#------------------------------------------------------------------------------ #$Date: 2021-10-07 07:41:32 +0300 (Thu, 07 Oct 2021) $ #$Revision: 269816 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/48/1564852.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564852 loop_ _publ_author_name 'Kodama, Shintaro' 'Hung, Vu Thai' 'Saeki, Tomokazu' 'Mihara, Kei' 'Yamamoto, Yuki' 'Sonoda, Motohiro' 'Nomoto, Akihiro' 'Ogawa, Akiya' _publ_section_title ; 2,2-Bis(phenylselanyl)-1-(p-tolyl)vinyl 2-Oxo-2-(p-tolyl)acetate ; _journal_issue 4 _journal_name_full Molbank _journal_page_first M1283 _journal_paper_doi 10.3390/M1283 _journal_volume 2021 _journal_year 2021 _chemical_formula_moiety 'C30 H24 O3 Se2' _chemical_formula_sum 'C30 H24 O3 Se2' _chemical_formula_weight 590.44 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _cell_angle_alpha 90.0000 _cell_angle_beta 91.229(6) _cell_angle_gamma 90.0000 _cell_formula_units_Z 4 _cell_length_a 9.62321(17) _cell_length_b 5.73648(10) _cell_length_c 45.1254(8) _cell_measurement_reflns_used 37001 _cell_measurement_temperature 123 _cell_measurement_theta_max 27.50 _cell_measurement_theta_min 3.06 _cell_volume 2490.50(8) _computing_cell_refinement 'RAPID AUTO' _computing_data_collection 'RAPID AUTO (Rigaku, ????)' _computing_data_reduction 'RAPID AUTO' _computing_molecular_graphics 'CrystalStructure 4.2' _computing_publication_material 'CrystalStructure 4.2 (Rigaku, 2015)' _computing_structure_refinement 'SHELXL Version 2014/7 (Sheldrick, 2008)' _computing_structure_solution 'SHELXT Version 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 123 _diffrn_detector_area_resol_mean 10.000 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Rigaku R-AXIS RAPID' _diffrn_measurement_method \w _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71075 _diffrn_reflns_av_R_equivalents 0.0465 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 7 _diffrn_reflns_limit_k_min -7 _diffrn_reflns_limit_l_max 58 _diffrn_reflns_limit_l_min -58 _diffrn_reflns_number 39479 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.485 _diffrn_reflns_theta_min 3.062 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 3.000 _exptl_absorpt_correction_T_max 0.942 _exptl_absorpt_correction_T_min 0.513 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'ABSCOR (Rigaku, 1995)' _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.575 _exptl_crystal_density_method 'not measured' _exptl_crystal_description prism _exptl_crystal_F_000 1184.00 _exptl_crystal_size_max 0.300 _exptl_crystal_size_mid 0.050 _exptl_crystal_size_min 0.020 _refine_diff_density_max 0.70 _refine_diff_density_min -0.43 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.054 _refine_ls_hydrogen_treatment constr _refine_ls_number_parameters 318 _refine_ls_number_reflns 5743 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0308 _refine_ls_R_factor_gt 0.0264 _refine_ls_shift/su_max 0.003 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w = 1/[\s^2^(Fo^2^)+(0.0347P)^2^+1.1850P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0652 _refine_ls_wR_factor_ref 0.0672 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5114 _reflns_number_total 5743 _reflns_threshold_expression F^2^>2.0\s(F^2^) _cod_data_source_file s5.cif _cod_data_source_block SP-8 _cod_database_code 1564852 _shelx_res_file ; shelxl.res created by SHELXL-2014/7 TITL SP-8 CELL 0.71075 9.62321 5.73648 45.12536 90.00000 91.22900 90.00000 ZERR 4 0.00017 0.00010 0.00082 0.00000 0.00640 0.00000 LATT 1 SYMM .50-X, .50+Y, .50-Z SFAC C H O SE UNIT 124 96 8 8 L.S. 5 FMAP 2 PLAN 20 WPDB -2 HTAB BOND $H CONF LIST 4 TEMP -150.0 ACTA SIZE 0.300 0.050 0.020 WGHT 0.034700 1.185000 FVAR 0.25082 SE1 4 0.386817 0.019521 0.361589 11.00000 0.02029 0.01862 = 0.02301 0.00226 0.00073 0.00113 SE2 4 0.228183 0.436844 0.322801 11.00000 0.02249 0.01964 = 0.01973 0.00262 -0.00162 -0.00056 O1 3 0.292825 0.331348 0.412304 11.00000 0.01884 0.02740 = 0.01933 0.00199 -0.00256 0.00017 O2 3 0.498963 0.502233 0.401348 11.00000 0.02863 0.03118 = 0.02176 0.00401 -0.00348 -0.00790 O3 3 0.430476 0.080035 0.452191 11.00000 0.03333 0.02461 = 0.02893 0.00654 -0.00619 -0.00577 C1 1 0.273780 0.294697 0.359835 11.00000 0.01701 0.01712 = 0.02185 0.00238 -0.00121 -0.00004 C2 1 0.232704 0.399605 0.384629 11.00000 0.01790 0.02121 = 0.02125 0.00261 -0.00349 -0.00138 C3 1 0.119397 0.571231 0.388548 11.00000 0.01877 0.02185 = 0.01850 0.00262 0.00076 0.00024 C4 1 0.138858 0.769767 0.405983 11.00000 0.02184 0.02545 = 0.01946 -0.00023 -0.00105 -0.00186 AFIX 43 H4 2 0.226959 0.799669 0.415100 11.00000 -1.20000 AFIX 0 C5 1 0.029690 0.923612 