 -1.50000 H28F 2 1.137899 0.359621 1.085740 10.33333 -1.50000 AFIX 0 C27 1 1.031825 0.400144 0.994516 10.33333 0.17811 0.21318 = 0.17723 0.03916 0.04371 -0.04901 AFIX 23 H27C 2 1.068844 0.446824 0.994573 10.33333 -1.20000 H27D 2 0.982052 0.413807 1.012689 10.33333 -1.20000 AFIX 0 C26 1 0.985880 0.366898 0.917753 10.33333 0.10602 0.06272 = 0.12039 -0.01706 0.03905 -0.01066 AFIX 23 H26C 2 0.941852 0.324855 0.917009 10.33333 -1.20000 H26D 2 1.035866 0.345602 0.902999 10.33333 -1.20000 AFIX 0 PART 0 PART 2 C22B 1 10.853001 10.542689 10.703589 10.66660 0.18002 0.10262 = 0.10583 -0.02946 0.04649 -0.06194 AFIX 23 H22C 2 0.868109 0.522508 0.663876 10.66660 -1.20000 H22D 2 0.785113 0.534658 0.694274 10.66660 -1.20000 AFIX 0 PART 0 PART 1 C24 1 10.831910 10.661751 10.631921 10.33330 0.17811 0.21318 = 0.17723 0.03916 0.04371 -0.04901 AFIX 137 H24A 2 0.850764 0.634205 0.597573 10.33330 -1.50000 H24B 2 0.832349 0.717047 0.623550 10.33330 -1.50000 H24C 2 0.768217 0.645772 0.627254 10.33330 -1.50000 AFIX 0 C23 1 10.904180 10.642590 10.709049 10.33330 0.17811 0.21318 = 0.17723 0.03916 0.04371 -0.04901 AFIX 23 H23C 2 0.967593 0.633553 0.707630 10.33330 -1.20000 H23D 2 0.908618 0.687322 0.739809 10.33330 -1.20000 AFIX 0 PART 0 PART 2 C24B 1 10.877390 10.687730 10.661251 10.66666 0.17811 0.21318 = 0.17723 0.03916 0.04371 -0.04901 AFIX 137 H24D 2 0.900175 0.663823 0.627264 10.66666 -1.50000 H24E 2 0.917119 0.732015 0.682737 10.66666 -1.50000 H24F 2 0.811984 0.704652 0.637318 10.66666 -1.50000 AFIX 0 C29B 1 0.877155 0.375038 0.714182 10.66666 0.13637 0.09218 = 0.12638 -0.02164 0.07307 -0.04485 AFIX 23 H29A 2 0.859525 0.321216 0.718735 10.66666 -1.20000 H29B 2 0.824686 0.398018 0.674602 10.66666 -1.20000 AFIX 0 C30B 1 0.965439 0.374099 0.694564 10.66667 0.18002 0.10262 = 0.10583 -0.02946 0.04649 -0.06194 AFIX 23 H30A 2 0.982352 0.427278 0.686973 10.66667 -1.20000 H30B 2 1.019208 0.351727 0.733574 10.66667 -1.20000 AFIX 0 C31B 1 0.947145 0.326965 0.627956 10.66667 0.17811 0.21318 = 0.17723 0.03916 0.04371 -0.04901 AFIX 23 H31A 2 0.902011 0.354085 0.586845 10.66667 -1.20000 H31B 2 0.919976 0.276455 0.632085 10.66667 -1.20000 AFIX 0 PART 0 PART 1 C29 1 0.956918 0.375602 0.761964 10.33333 0.08941 0.21969 = 0.08133 -0.02687 0.02739 0.00322 AFIX 23 H29C 2 0.974643 0.326816 0.788253 10.33333 -1.20000 H29D 2 1.014538 0.406936 0.771610 10.33333 -1.20000 AFIX 0 C30 1 0.908536 0.360215 0.683154 10.33333 0.18002 0.10262 = 0.10583 -0.02946 0.04649 -0.06194 AFIX 23 H30C 2 0.891317 0.409378 0.657434 10.33333 -1.20000 H30D 2 0.850050 0.330184 0.674025 10.33333 -1.20000 AFIX 0 C31 1 0.977707 0.314696 0.657592 10.33333 0.17811 0.21318 = 0.17723 0.03916 0.04371 -0.04901 AFIX 23 H31C 2 0.977710 0.259417 0.668605 10.33333 -1.20000 H31D 2 1.042879 0.334818 0.679032 10.33333 -1.20000 AFIX 0 PART 0 PART 2 C32B 1 1.043608 0.316182 0.618967 10.66660 0.17811 0.21318 = 0.17723 0.03916 0.04371 -0.04901 AFIX 137 H32A 2 1.081236 0.363062 0.633633 10.66660 -1.50000 H32B 2 1.032443 0.305589 0.569671 10.66660 -1.50000 H32C 2 1.077775 0.273118 0.647947 10.66660 -1.50000 AFIX 0 PART 0 PART 1 C32 1 0.934453 0.329446 0.573278 10.33333 0.17811 0.21318 = 0.17723 0.03916 0.04371 -0.04901 AFIX 137 H32D 2 0.872137 0.353458 0.559997 10.33333 -1.50000 H32E 2 0.928470 0.280400 0.548711 10.33333 -1.50000 H32F 2 0.976737 0.363351 0.560414 10.33333 -1.50000 AFIX 0 HKLF 4 REM 19kub41_0m_a.res in P2(1)/c REM R1 = 0.1130 for 3150 Fo > 4sig(Fo) and 0.2300 for all 9086 data REM 495 parameters refined using 46 restraints END WGHT 0.1954 0.0000 REM Highest difference peak 0.480, deepest hole -0.471, 1-sigma level 0.078 Q1 1 0.9778 0.6227 0.6792 11.00000 0.05 0.38 Q2 1 0.5897 0.2809 0.7512 11.00000 0.05 0.30 Q3 1 0.8155 0.4763 0.7641 11.00000 0.05 0.30 Q4 1 0.8494 0.3820 0.4961 11.00000 0.05 0.27 Q5 1 1.1497 0.4374 1.1304 11.00000 0.05 0.27 Q6 1 0.9082 0.5039 0.8525 11.00000 0.05 0.26 Q7 1 0.5997 0.0169 0.6735 11.00000 0.05 0.25 Q8 1 1.0135 0.3078 0.7065 11.00000 0.05 0.24 Q9 1 0.9905 0.2698 0.7196 11.00000 0.05 0.24 Q10 1 0.6732 0.2872 0.8103 11.00000 0.05 0.23 Q11 1 0.4498 0.5659 0.7635 11.00000 0.05 0.23 Q12 1 0.2383 0.5915 0.5306 11.00000 0.05 0.23 Q13 1 0.9634 0.2878 0.6789 11.00000 0.05 0.23 Q14 1 0.8804 0.2859 0.8669 11.00000 0.05 0.23 Q15 1 0.5624 0.1880 0.6648 11.00000 0.05 0.22 Q16 1 0.5341 0.3493 0.7821 11.00000 0.05 0.22 Q17 1 0.5224 0.3786 0.7188 11.00000 0.05 0.21 Q18 1 0.6296 -0.0217 0.5499 11.00000 0.05 0.21 Q19 1 1.0559 0.5793 0.7269 11.00000 0.05 0.20 Q20 1 0.8236 0.3522 0.5374 11.00000 0.05 0.20 Q21 1 0.7416 0.2737 0.9338 11.00000 0.05 0.20 Q22 1 0.4845 0.3189 0.7761 11.00000 0.05 0.20 Q23 1 1.1735 0.2697 1.0997 11.00000 0.05 0.20 Q24 1 0.8430 0.1005 0.7228 11.00000 0.05 0.20 Q25 1 0.5336 0.2571 0.6890 11.00000 0.05 0.20 Q26 1 0.5397 0.2182 0.5829 11.00000 0.05 0.19 Q27 1 0.5386 0.5759 0.7192 11.00000 0.05 0.19 Q28 1 0.5134 0.6219 0.7245 11.00000 0.05 0.19 Q29 1 0.4581 0.3013 0.8259 11.00000 0.05 0.19 Q30 1 0.9626 0.5582 0.7057 11.00000 0.05 0.19 Q31 1 1.1093 0.4077 0.6699 11.00000 0.05 0.19 Q32 1 1.0971 0.3984 0.6915 11.00000 0.05 0.19 Q33 1 0.6265 0.0848 0.7193 11.00000 0.05 0.19 Q34 1 0.7277 0.1661 0.4834 11.00000 0.05 0.19 Q35 1 0.5314 0.1172 0.6995 11.00000 0.05 0.19 Q36 1 0.6729 0.0802 0.5969 11.00000 0.05 0.19 Q37 1 0.8963 0.6235 0.5915 11.00000 0.05 0.19 Q38 1 0.4180 0.3324 0.8143 11.00000 0.05 0.18 Q39 1 0.5097 0.2971 0.7569 11.00000 0.05 0.18 Q40 1 1.1704 0.3801 0.6439 11.00000 0.05 0.18 ; _shelx_res_checksum 87768 _shelx_hkl_file ; 2 0 0 960.20 27.00 2 0 0 998.70 28.50 -2 0 0 922.31 28.20 -3 0 0 7879.81 210.58 3 0 0 7850.21 210.88 -4 0 0 2494.05 69.89 4 0 0 2408.16 70.19 -5 0 0 3408.86 97.69 5 0 0 3527.75 98.49 6 0 0 4868.01 132.09 -6 0 0 4474.05 130.59 7 0 0 2239.68 68.99 -7 0 0 2161.38 67.59 -8 0 0 24.70 9.60 8 0 0 14.80 9.70 -9 0 0 1038.90 39.60 9 0 0 1070.29 41.80 10 0 0 214.08 20.00 -10 0 0 190.28 17.40 -11 0 0 3.00 10.40 11 0 0 1.70 11.70 -12 0 0 -7.50 9.20 12 0 0 -5.90 12.00 13 0 0 -14.80 11.70 -13 0 0 -12.20 11.00 14 0 0 12.30 12.00 15 0 0 9.40 12.40 16 0 0 7.50 10.70 17 0 0 0.20 7.10 19 0 0 10.80 8.50 1 -1 0 34.70 3.10 -1 1 0 25.20 2.60 2 -1 0 3844.32 100.19 -2 1 0 3587.64 99.79 2 1 0 3616.64 98.99 2 1 0 3623.14 98.69 3 -1 0 46.70 7.20 3 1 0 49.00 5.50 3 1 0 52.89 6.40 -3 1 0 40.30 6.30 4 -1 0 7566.04 196.38 -4 -1 0 6568.74 193.98 -4 1 0 7363.26 195.68 4 1 0 7387.46 194.68 5 -1 0 5289.47 147.89 -5 -1 0 5135.89 145.79 -5 1 0 5335.77 146.99 5 1 0 5539.15 146.79 6 -1 0 13.30 10.40 -6 -1 0 28.90 9.20 6 1 0 6.30 8.70 -6 1 0 16.90 9.60 7 -1 0 33.10 13.90 7 1 0 21.90 10.50 -7 1 0 31.90 10.20 8 -1 0 -3.90 9.70 -8 -1 0 13.50 8.30 8 1 0 8.40 9.40 -8 1 0 0.10 8.30 -9 -1 0 190.28 15.90 9 -1 0 192.88 19.10 -9 1 0 172.88 16.10 9 1 0 165.38 17.30 -10 -1 0 62.39 12.10 10 -1 0 57.99 14.50 10 1 0 42.50 13.60 -10 1 0 60.19 11.60 -11 -1 0 85.79 13.90 11 -1 0 65.39 15.90 -11 1 0 92.59 14.80 11 1 0 51.99 13.80 12 -1 0 -0.90 11.90 -12 -1 0 16.50 11.10 12 1 0 1.90 13.10 -12 1 0 0.40 10.40 13 -1 0 5.30 12.00 -13 -1 0 0.50 10.10 13 1 0 5.80 13.60 14 -1 0 4.10 13.60 14 1 0 -4.20 14.30 15 -1 0 11.30 12.60 15 1 0 8.30 11.90 16 -1 0 7.00 10.30 16 1 0 16.40 11.60 17 -1 0 18.10 12.40 17 1 0 0.80 10.90 18 -1 0 7.90 9.90 18 1 0 6.90 9.30 19 -1 0 16.30 9.70 19 1 0 17.20 9.20 0 -2 0 31.40 4.30 0 2 0 39.50 3.80 0 2 0 33.10 4.00 -1 -2 0 2121.19 57.09 1 -2 0 2134.79 58.49 1 2 0 1958.00 56.79 -1 2 0 2090.29 58.29 1 2 0 2152.98 57.99 2 -2 0 1.50 5.50 -2 -2 0 8.30 4.20 2 2 0 -3.10 4.10 2 2 0 9.80 4.50 -2 2 0 -3.70 4.70 3 -2 0 2175.88 63.39 3 2 0 2241.48 61.89 3 2 0 2088.19 60.59 -3 2 0 2212.58 62.99 4 -2 0 44.60 8.60 -4 2 0 37.30 6.80 4 2 0 42.60 6.10 4 2 0 43.60 6.40 5 -2 0 505.35 23.00 -5 2 0 541.55 22.10 5 2 0 505.65 20.40 6 -2 0 308.47 20.80 6 2 0 305.57 17.60 -6 2 0 297.97 28.40 -7 -2 0 21.90 9.40 7 -2 0 3.50 11.70 7 2 0 -0.70 9.40 -7 2 0 9.80 9.30 -8 -2 0 25.00 8.60 8 -2 0 23.50 11.90 -8 2 0 35.60 10.20 9 -2 0 77.09 15.50 -9 -2 0 106.39 13.90 -9 2 0 92.89 13.00 9 2 0 59.29 11.70 10 -2 0 159.98 19.40 -10 -2 0 176.48 16.40 -10 2 0 175.18 16.90 10 2 0 180.48 18.30 11 -2 0 6.30 12.00 -11 -2 0 12.60 10.10 11 2 0 4.90 10.30 -11 2 0 15.90 16.10 -12 -2 0 10.60 15.70 12 -2 0 -1.00 13.60 12 2 0 5.40 12.10 -12 2 0 4.20 10.90 -13 -2 0 -9.40 9.80 13 -2 0 -2.20 14.90 13 2 0 3.50 10.90 14 -2 0 13.30 12.90 14 2 0 12.50 11.20 15 -2 0 11.70 12.50 15 2 0 1.00 9.40 16 -2 0 18.80 14.20 16 2 0 3.30 8.30 17 -2 0 0.50 10.20 17 2 0 4.80 9.50 18 -2 0 14.40 9.90 18 2 0 27.80 11.50 0 -3 0 3.00 5.90 0 3 0 -1.60 5.80 0 3 0 1.30 3.90 1 -3 0 5162.08 137.39 -1 -3 0 4915.61 135.59 1 3 0 4882.41 135.59 -1 3 0 5108.99 134.99 1 3 0 5164.08 136.69 -1 3 0 5076.79 136.99 2 -3 0 305.17 14.80 -2 -3 0 293.07 11.90 -2 3 0 305.67 10.00 2 3 0 290.47 12.00 -2 3 0 270.77 15.00 2 3 0 314.57 13.40 3 -3 0 949.71 32.00 -3 -3 0 944.11 29.00 3 3 0 956.30 30.50 3 3 0 937.31 28.60 -3 3 0 950.40 31.50 4 -3 0 1513.95 48.20 -4 -3 0 1499.95 44.80 -4 3 0 1498.65 47.40 4 3 0 1556.14 44.70 4 3 0 1537.35 46.40 5 -3 0 704.53 28.50 -5 -3 0 714.73 24.80 -5 3 0 669.03 27.00 5 3 0 701.43 25.10 6 -3 0 -7.90 9.10 -6 -3 0 -6.70 5.30 6 3 0 -6.30 8.60 -6 3 0 -8.90 8.70 7 -3 0 295.87 21.70 7 3 0 327.27 18.70 -7 3 0 335.57 20.20 8 -3 0 35.50 11.50 8 3 0 61.59 11.80 -8 3 0 82.39 12.80 9 -3 0 68.79 14.20 -9 -3 0 43.70 8.80 -9 3 0 92.89 13.80 9 3 0 78.09 12.10 10 -3 0 318.27 24.40 -10 -3 0 305.17 20.00 10 3 0 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9.70 -1 6 0 86.89 8.30 -1 6 0 101.19 11.20 1 6 0 74.59 9.60 1 6 0 106.79 10.70 2 -6 0 299.47 18.10 -2 -6 0 290.17 14.70 -2 6 0 301.07 13.30 2 6 0 309.77 16.20 2 6 0 303.17 15.00 -2 6 0 313.07 18.10 3 -6 0 383.26 22.00 -3 -6 0 405.86 17.70 3 6 0 407.36 19.80 3 6 0 372.06 17.40 -3 6 0 398.86 22.20 -4 -6 0 778.42 27.30 4 -6 0 766.32 33.10 4 6 0 718.73 29.70 -4 6 0 707.13 30.90 4 6 0 728.13 26.60 5 -6 0 73.69 15.30 -5 -6 0 93.79 11.60 5 6 0 86.99 10.90 5 6 0 65.79 12.10 -5 6 0 82.19 15.10 -6 -6 0 57.69 10.20 6 -6 0 42.80 13.70 6 6 0 41.10 9.40 -6 6 0 57.99 12.70 7 -6 0 133.79 17.40 -7 -6 0 149.19 13.00 7 6 0 131.29 13.00 -7 6 0 133.59 14.50 8 -6 0 -10.40 9.50 -8 -6 0 10.40 7.60 -8 6 0 16.80 9.40 8 6 0 5.60 7.80 -9 -6 0 -0.30 7.70 9 -6 0 -9.90 11.30 9 6 0 -2.80 7.70 -9 6 0 -1.10 9.00 -10 -6 0 97.99 14.40 10 -6 0 94.39 19.90 -10 6 0 76.29 14.70 -11 -6 0 33.40 11.00 11 -6 0 37.40 15.40 11 6 0 10.00 9.00 12 -6 0 16.20 15.00 -12 -6 0 -5.80 8.50 12 6 0 1.70 7.90 13 -6 0 11.80 17.40 -13 -6 0 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11.50 3 11 0 36.80 12.10 3 11 0 16.30 9.90 4 -11 0 10.80 11.00 4 11 0 -0.90 9.10 -4 11 0 0.80 10.80 4 11 0 -4.50 8.90 5 -11 0 27.20 12.70 5 11 0 46.00 10.50 -5 11 0 39.30 11.70 6 -11 0 -9.50 11.70 -6 -11 0 2.90 7.70 -6 11 0 2.20 11.40 6 11 0 5.20 9.30 7 -11 0 85.49 19.70 -7 -11 0 102.99 13.70 -7 11 0 64.69 13.70 7 11 0 88.19 12.80 -8 -11 0 8.70 8.50 8 -11 0 -6.70 13.00 -8 11 0 1.40 9.00 9 -11 0 -7.20 23.30 -9 -11 0 17.70 9.30 9 11 0 4.90 7.20 -10 -11 0 3.70 7.90 10 -11 0 -13.30 15.40 10 11 0 5.10 7.20 11 -11 0 -0.80 17.30 -11 -11 0 -0.60 8.70 11 11 0 2.50 7.20 12 -11 0 -2.00 16.90 -12 -11 0 -0.80 8.80 12 11 0 2.40 6.80 -13 -11 0 0.80 9.70 13 -11 0 -10.40 17.40 13 11 0 -0.70 6.90 14 -11 0 16.80 18.70 -14 -11 0 5.30 10.50 14 11 0 6.50 7.90 15 -11 0 18.30 19.00 15 11 0 6.70 7.80 16 11 0 19.20 9.00 0 12 0 12.20 11.70 0 12 0 25.80 12.00 -1 12 0 32.50 11.80 1 12 0 29.10 12.00 2 -12 0 38.10 13.10 2 12 0 87.39 14.70 -2 12 0 80.89 16.90 2 12 0 52.49 13.20 3 -12 0 18.90 12.50 3 12 0 18.00 11.70 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8.40 15 -11 -3 14.40 19.40 15 11 -3 8.40 9.00 14 -11 -3 20.80 16.90 14 11 -3 9.70 9.50 13 -11 -3 7.40 14.60 -13 -11 3 -3.60 9.00 13 11 -3 5.40 8.20 12 -11 -3 3.10 13.80 -12 -11 3 -12.10 8.90 12 11 -3 -0.10 8.50 11 -11 -3 0.20 14.00 -11 -11 3 19.80 11.30 11 11 -3 13.50 12.40 -10 -11 3 65.59 14.20 10 -11 -3 35.60 15.90 10 11 -3 18.30 12.80 10 11 -3 53.99 14.50 9 -11 -3 14.70 13.10 -9 -11 3 30.90 12.20 -9 11 3 17.70 13.00 9 11 -3 12.10 12.00 9 11 -3 30.60 13.30 8 -11 -3 27.70 13.60 -8 -11 3 36.40 12.10 8 11 -3 42.60 12.40 -8 11 3 45.50 13.80 8 11 -3 40.80 13.40 -7 -11 3 40.90 12.30 7 -11 -3 25.10 12.40 7 11 -3 16.40 10.20 7 11 -3 23.40 12.30 -7 11 3 27.90 10.70 6 -11 -3 24.40 11.20 -6 -11 3 57.59 12.80 -6 11 3 44.40 12.00 6 11 -3 22.60 12.40 6 11 -3 48.10 12.00 -5 -11 3 3.80 8.40 5 -11 -3 6.30 9.50 5 11 -3 4.80 10.70 5 11 -3 -7.60 8.10 -5 11 3 9.20 8.30 4 -11 -3 544.75 28.30 4 11 -3 601.34 28.90 4 11 -3 533.25 28.10 -4 11 3 564.14 27.20 3 -11 -3 164.88 16.20 3 11 -3 187.48 17.30 -3 11 3 169.98 16.70 3 11 -3 159.88 18.70 3 11 -3 176.98 20.20 2 -11 -3 2.50 7.90 2 11 -3 1.40 10.90 2 11 -3 6.10 11.00 -2 11 3 3.00 8.10 1 -11 -3 -1.10 8.30 1 11 -3 -12.00 9.80 1 11 -3 -2.80 10.70 -1 11 3 1.90 7.30 0 11 3 71.29 12.60 0 11 -3 78.29 16.00 0 11 3 59.29 11.90 0 11 -3 37.90 13.10 -1 11 -3 21.20 12.60 1 11 3 19.30 9.20 1 11 3 20.40 10.00 -1 11 -3 23.30 11.70 -2 11 -3 53.89 13.90 2 11 3 43.80 10.20 3 -11 3 37.20 14.40 -3 11 -3 50.99 13.10 -3 11 -3 45.90 9.60 4 -11 3 12.30 14.20 -4 11 -3 -3.20 6.70 -4 11 -3 -1.90 11.20 5 -11 3 127.59 21.10 -5 11 -3 146.69 20.60 -5 11 -3 109.49 11.40 6 -11 3 29.50 16.30 -6 11 -3 2.60 9.40 7 -11 3 -9.30 15.10 8 -11 3 23.20 18.70 9 -11 3 -14.30 15.00 10 -11 3 21.70 17.50 10 11 3 8.80 6.20 11 -11 3 1.00 15.80 11 11 3 2.60 8.20 12 -11 3 15.70 18.10 12 11 3 2.60 5.50 13 -11 3 -1.60 17.10 -13 -11 -3 5.90 9.10 13 11 3 8.20 6.20 -14 -11 -3 -1.20 12.30 14 -11 3 -6.70 16.40 14 11 3 7.30 6.10 15 11 3 20.80 8.60 17 12 -3 33.20 9.90 16 12 -3 20.00 10.10 15 -12 -3 29.90 17.20 15 12 -3 13.70 8.90 14 -12 -3 20.30 16.40 14 12 -3 24.60 9.40 -13 -12 3 0.70 9.60 13 -12 -3 8.20 15.50 13 12 -3 1.40 8.40 -12 -12 3 13.40 10.60 12 -12 -3 16.50 15.90 12 12 -3 8.20 8.70 -11 -12 3 2.40 9.60 11 -12 -3 -3.60 13.20 11 12 -3 12.70 12.70 -10 -12 3 32.40 12.40 10 -12 -3 9.20 14.50 10 12 -3 35.40 13.70 -9 -12 3 8.10 10.20 9 -12 -3 7.30 12.80 9 12 -3 9.70 11.50 9 12 -3 9.40 12.00 8 -12 -3 11.70 12.50 -8 -12 3 26.80 11.20 -8 12 3 15.30 12.50 8 12 -3 16.30 11.70 8 12 -3 7.90 12.40 7 -12 -3 -0.70 13.00 -7 -12 3 5.00 9.70 7 12 -3 20.40 13.10 -7 12 3 19.00 10.50 7 12 -3 28.60 12.70 -6 -12 3 108.29 16.30 6 -12 -3 63.49 13.60 6 12 -3 74.89 15.10 -6 12 3 101.69 16.70 6 12 -3 98.89 15.50 5 -12 -3 2.80 9.40 -5 12 3 6.00 9.40 5 12 -3 8.00 11.30 5 12 -3 21.60 10.70 4 -12 -3 -0.70 8.10 -4 12 3 10.50 9.70 4 12 -3 27.10 12.60 4 12 -3 11.40 11.30 4 12 -3 6.10 8.70 -3 12 3 120.79 16.30 3 12 -3 107.29 17.90 3 12 -3 86.09 14.50 3 12 -3 82.79 15.70 2 -12 -3 67.39 12.20 -2 12 3 106.29 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3 10.70 10.90 12 13 -3 -6.70 7.50 -11 -13 3 -1.40 10.10 11 -13 -3 -0.30 13.10 11 13 -3 -5.90 11.40 10 -13 -3 1.20 13.50 -10 -13 3 0.10 8.40 10 13 -3 -0.30 11.80 9 -13 -3 -0.50 12.00 -9 -13 3 2.20 9.90 9 13 -3 -7.70 11.90 8 -13 -3 -2.80 11.90 -8 -13 3 8.10 9.70 8 13 -3 0.90 11.80 8 13 -3 2.60 11.70 -7 -13 3 96.69 16.70 7 -13 -3 36.50 13.20 7 13 -3 72.39 15.60 -7 13 3 86.59 17.50 7 13 -3 54.99 17.50 6 13 -3 164.88 19.60 -6 13 3 115.09 23.20 6 13 -3 143.39 18.50 5 13 -3 127.19 18.30 5 13 -3 175.78 22.90 -5 13 3 105.49 15.20 5 13 -3 96.79 15.80 4 -13 -3 10.60 9.20 -4 13 3 32.70 12.10 4 13 -3 47.40 15.70 4 13 -3 42.90 14.70 4 13 -3 31.80 11.50 3 -13 -3 5.10 10.90 3 13 -3 2.00 12.30 -3 13 3 13.00 10.60 3 13 -3 7.80 9.40 3 13 -3 4.10 12.50 2 -13 -3 75.29 13.20 2 13 -3 128.99 15.90 2 13 -3 194.18 26.10 2 13 -3 119.29 19.50 -1 13 3 181.28 18.80 1 13 -3 140.29 20.20 1 13 -3 80.19 14.10 1 13 -3 116.89 20.50 0 13 3 60.49 14.80 0 13 -3 24.60 10.10 0 13 3 47.50 13.20 0 13 -3 42.60 15.10 0 13 -3 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39.20 13.30 7 14 -3 49.40 14.80 6 -14 -3 0.80 8.80 -6 14 3 11.20 9.80 6 14 -3 9.50 12.10 6 14 -3 5.70 13.00 5 -14 -3 5.90 10.50 5 14 -3 7.40 13.50 5 14 -3 4.20 11.00 -5 14 3 6.60 9.70 5 14 -3 6.40 15.10 4 14 -3 73.59 17.20 4 14 -3 108.09 20.90 4 14 -3 69.69 14.80 -4 14 3 106.39 17.70 3 -14 -3 174.98 20.00 3 14 -3 166.58 22.80 3 14 -3 180.88 19.80 3 14 -3 220.68 26.20 -3 14 3 218.18 21.50 -2 14 3 33.40 13.00 2 14 -3 44.20 15.80 2 14 -3 7.40 10.60 2 14 -3 9.80 13.00 -1 14 3 32.50 14.00 -1 14 3 39.50 12.90 1 14 -3 30.50 15.00 1 14 -3 26.60 11.30 1 14 -3 35.90 16.20 0 14 -3 6.40 10.30 0 14 3 -15.20 22.10 0 14 -3 -0.80 14.10 0 14 -3 -31.50 13.10 0 14 3 2.80 11.50 1 14 3 7.10 12.80 -1 14 -3 12.60 9.70 -1 14 -3 6.60 16.20 -1 14 -3 25.60 16.40 1 14 3 -8.20 10.80 -2 14 -3 1.40 9.20 -2 14 -3 16.80 15.70 2 14 3 21.60 12.50 -2 14 -3 -1.80 11.30 2 14 3 7.80 10.60 -3 14 -3 116.49 22.30 -3 14 -3 111.99 14.50 4 -14 3 11.40 13.80 -4 14 -3 14.10 14.80 5 -14 3 4.00 23.20 6 -14 3 9.60 13.50 7 -14 3 7.70 13.00 8 -14 3 11.10 14.00 9 -14 3 -1.70 11.50 10 -14 3 6.60 12.40 11 -14 3 14.20 10.60 12 -14 3 26.00 21.60 13 -14 3 15.80 24.10 15 15 -3 23.00 9.40 14 -15 -3 1.90 15.00 14 15 -3 -5.30 9.90 13 -15 -3 7.60 12.50 13 15 -3 1.20 8.10 -12 -15 3 5.10 11.50 12 -15 -3 -2.30 12.00 12 15 -3 1.00 9.20 -11 -15 3 7.10 10.90 11 -15 -3 -2.90 10.30 11 15 -3 -7.10 12.40 10 -15 -3 -12.60 8.70 10 15 -3 -2.30 12.00 -9 -15 3 11.00 9.90 9 -15 -3 -3.70 10.40 9 15 -3 -2.50 12.40 8 -15 -3 -3.70 8.40 8 15 -3 -0.20 12.70 7 -15 -3 0.80 10.80 7 15 -3 -12.10 12.70 7 15 -3 2.00 13.50 6 -15 -3 3.10 9.20 -6 15 3 18.40 10.90 6 15 -3 -6.90 10.60 6 15 -3 5.70 15.70 6 15 -3 -0.30 12.70 5 -15 -3 -2.00 9.20 5 15 -3 0.80 10.60 5 15 -3 -5.10 14.20 5 15 -3 2.70 14.20 -5 15 3 14.00 9.90 4 -15 -3 9.40 10.60 4 15 -3 43.90 16.60 4 15 -3 33.00 13.50 -4 15 3 68.79 15.80 4 15 -3 19.10 14.80 3 -15 -3 5.20 10.30 3 15 -3 -6.40 13.60 3 15 -3 1.60 13.90 -3 15 3 1.60 10.10 3 15 -3 3.70 10.50 -2 15 3 14.10 13.20 2 15 -3 29.60 15.40 2 15 -3 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4 11.70 9.50 18 8 -4 13.80 8.50 17 -8 -4 15.70 14.70 17 8 -4 12.10 9.40 16 -8 -4 18.50 17.80 16 8 -4 3.90 9.80 15 -8 -4 24.20 16.10 15 8 -4 0.70 8.30 14 -8 -4 11.70 15.20 14 8 -4 1.60 8.20 13 -8 -4 0.00 14.80 -13 -8 4 -6.40 4.70 13 8 -4 -3.60 7.80 -12 -8 4 -0.20 6.60 12 -8 -4 6.20 12.60 12 8 -4 -1.30 9.40 12 8 -4 -5.50 9.40 11 -8 -4 13.10 13.50 11 8 -4 2.10 10.70 11 8 -4 11.40 11.30 10 -8 -4 2.10 11.40 -10 -8 4 -5.30 3.20 10 8 -4 1.70 9.40 10 8 -4 9.00 11.90 -10 8 4 2.40 10.30 9 -8 -4 8.10 11.40 -9 -8 4 -0.80 4.20 9 8 -4 4.30 9.70 9 8 -4 7.10 11.00 8 -8 -4 250.07 21.70 8 8 -4 253.37 20.10 -8 8 4 247.18 19.20 -7 -8 4 38.80 9.70 7 -8 -4 35.50 10.90 -7 8 4 57.19 11.20 7 8 -4 46.60 12.00 6 -8 -4 113.99 9.20 6 -8 -4 101.69 13.60 -6 -8 4 104.69 13.60 6 8 -4 104.29 14.70 -6 8 4 105.99 13.20 -5 -8 4 19.10 10.00 5 -8 -4 17.40 9.80 5 8 -4 37.30 14.80 -5 8 4 9.90 8.20 4 -8 -4 28.20 10.70 -4 -8 4 50.09 11.40 4 8 -4 17.80 11.50 -4 8 4 37.90 10.60 3 -8 -4 11.20 9.20 -3 -8 4 41.60 12.70 3 8 -4 50.79 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4 4.50 9.10 5 -10 -4 3.50 8.60 5 -10 -4 2.00 5.60 -5 -10 4 4.40 5.00 -5 10 4 7.00 8.00 5 10 -4 3.60 10.50 4 -10 -4 5.70 7.30 -4 -10 4 19.30 9.90 -4 10 4 9.30 7.60 4 10 -4 22.00 11.90 3 -10 -4 4.20 6.10 3 -10 -4 -5.20 6.30 3 10 -4 -7.20 10.30 -3 10 4 9.90 7.20 2 -10 -4 26.90 8.00 2 -10 -4 7.20 6.10 2 10 -4 27.30 12.00 2 10 -4 50.99 14.40 -2 10 4 37.00 8.70 1 -10 -4 54.99 10.20 1 -10 -4 60.39 9.90 1 10 -4 61.39 15.60 1 10 -4 67.39 14.70 -1 10 4 78.29 10.70 0 -10 -4 20.30 9.20 0 10 -4 35.70 13.80 0 10 4 25.80 8.90 0 10 -4 42.70 13.80 -1 -10 -4 3.80 6.70 -1 10 -4 2.20 10.80 -1 10 -4 -1.00 9.90 -2 -10 -4 19.60 8.20 -2 10 -4 23.90 11.80 3 -10 4 168.98 22.00 -3 -10 -4 131.29 14.80 -3 10 -4 160.38 19.50 4 -10 4 125.29 18.60 -4 -10 -4 127.19 16.00 -4 10 -4 146.39 19.70 5 -10 4 7.80 14.30 -5 10 -4 -1.50 19.70 6 -10 4 -7.10 15.60 -6 10 -4 4.20 12.10 7 -10 4 10.90 16.20 -7 10 -4 32.50 15.20 8 -10 4 36.50 34.00 9 -10 4 -2.90 16.50 10 -10 4 14.00 18.10 11 -10 4 40.20 19.10 12 -10 4 8.20 17.30 -12 -10 -4 -11.50 6.90 12 10 4 6.90 6.30 13 -10 4 -4.60 16.40 -13 -10 -4 3.70 9.30 13 10 4 7.80 5.90 14 -10 4 17.10 18.30 -14 -10 -4 -20.10 10.70 14 10 4 12.50 7.70 15 -10 4 34.90 28.10 15 10 4 20.00 9.00 17 11 -4 14.20 8.80 16 -11 -4 18.00 16.40 16 11 -4 10.80 9.50 15 11 -4 9.90 9.90 14 -11 -4 17.70 16.40 13 -11 -4 16.60 14.90 -13 -11 4 11.60 11.60 13 11 -4 6.50 9.00 -12 -11 4 0.60 11.70 12 -11 -4 16.60 15.40 12 11 -4 2.40 8.20 11 -11 -4 15.30 15.10 -11 -11 4 12.20 11.60 11 11 -4 8.70 12.20 11 11 -4 11.20 13.60 -10 -11 4 58.49 13.90 10 11 -4 47.30 15.20 10 11 -4 45.20 13.90 -9 -11 4 14.20 11.50 9 -11 -4 -1.00 12.30 9 11 -4 8.70 12.40 9 11 -4 14.90 11.60 -9 11 4 21.30 13.00 8 -11 -4 10.60 13.40 8 11 -4 2.10 11.80 -8 11 4 26.20 12.00 -7 -11 4 20.50 10.40 7 -11 -4 4.70 9.50 -7 11 4 18.30 11.30 7 11 -4 26.10 11.00 7 11 -4 29.00 12.80 -6 -11 4 -11.20 7.10 6 -11 -4 -2.60 9.00 6 11 -4 12.10 11.40 6 11 -4 3.90 10.00 -6 11 4 -4.70 9.00 5 -11 -4 45.30 10.00 5 11 -4 95.59 16.70 -4 11 4 78.99 11.70 4 11 -4 86.79 14.80 3 -11 -4 23.70 16.20 3 -11 -4 29.30 8.60 3 11 -4 40.40 13.70 -3 11 4 43.60 9.80 3 11 -4 23.40 12.30 2 -11 -4 33.10 8.70 2 -11 -4 39.70 8.70 2 11 -4 62.39 15.40 2 11 -4 57.59 14.30 1 -11 -4 71.89 12.40 1 11 -4 66.69 16.40 1 11 -4 44.60 14.40 -1 11 4 75.59 11.60 0 -11 -4 4.60 7.40 0 11 4 1.10 8.50 0 11 -4 7.50 11.80 0 11 4 8.10 7.90 0 11 -4 12.10 11.40 -1 -11 -4 100.09 15.60 1 11 4 87.29 11.10 -1 11 -4 94.29 17.40 -1 11 -4 89.19 17.20 -2 -11 -4 2.80 6.80 -2 11 -4 -3.10 11.70 3 -11 4 27.90 13.90 -3 11 -4 13.70 12.00 4 -11 4 0.60 13.50 5 -11 4 26.20 15.90 -5 11 -4 12.70 12.60 6 -11 4 1.10 15.60 -6 11 -4 0.50 11.80 7 -11 4 7.80 17.40 8 -11 4 -4.20 15.80 9 -11 4 21.40 16.90 10 -11 4 9.10 17.50 11 -11 4 14.10 17.40 12 -11 4 -4.60 16.40 13 -11 4 23.00 22.60 14 -11 4 5.00 17.30 15 11 4 69.69 15.80 17 12 -4 16.80 9.40 16 -12 -4 -1.60 15.90 16 12 -4 6.60 8.30 15 -12 -4 6.00 15.50 15 12 -4 11.80 8.80 14 -12 -4 22.60 17.20 14 12 -4 9.20 12.10 -13 -12 4 -9.00 10.40 13 -12 -4 3.30 13.80 13 12 -4 3.00 9.10 12 -12 -4 1.60 14.20 -12 -12 4 -0.50 9.70 12 12 -4 -13.80 11.70 11 -12 -4 -0.70 12.20 -11 -12 4 -4.00 11.40 11 12 -4 -6.80 10.80 11 12 -4 2.90 12.90 10 -12 -4 2.90 12.70 -10 -12 4 -6.60 9.50 10 12 -4 -5.10 12.50 10 12 -4 20.00 12.80 9 -12 -4 7.10 10.60 -9 -12 4 3.00 9.90 9 12 -4 7.40 13.20 9 12 -4 4.60 12.10 -8 -12 4 40.80 13.80 8 -12 -4 7.70 11.10 -8 12 4 39.20 12.90 8 12 -4 19.10 10.80 8 12 -4 45.70 14.30 7 -12 -4 -1.80 9.30 -7 -12 4 2.80 10.30 -7 12 4 9.70 11.40 7 12 -4 -10.00 11.80 7 12 -4 -0.60 9.80 -6 -12 4 1.70 9.70 6 -12 -4 -1.60 8.10 -6 12 4 19.60 10.60 6 12 -4 15.90 11.60 6 12 -4 6.60 12.30 5 -12 -4 1.20 8.30 5 12 -4 11.90 12.10 5 12 -4 -14.30 8.50 -5 12 4 3.50 8.40 4 -12 -4 -1.60 7.50 4 12 -4 26.20 12.90 4 12 -4 3.80 10.90 -4 12 4 8.30 7.70 3 -12 -4 9.10 7.80 3 12 -4 14.60 12.10 3 12 -4 15.50 12.40 -3 12 4 14.10 8.70 2 -12 -4 214.08 18.00 2 12 -4 223.68 22.40 2 12 -4 224.48 23.20 -2 12 4 239.88 18.90 -1 12 4 10.60 8.80 1 12 -4 -1.60 12.40 1 12 -4 2.60 12.70 0 12 -4 24.50 12.90 0 12 4 11.80 9.90 0 12 -4 -5.30 11.70 0 12 4 13.00 9.00 -1 12 -4 165.58 21.40 -1 12 -4 156.18 21.70 1 12 4 104.39 13.70 -2 12 -4 17.00 12.30 3 -12 4 147.79 21.60 -3 12 -4 222.88 37.20 4 -12 4 201.18 25.50 -4 12 -4 217.98 16.10 -4 12 -4 180.98 23.60 5 -12 4 58.29 18.80 -5 12 -4 62.49 16.20 -5 12 -4 61.49 9.90 6 -12 4 2.90 15.90 -6 12 -4 9.10 7.20 7 -12 4 8.30 15.30 8 -12 4 24.40 16.40 9 -12 4 32.40 20.50 10 -12 4 -14.70 14.90 11 -12 4 10.80 18.40 12 -12 4 11.90 18.80 13 -12 4 9.70 17.40 16 13 -4 18.60 9.40 15 -13 -4 20.10 16.80 15 13 -4 9.90 9.00 14 -13 -4 -0.40 30.40 14 13 -4 16.40 9.90 13 -13 -4 8.40 12.80 13 13 -4 0.40 8.50 12 -13 -4 18.60 12.60 -12 -13 4 11.20 10.40 12 13 -4 -0.80 12.40 -11 -13 4 12.70 10.90 11 -13 -4 1.10 11.70 11 13 -4 -0.70 12.40 -10 -13 4 7.90 12.50 10 -13 -4 7.00 12.80 10 13 -4 34.00 15.20 10 13 -4 12.20 12.60 -9 -13 4 54.89 13.60 9 -13 -4 22.70 11.10 9 13 -4 43.70 14.30 9 13 -4 41.20 14.60 8 -13 -4 34.40 13.20 -8 -13 4 60.39 14.40 8 13 -4 60.79 15.90 -8 13 4 95.09 19.20 8 13 -4 50.99 14.00 7 -13 -4 10.00 9.80 -7 -13 4 25.00 12.80 7 13 -4 23.40 13.70 -7 13 4 20.30 12.30 7 13 -4 46.30 20.40 -6 -13 4 90.69 16.00 -6 13 4 93.19 16.70 6 13 -4 57.59 13.90 6 13 -4 89.89 17.60 5 -13 -4 155.68 18.00 5 13 -4 195.78 19.90 5 13 -4 168.28 21.70 -5 13 4 184.58 18.30 4 13 -4 130.59 17.00 4 13 -4 165.08 22.60 -4 13 4 151.78 18.00 4 13 -4 145.99 19.70 3 13 -4 61.99 13.60 3 13 -4 72.89 18.90 3 13 -4 53.69 16.90 -3 13 4 44.10 10.80 2 -13 -4 -2.70 8.20 2 13 -4 -2.30 12.70 -2 13 4 -2.00 10.10 2 13 -4 -18.40 12.30 2 13 -4 -1.30 9.60 -1 13 4 14.70 10.20 1 13 -4 5.70 14.00 1 13 -4 35.10 14.40 0 13 -4 202.68 23.30 0 13 4 160.78 18.20 0 13 -4 165.38 23.70 0 13 4 133.09 17.50 1 13 4 126.89 14.30 -1 13 -4 71.59 12.80 1 13 4 78.79 13.30 -1 13 -4 84.89 20.70 -1 13 -4 120.69 20.50 -2 13 -4 40.20 15.30 -2 13 -4 12.70 15.80 -2 13 -4 9.70 9.20 -3 13 -4 36.80 13.90 -3 13 -4 48.60 11.40 4 -13 4 -11.00 12.90 -4 13 -4 0.00 7.90 -4 13 -4 8.40 13.60 5 -13 4 9.50 15.50 -5 13 -4 36.70 9.30 6 -13 4 60.59 18.50 7 -13 4 8.10 15.50 8 -13 4 5.60 14.90 9 -13 4 8.70 12.40 10 -13 4 18.20 15.90 11 -13 4 13.10 13.10 12 -13 4 38.20 21.80 13 -13 4 2.30 19.70 16 14 -4 16.20 8.80 15 -14 -4 33.40 19.10 15 14 -4 7.40 9.40 14 -14 -4 11.50 14.20 14 14 -4 10.50 9.70 13 -14 -4 2.90 11.60 13 14 -4 -2.40 8.50 -12 -14 4 3.60 10.40 12 -14 -4 -7.80 11.90 12 14 -4 -16.00 11.70 -11 -14 4 30.80 11.20 11 -14 -4 8.90 11.30 11 14 -4 36.40 15.10 10 -14 -4 35.00 16.20 -10 -14 4 29.10 13.00 10 14 -4 30.70 15.10 9 -14 -4 17.50 11.40 -9 -14 4 24.60 12.20 9 14 -4 30.20 14.90 9 14 -4 38.90 13.90 -8 -14 4 10.20 10.40 8 -14 -4 8.40 10.20 8 14 -4 3.10 11.40 8 14 -4 0.90 13.20 -7 -14 4 -7.10 8.80 7 -14 -4 2.20 8.50 7 14 -4 7.30 11.70 7 14 -4 4.20 13.00 -7 14 4 16.00 10.60 6 -14 -4 5.30 9.90 6 14 -4 6.60 14.10 -6 14 4 21.60 11.70 6 14 -4 -12.20 11.80 5 -14 -4 -6.10 7.80 -5 14 4 11.70 10.60 5 14 -4 6.70 10.10 5 14 -4 1.90 14.40 5 14 -4 -1.80 14.50 -4 14 4 54.69 12.90 4 14 -4 31.00 15.20 4 14 -4 50.49 13.50 4 14 -4 45.30 16.30 3 -14 -4 12.50 10.10 3 14 -4 2.50 9.30 3 14 -4 -5.10 13.40 -3 14 4 10.50 9.00 3 14 -4 -1.60 13.30 2 -14 -4 12.50 8.60 2 14 -4 9.10 15.40 2 14 -4 25.50 14.80 2 14 -4 17.10 10.00 -2 14 4 8.50 10.60 1 14 -4 171.48 24.80 1 14 -4 127.19 17.30 -1 14 4 151.18 23.30 -1 14 4 159.38 17.40 1 14 -4 147.89 22.50 0 14 -4 203.68 20.00 0 14 4 213.68 22.60 0 14 -4 263.57 44.00 0 14 -4 199.88 25.60 0 14 4 217.88 21.20 -1 14 -4 -5.30 14.80 1 14 4 19.90 9.80 -1 14 -4 13.10 14.60 1 14 4 7.80 10.10 -1 14 -4 7.00 9.40 -2 14 -4 87.89 18.80 -2 14 -4 80.69 13.60 -2 14 -4 88.09 20.60 -3 14 -4 88.49 13.60 -3 14 -4 115.19 20.40 4 -14 4 97.59 18.10 5 -14 4 190.38 25.60 6 -14 4 91.99 17.80 7 -14 4 4.30 13.30 8 -14 4 -1.20 12.60 9 -14 4 -1.10 9.00 10 -14 4 4.70 11.20 11 -14 4 2.70 8.90 12 -14 4 1.70 7.60 15 15 -4 17.40 9.30 14 -15 -4 13.30 12.90 14 15 -4 4.80 9.80 13 -15 -4 23.20 15.00 13 15 -4 0.00 12.70 12 -15 -4 0.60 11.40 12 15 -4 -0.40 13.30 -11 -15 4 16.70 11.60 11 -15 -4 -5.20 10.30 11 15 -4 1.90 13.00 -10 -15 4 22.00 10.90 10 -15 -4 6.00 8.60 10 15 -4 17.60 14.00 9 -15 -4 1.80 9.60 -9 -15 4 10.20 10.10 9 15 -4 7.20 14.10 8 -15 -4 2.80 9.80 8 15 -4 -5.70 11.60 8 15 -4 -6.10 13.10 7 -15 -4 4.20 9.70 7 15 -4 9.90 12.90 7 15 -4 -9.90 12.80 6 -15 -4 27.60 9.70 6 15 -4 54.09 15.10 -6 15 4 84.99 17.40 6 15 -4 54.29 16.50 6 15 -4 64.69 20.40 5 -15 -4 32.90 11.90 -5 15 4 69.79 16.10 5 15 -4 59.19 17.60 5 15 -4 53.39 14.60 5 15 -4 97.89 20.60 4 -15 -4 22.30 10.30 4 15 -4 47.70 16.10 -4 15 4 34.70 11.20 4 15 -4 65.39 17.80 4 15 -4 66.19 19.30 3 -15 -4 7.20 9.10 3 15 -4 50.79 14.50 3 15 -4 37.00 20.10 -3 15 4 41.40 10.90 3 15 -4 23.60 16.10 2 15 -4 177.78 20.10 -2 15 4 167.88 19.30 2 15 -4 255.37 43.30 2 15 -4 199.88 26.40 -1 15 4 208.08 22.80 1 15 -4 262.07 27.60 1 15 -4 168.08 19.70 1 15 -4 302.37 28.90 -1 15 4 194.08 20.80 0 15 4 186.58 20.60 0 15 -4 209.08 27.30 0 15 4 186.48 31.00 0 15 -4 288.37 31.30 0 15 -4 170.68 19.00 -1 15 -4 51.99 19.40 -1 15 -4 92.19 20.70 -1 15 -4 76.49 14.50 1 15 4 58.49 13.60 1 15 4 40.90 20.80 -2 15 -4 46.90 19.00 -2 15 -4 70.79 23.30 -2 15 -4 47.70 12.80 -3 15 -4 45.10 12.10 -3 15 -4 41.30 19.20 5 -15 4 5.20 13.30 6 -15 4 1.50 10.70 7 -15 4 0.20 11.10 8 -15 4 4.70 11.80 9 -15 4 4.70 8.90 10 -15 4 35.50 20.80 11 -15 4 2.20 9.40 12 -15 4 2.00 15.20 14 16 -4 8.60 9.10 13 -16 -4 7.20 11.00 13 16 -4 2.50 8.50 12 -16 -4 1.70 9.80 12 16 -4 -9.40 16.20 -11 -16 4 4.10 13.30 11 -16 -4 0.80 9.80 11 16 -4 -0.10 13.10 -10 -16 4 19.50 11.50 10 -16 -4 6.40 10.90 10 16 -4 -1.50 13.40 9 -16 -4 -4.80 8.60 9 16 -4 -11.60 12.50 8 -16 -4 2.00 9.90 8 16 -4 -9.60 12.70 7 -16 -4 6.90 10.90 7 16 -4 1.70 11.90 7 16 -4 -12.70 12.90 7 16 -4 10.10 15.90 6 -16 -4 3.50 11.30 6 16 -4 29.50 15.50 6 16 -4 27.90 15.50 6 16 -4 27.70 14.00 5 16 -4 78.79 19.10 5 16 -4 121.19 23.20 -5 16 4 104.19 16.50 5 16 -4 50.49 14.50 4 -16 -4 12.60 9.20 4 16 -4 33.90 15.60 4 16 -4 66.39 15.90 4 16 -4 38.50 21.90 3 16 -4 20.10 14.70 3 16 -4 8.20 15.40 3 16 -4 3.60 12.20 -3 16 4 1.00 8.20 2 16 -4 3.10 15.40 2 16 -4 58.19 17.70 2 16 -4 25.40 12.90 -2 16 4 41.40 15.70 -2 16 4 36.90 11.50 1 16 -4 96.89 17.30 1 16 -4 143.19 24.10 -1 16 4 153.28 21.50 -1 16 4 157.18 20.00 1 16 -4 125.29 22.60 0 16 4 81.59 15.10 0 16 -4 38.20 18.80 0 16 -4 90.19 20.80 0 16 4 86.59 17.00 0 16 -4 71.79 14.80 -1 16 -4 21.50 17.30 1 16 4 38.00 12.60 1 16 4 62.29 13.50 -1 16 -4 14.50 12.00 -2 16 -4 45.70 12.80 -3 16 -4 -10.30 14.70 -4 16 -4 65.09 20.00 6 -16 4 13.80 10.50 7 -16 4 11.60 10.30 8 -16 4 0.70 7.30 9 -16 4 19.30 12.60 10 -16 4 0.10 11.30 11 -16 4 2.10 10.30 13 -17 -4 15.60 11.90 13 17 -4 1.80 8.70 12 -17 -4 4.20 9.80 12 17 -4 -15.60 13.20 11 -17 -4 1.30 10.50 11 17 -4 -15.00 12.40 10 -17 -4 4.50 10.80 10 17 -4 -6.30 13.80 9 -17 -4 7.60 11.60 9 17 -4 -11.30 12.60 8 -17 -4 8.00 10.90 8 17 -4 75.79 17.70 8 17 -4 6.60 13.70 7 -17 -4 6.10 11.20 7 17 -4 38.60 16.50 7 17 -4 30.30 15.60 6 -17 -4 0.30 18.90 6 17 -4 -5.70 14.00 6 17 -4 51.79 19.10 5 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709.83 33.50 -4 10 5 710.63 29.00 3 -10 -5 356.56 19.90 3 10 -5 360.16 24.60 2 -10 -5 120.99 12.50 2 -10 -5 113.29 11.80 2 10 -5 129.99 17.60 2 10 -5 133.19 17.80 -2 10 5 108.59 11.20 1 -10 -5 -3.30 7.00 1 -10 -5 -3.30 6.90 -1 10 5 7.50 5.90 1 10 -5 10.20 11.40 1 10 -5 2.40 11.00 0 -10 -5 -0.70 6.80 0 10 -5 -7.40 9.80 0 10 -5 16.00 11.70 -1 -10 -5 135.69 16.00 -1 10 -5 148.99 19.30 -1 10 -5 161.18 19.40 -2 -10 -5 -1.50 7.00 -2 10 -5 2.30 10.80 3 -10 5 48.10 15.90 -3 -10 -5 33.40 11.00 -3 10 -5 62.99 15.20 4 -10 5 -0.10 12.80 -4 -10 -5 10.10 10.00 -4 10 -5 16.80 11.60 -5 -10 -5 65.29 12.10 5 -10 5 65.59 17.60 -5 10 -5 84.09 16.80 6 -10 5 26.40 17.40 -6 -10 -5 16.60 11.30 -6 10 -5 25.70 13.50 7 -10 5 8.50 18.20 8 -10 5 -0.70 17.80 9 -10 5 -0.50 16.90 10 -10 5 17.70 18.40 11 -10 5 -7.90 17.00 12 -10 5 8.60 17.20 14 -10 5 9.70 17.20 14 10 5 7.80 6.20 17 11 -5 17.90 9.20 16 -11 -5 -5.50 14.50 16 11 -5 17.20 10.30 15 -11 -5 8.10 16.70 15 11 -5 9.60 10.80 14 -11 -5 17.40 14.60 14 11 -5 1.40 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13 -5 17.90 15.00 6 13 -5 -4.20 9.50 -6 13 5 19.40 10.20 5 -13 -5 1.90 8.10 -5 13 5 21.70 10.60 5 13 -5 -16.50 12.40 -4 13 5 101.29 14.90 4 13 -5 102.29 18.30 4 13 -5 117.89 22.30 3 -13 -5 3.00 7.30 3 13 -5 18.70 15.40 -3 13 5 23.30 10.10 3 13 -5 18.80 14.20 2 -13 -5 0.60 9.90 -2 13 5 -8.50 7.00 2 13 -5 -3.00 14.00 2 13 -5 -1.50 13.10 1 13 -5 95.39 19.60 1 13 -5 36.40 15.50 -1 13 5 52.19 9.80 0 13 5 139.59 16.80 0 13 -5 224.38 28.40 0 13 5 137.29 12.10 0 13 -5 188.98 23.90 -1 13 -5 -11.30 13.40 -1 13 -5 10.40 13.10 -2 13 -5 39.00 15.20 -2 13 -5 25.70 16.20 -3 13 -5 6.80 12.70 4 -13 5 2.20 15.10 5 -13 5 27.60 18.90 6 -13 5 4.80 14.50 -6 13 -5 24.50 8.40 7 -13 5 11.00 15.30 8 -13 5 -8.00 14.90 9 -13 5 14.10 13.70 10 -13 5 -4.90 14.10 11 -13 5 -5.10 11.20 12 -13 5 -1.00 11.70 16 14 -5 16.90 9.10 15 -14 -5 8.70 15.60 15 14 -5 8.00 8.90 14 -14 -5 -5.70 11.50 14 14 -5 6.30 9.80 13 -14 -5 -1.70 11.70 13 14 -5 6.30 13.10 12 -14 -5 9.10 11.10 12 14 -5 -7.40 13.40 11 -14 -5 -6.90 10.10 -11 -14 5 4.90 10.00 11 14 -5 -11.90 13.20 11 14 -5 9.80 12.30 -10 -14 5 -3.50 10.00 10 -14 -5 -1.90 8.70 10 14 -5 7.20 12.60 10 14 -5 1.10 14.30 -9 -14 5 0.70 9.70 9 -14 -5 4.00 9.50 9 14 -5 13.30 14.50 9 14 -5 -6.00 11.20 8 -14 -5 2.50 8.30 8 14 -5 -4.40 10.60 8 14 -5 5.90 13.50 -7 -14 5 16.70 11.30 7 -14 -5 2.20 9.70 -7 14 5 27.40 12.30 7 14 -5 7.30 13.80 7 14 -5 12.20 11.50 6 -14 -5 32.00 9.50 6 14 -5 56.89 15.00 5 -14 -5 35.70 9.70 5 14 -5 123.99 23.10 5 14 -5 71.09 18.10 -5 14 5 80.29 14.40 5 14 -5 64.59 15.10 4 -14 -5 -0.90 8.00 4 14 -5 -4.70 10.20 -4 14 5 2.50 9.30 4 14 -5 -3.40 13.90 4 14 -5 -10.70 11.90 3 -14 -5 9.20 8.90 3 14 -5 13.40 14.70 3 14 -5 17.80 16.40 -3 14 5 18.80 10.00 2 -14 -5 8.80 8.00 -2 14 5 28.70 9.90 2 14 -5 31.90 21.60 2 14 -5 27.40 16.90 -1 14 5 46.70 10.30 1 14 -5 32.00 16.00 -1 14 5 40.20 13.50 1 14 -5 47.40 16.90 0 14 -5 22.30 16.50 0 14 5 16.90 7.50 0 14 -5 18.80 15.10 0 14 5 3.10 10.80 -1 14 -5 22.40 15.80 -1 14 -5 -2.00 16.50 -2 14 -5 34.40 18.60 -2 14 -5 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2.80 13.50 