#------------------------------------------------------------------------------ #$Date: 2021-09-29 10:42:35 +0300 (Wed, 29 Sep 2021) $ #$Revision: 269363 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/47/1564741.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564741 loop_ _publ_author_name 'Mohite, S.S.' 'Patil-Deshmukh, A.B.' 'Chavan, S.S.' _publ_section_title ; Ru(III)-pseudohalide complexes with alkynyl functionalized salicylaldimine ligand and heterocyclic coligand: Synthesis, characterization, electrochemical and luminescence properties ; _journal_name_full 'Inorganica Chimica Acta' _journal_page_first 119586 _journal_paper_doi 10.1016/j.ica.2020.119586 _journal_volume 507 _journal_year 2020 _chemical_formula_moiety 'C31 H23 N O3' _chemical_formula_sum 'C31 H23 N O3' _chemical_formula_weight 457.50 _space_group_crystal_system monoclinic _space_group_IT_number 7 _space_group_name_Hall 'P -2yc' _space_group_name_H-M_alt 'P 1 c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 93.279(5) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 26.489(3) _cell_length_b 7.2195(7) _cell_length_c 6.2098(6) _cell_measurement_reflns_used 4942 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 72.46 _cell_measurement_theta_min 3.34 _cell_volume 1185.6(2) _computing_cell_refinement 'APEX3/SAINT (Bruker, 2016)' _computing_data_collection 'APEX3(Bruker, 2016)' _computing_data_reduction 'SAINT/XPREP (Bruker, 2016)' _computing_molecular_graphics 'ORTEP3 (Farrugia, 1997) and Mercury (Bruno et al., 2002)' _computing_publication_material 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT-2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 296(2) _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Bruker axs kappa apex3 CMOS Diffractometer' _diffrn_measurement_method '\w and \f scan' _diffrn_radiation_source 'micro-focus sealed tube' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_unetI/netI 0.1292 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 31 _diffrn_reflns_limit_h_min -30 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 7 _diffrn_reflns_limit_l_min -7 _diffrn_reflns_number 10184 _diffrn_reflns_point_group_measured_fraction_full 0.887 _diffrn_reflns_point_group_measured_fraction_max 0.887 _diffrn_reflns_theta_full 65.986 _diffrn_reflns_theta_max 65.986 _diffrn_reflns_theta_min 3.342 _exptl_absorpt_coefficient_mu 0.656 _exptl_absorpt_correction_T_max 0.7536 _exptl_absorpt_correction_T_min 0.5441 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS (Bruker, 2016)' _exptl_crystal_colour brown _exptl_crystal_density_diffrn 1.282 _exptl_crystal_description needle _exptl_crystal_F_000 480 _exptl_crystal_size_max 0.150 _exptl_crystal_size_mid 0.150 _exptl_crystal_size_min 0.100 _refine_diff_density_max 0.197 _refine_diff_density_min -0.205 _refine_diff_density_rms 0.045 _refine_ls_abs_structure_details ; Flack x determined using 886 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.2(3) _refine_ls_extinction_coef 0.010(4) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.023 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 318 _refine_ls_number_reflns 10184 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.023 _refine_ls_R_factor_all 0.1220 _refine_ls_R_factor_gt 0.0732 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0874P)^2^+0.0883P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1781 _refine_ls_wR_factor_ref 0.2045 _reflns_Friedel_coverage 0.781 _reflns_Friedel_fraction_full 0.779 _reflns_Friedel_fraction_max 0.779 _reflns_number_gt 6992 _reflns_number_total 10184 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ICA-2020-507-119586.cif _cod_data_source_block 1 _cod_original_sg_symbol_H-M 'P c' _cod_database_code 1564741 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.908 _shelx_estimated_absorpt_t_max 0.937 _shelx_res_file ; TITL 1_a.res in Pc 1.res created by SHELXL-2018/3 at 15:32:07 on 14-Jun-2019 CELL 1.54178 26.4886 7.2195 6.2098 90.000 93.279 90.000 ZERR 2.00 0.0025 0.0007 0.0006 0.000 0.005 0.000 LATT -1 SYMM X, - Y, 1/2 + Z SFAC C H N O UNIT 62 46 2 6 MERG 0 OMIT -3.00 132.00 EQIV $1 x, y, z+1 HTAB C17 O2_$1 EQIV $2 x+1, y, z+1 HTAB C30 O1_$2 EQIV $3 x-1, y, z HTAB C31 O3_$3 HTAB O2 N1 FMAP 2 PLAN 20 SIZE 0.10 0.15 0.15 ACTA BOND $H CONF L.S. 10 TEMP 23.00 WGHT 0.087400 0.088300 EXTI 0.010269 BASF 0.36685 FVAR 1.45782 C1 1 0.109249 0.747263 0.535436 11.00000 0.04409 0.05551 = 0.05414 0.00660 0.00578 0.00448 C2 1 0.117189 0.661156 0.339438 11.00000 0.04716 0.06343 = 0.05780 -0.00514 -0.00429 -0.00645 AFIX 43 H2 2 0.090735 0.601545 0.262738 11.00000 -1.20000 AFIX 0 C3 1 0.164623 0.665522 0.261060 11.00000 0.04982 0.06284 = 0.05622 -0.00196 0.00241 0.00095 AFIX 43 H3 2 0.169748 0.610181 0.128844 11.00000 -1.20000 AFIX 0 C4 1 0.204755 0.749379 0.372485 11.00000 0.04353 0.05681 = 0.05888 0.00567 -0.00345 0.00363 C5 1 0.196259 0.831290 0.570972 11.00000 0.05164 0.05989 = 0.06678 -0.00891 -0.00601 0.00212 AFIX 43 H5 2 0.222984 0.887222 0.649932 11.00000 -1.20000 AFIX 0 C6 1 0.148786 0.830406 0.651560 11.00000 0.03991 0.07086 = 0.05545 -0.00947 -0.00044 0.00131 AFIX 43 H6 2 0.143558 0.885737 0.783684 11.00000 -1.20000 AFIX 0 C7 1 0.253414 0.758243 0.279990 11.00000 0.04451 0.06187 = 0.06607 0.00628 -0.00280 0.00661 C8 1 0.291596 0.768368 0.189347 11.00000 0.04313 0.06317 = 0.07368 0.00733 0.00157 0.00086 C9 1 0.337286 0.762856 0.073599 11.00000 0.04513 0.05518 = 0.06640 0.00173 0.00057 0.00172 C10 1 0.334463 0.701701 -0.141580 11.00000 0.04176 0.07525 = 0.06535 0.00163 -0.00840 -0.00266 AFIX 43 H10 2 0.303149 0.676466 -0.210747 11.00000 -1.20000 AFIX 0 C11 1 0.378015 0.678948 -0.250672 11.00000 0.05347 0.06733 = 0.05124 0.00134 -0.01022 -0.00812 AFIX 43 H11 2 0.375843 0.636789 -0.392415 11.00000 -1.20000 AFIX 0 C12 1 0.424361 0.717836 -0.152238 11.00000 0.05183 0.06468 = 0.04585 0.00716 0.00149 0.00030 C13 1 0.428252 0.779755 0.063249 11.00000 0.04318 0.05490 = 0.05309 0.00167 -0.00231 0.00141 C14 1 0.383853 0.805350 0.170410 11.00000 0.04558 0.05667 = 0.05058 -0.00034 0.00038 0.00363 AFIX 43 H14 2 0.385805 0.852113 0.310185 11.00000 -1.20000 AFIX 0 C15 1 0.477192 0.801568 0.181665 11.00000 0.04613 0.06356 = 0.05069 -0.00388 0.00159 -0.00378 AFIX 43 H15 2 0.478245 0.837987 0.325505 11.00000 -1.20000 AFIX 0 C16 1 0.564892 0.766123 0.212121 11.00000 0.04677 0.04724 = 0.05137 -0.00084 -0.00180 -0.00044 C17 1 0.569644 0.686255 0.417199 11.00000 0.04654 0.06067 = 0.05497 0.00053 0.00744 -0.00523 AFIX 43 H17 2 0.541123 0.639719 0.479153 11.00000 -1.20000 AFIX 0 C18 1 0.615990 0.675500 0.528859 11.00000 0.05301 0.05802 = 0.05560 0.00404 0.00061 -0.00428 AFIX 43 H18 2 0.618470 0.621420 0.664980 11.00000 -1.20000 AFIX 0 C19 1 0.659279 0.745114 0.439388 11.00000 0.05081 0.05348 = 0.06353 -0.00199 -0.00243 0.00629 C20 1 0.654476 0.819806 0.231297 11.00000 0.04524 0.05837 = 0.06107 0.00289 0.00619 -0.00696 AFIX 43 H20 2 0.683000 0.864643 0.167855 11.00000 -1.20000 AFIX 0 C21 1 0.608622 0.827882 0.120062 11.00000 0.04835 0.05710 = 0.05033 0.00496 0.00470 0.00054 AFIX 43 H21 2 0.606495 0.875336 -0.019393 11.00000 -1.20000 AFIX 0 C22 1 0.707422 0.743998 0.558870 11.00000 0.04762 0.06091 = 0.06737 -0.00267 -0.00265 0.00379 C23 1 0.746537 0.749338 0.662634 11.00000 0.05313 0.05215 = 0.06459 -0.00381 -0.00351 0.00447 C24 1 0.795131 0.754048 0.775448 11.00000 0.04654 0.05402 = 0.06081 -0.00698 0.00219 0.00251 C25 1 0.804015 0.672182 0.975059 11.00000 0.04499 0.06583 = 0.06698 0.00602 -0.00126 -0.00401 AFIX 43 H25 2 0.777221 0.617676 1.041958 11.00000 -1.20000 AFIX 0 C26 1 0.851806 0.669111 1.078310 11.00000 0.05317 0.06603 = 0.05751 0.00752 0.00080 -0.00054 AFIX 43 H26 2 0.857142 0.611058 1.211360 11.00000 -1.20000 AFIX 0 C27 1 0.891385 0.753361 0.981055 11.00000 0.04465 0.05783 = 0.05853 -0.00709 -0.00290 0.00302 C28 1 0.883124 0.836641 0.782293 11.00000 0.05650 0.05944 = 0.05933 0.00165 0.00584 -0.00337 AFIX 43 H28 2 0.909863 0.893563 0.717527 11.00000 -1.20000 AFIX 0 C29 1 0.836300 0.836540 0.679730 11.00000 0.05260 0.06111 = 0.05176 0.00099 -0.00261 0.00191 AFIX 43 H29 2 0.831532 0.891724 0.544774 11.00000 -1.20000 AFIX 0 C30 1 0.951733 0.667159 1.265497 11.00000 0.06630 0.13121 = 0.07029 0.01351 -0.01724 0.00502 AFIX 33 H30A 2 0.986905 0.683637 1.307186 11.00000 -1.50000 H30B 2 0.931550 0.717117 1.375197 11.00000 -1.50000 H30C 2 0.944597 0.537500 1.247849 11.00000 -1.50000 AFIX 0 C31 1 0.048343 0.832314 0.789547 11.00000 0.06703 0.12174 = 0.08104 -0.01531 0.02466 0.00251 AFIX 33 H31A 2 0.013304 0.813356 0.814876 11.00000 -1.50000 H31B 2 0.068905 0.785812 0.909927 11.00000 -1.50000 H31C 2 0.054646 0.962285 0.772467 11.00000 -1.50000 AFIX 0 N1 3 0.518504 0.771570 0.091356 11.00000 0.04506 0.06076 = 0.05332 0.00410 -0.00220 -0.00317 O1 4 0.060479 0.736531 0.598563 11.00000 0.04417 0.08146 = 0.07365 -0.00609 0.01158 -0.00330 O2 4 0.467009 0.690105 -0.261315 11.00000 0.05081 0.10319 = 0.05424 -0.00583 0.00902 -0.00290 AFIX 83 H2A 2 0.491916 0.718605 -0.183907 11.00000 -1.50000 AFIX 0 O3 4 0.940095 0.760835 1.067333 11.00000 0.04667 0.08308 = 0.06906 0.00597 -0.00496 -0.00229 HKLF 5 REM 1_a.res in Pc REM wR2 = 0.2045, GooF = S = 1.023, Restrained GooF = 1.023 for all data REM R1 = 0.0732 for 6992 Fo > 4sig(Fo) and 0.1220 for all 10184 data REM 318 parameters refined using 2 restraints END WGHT 0.0874 0.0883 REM Highest