0.410025 11.00000 0.02791 0.02323 = 0.01931 -0.00145 0.00030 -0.00057 AFIX 43 H5 2 0.045110 1.059850 0.421604 11.00000 -1.20000 AFIX 0 C6 1 -0.101654 0.884050 0.397607 11.00000 0.02305 0.02367 = 0.02298 0.00484 0.00336 0.00171 C7 1 -0.120598 0.682839 0.380476 11.00000 0.01837 0.02899 = 0.02950 -0.00107 -0.00141 -0.00092 AFIX 43 H7 2 -0.209553 0.650666 0.371898 11.00000 -1.20000 AFIX 0 C8 1 -0.011897 0.529578 0.375796 11.00000 0.02237 0.02262 = 0.02512 -0.00272 -0.00113 -0.00204 AFIX 43 H8 2 -0.026748 0.395234 0.363832 11.00000 -1.20000 AFIX 0 C9 1 -0.220716 1.050094 0.402216 11.00000 0.02797 0.03007 = 0.03574 0.00158 0.00555 0.00719 AFIX 137 H9A 2 -0.306021 0.961208 0.405456 11.00000 -1.20000 H9B 2 -0.233148 1.148822 0.384635 11.00000 -1.20000 H9C 2 -0.200362 1.148170 0.419554 11.00000 -1.20000 AFIX 0 C10 1 0.521894 0.101956 0.332807 11.00000 0.01913 0.02313 = 0.02147 0.00262 -0.00106 0.00306 C11 1 0.551876 -0.058338 0.310980 11.00000 0.02933 0.02396 = 0.02832 -0.00166 -0.00009 0.00208 AFIX 43 H11 2 0.501237 -0.200194 0.309546 11.00000 -1.20000 AFIX 0 C12 1 0.656985 -0.010276 0.291085 11.00000 0.03481 0.03274 = 0.02603 -0.00206 0.00545 0.00669 AFIX 43 H12 2 0.679854 -0.121580 0.276383 11.00000 -1.20000 AFIX 0 C13 1 0.727809 0.198423 0.292700 11.00000 0.02442 0.03845 = 0.02606 0.00804 0.00440 0.00659 AFIX 43 H13 2 0.799368 0.230613 0.279110 11.00000 -1.20000 AFIX 0 C14 1 0.694835 0.361255 0.314099 11.00000 0.02299 0.02969 = 0.03294 0.00438 0.00030 -0.00299 AFIX 43 H14 2 0.742464 0.506255 0.314880 11.00000 -1.20000 AFIX 0 C15 1 0.592351 0.313084 0.334409 11.00000 0.02402 0.02562 = 0.02721 -0.00249 0.00040 -0.00190 AFIX 43 H15 2 0.570587 0.423629 0.349282 11.00000 -1.20000 AFIX 0 C16 1 0.134509 0.186158 0.302531 11.00000 0.01758 0.02306 = 0.02173 -0.00165 -0.00351 0.00405 C17 1 0.067508 0.010100 0.317548 11.00000 0.02139 0.02578 = 0.02657 0.00152 -0.00568 0.00182 AFIX 43 H17 2 0.067539 0.008910 0.338600 11.00000 -1.20000 AFIX 0 C18 1 0.000160 -0.164995 0.301535 11.00000 0.02282 0.02280 = 0.04321 0.00205 -0.01004 0.00175 AFIX 43 H18 2 -0.045620 -0.286618 0.311761 11.00000 -1.20000 AFIX 0 C19 1 -0.000987 -0.164240 0.270967 11.00000 0.02839 0.03036 = 0.04437 -0.01320 -0.01493 0.00789 AFIX 43 H19 2 -0.045577 -0.286560 0.260226 11.00000 -1.20000 AFIX 0 C20 1 0.062934 0.015011 0.256025 11.00000 0.02858 0.04972 = 0.02368 -0.01170 -0.00557 0.01098 AFIX 43 H20 2 0.060020 0.017970 0.234972 11.00000 -1.20000 AFIX 0 C21 1 0.131737 0.191691 0.271696 11.00000 0.02455 0.03545 = 0.02406 0.00021 0.00103 0.00339 AFIX 43 H21 2 0.176222 0.314470 0.261429 11.00000 -1.20000 AFIX 0 C22 1 0.428713 0.387227 0.417275 11.00000 0.02160 0.02110 = 0.02078 -0.00321 -0.00158 0.00157 C23 1 0.480319 0.268364 0.446219 11.00000 0.02045 0.02419 = 0.02161 0.00111 0.00037 0.00316 C24 1 0.589777 0.383236 0.464462 11.00000 0.02110 0.02389 = 0.02013 -0.00016 -0.00066 0.00209 C25 1 0.649329 0.597341 0.457296 11.00000 0.03764 0.02645 = 0.02621 0.00279 -0.00715 -0.00421 AFIX 43 H25 2 0.620966 0.675493 0.439619 11.00000 -1.20000 AFIX 0 C26 1 0.749340 0.696114 0.475799 11.00000 0.03830 0.02703 = 0.03317 -0.00039 -0.00473 -0.00852 AFIX 43 H26 2 0.790172 0.840366 0.470405 11.00000 -1.20000 AFIX 0 C27 1 0.791499 0.589159 0.502112 11.00000 0.02232 0.03596 = 0.02488 -0.00687 0.00078 0.00006 C28 1 0.730990 0.376285 0.509280 11.00000 0.02664 0.03585 = 0.02128 0.00277 -0.00323 -0.00011 AFIX 43 H28 2 0.758307 0.299941 0.527156 11.00000 -1.20000 AFIX 0 C29 1 0.631911 0.274392 0.490818 11.00000 0.02424 0.02963 = 0.02434 0.00444 -0.00143 0.00006 AFIX 43 H29 2 0.592158 0.129051 0.496114 11.00000 -1.20000 AFIX 0 C30 1 0.896585 0.703486 0.522479 11.00000 0.03124 0.04362 = 0.03007 -0.00856 -0.00455 -0.00415 AFIX 137 H30A 2 0.973089 0.765268 0.510833 11.00000 -1.20000 H30B 2 0.932925 0.588524 0.536717 11.00000 -1.20000 H30C 2 0.852281 0.831235 0.533170 11.00000 -1.20000 AFIX 0 HKLF 4 REM SP-8 REM R1 = 0.0264 for 5114 Fo > 4sig(Fo) and 0.0308 for all 5743 data REM 318 parameters refined using 0 restraints END WGHT 0.0347 1.1850 REM Instructions for potential hydrogen bonds HTAB C15 O2 REM Highest difference peak 0.697, deepest hole -0.433, 1-sigma level 0.073 Q1 1 0.2255 0.6377 0.3224 11.00000 0.05 0.70 Q2 1 0.3849 -0.1662 0.3610 11.00000 0.05 0.63 Q3 1 0.3095 0.3684 0.3186 11.00000 0.05 0.46 Q4 1 0.1374 0.5175 0.3253 11.00000 0.05 0.46 Q5 1 0.2941 0.1333 0.3621 11.00000 0.05 0.45 Q6 1 0.3138 0.5215 0.3181 11.00000 0.05 0.43 Q7 1 0.4646 0.1042 0.3600 11.00000 0.05 0.42 Q8 1 0.4441 0.1126 0.3428 11.00000 0.05 0.42 Q9 1 0.4525 -0.0394 0.3562 11.00000 0.05 0.42 Q10 1 0.1771 0.5040 0.3850 11.00000 0.05 0.42 