4 15 -5 13.60 18.90 3 -15 -5 5.20 8.30 -3 15 5 25.60 10.30 3 15 -5 10.40 15.20 3 15 -5 22.10 16.80 3 15 -5 10.00 11.80 -2 15 5 27.80 9.90 2 15 -5 25.30 12.60 2 15 -5 44.40 18.50 2 15 -5 20.20 14.90 -1 15 5 11.20 15.60 1 15 -5 15.40 11.30 1 15 -5 6.00 14.90 -1 15 5 5.20 8.20 1 15 -5 10.60 16.00 0 15 -5 6.00 13.90 0 15 -5 4.80 11.10 0 15 5 -12.20 10.60 0 15 -5 -2.10 15.40 -1 15 -5 -10.70 10.00 -1 15 -5 24.80 17.80 -1 15 -5 42.10 20.80 -2 15 -5 -2.30 8.30 -2 15 -5 -2.30 14.90 -3 15 -5 -4.40 15.30 -3 15 -5 4.20 9.20 -4 15 -5 -4.40 8.80 6 -15 5 4.90 12.20 7 -15 5 -4.20 10.10 8 -15 5 7.30 11.20 9 -15 5 15.80 13.40 10 -15 5 -4.30 10.00 11 -15 5 1.70 7.80 14 -16 -5 4.50 9.90 14 16 -5 7.20 10.00 13 -16 -5 9.60 9.40 13 16 -5 -12.40 13.70 12 -16 -5 -5.20 8.50 12 16 -5 -11.80 13.80 11 -16 -5 -0.30 8.60 11 16 -5 -42.00 26.50 10 -16 -5 7.30 11.40 10 16 -5 -13.30 14.10 9 -16 -5 0.50 9.70 9 16 -5 12.90 14.20 9 16 -5 9.20 11.70 8 -16 -5 1.00 10.00 8 16 -5 -12.90 11.00 8 16 -5 0.40 13.30 7 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13.10 12 -17 -5 6.40 11.50 12 17 -5 -0.50 14.60 11 -17 -5 16.10 11.40 11 17 -5 -14.20 14.30 10 -17 -5 0.70 9.60 9 -17 -5 8.50 10.90 9 17 -5 1.10 14.30 8 -17 -5 3.90 10.90 8 17 -5 -0.20 13.30 8 17 -5 1.80 12.90 7 -17 -5 6.30 11.00 7 17 -5 16.30 13.70 7 17 -5 -5.60 13.40 6 -17 -5 19.40 12.70 6 17 -5 23.30 13.50 6 17 -5 16.30 15.60 6 17 -5 89.19 25.50 5 -17 -5 1.50 11.20 5 17 -5 8.30 15.90 5 17 -5 20.00 19.10 5 17 -5 1.50 11.50 -5 17 5 32.80 10.90 4 -17 -5 -4.30 9.80 4 17 -5 -6.10 26.40 -4 17 5 9.50 9.30 4 17 -5 -16.90 10.40 4 17 -5 7.00 14.70 3 17 -5 17.80 17.40 -3 17 5 18.10 9.30 3 17 -5 28.20 12.80 2 17 -5 -22.50 8.70 2 17 -5 15.20 15.40 -2 17 5 11.50 8.50 -2 17 5 -3.80 12.90 -1 17 5 4.90 12.00 1 17 -5 13.10 29.10 1 17 -5 -2.90 13.20 -1 17 5 8.80 7.90 0 17 5 11.00 12.70 0 17 -5 28.70 12.30 0 17 5 52.89 10.60 0 17 -5 34.50 17.60 -1 17 -5 20.80 19.10 -1 17 -5 12.80 12.00 -2 17 -5 -3.60 10.50 -2 17 -5 -4.90 16.00 -3 17 -5 -1.30 16.10 -4 17 -5 5.30 16.40 -5 17 -5 -5.60 15.60 8 -17 5 -4.80 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11 -9 7 -6.40 15.20 12 -9 7 6.10 19.50 13 -9 7 9.30 18.20 14 -9 7 26.80 17.00 18 10 -7 11.00 9.10 17 -10 -7 15.60 15.70 17 10 -7 12.20 9.40 16 -10 -7 11.40 15.30 16 10 -7 -2.20 9.50 15 -10 -7 2.40 13.10 15 10 -7 -3.00 9.00 15 10 -7 10.10 13.50 14 -10 -7 -4.40 11.90 14 10 -7 -2.00 11.50 14 10 -7 9.20 10.90 13 -10 -7 6.60 13.90 13 10 -7 17.90 13.40 13 10 -7 -3.00 16.00 12 -10 -7 22.00 14.70 -12 -10 7 -1.70 12.80 12 10 -7 8.10 11.80 12 10 -7 11.60 13.80 11 -10 -7 97.49 28.70 -11 -10 7 116.19 20.80 11 10 -7 89.29 18.40 -10 -10 7 20.70 12.50 10 -10 -7 0.00 10.70 10 10 -7 15.00 14.70 -10 10 7 21.40 13.60 9 -10 -7 9.90 11.20 -9 -10 7 23.90 13.50 -9 10 7 4.60 10.90 9 10 -7 31.90 14.10 8 -10 -7 -0.90 8.50 -8 -10 7 9.40 11.70 -8 10 7 -1.20 10.60 8 10 -7 5.80 12.80 7 -10 -7 17.20 9.30 -7 -10 7 40.40 13.20 7 10 -7 43.10 14.40 -7 10 7 25.90 10.30 6 -10 -7 243.38 18.70 -6 -10 7 228.08 21.30 -6 10 7 240.68 18.00 6 10 -7 242.28 23.30 5 -10 -7 405.46 23.00 -5 -10 7 491.35 28.30 5 10 -7 454.35 28.60 -5 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16.00 12 -9 8 7.80 18.60 13 -9 8 6.80 16.30 17 -10 -8 54.29 19.50 16 -10 -8 9.80 15.40 16 10 -8 18.20 11.30 16 10 -8 -17.00 10.30 15 -10 -8 9.70 14.00 15 10 -8 3.20 9.40 15 10 -8 4.80 12.40 14 -10 -8 -3.10 12.20 14 10 -8 2.40 13.90 14 10 -8 -0.60 10.70 13 -10 -8 -10.80 11.10 13 10 -8 8.00 14.80 13 10 -8 -20.20 10.60 12 -10 -8 9.20 13.00 12 10 -8 -5.40 12.70 -11 -10 8 13.00 11.60 11 10 -8 11.70 13.80 10 -10 -8 4.60 9.70 -10 -10 8 -3.80 10.90 10 10 -8 2.80 14.90 -10 10 8 0.90 11.20 -9 -10 8 1.00 11.20 9 -10 -8 -8.70 8.80 -9 10 8 -3.20 11.30 9 10 -8 7.60 14.10 -8 -10 8 106.39 18.90 8 10 -8 56.49 16.90 -8 10 8 81.59 15.90 -7 -10 8 88.39 16.80 7 10 -8 86.89 18.20 -7 10 8 104.69 14.90 -6 -10 8 -10.00 9.90 6 -10 -8 -5.40 6.30 6 10 -8 9.00 14.00 -6 10 8 4.90 9.80 -5 -10 8 1.80 11.20 5 -10 -8 -4.50 5.70 -5 10 8 -6.10 8.10 5 10 -8 2.20 13.40 -4 -10 8 9.00 11.10 4 -10 -8 0.30 5.60 4 10 -8 15.00 13.10 -4 10 8 4.90 7.70 -3 10 8 39.70 8.60 3 10 -8 38.90 15.20 2 -10 -8 63.49 8.10 2 10 -8 63.29 16.30 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126.89 18.20 -3 7 10 127.99 12.50 2 -7 -10 18.60 4.60 2 7 -10 24.60 13.10 1 7 -10 -1.40 9.50 1 7 -10 13.70 12.00 0 7 -10 151.98 20.80 0 7 -10 119.89 19.00 -1 7 -10 40.80 14.50 -1 7 -10 39.00 15.50 -2 7 -10 8.20 12.90 -2 7 -10 9.80 11.50 -3 7 -10 -0.10 12.90 -3 7 -10 19.40 20.70 -4 7 -10 43.00 16.00 -5 7 -10 8.60 12.90 6 -7 10 -7.80 15.70 7 -7 10 -16.10 15.60 8 -7 10 12.70 16.90 9 -7 10 8.00 15.90 10 -7 10 19.00 16.30 11 -7 10 3.60 12.20 12 -7 10 5.70 12.70 13 -7 10 2.30 11.40 14 -7 10 10.30 13.50 19 8 -10 11.10 10.00 18 -8 -10 26.20 17.30 18 8 -10 8.90 10.10 18 8 -10 17.40 14.20 17 -8 -10 4.90 14.70 17 8 -10 9.30 11.60 17 8 -10 2.70 10.70 16 -8 -10 20.40 16.60 16 8 -10 2.80 10.90 16 8 -10 6.20 12.50 15 -8 -10 17.30 14.60 15 8 -10 -0.70 11.50 14 -8 -10 5.20 11.90 14 8 -10 2.10 15.20 13 -8 -10 -7.20 12.10 13 8 -10 3.10 13.60 12 -8 -10 17.30 12.70 11 -8 -10 55.69 14.90 -11 -8 10 71.69 17.70 -11 8 10 64.59 17.50 11 8 -10 90.19 19.90 -10 -8 10 12.90 12.80 10 -8 -10 9.50 11.50 10 8 -10 41.80 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9 -10 9.10 10.50 18 9 -10 10.90 12.70 17 -9 -10 1.00 13.70 17 9 -10 -17.40 10.30 17 9 -10 8.30 9.40 16 -9 -10 17.40 15.20 16 9 -10 11.00 12.70 16 9 -10 3.10 11.70 15 -9 -10 -1.50 13.00 15 9 -10 15.60 14.60 14 -9 -10 20.40 14.30 14 9 -10 8.40 16.10 13 -9 -10 3.90 12.90 13 9 -10 -1.70 14.20 12 -9 -10 2.20 11.20 12 9 -10 12.60 15.20 11 -9 -10 3.50 10.90 11 9 -10 35.80 17.30 -10 -9 10 21.50 13.10 10 -9 -10 9.50 11.50 10 9 -10 12.40 14.90 -10 9 10 10.50 12.40 -9 -9 10 2.80 12.30 9 -9 -10 2.70 9.70 9 9 -10 4.50 13.80 -8 -9 10 1.10 11.90 8 -9 -10 1.20 9.00 8 9 -10 11.30 14.50 -8 9 10 -1.90 10.40 7 -9 -10 -2.10 6.90 -7 9 10 -8.00 9.30 7 9 -10 18.20 15.60 -6 -9 10 8.20 12.00 6 -9 -10 -3.70 6.00 6 9 -10 -5.60 13.80 -6 9 10 -0.50 9.80 5 -9 -10 135.99 22.20 -5 -9 10 110.39 19.50 5 9 -10 104.09 19.70 -5 9 10 123.19 14.40 -4 -9 10 111.19 19.00 -4 9 10 105.79 13.10 4 9 -10 83.79 17.90 3 9 -10 53.49 15.80 -3 9 10 57.39 9.80 2 9 -10 88.89 18.20 2 9 -10 88.09 16.40 1 9 -10 179.18 22.70 1 9 -10 165.38 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16.00 -6 -10 10 223.38 24.20 6 10 -10 201.48 23.80 -6 10 10 183.78 18.20 -5 -10 10 43.00 17.30 5 -10 -10 16.10 7.00 -5 10 10 29.20 10.80 5 10 -10 45.50 17.30 -4 -10 10 81.09 25.40 4 10 -10 105.69 20.30 3 -10 -10 -0.30 4.80 3 10 -10 14.50 15.30 3 10 -10 14.80 14.70 -3 10 10 -9.30 7.30 2 10 -10 38.20 16.90 2 10 -10 36.20 14.00 1 10 -10 28.70 15.20 1 10 -10 60.09 17.10 0 10 -10 -19.10 13.60 0 10 -10 -15.10 12.20 -1 10 -10 3.90 12.70 -1 10 -10 1.10 12.70 -2 10 -10 21.80 14.10 -2 10 -10 3.60 12.50 -3 10 -10 34.10 17.30 -4 10 -10 30.60 20.80 7 -10 10 6.30 16.50 8 -10 10 4.80 17.00 9 -10 10 -11.40 16.40 10 -10 10 5.10 16.00 11 -10 10 3.60 15.60 12 -10 10 22.50 18.00 18 11 -10 6.30 14.80 18 11 -10 20.50 11.50 17 -11 -10 11.30 13.30 17 11 -10 8.70 12.10 17 11 -10 9.50 12.50 16 -11 -10 15.60 12.20 16 11 -10 -3.00 9.40 16 11 -10 9.80 12.30 15 -11 -10 4.40 11.00 15 11 -10 5.80 16.60 15 11 -10 -11.60 10.00 14 -11 -10 3.30 11.60 14 11 -10 -8.80 15.00 13 -11 -10 1.00 9.50 13 11 -10 1.80 15.30 12 -11 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7.00 -6 5 12 -4.70 8.50 6 5 -12 10.20 12.60 5 -5 -12 212.38 16.80 -5 -5 12 174.78 20.00 5 5 -12 183.18 20.60 -5 5 12 199.08 17.60 4 -5 -12 33.30 6.80 -4 -5 12 43.30 13.30 -4 5 12 94.99 21.00 4 5 -12 69.19 15.70 -3 -5 12 -6.70 11.10 3 -5 -12 8.20 5.60 3 5 -12 18.70 12.70 -3 5 12 7.00 9.00 -2 -5 12 148.49 19.60 2 -5 -12 133.89 10.10 -2 5 12 132.29 14.10 2 5 -12 129.79 19.20 1 -5 -12 11.00 4.50 1 5 -12 12.00 12.90 1 5 -12 10.40 12.40 -1 5 12 21.90 8.80 0 5 -12 56.29 14.10 0 5 -12 68.39 15.20 -1 5 -12 3.50 12.70 -1 5 -12 15.00 14.60 -2 5 -12 6.30 13.90 -2 5 -12 13.10 14.20 -3 5 -12 19.30 17.40 -3 5 -12 10.70 14.50 -4 5 -12 -2.90 13.60 -4 5 -12 41.30 16.80 -5 5 -12 87.69 20.30 -5 5 -12 96.99 21.00 -6 5 -12 118.89 30.90 -7 -5 -12 24.50 7.90 8 -5 12 9.10 12.40 9 -5 12 6.70 13.60 -9 -5 -12 6.40 8.00 -9 -5 -12 1.90 8.60 10 -5 12 -0.70 10.10 -10 -5 -12 -9.80 8.00 -11 -5 -12 -13.40 9.20 11 -5 12 0.40 11.60 12 -5 12 5.70 11.70 13 -5 12 13.70 11.60 19 6 -12 9.10 10.10 19 6 -12 16.80 12.00 18 -6 -12 35.10 16.10 18 6 -12 22.50 14.20 17 -6 -12 46.50 26.50 17 6 -12 1.30 14.10 16 -6 -12 37.10 15.60 16 6 -12 10.60 14.40 15 -6 -12 19.80 13.80 15 6 -12 8.60 16.10 14 -6 -12 22.10 14.90 14 6 -12 12.60 14.40 13 -6 -12 3.00 13.10 13 6 -12 13.10 15.10 12 6 -12 14.10 14.20 11 -6 -12 -2.30 10.10 11 6 -12 2.90 14.30 -11 6 12 -19.50 10.90 -10 -6 12 5.80 11.70 10 -6 -12 -0.80 9.50 10 6 -12 -1.10 13.70 -10 6 12 -2.40 10.70 9 -6 -12 118.39 15.70 -9 -6 12 135.69 22.30 -9 6 12 161.98 19.30 9 6 -12 135.39 20.10 8 -6 -12 8.50 8.30 -8 -6 12 19.90 11.80 8 6 -12 13.50 12.60 -8 6 12 11.90 11.40 7 -6 -12 5.00 8.10 -7 -6 12 -6.10 11.90 -7 6 12 -9.10 9.30 7 6 -12 -2.70 11.00 6 -6 -12 -0.80 6.30 -6 -6 12 2.60 10.80 6 6 -12 -0.50 12.80 -6 6 12 -1.30 9.10 -5 -6 12 -7.50 10.00 5 -6 -12 9.80 11.20 5 6 -12 -10.70 12.10 -5 6 12 5.60 9.00 -4 -6 12 0.40 11.40 4 -6 -12 2.20 5.60 -4 6 12 15.80 14.60 4 6 -12 7.50 11.20 3 -6 -12 120.19 10.50 -3 -6 12 184.58 21.70 3 6 -12 138.69 19.60 -3 6 12 123.39 13.90 2 -6 -12 5.40 4.20 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7 12 36.00 12.80 -7 -7 12 58.99 15.50 7 -7 -12 33.80 8.30 7 7 -12 102.49 19.70 -7 7 12 73.19 14.50 -6 -7 12 152.28 31.70 -6 7 12 125.99 16.00 6 7 -12 80.19 17.30 5 -7 -12 66.39 15.70 -5 -7 12 42.20 13.40 -5 7 12 50.09 11.80 5 7 -12 53.59 16.70 4 -7 -12 226.08 14.00 -4 -7 12 213.18 22.20 -4 7 12 214.58 19.50 4 7 -12 245.08 23.80 -3 -7 12 13.10 12.80 3 -7 -12 0.10 4.20 -3 7 12 6.20 8.80 3 7 -12 -0.90 12.70 2 -7 -12 2.40 3.80 -2 7 12 1.90 8.10 2 7 -12 7.90 12.50 1 7 -12 30.70 14.90 1 7 -12 7.40 10.70 0 7 -12 9.40 14.20 0 7 -12 16.30 23.50 -1 7 -12 157.68 23.70 -1 7 -12 183.78 25.10 -2 7 -12 65.79 19.30 -2 7 -12 45.30 16.40 -3 7 -12 17.10 15.40 -3 7 -12 29.30 13.90 -4 7 -12 40.40 19.00 -4 7 -12 48.30 21.40 -6 7 -12 4.20 15.60 9 -7 12 6.80 15.80 10 -7 12 -12.70 9.70 11 -7 12 2.30 9.30 12 -7 12 -4.40 10.80 19 8 -12 -2.50 12.60 18 -8 -12 19.30 15.60 18 8 -12 7.70 11.60 18 8 -12 15.60 12.70 17 -8 -12 14.10 14.20 17 8 -12 1.30 12.30 16 -8 -12 11.90 11.70 16 8 -12 3.40 13.30 15 -8 -12 12.10 12.10 15 8 -12 16.10 16.10 14 -8 -12 11.00 13.00 14 8 -12 13.90 15.40 13 -8 -12 -1.10 12.20 13 8 -12 10.50 15.20 12 -8 -12 2.90 11.30 12 8 -12 7.60 16.00 11 -8 -12 17.40 9.20 11 8 -12 83.39 20.60 10 8 -12 84.09 20.10 -10 8 12 88.59 17.80 -9 -8 12 58.59 19.00 9 8 -12 48.50 16.80 -9 8 12 58.79 17.90 -8 -8 12 -3.80 12.70 8 -8 -12 -5.20 6.30 -8 8 12 -3.70 11.00 8 8 -12 -8.90 14.30 -7 -8 12 6.60 12.80 7 -8 -12 0.90 6.20 7 8 -12 -15.80 13.60 -7 8 12 -2.00 10.60 -6 -8 12 19.00 12.60 6 -8 -12 1.20 6.10 6 8 -12 10.90 13.00 -6 8 12 3.60 10.20 -5 -8 12 2.20 12.10 5 -8 -12 -1.90 11.50 -5 8 12 -2.10 9.00 5 8 -12 -2.10 12.80 4 -8 -12 1.40 4.60 -4 -8 12 -5.10 13.80 4 8 -12 4.00 13.20 -4 8 12 -3.60 8.70 3 -8 -12 0.00 4.30 -3 8 12 7.10 9.50 3 8 -12 -0.50 14.00 2 8 -12 57.39 16.30 2 8 -12 50.89 15.30 1 8 -12 9.90 13.40 1 8 -12 24.30 16.00 0 8 -12 -1.00 13.30 0 8 -12 14.70 14.70 -1 8 -12 19.90 15.60 -1 8 -12 38.00 17.60 -2 8 -12 106.69 20.80 -2 8 -12 57.49 17.90 -3 8 -12 126.09 22.70 -5 8 -12 5.90 16.10 -6 8 -12 19.50 16.20 10 -8 12 -0.10 13.80 11 -8 12 43.40 18.20 12 -8 12 1.00 10.20 18 9 -12 11.90 10.70 18 9 -12 12.00 13.40 17 -9 -12 2.10 13.90 16 -9 -12 12.20 13.60 16 9 -12 -6.90 10.50 15 -9 -12 7.30 11.60 15 9 -12 20.00 16.70 14 -9 -12 23.00 12.00 14 9 -12 11.10 16.90 13 -9 -12 -7.90 9.40 13 9 -12 -5.40 15.00 12 -9 -12 -2.20 9.10 12 9 -12 11.50 18.00 11 -9 -12 2.90 9.40 11 9 -12 16.90 17.00 10 -9 -12 6.00 8.70 10 9 -12 11.50 33.30 -10 9 12 25.00 14.20 9 -9 -12 5.70 8.00 9 9 -12 29.50 16.40 -9 9 12 3.60 16.00 8 -9 -12 2.80 7.90 -8 -9 12 17.40 13.70 8 9 -12 28.70 16.80 -8 9 12 22.40 13.00 7 -9 -12 13.50 7.40 -7 -9 12 41.50 16.10 7 9 -12 24.40 16.60 -7 9 12 31.80 13.50 -6 -9 12 178.18 24.30 6 -9 -12 123.79 13.70 6 9 -12 149.39 22.70 -6 9 12 146.99 17.90 5 -9 -12 41.50 13.50 -5 -9 12 42.40 15.70 -5 9 12 38.10 11.70 5 9 -12 27.00 15.60 -4 -9 12 -10.10 12.10 4 -9 -12 0.70 6.00 -4 9 12 -8.00 9.60 4 9 -12 9.20 14.60 3 9 -12 32.70 16.30 -3 9 12 39.40 10.30 2 9 -12 346.97 28.00 2 9 -12 356.06 29.70 1 9 -12 66.09 18.80 1 9 -12 120.99 21.20 0 9 -12 35.60 16.50 0 9 -12 43.80 17.20 -1 9 -12 51.09 17.00 -1 9 -12 31.80 17.50 -2 9 -12 -0.60 16.70 -3 9 -12 -1.80 23.10 -4 9 -12 20.90 18.60 -5 9 -12 -11.80 14.40 -6 9 -12 24.90 17.70 11 -9 12 6.90 13.60 18 10 -12 3.20 13.40 18 10 -12 11.10 11.80 17 -10 -12 0.40 11.10 17 10 -12 -13.80 16.00 17 10 -12 0.10 10.70 16 -10 -12 9.70 16.10 16 10 -12 6.70 16.10 15 -10 -12 12.40 13.20 15 10 -12 -22.90 15.20 14 -10 -12 11.60 10.40 14 10 -12 4.10 15.50 13 -10 -12 11.50 12.10 13 10 -12 -7.60 14.90 12 -10 -12 6.90 10.40 12 10 -12 0.10 16.20 11 -10 -12 14.20 19.30 11 10 -12 -3.40 15.70 10 -10 -12 13.80 9.30 10 10 -12 24.40 17.00 -10 10 12 13.30 13.80 9 -10 -12 1.90 8.80 -9 10 12 -11.50 12.20 8 -10 -12 1.10 7.80 -8 10 12 -1.20 12.90 8 10 -12 10.00 16.80 -7 -10 12 56.89 19.10 -7 10 12 57.89 14.70 7 10 -12 66.19 19.40 6 -10 -12 8.80 7.50 -6 -10 12 25.50 15.60 -6 10 12 27.80 11.90 6 10 -12 21.50 15.10 -5 -10 12 17.90 15.90 5 -10 -12 8.90 6.70 5 10 -12 18.60 17.10 -5 10 12 11.20 10.80 4 -10 -12 1.70 5.80 4 10 -12 -1.40 15.00 -4 10 12 -1.40 10.30 3 10 -12 -8.00 12.40 3 10 -12 4.30 15.80 -3 10 12 -2.10 8.90 2 10 -12 130.19 23.10 2 10 -12 118.49 20.90 1 10 -12 131.59 23.70 1 10 -12 207.48 27.30 0 10 -12 1.10 14.80 -1 10 -12 17.10 19.20 -2 10 -12 -8.90 13.90 -3 10 -12 13.20 17.80 -4 10 -12 8.00 15.80 -5 10 -12 1.00 18.00 -6 10 -12 2.80 16.10 -7 10 -12 5.90 18.60 17 -11 -12 17.40 15.60 17 11 -12 12.10 11.40 17 11 -12 13.20 13.50 16 -11 -12 -1.20 10.20 16 11 -12 -2.80 15.70 15 -11 -12 1.90 7.70 15 11 -12 -22.60 15.30 14 -11 -12 -0.20 8.60 14 11 -12 -1.00 15.30 13 -11 -12 4.40 9.00 13 11 -12 -2.00 15.40 12 -11 -12 1.40 10.00 12 11 -12 -6.30 15.70 11 -11 -12 -3.60 8.70 11 11 -12 3.60 15.80 10 -11 -12 -1.20 7.60 10 11 -12 14.60 16.00 -9 11 12 55.29 15.50 9 11 -12 36.70 17.40 8 -11 -12 6.00 8.20 -8 11 12 1.90 12.80 8 11 -12 13.60 18.90 7 -11 -12 4.80 8.20 -7 11 12 -12.90 12.00 7 11 -12 1.10 18.00 6 -11 -12 10.90 8.50 6 11 -12 -7.40 16.00 -6 11 12 3.40 11.50 -5 11 12 46.80 12.70 5 11 -12 51.39 19.10 4 -11 -12 -0.50 5.10 4 11 -12 -2.60 15.80 3 11 -12 29.60 17.70 2 11 -12 1.40 15.40 1 11 -12 60.69 24.20 0 11 -12 96.39 24.30 -1 11 -12 55.59 18.70 -2 11 -12 -8.90 14.30 -3 11 -12 1.20 14.60 -4 11 -12 17.20 15.10 -5 11 -12 5.00 16.90 -6 11 -12 5.40 17.40 -7 11 -12 13.40 16.70 -8 11 -12 15.00 17.30 17 12 -12 7.50 13.20 17 12 -12 -14.30 10.20 16 -12 -12 10.90 10.70 16 12 -12 -5.30 19.00 16 12 -12 0.20 12.60 15 -12 -12 12.10 13.90 15 12 -12 -15.90 15.70 14 -12 -12 7.00 9.50 14 12 -12 3.00 17.40 13 -12 -12 9.30 9.00 13 12 -12 -3.90 15.10 12 -12 -12 -1.70 8.40 12 12 -12 14.70 18.10 11 -12 -12 -0.70 7.90 11 12 -12 3.30 17.10 10 -12 -12 -1.20 8.40 10 12 -12 6.70 17.30 9 -12 -12 8.90 8.20 -9 12 12 34.10 15.30 9 12 -12 45.50 19.40 8 -12 -12 8.90 8.10 8 12 -12 -5.20 16.00 7 12 -12 59.99 19.60 -7 12 12 71.19 15.70 6 -12 -12 1.20 6.20 -6 12 12 1.10 11.40 6 12 -12 3.80 16.30 5 -12 -12 11.90 6.10 -5 12 12 17.40 11.20 5 12 -12 5.70 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0.0003 0 18 6 1.0593 0.0018 0 18 7 -2.1445 -0.0001 0 18 8 0.5593 0.0009 0 18 9 -1.1035 0.0017 0 18 10 -1.9053 -0.0010 0 18 11 -0.9353 -0.0002 0 19 1 -1.7051 0.0008 0 19 2 -1.8861 0.0013 0 19 3 0.9737 0.0003 0 19 4 -1.5764 -0.0006 0 19 5 0.4254 0.0009 0 19 6 -0.9207 -0.0010 0 19 7 -0.7282 -0.0012 0 19 8 -1.7506 0.0008 0 19 9 -0.2754 0.0020 0 20 0 -0.3327 0.0001 0 20 3 -1.1926 -0.0008 0 20 4 -0.5044 -0.0016 0 20 5 0.5404 0.0022 0 20 6 0.8527 0.0011 0 20 7 -2.0065 0.0004 0 21 1 -1.3933 0.0005 1 0 2 -2.4172 0.0388 1 0 4 -27.9150 -0.0212 1 0 6 -0.1602 -0.0033 1 0 8 -1.5252 -0.0036 1 0 10 -1.5961 0.0085 1 0 12 -2.2612 0.0034 1 0 14 -0.5156 -0.0042 1 0 16 0.6846 -0.0021 1 0 18 -1.0216 -0.0017 1 0 20 0.1345 0.0033 1 0 22 0.1956 0.0012 1 1 0 20.2480 -0.0219 1 1 1 36.0865 -0.0198 1 1 2 28.4296 0.0153 1 1 3 -22.2282 -0.0036 1 1 4 -0.3914 0.0058 1 1 5 -4.4452 0.0180 1 1 6 -2.4823 -0.0024 1 1 7 -0.0939 0.0075 1 1 8 1.5255 0.0007 1 1 9 -1.4206 -0.0096 1 1 10 0.2261 -0.0031 