difference peak 0.197, deepest hole -0.205, 1-sigma level 0.045 Q1 1 0.2834 0.7075 0.3659 11.00000 0.05 0.20 Q2 1 0.6485 0.7425 0.4793 11.00000 0.05 0.19 Q3 1 0.8702 0.7458 1.0230 11.00000 0.05 0.18 Q4 1 1.0196 0.7402 1.2055 11.00000 0.05 0.17 Q5 1 0.5925 0.7338 0.1560 11.00000 0.05 0.16 Q6 1 0.4303 0.8322 -0.1021 11.00000 0.05 0.16 Q7 1 0.3773 0.7171 -0.3672 11.00000 0.05 0.16 Q8 1 0.7375 0.7951 0.5100 11.00000 0.05 0.16 Q9 1 0.7994 0.7789 0.8966 11.00000 0.05 0.16 Q10 1 0.5666 0.6750 0.3163 11.00000 0.05 0.16 Q11 1 0.3846 0.7767 0.4919 11.00000 0.05 0.15 Q12 1 0.4026 0.7416 -0.2263 11.00000 0.05 0.14 Q13 1 0.7096 0.8036 0.6629 11.00000 0.05 0.14 Q14 1 0.7388 0.6940 0.5370 11.00000 0.05 0.14 Q15 1 0.5742 0.7848 0.3515 11.00000 0.05 0.14 Q16 1 0.1637 0.7425 0.0049 11.00000 0.05 0.14 Q17 1 0.5247 0.7051 -0.0932 11.00000 0.05 0.14 Q18 1 0.3854 0.8838 -0.3332 11.00000 0.05 0.13 Q19 1 -0.0158 0.7615 0.6574 11.00000 0.05 0.13 Q20 1 0.7157 0.6822 0.6683 11.00000 0.05 0.13 ; _shelx_res_checksum 25669 _shelx_hkl_file ; 0 0 1 0.00 0.50 1 0 0 1 1.50 0.50 1 0 0 -1 0.80 0.40 1 0 0 -1 0.50 0.40 1 0 0 -3 -0.60 1.60 1 0 0 -3 1.50 1.40 1 0 0 3 2.30 2.10 1 -2 0 4 498.15 40.90 -2 0 0 -4 498.15 40.90 1 -2 0 4 538.65 41.60 -2 0 0 -4 538.65 41.60 1 0 0 5 -0.60 5.70 1 0 0 5 -5.70 5.50 1 0 0 5 -1.30 7.50 1 3 0 -6 71.39 7.80 -2 0 0 6 71.39 7.80 1 3 0 -6 73.69 8.60 -2 0 0 6 73.69 8.60 1 3 0 -6 45.70 9.70 -2 0 0 6 45.70 9.70 1 -3 0 6 61.79 9.80 -2 0 0 -6 61.79 9.80 1 0 0 7 2.50 2.60 1 0 0 7 6.10 3.00 1 0 -1 0 3.10 0.40 -2 0 1 0 3.10 0.40 1 0 -1 0 5.00 1.00 -2 0 1 0 5.00 1.00 1 0 1 0 2.20 0.60 -2 0 -1 0 2.20 0.60 1 0 1 0 2.20 0.40 -2 0 -1 0 2.20 0.40 1 0 1 0 2.40 1.10 -2 0 -1 0 2.40 1.10 1 0 1 -1 421.76 32.80 1 0 1 -1 411.36 32.80 1 0 1 -1 446.76 32.80 1 0 -1 -1 388.26 33.20 1 0 -1 1 390.96 32.70 1 0 -1 -1 419.66 32.80 1 0 -1 1 475.55 33.00 1 -1 -1 2 1228.18 91.79 -2 0 1 -2 1228.18 91.79 1 -1 1 2 1219.08 91.69 -2 0 -1 -2 1219.08 91.69 1 1 1 -2 1094.89 91.69 -2 0 -1 2 1094.89 91.69 1 -1 1 2 1202.18 91.99 -2 0 -1 -2 1202.18 91.99 1 0 1 -3 325.87 27.50 1 0 1 -3 341.67 27.20 1 0 -1 -3 357.66 27.50 1 0 -1 -3 347.57 27.10 1 -2 -1 4 44.60 5.80 -2 0 1 -4 44.60 5.80 1 -2 -1 4 45.80 6.80 -2 0 1 -4 45.80 6.80 1 -2 1 4 53.49 5.90 -2 0 -1 -4 53.49 5.90 1 -2 1 4 51.89 6.80 -2 0 -1 -4 51.89 6.80 1 0 1 5 4.60 5.30 1 0 1 5 15.40 10.40 1 0 1 5 13.30 6.60 1 0 -1 5 20.00 5.30 1 0 -1 5 15.50 6.10 1 0 -1 -5 18.80 7.40 1 0 -1 5 8.90 6.00 1 3 -1 -6 11.80 4.20 -2 0 1 6 11.80 4.20 1 3 -1 -6 2.70 5.50 -2 0 1 6 2.70 5.50 1 3 1 -6 11.60 4.40 -2 0 -1 6 11.60 4.40 1 3 1 -6 8.40 4.50 -2 0 -1 6 8.40 4.50 1 -3 1 6 4.00 6.00 -2 0 -1 -6 4.00 6.00 1 0 1 -7 9.40 5.00 1 0 1 7 22.30 4.90 1 0 1 7 15.90 3.50 1 0 -1 7 21.40 3.50 1 0 2 -1 175.48 14.30 1 0 2 -1 177.08 14.60 1 0 2 -1 206.88 14.40 1 0 -2 -1 174.78 16.80 1 0 -2 1 186.38 14.90 1 0 -2 1 158.78 14.30 1 0 -2 -1 186.08 14.30 1 0 -2 1 191.78 14.80 1 -1 -2 2 1567.94 127.09 -2 0 2 -2 1567.94 127.09 1 1 -2 -2 1737.13 127.19 -2 0 2 2 1737.13 127.19 1 -1 -2 2 1665.23 126.99 -2 0 2 -2 1665.23 126.99 1 1 2 -2 1664.63 127.29 -2 0 -2 2 1664.63 127.29 1 1 2 -2 1695.73 127.19 -2 0 -2 2 1695.73 127.19 1 -1 2 2 1678.53 126.79 -2 0 -2 -2 1678.53 126.79 1 -1 2 2 1622.04 126.99 -2 0 -2 -2 1622.04 126.99 1 -1 2 2 1494.05 127.89 -2 0 -2 -2 1494.05 127.89 1 0 2 -3 111.99 9.10 1 0 2 -3 95.49 9.30 1 0 -2 -3 104.49 9.20 1 0 -2 -3 102.59 8.90 1 -2 -2 4 202.18 18.20 -2 0 2 -4 202.18 18.20 1 -2 -2 4 196.38 17.40 -2 0 2 -4 196.38 17.40 1 -2 2 4 222.68 18.40 -2 0 -2 -4 222.68 18.40 1 0 2 5 9.00 5.10 1 0 2 5 18.20 12.90 1 0 2 5 11.50 6.10 1 0 -2 -5 8.50 7.40 1 0 -2 5 8.70 4.60 1 0 -2 5 13.40 5.30 1 0 -2 5 21.80 6.50 1 -3 -2 6 45.20 10.10 -2 0 2 -6 45.20 10.10 1 3 -2 -6 40.30 7.70 -2 0 2 6 40.30 7.70 1 3 2 -6 47.10 6.30 -2 0 -2 6 47.10 6.30 1 3 2 -6 54.99 6.40 -2 0 -2 6 54.99 6.40 1 3 2 -6 33.30 7.00 -2 0 -2 6 33.30 7.00 1 0 2 7 2.30 2.50 1 0 2 7 9.30 3.30 1 0 -2 7 7.40 2.60 1 0 -2 7 7.80 2.20 1 0 -3 0 2.20 0.90 -2 0 3 0 2.20 0.90 1 0 3 0 -0.40 2.50 -2 0 -3 0 -0.40 2.50 1 0 3 0 3.70 2.90 -2 0 -3 0 3.70 2.90 1 0 3 -1 214.08 17.10 1 0 3 -1 214.88 16.80 1 0 3 1 216.88 17.00 1 0 -3 1 219.78 17.90 1 0 -3 -1 184.68 16.50 1 0 -3 1 234.78 17.70 1 0 -3 -1 198.68 17.90 1 -1 -3 2 2513.95 189.18 -2 0 3 -2 2513.95 189.18 1 -1 -3 2 2170.18 189.58 -2 0 3 -2 2170.18 189.58 1 1 -3 -2 2202.48 189.38 -2 0 3 2 2202.48 189.38 1 -1 3 2 2593.64 191.08 -2 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5.30 1 -1 -4 5 8.50 4.10 1 -1 -4 5 -0.10 4.50 1 1 -4 -4 46.90 13.40 -2 -1 4 4 46.90 13.40 1 1 -4 -4 36.40 8.30 -2 -1 4 4 36.40 8.30 1 1 -4 -4 29.80 5.80 -2 -1 4 4 29.80 5.80 1 -1 -4 4 30.40 6.40 -2 1 4 -4 30.40 6.40 1 1 4 -4 34.10 7.90 -2 -1 -4 4 34.10 7.90 1 1 4 -4 35.80 8.60 -2 -1 -4 4 35.80 8.60 1 1 4 -3 44.80 6.60 1 1 4 -3 43.60 6.50 1 0 -4 2 244.18 23.10 -2 1 4 -2 244.18 23.10 1 0 -4 2 286.07 22.80 -2 1 4 -2 286.07 22.80 1 0 4 -2 291.27 24.90 -2 -1 -4 2 291.27 24.90 1 0 4 2 311.77 26.10 -2 1 -4 -2 311.77 26.10 1 0 4 -2 297.17 24.20 -2 -1 -4 2 297.17 24.20 1 1 4 -1 1515.45 114.39 1 1 4 -1 1623.64 115.19 1 -1 -4 1 1428.06 115.89 1 -1 -4 1 1453.85 115.99 1 1 -4 -1 1358.16 116.39 1 -1 -4 0 210.18 17.70 -2 -1 4 0 210.18 17.70 1 1 -4 0 206.78 17.80 -2 1 4 0 206.78 17.80 1 1 -4 0 212.08 17.30 -2 1 4 0 212.08 17.30 1 -1 4 0 212.78 19.10 -2 -1 -4 0 212.78 19.10 1 -1 4 0 247.58 19.30 -2 -1 -4 0 247.58 19.30 1 1 4 0 225.58 18.80 -2 1 -4 0 225.58 18.80 1 -1 4 -1 2596.14 186.88 1 1 4 1 2563.24 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-1 6 3 11.60 5.00 1 1 6 -3 2.10 6.10 1 1 6 -3 10.00 16.40 1 -1 6 3 11.30 8.80 1 -1 -6 3 12.40 5.30 1 0 -6 2 51.99 7.60 -2 1 6 -2 51.99 7.60 1 0 -6 2 79.49 20.40 -2 1 6 -2 79.49 20.40 1 0 -6 -2 44.40 9.10 -2 -1 6 2 44.40 9.10 1 0 6 -2 70.79 9.80 -2 -1 -6 2 70.79 9.80 1 1 6 -1 67.09 7.60 1 1 6 -1 57.09 10.80 1 -1 -6 1 54.29 10.50 1 -1 -6 1 50.09 14.70 1 1 -6 0 -1.00 8.80 -2 1 6 0 -1.00 8.80 1 1 -6 0 -2.40 3.70 -2 1 6 0 -2.40 3.70 1 1 -6 0 5.60 6.70 -2 1 6 0 5.60 6.70 1 -1 -6 0 7.10 9.20 -2 -1 6 0 7.10 9.20 1 -1 -6 0 -9.40 6.70 -2 -1 6 0 -9.40 6.70 1 1 6 0 -5.90 9.10 -2 1 -6 0 -5.90 9.10 1 -1 6 0 2.00 7.20 -2 -1 -6 0 2.00 7.20 1 -1 6 0 8.30 8.60 -2 -1 -6 0 8.30 8.60 1 1 6 1 164.58 16.60 1 -1 6 -1 161.58 17.60 1 1 6 1 186.78 18.50 1 -1 6 -1 183.08 15.10 1 1 -6 1 165.98 21.30 1 -1 -6 -1 141.09 19.70 1 1 -6 1 151.78 17.30 1 2 -6 -2 69.89 12.80 -2 1 6 2 69.89 12.80 1 -2 -6 2 50.49 7.70 -2 -1 6 -2 50.49 7.70 1 2 -6 -2 53.79 10.70 -2 1 6 2 53.79 10.70 1 2 6 -2 74.79 10.60 -2 1 -6 2 74.79 10.60 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6.60 -2 -1 -7 0 12.50 6.60 1 -1 7 -1 52.19 8.10 1 1 7 1 36.70 9.50 1 1 -7 1 32.10 7.20 1 2 -7 -2 75.99 11.00 -2 1 7 2 75.99 11.00 1 2 -7 -2 99.89 10.40 -2 1 7 2 99.89 10.40 1 -2 -7 2 80.89 10.50 -2 -1 7 -2 80.89 10.50 1 2 7 -2 107.69 10.80 -2 1 -7 2 107.69 10.80 1 1 7 3 7.90 3.80 1 1 7 3 12.70 5.70 1 1 7 3 12.60 6.80 1 1 -7 3 5.80 3.70 1 3 -7 -4 1.80 4.00 -2 1 7 4 1.80 4.00 1 3 -7 -4 10.40 4.20 -2 1 7 4 10.40 4.20 1 3 7 -4 2.20 2.50 -2 1 -7 4 2.20 2.50 1 -1 8 3 14.80 3.50 1 -1 -8 3 8.10 2.50 1 0 -8 -2 15.40 4.00 -2 -1 8 2 15.40 4.00 1 0 -8 2 2.00 8.30 -2 1 8 -2 2.00 8.30 1 0 8 -2 9.10 3.30 -2 -1 -8 2 9.10 3.30 1 1 8 -1 15.80 7.70 1 -1 8 1 18.10 5.20 1 -1 -8 1 13.90 4.40 1 -1 -8 0 30.40 9.40 -2 -1 8 0 30.40 9.40 1 1 -8 0 24.60 7.20 -2 1 8 0 24.60 7.20 1 1 -8 0 31.10 7.60 -2 1 8 0 31.10 7.60 1 -1 8 -1 11.90 7.30 1 1 8 1 9.10 5.10 1 -2 -8 2 19.10 9.00 -2 -1 8 -2 19.10 9.00 1 2 8 -2 21.50 4.60 -2 1 -8 2 21.50 4.60 1 1 8 3 6.10 6.70 1 1 8 3 0.40 3.40 1 1 -8 3 0.20 2.50 1 -2 0 7 -0.30 3.30 1 -2 0 7 0.60 4.30 1 -2 0 7 2.70 2.50 1 1 0 -6 91.29 10.60 -2 -2 0 6 91.29 10.60 1 1 0 -6 113.39 11.10 -2 -2 0 6 113.39 11.10 1 1 0 -6 115.29 12.60 -2 -2 0 6 115.29 12.60 1 -2 0 5 16.00 5.60 1 -2 0 5 8.70 7.70 1 -2 0 5 2.70 6.10 1 -2 0 3 -1.00 2.40 1 2 0 -3 0.70 1.60 1 2 0 -3 1.80 1.50 1 1 0 2 1985.40 148.59 -2 2 0 -2 1985.40 148.59 1 1 0 2 1755.02 148.29 -2 2 0 -2 1755.02 148.29 1 -1 0 -2 2020.20 148.69 -2 -2 0 2 2020.20 148.69 1 -2 0 1 0.30 0.70 1 2 0 -1 0.60 0.40 1 2 0 -1 0.60 0.30 1 -2 0 0 337.47 24.00 -2 -2 0 0 337.47 24.00 1 -2 0 0 290.37 24.10 -2 -2 0 0 290.37 24.10 1 2 0 0 303.17 24.10 -2 2 0 0 303.17 24.10 1 -3 0 2 961.90 71.19 -2 -2 0 -2 961.90 71.19 1 3 0 -2 870.91 70.79 -2 2 0 2 870.91 70.79 1 -2 0 -3 0.70 1.60 1 -2 0 -3 0.50 1.60 1 -4 0 4 46.70 5.40 -2 -2 0 -4 46.70 5.40 1 -4 0 4 39.90 6.30 -2 -2 0 -4 39.90 6.30 1 2 0 5 -2.40 5.10 1 2 0 5 9.90 5.20 1 2 0 5 -2.50 5.60 1 2 0 5 -10.00 7.70 1 5 0 -6 13.00 4.10 -2 2 0 6 13.00 4.10 1 5 0 -6 16.50 6.50 -2 2 0 6 16.50 6.50 1 5 0 -6 10.70 4.50 -2 2 0 6 10.70 4.50 1 2 0 7 -1.00 2.60 1 -2 0 -7 10.70 4.70 1 2 0 7 -3.80 5.10 1 2 0 7 0.30 2.80 1 -2 1 7 26.00 3.90 1 -2 1 7 26.80 5.00 1 -2 -1 7 33.40 3.90 1 -2 -1 7 21.80 3.80 1 1 -1 -6 -1.50 3.90 -2 -2 1 6 -1.50 3.90 1 1 -1 -6 -4.90 5.20 -2 -2 1 6 -4.90 5.20 1 -1 1 6 3.60 6.70 -2 2 -1 -6 3.60 6.70 1 1 1 -6 -3.00 4.00 -2 -2 -1 6 -3.00 4.00 1 1 1 -6 1.50 4.10 -2 -2 -1 6 1.50 4.10 1 -2 1 5 10.90 5.90 1 -2 1 5 16.90 6.80 1 2 -1 -5 8.80 7.90 1 -2 -1 5 15.60 6.30 1 -2 -1 5 23.30 6.00 1 0 -1 4 20.00 4.00 -2 2 1 -4 20.00 4.00 1 0 1 4 22.70 3.90 -2 2 -1 -4 22.70 3.90 1 0 1 4 37.30 5.80 -2 2 -1 -4 37.30 5.80 1 2 1 -3 2896.21 241.98 1 2 1 -3 3226.38 241.78 1 2 -1 -3 2899.61 241.98 1 -2 -1 3 3100.99 241.78 1 -2 -1 3 3469.75 242.68 1 2 -1 -3 3180.88 241.58 1 1 -1 2 272.57 21.40 -2 2 1 -2 272.57 