Q11 1 0.3030 -0.0696 0.3628 11.00000 0.05 0.41 Q12 1 0.3783 0.2356 0.3615 11.00000 0.05 0.41 Q13 1 0.2598 0.3248 0.3080 11.00000 0.05 0.40 Q14 1 0.1948 0.2587 0.3132 11.00000 0.05 0.40 Q15 1 0.4088 0.1448 0.3733 11.00000 0.05 0.39 Q16 1 -0.1573 0.9739 0.3998 11.00000 0.05 0.38 Q17 1 0.6613 0.4659 0.4950 11.00000 0.05 0.38 Q18 1 0.0372 -0.0680 0.2658 11.00000 0.05 0.37 Q19 1 0.0775 0.1185 0.3086 11.00000 0.05 0.37 Q20 1 0.4015 -0.0439 0.3776 11.00000 0.05 0.37 ; _shelx_res_checksum 43595 _shelx_hkl_file ; 0 0 7 0.08 0.29 0 0 7 -0.01 0.34 0 0 -7 0.03 0.31 0 0 -7 0.42 0.53 0 0 8 0.08 0.21 0 0 8 0.32 0.37 0 0 -8 0.06 0.22 0 0 -8 0.06 0.38 0 0 9 0.17 0.22 0 0 9 -0.02 0.41 0 0 -9 -0.03 0.23 0 0 -9 -0.33 0.40 0 0 10 841.41 19.75 0 0 10 840.35 21.12 0 0 -10 810.21 19.98 0 0 -10 847.11 19.70 0 0 -10 843.88 20.99 0 0 11 0.44 0.31 0 0 11 0.18 0.54 0 0 -11 0.66 0.47 0 0 -11 0.29 0.31 0 0 -11 0.75 0.84 0 0 12 27.61 1.17 0 0 12 29.38 1.36 0 0 -12 27.31 1.24 0 0 -12 26.89 1.14 0 0 -12 27.93 1.33 0 0 13 0.97 0.41 0 0 13 3.03 0.73 0 0 -13 1.22 0.89 0 0 -13 1.17 0.40 0 0 -13 1.32 0.69 0 0 14 852.42 21.07 0 0 14 855.36 22.73 0 0 -14 823.03 21.47 0 0 -14 856.79 21.10 0 0 -14 843.43 22.11 0 0 15 0.61 0.41 0 0 15 0.59 1.14 0 0 -15 0.56 0.63 0 0 -15 0.70 0.40 0 0 -15 0.85 1.08 0 0 16 125.74 3.27 0 0 16 132.74 4.04 0 0 -16 133.63 3.91 0 0 -16 124.47 3.22 0 0 -16 131.28 4.10 0 0 17 -0.29 0.62 0 0 17 -0.04 0.74 0 0 -17 -0.02 0.96 0 0 -17 0.63 0.60 0 0 -17 0.78 0.77 0 0 18 333.01 8.24 0 0 18 352.35 9.78 0 0 -18 327.38 9.05 0 0 -18 329.71 8.17 0 0 -18 353.66 9.86 0 0 19 1.31 0.71 0 0 19 2.36 1.42 0 0 -19 -0.22 0.77 0 0 -19 -0.21 0.70 0 0 -19 1.39 0.90 0 0 20 38.03 1.43 0 0 20 34.17 1.97 0 0 -20 40.59 1.95 0 0 -20 37.56 1.40 0 0 -20 36.37 2.67 0 0 21 4.08 0.96 0 0 21 3.62 1.26 0 0 -21 5.57 1.49 0 0 -21 0.63 1.00 0 0 -21 3.60 1.23 0 0 22 3521.10 106.03 0 0 22 3495.50 110.17 0 0 -22 3344.18 106.11 0 0 -22 3307.32 102.69 0 0 -22 3546.58 112.33 0 0 23 13.53 0.98 0 0 23 13.72 2.25 0 0 -23 6.75 1.25 0 0 -23 8.80 0.88 0 0 -23 10.10 1.75 0 0 24 10.34 1.21 0 0 24 17.46 1.60 0 0 -24 10.95 1.88 0 0 -24 10.02 1.22 0 0 -24 18.53 2.41 0 0 25 2.23 0.68 0 0 25 1.59 1.27 0 0 -25 2.45 1.10 0 0 -25 2.11 0.66 0 0 -25 1.12 1.27 0 0 26 977.58 27.33 0 0 26 1003.51 30.35 0 0 -26 993.59 29.24 0 0 -26 992.88 27.32 0 0 -26 1016.55 30.60 0 0 27 6.99 0.89 0 0 27 4.89 2.30 0 0 -27 1.76 1.33 0 0 -27 1.91 0.81 0 0 -27 5.90 1.66 0 0 28 420.66 11.81 0 0 28 436.49 13.76 0 0 -28 414.78 13.42 0 0 -28 447.40 14.85 0 0 29 2.89 0.80 0 0 29 2.35 1.49 0 0 -29 2.98 1.27 0 0 -29 3.25 1.56 0 0 30 8.13 1.29 0 0 30 6.80 1.79 0 0 -30 9.47 1.57 0 0 -30 7.29 1.79 0 0 31 2.68 0.83 0 0 31 2.34 2.44 0 0 -31 0.38 1.34 0 0 -31 1.46 1.63 0 0 32 544.11 15.34 0 0 32 542.01 17.74 0 0 -32 545.04 18.24 0 0 -32 547.31 18.85 0 0 33 5.22 1.38 0 0 33 5.97 1.98 0 0 -33 2.81 1.65 0 0 -33 4.72 2.04 0 0 34 245.95 7.44 0 0 34 271.64 9.97 0 0 -34 247.61 8.95 0 0 -34 271.60 10.01 0 0 35 1.35 1.28 0 0 35 1.85 2.77 0 0 -35 1.54 2.32 0 0 -35 1.35 1.88 0 0 36 28.74 1.73 0 0 36 27.12 4.40 0 0 -36 31.55 3.70 0 0 -36 29.16 4.42 0 0 37 0.16 1.20 0 0 37 0.50 1.83 0 0 -37 1.34 1.50 0 0 -37 0.71 1.83 0 0 38 20.91 1.48 0 0 38 22.61 3.02 0 0 -38 18.71 2.50 0 0 -38 25.09 3.05 0 0 39 0.67 1.17 0 0 39 0.07 2.74 0 0 -39 0.41 2.26 0 0 -39 -0.87 1.77 0 0 40 8.67 1.20 0 0 40 10.98 3.89 0 0 -40 9.35 2.23 0 0 -40 11.39 3.87 0 0 41 0.82 1.26 0 0 41 0.60 2.15 0 0 -41 1.36 1.74 0 0 -41 0.48 3.28 0 0 42 4.21 1.06 0 0 42 5.60 2.58 0 0 -42 5.21 2.22 0 0 -42 3.10 2.59 0 0 43 0.98 1.46 0 0 43 0.91 3.90 0 0 -43 2.56 3.06 0 0 -43 3.88 2.56 0 0 44 313.32 10.49 0 0 44 340.85 15.93 0 0 -44 342.58 13.28 0 0 -44 343.05 16.29 0 0 45 2.89 1.58 0 0 45 3.07 2.80 0 0 -45 3.00 2.28 0 0 -45 1.20 4.15 0 0 46 49.16 3.26 0 0 46 58.73 5.08 0 0 -46 53.94 5.88 0 0 -46 59.93 5.18 0 0 47 2.21 1.01 0 0 47 2.92 4.54 0 0 -47 1.71 2.38 0 0 -47 3.00 2.93 0 0 48 176.82 7.06 0 0 48 165.49 6.77 0 0 48 194.56 12.31 0 0 -48 197.16 9.39 0 0 -48 204.34 12.62 0 0 49 1.53 0.95 0 0 49 1.63 1.02 0 0 49 4.44 3.10 0 0 -49 3.18 2.48 0 0 -49 3.90 4.87 0 0 50 185.84 10.24 0 0 -50 179.00 11.11 0 0 -50 188.89 10.48 0 0 51 0.93 0.90 0 0 51 0.60 0.90 0 0 -51 3.47 2.47 0 0 -51 1.91 3.21 0 0 52 10.09 1.80 0 0 52 10.90 1.85 0 0 52 10.64 5.89 0 0 -52 16.70 3.44 0 0 -52 13.37 6.15 0 0 53 1.75 1.37 0 0 53 1.66 1.38 0 0 53 4.49 3.51 0 0 -53 3.31 4.12 0 0 -53 2.59 3.61 0 0 54 308.55 15.15 0 0 -54 301.52 14.49 0 0 -54 313.76 15.81 0 0 55 1.65 5.96 0 0 -55 2.44 2.99 0 0 -55 6.44 4.05 0 0 56 35.31 5.77 0 0 -56 29.11 6.52 0 0 -56 33.93 8.44 0 0 57 3.42 3.90 0 0 -57 1.97 3.06 0 0 -57 4.74 4.00 0 0 58 26.72 5.62 0 0 -58 29.91 