1 1 11 -2.3627 -0.0033 1 1 12 -0.2935 0.0014 1 1 13 -0.5382 -0.0013 1 1 14 -1.3329 -0.0006 1 1 15 0.5011 0.0056 1 1 16 0.3696 -0.0001 1 1 17 0.3968 0.0016 1 1 18 -1.8040 0.0007 1 1 19 0.2450 -0.0014 1 1 20 -1.4555 -0.0012 1 1 22 1.5524 -0.0016 1 2 0 28.7195 0.0227 1 2 1 42.7849 0.0214 1 2 2 10.4783 0.0167 1 2 3 15.9517 -0.0141 1 2 4 -3.7648 -0.0102 1 2 5 -4.0706 -0.0085 1 2 6 1.0341 -0.0067 1 2 7 2.9443 0.0085 1 2 8 0.7697 -0.0008 1 2 9 2.1465 0.0020 1 2 10 -0.3592 0.0077 1 2 11 0.3043 0.0007 1 2 12 -0.5924 0.0017 1 2 13 -2.0995 -0.0022 1 2 14 -0.5471 -0.0021 1 2 15 -0.9788 -0.0025 1 2 16 2.6302 -0.0035 1 2 17 -0.4173 0.0009 1 2 18 1.4957 -0.0001 1 2 19 -1.7877 0.0018 1 3 0 11.0909 -0.0298 1 3 1 6.1565 -0.0172 1 3 2 20.9535 0.0157 1 3 3 8.0299 0.0056 1 3 4 6.2152 0.0112 1 3 5 4.1487 0.0016 1 3 6 1.4910 -0.0018 1 3 7 0.0535 0.0036 1 3 8 3.0537 -0.0101 1 3 9 1.4205 -0.0048 1 3 10 1.4563 -0.0005 1 3 11 0.1596 -0.0026 1 3 12 -0.2679 0.0028 1 3 13 1.3024 0.0009 1 3 14 -1.4163 0.0037 1 3 15 0.0347 0.0029 1 3 16 -0.9438 0.0004 1 3 17 2.5955 0.0007 1 3 18 0.8363 -0.0025 1 3 19 0.6237 -0.0015 1 4 0 -5.0692 0.0032 1 4 1 7.1563 0.0089 1 4 2 4.1912 -0.0045 1 4 3 4.4600 -0.0215 1 4 4 2.1122 -0.0051 1 4 5 4.1049 -0.0050 1 4 6 0.5687 0.0024 1 4 7 2.3441 0.0068 1 4 8 0.6159 -0.0003 1 4 9 1.8996 0.0062 1 4 10 1.6405 0.0014 1 4 11 -0.4699 -0.0009 1 4 12 0.5621 -0.0001 1 4 13 -0.1395 -0.0051 1 4 14 0.1246 -0.0029 1 4 15 -0.2918 -0.0012 1 4 16 1.7188 0.0002 1 4 17 -0.5382 0.0023 1 4 18 0.9343 0.0003 1 4 19 0.8580 0.0037 1 4 20 0.1703 0.0013 1 4 22 0.4267 -0.0005 1 5 0 -1.2255 -0.0190 1 5 1 -0.1882 0.0092 1 5 2 1.4157 0.0086 1 5 3 -1.4573 0.0058 1 5 4 3.8775 0.0078 1 5 5 -1.9243 -0.0067 1 5 6 0.1666 -0.0007 1 5 7 -2.3112 -0.0014 1 5 8 -1.4764 -0.0077 1 5 9 1.1830 -0.0018 1 5 10 -0.7717 -0.0014 1 5 11 1.0797 0.0028 1 5 12 -0.0467 0.0035 1 5 13 0.5047 0.0005 1 5 14 0.1137 0.0035 1 5 15 0.0451 -0.0005 1 5 16 -0.3475 -0.0008 1 5 17 -1.2471 -0.0017 1 5 18 0.8144 -0.0029 1 5 19 0.2187 0.0003 1 5 20 -0.9704 -0.0013 1 5 21 1.1141 0.0005 1 6 1 4.6504 -0.0007 1 6 2 -1.4159 -0.0133 1 6 3 2.3492 -0.0045 1 6 4 -3.3101 0.0010 1 6 5 0.7118 -0.0025 1 6 6 -1.8328 0.0066 1 6 7 -3.5348 0.0042 1 6 8 -1.0684 0.0014 1 6 9 -3.2814 0.0027 1 6 10 0.9249 -0.0020 1 6 11 -1.6425 -0.0008 1 6 12 -0.9475 -0.0034 1 6 13 -0.4110 -0.0035 1 6 14 -0.4411 0.0005 1 6 15 1.3025 -0.0000 1 6 16 -0.3350 0.0020 1 6 17 -1.2624 0.0016 1 6 18 -2.9818 0.0014 1 6 19 -0.7103 0.0015 1 6 20 -1.2805 -0.0014 1 6 21 1.8110 0.0000 1 7 0 2.5208 0.0017 1 7 1 0.7585 0.0067 1 7 2 6.2848 0.0029 1 7 3 0.5774 0.0045 1 7 4 1.4737 -0.0017 1 7 5 -0.8491 -0.0037 1 7 6 -2.2457 0.0017 1 7 7 -1.1520 -0.0052 1 7 8 -4.8791 -0.0040 1 7 9 -0.4859 0.0004 1 7 10 -1.9232 0.0012 1 7 11 -0.6614 0.0039 1 7 12 -1.4089 0.0012 1 7 13 -0.4502 0.0021 1 7 14 -0.7472 0.0012 1 7 15 -1.2083 -0.0022 1 7 16 0.5114 0.0002 1 7 17 -2.0119 -0.0024 1 7 18 -0.3559 -0.0015 1 7 19 -4.8434 0.0006 1 7 20 -0.6719 0.0005 1 7 21 0.2447 0.0021 1 8 0 -1.7495 -0.0027 1 8 1 4.0188 -0.0043 1 8 2 0.5006 -0.0037 1 8 3 2.3793 0.0004 1 8 4 2.1421 -0.0010 1 8 5 0.6026 0.0015 1 8 6 1.1290 0.0036 1 8 7 -2.6568 0.0021 1 8 8 -0.7096 0.0031 1 8 9 -2.2661 -0.0015 1 8 10 -1.1795 -0.0031 1 8 11 -2.9129 -0.0008 1 8 12 -1.0682 -0.0026 1 8 13 -1.3789 -0.0013 1 8 14 -1.2984 0.0005 1 8 15 1.8794 0.0026 1 8 16 0.1245 0.0025 1 8 17 -1.2634 0.0000 1 8 18 -2.8871 0.0015 1 8 19 -1.2688 0.0001 1 8 20 -2.3722 -0.0015 1 9 0 1.2653 0.0040 1 9 1 -1.0454 0.0014 1 9 2 1.7103 -0.0010 1 9 3 2.3931 0.0006 1 9 4 -0.7508 -0.0006 1 9 5 1.5046 -0.0005 1 9 6 0.3339 -0.0025 1 9 7 0.9836 -0.0025 1 9 8 -0.7154 -0.0001 1 9 9 -0.5615 0.0002 1 9 10 -1.0710 0.0034 1 9 11 -1.2424 0.0030 1 9 12 -3.5011 -0.0007 1 9 13 -1.5486 0.0007 1 9 14 -1.1894 -0.0010 1 9 15 0.4473 -0.0018 1 9 16 -0.1849 -0.0017 1 9 17 1.6585 -0.0011 1 9 18 0.4823 0.0002 1 9 19 -4.0141 0.0004 1 9 20 -1.3306 0.0005 1 10 0 -3.3195 -0.0010 1 10 1 -0.2255 -0.0016 1 10 2 2.6281 0.0013 1 10 3 -0.1532 0.0003 1 10 4 1.2481 -0.0004 1 10 5 -0.3691 0.0007 1 10 6 0.3446 0.0022 1 10 7 0.2625 0.0032 1 10 8 0.3284 -0.0001 1 10 9 0.7426 -0.0033 1 10 10 1.1377 -0.0008 1 10 11 -2.8395 -0.0014 1 10 12 -0.6138 -0.0009 1 10 13 -3.6788 0.0002 1 10 14 -1.2921 0.0010 1 10 15 -0.9655 0.0013 1 10 16 1.2857 0.0014 1 10 17 0.1606 -0.0009 1 10 18 -1.3404 -0.0002 1 10 19 0.7957 -0.0018 1 11 0 -1.4641 -0.0002 1 11 1 0.1449 -0.0019 1 11 2 -0.9582 0.0003 1 11 3 1.5150 0.0004 1 11 4 0.0031 0.0013 1 11 5 0.1269 -0.0013 1 11 6 -0.3323 -0.0034 1 11 7 0.3290 -0.0003 1 11 8 -0.0331 0.0007 1 11 9 1.2942 0.0018 1 11 10 0.1990 0.0019 1 11 11 1.4249 -0.0001 1 11 12 -2.2709 -0.0006 1 11 13 -0.0096 0.0008 1 11 14 -2.6885 -0.0012 1 11 15 -1.5615 -0.0008 1 11 16 -1.0803 -0.0013 1 11 17 -0.5687 -0.0009 1 11 18 1.8562 0.0013 1 11 19 -3.2914 -0.0004 1 12 0 -0.2524 -0.0021 1 12 1 -1.1575 0.0015 1 12 2 0.5654 0.0001 1 12 3 0.2558 -0.0016 1 12 4 0.0141 0.0017 1 12 5 -1.2401 0.0011 1 12 6 0.4837 0.0013 1 12 7 -0.2933 0.0010 1 12 8 -0.2475 -0.0027 1 12 9 0.9615 -0.0013 1 12 10 2.0930 -0.0001 1 12 11 -0.6903 -0.0007 1 12 12 2.1339 0.0001 1 12 13 -1.0830 -0.0002 1 12 14 -0.2020 0.0007 1 12 15 0.4620 0.0024 1 12 16 -3.3470 0.0006 1 12 17 0.6904 -0.0003 1 13 0 0.3215 -0.0012 1 13 1 -0.7529 0.0018 1 13 2 -0.5618 -0.0005 1 13 3 1.0546 0.0004 1 13 4 -0.2252 0.0014 1 13 5 0.9082 -0.0030 1 13 6 -0.1816 -0.0005 1 13 7 -0.5292 0.0017 1 13 8 0.3596 0.0013 1 13 9 1.4194 0.0005 1 13 10 -0.2142 -0.0005 1 13 11 2.0180 0.0001 1 13 12 0.0768 0.0006 1 13 13 2.5255 -0.0006 1 13 14 2.9456 -0.0005 1 13 15 -2.0100 -0.0008 1 13 16 1.4202 -0.0016 1 13 17 -1.8130 -0.0007 1 14 0 0.9368 -0.0006 1 14 1 0.2672 0.0007 1 14 2 0.7628 -0.0014 1 14 3 -1.0995 0.0016 1 14 4 -0.0243 0.0018 1 14 5 0.6494 -0.0006 1 14 6 0.6850 0.0014 1 14 7 0.0632 -0.0008 1 14 8 1.7029 -0.0014 1 14 9 0.4310 0.0007 1 14 10 3.0751 0.0004 1 14 11 -0.3137 -0.0001 1 14 12 1.1128 -0.0010 1 14 13 1.1976 -0.0001 1 14 14 2.1651 0.0019 1 14 15 4.5807 0.0010 1 15 0 0.5353 0.0008 1 15 1 0.6003 0.0011 1 15 2 -0.2845 -0.0006 1 15 3 1.2178 0.0003 1 15 4 1.0387 -0.0014 1 15 5 0.0070 -0.0009 1 15 6 -1.7091 0.0011 1 15 7 1.0604 0.0008 1 15 8 -1.5312 0.0008 1 15 9 2.8952 -0.0006 1 15 10 1.5020 -0.0010 1 15 11 2.2774 0.0011 1 15 12 -0.0073 0.0005 1 15 13 1.9336 -0.0002 1 15 14 3.2601 -0.0015 1 15 15 -0.0995 -0.0001 1 16 0 0.6072 -0.0005 1 16 1 -1.4820 -0.0001 1 16 2 0.1042 0.0002 1 16 3 -0.6894 0.0020 1 16 4 -0.0804 0.0003 1 16 5 0.3775 -0.0002 1 16 6 1.6523 -0.0008 1 16 7 -3.9780 -0.0010 1 16 8 -0.7996 0.0005 1 16 9 -0.6489 -0.0003 1 16 10 1.6926 -0.0007 1 16 11 1.2199 0.0001 1 16 12 0.2476 -0.0005 1 16 13 1.3428 -0.0002 1 16 14 -0.1611 0.0005 1 17 0 -0.3014 -0.0002 1 17 1 0.5079 0.0002 1 17 2 -0.6058 -0.0009 1 17 3 -0.8149 -0.0013 1 17 4 -0.3528 0.0004 1 17 5 0.9301 0.0002 1 17 6 -2.9490 0.0006 1 17 7 -0.7939 0.0012 1 17 8 -2.6389 0.0012 1 17 9 -3.0752 -0.0027 1 17 10 0.5161 -0.0001 1 17 11 -0.0050 0.0008 1 17 12 0.9675 -0.0001 1 17 13 -1.0396 -0.0015 1 18 0 -1.1901 0.0008 1 18 1 -1.4393 -0.0000 1 18 2 -0.2813 -0.0002 1 18 3 -1.1889 0.0008 1 18 4 0.4629 -0.0000 1 18 5 0.4557 -0.0013 1 18 6 0.1610 -0.0009 1 18 7 -0.9626 0.0016 1 18 8 -3.7020 -0.0003 1 18 9 -2.5782 0.0001 1 18 10 -1.1956 0.0009 1 18 11 -0.6546 -0.0001 1 19 0 -0.3817 -0.0013 1 19 1 0.1936 0.0007 1 19 4 1.2122 0.0001 1 19 5 -0.7714 -0.0003 1 19 6 0.2810 0.0001 1 19 7 1.1515 0.0015 1 19 8 -1.8360 0.0001 1 19 9 -0.8687 0.0002 1 20 4 -0.0081 0.0002 1 20 5 -0.0407 -0.0020 1 20 6 1.3191 0.0000 1 21 0 0.2258 0.0011 2 0 2 -35.9117 -0.0306 2 0 4 -9.4791 0.0183 2 0 6 2.4917 0.0124 2 0 8 -1.6124 -0.0075 2 0 10 -1.1029 -0.0029 2 0 12 -0.9523 -0.0041 2 0 14 1.5103 0.0026 2 0 16 -1.0667 0.0030 2 0 18 3.3903 -0.0004 2 1 0 25.7070 0.0190 2 1 1 -3.4154 0.0423 2 1 2 11.3779 -0.0006 2 1 3 -18.3035 -0.0122 2 1 4 -6.8899 -0.0103 2 1 5 -1.7795 -0.0063 2 1 6 0.9930 0.0034 2 1 7 0.3349 -0.0096 2 1 8 0.7556 0.0014 2 1 9 -0.9859 0.0097 2 1 10 0.3975 -0.0001 2 1 11 -0.6724 0.0037 2 1 12 -0.8540 0.0027 2 1 13 -0.4506 -0.0009 2 1 14 0.9371 -0.0039 2 1 15 1.3975 -0.0041 2 1 16 1.0169 -0.0005 2 1 17 2.5811 -0.0020 2 1 18 -2.5488 -0.0000 2 1 19 0.4991 0.0026 2 2 0 18.6651 -0.0157 2 2 1 26.9232 0.0019 2 2 2 -5.3577 -0.0128 2 2 3 2.1557 0.0136 2 2 4 0.2696 0.0145 2 2 5 -1.9990 0.0015 2 2 6 -0.1109 0.0050 2 2 7 2.1565 -0.0055 2 2 8 -0.6616 -0.0020 2 2 9 0.1804 -0.0038 2 2 10 -1.2738 -0.0061 2 2 11 -0.1303 0.0023 2 2 12 0.1007 -0.0010 2 2 13 -1.3179 0.0012 2 2 14 1.2236 0.0043 2 2 15 1.6257 0.0006 2 2 16 3.5098 0.0012 2 2 17 -0.1341 -0.0008 2 2 18 2.4899 -0.0000 2 2 19 -1.7926 -0.0017 2 3 0 16.0196 0.0307 2 3 1 7.4453 0.0140 2 3 2 11.8148 -0.0209 2 3 3 5.5932 -0.0080 2 3 4 -0.0564 -0.0114 2 3 5 -0.4432 -0.0001 2 3 6 3.2360 0.0054 2 3 7 0.7474 -0.0034 2 3 8 1.9350 0.0066 2 3 9 -0.3313 0.0047 2 3 10 0.1060 0.0013 2 3 11 0.9837 0.0018 2 3 12 -1.9223 -0.0035 2 3 13 -0.1249 -0.0011 2 3 14 -0.6518 -0.0024 2 3 15 2.9519 -0.0028 2 3 16 0.4197 0.0008 2 3 17 5.4034 -0.0006 2 3 18 0.5780 0.0027 2 3 19 -2.3292 0.0012 2 4 0 1.0498 -0.0045 2 4 1 1.9842 -0.0044 2 4 2 2.3951 0.0062 2 4 3 6.5341 0.0167 2 4 4 2.8368 -0.0006 2 4 5 2.9137 0.0030 2 4 6 -0.9011 0.0000 2 4 7 1.4076 -0.0085 2 4 8 0.7285 -0.0011 2 4 9 0.3449 -0.0033 2 4 10 1.1756 -0.0011 2 4 11 -0.3212 0.0018 2 4 12 1.5697 -0.0001 2 4 13 -0.5556 0.0046 2 4 14 1.7877 0.0010 2 4 15 -1.7059 0.0011 2 4 16 1.8200 0.0001 2 4 17 1.7968 -0.0020 2 4 18 2.0156 -0.0007 2 4 19 0.0628 -0.0019 2 4 20 -0.5203 -0.0008 2 5 0 -0.3770 0.0140 2 5 1 -1.0370 -0.0069 2 5 2 2.0051 -0.0128 2 5 3 -2.6101 -0.0082 2 5 4 1.7824 -0.0039 2 5 5 -0.4722 0.0092 2 5 6 0.6076 0.0011 2 5 7 -0.0477 -0.0005 2 5 8 -0.0781 0.0071 2 5 9 1.5978 0.0007 2 5 10 -0.2585 0.0001 2 5 11 1.0278 -0.0017 2 5 12 -0.4463 -0.0030 2 5 13 0.6012 -0.0020 2 5 14 0.3122 -0.0029 2 5 15 1.7483 0.0009 2 5 16 -0.7456 0.0010 2 5 17 0.1285 0.0013 2 5 18 0.0061 0.0025 2 5 19 0.4997 0.0002 2 5 20 0.4688 0.0012 2 5 21 -0.0621 -0.0007 2 6 0 1.5491 0.0052 2 6 1 2.2881 0.0050 2 6 2 -2.5302 0.0096 2 6 3 2.3809 0.0044 2 6 4 -0.9895 -0.0021 2 6 5 -1.1550 0.0018 2 6 6 -1.8144 -0.0052 2 6 7 -2.1341 -0.0041 2 6 8 0.5741 -0.0009 2 6 9 -1.4561 -0.0030 2 6 10 0.7825 0.0028 2 6 11 0.4214 0.0017 2 6 12 -0.0891 0.0022 2 6 13 -0.4144 0.0030 2 6 14 1.3910 -0.0000 2 6 15 -0.3503 -0.0005 2 6 16 -1.4852 -0.0023 2 6 17 0.1667 -0.0019 2 6 18 -2.2955 -0.0004 2 6 19 0.4868 -0.0014 2 6 20 0.0741 0.0007 2 7 0 3.2347 -0.0004 2 7 1 -0.4930 -0.0099 2 7 2 2.7314 -0.0042 2 7 3 -0.5397 -0.0015 2 7 4 0.7165 0.0023 2 7 5 0.5402 0.0048 2 7 6 -2.0583 -0.0004 2 7 7 -0.0468 0.0033 2 7 8 -2.5287 0.0020 2 7 9 -0.0631 -0.0001 2 7 10 -0.7642 -0.0005 2 7 11 -0.5166 -0.0040 2 7 12 -1.3012 -0.0021 2 7 13 -0.9415 0.0001 2 7 14 1.0608 0.0004 2 7 15 0.0459 0.0018 2 7 16 0.3709 0.0007 2 7 17 -3.1087 0.0020 2 7 18 -1.3366 0.0012 2 7 19 -2.9184 -0.0013 2 7 20 1.1699 -0.0003 2 8 0 -1.7682 0.0032 2 8 1 3.2371 0.0023 2 8 2 0.6390 0.0035 2 8 3 0.6109 -0.0033 2 8 4 1.7133 -0.0011 2 8 5 -0.3944 0.0011 2 8 6 0.7278 -0.0037 2 8 7 -1.3024 -0.0033 2 8 8 -0.1886 -0.0016 2 8 9 -1.0900 0.0027 2 8 10 -0.8766 0.0032 2 8 11 -1.0318 -0.0001 2 8 12 -0.6979 0.0023 2 8 13 -0.4810 0.0008 2 8 14 -0.2133 -0.0016 2 8 15 -0.0547 -0.0008 2 8 16 -0.8050 -0.0016 2 8 17 0.5022 -0.0004 2 8 18 -4.5184 -0.0006 2 8 19 -0.0124 0.0008 2 8 20 -1.6723 0.0023 2 9 0 1.3389 -0.0046 2 9 1 -0.3678 -0.0002 2 9 2 -0.7968 0.0003 2 9 3 1.3144 -0.0009 2 9 4 0.7737 0.0019 2 9 5 0.7378 0.0009 2 9 6 0.1962 0.0012 2 9 7 0.3628 0.0020 2 9 8 0.1173 -0.0001 2 9 9 -0.3058 -0.0009 2 9 10 -2.0320 -0.0026 2 9 11 -0.0032 -0.0021 2 9 12 -2.0145 0.0001 2 9 13 -1.2872 -0.0007 2 9 14 0.7340 0.0009 2 9 15 1.1928 0.0020 2 9 16 0.1223 -0.0004 2 9 17 -2.8747 0.0013 2 9 18 -0.0781 0.0001 2 9 19 -2.9103 -0.0004 2 10 0 -1.3366 0.0008 2 10 1 -0.2060 0.0005 2 10 2 0.6725 -0.0015 2 10 3 -0.9503 -0.0001 2 10 4 -0.5206 0.0012 2 10 5 0.7585 -0.0016 2 10 6 0.3949 -0.0022 2 10 7 0.4986 -0.0021 2 10 8 1.2904 0.0006 2 10 9 -0.5037 0.0033 2 10 10 0.2593 0.0013 2 10 11 -2.3023 -0.0005 2 10 12 -1.2641 0.0007 2 10 13 -1.6987 -0.0009 2 10 14 0.2204 -0.0001 2 10 15 -1.7181 -0.0023 2 10 16 0.2026 -0.0015 2 10 17 1.1450 0.0001 2 10 18 -3.7867 -0.0004 2 10 19 0.2175 0.0005 2 11 0 -1.5933 0.0007 2 11 1 0.3578 0.0007 2 11 2 -0.4190 -0.0005 2 11 3 -0.2810 0.0012 2 11 4 0.2344 -0.0014 2 11 5 -0.9134 0.0013 2 11 6 -0.3751 0.0028 2 11 7 1.0895 -0.0007 2 11 8 0.8714 -0.0015 2 11 9 1.4476 -0.0007 2 11 10 -0.7780 -0.0018 2 11 11 1.5297 0.0002 2 11 12 -2.9320 0.0001 2 11 13 -1.4835 0.0006 2 11 14 -2.5994 0.0014 2 11 15 -0.6016 0.0008 2 11 16 -0.0843 0.0008 2 11 17 -3.9100 0.0001 2 11 18 1.2019 -0.0005 2 12 0 -1.6282 0.0000 2 12 1 -1.4496 -0.0018 2 12 2 -1.0064 0.0010 2 12 3 -0.0362 0.0014 2 12 4 -0.0984 -0.0018 2 12 5 0.0278 -0.0008 2 12 6 0.0307 -0.0015 2 12 7 0.0353 -0.0008 2 12 8 1.9260 0.0026 2 12 9 0.3101 0.0018 2 12 10 1.7309 -0.0006 2 12 11 -0.7413 -0.0006 2 12 12 1.6672 0.0002 2 12 13 -0.7359 0.0011 2 12 14 -1.8295 -0.0004 2 12 15 -2.0094 -0.0014 2 12 16 -3.5265 -0.0003 2 12 17 0.4466 0.0020 2 13 0 0.0016 0.0013 2 13 1 -0.7769 -0.0011 2 13 2 -0.6817 0.0007 2 13 3 -0.5391 -0.0004 2 13 4 -0.2232 -0.0000 2 13 5 -0.4751 0.0028 2 13 6 0.0472 0.0001 2 13 7 1.5961 -0.0026 2 13 9 1.8971 -0.0008 2 13 10 0.1911 0.0003 2 13 11 3.0193 -0.0001 2 13 12 -0.3298 0.0002 2 13 13 0.7298 0.0000 2 13 14 1.1715 0.0007 2 13 15 -1.8809 0.0014 2 13 16 -0.1479 0.0001 2 14 0 -1.0248 0.0008 2 14 1 -0.6492 -0.0002 2 14 2 0.2134 0.0013 2 14 3 0.7823 -0.0008 2 14 4 0.1701 -0.0017 2 14 5 0.2391 -0.0000 2 14 6 0.2469 -0.0002 2 14 7 -0.7917 0.0024 2 14 8 3.5072 0.0006 2 14 9 0.3150 -0.0012 2 14 10 1.6714 -0.0009 2 14 11 -1.0190 -0.0001 2 14 12 3.0844 0.0000 2 14 13 2.7195 0.0003 2 14 14 -0.3800 0.0007 2 14 15 1.8285 -0.0024 2 14 16 -2.2502 -0.0019 2 15 0 -0.0804 -0.0006 2 15 1 0.1944 -0.0009 2 15 2 -0.8870 0.0012 2 15 3 -0.8530 0.0008 2 15 4 1.0067 0.0001 2 15 5 0.4568 0.0010 2 15 6 -2.2512 -0.0010 2 15 7 2.6776 -0.0010 2 15 8 -0.4748 -0.0007 2 15 9 2.6442 0.0007 2 15 10 0.3860 0.0013 2 15 11 1.3990 -0.0016 2 15 12 -1.4473 -0.0011 2 15 13 -0.2301 0.0009 2 15 14 4.0026 0.0016 2 15 15 0.7332 0.0005 2 16 0 0.2344 0.0005 2 16 1 -1.0334 -0.0005 2 16 2 -0.9543 0.0008 2 16 3 1.0581 -0.0018 2 16 4 -0.0443 -0.0007 2 16 5 -2.5953 0.0009 2 16 6 0.0651 0.0019 2 16 7 -3.5311 0.0010 2 16 8 0.5075 -0.0018 2 16 9 1.5676 -0.0005 2 16 10 0.9851 -0.0005 2 16 11 -0.9516 0.0002 2 16 12 0.1897 0.0006 2 16 13 0.7268 -0.0000 2 17 0 -0.6567 -0.0009 2 17 1 -0.7926 0.0004 2 17 2 -1.1597 0.0014 2 17 3 -1.0861 -0.0002 2 17 4 0.1413 -0.0001 2 17 5 0.1020 -0.0004 2 17 6 -2.3318 -0.0002 2 17 7 -3.5055 -0.0004 2 17 8 -2.0033 0.0001 2 17 9 -1.0136 -0.0003 2 17 10 0.7145 -0.0007 2 17 11 0.1339 -0.0005 2 17 12 -0.9674 0.0004 2 18 0 1.2089 0.0000 2 18 1 -0.0060 -0.0014 2 18 2 -1.4086 -0.0010 2 18 3 1.2969 -0.0005 2 18 4 -1.7593 -0.0005 2 18 5 0.9584 0.0000 2 18 6 -1.3286 0.0011 2 18 7 -2.8210 0.0007 2 18 8 -3.2262 -0.0015 2 18 9 -1.5080 -0.0009 2 18 10 -1.5662 -0.0008 2 19 0 -0.2849 -0.0002 2 19 1 -1.4570 -0.0004 2 19 3 -1.4522 0.0002 2 19 4 2.2935 -0.0022 2 19 5 0.4595 -0.0004 2 19 6 0.3315 -0.0005 2 19 7 -0.5446 -0.0012 2 19 8 -2.8932 -0.0000 2 20 4 -1.1771 -0.0002 2 20 5 0.9734 0.0008 3 0 0 -12.6437 0.0335 3 0 2 -19.3821 0.0041 3 0 4 -0.6268 -0.0103 3 0 6 1.4979 -0.0099 3 0 8 0.6309 0.0044 3 0 10 0.0866 0.0073 3 0 12 0.2881 -0.0019 3 0 14 -0.2841 -0.0025 3 0 16 4.8985 -0.0024 3 0 18 8.6835 0.0004 3 0 20 1.8711 0.0023 3 1 0 14.3037 -0.0099 3 1 1 -18.8872 -0.0452 3 1 2 -2.0143 0.0075 3 1 3 -8.3835 0.0157 3 1 4 -3.5672 0.0024 3 1 5 3.7543 0.0087 3 1 6 0.3852 0.0012 3 1 7 -1.1931 0.0014 3 1 8 -0.0989 -0.0033 3 1 9 -0.1970 -0.0062 3 1 10 0.8088 0.0015 3 1 11 -0.9079 -0.0037 3 1 12 0.2192 -0.0009 3 1 13 1.6878 0.0020 3 1 14 2.4483 -0.0013 3 1 15 1.5300 0.0026 3 1 16 -1.3897 0.0017 3 1 17 7.4298 0.0010 3 1 18 -2.0456 -0.0010 3 2 0 -0.6225 0.0248 3 2 1 11.7436 -0.0010 3 2 2 -1.3959 0.0046 3 2 3 -6.7621 -0.0176 3 2 4 -2.8181 -0.0093 3 2 5 -0.3864 0.0033 3 2 6 -1.0581 -0.0064 3 2 7 0.3543 0.0050 3 2 8 -1.5141 0.0041 3 2 9 0.8164 0.0016 3 2 10 -0.3494 0.0044 3 2 11 -1.0999 -0.0003 3 2 12 0.1757 0.0014 3 2 13 1.2201 -0.0033 3 2 14 1.3939 -0.0040 3 2 15 1.8297 -0.0007 3 2 16 7.9386 -0.0021 3 2 17 -3.0292 0.0006 3 2 18 1.3443 0.0010 3 3 0 8.2747 -0.0253 3 3 1 3.3786 -0.0126 3 3 2 2.3662 0.0196 3 3 3 1.0177 0.0116 3 3 4 0.7756 0.0096 3 3 5 -1.0128 -0.0001 3 3 6 -0.0696 -0.0061 3 3 7 -1.9426 0.0031 3 3 8 0.1400 -0.0058 3 3 9 -0.7494 -0.0049 3 3 10 -0.7702 