21.40 1 1 1 2 274.97 21.20 -2 2 -1 -2 274.97 21.20 1 -1 1 -2 243.38 21.40 -2 -2 -1 2 243.38 21.40 1 1 1 2 295.97 21.60 -2 2 -1 -2 295.97 21.60 1 -2 -1 0 116.99 9.60 -2 -2 1 0 116.99 9.60 1 -2 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4.70 1 2 -1 5 8.80 5.20 1 5 -1 -6 11.30 4.50 -2 2 1 6 11.30 4.50 1 5 -1 -6 14.50 5.80 -2 2 1 6 14.50 5.80 1 5 -1 -6 9.00 4.70 -2 2 1 6 9.00 4.70 1 5 1 -6 15.80 4.60 -2 2 -1 6 15.80 4.60 1 -5 1 6 15.70 5.90 -2 -2 -1 -6 15.70 5.90 1 5 1 -6 20.30 4.60 -2 2 -1 6 20.30 4.60 1 2 1 7 14.70 3.50 1 2 1 7 27.10 5.10 1 -2 1 -7 23.60 4.80 1 2 -1 7 19.50 3.60 1 2 -1 7 17.70 3.30 1 -2 2 7 1.20 3.10 1 -2 2 7 7.20 2.70 1 2 2 -7 0.00 5.80 1 -2 -2 7 6.30 2.30 1 -2 -2 7 3.60 2.40 1 1 -2 -6 59.29 8.80 -2 -2 2 6 59.29 8.80 1 1 -2 -6 55.69 15.70 -2 -2 2 6 55.69 15.70 1 1 -2 -6 52.29 7.80 -2 -2 2 6 52.29 7.80 1 1 2 -6 72.09 7.60 -2 -2 -2 6 72.09 7.60 1 1 2 -6 74.59 8.50 -2 -2 -2 6 74.59 8.50 1 -2 2 5 16.50 5.20 1 -2 2 5 -3.00 5.70 1 -2 2 5 12.70 12.40 1 2 2 -5 22.10 5.30 1 -2 -2 5 14.10 6.10 1 -2 -2 5 9.00 5.40 1 -2 -2 5 8.80 5.80 1 0 -2 4 165.58 16.50 -2 2 2 -4 165.58 16.50 1 0 -2 4 221.08 17.50 -2 2 2 -4 221.08 17.50 1 0 2 4 202.38 17.40 -2 2 -2 -4 202.38 17.40 1 2 2 -3 94.09 9.20 1 2 2 -3 107.29 8.90 1 2 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-6 4.80 9.50 -2 -2 3 6 4.80 9.50 1 1 3 -6 1.40 4.70 -2 -2 -3 6 1.40 4.70 1 1 3 -6 2.40 3.20 -2 -2 -3 6 2.40 3.20 1 1 3 -6 -0.90 4.10 -2 -2 -3 6 -0.90 4.10 1 2 3 -5 9.40 5.00 1 -2 3 5 -5.80 9.90 1 -2 3 5 3.20 6.30 1 -2 3 5 2.20 6.30 1 -2 -3 5 2.50 8.00 1 -2 -3 5 3.00 5.20 1 -2 -3 5 6.00 4.40 1 0 -3 -4 94.69 12.50 -2 -2 3 4 94.69 12.50 1 0 -3 -4 77.79 9.50 -2 -2 3 4 77.79 9.50 1 0 -3 4 71.99 9.00 -2 2 3 -4 71.99 9.00 1 0 3 -4 97.79 10.60 -2 -2 -3 4 97.79 10.60 1 2 3 -3 382.26 29.40 1 2 3 -3 324.17 29.40 1 2 3 -3 399.16 29.90 1 2 -3 -3 365.36 29.60 1 1 -3 2 373.16 29.40 -2 2 3 -2 373.16 29.40 1 1 -3 2 330.47 29.70 -2 2 3 -2 330.47 29.70 1 -1 3 -2 368.56 30.30 -2 -2 -3 2 368.56 30.30 1 1 3 2 430.76 29.60 -2 2 -3 -2 430.76 29.60 1 -1 3 -2 362.26 30.30 -2 -2 -3 2 362.26 30.30 1 2 3 -1 3379.76 242.48 1 -2 3 1 3296.67 242.08 1 2 3 -1 3194.28 241.88 1 2 -3 -1 2924.21 243.28 1 2 -3 -1 2732.73 241.58 1 -2 -3 1 3141.99 242.78 1 -2 -3 1 3263.37 243.08 1 2 -3 0 46.20 4.70 -2 2 3 0 46.20 4.70 1 2 -3 0 51.69 4.60 -2 2 3 0 51.69 4.60 1 -2 -3 0 49.50 5.00 -2 -2 3 0 49.50 5.00 1 -2 -3 0 50.39 4.40 -2 -2 3 0 50.39 4.40 1 -2 3 0 58.89 4.40 -2 -2 -3 0 58.89 4.40 1 -2 3 0 54.39 6.10 -2 -2 -3 0 54.39 6.10 1 -2 3 0 59.59 5.90 -2 -2 -3 0 59.59 5.90 1 2 3 0 60.49 6.30 -2 2 -3 0 60.49 6.30 1 -2 3 -1 2474.55 184.18 1 2 3 1 2595.04 184.08 1 -2 3 -1 2418.26 183.68 1 -2 -3 -1 2322.47 183.58 1 2 -3 1 2235.08 184.68 1 -2 -3 -1 2300.97 184.88 1 -2 -3 -1 2296.97 185.18 1 -3 -3 2 217.18 17.00 -2 -2 3 -2 217.18 17.00 1 -3 -3 2 190.58 17.10 -2 -2 3 -2 190.58 17.10 1 -3 3 2 219.98 18.70 -2 -2 -3 -2 219.98 18.70 1 3 3 -2 208.38 18.10 -2 2 -3 2 208.38 18.10 1 -3 3 2 228.78 17.30 -2 -2 -3 -2 228.78 17.30 1 -2 3 -3 96.69 8.20 1 2 3 3 82.59 8.30 1 -2 -3 -3 77.39 8.50 1 4 -3 -4 0.50 7.00 -2 2 3 4 0.50 7.00 1 4 -3 -4 28.00 7.10 -2 2 3 4 28.00 7.10 1 4 -3 -4 22.70 11.80 -2 2 3 4 22.70 11.80 1 4 3 -4 10.80 6.70 -2 2 -3 4 10.80 6.70 1 -4 3 4 17.10 7.20 -2 -2 -3 -4 17.10 7.20 1 -4 3 4 15.00 8.70 -2 -2 -3 -4 15.00 8.70 1 4 3 -4 9.80 5.60 -2 2 -3 4 9.80 5.60 1 2 3 5 19.20 5.70 1 2 3 5 9.80 10.30 1 2 3 5 18.10 5.60 1 -2 3 -5 13.00 4.70 1 -2 -3 -5 8.50 7.30 1 2 -3 5 21.40 5.30 1 2 -3 5 16.00 6.40 1 2 -3 5 16.70 4.70 1 5 -3 -6 26.10 9.70 -2 2 3 6 26.10 9.70 1 -5 -3 6 36.30 7.30 -2 -2 3 -6 36.30 7.30 1 5 -3 -6 28.90 6.00 -2 2 3 6 28.90 6.00 1 5 -3 -6 26.60 6.50 -2 2 3 6 26.60 6.50 1 5 3 -6 17.30 5.20 -2 2 -3 6 17.30 5.20 1 5 3 -6 25.40 4.90 -2 2 -3 6 25.40 4.90 1 5 3 -6 31.00 5.40 -2 2 -3 6 31.00 5.40 1 2 3 7 2.70 2.70 1 2 -3 7 4.20 1.80 1 1 -4 -6 25.10 6.50 -2 -2 4 6 25.10 6.50 1 1 -4 -6 24.60 4.70 -2 -2 4 6 24.60 4.70 1 1 4 -6 20.50 3.40 -2 -2 -4 6 20.50 3.40 1 -2 4 5 6.50 4.40 1 -2 4 5 1.60 8.40 1 2 4 -5 6.50 5.60 1 -2 4 5 -0.60 5.10 1 -2 -4 5 4.70 3.70 1 -2 -4 5 -6.00 4.50 1 0 -4 -4 46.70 7.20 -2 -2 4 4 46.70 7.20 1 0 -4 4 44.10 6.90 -2 2 4 -4 44.10 6.90 1 0 -4 -4 46.00 9.60 -2 -2 4 4 46.00 9.60 1 0 4 -4 41.90 9.20 -2 -2 -4 4 41.90 9.20 1 0 4 -4 42.20 8.00 -2 -2 -4 4 42.20 8.00 1 2 4 -3 31.40 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16.60 6.70 1 -4 -4 4 24.50 5.60 -2 -2 4 -4 24.50 5.60 1 4 4 -4 18.80 6.10 -2 2 -4 4 18.80 6.10 1 4 4 -4 17.70 5.80 -2 2 -4 4 17.70 5.80 1 2 4 5 1.70 8.00 1 -2 4 -5 7.30 5.30 1 2 4 5 -3.30 5.00 1 2 -4 5 0.20 3.70 1 2 -4 5 -3.50 4.30 1 5 -4 -6 19.80 6.40 -2 2 4 6 19.80 6.40 1 5 -4 -6 7.40 3.70 -2 2 4 6 7.40 3.70 1 5 4 -6 9.00 2.40 -2 2 -4 6 9.00 2.40 1 5 4 -6 8.60 2.70 -2 2 -4 6 8.60 2.70 1 1 -5 -6 1.30 4.10 -2 -2 5 6 1.30 4.10 1 1 -5 -6 3.40 4.00 -2 -2 5 6 3.40 4.00 1 1 5 -6 0.80 2.30 -2 -2 -5 6 0.80 2.30 1 1 5 -6 0.60 2.00 -2 -2 -5 6 0.60 2.00 1 -2 5 5 13.40 5.00 1 2 5 -5 6.10 5.70 1 -2 5 5 15.70 7.60 1 -2 5 5 12.90 4.40 1 -2 -5 5 13.40 3.70 1 -2 -5 5 2.90 3.70 1 0 -5 -4 21.40 6.70 -2 -2 5 4 21.40 6.70 1 0 -5 -4 19.50 4.60 -2 -2 5 4 19.50 4.60 1 0 -5 4 4.40 5.00 -2 2 5 -4 4.40 5.00 1 0 -5 -4 19.30 9.70 -2 -2 5 4 19.30 9.70 1 0 5 -4 12.10 5.10 -2 -2 -5 4 12.10 5.10 1 0 5 -4 9.40 4.90 -2 -2 -5 4 9.40 4.90 1 2 5 -3 -11.20 20.00 1 -2 5 3 5.10 11.10 1 -2 5 3 3.30 4.70 1 2 5 -3 11.80 4.10 1 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8.70 -2 2 5 4 -3.30 8.70 1 -4 -5 4 13.90 4.60 -2 -2 5 -4 13.90 4.60 1 4 5 -4 9.20 4.60 -2 2 -5 4 9.20 4.60 1 4 5 -4 -0.60 4.70 -2 2 -5 4 -0.60 4.70 1 2 5 5 16.70 5.80 1 -2 5 -5 7.40 5.40 1 2 -5 5 17.90 3.80 1 2 -5 5 20.90 4.70 1 5 -5 -6 -2.60 4.30 -2 2 5 6 -2.60 4.30 1 5 -5 -6 -3.30 4.00 -2 2 5 6 -3.30 4.00 1 5 5 -6 -0.70 2.00 -2 2 -5 6 -0.70 2.00 1 5 5 -6 2.10 2.40 -2 2 -5 6 2.10 2.40 1 -2 6 5 7.30 4.90 1 -2 6 5 -2.20 4.20 1 -2 -6 5 4.80 2.80 1 -2 -6 5 2.00 2.40 1 0 -6 4 7.50 5.00 -2 2 6 -4 7.50 5.00 1 0 -6 -4 10.20 6.10 -2 -2 6 4 10.20 6.10 1 0 -6 -4 10.10 3.90 -2 -2 6 4 10.10 3.90 1 0 6 -4 8.10 4.10 -2 -2 -6 4 8.10 4.10 1 0 6 -4 10.00 5.20 -2 -2 -6 4 10.00 5.20 1 -2 6 3 9.80 8.90 1 2 6 -3 11.50 6.50 1 -2 6 3 -0.80 4.50 1 2 6 -3 4.90 15.60 1 -2 -6 3 6.90 4.80 1 1 -6 2 87.99 9.80 -2 2 6 -2 87.99 9.80 1 -1 -6 -2 90.09 11.60 -2 -2 6 2 90.09 11.60 1 1 -6 2 102.29 23.40 -2 2 6 -2 102.29 23.40 1 -1 6 -2 97.19 13.30 -2 -2 -6 2 97.19 13.30 1 2 6 -1 5.70 3.70 1 2 6 -1 2.10 6.70 1 -2 6 1 18.70 6.60 1 -2 -6 1 5.00 6.10 1 2 -6 0 15.70 9.00 -2 2 6 0 15.70 9.00 1 -2 -6 0 7.90 5.30 -2 -2 6 0 7.90 5.30 1 2 -6 0 19.60 6.90 -2 2 6 0 19.60 6.90 1 2 -6 0 22.60 5.50 -2 2 6 0 22.60 5.50 1 -2 -6 0 17.40 7.40 -2 -2 6 0 17.40 7.40 1 2 6 0 21.90 9.20 -2 2 -6 0 21.90 9.20 1 -2 6 0 10.80 9.90 -2 -2 -6 0 10.80 9.90 1 -2 6 0 32.70 7.80 -2 -2 -6 0 32.70 7.80 1 2 6 1 80.59 11.60 1 -2 6 -1 85.89 13.40 1 2 6 1 88.39 13.20 1 2 6 1 99.39 9.90 1 2 -6 1 86.89 19.70 1 2 -6 1 112.89 13.40 1 -2 -6 -1 91.49 15.70 1 3 -6 -2 100.59 15.10 -2 2 6 2 100.59 15.10 1 -3 -6 2 76.29 9.60 -2 -2 6 -2 76.29 9.60 1 3 -6 -2 92.19 15.10 -2 2 6 2 92.19 15.10 1 3 -6 -2 71.49 19.10 -2 2 6 2 71.49 19.10 1 3 6 -2 95.59 15.40 -2 2 -6 2 95.59 15.40 1 2 6 3 1.70 6.40 1 2 6 3 -0.70 6.00 1 2 6 3 6.40 4.90 1 -2 6 -3 -4.50 4.90 1 2 -6 3 -4.00 4.90 1 4 -6 -4 10.70 6.40 -2 2 6 4 10.70 6.40 1 -4 -6 4 10.40 5.40 -2 -2 6 -4 10.40 5.40 1 4 -6 -4 10.30 5.20 -2 2 6 4 10.30 5.20 1 4 -6 -4 9.70 7.40 -2 2 6 4 9.70 7.40 1 4 6 -4 10.70 4.00 -2 2 -6 4 10.70 4.00 1 2 6 5 8.10 7.80 1 2 6 5 3.00 4.10 1 2 -6 5 0.70 2.30 1 0 -7 -4 3.10 4.60 -2 -2 7 4 3.10 4.60 1 0 -7 -4 0.90 3.80 -2 -2 7 4 0.90 3.80 1 0 -7 -4 6.90 3.00 -2 -2 7 4 6.90 3.00 1 0 7 -4 7.90 2.50 -2 -2 -7 4 7.90 2.50 1 -2 7 3 8.80 6.10 1 2 7 -3 -2.90 11.90 1 -2 7 3 -7.90 5.60 1 -2 7 3 2.70 4.50 1 -2 -7 3 -1.20 4.30 1 -1 -7 -2 123.09 12.30 -2 -2 7 2 123.09 12.30 1 1 -7 2 139.79 19.20 -2 2 7 -2 139.79 19.20 1 -1 -7 -2 115.69 11.00 -2 -2 7 2 115.69 11.00 1 1 -7 2 94.19 11.20 -2 2 7 -2 94.19 11.20 1 -1 7 -2 82.69 11.40 -2 -2 -7 2 82.69 11.40 1 2 7 -1 6.80 5.10 1 -2 7 1 -0.30 5.00 1 -2 7 1 -7.30 5.90 1 2 7 -1 13.30 11.30 1 -2 -7 1 8.40 5.20 1 2 -7 0 7.30 8.20 -2 2 7 0 7.30 8.20 1 -2 -7 0 6.00 5.90 -2 -2 7 0 6.00 5.90 1 2 -7 0 5.00 5.30 -2 2 7 0 5.00 5.30 1 -2 -7 0 11.50 8.20 -2 -2 7 0 11.50 8.20 1 2 -7 0 -0.70 4.90 -2 2 7 0 -0.70 4.90 1 -2 7 0 9.20 6.00 -2 -2 -7 0 9.20 6.00 1 -2 7 0 19.00 18.10 -2 -2 -7 0 19.00 18.10 1 2 7 1 62.89 9.00 1 2 7 1 57.39 10.60 1 2 -7 1 65.59 10.30 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7.60 4.20 -2 -4 -1 6 7.60 4.20 1 -1 1 -6 5.30 4.40 -2 -4 -1 6 5.30 4.40 1 -4 1 5 15.40 6.30 1 -4 1 5 9.80 5.50 1 -4 1 5 24.60 7.00 1 -4 -1 5 17.00 12.20 1 -4 -1 5 25.40 6.10 1 4 -1 -5 23.50 8.90 1 -4 -1 5 8.10 6.20 1 2 -1 4 0.90 3.10 -2 4 1 -4 0.90 3.10 1 2 -1 4 4.50 3.70 -2 4 1 -4 4.50 3.70 1 2 1 4 6.40 3.50 -2 4 -1 -4 6.40 3.50 1 4 1 -3 115.69 10.30 1 4 1 -3 119.39 9.80 1 -4 -1 3 113.99 10.40 1 4 -1 -3 115.69 10.10 1 4 -1 -3 114.49 9.50 1 -4 -1 3 119.59 10.20 1 3 -1 2 186.78 14.70 -2 4 1 -2 186.78 14.70 1 3 -1 2 166.68 14.90 -2 4 1 -2 166.68 14.90 1 -3 1 -2 195.78 15.10 -2 -4 -1 2 195.78 15.10 1 -3 1 -2 204.58 15.10 -2 -4 -1 2 204.58 15.10 1 3 1 2 186.08 14.50 -2 4 -1 -2 186.08 14.50 1 3 1 2 173.98 14.90 -2 4 -1 -2 173.98 14.90 1 4 1 -1 830.72 60.99 1 4 1 -1 699.33 61.09 1 4 -1 -1 798.32 60.79 1 -4 -1 1 855.71 61.49 1 -4 -1 1 858.51 61.39 1 4 -1 -1 688.73 60.99 1 4 -1 0 