4.48 0 0 -58 30.03 5.93 0 1 0 0.17 0.22 0 1 0 0.34 0.29 0 1 0 -0.09 0.20 0 -1 0 0.02 0.25 0 -1 0 0.12 0.31 0 1 1 128.17 2.73 0 1 1 130.51 3.18 0 1 -1 127.30 2.91 0 1 1 132.05 2.89 0 1 -1 125.57 3.06 0 1 -1 126.12 2.72 0 -1 1 127.04 2.92 0 -1 1 129.76 3.17 0 -1 -1 126.24 2.76 0 -1 1 132.30 2.92 0 -1 -1 129.73 3.14 0 -1 -1 131.87 2.91 0 1 -2 893.46 21.51 0 1 2 952.59 22.33 0 1 2 901.55 21.88 0 1 -2 909.57 21.44 0 1 -2 940.09 21.46 0 -1 2 937.26 21.70 0 -1 -2 890.85 20.45 0 -1 2 874.50 21.05 0 -1 -2 907.92 22.00 0 -1 -2 974.81 22.88 0 1 3 402.06 9.44 0 1 -3 393.99 8.65 0 1 -3 385.64 9.17 0 1 3 419.65 9.64 0 -1 3 386.33 9.05 0 -1 -3 395.46 9.35 0 -1 3 411.03 9.00 0 -1 -3 426.31 9.57 0 1 4 320.22 7.74 0 1 -4 324.97 6.91 0 1 -4 327.48 7.68 0 1 4 334.11 7.67 0 1 -4 348.51 7.48 0 -1 -4 325.79 7.76 0 -1 4 319.24 7.84 0 -1 -4 338.95 7.75 0 -1 4 324.93 6.88 0 1 -5 128.82 3.31 0 1 5 129.72 3.23 0 1 5 130.23 3.43 0 1 -5 126.78 2.67 0 1 -5 129.43 2.86 0 -1 5 131.78 2.82 0 -1 -5 129.69 3.43 0 -1 5 124.87 3.26 0 -1 -5 130.71 3.26 0 -1 5 127.08 3.05 0 1 -6 307.98 7.58 0 1 6 316.02 7.61 0 1 6 315.18 8.08 0 1 -6 313.40 6.48 0 1 -6 330.59 7.29 0 -1 6 329.23 6.65 0 -1 -6 312.42 7.72 0 -1 6 309.43 7.60 0 -1 -6 320.55 7.93 0 -1 6 322.92 7.21 0 1 -7 26.95 1.20 0 1 7 25.00 1.12 0 1 7 25.79 1.53 0 1 -7 25.25 0.66 0 1 -7 26.83 0.92 0 -1 7 25.65 0.66 0 -1 -7 25.84 1.24 0 -1 7 24.77 1.18 0 -1 -7 25.85 1.14 0 -1 7 25.34 0.91 0 1 8 473.02 11.93 0 1 8 448.50 11.26 0 1 -8 443.55 11.22 0 1 -8 483.04 11.24 0 1 -8 464.10 9.22 0 -1 -8 455.42 11.35 0 -1 8 446.04 11.17 0 -1 -8 474.09 11.67 0 -1 8 478.41 11.28 0 1 9 114.20 3.29 0 1 9 121.69 3.50 0 1 -9 118.14 3.43 0 1 -9 128.71 2.19 0 1 -9 122.79 2.11 0 1 -9 117.09 2.97 0 -1 9 119.47 3.45 0 -1 9 118.20 3.03 0 -1 -9 117.53 3.33 0 -1 -9 120.76 3.79 0 1 10 275.85 7.56 0 1 10 265.74 6.90 0 1 -10 263.56 7.02 0 1 -10 278.61 6.69 0 -1 10 260.85 7.24 0 -1 10 272.01 6.61 0 -1 -10 276.68 7.51 0 -1 -10 259.76 6.81 0 1 11 2798.75 81.87 0 1 11 2729.43 79.66 0 1 -11 2795.44 81.41 0 1 -11 2871.88 81.52 0 -1 11 2730.28 79.44 0 -1 11 2793.84 80.22 0 -1 -11 2887.46 83.51 0 -1 -11 2714.29 79.59 0 1 12 27.05 1.48 0 1 12 28.94 1.43 0 1 -12 28.32 2.03 0 1 -12 28.52 1.58 0 -1 12 27.82 1.46 0 -1 12 27.99 1.27 0 -1 -12 26.05 2.04 0 -1 -12 28.83 1.46 0 1 13 414.27 10.88 0 1 13 386.06 10.20 0 1 -13 376.91 10.25 0 1 -13 440.88 11.23 0 -1 13 375.93 10.69 0 -1 13 412.94 10.76 0 -1 -13 409.04 10.89 0 -1 -13 379.50 10.51 0 1 14 13.25 1.70 0 1 14 13.20 1.53 0 1 -14 14.54 1.27 0 1 -14 12.30 1.35 0 -1 14 12.88 1.21 0 -1 14 13.57 0.99 0 -1 -14 12.43 1.26 0 -1 -14 12.67 1.08 0 1 15 1077.28 29.28 0 1 15 1123.39 30.71 0 1 -15 1129.41 30.21 0 1 -15 1060.01 29.45 0 -1 15 1126.99 30.66 0 -1 -15 1147.78 32.00 0 -1 -15 1099.71 30.09 0 1 16 0.00 0.71 0 1 16 -0.21 0.84 0 1 -16 -0.42 0.64 0 1 -16 -0.62 0.84 0 -1 16 -0.74 0.72 0 -1 -16 -0.72 1.41 0 -1 -16 -1.08 1.07 0 1 17 1885.22 54.20 0 1 17 1915.11 55.50 0 1 -17 1904.96 55.26 0 1 -17 1890.79 55.26 0 -1 17 1945.62 55.57 0 -1 -17 1962.96 57.27 0 -1 -17 1864.72 54.15 0 1 18 49.50 2.15 0 1 18 51.48 2.44 0 1 -18 48.67 2.20 0 1 -18 49.29 2.39 0 -1 18 49.44 2.76 0 -1 -18 51.16 2.54 0 -1 -18 47.47 2.09 0 1 19 1.72 0.79 0 1 -19 1.47 0.86 0 1 19 2.05 1.04 0 1 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3.73 0 1 -41 11.46 2.51 0 -1 41 5.30 0.75 0 -1 41 6.71 0.74 0 -1 41 5.96 3.60 0 -1 -41 4.91 2.85 0 -1 -41 8.50 2.84 0 1 42 1.22 1.40 0 1 42 1.79 2.53 0 1 -42 1.99 2.27 0 1 -42 4.64 2.36 0 -1 42 0.80 0.55 0 -1 42 0.55 0.58 0 -1 42 1.04 2.20 0 -1 -42 4.90 3.81 0 -1 -42 1.86 1.74 0 1 43 454.75 16.74 0 1 43 470.02 20.07 0 1 -43 467.37 18.08 0 1 -43 486.95 19.98 0 -1 43 451.24 17.59 0 -1 -43 464.12 20.40 0 -1 -43 455.40 16.69 0 1 44 2.39 1.69 0 1 44 6.12 3.01 0 1 -44 5.31 3.86 0 1 -44 8.07 3.80 0 -1 44 2.41 0.61 0 -1 44 1.39 0.58 0 -1 44 3.45 2.73 0 -1 -44 4.55 3.17 0 -1 -44 3.90 2.98 0 1 45 85.59 5.34 0 1 45 97.33 6.64 0 1 -45 96.14 6.16 0 1 -45 93.05 5.91 0 -1 45 93.72 6.02 0 -1 -45 95.26 6.73 0 -1 -45 87.40 5.14 0 1 46 12.67 2.15 0 1 46 18.78 5.68 0 1 -46 15.76 3.54 0 1 -46 14.81 3.43 0 -1 46 17.75 5.13 0 -1 -46 20.27 4.11 0 -1 -46 16.08 2.63 0 1 47 36.56 2.95 0 1 47 38.99 4.84 0 1 -47 37.87 4.35 0 1 -47 42.82 4.59 0 -1 47 36.88 4.35 0 -1 -47 38.58 7.16 0 -1 -47 39.45 4.70 0 1 48 6.55 2.67 0 1 48 8.67 3.65 0 1 -48 6.17 4.99 0 1 -48 5.50 4.70 0 -1 48 6.28 3.25 0 -1 -48 10.18 5.65 0 -1 -48 7.02 2.37 0 1 49 25.92 2.63 0 1 49 28.75 6.92 0 1 -49 31.03 4.34 0 1 -49 30.01 4.23 0 -1 49 25.75 4.35 0 -1 -49 31.19 4.88 0 -1 -49 28.68 4.61 0 1 50 2.74 2.37 0 1 50 1.96 3.37 0 1 -50 2.87 2.97 0 1 -50 2.67 2.88 0 -1 50 3.63 3.03 0 -1 -50 