0.0011 3 3 11 0.4700 -0.0013 3 3 12 -1.1179 0.0022 3 3 13 1.2798 0.0018 3 3 14 0.1538 0.0029 3 3 15 4.4078 0.0016 3 3 16 0.7709 -0.0015 3 3 17 3.9659 -0.0003 3 3 18 0.7947 -0.0022 3 4 0 0.9150 0.0064 3 4 1 3.9269 -0.0079 3 4 2 2.6180 -0.0090 3 4 3 0.7147 -0.0124 3 4 4 -0.8193 0.0033 3 4 5 1.2009 0.0007 3 4 6 -0.3399 0.0012 3 4 7 1.0535 0.0074 3 4 8 -0.1709 -0.0004 3 4 9 0.7442 0.0032 3 4 10 1.6153 0.0016 3 4 11 -1.9370 -0.0027 3 4 12 1.0015 -0.0018 3 4 13 -0.7986 -0.0032 3 4 14 1.1615 -0.0012 3 4 15 -0.3133 0.0002 3 4 16 4.2800 0.0009 3 4 17 1.0530 0.0020 3 4 18 -0.1300 0.0003 3 4 19 0.1851 0.0018 3 4 20 -2.7655 0.0007 3 5 0 -2.1513 -0.0122 3 5 1 -1.6376 0.0069 3 5 2 1.4238 0.0163 3 5 3 0.1283 0.0048 3 5 4 1.3011 0.0023 3 5 5 -0.9528 -0.0064 3 5 6 0.4123 -0.0028 3 5 7 -0.4547 -0.0004 3 5 8 0.8833 -0.0059 3 5 9 2.1066 0.0003 3 5 10 0.0577 0.0006 3 5 11 0.9352 0.0009 3 5 12 -0.1573 0.0039 3 5 13 2.4669 0.0005 3 5 14 -1.4770 0.0009 3 5 15 0.9225 -0.0000 3 5 16 -0.3801 -0.0016 3 5 17 0.2804 -0.0009 3 5 18 1.3855 -0.0021 3 5 19 -0.3842 0.0003 3 5 20 -0.3013 0.0006 3 6 0 0.3760 -0.0070 3 6 1 1.7474 -0.0058 3 6 2 -2.1939 -0.0085 3 6 3 -0.2242 -0.0023 3 6 4 -0.8913 0.0068 3 6 5 0.4681 -0.0013 3 6 6 -0.4386 0.0030 3 6 7 -0.5221 0.0033 3 6 8 0.9920 0.0009 3 6 9 1.3558 0.0012 3 6 10 0.7637 -0.0028 3 6 11 -0.7338 -0.0013 3 6 12 0.7476 -0.0014 3 6 13 -0.3478 -0.0031 3 6 14 1.4531 0.0012 3 6 15 0.2799 0.0003 3 6 16 0.1254 0.0017 3 6 17 -1.5720 0.0011 3 6 18 -1.1324 -0.0002 3 6 19 0.8790 0.0012 3 6 20 0.1708 -0.0007 3 7 0 2.0054 0.0013 3 7 1 -0.8507 0.0090 3 7 2 2.0467 0.0022 3 7 3 0.7902 0.0017 3 7 4 -0.4268 -0.0012 3 7 5 -0.3886 -0.0058 3 7 6 -0.5964 -0.0009 3 7 7 -0.0916 -0.0009 3 7 8 -0.0034 -0.0020 3 7 9 0.3454 0.0015 3 7 10 0.7489 0.0008 3 7 11 -0.3040 0.0035 3 7 12 -0.8180 0.0014 3 7 13 1.3687 -0.0001 3 7 15 0.3553 -0.0019 3 7 16 -0.5068 -0.0009 3 7 17 -2.1159 -0.0014 3 7 18 0.6266 -0.0008 3 7 19 -2.0986 0.0007 3 8 0 -1.2588 -0.0052 3 8 1 0.5751 -0.0051 3 8 2 0.4067 -0.0021 3 8 3 0.5507 0.0048 3 8 4 1.0907 0.0009 3 8 5 0.5717 -0.0017 3 8 6 0.5961 0.0032 3 8 7 -0.3824 0.0018 3 8 8 0.1132 0.0013 3 8 9 0.8232 -0.0012 3 8 10 0.5428 -0.0027 3 8 11 -0.9711 -0.0008 3 8 12 -0.0965 -0.0019 3 8 13 -0.0518 0.0005 3 8 14 -0.1172 0.0016 3 8 15 0.4521 0.0004 3 8 16 -1.2271 0.0020 3 8 17 -0.6292 0.0010 3 8 18 -3.6468 -0.0000 3 8 19 -0.0822 -0.0008 3 9 0 0.9211 0.0024 3 9 1 -0.5602 0.0000 3 9 2 -0.3803 -0.0004 3 9 3 0.1271 -0.0003 3 9 4 -0.3317 -0.0013 3 9 5 0.7307 -0.0018 3 9 6 0.7681 -0.0022 3 9 7 0.6541 -0.0022 3 9 8 0.4435 0.0017 3 9 9 0.9361 0.0018 3 9 10 0.1746 0.0012 3 9 11 -0.6376 0.0016 3 9 12 0.5139 -0.0002 3 9 13 0.2516 -0.0005 3 9 14 -0.8321 -0.0018 3 9 15 -0.5498 -0.0009 3 9 16 -0.9001 0.0004 3 9 17 -3.2749 -0.0012 3 9 18 0.5817 0.0008 3 9 19 -2.9205 0.0017 3 10 0 -0.9036 -0.0012 3 10 1 -1.0932 0.0004 3 10 2 0.1236 0.0019 3 10 3 0.0175 0.0005 3 10 4 -1.0463 -0.0002 3 10 5 0.4572 0.0007 3 10 6 0.3379 0.0009 3 10 7 0.5487 0.0018 3 10 8 0.6815 -0.0005 3 10 9 0.2683 -0.0038 3 10 10 0.8188 -0.0012 3 10 11 -0.4116 0.0008 3 10 12 -1.1785 -0.0003 3 10 13 -0.9620 0.0005 3 10 14 -0.1689 0.0009 3 10 15 -0.7343 0.0007 3 10 16 -2.2677 0.0002 3 10 17 -0.1612 0.0003 3 10 18 -3.8114 -0.0003 3 11 0 -0.9991 -0.0014 3 11 1 -0.7378 -0.0009 3 11 2 0.0701 -0.0004 3 11 3 -1.8003 0.0009 3 11 4 0.3272 0.0006 3 11 5 0.0123 -0.0026 3 11 6 0.4272 -0.0023 3 11 7 1.1268 0.0018 3 11 8 0.1855 0.0021 3 11 9 1.0998 0.0007 3 11 10 0.0611 0.0008 3 11 11 -1.6855 -0.0003 3 11 12 -0.5862 -0.0002 3 11 13 -0.6945 0.0000 3 11 14 -2.8876 -0.0006 3 11 15 -1.8087 -0.0008 3 11 16 -0.8563 0.0007 3 11 17 -2.2705 -0.0005 3 12 0 -1.8974 -0.0004 3 12 1 -0.3370 0.0004 3 12 2 -0.8100 -0.0001 3 12 3 0.2268 -0.0012 3 12 4 -1.4244 0.0009 3 12 5 -0.1078 0.0006 3 12 6 1.2255 0.0007 3 12 7 1.0378 0.0003 3 12 8 0.4783 -0.0022 3 12 9 1.2486 -0.0012 3 12 10 1.3391 0.0007 3 12 11 0.0802 0.0012 3 12 12 -0.9803 -0.0001 3 12 13 -2.8744 0.0007 3 12 14 -2.3140 -0.0001 3 12 15 -1.4339 0.0009 3 12 17 0.1703 0.0005 3 13 0 -0.8842 -0.0013 3 13 1 -1.3643 0.0009 3 13 2 0.1454 0.0004 3 13 3 -0.9121 -0.0007 3 13 4 0.6607 -0.0004 3 13 5 -0.1148 -0.0029 3 13 6 0.4562 0.0002 3 13 7 1.5462 0.0019 3 13 8 1.0539 0.0012 3 13 9 1.3228 -0.0002 3 13 10 0.2840 -0.0012 3 13 11 0.6259 -0.0006 3 13 12 1.7668 0.0015 3 13 13 -0.6820 0.0006 3 13 14 -1.3556 -0.0028 3 13 15 -4.5720 0.0003 3 13 16 -1.4629 0.0013 3 14 0 -0.5209 -0.0012 3 14 1 -0.0386 0.0013 3 14 2 -0.4038 -0.0014 3 14 3 0.8296 0.0003 3 14 4 -1.2007 0.0024 3 14 5 -0.3503 0.0000 3 14 6 2.1940 -0.0013 3 14 7 0.3478 -0.0013 3 14 8 1.0695 -0.0008 3 14 9 1.0300 0.0002 3 14 10 0.9844 -0.0002 3 14 11 0.8632 0.0006 3 14 12 -0.5220 0.0006 3 14 13 1.4037 -0.0013 3 14 14 -1.8532 0.0010 3 14 15 -0.3384 0.0006 3 15 0 -0.9884 0.0008 3 15 1 -0.8110 0.0015 3 15 2 1.1002 -0.0021 3 15 3 -0.3330 -0.0000 3 15 4 0.1765 -0.0002 3 15 5 0.5642 -0.0004 3 15 6 -1.9736 0.0024 3 15 7 1.9231 0.0011 3 15 8 1.2699 -0.0001 3 15 9 0.2348 -0.0015 3 15 10 -1.2872 -0.0009 3 15 11 -0.6932 0.0005 3 15 12 1.8080 0.0004 3 15 13 -0.5856 0.0004 3 15 14 0.9889 -0.0001 3 16 0 -0.8541 0.0003 3 16 1 -1.4267 0.0002 3 16 2 -2.1167 0.0002 3 16 3 -0.1148 0.0011 3 16 4 -0.3834 0.0004 3 16 5 -2.0407 -0.0005 3 16 6 0.4555 -0.0005 3 16 7 -0.7440 -0.0012 3 16 8 0.4376 0.0005 3 16 9 0.8410 0.0013 3 16 10 -0.0430 -0.0001 3 16 11 -2.0092 0.0003 3 16 12 -3.5294 -0.0019 3 16 13 0.9476 0.0006 3 17 0 -0.3887 -0.0002 3 17 1 -1.6750 -0.0000 3 17 2 -0.2111 -0.0012 3 17 3 -2.5275 -0.0010 3 17 4 -0.4799 -0.0002 3 17 5 -1.7005 0.0020 3 17 6 -3.1164 0.0004 3 17 7 -1.3044 -0.0011 3 17 8 0.3879 -0.0007 3 17 9 -0.0448 -0.0019 3 17 10 -0.2778 0.0003 3 17 11 -2.0495 0.0009 3 18 0 -0.4314 -0.0002 3 18 1 0.8504 0.0008 3 18 2 -2.7189 -0.0003 3 18 3 1.4075 -0.0008 3 18 4 -1.4691 0.0000 3 18 5 -0.5434 -0.0016 3 18 6 -1.9898 -0.0009 3 18 7 -2.7245 0.0003 3 18 8 -2.2376 0.0007 3 18 9 0.6265 -0.0017 3 19 0 1.3738 -0.0015 3 19 1 -1.3015 0.0008 3 19 3 -2.8703 0.0011 3 19 4 2.4031 0.0002 3 19 5 0.9561 -0.0005 3 19 6 -2.0846 -0.0011 3 19 7 -0.8707 0.0008 3 20 3 1.6187 0.0009 3 20 4 1.2529 0.0003 4 0 0 -12.7731 -0.0457 4 0 2 -8.3923 -0.0026 4 0 4 6.2473 0.0174 4 0 6 1.4404 0.0038 4 0 8 0.6647 -0.0033 4 0 10 -1.6026 -0.0052 4 0 12 0.6513 -0.0020 4 0 14 0.2003 0.0035 4 0 16 11.6892 0.0009 4 1 0 3.3942 0.0116 4 1 1 -8.5884 0.0313 4 1 2 -5.7137 -0.0099 4 1 3 1.3149 -0.0155 4 1 4 -2.7737 -0.0009 4 1 5 -0.3457 -0.0079 4 1 6 -0.3111 0.0025 4 1 7 0.8957 0.0000 4 1 8 1.1446 0.0002 4 1 9 -1.0979 0.0068 4 1 10 0.5621 0.0017 4 1 11 0.5294 0.0015 4 1 12 1.0660 -0.0011 4 1 13 -1.2309 -0.0026 4 1 14 0.6814 -0.0011 4 1 15 7.0184 -0.0031 4 1 16 -4.9857 -0.0002 4 1 17 12.5724 0.0002 4 1 18 0.3909 -0.0003 4 2 0 -1.7085 -0.0293 4 2 1 -3.8090 0.0068 4 2 2 -4.3303 0.0031 4 2 3 -4.0752 0.0148 4 2 4 -0.0199 0.0080 4 2 5 -2.0707 -0.0015 4 2 6 -1.8635 0.0040 4 2 7 -0.3613 -0.0059 4 2 8 -1.7482 -0.0041 4 2 9 0.9116 0.0003 4 2 10 -0.9728 -0.0042 4 2 11 -0.0609 0.0003 4 2 12 0.6085 0.0011 4 2 13 1.9745 0.0016 4 2 14 3.5073 0.0026 4 2 15 -2.8976 0.0001 4 2 16 7.8831 0.0008 4 2 17 -2.4491 -0.0012 4 3 0 3.0609 0.0157 4 3 1 1.9536 0.0115 4 3 2 -3.1673 -0.0188 4 3 3 -1.4356 -0.0101 4 3 4 -3.1939 -0.0023 4 3 5 -2.7537 0.0012 4 3 6 -0.5428 0.0055 4 3 7 -1.7911 -0.0018 4 3 8 1.1360 0.0053 4 3 9 -1.0926 0.0037 4 3 10 -1.6389 -0.0020 4 3 11 0.8663 0.0013 4 3 12 -0.2965 -0.0025 4 3 13 -0.4010 -0.0022 4 3 14 1.0683 -0.0009 4 3 15 6.1938 -0.0011 4 3 16 -1.7970 0.0006 4 3 17 1.6735 -0.0002 4 3 20 1.6989 -0.0008 4 4 0 1.7920 -0.0060 4 4 1 -2.1743 0.0130 4 4 2 0.4062 0.0085 4 4 3 0.6162 0.0132 4 4 4 -0.4467 -0.0021 4 4 5 -1.0523 -0.0037 4 4 6 -1.8727 -0.0008 4 4 7 1.4762 -0.0062 4 4 8 0.1861 -0.0008 4 4 9 -0.8439 -0.0013 4 4 10 0.5081 -0.0008 4 4 11 -1.2131 0.0025 4 4 12 -0.0749 0.0000 4 4 13 -0.1520 0.0036 4 4 14 1.7826 0.0023 4 4 15 -0.5467 -0.0013 4 4 16 1.8418 -0.0007 4 4 17 1.6859 -0.0020 4 4 18 -2.7269 -0.0004 4 5 0 -0.7505 0.0079 4 5 1 0.0304 -0.0090 4 5 2 -0.8472 -0.0140 4 5 3 -0.7557 -0.0011 4 5 4 0.0131 -0.0017 4 5 5 -0.8922 0.0059 4 5 6 1.1989 0.0033 4 5 7 0.5946 -0.0016 4 5 8 1.8766 0.0043 4 5 9 1.2129 0.0001 4 5 10 -0.9023 -0.0006 4 5 11 0.9301 -0.0020 4 5 12 -0.9768 -0.0037 4 5 13 -0.2125 -0.0000 4 5 14 0.3654 -0.0012 4 5 15 1.2073 0.0016 4 5 16 -0.6878 0.0016 4 5 17 -0.0309 0.0003 4 5 18 -0.1694 0.0018 4 5 19 -2.6373 0.0009 4 6 0 -0.2682 0.0077 4 6 1 0.0719 0.0087 4 6 2 -0.2050 0.0082 4 6 3 0.7059 0.0004 4 6 4 -1.2087 -0.0075 4 6 5 -0.0564 -0.0002 4 6 6 -1.0604 -0.0023 4 6 7 1.7448 -0.0040 4 6 8 1.1822 0.0005 4 6 9 0.7243 -0.0005 4 6 10 0.4667 0.0022 4 6 11 -0.5550 0.0018 4 6 12 1.1586 0.0012 4 6 13 -0.0835 0.0014 4 6 14 1.9351 -0.0010 4 6 15 -1.3167 -0.0012 4 6 16 0.0655 -0.0016 4 6 17 -0.1536 -0.0011 4 6 18 -2.0250 0.0005 4 6 19 0.6757 -0.0004 4 7 0 1.3057 -0.0036 4 7 1 -0.5072 -0.0065 4 7 2 0.3670 -0.0012 4 7 3 -0.7193 0.0005 4 7 4 1.1294 0.0008 4 7 5 -0.5831 0.0051 4 7 6 -0.2881 0.0001 4 7 7 0.2597 0.0020 4 7 8 1.7427 0.0017 4 7 9 0.3623 -0.0019 4 7 10 -0.2287 -0.0012 4 7 11 1.1193 -0.0027 4 7 12 -1.2260 -0.0013 4 7 13 0.5792 0.0008 4 7 14 0.4463 0.0004 4 7 15 1.7719 0.0019 4 7 16 -0.7992 0.0004 4 7 17 -1.6105 0.0002 4 7 18 -0.2184 0.0003 4 7 19 -1.0380 -0.0003 4 8 0 -1.1148 0.0053 4 8 1 1.3297 0.0034 4 8 2 0.2523 0.0009 4 8 3 0.0260 -0.0034 4 8 4 0.5543 -0.0026 4 8 5 -0.3790 -0.0003 4 8 6 0.6053 -0.0016 4 8 7 1.4775 -0.0005 4 8 8 0.7067 0.0005 4 8 9 1.0380 0.0014 4 8 10 0.5069 0.0030 4 8 11 -0.0982 0.0004 4 8 13 -0.4984 -0.0001 4 8 14 0.8915 -0.0011 4 8 15 -1.7357 -0.0001 4 8 16 -0.8018 -0.0011 4 8 17 0.6001 0.0000 4 8 18 -2.1354 0.0007 4 9 0 0.0175 -0.0021 4 9 1 -0.0950 -0.0001 4 9 2 -1.2759 0.0030 4 9 3 0.5693 -0.0002 4 9 4 0.4241 -0.0007 4 9 5 0.3876 0.0013 4 9 6 0.2828 0.0020 4 9 7 1.0417 0.0013 4 9 8 1.7821 -0.0019 4 9 9 1.3119 -0.0011 4 9 10 0.8654 -0.0007 4 9 11 0.4515 -0.0022 4 9 12 0.1556 0.0008 4 9 13 -1.5930 0.0013 4 9 14 -1.3100 0.0006 4 9 15 -0.4813 0.0008 4 9 16 -1.0443 0.0008 4 9 17 -2.7648 0.0011 4 9 18 0.0950 0.0006 4 10 0 0.3679 0.0001 4 10 1 -0.0935 0.0005 4 10 2 -1.0718 -0.0003 4 10 3 -0.7202 -0.0008 4 10 4 -0.0320 -0.0009 4 10 5 -0.2178 -0.0004 4 10 6 0.6645 -0.0015 4 10 7 0.2679 -0.0007 4 10 8 1.4360 0.0011 4 10 10 -1.0020 0.0003 4 10 11 1.8309 -0.0004 4 10 12 -1.4883 0.0004 4 10 13 -0.4928 -0.0014 4 10 14 0.0001 -0.0011 4 10 15 -3.1954 0.0011 4 10 16 -2.0198 -0.0017 4 10 17 0.3288 0.0001 4 11 0 0.2362 0.0011 4 11 1 -0.1260 0.0023 4 11 2 -0.1575 0.0001 4 11 3 -0.5735 -0.0009 4 11 4 -0.0029 0.0001 4 11 5 0.0542 0.0017 4 11 6 -0.2933 0.0026 4 11 7 0.0583 -0.0010 4 11 9 -0.7777 -0.0015 4 11 10 1.6673 0.0003 4 11 11 -1.1883 0.0002 4 11 12 -1.0933 0.0008 4 11 13 -1.9556 -0.0006 4 11 14 -2.1401 0.0019 4 11 15 0.3568 0.0000 4 11 16 -0.0441 -0.0011 4 11 17 -2.1487 -0.0003 4 12 0 -0.5690 -0.0000 4 12 1 0.1238 -0.0009 4 12 2 -1.6590 0.0000 4 12 3 0.5355 0.0008 4 12 4 0.0757 -0.0024 4 12 5 0.5728 -0.0010 4 12 6 0.5538 0.0008 4 12 8 0.3533 0.0013 4 12 9 0.7494 0.0010 4 12 10 -2.1646 -0.0009 4 12 11 1.1387 -0.0000 4 12 12 -2.2177 -0.0013 4 12 13 -1.5707 -0.0010 4 12 14 -1.3506 0.0005 4 12 15 -2.3270 0.0001 4 12 16 -0.5715 0.0005 4 13 0 0.5113 0.0016 4 13 1 -0.5450 -0.0016 4 13 2 0.4875 -0.0001 4 13 3 -1.1190 0.0002 4 13 4 -0.2266 -0.0007 4 13 5 0.8194 0.0019 4 13 8 1.4576 -0.0017 4 13 9 -1.0764 0.0003 4 13 10 3.0919 0.0017 4 13 11 -1.2310 0.0009 4 13 12 -0.6841 -0.0010 4 13 13 -3.8766 -0.0004 4 13 14 -2.1024 -0.0008 4 13 15 -0.8753 0.0018 4 14 0 -0.0053 0.0005 4 14 1 0.5500 -0.0003 4 14 2 -0.4595 0.0014 4 14 3 0.8047 -0.0011 4 14 4 -0.1863 -0.0022 4 14 5 0.1394 0.0011 4 14 7 1.4564 0.0011 4 14 8 -0.3001 0.0006 4 14 9 1.0567 -0.0017 4 14 10 -2.1016 -0.0001 4 14 11 3.2125 0.0002 4 14 12 -1.6492 0.0015 4 14 13 0.6371 -0.0015 4 14 14 -4.0946 -0.0002 4 15 0 -0.4938 0.0001 4 15 1 -0.7385 -0.0008 4 15 2 0.6608 0.0011 4 15 5 0.4285 0.0001 4 15 6 0.4591 -0.0018 4 15 7 -0.2442 0.0001 4 15 8 0.4834 -0.0003 4 15 9 -2.1687 0.0009 4 15 10 2.2275 0.0012 4 15 11 -2.3177 0.0003 4 15 12 1.1512 -0.0009 4 15 13 -2.9678 -0.0003 4 16 0 -1.7150 0.0005 4 16 1 -1.5234 -0.0012 4 16 2 -1.6457 -0.0006 4 16 4 -0.6551 0.0001 4 16 5 -0.8450 0.0011 4 16 6 0.3403 0.0014 4 16 7 0.7854 0.0004 4 16 8 -0.6442 -0.0018 4 16 9 -0.5925 0.0001 4 16 10 -3.2282 0.0007 4 16 11 0.6133 0.0004 4 16 12 -0.6700 -0.0018 4 17 0 -1.4704 0.0002 4 17 1 -3.3391 -0.0002 4 17 2 -1.2890 0.0011 4 17 3 -2.4456 -0.0002 4 17 4 -1.1817 -0.0014 4 17 5 -0.4244 -0.0006 4 17 6 -0.8332 -0.0009 4 17 7 0.4125 -0.0003 4 17 8 0.5203 -0.0002 4 17 9 -0.6970 0.0020 4 17 10 -0.4347 0.0024 4 18 0 -0.3344 -0.0000 4 18 1 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13 1.4846 -0.0025 5 4 14 0.4763 -0.0002 5 4 15 -0.9523 0.0014 5 4 16 0.3509 -0.0001 5 4 17 -1.1106 0.0015 5 4 18 -4.3664 0.0016 5 4 19 -0.2894 -0.0013 5 5 0 -3.0754 -0.0027 5 5 1 0.5303 0.0075 5 5 2 -0.5482 0.0115 5 5 3 -0.5793 -0.0011 5 5 4 -0.6932 -0.0013 5 5 5 -0.8396 -0.0058 5 5 6 1.5929 -0.0036 5 5 7 0.4029 0.0009 5 5 8 0.3727 -0.0028 5 5 9 0.3201 0.0007 5 5 10 -1.6591 0.0015 5 5 11 -2.0773 0.0007 5 5 12 1.3699 0.0029 5 5 13 -0.3960 0.0009 5 5 14 -0.3491 -0.0005 5 5 15 0.5497 -0.0014 5 5 16 -0.8764 -0.0009 5 5 17 -2.7185 0.0003 5 5 18 0.2047 -0.0018 5 5 19 -3.3749 0.0003 5 6 0 0.5141 -0.0069 5 6 1 -0.2220 -0.0091 5 6 2 -1.6004 -0.0059 5 6 3 -0.3028 -0.0007 5 6 4 -1.3791 0.0063 5 6 5 0.3299 0.0007 5 6 6 0.1240 0.0015 5 6 7 0.8268 0.0036 5 6 8 0.3874 -0.0008 5 6 9 0.2689 0.0002 5 6 10 0.4209 -0.0022 5 6 11 -0.7068 -0.0020 5 6 12 -0.6450 -0.0002 5 6 13 1.2975 -0.0015 5 6 14 1.1269 0.0013 5 6 15 -0.4481 0.0015 5 6 16 -0.2153 0.0005 5 6 17 -0.7165 0.0013 5 6 18 -3.1454 0.0011 5 7 0 0.5946 0.0036 5 7 1 -0.6828 0.0063 5 7 2 1.2879 0.0011 5 7 3 -1.0310 -0.0031 5 7 4 -1.1627 -0.0009 5 7 5 -0.2801 -0.0030 5 7 6 0.7854 -0.0004 5 7 7 -0.1402 -0.0005 5 7 8 0.9210 -0.0006 5 7 9 0.6341 0.0022 5 7 10 -0.6554 0.0005 5 7 11 -0.3740 0.0019 5 7 13 1.8899 -0.0012 5 7 14 -0.4122 -0.0005 5 7 15 1.9255 -0.0019 5 7 16 0.2313 -0.0004 5 7 17 -2.1225 0.0006 5 7 18 0.7929 -0.0009 5 8 0 -0.7511 -0.0045 5 8 1 -0.3762 -0.0005 5 8 2 -0.2437 -0.0011 5 8 3 0.3366 0.0021 5 8 4 0.4829 0.0035 5 8 5 0.2123 -0.0000 5 8 6 0.3129 0.0022 5 8 7 1.1607 0.0010 5 8 8 0.5056 -0.0003 5 8 9 0.4352 -0.0017 5 8 12 -0.9284 -0.0002 5 8 13 -0.9765 0.0006 5 8 14 1.0350 0.0021 5 8 15 0.1135 0.0004 5 8 16 0.4681 0.0008 5 8 17 1.4064 -0.0005 5 9 0 -0.0255 0.0028 5 9 1 -0.3204 -0.0004 5 9 2 -0.2409 -0.0031 5 9 3 0.3302 -0.0003 5 9 4 -1.1931 0.0001 5 9 5 1.3835 -0.0017 5 9 6 0.9904 -0.0010 5 9 7 1.0554 -0.0002 5 9 8 1.0029 0.0015 5 9 9 0.7230 0.0015 5 9 11 -2.1554 0.0012 5 9 12 0.2313 -0.0014 5 9 13 0.3004 -0.0011 5 9 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8 5 0 -0.3031 -0.0052 8 5 1 -1.4120 -0.0032 8 5 2 -1.6469 -0.0038 8 5 3 0.0468 0.0045 8 5 4 -0.3141 0.0011 8 5 5 0.2618 0.0001 8 5 6 0.4354 0.0041 8 5 7 0.1364 0.0002 8 5 8 -0.1597 -0.0005 8 5 9 -1.6549 -0.0018 8 5 10 1.8176 -0.0012 8 5 11 0.2514 -0.0002 8 5 12 -0.1791 -0.0020 8 5 14 1.4977 0.0020 8 5 15 1.4124 0.0012 8 5 16 4.5638 0.0007 8 6 0 -0.2195 0.0060 8 6 1 -0.6275 0.0033 8 6 2 0.0331 -0.0015 8 6 3 -1.8466 -0.0005 8 6 4 -0.2806 -0.0033 8 6 5 -0.1240 -0.0018 8 6 6 1.6765 0.0003 8 6 7 1.8253 -0.0015 8 6 8 -0.3302 0.0006 8 6 9 0.6562 0.0011 8 6 10 -2.2325 0.0019 8 6 11 0.8595 0.0018 8 6 14 1.1786 -0.0018 8 6 15 4.3575 -0.0001 8 7 0 0.6207 -0.0027 8 7 1 0.1334 -0.0002 8 7 2 -0.9608 0.0013 8 7 3 0.7257 0.0022 8 7 4 -1.3625 -0.0017 8 7 5 -0.1799 0.0015 8 7 6 0.1992 0.0020 8 7 7 -0.4422 -0.0003 8 7 9 -0.8825 -0.0024 8 7 10 0.2829 -0.0002 8 7 11 0.1031 0.0000 8 7 14 4.1177 0.0008 8 7 15 1.7664 0.0003 8 8 0 0.2076 0.0018 8 8 1 1.5053 -0.0020 8 8 2 0.9267 -0.0016 8 8 3 -1.4918 0.0001 8 8 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0.5799 0.0007 8 11 12 -3.6739 0.0010 8 12 0 0.6821 0.0002 8 12 1 0.2269 -0.0002 8 12 2 0.1289 -0.0001 8 12 3 -1.0622 -0.0003 8 12 4 0.0375 -0.0013 8 12 5 -0.8630 -0.0010 8 12 6 -1.2426 0.0014 8 12 7 -0.9584 0.0015 8 12 8 -1.9572 -0.0002 8 12 9 -1.8781 -0.0015 8 12 12 4.0629 0.0004 8 13 0 1.1964 0.0006 8 13 1 0.5756 -0.0016 8 13 2 -0.5060 -0.0004 8 13 3 0.8453 0.0012 8 13 4 -0.2205 0.0001 8 13 5 1.2805 -0.0016 8 13 6 -1.2658 -0.0009 8 13 7 -3.0332 -0.0003 8 13 8 -2.2819 -0.0004 8 13 9 -1.4706 -0.0007 8 13 11 3.1933 0.0006 8 14 0 1.7925 0.0010 8 14 1 -0.6059 -0.0005 8 14 2 0.3158 -0.0008 8 14 3 1.3122 -0.0006 8 14 4 0.3553 -0.0002 8 14 5 0.7753 0.0015 8 14 6 1.6948 -0.0007 8 14 7 -1.5008 0.0006 8 14 8 -0.7518 -0.0009 