56.49 4.60 -2 4 1 0 56.49 4.60 1 -4 -1 0 61.29 4.60 -2 -4 1 0 61.29 4.60 1 -4 1 0 56.89 4.90 -2 -4 -1 0 56.89 4.90 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15.30 4.60 -2 -4 3 4 15.30 4.60 1 -2 -3 -4 8.00 7.10 -2 -4 3 4 8.00 7.10 1 -2 3 -4 4.00 7.50 -2 -4 -3 4 4.00 7.50 1 -2 3 -4 1.10 5.80 -2 -4 -3 4 1.10 5.80 1 2 3 4 144.19 73.99 -2 4 -3 -4 144.19 73.99 1 4 3 -3 84.59 9.00 1 4 3 -3 96.39 8.40 1 4 3 -3 99.29 8.60 1 4 -3 -3 73.89 9.00 1 3 -3 2 239.78 18.80 -2 4 3 -2 239.78 18.80 1 3 -3 2 252.17 19.30 -2 4 3 -2 252.17 19.30 1 -3 3 -2 228.88 19.60 -2 -4 -3 2 228.88 19.60 1 3 3 2 200.78 18.80 -2 4 -3 -2 200.78 18.80 1 -3 3 -2 255.07 20.00 -2 -4 -3 2 255.07 20.00 1 4 3 -1 71.99 6.40 1 4 3 -1 71.09 6.10 1 4 -3 -1 75.99 7.30 1 -4 -3 1 62.39 6.90 1 -4 -3 1 74.89 7.30 1 4 -3 0 225.98 17.50 -2 4 3 0 225.98 17.50 1 4 -3 0 206.28 17.70 -2 4 3 0 206.28 17.70 1 -4 -3 0 218.48 17.70 -2 -4 3 0 218.48 17.70 1 -4 -3 0 212.68 17.20 -2 -4 3 0 212.68 17.20 1 -4 3 0 204.68 18.20 -2 -4 -3 0 204.68 18.20 1 -4 3 0 241.58 17.40 -2 -4 -3 0 241.58 17.40 1 4 3 0 231.88 18.80 -2 4 -3 0 231.88 18.80 1 -4 3 0 222.68 18.60 -2 -4 -3 0 222.68 18.60 1 -4 3 -1 4.60 1.80 1 -4 3 -1 5.60 1.30 1 4 3 1 4.20 1.70 1 -4 -3 -1 2.70 3.10 1 -4 -3 -1 8.40 2.90 1 4 -3 1 8.50 3.40 1 -5 -3 2 1854.41 143.49 -2 -4 3 -2 1854.41 143.49 1 5 -3 -2 1693.03 143.89 -2 4 3 2 1693.03 143.89 1 -5 3 2 1929.91 145.29 -2 -4 -3 -2 1929.91 145.29 1 -5 3 2 1940.71 143.69 -2 -4 -3 -2 1940.71 143.69 1 -4 3 -3 311.57 24.40 1 4 3 3 319.27 24.60 1 -4 -3 -3 273.67 24.50 1 6 -3 -4 330.87 28.10 -2 4 3 4 330.87 28.10 1 6 3 -4 351.16 27.50 -2 4 -3 4 351.16 27.50 1 6 3 -4 291.57 27.50 -2 4 -3 4 291.57 27.50 1 4 3 5 4.50 5.00 1 -4 3 -5 8.90 4.40 1 4 3 5 10.60 5.40 1 4 3 5 15.60 10.50 1 4 -3 5 14.10 5.00 1 4 -3 5 7.20 4.30 1 -4 -3 -5 5.50 6.20 1 4 -3 5 21.80 8.70 1 7 -3 -6 0.20 4.50 -2 4 3 6 0.20 4.50 1 -7 -3 6 8.20 8.30 -2 -4 3 -6 8.20 8.30 1 7 -3 -6 6.00 4.00 -2 4 3 6 6.00 4.00 1 7 -3 -6 0.60 8.80 -2 4 3 6 0.60 8.80 1 7 3 -6 6.90 4.50 -2 4 -3 6 6.90 4.50 1 7 3 -6 4.10 3.10 -2 4 -3 6 4.10 3.10 1 7 3 -6 9.60 4.20 -2 4 -3 6 9.60 4.20 1 4 3 7 6.80 3.30 1 -4 3 -7 8.00 4.60 1 -1 -4 -6 8.50 3.30 -2 -4 4 6 8.50 3.30 1 -1 -4 -6 6.80 6.30 -2 -4 4 6 6.80 6.30 1 -1 4 -6 3.80 2.70 -2 -4 -4 6 3.80 2.70 1 -1 4 -6 9.00 2.40 -2 -4 -4 6 9.00 2.40 1 4 4 -5 22.30 5.80 1 -4 4 5 12.10 8.30 1 -4 4 5 18.00 5.30 1 -4 4 5 6.20 4.10 1 -4 -4 5 11.00 4.20 1 -4 -4 5 7.00 4.50 1 -2 -4 -4 19.50 4.70 -2 -4 4 4 19.50 4.70 1 2 -4 4 18.10 5.20 -2 4 4 -4 18.10 5.20 1 -2 -4 -4 19.30 6.80 -2 -4 4 4 19.30 6.80 1 -2 4 -4 26.90 6.90 -2 -4 -4 4 26.90 6.90 1 -2 4 -4 15.30 6.00 -2 -4 -4 4 15.30 6.00 1 4 4 -3 4.70 4.10 1 4 4 -3 6.90 6.90 1 3 -4 2 607.34 47.50 -2 4 4 -2 607.34 47.50 1 3 -4 2 611.24 48.10 -2 4 4 -2 611.24 48.10 1 -3 4 -2 590.34 52.09 -2 -4 -4 2 590.34 52.09 1 4 4 -1 76.89 7.00 1 4 4 -1 86.19 7.20 1 -4 -4 1 73.39 9.50 1 -4 -4 1 76.89 8.80 1 4 -4 -1 56.39 12.30 1 4 -4 0 607.04 51.59 -2 4 4 0 607.04 51.59 1 4 -4 0 644.44 51.09 -2 4 4 0 644.44 51.09 1 -4 4 0 684.63 52.99 -2 -4 -4 0 684.63 52.99 1 -4 4 0 642.14 52.89 -2 -4 -4 0 642.14 52.89 1 4 4 0 707.13 52.99 -2 4 -4 0 707.13 52.99 1 4 4 1 35.80 4.00 1 -4 4 -1 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6 0.50 2.00 1 -4 5 5 17.60 6.50 1 -4 5 5 10.00 4.70 1 4 5 -5 11.20 6.30 1 -4 5 5 14.40 4.70 1 -4 -5 5 5.80 4.20 1 -4 -5 5 13.00 3.70 1 -2 -5 -4 5.70 4.00 -2 -4 5 4 5.70 4.00 1 2 -5 4 4.20 5.00 -2 4 5 -4 4.20 5.00 1 -2 -5 -4 -3.70 8.30 -2 -4 5 4 -3.70 8.30 1 -2 -5 -4 -11.60 8.10 -2 -4 5 4 -11.60 8.10 1 -2 5 -4 6.40 5.20 -2 -4 -5 4 6.40 5.20 1 -2 5 -4 2.20 4.70 -2 -4 -5 4 2.20 4.70 1 4 5 -3 157.18 26.90 1 -4 5 3 94.29 11.70 1 4 5 -3 141.39 12.00 1 -4 5 3 133.59 18.10 1 -4 -5 3 117.79 13.00 1 -4 -5 3 84.59 12.50 1 3 -5 2 27.60 18.50 -2 4 5 -2 27.60 18.50 1 -3 -5 -2 22.60 13.60 -2 -4 5 2 22.60 13.60 1 3 -5 2 38.90 5.80 -2 4 5 -2 38.90 5.80 1 -3 -5 -2 39.80 8.90 -2 -4 5 2 39.80 8.90 1 3 -5 2 41.50 7.40 -2 4 5 -2 41.50 7.40 1 -3 5 -2 43.30 9.20 -2 -4 -5 2 43.30 9.20 1 -3 5 -2 31.60 9.10 -2 -4 -5 2 31.60 9.10 1 4 5 -1 24.00 4.10 1 4 5 -1 29.50 5.10 1 -4 -5 1 16.40 7.10 1 -4 -5 1 25.30 10.10 1 4 -5 0 28.80 4.50 -2 4 5 0 28.80 4.50 1 -4 -5 0 35.30 4.90 -2 -4 5 0 35.30 4.90 1 4 5 0 42.80 9.70 -2 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1.10 5.00 1 4 -7 0 6.30 5.00 -2 4 7 0 6.30 5.00 1 -4 -7 0 4.50 5.80 -2 -4 7 0 4.50 5.80 1 -4 -7 0 3.90 10.10 -2 -4 7 0 3.90 10.10 1 4 -7 0 2.80 7.60 -2 4 7 0 2.80 7.60 1 -4 7 0 6.30 5.50 -2 -4 -7 0 6.30 5.50 1 4 7 1 1.80 4.90 1 4 7 1 4.00 6.40 1 -4 -7 -1 4.60 5.90 1 5 -7 -2 1.10 4.50 -2 4 7 2 1.10 4.50 1 5 -7 -2 14.50 8.00 -2 4 7 2 14.50 8.00 1 5 -7 -2 12.30 6.10 -2 4 7 2 12.30 6.10 1 -5 -7 2 -17.00 12.60 -2 -4 7 -2 -17.00 12.60 1 5 7 -2 10.40 5.20 -2 4 -7 2 10.40 5.20 1 4 7 3 32.90 7.00 1 4 -7 3 44.70 5.70 1 6 -7 -4 2.80 4.50 -2 4 7 4 2.80 4.50 1 6 -7 -4 1.30 4.10 -2 4 7 4 1.30 4.10 1 6 7 -4 5.10 2.40 -2 4 -7 4 5.10 2.40 1 -4 8 3 6.70 3.60 1 -4 8 3 0.90 2.10 1 -4 -8 3 4.60 2.30 1 -3 -8 -2 38.80 5.70 -2 -4 8 2 38.80 5.70 1 -3 -8 -2 43.90 5.10 -2 -4 8 2 43.90 5.10 1 3 -8 2 62.49 10.00 -2 4 8 -2 62.49 10.00 1 -3 8 -2 51.39 5.30 -2 -4 -8 2 51.39 5.30 1 -4 8 1 4.50 5.20 1 4 8 -1 7.30 7.00 1 -4 8 1 7.60 3.10 1 -4 -8 1 5.30 3.70 1 4 -8 0 44.40 9.30 -2 4 8 0 44.40 9.30 1 4 -8 0 37.50 8.00 -2 4 8 0 37.50 8.00 1 -4 8 0 33.80 6.30 -2 -4 -8 0 33.80 6.30 1 4 8 1 0.10 5.00 1 -4 8 -1 -1.10 8.20 1 4 8 1 1.20 7.10 1 5 -8 -2 132.19 13.60 -2 4 8 2 132.19 13.60 1 5 -8 -2 134.09 12.10 -2 4 8 2 134.09 12.10 1 4 8 3 0.90 3.60 1 -5 0 7 2.80 2.40 1 -5 0 7 -2.10 3.90 1 -2 0 -6 15.50 5.00 -2 -5 0 6 15.50 5.00 1 -2 0 -6 15.80 5.00 -2 -5 0 6 15.80 5.00 1 -2 0 -6 20.70 6.20 -2 -5 0 6 20.70 6.20 1 -5 0 5 -9.00 6.10 1 -5 0 5 -0.40 7.00 1 -5 0 5 -1.90 6.20 1 3 0 4 218.98 18.70 -2 5 0 -4 218.98 18.70 1 3 0 4 218.88 18.00 -2 5 0 -4 218.88 18.00 1 5 0 -3 2.40 1.90 1 5 0 -3 -0.40 1.50 1 -5 0 3 2.20 3.00 1 4 0 2 320.27 22.50 -2 5 0 -2 320.27 22.50 1 -4 0 -2 286.07 23.90 -2 -5 0 2 286.07 23.90 1 4 0 2 244.98 22.00 -2 5 0 -2 244.98 22.00 1 5 0 -1 1.10 0.60 1 -5 0 1 1.60 1.20 1 5 0 -1 0.30 0.40 1 -5 0 0 110.29 8.50 -2 -5 0 0 110.29 8.50 1 -5 0 0 105.69 8.80 -2 -5 0 0 105.69 8.80 1 5 0 0 101.39 8.80 -2 5 0 0 101.39 8.80 1 -5 0 0 113.89 8.80 -2 -5 0 0 113.89 8.80 1 -5 0 -1 0.80 0.50 1 5 0 1 1.00 1.00 1 -5 0 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1.60 4.30 1 5 6 -3 -7.00 4.20 1 -5 6 3 0.40 7.80 1 -5 -6 3 -0.90 4.80 1 4 -6 2 678.03 62.69 -2 5 6 -2 678.03 62.69 1 -4 -6 -2 721.43 55.29 -2 -5 6 2 721.43 55.29 1 4 -6 2 651.03 54.99 -2 5 6 -2 651.03 54.99 1 -4 6 -2 740.13 56.09 -2 -5 -6 2 740.13 56.09 1 -4 6 -2 636.24 59.79 -2 -5 -6 2 636.24 59.79 1 5 6 -1 2.90 3.80 1 -5 6 1 9.50 6.70 1 5 6 -1 -11.20 11.20 1 -5 -6 1 10.50 6.10 1 -5 -6 1 -5.30 10.30 1 5 -6 0 177.78 19.90 -2 5 6 0 177.78 19.90 1 5 -6 0 201.08 18.60 -2 5 6 0 201.08 18.60 1 5 -6 0 231.78 22.40 -2 5 6 0 231.78 22.40 1 -5 6 0 249.88 20.50 -2 -5 -6 0 249.88 20.50 1 -5 6 0 235.98 24.00 -2 -5 -6 0 235.98 24.00 1 -5 6 -1 5.40 5.40 1 5 6 1 19.30 6.40 1 5 6 1 6.70 8.50 1 5 6 1 16.90 4.70 1 -5 -6 -1 20.90 10.10 1 -5 -6 -1 4.70 6.70 1 6 -6 -2 123.79 14.80 -2 5 6 2 123.79 14.80 1 6 -6 -2 145.59 14.80 -2 5 6 2 145.59 14.80 1 -6 -6 2 155.28 14.60 -2 -5 6 -2 155.28 14.60 1 6 6 -2 168.18 16.10 -2 5 -6 2 168.18 16.10 1 -6 6 2 155.18 16.70 -2 -5 -6 -2 155.18 16.70 1 -6 6 2 187.78 21.80 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7 1 33.30 8.50 1 -5 -7 -1 54.29 8.90 1 -6 -7 2 16.00 16.90 -2 -5 7 -2 16.00 16.90 1 6 -7 -2 8.50 9.20 -2 5 7 2 8.50 9.20 1 6 -7 -2 -4.30 6.30 -2 5 7 2 -4.30 6.30 1 6 7 -2 3.30 5.50 -2 5 -7 2 3.30 5.50 1 5 7 3 43.10 7.20 1 7 -7 -4 -2.00 4.40 -2 5 7 4 -2.00 4.40 1 7 -7 -4 12.60 4.60 -2 5 7 4 12.60 4.60 1 7 7 -4 5.20 2.50 -2 5 -7 4 5.20 2.50 1 5 8 -3 20.20 10.60 1 -5 8 3 -4.70 3.70 1 -5 8 3 1.40 2.20 1 -5 -8 3 2.50 2.20 1 -4 -8 -2 114.49 9.90 -2 -5 8 2 114.49 9.90 1 -4 -8 -2 117.19 10.50 -2 -5 8 2 117.19 10.50 1 4 -8 2 102.49 12.80 -2 5 8 -2 102.49 12.80 1 -4 8 -2 117.79 10.10 -2 -5 -8 2 117.79 10.10 1 -5 8 1 8.80 3.20 1 -5 8 1 4.70 5.30 1 5 8 -1 22.50 6.90 1 -5 -8 1 12.80 3.80 1 5 -8 0 39.00 9.70 -2 5 8 0 39.00 9.70 1 5 -8 0 38.40 7.50 -2 5 8 0 38.40 7.50 1 -5 8 0 38.30 6.10 -2 -5 -8 0 38.30 6.10 1 5 8 1 11.40 6.90 1 -5 8 -1 10.10 8.50 1 5 8 1 5.40 5.00 1 6 -8 -2 25.70 5.30 -2 5 8 2 25.70 5.30 1 6 -8 -2 28.80 8.30 -2 5 8 2 28.80 8.30 1 5 8 3 4.70 3.50 1 -6 0 7 8.50 3.90 1 -6 0 7 0.40 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7.10 5.00 1 -4 -1 -6 -6.20 4.30 -2 -7 1 6 -6.20 4.30 1 -4 1 -6 4.20 3.90 -2 -7 -1 6 4.20 3.90 1 -4 1 -6 -0.80 4.30 -2 -7 -1 6 -0.80 4.30 1 -4 1 -6 12.80 6.50 -2 -7 -1 6 12.80 6.50 1 -7 1 5 36.40 6.80 1 -7 1 5 28.90 7.20 1 -7 1 5 52.19 8.60 1 -7 -1 5 37.80 8.40 1 7 -1 -5 165.88 86.49 1 -7 -1 5 37.40 7.90 1 -7 -1 5 32.00 8.40 1 5 -1 4 77.69 7.80 -2 7 1 -4 77.69 7.80 1 5 -1 4 81.99 9.10 -2 7 1 -4 81.99 9.10 1 -5 -1 -4 62.99 13.00 -2 -7 1 4 62.99 13.00 1 5 1 4 70.89 8.60 -2 7 -1 -4 70.89 8.60 1 7 1 -3 33.50 3.80 1 -7 1 3 31.60 6.60 1 7 1 -3 34.60 4.60 1 7 1 -3 30.70 4.20 1 7 -1 -3 33.90 3.80 1 7 -1 -3 30.50 4.20 1 -7 -1 3 43.80 5.60 1 -7 -1 3 36.20 5.20 1 6 -1 2 88.99 7.50 -2 7 1 -2 88.99 7.50 1 -6 -1 -2 103.79 9.10 -2 -7 1 2 103.79 9.10 1 6 -1 2 103.79 7.90 -2 7 1 -2 103.79 7.90 1 6 -1 2 81.29 7.70 -2 7 1 -2 81.29 7.70 1 6 1 2 84.39 7.20 -2 7 -1 -2 84.39 7.20 1 -6 1 -2 82.39 7.90 -2 -7 -1 2 82.39 7.90 