2.00 3.43 0 -1 -50 1.98 3.26 0 1 51 15.09 2.10 0 1 -51 23.66 6.08 0 1 -51 19.93 4.00 0 -1 51 20.03 5.94 0 -1 -51 18.87 4.59 0 -1 -51 18.55 3.10 0 1 52 6.05 2.60 0 1 52 9.18 4.06 0 1 -52 6.38 3.62 0 1 -52 9.65 5.19 0 -1 52 9.25 3.50 0 -1 -52 9.42 6.41 0 -1 -52 8.77 3.87 0 1 53 9.17 2.01 0 1 53 13.29 6.80 0 1 -53 13.96 4.01 0 1 -53 14.68 3.87 0 -1 53 12.30 3.91 0 -1 -53 11.61 6.83 0 -1 -53 11.19 2.89 0 1 54 6.40 2.46 0 1 54 5.71 4.24 0 1 -54 4.83 5.75 0 1 -54 5.19 3.69 0 -1 54 6.75 3.77 0 -1 -54 8.94 4.34 0 -1 -54 5.82 2.64 0 1 55 31.80 3.01 0 1 55 43.64 6.23 0 1 -55 42.06 5.59 0 1 -55 41.80 5.40 0 -1 55 44.42 5.49 0 -1 -55 42.69 6.43 0 -1 -55 37.13 5.75 0 1 56 8.25 2.62 0 1 56 8.97 1.90 0 1 56 8.89 7.32 0 1 -56 10.98 4.23 0 1 -56 11.84 6.10 0 -1 56 10.02 6.41 0 -1 -56 15.14 4.93 0 -1 -56 10.42 2.99 0 1 57 2.52 2.20 0 1 57 1.88 2.22 0 1 57 5.71 4.26 0 1 -57 2.54 5.66 0 1 -57 4.45 3.44 0 -1 57 2.03 3.71 0 -1 -57 6.61 6.51 0 -1 -57 3.18 2.56 0 1 58 5.39 1.65 0 1 58 5.97 1.66 0 1 58 11.66 4.73 0 1 -58 7.41 6.16 0 1 -58 9.89 3.93 0 -1 58 11.46 4.31 0 -1 -58 7.89 4.92 0 -1 -58 4.26 4.33 0 2 0 1790.17 49.38 0 2 0 1856.33 52.05 0 2 0 1976.24 53.21 0 -2 0 1891.98 52.90 0 -2 0 1907.78 51.32 0 -2 0 1849.99 51.06 0 2 1 415.03 10.29 0 2 -1 448.71 11.01 0 2 -1 437.55 11.59 0 2 1 425.31 11.29 0 2 -1 426.79 11.06 0 2 1 452.75 10.99 0 -2 1 438.76 11.55 0 -2 -1 419.22 10.50 0 -2 -1 439.29 11.46 0 -2 1 455.19 11.16 0 -2 -1 444.93 10.87 0 -2 1 428.23 10.83 0 2 -2 366.89 9.11 0 2 -2 374.66 9.66 0 2 2 381.90 10.13 0 2 -2 376.39 9.60 0 2 2 390.67 9.62 0 -2 2 380.25 9.80 0 -2 -2 376.55 9.37 0 -2 -2 381.53 10.08 0 -2 2 385.78 9.28 0 -2 -2 376.80 9.31 0 -2 2 373.48 9.63 0 2 3 2.82 0.86 0 2 3 3.08 0.56 0 2 -3 3.05 0.67 0 2 -3 3.24 0.61 0 2 -3 2.83 0.48 0 -2 3 3.18 0.64 0 -2 3 3.19 1.03 0 -2 -3 3.08 0.72 0 -2 -3 3.69 0.83 0 -2 -3 3.25 0.89 0 2 -4 1956.81 55.51 0 2 4 2018.51 56.39 0 2 4 1957.68 56.06 0 2 -4 2026.26 55.79 0 2 -4 1952.35 52.79 0 -2 4 1932.61 54.48 0 -2 -4 2008.02 54.06 0 -2 4 1922.22 55.22 0 -2 -4 1967.67 55.89 0 -2 -4 2028.23 56.43 0 2 -5 74.81 2.54 0 2 5 82.71 2.86 0 2 5 75.99 2.85 0 2 -5 74.31 2.26 0 -2 -5 73.86 2.19 0 -2 5 76.51 2.27 0 -2 -5 76.63 2.80 0 -2 5 75.74 2.58 0 -2 -5 84.66 2.61 0 2 -6 379.66 9.27 0 2 6 365.72 9.49 0 2 6 364.13 10.02 0 2 -6 360.47 9.69 0 2 -6 364.26 9.07 0 2 -6 358.39 9.09 0 -2 -6 347.96 8.23 0 -2 6 366.17 9.23 0 -2 -6 367.18 10.05 0 -2 -6 375.09 10.12 0 -2 6 360.46 9.61 0 2 -7 182.05 5.23 0 2 7 189.24 5.56 0 2 7 182.90 5.52 0 2 -7 178.75 4.51 0 2 -7 183.07 4.75 0 -2 7 177.99 4.66 0 -2 -7 178.76 5.39 0 -2 7 175.34 5.14 0 -2 -7 185.93 5.19 0 -2 -7 172.88 4.17 0 2 8 13.57 1.28 0 2 -8 12.76 0.72 0 2 -8 13.29 1.16 0 2 8 13.81 1.47 0 2 -8 15.41 0.98 0 -2 -8 13.19 1.29 0 -2 8 12.07 1.13 0 -2 -8 14.69 1.09 0 -2 8 13.18 0.93 0 2 9 1053.86 29.24 0 2 -9 1035.50 26.19 0 2 -9 1022.99 28.91 0 2 9 1050.59 28.78 0 2 -9 1094.30 28.14 0 -2 -9 1064.75 29.53 0 -2 9 1037.21 29.02 0 -2 -9 1070.77 29.80 0 -2 9 1073.03 26.81 0 2 10 137.75 5.18 0 2 -10 136.28 3.32 0 2 -10 138.28 4.41 0 2 10 146.39 4.43 0 2 -10 144.15 3.78 0 -2 -10 139.39 4.60 0 -2 10 137.09 4.37 0 -2 -10 144.21 4.82 0 -2 10 137.16 3.48 0 2 11 43.29 2.41 0 2 11 45.89 2.84 0 2 -11 45.65 2.68 0 2 -11 42.52 1.53 0 2 -11 44.37 1.42 0 -2 -11 46.07 2.30 0 -2 11 47.12 2.16 0 -2 -11 44.99 2.03 0 -2 11 42.63 1.94 0 2 12 4.06 1.37 0 2 12 4.70 1.10 0 2 -12 3.95 1.08 0 2 -12 3.78 0.63 0 2 -12 5.03 0.52 0 -2 -12 5.60 1.15 0 -2 12 4.34 1.60 0 -2 -12 4.21 0.99 0 -2 12 3.31 0.64 0 2 13 1132.47 31.63 0 2 13 1089.94 31.14 0 2 -13 1087.02 31.82 0 2 -13 1132.75 30.40 0 2 -13 1143.98 27.45 0 -2 -13 1098.12 32.13 0 -2 13 1057.27 30.29 0 -2 -13 1117.92 31.62 0 -2 13 1105.24 29.91 0 2 14 122.03 4.17 0 2 14 128.42 4.53 0 2 -14 127.30 4.46 0 2 -14 121.83 3.54 0 2 -14 122.72 2.70 0 -2 -14 127.55 5.07 0 -2 14 124.77 4.98 0 -2 -14 123.50 4.31 0 -2 14 117.10 3.56 0 2 15 34.76 1.93 0 2 15 29.03 1.95 0 2 -15 30.47 2.02 0 2 -15 33.01 0.83 0 2 -15 30.66 0.78 0 2 -15 33.84 1.50 0 -2 15 28.43 1.95 0 -2 15 34.69 1.98 0 -2 -15 35.24 1.92 0 -2 -15 31.08 1.97 0 2 16 318.70 10.02 0 2 16 315.47 10.17 0 2 -16 307.24 9.46 0 2 -16 335.25 6.38 0 2 -16 322.03 6.19 0 2 -16 320.41 9.03 0 -2 16 305.65 9.88 0 -2 16 315.15 9.09 0 -2 -16 312.62 9.48 0 -2 -16 315.91 9.60 0 2 17 9.22 1.36 0 2 17 7.14 1.34 0 2 -17 6.21 2.13 0 2 -17 7.21 1.32 0 -2 17 7.62 1.34 0 -2 17 7.18 1.36 0 -2 -17 7.15 1.93 0 -2 -17 6.55 1.37 0 2 18 105.47 4.67 0 2 18 101.28 4.02 0 2 -18 98.80 4.06 0 2 -18 103.84 3.86 0 -2 18 98.04 4.67 0 -2 18 100.32 3.43 0 -2 -18 106.62 4.07 0 -2 -18 99.95 4.65 0 2 19 16.18 1.69 0 2 19 16.62 1.73 0 2 -19 16.64 1.83 0 2 -19 16.70 