8 15 0 -0.4507 0.0011 8 15 1 -0.9439 0.0003 8 15 2 1.9108 0.0000 8 15 3 -0.7874 0.0005 8 15 4 -0.0062 0.0005 8 15 5 4.8316 -0.0019 8 15 6 -0.8986 0.0006 8 15 7 2.5827 0.0001 8 16 0 1.1332 0.0005 8 16 1 0.5338 -0.0016 8 16 2 -1.1003 -0.0005 8 16 3 -0.8182 0.0006 8 16 4 1.6391 0.0005 8 16 5 -0.9807 0.0007 8 16 6 3.5206 -0.0013 8 17 0 0.7880 0.0005 8 17 1 -0.5365 -0.0008 8 17 2 1.7146 0.0004 8 17 3 -0.4182 -0.0009 8 17 4 -1.3500 -0.0007 8 17 5 0.6411 -0.0012 8 18 1 0.8043 0.0008 8 18 2 -1.2767 0.0011 9 0 0 1.0171 0.0108 9 0 2 -1.1219 -0.0088 9 0 4 -0.8116 -0.0032 9 0 6 1.4195 0.0027 9 0 8 2.9328 0.0028 9 0 10 -0.5798 -0.0007 9 0 12 -7.3085 -0.0018 9 0 14 -3.0847 -0.0008 9 1 0 0.7949 0.0018 9 1 1 -0.3783 0.0054 9 1 2 0.4597 0.0012 9 1 3 -1.2086 0.0047 9 1 4 -0.1405 0.0013 9 1 5 0.7114 0.0026 9 1 6 -0.6305 -0.0016 9 1 7 1.7235 -0.0060 9 1 8 0.1084 0.0003 9 1 9 0.7530 -0.0002 9 1 10 1.3743 -0.0004 9 1 11 -4.1301 0.0004 9 1 12 -1.8554 0.0007 9 1 13 -3.7111 0.0022 9 1 14 -2.8847 0.0009 9 1 15 -2.4056 0.0002 9 2 0 0.7248 0.0072 9 2 1 0.7970 -0.0077 9 2 2 -0.4858 -0.0082 9 2 3 -1.0619 0.0008 9 2 4 -0.1569 -0.0014 9 2 5 0.3730 0.0023 9 2 6 0.5194 0.0021 9 2 7 -0.7425 0.0008 9 2 8 0.2248 0.0014 9 2 9 1.0553 -0.0011 9 2 10 -0.5624 0.0006 9 2 11 -1.1560 -0.0008 9 2 12 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11 -0.2991 0.0007 9 5 12 0.2293 0.0012 9 5 13 0.4481 -0.0004 9 5 14 3.2864 -0.0023 9 6 0 -0.2755 -0.0036 9 6 1 -0.4928 -0.0018 9 6 2 -0.4366 0.0026 9 6 3 -0.4953 -0.0002 9 6 4 1.3420 0.0014 9 6 5 0.6977 0.0020 9 6 6 0.5404 -0.0004 9 6 7 0.5009 0.0003 9 6 8 -1.0559 -0.0015 9 6 9 -0.0789 -0.0005 9 6 10 -0.4035 -0.0005 9 6 11 -0.4274 -0.0020 9 6 12 -0.5083 0.0002 9 6 14 2.5736 0.0011 9 7 0 0.8327 0.0010 9 7 1 0.1005 -0.0013 9 7 2 -1.4226 -0.0017 9 7 3 0.3438 -0.0028 9 7 4 -1.1324 0.0008 9 7 5 0.4238 0.0004 9 7 6 1.3133 -0.0016 9 7 7 0.1243 -0.0001 9 7 8 0.4450 0.0011 9 7 9 -2.0422 0.0022 9 7 10 -1.9015 0.0008 9 7 11 -1.2245 -0.0004 9 7 12 0.6244 -0.0007 9 7 14 4.1991 -0.0002 9 8 0 1.0435 -0.0004 9 8 1 -0.4121 0.0034 9 8 2 0.7775 0.0011 9 8 3 -1.3079 -0.0020 9 8 4 -0.2917 0.0017 9 8 5 -0.1100 0.0017 9 8 6 -1.7159 0.0005 9 8 7 0.4710 -0.0012 9 8 8 0.3507 -0.0014 9 8 9 -0.5498 0.0004 9 8 10 -0.0766 -0.0007 9 8 11 -0.1607 -0.0002 9 9 0 0.7894 -0.0011 9 9 1 0.7330 -0.0011 9 9 2 0.4527 -0.0010 9 9 3 -0.2591 0.0005 9 9 4 0.4132 0.0007 9 9 5 -0.5735 -0.0006 9 9 6 -0.6614 0.0002 9 9 7 1.1997 0.0011 9 9 8 0.7854 0.0012 9 9 9 -0.1030 0.0009 9 9 10 0.1102 0.0001 9 9 11 -1.5523 0.0010 9 10 0 -0.3693 0.0017 9 10 1 0.5748 0.0008 9 10 2 -0.2026 -0.0006 9 10 3 0.8278 -0.0007 9 10 4 1.5071 0.0014 9 10 5 -0.2987 0.0018 9 10 6 -0.6313 0.0000 9 10 7 1.3852 -0.0024 9 10 8 0.6063 -0.0010 9 10 9 2.6486 0.0011 9 10 10 2.5428 -0.0004 9 10 11 -1.6633 -0.0002 9 11 0 0.2335 -0.0013 9 11 1 -1.0077 -0.0002 9 11 2 0.4909 0.0004 9 11 3 0.9660 -0.0007 9 11 4 0.8075 -0.0007 9 11 5 0.5563 0.0007 9 11 6 0.1577 0.0014 9 11 7 -0.6697 -0.0001 9 11 8 1.4890 0.0003 9 11 9 1.6714 -0.0010 9 11 10 -0.1491 -0.0004 9 12 0 -1.0582 -0.0010 9 12 1 -0.9312 -0.0005 9 12 2 -0.4835 -0.0009 9 12 3 -1.2001 -0.0002 9 12 4 2.0698 0.0007 9 12 5 0.2455 0.0007 9 12 6 -2.3781 -0.0011 9 12 7 0.7024 -0.0012 9 12 8 -2.3039 -0.0001 9 12 9 -0.3961 0.0002 9 12 10 5.0437 -0.0011 9 13 0 0.1387 0.0001 9 13 1 1.3176 -0.0009 9 13 2 -1.0880 -0.0001 9 13 3 -0.4989 -0.0009 9 13 4 1.0853 -0.0003 9 13 5 -1.6224 0.0008 9 13 6 -0.0956 0.0012 9 13 7 -2.2390 -0.0004 9 13 8 -3.8558 -0.0008 9 14 0 1.0214 -0.0017 9 14 1 1.0398 0.0002 9 14 2 -1.3421 0.0014 9 14 3 1.4830 0.0006 9 14 4 2.0084 0.0000 9 14 5 -0.7287 0.0005 9 14 6 0.3953 -0.0006 9 14 7 -2.9892 -0.0004 9 14 8 -2.1302 0.0007 9 15 0 0.4309 -0.0007 9 15 1 -0.1478 0.0006 9 15 2 0.6206 -0.0000 9 15 3 1.1924 0.0006 9 15 4 0.0222 0.0022 9 15 5 3.2924 0.0012 9 15 6 0.3599 0.0007 9 15 7 -0.1027 -0.0014 9 16 0 -0.4223 0.0000 9 16 1 1.2433 0.0017 9 16 2 -1.1975 0.0008 9 16 3 -0.7897 0.0003 9 16 4 3.6846 0.0000 9 16 5 0.2313 0.0013 9 17 0 1.1053 -0.0005 9 17 1 -0.9596 -0.0003 9 17 2 -2.1269 0.0009 10 0 0 -0.7782 -0.0019 10 0 2 -1.2463 0.0089 10 0 4 0.4094 0.0008 10 0 6 1.5398 -0.0025 10 0 8 2.5659 -0.0017 10 0 10 -3.5895 -0.0002 10 0 12 -6.1449 0.0023 10 0 14 -1.4818 0.0004 10 1 0 0.7344 -0.0056 10 1 1 -1.4544 -0.0094 10 1 2 -0.4865 0.0005 10 1 3 -0.1614 -0.0017 10 1 4 0.0452 0.0002 10 1 5 0.2049 -0.0015 10 1 6 -0.2991 -0.0002 10 1 7 1.3827 0.0039 10 1 8 0.5448 0.0018 10 1 9 1.0252 -0.0000 10 1 10 0.1848 0.0002 10 1 11 -4.9100 -0.0015 10 1 12 -3.3639 0.0001 10 1 13 -4.6736 -0.0015 10 1 14 -2.0697 -0.0005 10 2 0 0.3020 0.0004 10 2 1 0.0719 0.0057 10 2 2 -0.6722 0.0048 10 2 3 0.2375 -0.0018 10 2 4 -0.4537 0.0018 10 2 5 -0.2681 -0.0018 10 2 6 -0.0839 -0.0041 10 2 7 -0.4201 -0.0006 10 2 8 0.7461 -0.0020 10 2 9 1.3127 0.0008 10 2 10 -0.6516 0.0009 10 2 11 -2.1081 0.0017 10 2 12 -1.9772 0.0013 10 2 13 -3.8715 0.0006 10 2 14 0.0207 0.0013 10 3 0 0.2351 -0.0102 10 3 1 -0.4184 -0.0054 10 3 2 -0.6918 -0.0007 10 3 3 0.3232 0.0015 10 3 4 1.1020 0.0022 10 3 5 0.2566 -0.0019 10 3 6 0.1951 0.0023 10 3 7 -0.8455 0.0031 10 3 8 -0.3555 -0.0017 10 3 9 1.6988 -0.0004 10 3 10 -0.8133 -0.0003 10 3 11 1.0832 -0.0017 10 3 12 -2.2290 -0.0007 10 3 13 -0.8794 -0.0004 10 3 14 2.8438 0.0014 10 4 0 0.5052 0.0033 10 4 1 -0.7931 0.0037 10 4 2 0.0179 -0.0014 10 4 3 0.6435 -0.0025 10 4 4 -0.1559 -0.0000 10 4 5 0.7824 -0.0030 10 4 6 1.1269 -0.0005 10 4 7 -0.4407 -0.0001 10 4 8 1.1818 -0.0000 10 4 9 -0.8909 0.0015 10 4 10 1.3534 0.0007 10 4 11 -0.3694 0.0023 10 4 12 -0.3579 0.0006 10 4 13 2.4129 -0.0019 10 5 0 -0.6047 -0.0083 10 5 1 -0.7135 -0.0002 10 5 2 0.2249 0.0015 10 5 3 0.8300 0.0029 10 5 4 0.7669 0.0006 10 5 5 1.4131 -0.0019 10 5 6 -0.0091 0.0025 10 5 7 -0.4485 0.0015 10 5 8 -1.6559 -0.0009 10 5 9 0.5295 -0.0008 10 5 10 -0.3294 -0.0014 10 5 11 -0.1518 -0.0003 10 5 12 0.2036 -0.0009 10 5 13 2.0194 0.0001 10 6 0 -0.6261 0.0023 10 6 1 -0.2728 -0.0007 10 6 2 0.4181 -0.0046 10 6 3 -0.3403 0.0008 10 6 4 0.1579 0.0002 10 6 5 0.4346 -0.0025 10 6 6 0.8394 -0.0005 10 6 7 0.1934 0.0004 10 6 8 -1.1189 0.0015 10 6 9 -1.7973 0.0010 10 6 10 -2.0116 0.0005 10 6 11 -1.3041 0.0010 10 6 12 -0.4203 -0.0009 10 7 0 0.3426 0.0006 10 7 1 0.0979 0.0014 10 7 2 -0.3334 0.0017 10 7 3 1.1040 0.0026 10 7 4 -0.0729 -0.0006 10 7 5 -0.5482 -0.0003 10 7 6 0.8813 0.0014 10 7 7 -1.0886 -0.0008 10 7 8 -0.8804 -0.0012 10 7 9 -0.8277 -0.0015 10 7 10 -0.4744 -0.0004 10 7 11 -1.8017 0.0004 10 7 12 -0.1932 0.0001 10 8 0 0.0342 -0.0017 10 8 1 -0.7014 -0.0032 10 8 2 1.1848 -0.0005 10 8 3 0.2058 0.0017 10 8 4 -0.5741 -0.0006 10 8 5 0.5773 -0.0011 10 8 6 1.5488 0.0006 10 8 7 1.2448 0.0009 10 8 8 0.2358 0.0013 10 8 9 0.0552 0.0002 10 8 10 -3.2042 0.0008 10 8 11 1.2087 -0.0002 10 8 12 -0.8172 -0.0008 10 9 0 0.3798 0.0016 10 9 1 0.6902 0.0010 10 9 2 0.6635 -0.0006 10 9 3 1.0443 0.0003 10 9 4 -0.4441 0.0003 10 9 5 0.5234 0.0009 10 9 6 0.9633 -0.0015 10 9 7 1.4537 -0.0004 10 9 8 2.8785 -0.0002 10 9 9 0.4622 -0.0011 10 9 10 1.5465 -0.0000 10 9 11 -3.0845 0.0021 10 10 0 -0.0657 -0.0018 10 10 1 1.1421 -0.0018 10 10 2 1.6273 0.0006 10 10 3 1.3808 0.0011 10 10 4 1.3064 -0.0008 10 10 5 -0.8890 -0.0016 10 10 6 1.3582 0.0008 10 10 7 2.1120 0.0018 10 10 8 1.2839 -0.0010 10 10 9 2.9377 -0.0012 10 10 10 -3.0543 0.0009 10 11 0 0.0469 0.0001 10 11 1 -1.0400 -0.0015 10 11 2 -0.1159 -0.0008 10 11 3 3.3941 0.0003 10 11 4 -0.8645 0.0015 10 11 5 0.5856 -0.0004 10 11 6 1.2285 -0.0016 10 11 7 -2.5894 -0.0009 10 11 8 3.6687 0.0002 10 11 9 1.7700 -0.0011 10 11 10 -1.2656 -0.0008 10 12 0 -0.5410 -0.0009 10 12 1 -2.1084 0.0009 10 12 2 1.1201 -0.0006 10 12 3 -0.0702 0.0001 10 12 4 -0.3718 -0.0005 10 12 5 1.5156 0.0005 10 12 6 -3.0769 0.0012 10 12 7 0.1710 0.0014 10 12 8 0.5754 -0.0019 10 12 9 -1.4646 -0.0004 10 13 0 -0.8628 0.0004 10 13 1 -2.1364 -0.0004 10 13 2 -0.9512 0.0003 10 13 3 -0.4261 0.0016 10 13 4 -0.0549 0.0012 10 13 5 -0.7134 -0.0010 10 13 6 -0.2985 -0.0006 10 13 7 -2.9160 0.0018 10 13 8 -1.0944 0.0011 10 14 0 1.0291 0.0007 10 14 1 0.1809 -0.0005 10 14 2 -0.6121 0.0001 10 14 3 -0.5210 0.0012 10 14 4 -0.7202 0.0016 10 14 5 -0.0748 0.0005 10 14 6 -2.1311 0.0009 10 15 0 1.5496 0.0012 10 15 1 -1.7752 0.0013 10 15 2 1.3513 0.0007 10 15 3 1.8276 0.0013 10 15 4 -0.9553 0.0010 10 15 5 1.2543 0.0001 10 16 0 -1.1981 0.0002 10 16 1 -0.4753 0.0003 10 16 2 1.6408 0.0012 10 16 3 -1.8420 0.0009 11 0 0 -0.8567 -0.0038 11 0 2 0.7290 -0.0052 11 0 4 0.3615 -0.0011 11 0 6 0.2702 0.0038 11 0 8 1.2242 0.0013 11 0 10 -3.1001 -0.0006 11 0 12 -5.4480 -0.0012 11 1 0 0.0561 0.0036 11 1 1 0.7094 0.0128 11 1 2 0.1318 0.0000 11 1 3 -0.1739 -0.0012 11 1 4 -0.0962 -0.0005 11 1 5 -0.1927 -0.0007 11 1 6 -0.8587 0.0003 11 1 7 0.9355 -0.0040 11 1 8 0.6155 0.0007 11 1 9 -0.3504 0.0011 11 1 10 -0.9095 -0.0008 11 1 11 -3.4241 0.0016 11 1 12 -2.5139 0.0012 11 2 0 -0.5474 -0.0053 11 2 1 0.0772 -0.0031 11 2 2 -0.0312 -0.0031 11 2 3 0.5486 0.0032 11 2 4 0.0877 -0.0010 11 2 5 -0.0378 0.0007 11 2 6 -1.1427 0.0020 11 2 7 -0.0869 0.0006 11 2 8 1.2911 0.0017 11 2 9 -0.6237 -0.0001 11 2 10 1.8992 -0.0014 11 2 11 -3.2240 -0.0004 11 2 12 -0.8301 -0.0021 11 3 0 0.3490 0.0102 11 3 1 0.7971 0.0062 11 3 2 0.8640 -0.0034 11 3 3 -0.7153 -0.0025 11 3 4 1.0492 -0.0021 11 3 5 -0.5371 0.0011 11 3 6 -0.6013 -0.0010 11 3 7 0.9467 -0.0032 11 3 8 -0.5366 0.0015 11 3 9 3.2368 0.0009 11 3 10 -1.7371 0.0017 11 3 11 0.8182 0.0003 11 3 12 1.0000 0.0004 11 4 0 -0.5047 -0.0039 11 4 1 0.5727 -0.0020 11 4 2 0.0470 0.0029 11 4 3 0.9316 0.0027 11 4 4 1.1893 -0.0012 11 4 5 0.4554 0.0023 11 4 6 -0.2227 0.0017 11 4 7 -1.3735 -0.0004 11 4 8 1.7877 0.0004 11 4 9 -1.3724 -0.0010 11 4 10 2.0047 -0.0016 11 4 11 0.2948 -0.0011 11 4 12 0.1883 -0.0013 11 5 0 -0.0940 0.0062 11 5 1 0.6111 -0.0012 11 5 2 -0.2394 -0.0028 11 5 3 -0.5717 -0.0025 11 5 4 0.0020 -0.0014 11 5 5 0.2306 0.0024 11 5 6 -0.7928 -0.0016 11 5 7 1.0772 -0.0002 11 5 8 -1.1790 0.0017 11 5 9 0.3524 0.0004 11 5 10 -1.0957 0.0016 11 5 11 -1.0124 -0.0001 11 5 12 1.1789 -0.0008 11 6 0 0.1056 -0.0012 11 6 1 1.1235 0.0031 11 6 2 0.1464 0.0046 11 6 3 -0.3969 -0.0006 11 6 4 0.1436 -0.0006 11 6 5 -0.3274 0.0018 11 6 6 -1.3284 -0.0000 11 6 7 -1.3289 -0.0008 11 6 8 -0.7606 -0.0011 11 6 9 -0.7695 -0.0008 11 6 10 -0.2718 -0.0003 11 6 11 -0.7338 -0.0013 11 7 0 0.6929 0.0004 11 7 1 1.2133 -0.0026 11 7 2 0.3385 -0.0015 11 7 3 -0.6731 -0.0014 11 7 4 0.5274 0.0007 11 7 5 -0.2726 0.0003 11 7 6 0.8853 -0.0013 11 7 7 0.1057 0.0010 11 7 8 -0.0905 0.0009 11 7 9 -2.0530 0.0006 11 7 10 -1.0108 0.0001 11 7 11 0.3175 0.0003 11 8 0 1.0581 0.0017 11 8 1 1.6306 0.0026 11 8 2 0.2321 0.0008 11 8 3 0.3627 -0.0017 11 8 4 0.1818 -0.0003 11 8 5 1.1748 0.0006 11 8 6 0.5009 0.0005 11 8 7 2.0010 -0.0018 11 8 8 -0.3424 -0.0020 11 8 9 0.8387 0.0006 11 8 10 -1.4462 0.0010 11 9 0 0.1539 -0.0030 11 9 1 0.7514 -0.0004 11 9 2 1.2674 0.0008 11 9 3 0.2943 -0.0010 11 9 4 -0.4752 -0.0013 11 9 5 1.6301 0.0008 11 9 6 1.8221 0.0004 11 9 7 2.2859 0.0005 11 9 8 3.2179 0.0004 11 9 9 -5.0764 0.0005 11 9 10 2.1614 -0.0017 11 10 0 0.0569 0.0011 11 10 1 0.9967 0.0000 11 10 2 0.9710 -0.0013 11 10 3 -2.3185 -0.0004 11 10 4 2.0770 0.0009 11 10 5 -1.1957 -0.0006 11 10 6 -0.6300 -0.0004 11 10 7 5.2828 -0.0012 11 10 8 -1.9332 -0.0005 11 10 9 2.4193 0.0003 11 11 0 -0.7642 -0.0003 11 11 1 1.4363 0.0004 11 11 2 -0.9885 0.0013 11 11 3 2.2662 -0.0015 11 11 4 -0.9523 -0.0015 11 11 5 -2.2893 0.0014 11 11 6 1.6195 0.0019 11 11 7 -1.1158 -0.0005 11 12 0 -1.1946 -0.0005 11 12 1 -1.9748 -0.0001 11 12 2 0.2214 -0.0001 11 12 3 -1.2362 0.0013 11 12 4 1.1251 -0.0003 11 12 5 0.8489 -0.0003 11 12 6 -3.6344 0.0004 11 12 7 2.3810 0.0005 11 13 0 -1.4295 0.0004 11 13 1 -0.4486 0.0004 11 13 2 -2.5057 0.0013 11 13 3 -0.6549 -0.0011 11 13 4 1.1196 -0.0007 11 13 5 -2.6288 0.0025 11 13 6 1.6981 0.0015 11 14 0 -1.1424 -0.0005 11 14 1 -0.3012 0.0002 11 14 2 -2.1892 0.0014 11 14 3 -1.8567 0.0006 11 14 4 0.1827 -0.0006 11 15 0 1.9757 -0.0016 11 15 1 0.5654 -0.0005 11 15 3 1.0159 -0.0001 11 16 0 -0.3650 0.0008 12 0 0 1.6205 0.0128 12 0 2 0.5552 0.0030 12 0 4 -1.0264 -0.0010 12 0 6 -0.5955 -0.0015 12 0 8 -0.0901 -0.0012 12 0 10 -1.6838 0.0021 12 1 0 -0.3963 -0.0042 12 1 1 -0.2408 -0.0130 12 1 2 0.1173 0.0026 12 1 3 0.5877 0.0018 12 1 4 -0.7246 -0.0005 12 1 5 -1.2318 0.0013 12 1 6 0.0131 0.0010 12 1 7 -0.6352 0.0035 12 1 8 -0.1477 0.0000 12 1 9 1.7026 -0.0006 12 1 10 -0.6081 -0.0008 12 1 11 -0.4045 -0.0017 12 2 0 0.6060 0.0100 12 2 1 0.2836 0.0016 12 2 2 -0.0810 0.0008 12 2 3 -0.0846 -0.0037 12 2 4 -0.9505 -0.0003 12 2 5 -0.4631 0.0001 12 2 6 -0.5372 -0.0029 12 2 7 -0.5628 0.0012 12 2 8 2.3122 -0.0004 12 2 9 -1.4689 -0.0007 12 2 10 2.4999 0.0014 12 2 11 1.1741 0.0010 12 3 0 0.6522 -0.0098 12 3 1 -0.8471 -0.0059 12 3 2 0.5244 0.0050 12 3 3 0.7979 0.0023 12 3 4 -0.0341 0.0021 12 3 5 -0.3802 -0.0008 12 3 6 0.4027 0.0010 12 3 7 0.7732 0.0028 12 3 8 -2.7088 -0.0018 12 3 9 3.5721 -0.0011 12 3 10 -0.5858 -0.0005 12 3 11 1.2691 -0.0021 12 4 0 0.7299 0.0050 12 4 1 -0.2288 -0.0002 12 4 2 -0.1219 -0.0035 12 4 3 -0.1583 -0.0038 12 4 4 -1.0292 0.0019 12 4 5 0.2140 -0.0012 12 4 6 1.3808 -0.0006 12 4 7 -1.0819 0.0009 12 4 8 2.7030 -0.0007 12 4 9 -2.0000 0.0019 12 4 10 -0.6445 -0.0002 12 5 0 0.3051 -0.0046 12 5 1 -0.3459 0.0025 12 5 2 -0.0059 0.0038 12 5 3 -0.2096 0.0028 12 5 4 -1.0993 0.0008 12 5 5 -0.0024 -0.0014 12 5 6 -0.3183 0.0009 12 5 7 0.5497 0.0001 12 5 8 -1.2325 -0.0017 12 5 9 0.7352 -0.0017 12 5 10 0.7395 -0.0011 12 6 0 0.7326 -0.0002 12 6 1 -0.4716 -0.0035 12 6 2 -0.8729 -0.0034 12 6 3 -1.0082 -0.0001 12 6 4 -1.5419 0.0014 12 6 5 -0.1973 -0.0018 12 6 6 0.2778 0.0006 12 6 7 0.2407 0.0006 12 6 8 0.8527 0.0001 12 6 9 -0.4331 0.0005 12 6 10 1.5792 0.0009 12 7 0 2.5043 0.0008 12 7 1 -0.1730 0.0028 12 7 2 0.6498 0.0003 12 7 3 -1.1224 0.0002 12 7 4 -0.2036 0.0001 12 7 5 -0.6991 -0.0001 12 7 6 1.0097 -0.0008 12 7 7 -1.0018 -0.0015 12 7 8 -1.1705 -0.0010 12 7 9 3.0185 -0.0000 12 8 0 -0.2468 -0.0020 12 8 1 1.3253 -0.0026 12 8 2 -0.7054 -0.0021 12 8 3 0.3696 0.0014 12 8 4 -0.5957 0.0002 12 8 5 2.0399 -0.0017 12 8 6 1.4706 0.0011 12 8 7 0.2367 0.0014 12 8 8 -1.7446 0.0004 12 8 9 0.0226 -0.0018 12 9 0 1.8516 0.0022 12 9 1 -1.2430 -0.0003 12 9 2 -0.5989 -0.0006 12 9 3 -0.0444 -0.0001 12 9 4 -1.2533 0.0003 12 9 5 1.2233 0.0010 12 9 6 3.6317 -0.0012 12 9 7 -2.4044 -0.0017 12 9 8 0.7043 0.0006 12 10 0 -1.6370 -0.0003 12 10 1 -0.8411 0.0009 12 10 2 1.5328 -0.0001 12 10 3 -2.3901 0.0001 12 10 4 -0.6718 0.0003 12 10 5 1.6547 0.0001 12 10 6 -0.3186 0.0010 12 10 7 3.8122 0.0025 12 11 0 -0.6201 -0.0000 12 11 1 -0.5176 -0.0014 12 11 2 -2.7438 -0.0003 12 11 3 2.0633 0.0001 12 11 4 -1.0357 0.0010 12 11 5 -1.9386 0.0002 12 12 0 -0.6308 0.0014 12 12 1 -2.9961 0.0015 12 12 2 2.6455 -0.0024 12 12 3 0.2571 -0.0016 12 12 4 -1.6741 0.0009 12 12 5 4.4520 -0.0002 12 13 0 -1.9983 -0.0006 12 13 1 -2.2811 -0.0004 12 13 2 -2.1076 0.0000 12 13 3 0.8511 -0.0004 12 13 4 2.4218 -0.0012 12 14 0 -0.9219 -0.0002 12 14 1 -3.9507 -0.0004 12 14 2 0.3234 -0.0024 12 15 0 -1.4520 -0.0011 13 0 0 -1.0497 -0.0129 13 0 2 -0.5219 -0.0031 13 0 4 -0.3402 0.0038 13 0 6 -2.7012 0.0026 13 0 8 2.2616 0.0003 13 1 0 0.2416 0.0046 13 1 1 0.2795 0.0121 13 1 2 -0.5901 -0.0023 13 1 3 -0.7563 -0.0026 13 1 4 -0.0143 -0.0004 13 1 5 -1.6819 -0.0010 13 1 6 0.0467 0.0009 13 1 7 0.0908 -0.0034 13 1 8 0.2730 -0.0017 13 1 9 3.4501 0.0020 13 2 0 -2.3779 -0.0117 13 2 1 -0.4398 0.0007 13 2 2 0.3913 -0.0008 13 2 3 -0.8636 0.0035 13 2 4 0.4862 0.0017 13 2 5 1.0927 0.0011 13 2 6 -2.1325 0.0022 13 2 7 -1.5577 -0.0018 13 2 8 2.9186 0.0010 13 2 9 0.3522 -0.0009 13 3 0 0.0551 0.0092 13 3 1 0.4729 0.0044 13 3 2 -2.2994 -0.0064 13 3 3 -0.6644 -0.0021 13 3 4 1.6256 -0.0012 13 3 5 -0.4767 0.0006 13 3 6 -0.9856 0.0005 13 3 7 1.3366 -0.0016 13 3 8 -3.8464 0.0007 13 3 9 1.6176 0.0005 13 4 0 -0.0586 -0.0043 13 4 1 -0.6255 0.0019 13 4 2 -0.6036 0.0037 13 4 3 -0.7281 0.0036 13 4 4 0.4857 -0.0010 13 4 5 1.1898 0.0016 13 4 6 0.7461 0.0006 13 4 7 -2.6544 -0.0020 13 4 8 -0.2601 -0.0005 13 4 9 -1.2523 -0.0004 13 5 0 -0.1677 0.0043 13 5 1 -0.0440 -0.0017 13 5 2 -2.1340 -0.0046 13 5 3 -1.5777 -0.0014 13 5 4 0.1831 -0.0009 13 5 5 0.3581 0.0013 13 5 6 0.6867 -0.0007 13 5 7 2.1416 -0.0013 13 5 8 -0.1768 0.0020 13 6 0 0.1034 0.0014 13 6 1 0.3636 0.0024 13 6 2 -1.1931 0.0037 13 6 3 -1.5671 0.0008 13 6 4 -0.1995 -0.0013 13 6 5 0.4185 0.0007 13 6 6 -0.5402 -0.0014 13 6 7 0.3090 -0.0018 13 6 8 3.6644 -0.0017 13 7 0 0.4230 -0.0024 13 7 1 -1.2724 -0.0033 13 7 2 -1.7650 -0.0002 13 7 3 -0.6575 -0.0003 13 7 4 1.2928 -0.0007 13 7 5 -1.2127 0.0013 13 7 6 -0.8641 -0.0002 13 7 