1 6 1 2 104.79 7.90 -2 7 -1 -2 104.79 7.90 1 -6 1 -2 80.29 8.20 -2 -7 -1 2 80.29 8.20 1 7 1 -1 2574.64 209.48 1 -7 1 1 2601.94 209.18 1 -7 -1 1 2893.01 210.08 1 -7 -1 1 2784.12 209.98 1 -7 -1 0 187.78 14.70 -2 -7 1 0 187.78 14.70 1 7 -1 0 174.68 14.20 -2 7 1 0 174.68 14.20 1 -7 1 0 177.68 14.50 -2 -7 -1 0 177.68 14.50 1 -7 1 0 180.28 14.60 -2 -7 -1 0 180.28 14.60 1 -7 1 -1 1962.30 152.48 1 -7 1 -1 2013.20 152.48 1 7 1 1 2184.18 152.88 1 -7 1 -1 1661.83 152.48 1 -7 -1 -1 1848.12 152.68 1 -7 -1 -1 2028.60 152.78 1 -7 -1 -1 2118.79 152.88 1 -8 -1 2 69.89 6.20 -2 -7 1 -2 69.89 6.20 1 -8 -1 2 76.89 6.40 -2 -7 1 -2 76.89 6.40 1 -8 1 2 72.39 6.50 -2 -7 -1 -2 72.39 6.50 1 -8 1 2 64.29 6.60 -2 -7 -1 -2 64.29 6.60 1 -8 1 2 74.59 7.50 -2 -7 -1 -2 74.59 7.50 1 -7 1 -3 136.49 12.60 1 -7 1 -3 145.09 12.40 1 7 1 3 155.68 12.80 1 -7 -1 -3 155.18 12.60 1 -7 -1 -3 149.69 12.70 1 -9 -1 4 65.09 8.70 -2 -7 1 -4 65.09 8.70 1 -9 -1 4 55.49 7.60 -2 -7 1 -4 55.49 7.60 1 -9 1 4 75.09 7.90 -2 -7 -1 -4 75.09 7.90 1 -9 1 4 73.29 9.00 -2 -7 -1 -4 73.29 9.00 1 7 1 5 137.89 14.10 1 7 1 5 158.18 14.50 1 7 1 5 142.89 14.90 1 7 -1 5 143.09 13.60 1 -7 -1 -5 126.39 16.30 1 7 -1 5 146.49 14.60 1 7 -1 5 169.38 14.40 1 10 -1 -6 37.50 7.50 -2 7 1 6 37.50 7.50 1 10 -1 -6 35.10 6.40 -2 7 1 6 35.10 6.40 1 10 -1 -6 45.80 6.20 -2 7 1 6 45.80 6.20 1 10 1 -6 48.50 7.20 -2 7 -1 6 48.50 7.20 1 -10 1 6 28.10 6.60 -2 -7 -1 -6 28.10 6.60 1 10 1 -6 36.70 5.60 -2 7 -1 6 36.70 5.60 1 -7 1 -7 7.10 4.10 1 7 1 7 6.90 2.50 1 7 1 7 18.50 5.20 1 7 -1 7 7.20 2.30 1 -7 -1 -7 13.80 4.20 1 -7 2 7 2.50 2.90 1 -7 2 7 9.90 2.80 1 -7 -2 7 4.10 2.30 1 -7 -2 7 4.20 2.30 1 -4 -2 -6 13.80 4.40 -2 -7 2 6 13.80 4.40 1 -4 -2 -6 28.10 12.00 -2 -7 2 6 28.10 12.00 1 -4 -2 -6 15.30 4.90 -2 -7 2 6 15.30 4.90 1 -4 2 -6 8.30 4.30 -2 -7 -2 6 8.30 4.30 1 -4 2 -6 18.40 4.40 -2 -7 -2 6 18.40 4.40 1 -7 2 5 32.30 6.60 1 -7 2 5 42.10 9.00 1 -7 2 5 37.30 7.90 1 -7 -2 5 57.69 8.00 1 7 -2 -5 55.09 84.79 1 -7 -2 5 58.39 8.90 1 -5 -2 -4 18.40 10.70 -2 -7 2 4 18.40 10.70 1 5 -2 4 2.40 5.00 -2 7 2 -4 2.40 5.00 1 5 -2 4 4.30 4.00 -2 7 2 -4 4.30 4.00 1 5 -2 4 12.30 4.10 -2 7 2 -4 12.30 4.10 1 5 2 4 12.70 5.10 -2 7 -2 -4 12.70 5.10 1 7 2 -3 223.48 18.20 1 7 2 -3 215.28 17.40 1 7 2 -3 185.88 17.50 1 -7 -2 3 214.58 17.70 1 -7 -2 3 211.68 18.10 1 6 -2 2 50.29 4.40 -2 7 2 -2 50.29 4.40 1 6 -2 2 43.40 4.60 -2 7 2 -2 43.40 4.60 1 -6 2 -2 48.20 5.20 -2 -7 -2 2 48.20 5.20 1 -6 2 -2 49.50 5.50 -2 -7 -2 2 49.50 5.50 1 7 2 -1 1194.78 90.49 1 7 2 -1 1101.09 90.09 1 -7 -2 1 1162.48 90.79 1 -7 -2 1 1194.68 90.79 1 7 -2 0 523.15 41.00 -2 7 2 0 523.15 41.00 1 -7 -2 0 572.34 40.80 -2 -7 2 0 572.34 40.80 1 7 -2 0 516.85 41.30 -2 7 2 0 516.85 41.30 1 -7 2 0 508.65 41.60 -2 -7 -2 0 508.65 41.60 1 -7 2 0 511.95 41.60 -2 -7 -2 0 511.95 41.60 1 -7 2 -1 345.47 27.60 1 -7 2 -1 357.96 27.80 1 7 2 1 366.36 28.10 1 -7 -2 -1 355.16 28.50 1 -7 -2 -1 353.46 28.60 1 -7 -2 -1 350.16 28.10 1 -8 -2 2 385.06 31.80 -2 -7 2 -2 385.06 31.80 1 -8 -2 2 413.06 31.80 -2 -7 2 -2 413.06 31.80 1 -8 2 2 436.16 32.10 -2 -7 -2 -2 436.16 32.10 1 -8 2 2 377.96 32.80 -2 -7 -2 -2 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6 -13.10 7.80 1 -4 -3 -6 11.00 3.90 -2 -7 3 6 11.00 3.90 1 -4 3 -6 8.90 4.80 -2 -7 -3 6 8.90 4.80 1 -4 3 -6 2.50 3.10 -2 -7 -3 6 2.50 3.10 1 7 3 -5 0.90 6.30 1 -7 3 5 -1.50 5.20 1 -7 3 5 3.80 3.60 1 -7 -3 5 5.70 5.30 1 -7 -3 5 -2.50 5.10 1 -7 -3 5 -0.90 4.40 1 -5 -3 -4 141.99 13.60 -2 -7 3 4 141.99 13.60 1 5 -3 4 134.59 14.00 -2 7 3 -4 134.59 14.00 1 -5 -3 -4 159.98 15.20 -2 -7 3 4 159.98 15.20 1 5 3 4 129.99 83.99 -2 7 -3 -4 129.99 83.99 1 -5 3 -4 145.79 14.30 -2 -7 -3 4 145.79 14.30 1 -5 3 -4 168.48 15.70 -2 -7 -3 4 168.48 15.70 1 5 3 4 144.19 38.90 -2 7 -3 -4 144.19 38.90 1 -5 3 -4 121.39 16.30 -2 -7 -3 4 121.39 16.30 1 7 3 -3 609.94 45.30 1 7 3 -3 582.84 44.90 1 -7 -3 3 559.04 46.60 1 -7 -3 3 513.95 46.20 1 6 -3 2 87.69 7.60 -2 7 3 -2 87.69 7.60 1 6 -3 2 82.99 7.90 -2 7 3 -2 82.99 7.90 1 -6 3 -2 86.69 8.50 -2 -7 -3 2 86.69 8.50 1 -6 3 -2 87.29 9.30 -2 -7 -3 2 87.29 9.30 1 7 3 -1 232.58 17.90 1 7 3 -1 210.78 17.50 1 -7 -3 1 220.18 18.70 1 -7 -3 1 210.68 18.20 1 -7 -3 0 128.59 9.80 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95.89 9.60 1 10 3 -6 111.39 9.50 -2 7 -3 6 111.39 9.50 1 -10 3 6 103.99 10.50 -2 -7 -3 -6 103.99 10.50 1 -4 -4 -6 27.60 6.80 -2 -7 4 6 27.60 6.80 1 -4 4 -6 24.80 6.00 -2 -7 -4 6 24.80 6.00 1 -4 4 -6 26.40 3.50 -2 -7 -4 6 26.40 3.50 1 -7 4 5 24.40 5.30 1 -7 4 5 30.30 5.80 1 -7 -4 5 32.40 6.40 1 -7 -4 5 24.20 5.20 1 -5 -4 -4 3.70 6.50 -2 -7 4 4 3.70 6.50 1 5 -4 4 1.30 21.20 -2 7 4 -4 1.30 21.20 1 5 -4 4 3.90 4.70 -2 7 4 -4 3.90 4.70 1 -5 4 -4 -4.40 6.50 -2 -7 -4 4 -4.40 6.50 1 5 4 4 113.39 72.19 -2 7 -4 -4 113.39 72.19 1 -5 4 -4 12.00 4.80 -2 -7 -4 4 12.00 4.80 1 7 4 -3 117.69 10.90 1 -7 4 3 97.99 11.40 1 7 4 -3 116.89 28.10 1 -7 -4 3 105.79 13.80 1 7 -4 -3 115.69 80.99 1 7 -4 -3 175.28 34.20 1 -7 -4 3 97.49 15.20 1 -7 -4 3 105.29 12.00 1 6 -4 2 33.20 4.80 -2 7 4 -2 33.20 4.80 1 6 -4 2 28.80 3.90 -2 7 4 -2 28.80 3.90 1 -6 4 -2 25.10 7.40 -2 -7 -4 2 25.10 7.40 1 -6 4 -2 36.10 7.50 -2 -7 -4 2 36.10 7.50 1 7 4 -1 368.76 28.90 1 7 4 -1 366.66 28.60 1 -7 -4 1 354.86 30.70 1 -7 -4 1 341.67 30.20 1 7 -4 0 199.18 17.20 -2 7 4 0 199.18 17.20 1 -7 4 0 219.38 19.50 -2 -7 -4 0 219.38 19.50 1 -7 4 0 210.18 18.70 -2 -7 -4 0 210.18 18.70 1 -7 4 -1 158.88 13.10 1 7 4 1 159.68 13.00 1 -7 -4 -1 148.19 15.20 1 -7 -4 -1 143.49 15.50 1 8 -4 -2 10.10 3.10 -2 7 4 2 10.10 3.10 1 -8 -4 2 9.00 3.10 -2 -7 4 -2 9.00 3.10 1 -8 -4 2 6.70 4.50 -2 -7 4 -2 6.70 4.50 1 -8 4 2 11.20 7.20 -2 -7 -4 -2 11.20 7.20 1 7 4 3 15.70 4.60 1 7 4 3 3.00 8.70 1 -7 4 -3 8.30 3.90 1 7 4 3 25.00 12.30 1 7 4 3 -8.20 10.70 1 -7 -4 -3 0.00 10.80 1 7 -4 3 10.20 6.60 1 -7 -4 -3 7.30 6.70 1 9 -4 -4 382.16 37.40 -2 7 4 4 382.16 37.40 1 9 -4 -4 318.47 33.50 -2 7 4 4 318.47 33.50 1 9 4 -4 348.07 30.90 -2 7 -4 4 348.07 30.90 1 7 4 5 21.20 8.20 1 -7 4 -5 15.10 5.50 1 7 4 5 16.80 5.60 1 7 -4 5 11.60 4.10 1 7 -4 5 13.80 4.10 1 10 -4 -6 52.39 5.90 -2 7 4 6 52.39 5.90 1 10 -4 -6 49.20 9.00 -2 7 4 6 49.20 9.00 1 10 4 -6 55.39 5.30 -2 7 -4 6 55.39 5.30 1 10 4 -6 58.29 5.40 -2 7 -4 6 58.29 5.40 1 -4 -5 -6 2.70 3.50 -2 -7 5 6 2.70 3.50 1 -4 -5 -6 4.60 3.40 -2 -7 5 6 4.60 3.40 1 -4 5 -6 0.80 3.10 -2 -7 -5 6 0.80 3.10 1 -4 5 -6 3.30 1.80 -2 -7 -5 6 3.30 1.80 1 -7 5 5 26.00 3.80 1 -7 5 5 16.80 4.50 1 -7 5 5 25.80 8.50 1 -7 -5 5 20.70 4.70 1 -7 -5 5 16.20 3.80 1 -5 -5 -4 23.10 4.50 -2 -7 5 4 23.10 4.50 1 5 -5 4 3.50 17.90 -2 7 5 -4 3.50 17.90 1 5 -5 4 20.20 5.60 -2 7 5 -4 20.20 5.60 1 -5 -5 -4 29.10 9.20 -2 -7 5 4 29.10 9.20 1 -5 5 -4 14.60 5.60 -2 -7 -5 4 14.60 5.60 1 -5 5 -4 22.50 5.20 -2 -7 -5 4 22.50 5.20 1 -7 5 3 587.04 47.80 1 7 5 -3 598.34 56.49 1 -7 -5 3 577.24 48.90 1 -7 -5 3 617.54 48.20 1 6 -5 2 11.50 3.70 -2 7 5 -2 11.50 3.70 1 6 -5 2 0.50 16.40 -2 7 5 -2 0.50 16.40 1 -6 -5 -2 16.70 6.70 -2 -7 5 2 16.70 6.70 1 -6 5 -2 4.30 8.50 -2 -7 -5 2 4.30 8.50 1 -6 5 -2 17.20 6.30 -2 -7 -5 2 17.20 6.30 1 -6 5 -2 9.80 7.40 -2 -7 -5 2 9.80 7.40 1 7 5 -1 16.80 4.20 1 7 5 -1 8.80 3.30 1 7 5 -1 18.60 16.50 1 -7 -5 1 -2.70 6.90 1 -7 -5 1 14.20 9.70 1 -7 5 0 10.60 9.70 -2 -7 -5 0 10.60 9.70 1 -7 5 0 18.20 7.10 -2 -7 -5 0 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-6 2 19.30 5.80 -2 -7 6 -2 19.30 5.80 1 8 -6 -2 23.40 8.30 -2 7 6 2 23.40 8.30 1 8 -6 -2 19.50 8.40 -2 7 6 2 19.50 8.40 1 8 6 -2 15.50 6.90 -2 7 -6 2 15.50 6.90 1 -8 6 2 10.60 13.30 -2 -7 -6 -2 10.60 13.30 1 -8 6 2 20.80 6.30 -2 -7 -6 -2 20.80 6.30 1 7 6 3 3.30 7.80 1 7 6 3 3.40 7.10 1 -7 6 -3 4.60 5.70 1 7 -6 3 6.60 4.80 1 9 -6 -4 170.28 17.20 -2 7 6 4 170.28 17.20 1 9 6 -4 171.38 14.70 -2 7 -6 4 171.38 14.70 1 7 6 5 3.40 4.50 1 7 6 5 -9.10 29.50 1 7 -6 5 3.30 2.00 1 -5 -7 -4 5.00 2.30 -2 -7 7 4 5.00 2.30 1 -5 -7 -4 11.00 4.70 -2 -7 7 4 11.00 4.70 1 -5 -7 -4 4.40 3.00 -2 -7 7 4 4.40 3.00 1 -5 7 -4 4.60 2.60 -2 -7 -7 4 4.60 2.60 1 7 7 -3 207.08 20.60 1 -7 7 3 190.28 16.80 1 -7 -7 3 211.38 17.50 1 6 -7 2 -7.30 10.00 -2 7 7 -2 -7.30 10.00 1 6 -7 2 -1.40 4.80 -2 7 7 -2 -1.40 4.80 1 -6 -7 -2 3.40 4.50 -2 -7 7 2 3.40 4.50 1 -6 7 -2 -9.90 4.70 -2 -7 -7 2 -9.90 4.70 1 -7 7 1 2.10 5.30 1 7 7 -1 20.30 11.00 1 7 7 -1 9.40 5.10 1 7 7 -1 21.70 9.30 1 -7 -7 1 4.70 4.90 1 7 -7 0 12.80 5.40 -2 7 7 0 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5.80 -2 7 8 0 3.30 5.80 1 -7 8 0 11.60 3.60 -2 -7 -8 0 11.60 3.60 1 7 8 1 15.10 6.70 1 -7 8 -1 8.20 8.50 1 7 8 1 10.90 5.00 1 -7 -8 -1 9.40 4.90 1 8 -8 -2 17.60 7.20 -2 7 8 2 17.60 7.20 1 -8 0 7 1.40 2.40 1 -8 0 7 7.40 3.80 1 -5 0 -6 23.40 6.00 -2 -8 0 6 23.40 6.00 1 -5 0 -6 22.20 5.20 -2 -8 0 6 22.20 5.20 1 -8 0 5 3.30 4.30 1 -8 0 5 -3.30 6.60 1 -8 0 5 -1.20 5.70 1 6 0 4 432.26 32.60 -2 8 0 -4 432.26 32.60 1 -6 0 -4 375.36 33.50 -2 -8 0 4 375.36 33.50 1 -6 0 -4 375.86 33.70 -2 -8 0 4 375.86 33.70 1 -8 0 3 4.70 3.60 1 -8 0 3 1.90 3.40 1 8 0 -3 0.60 1.70 1 8 0 -3 2.60 2.20 1 7 0 2 1472.45 110.99 -2 8 0 -2 1472.45 110.99 1 -7 0 -2 1377.26 111.79 -2 -8 0 2 1377.26 111.79 1 7 0 2 1447.46 111.19 -2 8 0 -2 1447.46 111.19 1 -8 0 1 -1.10 1.80 1 8 0 -1 0.30 0.60 1 -8 0 0 1623.14 122.99 -2 -8 0 0 1623.14 122.99 1 -8 0 0 1549.14 123.09 -2 -8 0 0 1549.14 123.09 1 -8 0 -1 -0.20 0.90 1 -8 0 -1 -0.20 1.50 1 8 0 1 3.70 1.50 1 -8 0 -1 -2.50 1.10 1 9 0 -2 471.05 37.30 -2 8 0 2 471.05 37.30 1 -8 0 -3 2.50 2.20 1 -8 0 -3 -3.90 2.20 1 -10 0 4 678.83 