1.26 0 -2 19 18.32 1.74 0 -2 19 15.78 1.27 0 -2 -19 18.57 1.74 0 -2 -19 15.94 2.35 0 2 20 23.22 2.55 0 2 20 20.10 1.88 0 2 -20 20.21 1.43 0 2 -20 23.97 2.15 0 -2 20 21.03 2.02 0 -2 -20 20.76 2.68 0 -2 -20 22.71 1.93 0 2 21 419.20 13.58 0 2 21 422.96 12.93 0 2 -21 429.59 12.33 0 2 -21 416.75 13.14 0 -2 21 412.15 12.24 0 -2 -21 425.10 13.24 0 -2 -21 416.29 12.80 0 2 22 1126.30 33.64 0 2 22 1124.09 33.80 0 2 -22 1137.08 33.57 0 2 -22 1146.46 34.85 0 -2 22 1137.07 33.59 0 -2 -22 1121.22 34.57 0 -2 -22 1129.35 33.93 0 2 23 48.01 2.82 0 2 23 52.07 3.09 0 2 -23 56.06 2.62 0 2 -23 45.61 3.01 0 -2 23 56.29 2.58 0 -2 -23 52.96 3.21 0 -2 -23 47.04 3.67 0 2 24 17.37 2.64 0 2 24 17.30 2.89 0 2 -24 18.49 1.57 0 2 -24 14.69 2.09 0 -2 24 18.35 1.63 0 -2 -24 17.81 2.08 0 -2 -24 15.99 1.84 0 2 25 1.33 1.23 0 2 25 0.33 1.38 0 2 -25 0.23 1.48 0 2 -25 1.34 1.34 0 -2 25 0.78 1.61 0 -2 -25 0.95 1.41 0 -2 -25 -0.13 1.27 0 2 26 577.48 17.86 0 2 26 562.98 18.74 0 2 -26 557.30 16.95 0 2 -26 560.77 18.03 0 -2 26 561.35 17.12 0 -2 -26 560.01 18.33 0 -2 -26 577.53 18.79 0 2 27 83.95 4.03 0 2 27 82.95 4.33 0 2 -27 81.44 4.40 0 2 -27 76.41 4.32 0 -2 27 80.29 3.92 0 -2 -27 82.96 4.47 0 -2 -27 76.59 3.89 0 2 28 1188.77 38.07 0 2 28 1169.17 37.05 0 2 -28 1170.40 36.07 0 2 -28 1196.23 38.04 0 -2 28 1161.35 36.31 0 -2 -28 1198.31 39.67 0 -2 -28 1161.78 36.82 0 2 29 48.32 3.17 0 2 29 47.40 3.50 0 2 -29 49.61 2.89 0 2 -29 45.13 3.55 0 -2 29 43.20 3.81 0 -2 -29 46.04 4.85 0 -2 -29 44.69 3.11 0 2 30 8.86 1.82 0 2 30 6.45 2.05 0 2 -30 6.00 1.55 0 2 -30 6.49 2.13 0 -2 -30 7.20 1.12 0 -2 -30 7.80 2.59 0 -2 -30 4.37 3.19 0 -2 30 4.47 2.35 0 2 31 82.34 5.17 0 2 31 83.06 5.88 0 2 -31 74.75 3.82 0 2 -31 84.40 4.75 0 -2 -31 76.11 3.78 0 -2 -31 77.75 4.03 0 -2 -31 79.14 5.91 0 -2 31 72.01 4.78 0 2 32 210.19 8.03 0 2 32 216.30 8.71 0 2 -32 208.98 7.82 0 2 -32 217.08 8.82 0 -2 -32 201.48 6.83 0 -2 -32 212.53 8.06 0 -2 -32 215.65 10.25 0 -2 32 210.83 7.97 0 2 33 67.20 3.84 0 2 33 60.01 4.24 0 2 -33 65.64 4.54 0 2 -33 67.85 4.48 0 -2 -33 65.98 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4.78 0 -3 -48 10.50 1.84 0 3 49 25.20 5.57 0 3 49 24.71 7.54 0 3 -49 25.66 3.86 0 3 -49 21.33 7.54 0 -3 49 22.39 3.70 0 -3 -49 22.87 5.25 0 -3 -49 14.59 2.89 0 3 50 73.43 5.90 0 3 50 72.44 7.38 0 3 -50 82.18 7.32 0 3 -50 62.06 7.27 0 -3 50 57.92 5.60 0 -3 -50 72.32 7.63 0 3 51 4.53 2.55 0 3 51 -4.32 3.62 0 3 -51 0.54 2.44 0 3 -51 2.24 3.60 0 -3 51 1.12 2.47 0 -3 -51 2.17 3.84 0 -3 -51 -1.31 1.84 0 3 52 116.29 9.39 0 3 52 117.28 12.61 0 3 -52 126.57 9.57 0 3 -52 102.47 7.27 0 -3 52 96.76 7.33 0 -3 -52 118.44 12.98 0 3 53 4.33 2.77 0 3 53 3.09 4.23 0 3 -53 2.40 4.36 0 3 -53 0.64 4.06 0 -3 53 3.43 2.88 0 -3 -53 2.99 6.90 0 -3 -53 1.35 2.09 0 4 0 144.40 5.56 0 4 0 147.97 5.20 0 -4 0 149.38 6.37 0 -4 0 146.80 4.84 0 -4 0 151.53 5.55 0 4 1 34.67 3.35 0 4 -1 34.68 2.37 0 4 -1 37.39 1.80 0 4 1 37.74 2.36 0 -4 1 33.28 2.03 0 -4 -1 33.26 3.23 0 -4 -1 33.93 1.91 0 -4 -1 36.77 1.91 0 -4 1 35.44 2.34 0 4 2 63.71 4.25 0 4 2 58.84 3.05 0 4 -2 70.22 2.94 0 4 -2 65.02 3.22 0 4 -2 62.66 2.51 0 -4 2 67.97 3.58 0 -4 -2 66.53 3.32 0 -4 2 70.09 3.26 0 -4 -2 66.49 3.17 0 -4 -2 65.00 3.20 0 4 3 250.96 8.63 0 4 3 239.33 7.90 0 4 -3 247.44 7.89 0 4 -3 247.55 8.81 0 4 -3 249.16 7.72 0 -4 3 241.09 7.80 0 -4 -3 254.10 8.70 0 -4 3 250.47 8.19 0 -4 -3 242.98 7.55 0 -4 -3 243.63 7.50 0 4 4 238.02 8.38 0 4 4 240.38 7.91 0 4 -4 239.54 7.75 0 4 -4 240.22 8.54 0 4 -4 232.98 6.99 0 -4 4 234.67 8.27 0 -4 -4 244.34 8.53 0 -4 4 238.39 8.48 0 -4 -4 236.05 7.97 0 -4 -4 225.83 7.44 0 4 5 20.19 2.22 0 4 5 22.83 2.13 0 4 -5 20.38 1.78 0 4 -5 21.70 1.78 0 4 -5 22.32 1.77 0 -4 5 20.60 1.78 0 -4 -5 20.62 2.19 0 -4 5 21.35 1.72 0 -4 -5 21.02 1.59 0 -4 -5 20.77 1.81 0 4 -6 30.77 2.05 0 4 6 31.84 1.94 0 4 6 36.55 2.73 0 4 -6 33.84 2.10 0 4 -6 38.09 2.34 0 4 -6 31.32 1.63 0 -4 -6 37.76 2.64 0 -4 6 34.26 2.12 0 -4 -6 32.20 2.58 0 -4 -6 33.50 1.70 0 -4 6 36.64 2.96 0 4 -7 327.80 9.82 0 4 7 326.62 10.16 0 4 7 339.13 11.41 0 4 -7 325.25 10.69 0 4 -7 339.25 11.60 0 4 -7 322.11 9.66 0 -4 -7 340.08 11.41 0 -4 7 335.64 10.41 0 -4 -7 329.21 10.26 0 -4 -7 325.63 9.76 0 -4 7 326.78 10.46 0 4 -8 206.57 6.51 0 4 8 205.80 6.80 0 4 8 205.17 7.69 0 4 -8 193.54 6.50 0 4 -8 198.06 7.07 0 4 -8 196.65 5.99 0 -4 -8 199.20 7.51 0 -4 8 192.02 6.45 0 -4 -8 201.01 6.73 0 -4 -8 192.47 6.14 0 -4 8 194.82 6.90 0 4 9 459.79 14.40 0 4 9 468.32 15.31 0 4 -9 430.74 12.64 0 4 -9 449.55 14.54 0 4 -9 467.81 14.21 0 4 -9 434.93 12.82 0 -4 -9 471.34 15.38 0 -4 -9 445.47 13.87 0 -4 9 461.20 15.36 0 -4 -9 437.36 12.36 0 4 10 130.48 4.89 0 4 10 126.24 5.60 0 4 -10 134.95 4.58 0 4 -10 128.74 