7 2.1891 0.0005 13 8 0 -0.4234 0.0017 13 8 1 0.2492 0.0015 13 8 2 -1.6836 0.0004 13 8 3 -0.3289 -0.0004 13 8 4 0.5172 0.0010 13 8 5 1.2028 -0.0000 13 8 6 -1.6081 -0.0012 13 8 7 -4.1778 -0.0012 13 9 0 -0.0144 -0.0008 13 9 1 -0.5915 0.0000 13 9 2 -1.2200 0.0022 13 9 3 0.3553 0.0000 13 9 4 2.6844 -0.0009 13 9 5 0.6944 0.0003 13 9 6 -0.4296 0.0029 13 10 0 -1.2986 0.0005 13 10 1 -1.2363 0.0001 13 10 2 0.8493 -0.0005 13 10 3 -0.5645 0.0017 13 10 4 1.9205 0.0005 13 11 0 -2.4574 0.0002 13 11 1 2.6051 -0.0004 13 11 2 -0.7735 0.0009 13 11 3 2.1628 -0.0009 13 11 4 5.6981 -0.0019 13 12 0 -0.9544 -0.0014 13 12 1 -2.9257 -0.0017 13 12 2 1.8952 -0.0008 13 12 3 4.1528 -0.0008 13 13 0 -4.1384 -0.0000 13 13 1 1.0442 -0.0015 14 0 0 -0.6084 0.0139 14 0 2 0.0585 0.0024 14 0 4 -0.7640 -0.0021 14 0 6 0.1598 -0.0033 14 0 8 4.3153 0.0005 14 1 0 0.6177 -0.0035 14 1 1 -1.6668 -0.0126 14 1 2 -0.0180 0.0018 14 1 3 2.0677 0.0042 14 1 4 0.7857 0.0003 14 1 5 -2.2013 0.0006 14 1 6 0.5278 -0.0007 14 1 7 1.7709 0.0019 14 2 0 -0.7568 0.0105 14 2 1 -1.7956 -0.0012 14 2 2 1.2294 0.0008 14 2 3 1.2189 -0.0038 14 2 4 -1.4928 -0.0016 14 2 5 0.7584 0.0003 14 2 6 -1.2665 -0.0027 14 2 7 -2.5698 0.0001 14 3 0 -2.4575 -0.0072 14 3 1 -0.8014 -0.0042 14 3 2 -0.4441 0.0057 14 3 3 0.7074 0.0032 14 3 4 1.8815 0.0030 14 3 5 -0.9547 0.0001 14 3 6 -3.4337 -0.0015 14 3 7 -1.7937 0.0022 14 4 0 0.8659 0.0036 14 4 1 -2.9127 -0.0034 14 4 2 -1.5045 -0.0027 14 4 3 0.5718 -0.0033 14 4 4 -0.4142 0.0006 14 4 5 0.5482 -0.0010 14 4 6 0.4450 -0.0000 14 4 7 -4.5404 0.0019 14 5 0 0.2423 -0.0040 14 5 1 -0.5055 0.0024 14 5 2 -0.4208 0.0040 14 5 3 -0.3342 0.0004 14 5 4 -0.4248 0.0014 14 5 5 1.1314 -0.0019 14 5 6 1.2462 -0.0011 14 6 0 -0.3359 -0.0016 14 6 1 -1.8784 -0.0022 14 6 2 1.3154 -0.0031 14 6 3 -0.9816 -0.0005 14 6 4 -1.7614 0.0006 14 6 5 1.3448 -0.0015 14 6 6 1.9371 -0.0002 14 7 0 -1.3890 0.0010 14 7 1 1.0085 0.0028 14 7 2 -0.3177 0.0012 14 7 3 0.3074 0.0009 14 7 4 -0.0970 0.0006 14 7 5 -1.9299 -0.0005 14 8 0 -1.2947 -0.0010 14 8 1 -2.5052 0.0004 14 8 2 2.3241 0.0002 14 8 3 2.9426 0.0002 14 8 4 -0.5996 0.0003 14 8 5 -2.8379 0.0005 14 9 0 -0.5737 0.0014 14 9 1 1.3291 0.0005 14 9 2 1.9930 0.0002 14 9 3 3.0187 -0.0001 14 9 4 2.2461 0.0007 14 10 0 0.6078 0.0006 14 10 1 0.6454 0.0028 14 10 2 6.0339 -0.0004 14 10 3 6.0389 -0.0013 14 11 0 -2.6446 -0.0014 14 11 1 3.8413 -0.0012 14 12 0 -0.1861 0.0009 15 0 0 -2.5021 -0.0139 15 0 2 2.5238 -0.0015 15 0 4 2.7740 0.0023 15 1 0 1.9990 0.0031 15 1 1 1.9608 0.0098 15 1 2 -0.0042 -0.0030 15 1 3 1.0201 -0.0039 15 1 4 1.1735 -0.0011 15 1 5 0.5788 -0.0029 15 2 0 -1.0012 -0.0109 15 2 1 0.6545 0.0013 15 2 2 1.3664 0.0000 15 2 3 1.7807 0.0037 15 2 4 -0.4790 0.0011 15 2 5 -1.7533 0.0003 15 3 0 -0.9082 0.0059 15 3 1 -0.3042 0.0044 15 3 2 0.2653 -0.0050 15 3 3 -1.3331 -0.0022 15 3 4 0.7897 -0.0018 15 3 5 -1.7809 0.0006 15 4 0 -1.1843 -0.0027 15 4 1 0.5948 0.0022 15 4 2 -2.3954 0.0022 15 4 3 -0.1577 0.0040 15 4 4 2.0041 -0.0000 15 4 5 -2.4382 -0.0002 15 5 0 2.2942 0.0019 15 5 1 -0.0836 -0.0027 15 5 2 -3.2135 -0.0033 15 5 3 -0.4613 -0.0015 15 5 4 1.0892 -0.0026 15 6 0 3.8530 0.0016 15 6 1 1.2136 0.0021 15 6 2 1.3684 0.0015 15 6 3 -1.7950 0.0013 15 6 4 -1.4850 -0.0004 15 7 0 -1.4982 0.0001 15 7 1 5.8644 -0.0012 15 7 2 0.5516 0.0004 15 7 3 -1.0088 -0.0001 15 8 0 4.5437 0.0027 15 8 1 2.5543 0.0003 15 8 2 3.4829 0.0000 15 9 0 0.2247 0.0002 15 9 1 6.6378 0.0003 15 10 0 6.0131 0.0001 16 0 0 0.4116 0.0113 16 0 2 4.0918 0.0008 16 1 0 1.4052 -0.0032 16 1 1 0.2558 -0.0093 16 1 2 -0.2292 0.0009 16 1 3 4.8445 0.0029 16 2 0 1.2496 0.0082 16 2 1 -0.0654 -0.0011 16 2 2 -0.0455 -0.0002 16 2 3 -0.2753 -0.0030 16 3 0 1.5434 -0.0039 16 3 1 -3.6831 -0.0031 16 3 2 1.4261 0.0045 16 4 0 -3.5465 0.0018 16 4 1 -1.5255 -0.0016 16 4 2 -1.2955 -0.0019 16 5 0 3.3293 -0.0023 16 5 1 -1.3426 0.0011 16 5 2 -3.2782 0.0025 16 6 0 5.6804 -0.0018 16 6 1 -1.9635 -0.0004 16 7 0 3.4692 0.0007 17 0 0 -3.3580 -0.0090 17 1 0 -0.9063 0.0022 17 2 0 -3.3715 -0.0068 0 0 0 0.0 0.0 ; _shelx_fab_checksum 21429 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S1 S 0.54131(10) 0.18024(7) 0.58132(8) 0.0594(5) Uani 1 1 d . . . . . N2 N 0.5044(3) 0.3566(3) 0.5148(3) 0.0643(12) Uani 1 1 d . . . . . N1 N 0.3480(3) 0.1740(2) 0.6123(3) 0.0668(13) Uani 1 1 d . . . . . O3 O 0.3641(3) 0.3790(3) 0.4182(2) 0.0913(14) Uani 1 1 d . . . . . O2 O 0.3243(4) 0.2844(3) 0.5421(3) 0.1026(16) Uani 1 1 d . . . . . O4 O 0.6310(4) 0.3718(3) 0.6210(3) 0.1025(16) Uani 1 1 d . . . . . O1 O 0.3608(4) 0.0895(3) 0.7040(3) 0.1073(17) Uani 1 1 d . . . . . N3 N 0.8845(4) 0.4187(3) 0.7827(3) 0.102(2) Uani 1 1 d D . . . . C13 C 0.4164(5) 0.3939(3) 0.4777(4) 0.0676(16) Uani 1 1 d . . . . . C14 C 0.4066(5) 0.4546(3) 0.5274(4) 0.0746(17) Uani 1 1 d . . . . . C10 C 0.3307(5) 0.2534(4) 0.5970(4) 0.0770(17) Uani 1 1 d . . . . . C3 C 0.3499(5) 0.1553(4) 0.6806(4) 0.0762(18) Uani 1 1 d . . . . . C2 C 0.3583(4) 0.1181(3) 0.5606(4) 0.0758(18) Uani 1 1 d . . . . . H2A H 0.329448 0.139885 0.512874 0.091 Uiso 1 1 calc R . . . . H2B H 0.323753 0.070481 0.562180 0.091 Uiso 1 1 calc R . . . . C11 C 0.4989(4) 0.2148(3) 0.4899(3) 0.0679(16) Uani 1 1 d . . . . . H11A H 0.516337 0.177160 0.460672 0.082 Uiso 1 1 calc R . . . . H11B H 0.429155 0.218584 0.471779 0.082 Uiso 1 1 calc R . . . . C4 C 0.3345(5) 0.2289(3) 0.7127(4) 0.0741(17) Uani 1 1 d . . . . . C9 C 0.3235(5) 0.2875(4) 0.6631(4) 0.0762(18) Uani 1 1 d . . . . . C19 C 0.4868(5) 0.4521(3) 0.5891(4) 0.0760(18) Uani 1 1 d . . . . . C1 C 0.4633(4) 0.0981(3) 0.5753(4) 0.0711(17) Uani 1 1 d . . . . . H1A H 0.465546 0.063767 0.537536 0.085 Uiso 1 1 calc R . . . . H1B H 0.488517 0.069069 0.619820 0.085 Uiso 1 1 calc R . . . . C12 C 0.5405(5) 0.2934(3) 0.4835(3) 0.0762(18) Uani 1 1 d . . . . . H12A H 0.610064 0.291013 0.506883 0.091 Uiso 1 1 calc R . . . . H12B H 0.525622 0.304681 0.433336 0.091 Uiso 1 1 calc R . . . . C20 C 0.5523(5) 0.3895(4) 0.5798(4) 0.0761(18) Uani 1 1 d . . . . . C15 C 0.3324(6) 0.5067(4) 0.5198(4) 0.098(2) Uani 1 1 d . . . . . H15 H 0.276998 0.507938 0.478561 0.118 Uiso 1 1 calc R . . . . B2 B 0.6580(4) 0.1262(3) 0.5978(4) 0.0575(16) Uani 1 1 d . . . . . B9 B 0.6747(5) 0.0731(4) 0.5271(4) 0.0707(19) Uani 1 1 d . . . . . H9 H 0.615156 0.063669 0.475538 0.085 Uiso 1 1 calc R . . . . B5 B 0.6786(5) 0.0221(4) 0.6071(4) 0.076(2) Uani 1 1 d . . . . . H5 H 0.629763 -0.027696 0.601994 0.092 Uiso 1 1 calc R . . . . C5 C 0.3301(5) 0.2453(5) 0.7787(4) 0.100(2) Uani 1 1 d . . . . . H5A H 0.337200 0.206086 0.812381 0.121 Uiso 1 1 calc R . . . . C18 C 0.4985(7) 0.5030(4) 0.6465(4) 0.109(3) Uani 1 1 d . . . . . H18 H 0.553673 0.502123 0.687845 0.130 Uiso 1 1 calc R . . . . C16 C 0.3447(8) 0.5571(5) 0.5768(6) 0.120(3) Uani 1 1 d . . . . . H16 H 0.297366 0.594149 0.572824 0.143 Uiso 1 1 calc R . . . . C17 C 0.4245(9) 0.5538(5) 0.6384(6) 0.121(3) Uani 1 1 d . . . . . H17 H 0.428547 0.587190 0.675921 0.145 Uiso 1 1 calc R . . . . C8 C 0.3068(6) 0.3656(4) 0.6771(5) 0.110(3) Uani 1 1 d . . . . . H8 H 0.298945 0.405313 0.643789 0.132 Uiso 1 1 calc R . . . . B6 B 0.7477(5) 0.1592(4) 0.5654(4) 0.071(2) Uani 1 1 d . . . . . H6 H 0.744711 0.218159 0.542699 0.085 Uiso 1 1 calc R . . . . B1 B 0.7039(5) 0.0832(4) 0.6790(4) 0.077(2) Uani 1 1 d . . . . . H1 H 0.678483 0.082139 0.723855 0.092 Uiso 1 1 calc R . . . . C6 C 0.3148(7) 0.3222(6) 0.7926(5) 0.125(3) Uani 1 1 d . . . . . H6A H 0.312613 0.334999 0.836947 0.150 Uiso 1 1 calc R . . . . B7 B 0.8490(5) 0.1020(4) 0.6170(4) 0.074(2) Uani 1 1 d . . . . . H7 H 0.926500 0.115150 0.635370 0.088 Uiso 1 1 calc R . . . . B3 B 0.7786(5) 0.1479(4) 0.6607(4) 0.080(2) Uani 1 1 d . . . . . H3 H 0.808048 0.197032 0.697667 0.095 Uiso 1 1 calc R . . . . B8 B 0.7803(5) 0.0138(5) 0.5810(5) 0.092(3) Uani 1 1 d . . . . . H8A H 0.804607 -0.044280 0.571233 0.110 Uiso 1 1 calc R . . . . B4 B 0.8007(5) 0.0409(5) 0.6711(4) 0.084(2) Uani 1 1 d . . . . . H4 H 0.848000 0.005558 0.716135 0.100 Uiso 1 1 calc R . . . . C7 C 0.3028(7) 0.3793(5) 0.7437(6) 0.127(3) Uani 1 1 d . . . . . H7A H 0.291380 0.430015 0.755347 0.152 Uiso 1 1 calc R . . . . B10 B 0.7871(6) 0.0862(5) 0.5298(5) 0.095(3) Uani 1 1 d . . . . . H10 H 0.812434 0.085503 0.484941 0.115 Uiso 1 1 calc R . . . . C21B C 0.9179(7) 0.5061(5) 0.7757(5) 0.099(3) Uani 0.666 1 d D . P A 2 H21A H 0.914490 0.537492 0.814813 0.118 Uiso 0.666 1 calc R . P A 2 H21B H 0.984317 0.505729 0.778751 0.118 Uiso 0.666 1 calc R . P A 2 C26B C 0.9868(10) 0.4100(7) 0.9163(7) 0.097(3) Uani 0.6666 1 d D . P A 2 H26A H 0.927334 0.414362 0.925077 0.117 Uiso 0.6666 1 calc R . P A 2 H26B H 1.015646 0.461612 0.920813 0.117 Uiso 0.6666 1 calc R . P A 2 C22 C 0.875010 0.573520 0.739539 0.131(3) Uani 0.3333 1 d D . P A 1 H22A H 0.936519 0.566585 0.778556 0.158 Uiso 0.3333 1 calc R . P A 1 H22B H 0.837101 0.602183 0.761540 0.158 Uiso 0.3333 1 calc R . P A 1 C27B C 1.0574(14) 0.3523(11) 0.9706(10) 0.196(3) Uani 0.6666 1 d D . P A 2 H27A H 1.026405 0.301858 0.968143 0.235 Uiso 0.6666 1 calc R . P A 2 H27B H 1.114319 0.344762 0.958976 0.235 Uiso 0.6666 1 calc R . P A 2 C33B C 0.7895(7) 0.4230(7) 0.7896(6) 0.098(3) Uani 0.6667 1 d D . P A 2 H33A H 0.741966 0.443386 0.745761 0.118 Uiso 0.6667 1 calc R . P A 2 H33B H 0.793044 0.458119 0.828366 0.118 Uiso 0.6667 1 calc R . P A 2 C28B C 1.0856(13) 0.3856(9) 1.0449(10) 0.134(5) Uani 0.6666 1 d D . P A 2 H28A H 1.112046 0.437045 1.046114 0.201 Uiso 0.6666 1 calc GR . P A 2 H28B H 1.133040 0.352385 1.078220 0.201 Uiso 0.6666 1 calc GR . P A 2 H28C H 1.029825 0.388588 1.057698 0.201 Uiso 0.6666 1 calc GR . P A 2 C25B C 0.9667(8) 0.3770(6) 0.8415(6) 0.105(3) Uani 0.6666 1 d D . P A 2 H25A H 0.950823 0.321934 0.841217 0.126 Uiso 0.6666 1 calc R . P A 2 H25B H 1.024806 0.381105 0.830905 0.126 Uiso 0.6666 1 calc R . P A 2 C21 C 0.8381(14) 0.4989(8) 0.7463(12) 0.099(3) Uani 0.3333 1 d D . P A 1 H21C H 0.800834 0.484133 0.697245 0.118 Uiso 0.3333 1 calc R . P A 1 H21D H 0.790934 0.510236 0.767598 0.118 Uiso 0.3333 1 calc R . P A 1 C23B C 0.881961 0.628761 0.718850 0.196(3) Uani 0.6667 1 d D . P A 2 H23A H 0.842891 0.649923 0.743867 0.235 Uiso 0.6667 1 calc R . P A 2 H23B H 0.948001 0.628944 0.752784 0.235 Uiso 0.6667 1 calc R . P A 2 C25 C 0.9300(18) 0.4328(12) 0.8645(9) 0.105(3) Uani 0.3333 1 d D . P A 1 H25C H 0.878524 0.450089 0.879416 0.126 Uiso 0.3333 1 calc R . P A 1 H25D H 0.974068 0.476536 0.871882 0.126 Uiso 0.3333 1 calc R . P A 1 C34B C 0.7593(14) 0.3413(10) 0.8047(11) 0.102(4) Uani 0.6667 1 d D . P A 2 H34A H 0.754791 0.305530 0.766140 0.123 Uiso 0.6667 1 calc R . P A 2 H34B H 0.805180 0.320652 0.849112 0.123 Uiso 0.6667 1 calc R . P A 2 C35B C 0.6636(15) 0.3530(12) 0.8098(18) 0.196(3) Uani 0.6667 1 d D . P A 2 H35A H 0.619974 0.371164 0.763432 0.235 Uiso 0.6667 1 calc R . P A 2 H35B H 0.670042 0.395248 0.843449 0.235 Uiso 0.6667 1 calc R . P A 2 C36B C 0.615(2) 0.2862(9) 0.8314(13) 0.184(8) Uani 0.6667 1 d D . P A 2 H36A H 0.658637 0.264322 0.875549 0.277 Uiso 0.6667 1 calc GR . P A 2 H36B H 0.598239 0.246706 0.794844 0.277 Uiso 0.6667 1 calc GR . P A 2 H36C H 0.558247 0.304634 0.837668 0.277 Uiso 0.6667 1 calc GR . P A 2 C33 C 0.8113(15) 0.3523(12) 0.7828(13) 0.098(3) Uani 0.3333 1 d D . P A 1 H33C H 0.772111 0.340812 0.733330 0.118 Uiso 0.3333 1 calc R . P A 1 H33D H 0.848647 0.305552 0.802512 0.118 Uiso 0.3333 1 calc R . P A 1 C34 C 0.743(3) 0.365(2) 0.822(2) 0.102(4) Uani 0.3333 1 d D . P A 1 H34C H 0.777694 0.343802 0.869689 0.123 Uiso 0.3333 1 calc R . P A 1 H34D H 0.743502 0.421446 0.828889 0.123 Uiso 0.3333 1 calc R . P A 1 C35 C 0.639(2) 0.342(2) 0.806(4) 0.196(3) Uani 0.3333 1 d D . P A 1 H35C H 0.616917 0.364029 0.841768 0.235 Uiso 0.3333 1 calc R . P A 1 H35D H 0.598516 0.361993 0.759650 0.235 Uiso 0.3333 1 calc R . P A 1 C36 C 0.631(4) 0.2539(19) 0.807(3) 0.184(8) Uani 0.3333 1 d D . P A 1 H36D H 0.639537 0.232783 0.765015 0.277 Uiso 0.3333 1 calc GR . P A 1 H36E H 0.568575 0.239471 0.805949 0.277 Uiso 0.3333 1 calc GR . P A 1 H36F H 0.679869 0.233336 0.848875 0.277 Uiso 0.3333 1 calc GR . P A 1 C28 C 1.097(3) 0.3371(19) 1.0410(15) 0.134(5) Uani 0.3333 1 d D . P A 1 H28D H 1.136376 0.315562 1.016963 0.201 Uiso 0.3333 1 calc GR . P A 1 H28E H 1.058604 0.296423 1.049797 0.201 Uiso 0.3333 1 calc GR . P A 1 H28F H 1.137899 0.359621 1.085740 0.201 Uiso 0.3333 1 calc GR . P A 1 C27 C 1.032(3) 0.4001(17) 0.9945(16) 0.196(3) Uani 0.3333 1 d D . P A 1 H27C H 1.068844 0.446824 0.994573 0.235 Uiso 0.3333 1 calc R . P A 1 H27D H 0.982052 0.413807 1.012689 0.235 Uiso 0.3333 1 calc R . P A 1 C26 C 0.9859(19) 0.3669(13) 0.9178(13) 0.097(3) Uani 0.3333 1 d D . P A 1 H26C H 0.941852 0.324855 0.917009 0.117 Uiso 0.3333 1 calc R . P A 1 H26D H 1.035866 0.345602 0.902999 0.117 Uiso 0.3333 1 calc R . P A 1 C22B C 0.853001 0.542689 0.703589 0.131(3) Uani 0.6666 1 d D . P A 2 H22C H 0.868109 0.522508 0.663876 0.158 Uiso 0.6666 1 calc R . P A 2 H22D H 0.785113 0.534658 0.694274 0.158 Uiso 0.6666 1 calc R . P A 2 C24 C 0.831910 0.661751 0.631921 0.196(3) Uani 0.3333 1 d D . P A 1 H24A H 0.850764 0.634205 0.597573 0.294 Uiso 0.3333 1 calc GR . P A 1 H24B H 0.832349 0.717047 0.623550 0.294 Uiso 0.3333 1 calc GR . P A 1 H24C H 0.768217 0.645772 0.627254 0.294 Uiso 0.3333 1 calc GR . P A 1 C23 C 0.904180 0.642590 0.709049 0.196(3) Uani 0.3333 1 d D . P A 1 H23C H 0.967593 0.633553 0.707630 0.235 Uiso 0.3333 1 calc R . P A 1 H23D H 0.908618 0.687322 0.739809 0.235 Uiso 0.3333 1 calc R . P A 1 C24B C 0.877390 0.687730 0.661251 0.196(3) Uani 0.6667 1 d D . P A 2 H24D H 0.900175 0.663823 0.627264 0.294 Uiso 0.6667 1 calc GR . P A 2 H24E H 0.917119 0.732015 0.682737 0.294 Uiso 0.6667 1 calc GR . P A 2 H24F H 0.811984 0.704652 0.637318 0.294 Uiso 0.6667 1 calc GR . P A 2 C29B C 0.8772(10) 0.3750(7) 0.7142(7) 0.111(4) Uani 0.6667 1 d D . P A 2 H29A H 0.859525 0.321216 0.718735 0.134 Uiso 0.6667 1 calc R . P A 2 H29B H 0.824686 0.398018 0.674602 0.134 Uiso 0.6667 1 calc R . P A 2 C30B C 0.9654(10) 0.3741(8) 0.6946(7) 0.131(3) Uani 0.6667 1 d D . P A 2 H30A H 0.982352 0.427278 0.686973 0.158 Uiso 0.6667 1 calc R . P A 2 H30B H 1.019208 0.351727 0.733574 0.158 Uiso 0.6667 1 calc R . P A 2 C31B C 0.9471(12) 0.3270(13) 0.6280(8) 0.196(3) Uani 0.6667 1 d D . P A 2 H31A H 0.902011 0.354085 0.586845 0.235 Uiso 0.6667 1 calc R . P A 2 H31B H 0.919976 0.276455 0.632085 0.235 Uiso 0.6667 1 calc R . P A 2 C29 C 0.9569(15) 0.3756(18) 0.7620(11) 0.131(11) Uani 0.3333 1 d D . P A 1 H29C H 0.974643 0.326816 0.788253 0.158 Uiso 0.3333 1 calc R . P A 1 H29D H 1.014538 0.406936 0.771610 0.158 Uiso 0.3333 1 calc R . P A 1 C30 C 0.9085(19) 0.3602(19) 0.6832(12) 0.131(3) Uani 0.3333 1 d D . P A 1 H30C H 0.891317 0.409378 0.657434 0.158 Uiso 0.3333 1 calc R . P A 1 H30D H 0.850050 0.330184 0.674025 0.158 Uiso 0.3333 1 calc R . P A 1 C31 C 0.978(3) 0.315(2) 0.6576(13) 0.196(3) Uani 0.3333 1 d D . P A 1 H31C H 0.977710 0.259417 0.668605 0.235 Uiso 0.3333 1 calc R . P A 1 H31D H 1.042879 0.334818 0.679032 0.235 Uiso 0.3333 1 calc R . P A 1 C32B C 1.0436(12) 0.3162(11) 0.6190(10) 0.196(3) Uani 0.6666 1 d D . P A 2 H32A H 1.081236 0.363062 0.633633 0.294 Uiso 0.6666 1 calc GR . P A 2 H32B H 1.032443 0.305589 0.569671 0.294 Uiso 0.6666 1 calc GR . P A 2 H32C H 1.077775 0.273118 0.647947 0.294 Uiso 0.6666 1 calc GR . P A 2 C32 C 0.934(3) 0.329(2) 0.5733(13) 0.196(3) Uani 0.3333 1 d D . P A 1 H32D H 0.872137 0.353458 0.559997 0.294 Uiso 0.3333 1 calc GR . P A 1 H32E H 0.928470 0.280400 0.548711 0.294 Uiso 0.3333 1 calc GR . P A 1 H32F H 0.976737 0.363351 0.560414 0.294 Uiso 0.3333 1 calc GR . P A 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1 0.0698(9) 0.0366(7) 0.0714(10) -0.0036(7) 0.0257(8) 0.0000(6) N2 0.078(3) 0.047(3) 0.061(3) 0.009(3) 0.017(3) 0.009(2) N1 0.076(3) 0.040(3) 0.088(4) -0.005(3) 0.035(3) 0.003(2) O3 0.098(3) 0.095(3) 0.064(3) 0.005(3) 0.009(3) 0.021(3) O2 0.156(5) 0.068(3) 0.108(4) 0.020(3) 0.077(4) 0.024(3) O4 0.109(4) 0.088(4) 0.083(3) -0.001(3) 0.003(3) -0.006(3) O1 0.142(4) 0.061(3) 0.124(4) 0.025(3) 0.054(4) 0.016(3) N3 0.096(4) 0.096(5) 0.099(5) -0.041(4) 0.018(4) -0.032(4) C13 0.085(4) 0.054(3) 0.060(4) 0.009(3) 0.022(3) 0.004(3) C14 0.107(5) 0.045(3) 0.077(5) 0.005(3) 0.040(4) 0.007(3) C10 0.088(4) 0.056(4) 0.096(5) 0.001(4) 0.043(4) 0.003(3) C3 0.087(4) 0.058(4) 0.084(5) 0.004(4) 0.033(4) -0.001(3) C2 0.078(4) 0.051(3) 0.104(5) -0.021(3) 0.040(4) -0.009(3) C11 0.082(4) 0.053(3) 0.065(4) -0.007(3) 0.023(3) 0.009(3) C4 0.095(5) 0.054(4) 0.073(4) 0.007(3) 0.030(4) 0.003(3) C9 0.086(4) 0.058(4) 0.091(5) -0.012(4) 0.041(4) -0.002(3) C19 