53.79 -2 -8 0 -4 678.83 53.79 1 8 0 5 2.10 5.00 1 8 0 5 -2.00 4.30 1 8 0 5 -2.80 9.50 1 -11 0 6 317.67 27.40 -2 -8 0 -6 317.67 27.40 1 11 0 -6 312.97 25.70 -2 8 0 6 312.97 25.70 1 11 0 -6 292.47 26.90 -2 8 0 6 292.47 26.90 1 8 0 7 5.60 2.40 1 -8 0 -7 -2.40 3.70 1 8 0 7 6.00 2.40 1 -8 1 7 -1.00 2.40 1 -8 1 7 5.80 2.90 1 -8 -1 7 -6.10 4.30 1 -8 -1 7 6.80 2.30 1 -5 -1 -6 1.30 4.80 -2 -8 1 6 1.30 4.80 1 -5 -1 -6 -6.90 4.00 -2 -8 1 6 -6.90 4.00 1 -5 1 -6 4.70 3.90 -2 -8 -1 6 4.70 3.90 1 -5 1 -6 -1.50 3.80 -2 -8 -1 6 -1.50 3.80 1 -5 1 -6 8.20 6.30 -2 -8 -1 6 8.20 6.30 1 -8 1 5 365.56 27.20 1 -8 1 5 307.27 28.10 1 -8 1 5 303.77 28.20 1 -8 -1 5 342.57 28.50 1 -8 -1 5 316.97 27.70 1 -8 -1 5 315.47 28.30 1 -6 -1 -4 89.79 13.10 -2 -8 1 4 89.79 13.10 1 6 -1 4 71.69 8.00 -2 8 1 -4 71.69 8.00 1 6 -1 4 81.79 9.70 -2 8 1 -4 81.79 9.70 1 6 1 4 75.79 9.20 -2 8 -1 -4 75.79 9.20 1 -6 1 -4 63.69 11.40 -2 -8 -1 4 63.69 11.40 1 8 1 -3 43.70 5.00 1 -8 1 3 32.00 7.20 1 8 1 -3 48.40 4.50 1 8 1 -3 41.30 5.30 1 8 -1 -3 43.50 5.30 1 -8 -1 3 48.90 6.40 1 -8 -1 3 41.30 5.70 1 7 -1 2 84.29 6.90 -2 8 1 -2 84.29 6.90 1 7 -1 2 80.89 7.20 -2 8 1 -2 80.89 7.20 1 -7 -1 -2 73.79 8.30 -2 -8 1 2 73.79 8.30 1 7 -1 2 77.39 7.30 -2 8 1 -2 77.39 7.30 1 7 1 2 91.59 6.50 -2 8 -1 -2 91.59 6.50 1 -7 1 -2 73.09 7.50 -2 -8 -1 2 73.09 7.50 1 -7 1 -2 83.39 7.60 -2 -8 -1 2 83.39 7.60 1 7 1 2 82.79 7.30 -2 8 -1 -2 82.79 7.30 1 8 1 -1 463.35 33.20 1 -8 1 1 393.26 32.90 1 -8 -1 1 426.96 33.70 1 -8 -1 1 416.46 33.70 1 8 -1 0 268.57 22.10 -2 8 1 0 268.57 22.10 1 -8 -1 0 324.47 22.70 -2 -8 1 0 324.47 22.70 1 -8 1 0 286.67 22.40 -2 -8 -1 0 286.67 22.40 1 -8 1 0 239.28 23.20 -2 -8 -1 0 239.28 23.20 1 8 1 1 695.93 49.99 1 -8 1 -1 662.03 49.70 1 -8 1 -1 564.34 49.60 1 -8 -1 -1 649.54 49.80 1 -8 -1 -1 614.04 49.80 1 -8 -1 -1 638.04 49.90 1 9 -1 -2 224.68 19.30 -2 8 1 2 224.68 19.30 1 -9 -1 2 238.18 18.10 -2 -8 1 -2 238.18 18.10 1 -9 -1 2 239.08 18.20 -2 -8 1 -2 239.08 18.20 1 -9 1 2 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5.30 1 -8 2 5 17.30 6.00 1 -8 2 5 18.70 5.90 1 -8 2 5 14.30 4.10 1 8 -2 -5 48.40 104.39 1 -8 -2 5 19.10 5.60 1 -8 -2 5 19.00 6.20 1 6 -2 4 241.58 19.50 -2 8 2 -4 241.58 19.50 1 -6 -2 -4 201.38 21.40 -2 -8 2 4 201.38 21.40 1 6 -2 4 188.38 17.90 -2 8 2 -4 188.38 17.90 1 -6 -2 -4 202.58 23.30 -2 -8 2 4 202.58 23.30 1 6 -2 4 209.08 18.20 -2 8 2 -4 209.08 18.20 1 6 2 4 249.78 91.49 -2 8 -2 -4 249.78 91.49 1 6 2 4 226.18 19.30 -2 8 -2 -4 226.18 19.30 1 8 2 -3 8.40 2.40 1 -8 2 3 7.90 7.30 1 8 -2 -3 7.90 3.20 1 -8 -2 3 8.60 4.20 1 -8 -2 3 13.50 3.80 1 7 -2 2 461.65 37.70 -2 8 2 -2 461.65 37.70 1 7 -2 2 460.95 37.90 -2 8 2 -2 460.95 37.90 1 7 2 2 496.65 37.90 -2 8 -2 -2 496.65 37.90 1 -7 2 -2 498.45 38.50 -2 -8 -2 2 498.45 38.50 1 -7 2 -2 486.55 38.40 -2 -8 -2 2 486.55 38.40 1 8 2 -1 187.78 15.40 1 8 2 -1 197.28 15.70 1 -8 -2 1 198.18 16.20 1 -8 -2 1 191.18 16.00 1 8 -2 0 759.22 59.59 -2 8 2 0 759.22 59.59 1 -8 -2 0 845.82 59.39 -2 -8 2 0 845.82 59.39 1 8 -2 0 735.23 59.89 -2 8 2 0 735.23 59.89 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1.00 2.40 1 -16 6 3 0.70 4.00 1 16 6 -3 7.20 8.00 1 -16 6 3 1.20 3.30 1 -16 -6 3 0.80 3.20 1 16 -6 -3 48.80 53.79 1 15 -6 2 48.70 8.60 -2 16 6 -2 48.70 8.60 1 15 -6 2 68.39 16.10 -2 16 6 -2 68.39 16.10 1 -15 6 -2 53.09 8.60 -2 -16 -6 2 53.09 8.60 1 16 6 -1 2.20 4.90 1 16 6 -1 -7.90 11.90 1 16 6 -1 -6.10 7.10 1 -16 -6 1 -3.80 5.10 1 -16 -6 1 -4.60 4.80 1 16 -6 0 2.50 8.20 -2 16 6 0 2.50 8.20 1 16 -6 0 16.30 13.90 -2 16 6 0 16.30 13.90 1 16 -6 0 3.90 5.10 -2 16 6 0 3.90 5.10 1 16 -6 0 -4.20 12.00 -2 16 6 0 -4.20 12.00 1 -16 6 0 4.60 5.40 -2 -16 -6 0 4.60 5.40 1 -16 6 0 11.50 4.90 -2 -16 -6 0 11.50 4.90 1 16 6 1 -9.40 7.80 1 16 6 1 4.40 5.60 1 -16 -6 -1 0.50 4.50 1 17 -6 -2 141.49 16.80 -2 16 6 2 141.49 16.80 1 17 -6 -2 136.99 14.20 -2 16 6 2 136.99 14.20 1 -17 6 2 146.59 13.30 -2 -16 -6 -2 146.59 13.30 1 16 6 3 0.20 6.50 1 16 6 3 2.60 6.80 1 -16 -6 -3 4.70 3.20 1 18 -6 -4 11.70 4.90 -2 16 6 4 11.70 4.90 1 -18 6 4 12.40 3.10 -2 -16 -6 -4 12.40 3.10 1 -16 7 3 30.50 3.80 1 16 7 -3 22.20 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15 0 4 43.10 19.90 -2 17 0 -4 43.10 19.90 1 -17 0 3 -5.60 5.60 1 17 0 -3 -8.30 20.40 1 -17 0 3 0.00 6.50 1 17 0 -3 -5.10 12.70 1 -16 0 -2 24.40 5.90 -2 -17 0 2 24.40 5.90 1 -16 0 -2 21.00 7.10 -2 -17 0 2 21.00 7.10 1 -17 0 1 3.40 4.40 1 -17 0 1 -1.80 5.30 1 -17 0 0 147.39 15.70 -2 -17 0 0 147.39 15.70 1 -17 0 -1 1.10 3.90 1 17 0 1 0.20 3.30 1 -18 0 2 77.89 9.70 -2 -17 0 -2 77.89 9.70 1 17 0 3 -21.80 69.79 1 17 0 3 2.80 7.10 1 17 0 3 0.40 4.90 1 17 0 3 3.40 9.90 1 19 0 -4 119.39 12.60 -2 17 0 4 119.39 12.60 1 19 0 -4 142.69 14.00 -2 17 0 4 142.69 14.00 1 19 0 -4 135.49 16.50 -2 17 0 4 135.49 16.50 1 17 0 5 -16.80 64.19 1 17 0 5 6.80 3.50 1 -17 0 -5 6.00 10.80 1 17 0 5 5.70 7.50 1 -20 0 6 7.30 3.80 -2 -17 0 -6 7.30 3.80 1 20 0 -6 4.10 2.80 -2 17 0 6 4.10 2.80 1 -14 -1 -6 9.40 2.60 -2 -17 1 6 9.40 2.60 1 14 -1 6 -4.00 17.10 -2 17 1 -6 -4.00 17.10 1 -14 -1 -6 7.10 3.10 -2 -17 1 6 7.10 3.10 1 -14 1 -6 9.50 4.10 -2 -17 -1 6 9.50 4.10 1 -14 1 -6 8.80 2.90 -2 -17 -1 6 8.80 2.90 1 14 1 6 36.40 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-2 42.70 13.50 1 -26 2 -2 26.50 4.90 -2 -27 -2 2 26.50 4.90 1 26 2 2 142.79 68.89 -2 27 -2 -2 142.79 68.89 1 -26 2 -2 22.80 4.70 -2 -27 -2 2 22.80 4.70 1 26 2 2 13.80 15.10 -2 27 -2 -2 13.80 15.10 1 27 -2 -1 152.98 74.49 1 27 -2 0 -42.30 67.39 -2 27 2 0 -42.30 67.39 1 27 -2 0 10.50 12.20 -2 27 2 0 10.50 12.20 1 27 2 1 -12.40 67.99 1 27 2 1 -17.10 15.70 1 27 2 1 -5.40 6.40 1 27 -2 1 118.89 73.19 1 -27 -2 -1 4.10 4.40 1 28 -2 -2 10.30 4.40 -2 27 2 2 10.30 4.40 1 28 -2 -2 9.70 10.20 -2 27 2 2 9.70 10.20 1 28 -2 -2 -22.10 45.30 -2 27 2 2 -22.10 45.30 1 -28 2 2 12.00 5.50 -2 -27 -2 -2 12.00 5.50 1 -28 2 2 9.60 4.10 -2 -27 -2 -2 9.60 4.10 1 28 2 -2 22.60 47.50 -2 27 -2 2 22.60 47.50 1 27 2 3 15.50 3.80 1 27 2 3 4.80 33.70 1 -27 -2 -3 14.00 4.00 1 -27 -2 -3 16.40 3.20 1 27 3 -3 17.30 6.70 1 -27 3 3 4.70 3.50 1 27 3 -3 11.80 9.60 1 -27 -3 3 8.80 2.60 1 -27 -3 3 6.70 2.90 1 -27 -3 3 13.60 2.70 1 26 -3 2 53.09 15.30 -2 27 3 -2 53.09 15.30 1 26 -3 2 45.80 8.90 -2 27 3 -2 45.80 8.90 1 26 -3 2 69.69 10.60 -2 27 3 -2 69.69 10.60 1 -26 3 -2 45.10 5.90 -2 -27 -3 2 45.10 5.90 1 -26 3 -2 53.79 5.40 -2 -27 -3 2 53.79 5.40 1 27 3 -1 9.70 7.60 1 27 -3 0 37.40 87.59 -2 27 3 0 37.40 87.59 1 27 3 0 110.29 51.49 -2 27 -3 0 110.29 51.49 1 27 3 1 18.40 5.10 1 27 3 1 37.30 10.40 1 27 3 1 21.50 7.80 1 27 3 1 87.39 54.19 1 27 -3 1 -41.00 51.99 1 28 -3 -2 26.30 4.90 -2 27 3 2 26.30 4.90 1 28 -3 -2 -24.70 39.80 -2 27 3 2 -24.70 39.80 1 28 -3 -2 30.00 8.50 -2 27 3 2 30.00 8.50 1 -28 3 2 26.40 5.60 -2 -27 -3 -2 26.40 5.60 1 27 3 3 4.60 3.80 1 27 3 3 1.80 29.00 1 -27 -3 -3 12.20 2.60 1 -27 -3 -3 7.60 3.10 1 27 4 -3 11.20 8.60 1 27 4 -3 -2.40 5.80 1 -27 -4 3 2.70 2.50 1 -27 -4 3 2.60 2.10 1 26 -4 2 27.00 10.50 -2 27 4 -2 27.00 10.50 1 26 -4 2 32.50 6.40 -2 27 4 -2 32.50 6.40 1 -26 4 -2 22.40 3.40 -2 -27 -4 2 22.40 3.40 1 -26 4 -2 20.80 3.10 -2 -27 -4 2 20.80 3.10 1 26 4 2 -32.50 34.30 -2 27 -4 -2 -32.50 34.30 1 27 4 -1 22.20 7.40 1 27 4 -1 12.40 6.00 1 -27 -4 1 17.50 3.40 1 27 -4 0 7.30 7.30 -2 27 4 0 7.30 7.30 1 -27 4 0 16.70 3.50 -2 -27 -4 0 16.70 3.50 1 -27 4 0 17.50 3.30 -2 -27 -4 0 17.50 3.30 1 27 4 0 11.70 49.50 -2 27 -4 0 11.70 49.50 1 27 4 1 8.90 6.90 1 27 4 1 12.20 8.00 1 -27 -4 -1 2.70 4.60 1 28 -4 -2 14.20 6.70 -2 27 4 2 14.20 6.70 1 -28 4 2 9.70 3.60 -2 -27 -4 -2 9.70 3.60 1 -28 4 2 7.80 2.20 -2 -27 -4 -2 7.80 2.20 1 27 -5 0 12.20 6.70 -2 27 5 0 12.20 6.70 1 27 -5 0 5.50 5.50 -2 27 5 0 5.50 5.50 1 -27 5 0 4.40 2.00 -2 -27 -5 0 4.40 2.00 1 -26 0 -4 14.00 2.50 -2 -28 0 4 14.00 2.50 1 26 0 4 20.80 8.80 -2 28 0 -4 20.80 8.80 1 -26 0 -4 7.30 3.10 -2 -28 0 4 7.30 3.10 1 28 0 -3 -6.40 6.20 1 -28 0 3 4.00 2.60 1 28 0 -3 3.80 11.30 1 27 0 2 12.10 8.10 -2 28 0 -2 12.10 8.10 1 -27 0 -2 14.50 4.00 -2 -28 0 2 14.50 4.00 1 27 0 2 94.59 51.89 -2 28 0 -2 94.59 51.89 1 27 0 2 25.50 15.40 -2 28 0 -2 25.50 15.40 1 28 0 -1 130.09 71.19 1 28 0 0 6.40 12.30 -2 28 0 0 6.40 12.30 1 28 0 0 23.00 14.40 -2 28 0 0 23.00 14.40 1 28 0 0 28.20 59.19 -2 28 0 0 28.20 59.19 1 28 0 1 -39.00 63.29 1 28 0 1 13.80 13.50 1 29 0 -2 20.90 43.20 -2 28 0 2 20.90 43.20 1 28 0 3 -5.20 34.00 1 26 -1 4 5.10 5.80 -2 28 1 -4 5.10 5.80 1 -26 -1 -4 6.60 2.30 -2 -28 1 4 6.60 2.30 1 26 -1 4 15.60 8.80 -2 28 1 -4 15.60 8.80 1 26 1 4 -1.70 10.40 -2 28 -1 -4 -1.70 10.40 1 -26 1 -4 3.30 2.30 -2 -28 -1 4 3.30 2.30 1 26 1 4 48.50 39.70 -2 28 -1 -4 48.50 39.70 1 -26 1 -4 3.70 2.60 -2 -28 -1 4 3.70 2.60 1 -28 1 3 14.40 3.40 1 28 1 -3 -0.70 11.00 1 28 1 -3 -2.90 5.80 1 28 -1 -3 7.60 6.30 1 28 -1 -3 13.50 11.30 1 -28 -1 3 2.90 2.50 1 27 -1 2 13.90 14.20 -2 28 1 -2 13.90 14.20 1 -27 -1 -2 18.00 6.20 -2 -28 1 2 18.00 6.20 1 27 -1 2 -29.60 52.29 -2 28 1 -2 -29.60 52.29 1 27 -1 2 20.10 7.50 -2 28 1 -2 20.10 7.50 1 27 1 2 10.00 15.40 -2 28 -1 -2 10.00 15.40 1 27 1 2 17.90 8.40 -2 28 -1 -2 17.90 8.40 1 -27 1 -2 10.60 3.60 -2 -28 -1 2 10.60 3.60 1 28 1 -1 81.59 76.19 1 28 1 -1 15.60 13.90 1 28 -1 -1 31.60 11.50 1 28 -1 -1 119.39 65.69 1 28 -1 0 73.19 72.09 -2 28 1 0 73.19 72.09 1 28 1 0 140.29 52.89 -2 28 -1 0 140.29 52.89 1 28 1 1 45.00 70.09 1 28 1 1 21.10 10.80 1 -28 -1 -1 13.10 5.30 1 28 -1 1 25.50 55.29 1 29 -1 -2 11.50 4.70 -2 28 1 2 11.50 4.70 1 29 -1 -2 5.20 44.00 -2 28 1 2 5.20 44.00 