6.10 0 4 -10 122.93 4.42 0 4 -10 121.91 4.04 0 -4 10 128.50 5.17 0 -4 -10 127.07 5.61 0 -4 -10 131.30 5.01 0 -4 -10 116.96 3.78 0 4 11 3.08 1.23 0 4 11 3.09 1.79 0 4 -11 2.54 1.11 0 4 -11 2.58 1.48 0 4 -11 2.67 1.41 0 4 -11 2.81 1.15 0 -4 11 2.94 2.15 0 -4 -11 2.57 1.72 0 -4 -11 3.16 1.28 0 -4 -11 2.96 0.98 0 4 12 67.31 4.02 0 4 12 70.17 4.15 0 4 -12 67.14 2.68 0 4 -12 69.24 4.69 0 4 -12 69.94 3.38 0 4 -12 65.86 2.61 0 -4 12 69.04 3.61 0 -4 -12 70.60 4.11 0 -4 -12 69.67 3.40 0 -4 -12 61.55 2.71 0 4 13 421.11 13.36 0 4 13 442.02 14.96 0 4 -13 425.09 12.43 0 4 -13 440.17 14.54 0 4 -13 415.99 12.41 0 4 -13 393.19 12.18 0 -4 13 435.82 14.24 0 -4 -13 436.44 14.78 0 -4 -13 427.11 13.81 0 -4 -13 408.04 11.71 0 4 14 257.70 8.65 0 4 14 255.60 9.60 0 4 -14 255.97 7.61 0 4 -14 248.46 10.08 0 4 -14 238.55 7.33 0 4 -14 241.43 7.44 0 -4 14 241.69 9.68 0 -4 -14 250.60 9.41 0 -4 -14 253.11 9.81 0 -4 -14 227.22 6.97 0 4 15 231.18 9.04 0 4 15 242.37 9.21 0 4 -15 234.48 7.41 0 4 -15 243.91 8.94 0 4 -15 224.21 6.87 0 4 -15 220.72 7.34 0 -4 15 243.10 8.73 0 -4 -15 243.65 9.40 0 -4 -15 234.39 8.42 0 -4 -15 215.66 6.60 0 4 16 12.52 1.84 0 4 16 17.04 2.57 0 4 -16 17.99 2.26 0 4 -16 13.77 1.29 0 4 -16 14.44 1.09 0 4 -16 11.95 1.16 0 -4 16 17.44 3.29 0 -4 -16 15.51 1.31 0 -4 -16 14.95 1.94 0 -4 -16 17.38 2.67 0 4 -17 -0.29 1.14 0 4 17 0.21 2.63 0 4 17 1.09 1.82 0 4 -17 -0.40 1.15 0 4 -17 0.02 2.28 0 4 -17 -0.18 2.25 0 4 -17 -0.03 0.59 0 -4 -17 1.26 1.72 0 -4 -17 1.17 0.77 0 -4 -17 0.97 1.97 0 -4 17 0.04 1.49 0 4 18 236.02 8.44 0 4 18 237.80 10.94 0 4 -18 232.86 9.00 0 4 -18 216.54 7.55 0 4 -18 214.78 6.73 0 4 -18 219.82 7.58 0 -4 18 239.26 9.01 0 -4 -18 207.59 6.30 0 -4 -18 235.86 8.78 0 -4 -18 234.75 9.26 0 4 -19 322.28 10.28 0 4 19 341.14 13.98 0 4 19 335.40 12.37 0 4 -19 297.67 10.28 0 4 -19 346.19 12.25 0 4 -19 300.42 9.11 0 4 -19 308.70 9.14 0 -4 -19 342.24 12.50 0 -4 -19 307.91 8.89 0 -4 -19 330.45 12.60 0 -4 19 348.47 13.37 0 4 -20 16.66 1.33 0 4 20 19.31 3.02 0 4 20 23.37 2.37 0 4 -20 17.47 2.63 0 4 -20 20.06 1.09 0 4 -20 26.84 2.27 0 -4 20 16.93 2.67 0 -4 -20 24.42 2.52 0 -4 -20 18.00 3.02 0 4 -21 92.29 3.14 0 4 21 107.22 5.72 0 4 21 103.69 5.90 0 4 -21 109.81 6.83 0 4 -21 94.27 2.93 0 4 -21 99.71 4.36 0 -4 21 111.03 5.37 0 -4 -21 106.94 6.29 0 -4 -21 107.16 7.11 0 4 22 105.58 5.77 0 4 22 102.55 5.03 0 4 -22 92.02 2.82 0 4 -22 106.75 5.50 0 4 -22 93.89 4.37 0 4 -22 87.87 2.62 0 -4 -22 85.13 3.21 0 -4 -22 97.84 5.11 0 -4 -22 102.52 7.12 0 4 23 13.78 2.90 0 4 23 9.83 3.29 0 4 -23 10.21 0.76 0 4 -23 14.72 2.68 0 4 -23 8.28 1.88 0 4 -23 10.18 0.73 0 -4 -23 10.54 0.83 0 -4 -23 9.65 2.31 0 -4 -23 13.07 2.57 0 4 24 105.60 6.07 0 4 24 103.01 5.24 0 4 -24 99.47 5.75 0 4 -24 105.07 4.68 0 -4 -24 107.43 6.75 0 -4 -24 105.87 5.90 0 4 25 6.42 3.94 0 4 25 5.89 3.15 0 4 -25 6.33 2.47 0 4 -25 3.79 1.81 0 -4 -25 6.11 2.27 0 -4 -25 6.87 2.64 0 4 26 447.15 16.41 0 4 26 421.61 15.28 0 4 -26 447.33 18.09 0 4 -26 388.56 12.96 0 -4 -26 408.07 15.54 0 -4 -26 429.85 16.45 0 4 27 55.04 4.62 0 4 27 56.90 4.15 0 4 -27 57.44 6.12 0 4 -27 51.60 2.87 0 -4 -27 55.42 5.81 0 -4 -27 55.07 6.38 0 4 28 52.29 4.60 0 4 28 48.54 5.35 0 4 -28 49.33 6.31 0 4 -28 47.21 3.69 0 -4 -28 48.55 5.55 0 -4 -28 54.81 6.03 0 4 29 96.00 5.97 0 4 29 93.48 5.46 0 4 -29 90.99 5.96 0 4 -29 86.67 4.05 0 -4 -29 93.47 5.75 0 -4 -29 93.56 5.92 0 4 30 48.95 6.28 0 4 30 39.23 5.23 0 4 -30 41.88 4.30 0 4 -30 36.53 2.61 0 -4 -30 41.72 4.07 0 -4 -30 40.94 4.19 0 4 31 63.54 6.82 0 4 31 59.07 4.57 0 4 -31 58.66 5.08 0 4 -31 52.27 3.98 0 -4 -31 57.68 4.77 0 -4 -31 63.41 4.96 0 4 32 53.98 4.73 0 4 32 51.81 4.35 0 4 -32 45.89 3.06 0 4 -32 48.02 4.87 0 -4 32 41.89 3.13 0 -4 -32 52.54 6.35 0 -4 -32 53.85 6.62 0 4 33 67.87 5.25 0 4 33 62.70 6.68 0 4 -33 71.09 5.52 0 4 -33 58.02 4.37 0 -4 33 50.54 3.53 0 -4 -33 69.09 7.17 0 4 34 1.94 2.82 0 4 34 2.83 2.68 0 4 -34 2.79 1.54 0 4 -34 1.52 3.06 0 -4 -34 2.22 1.00 0 -4 -34 4.41 2.81 0 -4 -34 4.05 4.11 0 -4 34 2.95 2.61 0 4 35 394.12 18.06 0 4 35 377.96 15.33 0 4 -35 331.35 12.74 0 4 -35 401.41 16.69 0 -4 35 303.84 12.79 0 -4 -35 376.96 16.08 0 -4 -35 398.88 16.11 0 4 36 29.77 4.36 0 4 36 28.98 4.22 0 4 -36 28.92 2.86 0 4 -36 33.78 4.60 0 -4 36 24.04 4.03 0 -4 -36 32.37 4.42 0 -4 -36 32.44 4.27 0 4 37 48.98 5.12 0 4 37 52.62 4.91 0 4 -37 49.38 5.56 0 4 -37 44.65 3.38 0 -4 37 44.54 4.81 0 -4 -37 51.15 5.18 0 4 38 -1.50 2.71 0 4 38 4.16 4.02 0 4 -38 1.61 1.49 0 4 -38 -3.37 3.01 0 -4 38 0.21 1.65 0 -4 -38 1.38 2.72 0 -4 -38 1.06 0.96 0 4 39 59.85 7.38 0 4 39 57.33 5.37 0 4 -39 59.03 5.94 0 4 -39 44.74 3.66 0 -4 39 41.18 3.78 0 -4 -39 55.20 5.57 0 4 40 18.26 4.04 0 4 40 20.90 4.17 0 4 -40 