0.113(5) 0.041(3) 0.077(5) -0.007(3) 0.038(4) -0.011(3) C1 0.074(4) 0.042(3) 0.098(5) -0.008(3) 0.034(3) -0.005(3) C12 0.099(5) 0.054(3) 0.080(5) 0.006(3) 0.038(4) 0.012(3) C20 0.098(5) 0.052(4) 0.064(5) 0.008(4) 0.013(4) -0.004(4) C15 0.126(6) 0.063(4) 0.112(6) 0.008(4) 0.052(5) 0.030(4) B2 0.062(4) 0.035(3) 0.072(5) -0.001(3) 0.022(3) 0.002(3) B9 0.077(5) 0.057(4) 0.075(5) -0.004(4) 0.024(4) 0.011(3) B5 0.073(4) 0.038(3) 0.112(6) 0.005(4) 0.026(4) -0.001(3) C5 0.125(6) 0.108(6) 0.066(5) -0.004(5) 0.032(4) -0.009(5) C18 0.173(8) 0.056(4) 0.094(6) -0.018(4) 0.046(6) -0.020(5) C16 0.174(9) 0.052(4) 0.162(9) -0.002(6) 0.096(8) 0.018(6) C17 0.208(11) 0.048(4) 0.133(9) -0.017(5) 0.095(8) 0.001(6) C8 0.160(7) 0.054(4) 0.146(8) -0.006(5) 0.091(7) -0.001(4) B6 0.065(4) 0.055(4) 0.090(5) 0.018(4) 0.024(4) 0.002(3) B1 0.088(5) 0.058(4) 0.083(5) 0.010(4) 0.031(4) 0.001(4) C6 0.174(9) 0.114(7) 0.097(7) -0.035(6) 0.062(6) -0.017(7) B7 0.063(4) 0.059(4) 0.096(6) 0.007(4) 0.026(4) 0.000(3) B3 0.082(5) 0.059(4) 0.085(6) -0.015(4) 0.017(4) -0.013(4) B8 0.071(5) 0.081(5) 0.117(7) -0.026(5) 0.026(5) 0.014(4) B4 0.074(5) 0.073(5) 0.086(6) 0.021(5) 0.010(4) 0.005(4) C7 0.192(10) 0.078(6) 0.137(8) -0.031(6) 0.093(8) 0.002(6) B10 0.087(6) 0.103(7) 0.095(6) 0.011(6) 0.032(5) 0.024(5) C21B 0.088(7) 0.093(7) 0.107(8) -0.043(6) 0.027(6) -0.034(6) C26B 0.106(7) 0.063(8) 0.120(8) -0.017(9) 0.039(6) -0.011(8) C22 0.180(9) 0.103(7) 0.106(7) -0.029(5) 0.046(7) -0.062(6) C27B 0.178(6) 0.213(7) 0.177(7) 0.039(6) 0.044(6) -0.049(5) C33B 0.086(7) 0.117(9) 0.101(7) -0.030(7) 0.044(6) -0.007(6) C28B 0.118(9) 0.128(15) 0.167(12) 0.004(13) 0.067(8) 0.013(12) C25B 0.104(8) 0.076(7) 0.135(10) 0.003(7) 0.044(7) -0.011(6) C21 0.088(7) 0.093(7) 0.107(8) -0.043(6) 0.027(6) -0.034(6) C23B 0.178(6) 0.213(7) 0.177(7) 0.039(6) 0.044(6) -0.049(5) C25 0.104(8) 0.076(7) 0.135(10) 0.003(7) 0.044(7) -0.011(6) C34B 0.120(10) 0.093(13) 0.102(13) -0.033(7) 0.049(7) -0.041(9) C35B 0.178(6) 0.213(7) 0.177(7) 0.039(6) 0.044(6) -0.049(5) C36B 0.31(2) 0.081(13) 0.20(2) -0.034(12) 0.140(16) -0.078(16) C33 0.086(7) 0.117(9) 0.101(7) -0.030(7) 0.044(6) -0.007(6) C34 0.120(10) 0.093(13) 0.102(13) -0.033(7) 0.049(7) -0.041(9) C35 0.178(6) 0.213(7) 0.177(7) 0.039(6) 0.044(6) -0.049(5) C36 0.31(2) 0.081(13) 0.20(2) -0.034(12) 0.140(16) -0.078(16) C28 0.118(9) 0.128(15) 0.167(12) 0.004(13) 0.067(8) 0.013(12) C27 0.178(6) 0.213(7) 0.177(7) 0.039(6) 0.044(6) -0.049(5) C26 0.106(7) 0.063(8) 0.120(8) -0.017(9) 0.039(6) -0.011(8) C22B 0.180(9) 0.103(7) 0.106(7) -0.029(5) 0.046(7) -0.062(6) C24 0.178(6) 0.213(7) 0.177(7) 0.039(6) 0.044(6) -0.049(5) C23 0.178(6) 0.213(7) 0.177(7) 0.039(6) 0.044(6) -0.049(5) C24B 0.178(6) 0.213(7) 0.177(7) 0.039(6) 0.044(6) -0.049(5) C29B 0.136(11) 0.092(8) 0.126(12) -0.022(9) 0.073(10) -0.045(8) C30B 0.180(9) 0.103(7) 0.106(7) -0.029(5) 0.046(7) -0.062(6) C31B 0.178(6) 0.213(7) 0.177(7) 0.039(6) 0.044(6) -0.049(5) C29 0.089(17) 0.22(4) 0.081(18) -0.03(2) 0.027(15) 0.00(2) C30 0.180(9) 0.103(7) 0.106(7) -0.029(5) 0.046(7) -0.062(6) C31 0.178(6) 0.213(7) 0.177(7) 0.039(6) 0.044(6) -0.049(5) C32B 0.178(6) 0.213(7) 0.177(7) 0.039(6) 0.044(6) -0.049(5) C32 0.178(6) 0.213(7) 0.177(7) 0.039(6) 0.044(6) -0.049(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C11 S1 B2 107.0(3) . . C1 S1 C11 102.2(3) . . C1 S1 B2 99.4(3) . . C13 N2 C12 122.2(5) . . C20 N2 C13 112.4(5) . . C20 N2 C12 125.3(5) . . C10 N1 C3 111.9(5) . . C10 N1 C2 122.6(5) . . C3 N1 C2 125.4(5) . . C33B N3 C21B 107.7(7) . . C33B N3 C25B 118.2(8) . . C33B N3 C29B 110.8(7) . . C25B N3 C21B 108.4(6) . . C25B N3 C29B 103.9(8) . . C25 N3 C21 107.6(12) . . C25 N3 C33 98.2(13) . . C33 N3 C21 116.0(12) . . C29B N3 C21B 107.3(7) . . C29 N3 C21 122.5(15) . . C29 N3 C25 107.1(13) . . C29 N3 C33 102.7(16) . . N2 C13 C14 105.4(5) . . O3 C13 N2 125.1(6) . . O3 C13 C14 129.5(6) . . C19 C14 C13 108.5(6) . . C19 C14 C15 121.1(6) . . C15 C14 C13 130.4(7) . . N1 C10 C9 104.6(6) . . O2 C10 N1 125.5(6) . . O2 C10 C9 130.0(6) . . N1 C3 C4 106.6(5) . . O1 C3 N1 123.2(6) . . O1 C3 C4 130.2(7) . . N1 C2 H2A 109.1 . . N1 C2 H2B 109.1 . . N1 C2 C1 112.4(5) . . H2A C2 H2B 107.9 . . C1 C2 H2A 109.1 . . C1 C2 H2B 109.1 . . S1 C11 H11A 109.2 . . S1 C11 H11B 109.2 . . H11A C11 H11B 107.9 . . C12 C11 S1 112.2(4) . . C12 C11 H11A 109.2 . . C12 C11 H11B 109.2 . . C9 C4 C3 107.5(6) . . C9 C4 C5 120.8(6) . . C5 C4 C3 131.7(7) . . C4 C9 C10 109.4(5) . . C4 C9 C8 121.9(6) . . C8 C9 C10 128.7(7) . . C14 C19 C20 107.5(6) . . C14 C19 C18 121.8(7) . . C18 C19 C20 130.7(7) . . S1 C1 H1A 108.4 . . S1 C1 H1B 108.4 . . C2 C1 S1 115.6(4) . . C2 C1 H1A 108.4 . . C2 C1 H1B 108.4 . . H1A C1 H1B 107.4 . . N2 C12 C11 113.4(5) . . N2 C12 H12A 108.9 . . N2 C12 H12B 108.9 . . C11 C12 H12A 108.9 . . C11 C12 H12B 108.9 . . H12A C12 H12B 107.7 . . N2 C20 C19 106.2(6) . . O4 C20 N2 126.4(7) . . O4 C20 C19 127.5(7) . . C14 C15 H15 121.7 . . C14 C15 C16 116.7(8) . . C16 C15 H15 121.7 . . B9 B2 S1 120.1(4) . . B9 B2 B5 60.8(4) . . B9 B2 B6 61.6(4) . . B9 B2 B3 105.4(5) . . B5 B2 S1 127.7(4) . . B5 B2 B3 92.4(4) . . B6 B2 S1 123.3(4) . . B6 B2 B5 103.2(4) . . B6 B2 B3 60.3(4) . . B1 B2 S1 113.6(4) . . B1 B2 B9 115.2(5) . . B1 B2 B5 58.5(4) . . B1 B2 B6 113.6(5) . . B1 B2 B3 58.1(4) . . B3 B2 S1 129.4(4) . . B2 B9 H9 121.6 . . B2 B9 B5 60.2(4) . . B2 B9 B6 59.3(4) . . B2 B9 B8 98.6(5) . . B5 B9 H9 121.1 . . B5 B9 B6 101.2(5) . . B5 B9 B8 58.3(4) . . B6 B9 H9 131.7 . . B6 B9 B8 86.9(5) . . B8 B9 H9 133.7 . . B10 B9 B2 109.8(6) . . B10 B9 H9 120.2 . . B10 B9 B5 109.4(6) . . B10 B9 B6 56.1(4) . . B10 B9 B8 55.1(4) . . B2 B5 B9 59.0(4) . . B2 B5 H5 132.2 . . B2 B5 B4 89.3(4) . . B9 B5 H5 119.1 . . B9 B5 B4 103.7(5) . . B1 B5 B2 57.4(4) . . B1 B5 B9 112.5(5) . . B1 B5 H5 118.9 . . B1 B5 B8 110.5(5) . . B1 B5 B4 56.4(4) . . B8 B5 B2 100.2(5) . . B8 B5 B9 61.9(4) . . B8 B5 H5 121.2 . . B8 B5 B4 59.1(4) . . B4 B5 H5 130.9 . . C4 C5 H5A 121.4 . . C6 C5 C4 117.2(8) . . C6 C5 H5A 121.4 . . C19 C18 H18 121.8 . . C17 C18 C19 116.5(8) . . C17 C18 H18 121.8 . . C15 C16 H16 119.1 . . C17 C16 C15 121.9(8) . . C17 C16 H16 119.1 . . C18 C17 H17 119.0 . . C16 C17 C18 122.0(9) . . C16 C17 H17 119.0 . . C9 C8 H8 122.3 . . C7 C8 C9 115.4(8) . . C7 C8 H8 122.3 . . B2 B6 B9 59.2(4) . . B2 B6 H6 121.4 . . B2 B6 B3 60.7(4) . . B9 B6 H6 129.5 . . B7 B6 B2 101.8(5) . . B7 B6 B9 92.9(4) . . B7 B6 H6 129.9 . . B7 B6 B3 59.6(4) . . B3 B6 B9 103.9(5) . . B3 B6 H6 119.6 . . B10 B6 B2 110.8(5) . . B10 B6 B9 57.3(4) . . B10 B6 H6 118.5 . . B10 B6 B7 58.4(4) . . B10 B6 B3 112.7(6) . . B2 B1 B5 64.1(4) . . B2 B1 H1 131.4 . . B2 B1 B3 64.7(4) . . B5 B1 H1 130.5 . . B3 B1 B5 99.8(6) . . B3 B1 H1 129.7 . . B4 B1 B2 98.7(5) . . B4 B1 B5 65.5(5) . . B4 B1 H1 129.9 . . B4 B1 B3 66.6(5) . . C5 C6 H6A 119.1 . . C7 C6 C5 121.9(8) . . C7 C6 H6A 119.1 . . B6 B7 H7 130.3 . . B6 B7 B3 61.1(4) . . B6 B7 B8 89.4(5) . . B6 B7 B4 102.9(5) . . B3 B7 H7 118.9 . . B3 B7 B8 102.2(5) . . B3 B7 B4 61.7(4) . . B8 B7 H7 132.2 . . B8 B7 B4 58.4(4) . . B4 B7 H7 120.7 . . B10 B7 B6 57.1(4) . . B10 B7 H7 119.3 . . B10 B7 B3 113.0(5) . . B10 B7 B8 55.7(5) . . B10 B7 B4 110.1(6) . . B2 B3 H3 132.2 . . B2 B3 B4 88.1(4) . . B6 B3 B2 58.9(4) . . B6 B3 H3 121.1 . . B6 B3 B4 101.0(5) . . B1 B3 B2 57.2(4) . . B1 B3 B6 111.5(5) . . B1 B3 B7 112.0(5) . . B1 B3 H3 118.6 . . B1 B3 B4 56.0(4) . . B7 B3 B2 100.4(5) . . B7 B3 B6 59.3(4) . . B7 B3 H3 120.6 . . B7 B3 B4 60.7(4) . . B4 B3 H3 131.8 . . B9 B8 H8A 130.9 . . B5 B8 B9 59.8(4) . . B5 B8 B7 103.6(5) . . B5 B8 H8A 119.8 . . B7 B8 B9 90.8(5) . . B7 B8 H8A 130.2 . . B4 B8 B9 104.1(5) . . B4 B8 B5 61.7(5) . . B4 B8 B7 61.4(4) . . B4 B8 H8A 118.2 . . B10 B8 B9 57.0(5) . . B10 B8 B5 112.5(6) . . B10 B8 B7 57.8(5) . . B10 B8 H8A 117.9 . . B10 B8 B4 114.7(6) . . B5 B4 B7 100.9(5) . . B5 B4 B3 90.2(5) . . B5 B4 H4 130.7 . . B1 B4 B5 58.1(4) . . B1 B4 B7 110.6(5) . . B1 B4 B3 57.5(4) . . B1 B4 B8 112.2(5) . . B1 B4 H4 118.2 . . B7 B4 B3 57.6(4) . . B7 B4 H4 121.8 . . B3 B4 H4 131.8 . . B8 B4 B5 59.2(4) . . B8 B4 B7 60.2(5) . . B8 B4 B3 100.6(5) . . B8 B4 H4 120.8 . . C8 C7 H7A 118.6 . . C6 C7 C8 122.9(7) . . C6 C7 H7A 118.6 . . B9 B10 B7 102.4(6) . . B9 B10 H10 128.0 . . B6 B10 B9 66.6(5) . . B6 B10 B7 64.6(5) . . B6 B10 H10 130.5 . . B7 B10 H10 129.6 . . B8 B10 B9 67.9(5) . . B8 B10 B6 100.5(6) . . B8 B10 B7 66.5(5) . . B8 B10 H10 129.0 . . N3 C21B H21A 109.5 . . N3 C21B H21B 109.5 . . H21A C21B H21B 108.1 . . C22B C21B N3 110.6(6) . . C22B C21B H21A 109.5 . . C22B C21B H21B 109.5 . . H26A C26B H26B 108.6 . . C27B C26B H26A 110.3 . . C27B C26B H26B 110.3 . . C25B C26B H26A 110.3 . . C25B C26B H26B 110.3 . . C25B C26B C27B 107.0(11) . . H22A C22 H22B 103.3 . . C21 C22 H22A 95.6 . . C21 C22 H22B 95.6 . . C21 C22 C23 161.8(9) . . C23 C22 H22A 95.6 . . C23 C22 H22B 95.6 . . C26B C27B H27A 109.9 . . C26B C27B H27B 109.9 . . H27A C27B H27B 108.3 . . C28B C27B C26B 109.0(16) . . C28B C27B H27A 109.9 . . C28B C27B H27B 109.9 . . N3 C33B H33A 109.7 . . N3 C33B H33B 109.7 . . N3 C33B C34B 109.7(10) . . H33A C33B H33B 108.2 . . C34B C33B H33A 109.7 . . C34B C33B H33B 109.7 . . C27B C28B H28A 109.5 . . C27B C28B H28B 109.5 . . C27B C28B H28C 109.5 . . H28A C28B H28B 109.5 . . H28A C28B H28C 109.5 . . H28B C28B H28C 109.5 . . N3 C25B H25A 108.9 . . N3 C25B H25B 108.9 . . C26B C25B N3 113.6(9) . . C26B C25B H25A 108.9 . . C26B C25B H25B 108.9 . . H25A C25B H25B 107.7 . . N3 C21 H21C 103.5 . . N3 C21 H21D 103.5 . . C22 C21 N3 134.7(14) . . C22 C21 H21C 103.5 . . C22 C21 H21D 103.5 . . H21C C21 H21D 105.3 . . H23A C23B H23B 106.5 . . C22B C23B H23A 106.4 . . C22B C23B H23B 106.4 . . C24B C23B H23A 106.4 . . C24B C23B H23B 106.4 . . C24B C23B C22B 123.680(3) . . N3 C25 H25C 106.8 . . N3 C25 H25D 106.8 . . N3 C25 C26 122.0(17) . . H25C C25 H25D 106.7 . . C26 C25 H25C 106.8 . . C26 C25 H25D 106.8 . . C33B C34B H34A 110.8 . . C33B C34B H34B 110.8 . . H34A C34B H34B 108.9 . . C35B C34B C33B 104.7(13) . . C35B C34B H34A 110.8 . . C35B C34B H34B 110.8 . . C34B C35B H35A 107.4 . . C34B C35B H35B 107.4 . . C34B C35B C36B 119.8(17) . . H35A C35B H35B 106.9 . . C36B C35B H35A 107.4 . . C36B C35B H35B 107.4 . . C35B C36B H36A 109.5 . . C35B C36B H36B 109.5 . . C35B C36B H36C 109.5 . . H36A C36B H36B 109.5 . . H36A C36B H36C 109.5 . . H36B C36B H36C 109.5 . . N3 C33 H33C 107.4 . . N3 C33 H33D 107.4 . . H33C C33 H33D 106.9 . . C34 C33 N3 119.6(18) . . C34 C33 H33C 107.4 . . C34 C33 H33D 107.4 . . C33 C34 H34C 104.1 . . C33 C34 H34D 104.1 . . H34C C34 H34D 105.5 . . C35 C34 C33 133(4) . . C35 C34 H34C 104.1 . . C35 C34 H34D 104.1 . . C34 C35 H35C 109.7 . . C34 C35 H35D 109.7 . . H35C C35 H35D 108.2 . . C36 C35 C34 109.7(19) . . C36 C35 H35C 109.7 . . C36 C35 H35D 109.7 . . C35 C36 H36D 109.5 . . C35 C36 H36E 109.5 . . C35 C36 H36F 109.5 . . H36D C36 H36E 109.5 . . H36D C36 H36F 109.5 . . H36E C36 H36F 109.5 . . H28D C28 H28E 109.5 . . H28D C28 H28F 109.5 . . H28E C28 H28F 109.5 . . C27 C28 H28D 109.5 . . C27 C28 H28E 109.5 . . C27 C28 H28F 109.5 . . C28 C27 H27C 110.2 . . C28 C27 H27D 110.2 . . C28 C27 C26 107.5(16) . . H27C C27 H27D 108.5 . . C26 C27 H27C 110.2 . . C26 C27 H27D 110.2 . . C25 C26 H26C 109.6 . . C25 C26 H26D 109.6 . . C27 C26 C25 110.3(19) . . C27 C26 H26C 109.6 . . C27 C26 H26D 109.6 . . H26C C26 H26D 108.1 . . C21B C22B H22C 111.8 . . C21B C22B H22D 111.8 . . C23B C22B C21B 99.7(3) . . C23B C22B H22C 111.8 . . C23B C22B H22D 111.8 . . H22C C22B H22D 109.6 . . H24A C24 H24B 109.5 . . H24A C24 H24C 109.5 . . H24B C24 H24C 109.5 . . C23 C24 H24A 109.5 . . C23 C24 H24B 109.5 . . C23 C24 H24C 109.5 . . C22 C23 C24 112.366(3) . . C22 C23 H23C 109.1 . . C22 C23 H23D 109.1 . . C24 C23 H23C 109.1 . . C24 C23 H23D 109.1 . . H23C C23 H23D 107.9 . . C23B C24B H24D 109.5 . . C23B C24B H24E 109.5 . . C23B C24B H24F 109.5 . . H24D C24B H24E 109.5 . . H24D C24B H24F 109.5 . . H24E C24B H24F 109.5 . . N3 C29B H29A 108.0 . . N3 C29B H29B 108.0 . . H29A C29B H29B 107.2 . . C30B C29B N3 117.4(10) . . C30B C29B H29A 108.0 . . C30B C29B H29B 108.0 . . C29B C30B H30A 109.5 . . C29B C30B H30B 109.5 . . H30A C30B H30B 108.1 . . C31B C30B C29B 110.5(10) . . C31B C30B H30A 109.5 . . C31B C30B H30B 109.5 . . C30B C31B H31A 110.2 . . C30B C31B H31B 110.2 . . C30B C31B C32B 107.6(12) . . H31A C31B H31B 108.5 . . C32B C31B H31A 110.2 . . C32B C31B H31B 110.2 . . N3 C29 H29C 110.7 . . N3 C29 H29D 110.7 . . N3 C29 C30 105.4(16) . . H29C C29 H29D 108.8 . . C30 C29 H29C 110.7 . . C30 C29 H29D 110.7 . . C29 C30 H30C 109.9 . . C29 C30 H30D 109.9 . . C29 C30 C31 108.9(16) . . H30C C30 H30D 108.3 . . C31 C30 H30C 109.9 . . C31 C30 H30D 109.9 . . C30 C31 H31C 111.2 . . C30 C31 H31D 111.2 . . C30 C31 C32 102.7(16) . . H31C C31 H31D 109.2 . . C32 C31 H31C 111.2 . . C32 C31 H31D 111.2 . . C31B C32B H32A 109.5 . . C31B C32B H32B 109.5 . . C31B C32B H32C 109.5 . . H32A C32B H32B 109.5 . . H32A C32B H32C 109.5 . . H32B C32B H32C 109.5 . . C31 C32 H32D 109.5 . . C31 C32 H32E 109.5 . . C31 C32 H32F 109.5 . . H32D C32 H32E 109.5 . . H32D C32 H32F 109.5 . . H32E C32 H32F 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 S1 C11 1.808(6) . S1 C1 1.799(5) . S1 B2 1.890(6) . N2 C13 1.401(7) . N2 C12 1.450(7) . N2 C20 1.359(8) . N1 C10 1.394(8) . N1 C3 1.401(8) . N1 C2 1.461(7) . O3 C13 1.191(7) . O2 C10 1.196(7) . O4 C20 1.200(7) . O1 C3 1.206(7) . N3 C21B 1.596(10) . N3 C33B 1.477(10) . N3 C25B 1.530(11) . N3 C21 1.586(14) . N3 C25 1.549(17) . N3 C33 1.577(16) . N3 C29B 1.534(11) . N3 C29 1.489(13) . C13 C14 1.485(8) . C14 C19 1.370(9) . C14 C15 1.386(9) . C10 C9 1.493(9) . C3 C4 1.470(9) . C2 H2A 0.9700 . C2 H2B 0.9700 . C2 C1 1.522(8) . C11 H11A 0.9700 . C11 H11B 0.9700 . C11 C12 1.504(8) . C4 C9 1.378(8) . C4 C5 1.383(9) . C9 C8 1.404(9) . C19 C20 1.506(9) . C19 C18 1.404(9) . C1 H1A 0.9700 . C1 H1B 0.9700 . C12 H12A 0.9700 . C12 H12B 0.9700 . C15 H15 0.9300 . C15 C16 1.390(11) . B2 B9 1.781(9) . B2 B5 1.803(8) . B2 B6 1.783(9) . B2 B1 1.688(10) . B2 B3 1.816(10) . B9 H9 1.1000 . B9 B5 1.813(11) . B9 B6 1.824(10) . B9 B8 1.850(10) . B9 B10 1.673(11) . B5 H5 1.1000 . B5 B1 1.709(11) . B5 B8 1.785(11) . B5 B4 1.830(10) . C5 H5A 0.9300 . C5 C6 1.380(11) . C18 H18 0.9300 . C18 C17 1.367(12) . C16 H16 0.9300 . C16 C17 1.366(12) . C17 H17 0.9300 . C8 H8 0.9300 . C8 C7 1.384(11) . B6 H6 1.1000 . B6 B7 1.777(10) . B6 B3 1.808(11) . B6 B10 1.651(11) . B1 H1 1.1000 . B1 B3 1.705(10) . B1 B4 1.676(11) . C6 H6A 0.9300 . C6 C7 1.349(11) . B7 H7 1.1000 . B7 B3 1.781(11) . B7 B8 1.816(11) . B7 B4 1.837(11) . B7 B10 1.674(12) . B3 H3 1.1000 . B3 B4 1.856(11) . B8 H8A 1.1000 . B8 B4 1.783(12) . B8 B10 1.636(12) . B4 H4 1.1000 . C7 H7A 0.9300 . B10 H10 1.1000 . C21B H21A 0.9700 . C21B H21B 0.9700 . C21B C22B 1.547(9) . C26B H26A 0.9700 . C26B H26B 0.9700 . C26B C27B 1.559(12) . C26B C25B 1.528(13) . C22 H22A 0.9700 . C22 H22B 0.9700 . C22 C21 1.415(11) . C22 C23 1.46811(7) . C27B H27A 0.9700 . C27B H27B 0.9700 . C27B C28B 1.506(15) . C33B H33A 0.9700 . C33B H33B 0.9700 . C33B C34B 1.530(19) . C28B H28A 0.9600 . C28B H28B 0.9600 . C28B H28C 0.9600 . C25B H25A 0.9700 . C25B H25B 0.9700 . C21 H21C 0.9700 . C21 H21D 0.9700 . C23B H23A 0.9700 . C23B H23B 0.9700 . C23B C22B 1.53143(9) . C23B C24B 1.51768(7) . C25 H25C 0.9700 . C25 H25D 0.9700 . C25 C26 1.565(17) . C34B H34A 0.9700 . C34B H34B 0.9700 . C34B C35B 1.483(16) . C35B H35A 0.9700 . C35B H35B 0.9700 . C35B C36B 1.498(13) . C36B H36A 0.9600 . C36B H36B 0.9600 . C36B H36C 0.9600 . C33 H33C 0.9700 . C33 H33D 0.9700 . C33 C34 1.522(18) . C34 H34C 0.9700 . C34 H34D 0.9700 . C34 C35 1.520(19) . C35 H35C 0.9700 . C35 H35D 0.9700 . C35 C36 1.507(19) . C36 H36D 0.9600 . C36 H36E 0.9600 . C36 H36F 0.9600 . C28 H28D 0.9600 . C28 H28E 0.9600 . C28 H28F 0.9600 . C28 C27 1.521(19) . C27 H27C 0.9700 . C27 H27D 0.9700 . C27 C26 1.548(14) . C26 H26C 0.9700 . C26 H26D 0.9700 . C22B H22C 0.9700 . C22B H22D 0.9700 . C24 H24A 0.9600 . C24 H24B 0.9600 . C24 H24C 0.9600 . C24 C23 1.56258(11) . C23 H23C 0.9700 . C23 H23D 0.9700 . C24B H24D 0.9600 . C24B H24E 0.9600 . C24B H24F 0.9600 . C29B H29A 0.9700 . C29B H29B 0.9700 . C29B C30B 1.509(11) . C30B H30A 0.9700 . C30B H30B 0.9700 . C30B C31B 1.499(12) . C31B H31A 0.9700 . C31B H31B 0.9700 . C31B C32B 1.527(15) . C29 H29C 0.9700 . C29 H29D 0.9700 . C29 C30 1.503(14) . C30 H30C 0.9700 . C30 H30D 0.9700 . C30 C31 1.526(19) . C31 H31C 0.9700 . C31 H31D 0.9700 . C31 C32 1.596(18) . C32B H32A 0.9600 . C32B H32B 0.9600 . C32B H32C 0.9600 . C32 H32D 0.9600 . C32 H32E 0.9600 . C32 H32F 0.9600 .