1 29 -1 -2 12.30 12.10 -2 28 1 2 12.30 12.10 1 29 1 -2 57.89 44.70 -2 28 -1 2 57.89 44.70 1 -29 1 2 10.90 4.80 -2 -28 -1 -2 10.90 4.80 1 28 1 3 -30.00 32.20 1 -28 -1 -3 5.20 3.40 1 28 -1 3 -13.90 37.10 1 -28 2 3 9.70 4.10 1 28 2 -3 31.40 10.20 1 28 2 -3 15.80 6.20 1 -28 -2 3 15.00 3.00 1 28 -2 -3 16.20 10.90 1 -28 -2 3 6.50 3.80 1 27 -2 2 9.20 8.20 -2 28 2 -2 9.20 8.20 1 27 -2 2 15.80 7.00 -2 28 2 -2 15.80 7.00 1 27 -2 2 22.20 13.50 -2 28 2 -2 22.20 13.50 1 -27 2 -2 7.60 3.70 -2 -28 -2 2 7.60 3.70 1 -27 2 -2 8.40 2.90 -2 -28 -2 2 8.40 2.90 1 27 2 2 5.20 14.40 -2 28 -2 -2 5.20 14.40 1 28 2 -1 24.60 8.40 1 28 2 -1 15.10 8.30 1 -28 -2 1 15.90 3.50 1 -28 -2 1 15.70 4.00 1 28 -2 0 43.40 59.09 -2 28 2 0 43.40 59.09 1 28 2 1 45.70 48.70 1 28 2 1 13.80 4.50 1 28 2 1 4.80 8.40 1 -28 -2 -1 9.40 3.90 1 28 -2 1 31.60 48.50 1 29 -2 -2 4.30 4.00 -2 28 2 2 4.30 4.00 1 29 -2 -2 12.60 8.90 -2 28 2 2 12.60 8.90 1 29 -2 -2 -6.60 39.90 -2 28 2 2 -6.60 39.90 1 -29 2 2 7.50 3.40 -2 -28 -2 -2 7.50 3.40 1 29 2 -2 23.90 41.20 -2 28 -2 2 23.90 41.20 1 28 2 3 2.70 28.40 1 28 2 3 5.30 3.40 1 -28 -2 -3 5.70 2.50 1 28 3 -3 8.90 9.20 1 28 3 -3 17.70 6.10 1 -28 3 3 22.10 3.60 1 -28 -3 3 16.10 3.50 1 -28 -3 3 14.80 3.40 1 -28 -3 3 12.30 3.00 1 27 -3 2 56.49 15.60 -2 28 3 -2 56.49 15.60 1 27 -3 2 43.80 7.30 -2 28 3 -2 43.80 7.30 1 27 -3 2 33.00 9.40 -2 28 3 -2 33.00 9.40 1 -27 3 -2 40.70 4.10 -2 -28 -3 2 40.70 4.10 1 -27 3 -2 27.70 4.50 -2 -28 -3 2 27.70 4.50 1 28 3 -1 35.80 7.60 1 28 3 -1 36.30 8.20 1 -28 -3 1 28.30 4.50 1 -28 -3 1 27.00 4.20 1 28 -3 0 18.00 8.50 -2 28 3 0 18.00 8.50 1 28 -3 0 28.80 7.90 -2 28 3 0 28.80 7.90 1 -28 3 0 19.60 4.10 -2 -28 -3 0 19.60 4.10 1 28 3 0 -15.80 45.00 -2 28 -3 0 -15.80 45.00 1 28 3 1 -25.50 49.99 1 28 -3 1 -38.00 44.10 1 29 -3 -2 35.20 42.70 -2 28 3 2 35.20 42.70 1 29 -3 -2 24.50 5.10 -2 28 3 2 24.50 5.10 1 -29 3 2 19.90 5.30 -2 -28 -3 -2 19.90 5.30 1 -29 3 2 27.90 3.50 -2 -28 -3 -2 27.90 3.50 1 27 -4 2 13.50 6.10 -2 28 4 -2 13.50 6.10 1 27 4 2 -40.70 31.60 -2 28 -4 -2 -40.70 31.60 1 -27 4 -2 3.70 2.40 -2 -28 -4 2 3.70 2.40 1 28 4 -1 9.20 6.10 1 28 4 -1 12.80 7.40 1 -28 -4 1 17.20 3.10 1 -28 -4 1 10.90 2.30 1 28 -4 0 38.10 7.60 -2 28 4 0 38.10 7.60 1 28 4 0 136.49 65.29 -2 28 -4 0 136.49 65.29 1 28 4 1 10.30 13.00 1 28 4 1 8.50 6.20 1 -28 -4 -1 8.00 3.00 1 -29 0 3 7.90 3.10 1 -29 0 3 5.00 2.40 1 29 0 -3 -16.00 10.80 1 29 0 -3 -1.20 6.10 1 29 0 0 45.60 47.90 -2 29 0 0 45.60 47.90 1 29 0 0 48.00 13.50 -2 29 0 0 48.00 13.50 1 29 0 1 11.00 42.30 1 29 0 1 19.80 12.70 1 30 0 -2 -31.80 38.40 -2 29 0 2 -31.80 38.40 1 29 0 3 27.20 30.30 1 29 1 -3 -2.20 10.20 1 -29 1 3 4.90 2.60 1 29 1 -3 -1.50 6.10 1 -29 -1 3 5.60 2.70 1 29 -1 -3 4.00 10.60 1 -29 -1 3 0.20 2.20 1 28 -1 2 40.30 14.30 -2 29 1 -2 40.30 14.30 1 28 -1 2 21.80 7.10 -2 29 1 -2 21.80 7.10 1 28 -1 2 -19.40 53.39 -2 29 1 -2 -19.40 53.39 1 28 1 2 23.20 8.00 -2 29 -1 -2 23.20 8.00 1 29 1 -1 73.79 50.39 1 29 1 -1 13.60 8.80 1 -29 -1 1 9.70 4.60 1 29 -1 -1 25.90 10.50 1 29 -1 0 58.39 13.20 -2 29 1 0 58.39 13.20 1 29 -1 0 25.30 52.79 -2 29 1 0 25.30 52.79 1 29 1 0 113.79 46.20 -2 29 -1 0 113.79 46.20 1 29 1 1 21.30 9.90 1 29 1 1 1.40 45.10 1 29 -1 1 30.70 41.00 1 30 -1 -2 33.90 14.50 -2 29 1 2 33.90 14.50 1 30 -1 -2 24.70 36.30 -2 29 1 2 24.70 36.30 1 30 1 -2 39.60 37.50 -2 29 -1 2 39.60 37.50 1 29 1 3 20.80 26.10 1 -29 2 3 5.70 2.90 1 29 2 -3 -2.40 5.00 1 29 2 -3 -2.30 9.70 1 29 -2 -3 8.40 10.30 1 -29 -2 3 4.10 1.90 1 -29 -2 3 2.40 2.40 1 29 2 -1 21.90 7.90 1 29 2 -1 23.40 7.90 1 29 2 -1 -64.29 56.99 1 -29 -2 1 21.60 4.70 1 -29 -2 1 29.90 4.40 1 29 -2 0 106.29 52.39 -2 29 2 0 106.29 52.39 1 29 2 1 23.50 8.20 1 29 2 1 -20.10 40.60 1 30 -2 -2 45.90 8.40 -2 29 2 2 45.90 8.40 1 30 -2 -2 9.70 33.70 -2 29 2 2 9.70 33.70 1 -30 2 2 38.70 4.80 -2 -29 -2 -2 38.70 4.80 1 30 2 -2 25.60 41.80 -2 29 -2 2 25.60 41.80 1 28 -3 2 23.50 6.30 -2 29 3 -2 23.50 6.30 1 28 3 2 62.39 30.40 -2 29 -3 -2 62.39 30.40 1 -28 3 -2 25.30 3.10 -2 -29 -3 2 25.30 3.10 1 29 -3 0 34.50 7.70 -2 29 3 0 34.50 7.70 1 29 -3 0 39.60 8.80 -2 29 3 0 39.60 8.80 1 29 3 0 51.69 36.80 -2 29 -3 0 51.69 36.80 1 -29 3 0 22.70 3.80 -2 -29 -3 0 22.70 3.80 1 29 3 1 -27.20 37.60 1 29 3 1 13.70 6.60 1 30 -3 -2 40.10 7.40 -2 29 3 2 40.10 7.40 1 30 -3 -2 25.10 31.60 -2 29 3 2 25.10 31.60 1 -30 3 2 54.29 4.60 -2 -29 -3 -2 54.29 4.60 1 29 4 -1 8.10 6.70 1 29 4 -1 0.70 4.70 1 -29 -4 1 10.80 2.40 1 -29 -4 1 6.60 2.20 1 29 -4 -1 35.20 36.50 1 29 -4 0 6.60 6.60 -2 29 4 0 6.60 6.60 1 29 -4 0 17.30 6.50 -2 29 4 0 17.30 6.50 1 -29 4 0 16.00 2.80 -2 -29 -4 0 16.00 2.80 1 -29 4 0 13.70 2.70 -2 -29 -4 0 13.70 2.70 1 30 0 -3 11.40 41.20 1 -30 0 3 5.40 3.10 1 30 0 -3 4.50 5.70 1 30 0 -3 14.50 10.20 1 29 0 2 68.49 9.70 -2 30 0 -2 68.49 9.70 1 29 0 2 75.79 42.60 -2 30 0 -2 75.79 42.60 1 -29 0 -2 76.09 6.90 -2 -30 0 2 76.09 6.90 1 30 0 0 75.39 43.40 -2 30 0 0 75.39 43.40 1 30 0 1 28.90 37.80 1 31 0 -2 21.50 30.60 -2 30 0 2 21.50 30.60 1 30 1 -3 54.49 11.80 1 -30 1 3 33.30 3.60 1 -30 -1 3 31.80 3.80 1 30 -1 -3 18.20 10.60 1 -30 -1 3 30.50 3.70 1 -29 -1 -2 19.40 4.40 -2 -30 1 2 19.40 4.40 1 29 -1 2 30.10 6.90 -2 30 1 -2 30.10 6.90 1 -29 1 -2 24.70 3.90 -2 -30 -1 2 24.70 3.90 1 30 1 -1 46.20 40.60 1 30 -1 0 60.09 42.40 -2 30 1 0 60.09 42.40 1 30 1 1 2.20 38.10 1 30 1 1 20.10 9.50 1 30 -1 1 89.49 37.20 1 -30 -1 -1 32.10 5.40 1 31 -1 -2 20.10 28.50 -2 30 1 2 20.10 28.50 1 -31 1 2 8.40 3.20 -2 -30 -1 -2 8.40 3.20 1 31 1 -2 -9.20 32.20 -2 30 -1 2 -9.20 32.20 1 29 -2 2 43.10 7.50 -2 30 2 -2 43.10 7.50 1 -29 2 -2 33.00 5.10 -2 -30 -2 2 33.00 5.10 1 -29 2 -2 46.10 4.30 -2 -30 -2 2 46.10 4.30 1 30 2 -1 6.60 7.00 1 30 2 -1 -85.39 70.09 1 30 2 -1 10.10 6.90 1 -30 -2 1 9.40 3.30 1 30 -2 0 -3.00 38.70 -2 30 2 0 -3.00 38.70 1 30 -2 0 35.50 9.40 -2 30 2 0 35.50 9.40 1 30 2 1 -28.30 33.80 1 30 2 1 11.80 7.90 1 30 -2 1 41.60 33.20 1 -30 -2 -1 14.30 3.40 1 31 -2 -2 13.90 27.80 -2 30 2 2 13.90 27.80 1 31 -2 -2 12.80 8.80 -2 30 2 2 12.80 8.80 1 29 -3 2 47.60 6.80 -2 30 3 -2 47.60 6.80 1 -29 3 -2 51.39 4.30 -2 -30 -3 2 51.39 4.30 1 -29 3 -2 42.20 4.80 -2 -30 -3 2 42.20 4.80 1 30 -3 0 17.80 7.70 -2 30 3 0 17.80 7.70 1 30 -3 0 29.80 7.40 -2 30 3 0 29.80 7.40 1 -30 3 0 16.10 3.00 -2 -30 -3 0 16.10 3.00 1 30 3 0 63.99 31.80 -2 30 -3 0 63.99 31.80 1 -30 3 0 15.00 3.50 -2 -30 -3 0 15.00 3.50 1 30 3 1 6.50 5.70 1 -30 -3 -1 9.30 2.20 1 -30 0 -2 22.30 3.70 -2 -31 0 2 22.30 3.70 1 -30 0 -2 24.40 3.90 -2 -31 0 2 24.40 3.90 1 30 0 2 65.59 40.50 -2 31 0 -2 65.59 40.50 1 30 0 2 31.60 6.80 -2 31 0 -2 31.60 6.80 1 31 0 0 145.79 35.00 -2 31 0 0 145.79 35.00 1 31 0 1 72.79 33.40 1 32 0 -2 12.80 26.50 -2 31 0 2 12.80 26.50 1 -30 -1 -2 13.00 3.40 -2 -31 1 2 13.00 3.40 1 30 -1 2 -0.60 6.00 -2 31 1 -2 -0.60 6.00 1 30 1 2 56.79 30.20 -2 31 -1 -2 56.79 30.20 1 31 1 -1 50.09 37.70 1 31 -1 0 88.79 33.60 -2 31 1 0 88.79 33.60 1 31 1 1 24.00 31.60 1 31 1 1 14.30 8.30 1 -31 -1 -1 9.50 3.10 1 30 -2 2 7.80 5.30 -2 31 2 -2 7.80 5.30 1 30 2 2 40.20 25.50 -2 31 -2 -2 40.20 25.50 1 -30 2 -2 3.10 2.00 -2 -31 -2 2 3.10 2.00 1 -31 -2 -1 1.10 2.40 1 31 -2 1 -1.70 30.00 1 -31 0 -2 142.49 11.50 -2 -32 0 2 142.49 11.50 1 32 0 -1 116.29 33.10 1 32 0 0 96.29 26.00 -2 32 0 0 96.29 26.00 1 32 0 1 66.89 27.60 1 32 1 -1 38.80 7.30 1 32 1 -1 -32.40 39.80 1 -32 -1 1 19.90 3.30 1 32 -1 0 54.79 31.40 -2 32 1 0 54.79 31.40 1 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 72060 loop_ _space_group_symop_operation_xyz 'x, y, z' 'x, -y, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.1092(3) 0.7473(11) 0.5354(13) 0.051(2) Uani 1 1 d . . . . . C2 C 0.1172(3) 0.6612(11) 0.3394(13) 0.056(2) Uani 1 1 d . . . . . H2 H 0.090735 0.601545 0.262738 0.068 Uiso 1 1 calc R U . . . C3 C 0.1646(3) 0.6655(11) 0.2611(13) 0.056(2) Uani 1 1 d . . . . . H3 H 0.169748 0.610181 0.128844 0.068 Uiso 1 1 calc R U . . . C4 C 0.2048(3) 0.7494(11) 0.3725(15) 0.0533(19) Uani 1 1 d . . . . . C5 C 0.1963(3) 0.8313(12) 0.5710(14) 0.060(2) Uani 1 1 d . . . . . H5 H 0.222984 0.887222 0.649932 0.072 Uiso 1 1 calc R U . . . C6 C 0.1488(3) 0.8304(13) 0.6516(14) 0.056(2) Uani 1 1 d . . . . . H6 H 0.143558 0.885737 0.783684 0.067 Uiso 1 1 calc R U . . . C7 C 0.2534(4) 0.7582(12) 0.2800(15) 0.058(2) Uani 1 1 d . . . . . C8 C 0.2916(4) 0.7684(12) 0.1893(17) 0.060(2) Uani 1 1 d . . . . . C9 C 0.3373(3) 0.7629(13) 0.0736(15) 0.056(2) Uani 1 1 d . . . . . C10 C 0.3345(4) 0.7017(12) -0.1416(16) 0.061(2) Uani 1 1 d . . . . . H10 H 0.303149 0.676466 -0.210747 0.073 Uiso 1 1 calc R U . . . C11 C 0.3780(3) 0.6789(12) -0.2507(13) 0.058(2) Uani 1 1 d . . . . . H11 H 0.375843 0.636789 -0.392415 0.069 Uiso 1 1 calc R U . . . C12 C 0.4244(3) 0.7178(12) -0.1522(12) 0.054(2) Uani 1 1 d . . . . . C13 C 0.4283(3) 0.7798(11) 0.0632(13) 0.0506(19) Uani 1 1 d . . . . . C14 C 0.3839(3) 0.8053(10) 0.1704(13) 0.051(2) Uani 1 1 d . . . . . H14 H 0.385805 0.852113 0.310185 0.061 Uiso 1 1 calc R U . . . C15 C 0.4772(3) 0.8016(12) 0.1817(13) 0.054(2) Uani 1 1 d . . . . . H15 H 0.478245 0.837987 0.325505 0.064 Uiso 1 1 calc R U . . . C16 C 0.5649(3) 0.7661(10) 0.2121(13) 0.0486(19) Uani 1 1 d . . . . . C17 C 0.5696(3) 0.6863(11) 0.4172(13) 0.054(2) Uani 1 1 d . . . . . H17 H 0.541123 0.639719 0.479153 0.065 Uiso 1 1 calc R U . . . C18 C 0.6160(3) 0.6755(12) 0.5289(13) 0.056(2) Uani 1 1 d . . . . . H18 H 0.618470 0.621420 0.664980 0.067 Uiso 1 1 calc R U . . . C19 C 0.6593(4) 0.7451(13) 0.4394(17) 0.056(2) Uani 1 1 d . . . . . C20 C 0.6545(3) 0.8198(11) 0.2313(13) 0.055(2) Uani 1 1 d . . . . . H20 H 0.683000 0.864643 0.167855 0.066 Uiso 1 1 calc R U . . . C21 C 0.6086(3) 0.8279(11) 0.1201(13) 0.052(2) Uani 1 1 d . . . . . H21 H 0.606495 0.875336 -0.019393 0.062 Uiso 1 1 calc R U . . . C22 C 0.7074(4) 0.7440(11) 0.5589(17) 0.059(2) Uani 1 1 d . . . . . C23 C 0.7465(4) 0.7493(11) 0.6626(16) 0.057(2) Uani 1 1 d . . . . . C24 C 0.7951(3) 0.7540(12) 0.7754(15) 0.054(2) Uani 1 1 d . . . . . C25 C 0.8040(3) 0.6722(12) 0.9751(15) 0.059(2) Uani 1 1 d . . . . . H25 H 0.777221 0.617676 1.041958 0.071 Uiso 1 1 calc R U . . . C26 C 0.8518(3) 0.6691(12) 1.0783(15) 0.059(2) Uani 1 1 d . . . . . H26 H 0.857142 0.611058 1.211360 0.071 Uiso 1 1 calc R U . . . C27 C 0.8914(3) 0.7534(12) 0.9811(14) 0.054(2) Uani 1 1 d . . . . . C28 C 0.8831(3) 0.8366(11) 0.7823(13) 0.058(2) Uani 1 1 d . . . . . H28 H 0.909863 0.893563 0.717527 0.070 Uiso 1 1 calc R U . . . C29 C 0.8363(3) 0.8365(12) 0.6797(13) 0.055(2) Uani 1 1 d . . . . . H29 H 0.831532 0.891724 0.544774 0.066 Uiso 1 1 calc R U . . . C30 C 0.9517(5) 0.6672(15) 1.2655(18) 0.090(3) Uani 1 1 d . . . . . H30A H 0.986905 0.683637 1.307186 0.135 Uiso 1 1 calc R U . . . H30B H 0.931550 0.717117 1.375197 0.135 Uiso 1 1 calc R U . . . H30C H 0.944597 0.537500 1.247849 0.135 Uiso 1 1 calc R U . . . C31 C 0.0483(4) 0.8323(17) 0.7895(19) 0.089(3) Uani 1 1 d . . . . . H31A H 0.013304 0.813356 0.814876 0.134 Uiso 1 1 calc R U . . . H31B H 0.068905 0.785812 0.909927 0.134 Uiso 1 1 calc R U . . . H31C H 0.054646 0.962285 0.772467 0.134 Uiso 1 1 calc R U . . . N1 N 0.5185(3) 0.7716(10) 0.0914(12) 0.0532(18) Uani 1 1 d . . . . . O1 O 0.0605(2) 0.7365(8) 0.5986(11) 0.0661(17) Uani 1 1 d . . . . . O2 O 0.4670(2) 0.6901(9) -0.2613(9) 0.0692(17) Uani 1 1 d . . . . . H2A H 0.491916 0.718605 -0.183907 0.104 Uiso 1 1 calc R U . . . O3 O 0.9401(2) 0.7608(8) 1.0673(11) 0.0666(17) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.044(5) 0.056(5) 0.054(5) 0.007(4) 0.006(4) 0.004(4) C2 0.047(5) 0.063(5) 0.058(5) -0.005(4) -0.004(4) -0.006(4) C3 0.050(5) 0.063(5) 0.056(4) -0.002(4) 0.002(4) 0.001(4) C4 0.044(5) 0.057(5) 0.059(5) 0.006(4) -0.003(4) 0.004(4) C5 0.052(5) 0.060(5) 0.067(5) -0.009(4) -0.006(4) 0.002(4) C6 0.040(5) 0.071(6) 0.055(5) -0.009(4) 0.000(3) 0.001(4) C7 0.045(5) 0.062(6) 0.066(5) 0.006(4) -0.003(4) 0.007(4) C8 0.043(5) 0.063(5) 0.074(6) 0.007(5) 0.002(4) 0.001(4) C9 0.045(5) 0.055(5) 0.066(5) 0.002(4) 0.001(4) 0.002(4) C10 0.042(5) 0.075(6) 0.065(5) 0.002(4) -0.008(4) -0.003(4) C11 0.053(5) 0.067(5) 0.051(4) 0.001(4) -0.010(4) -0.008(4) C12 0.052(6) 0.065(5) 0.046(4) 0.007(4) 0.001(4) 0.000(4) C13 0.043(5) 0.055(5) 0.053(4) 0.002(4) -0.002(4) 0.001(4) C14 0.046(5) 0.057(5) 0.051(4) 0.000(4) 0.000(4) 0.004(4) C15 0.046(5) 0.064(5) 0.051(4) -0.004(4) 0.002(4) -0.004(3) C16 0.047(5) 0.047(5) 0.051(4) -0.001(4) -0.002(4) 0.000(4) C17 0.047(5) 0.061(5) 0.055(4) 0.001(4) 0.007(4) -0.005(4) C18 0.053(6) 0.058(5) 0.056(5) 0.004(4) 0.001(4) -0.004(4) C19 0.051(5) 0.053(5) 0.064(5) -0.002(4) -0.002(4) 0.006(4) C20 0.045(5) 0.058(5) 0.061(5) 0.003(4) 0.006(4) -0.007(3) C21 0.048(5) 0.057(5) 0.050(4) 0.005(4) 0.005(4) 0.001(4) C22 0.048(5) 0.061(6) 0.067(6) -0.003(4) -0.003(4) 0.004(4) C23 0.053(6) 0.052(5) 0.065(5) -0.004(4) -0.004(4) 0.004(4) C24 0.047(5) 0.054(5) 0.061(5) -0.007(4) 0.002(4) 0.003(4) C25 0.045(5) 0.066(6) 0.067(5) 0.006(4) -0.001(4) -0.004(4) C26 0.053(5) 0.066(5) 0.058(5) 0.008(4) 0.001(4) -0.001(4) C27 0.045(5) 0.058(5) 0.059(5) -0.007(4) -0.003(4) 0.003(4) C28 0.056(5) 0.059(5) 0.059(5) 0.002(4) 0.006(4) -0.003(4) C29 0.053(5) 0.061(5) 0.052(4) 0.001(4) -0.003(4) 0.002(4) C30 0.066(7) 0.131(9) 0.070(6) 0.014(7) -0.017(5) 0.005(6) C31 0.067(7) 0.122(9) 0.081(6) -0.015(6) 0.025(6) 0.003(6) N1 0.045(5) 0.061(5) 0.053(4) 0.004(3) -0.002(3) -0.003(3) O1 0.044(4) 0.081(5) 0.074(4) -0.006(3) 0.012(3) -0.003(3) O2 0.051(4) 0.103(5) 0.054(3) -0.006(3) 0.009(3) -0.003(3) O3 0.047(4) 0.083(4) 0.069(4) 0.006(3) -0.005(3) -0.002(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 O1 C1 C6 125.1(8) . . O1 C1 C2 114.6(8) . . C6 C1 C2 120.3(8) . . C3 C2 C1 119.1(8) . . C3 C2 H2 120.5 . . C1 C2 H2 120.5 . . C2 C3 C4 121.9(8) . . C2 C3 H3 119.1 . . C4 C3 H3 119.1 . . C3 C4 C5 118.1(8) . . C3 C4 C7 120.1(9) . . C5 C4 C7 121.7(8) . . C6 C5 C4 120.9(8) . . C6 C5 H5 119.5 . . C4 C5 H5 119.5 . . C1 C6 C5 119.6(8) . . C1 C6 H6 120.2 . . C5 C6 H6 120.2 . . C8 C7 C4 175.1(9) . . C7 C8 C9 174.7(10) . . C14 C9 C10 118.9(9) . . C14 C9 C8 122.2(9) . . C10 C9 C8 118.8(9) . . C11 C10 C9 120.2(9) . . C11 C10 H10 119.9 . . C9 C10 H10 119.9 . . C12 C11 C10 120.6(8) . . C12 C11 H11 119.7 . . C10 C11 H11 119.7 . . O2 C12 C11 119.7(7) . . O2 C12 C13 120.0(8) . . C11 C12 C13 120.3(8) . . C14 C13 C12 118.5(7) . . C14 C13 C15 119.5(7) . . C12 C13 C15 121.8(8) . . C9 C14 C13 121.4(8) . . C9 C14 H14 119.3 . . C13 C14 H14 119.3 . . N1 C15 C13 121.2(8) . . N1 C15 H15 119.4 . . C13 C15 H15 119.4 . . C21 C16 C17 118.2(8) . . C21 C16 N1 119.7(7) . . C17 C16 N1 122.0(8) . . C18 C17 C16 120.9(8) . . C18 C17 H17 119.6 . . C16 C17 H17 119.6 . . C17 C18 C19 120.5(9) . . C17 C18 H18 119.7 . . C19 C18 H18 119.7 . . C18 C19 C20 118.2(9) . . C18 C19 C22 121.1(10) . . C20 C19 C22 120.6(10) . . C21 C20 C19 121.0(8) . . C21 C20 H20 119.5 . . C19 C20 H20 119.5 . . C20 C21 C16 121.0(7) . . C20 C21 H21 119.5 . . C16 C21 H21 119.5 . . C23 C22 C19 177.2(10) . . C22 C23 C24 176.5(10) . . C25 C24 C29 117.7(8) . . C25 C24 C23 122.1(8) . . C29 C24 C23 120.1(9) . . C24 C25 C26 121.7(9) . . C24 C25 H25 119.1 . . C26 C25 H25 119.1 . . C27 C26 C25 119.1(8) . . C27 C26 H26 120.4 . . C25 C26 H26 120.4 . . O3 C27 C28 115.5(9) . . O3 C27 C26 124.6(8) . . C28 C27 C26 119.9(9) . . C29 C28 C27 120.8(8) . . C29 C28 H28 119.6 . . C27 C28 H28 119.6 . . C28 C29 C24 120.7(8) . . C28 C29 H29 119.6 . . C24 C29 H29 119.6 . . O3 C30 H30A 109.5 . . O3 C30 H30B 109.5 . . H30A C30 H30B 109.5 . . O3 C30 H30C 109.5 . . H30A C30 H30C 109.5 . . H30B C30 H30C 109.5 . . O1 C31 H31A 109.5 . . O1 C31 H31B 109.5 . . H31A C31 H31B 109.5 . . O1 C31 H31C 109.5 . . H31A C31 H31C 109.5 . . H31B C31 H31C 109.5 . . C15 N1 C16 121.1(7) . . C1 O1 C31 118.1(7) . . C12 O2 H2A 109.5 . . C27 O3 C30 118.2(8) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 C1 O1 1.373(11) . C1 C6 1.375(12) . C1 C2 1.393(12) . C2 C3 1.374(11) . C2 H2 0.9300 . C3 C4 1.375(12) . C3 H3 0.9300 . C4 C5 1.397(12) . C4 C7 1.442(14) . C5 C6 1.380(11) . C5 H5 0.9300 . C6 H6 0.9300 . C7 C8 1.188(12) . C8 C9 1.443(13) . C9 C14 1.376(13) . C9 C10 1.405(14) . C10 C11 1.381(12) . C10 H10 0.9300 . C11 C12 1.369(12) . C11 H11 0.9300 . C12 O2 1.365(10) . C12 C13 1.409(11) . C13 C14 1.396(11) . C13 C15 1.462(11) . C14 H14 0.9300 . C15 N1 1.276(10) . C15 H15 0.9300 . C16 C21 1.394(11) . C16 C17 1.397(11) . C16 N1 1.403(11) . C17 C18 1.377(12) . C17 H17 0.9300 . C18 C19 1.396(13) . C18 H18 0.9300 . C19 C20 1.399(14) . C19 C22 1.438(15) . C20 C21 1.364(11) . C20 H20 0.9300 . C21 H21 0.9300 . C22 C23 1.189(12) . C23 C24 1.430(12) . C24 C25 1.381(13) . C24 C29 1.404(13) . C25 C26 1.386(13) . C25 H25 0.9300 . C26 C27 1.381(12) . C26 H26 0.9300 . C27 O3 1.370(11) . C27 C28 1.379(12) . C28 C29 1.361(11) . C28 H28 0.9300 . C29 H29 0.9300 . C30 O3 1.422(12) . C30 H30A 0.9600 . C30 H30B 0.9600 . C30 H30C 0.9600 . C31 O1 1.425(12) . C31 H31A 0.9600 . C31 H31B 0.9600 . C31 H31C 0.9600 . O2 H2A 0.8200 . loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag C17 H17 O2 0.93 2.64 3.464(11) 148.7 1_556 yes C30 H30A O1 0.96 2.61 3.485(12) 151.6 1_656 yes C31 H31A O3 0.96 2.59 3.468(12) 152.2 1_455 yes O2 H2A N1 0.82 1.85 2.581(9) 147.6 . yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 O1 C1 C2 C3 179.4(8) . . . . C6 C1 C2 C3 -2.0(12) . . . . C1 C2 C3 C4 1.3(13) . . . . C2 C3 C4 C5 0.1(12) . . . . C2 C3 C4 C7 -177.2(8) . . . . C3 C4 C5 C6 -0.9(13) . . . . C7 C4 C5 C6 176.4(9) . . . . O1 C1 C6 C5 179.7(8) . . . . C2 C1 C6 C5 1.2(14) . . . . C4 C5 C6 C1 0.2(14) . . . . C14 C9 C10 C11 2.2(14) . . . . C8 C9 C10 C11 -174.2(9) . . . . C9 C10 C11 C12 -0.9(14) . . . . C10 C11 C12 O2 178.4(8) . . . . C10 C11 C12 C13 0.7(13) . . . . O2 C12 C13 C14 -179.5(8) . . . . C11 C12 C13 C14 -1.9(12) . . . . O2 C12 C13 C15 -5.1(12) . . . . C11 C12 C13 C15 172.6(9) . . . . C10 C9 C14 C13 -3.4(13) . . . . C8 C9 C14 C13 172.8(8) . . . . C12 C13 C14 C9 3.2(12) . . . . C15 C13 C14 C9 -171.4(8) . . . . C14 C13 C15 N1 177.0(8) . . . . C12 C13 C15 N1 2.6(13) . . . . C21 C16 C17 C18 2.5(12) . . . . N1 C16 C17 C18 177.2(8) . . . . C16 C17 C18 C19 0.3(13) . . . . C17 C18 C19 C20 -2.2(13) . . . . C17 C18 C19 C22 176.6(9) . . . . C18 C19 C20 C21 1.3(13) . . . . C22 C19 C20 C21 -177.5(8) . . . . C19 C20 C21 C16 1.6(13) . . . . C17 C16 C21 C20 -3.4(12) . . . . N1 C16 C21 C20 -178.3(8) . . . . C29 C24 C25 C26 -0.6(13) . . . . C23 C24 C25 C26 176.6(9) . . . . C24 C25 C26 C27 1.3(14) . . . . C25 C26 C27 O3 179.5(9) . . . . C25 C26 C27 C28 -0.9(13) . . . . O3 C27 C28 C29 179.4(8) . . . . C26 C27 C28 C29 -0.2(13) . . . . C27 C28 C29 C24 1.0(13) . . . . C25 C24 C29 C28 -0.6(13) . . . . C23 C24 C29 C28 -177.8(8) . . . . C13 C15 N1 C16 -170.6(7) . . . . C21 C16 N1 C15 -147.0(8) . . . . C17 C16 N1 C15 38.4(13) . . . . C6 C1 O1 C31 5.8(13) . . . . C2 C1 O1 C31 -175.6(8) . . . . C28 C27 O3 C30 -176.0(8) . . . . C26 C27 O3 C30 3.6(13) . . . .