21.33 4.69 0 4 -40 16.27 2.54 0 -4 40 14.53 3.94 0 -4 -40 24.80 4.40 0 4 41 252.70 12.15 0 4 41 239.18 14.46 0 4 -41 250.19 12.76 0 4 -41 201.32 10.62 0 -4 41 186.61 10.81 0 -4 -41 241.82 12.56 0 4 42 33.69 4.79 0 4 42 37.98 5.12 0 4 -42 33.89 5.43 0 4 -42 32.00 3.39 0 -4 42 30.74 3.60 0 -4 -42 40.59 5.40 0 4 43 26.41 6.44 0 4 43 22.15 4.73 0 4 -43 25.69 5.10 0 4 -43 20.77 4.14 0 -4 43 19.61 3.01 0 -4 -43 22.92 4.86 0 4 44 33.19 4.99 0 4 44 38.05 7.56 0 4 -44 39.40 8.33 0 4 -44 25.08 3.26 0 -4 44 22.15 3.42 0 -4 -44 34.27 5.39 0 4 45 39.43 5.20 0 4 45 35.81 5.46 0 4 -45 37.68 8.82 0 4 -45 27.63 4.99 0 -4 45 28.42 3.61 0 -4 -45 39.77 5.78 0 4 46 73.27 8.75 0 4 46 71.71 6.99 0 4 -46 68.11 10.13 0 4 -46 55.83 4.70 0 -4 46 51.40 4.76 0 -4 -46 71.63 7.20 0 4 47 42.53 5.37 0 4 47 36.56 8.38 0 4 -47 42.40 6.52 0 4 -47 30.75 5.08 0 -4 47 33.48 5.32 0 -4 -47 45.22 6.38 0 4 48 40.90 5.29 0 4 48 37.96 6.00 0 4 -48 50.97 6.53 0 4 -48 28.28 3.73 0 -4 48 22.28 5.31 0 -4 -48 37.40 6.17 0 4 49 15.47 6.37 0 4 49 15.68 5.15 0 4 -49 15.66 5.69 0 4 -49 12.48 2.98 0 -4 49 14.15 4.52 0 -4 -49 16.62 5.32 0 5 0 0.24 1.35 0 5 0 0.49 0.76 0 -5 0 -0.29 1.41 0 -5 0 -1.42 1.34 0 5 1 56.27 3.62 0 5 -1 54.70 3.54 0 5 1 52.42 2.64 0 5 -1 53.69 2.58 0 -5 1 48.05 2.82 0 -5 -1 53.13 2.87 0 -5 1 55.28 3.56 0 -5 -1 55.69 4.68 0 5 2 247.10 10.66 0 5 -2 241.07 10.14 0 5 2 230.28 8.38 0 5 -2 223.73 8.14 0 -5 2 240.10 8.41 0 -5 -2 235.66 8.05 0 -5 2 244.58 9.09 0 -5 -2 253.39 10.64 0 5 -3 306.70 11.75 0 5 3 301.75 12.37 0 5 3 296.70 10.44 0 5 -3 290.13 9.97 0 -5 -3 301.87 11.21 0 -5 -3 291.43 10.07 0 -5 -3 299.04 10.63 0 -5 3 289.95 10.79 0 5 -4 204.55 7.84 0 5 4 212.22 9.76 0 5 4 191.51 6.76 0 5 -4 172.91 6.10 0 5 -4 192.49 7.16 0 -5 -4 213.25 8.59 0 -5 -4 195.12 7.04 0 -5 4 205.88 7.57 0 -5 -4 199.02 7.44 0 5 -5 57.48 3.46 0 5 5 59.05 4.13 0 5 5 60.55 3.02 0 5 -5 59.09 2.74 0 5 -5 64.64 3.40 0 -5 -5 58.00 3.96 0 -5 -5 62.10 3.86 0 -5 5 55.61 3.24 0 -5 -5 53.98 2.72 0 5 6 -0.07 1.58 0 5 6 0.90 1.87 0 5 -6 0.30 1.25 0 5 -6 -0.09 1.32 0 5 -6 1.38 1.95 0 5 -6 2.36 1.24 0 -5 -6 -0.16 1.76 0 -5 -6 1.48 1.68 0 -5 6 1.06 1.98 0 -5 -6 0.23 1.31 0 5 7 32.52 2.28 0 5 7 32.31 3.33 0 5 -7 32.66 2.39 0 5 -7 32.25 2.62 0 5 -7 31.30 2.46 0 5 -7 29.71 2.39 0 -5 -7 34.38 3.25 0 -5 -7 32.53 2.94 0 -5 7 30.82 2.59 0 -5 -7 29.31 2.41 0 5 8 215.01 7.76 0 5 8 234.60 9.42 0 5 -8 196.99 6.73 0 5 -8 234.01 9.54 0 5 -8 222.95 8.04 0 5 -8 210.77 6.97 0 -5 -8 237.83 9.53 0 -5 -8 216.31 7.97 0 -5 8 223.14 8.41 0 -5 -8 212.14 7.16 0 5 9 -0.18 1.78 0 5 9 -0.65 1.91 0 5 -9 1.18 1.17 0 5 -9 1.30 1.45 0 5 -9 -0.04 1.79 0 5 -9 0.56 0.78 0 -5 -9 0.11 1.89 0 -5 -9 0.39 1.14 0 -5 9 -0.22 2.06 0 -5 -9 1.16 1.17 0 5 10 9.56 1.69 0 5 10 9.99 2.54 0 5 -10 9.66 1.54 0 5 -10 11.51 3.01 0 5 -10 9.45 1.59 0 5 -10 9.14 1.18 0 -5 -10 9.24 2.63 0 -5 -10 9.92 1.66 0 -5 10 10.21 1.97 0 -5 -10 9.27 1.56 0 5 11 41.94 3.50 0 5 11 43.56 3.85 0 5 -11 36.71 2.03 0 5 -11 45.47 3.24 0 5 -11 40.06 3.28 0 5 -11 34.96 2.47 0 -5 -11 42.54 3.75 0 -5 -11 39.11 2.78 0 -5 11 41.94 3.19 0 -5 -11 39.28 1.99 0 5 -12 3.03 1.20 0 5 12 3.14 2.20 0 5 12 2.09 1.38 0 5 -12 3.39 1.82 0 5 -12 2.08 1.27 0 5 -12 1.02 1.31 0 -5 -12 2.62 2.28 0 -5 12 5.00 2.62 0 -5 -12 2.98 2.21 0 5 13 0.45 1.75 0 5 13 2.32 1.88 0 5 -13 -0.48 0.68 0 5 -13 -0.92 1.50 0 5 -13 -1.16 0.91 0 5 -13 0.00 1.04 0 -5 -13 2.23 1.88 0 -5 -13 0.23 1.87 0 -5 13 -0.78 2.24 0 -5 -13 0.46 0.93 0 5 14 4.72 1.69 0 5 14 6.86 2.56 0 5 -14 5.44 1.42 0 5 -14 11.05 3.22 0 5 -14 6.40 1.86 0 5 -14 4.37 1.00 0 -5 -14 6.66 2.67 0 -5 -14 4.08 2.50 0 -5 14 5.97 2.06 0 -5 -14 5.40 1.23 0 5 15 128.87 6.60 0 5 15 135.07 7.07 0 5 -15 112.25 4.25 0 5 -15 140.23 6.58 0 5 -15 121.36 4.73 0 5 -15 109.27 4.84 0 -5 -15 139.96 6.91 0 -5 -15 125.03 5.75 0 -5 15 134.66 6.26 0 -5 -15 112.57 4.23 0 5 16 21.31 2.37 0 5 16 21.40 3.43 0 5 -16 19.07 1.48 0 5 -16 22.13 4.10 0 5 -16 19.32 1.68 0 5 -16 18.12 2.04 0 -5 16 22.03 4.02 0 -5 -16 19.69 3.31 0 -5 -16 21.15 2.48 0 -5 -16 16.82 1.22 0 5 17 0.83 2.32 0 5 17 -0.28 2.30 0 5 -17 1.70 1.25 0 5 -17 1.02 1.91 0 5 -17 0.74 0.86 0 5 -17 -0.09 1.25 0 -5 17 0.78 1.85 0 -5 -17 0.52 2.30 0 -5 -17 1.12 2.42 0 -5 -17 0.62 0.83 0 5 -18 144.59 5.82 0 5 18 164.53 8.17 0 5 18 154.53 6.86 0 5 -18 165.53 7.74 0 5 -18 140.21 5.65 0 -5 -18 171.66 8.36 0 -5 -18 151.30 7.02 0 -5 18 168.09 7.74 0 5 19 137.11 7.51 0 5 19 129.76 7.24 0 5 -19 127.67 8.24 0 5 -19 109.64 4.33 0 5 -19 119.55 5.21 0 -5 -19 135.12 7.49 0 -5 -19 125.12 7.42 0 5 20 27.94 5.68 0 5 20 26.70 2.84 0 5 -20 32.05 3.51 0 5 -20 25.35 1.63 0 5 -20 21.89 1.73 0 5 -20 21.83 1.79 0 5 -20 23.66 2.07 0 -5 -20 20.60 1.51 0 -5 -20 25.63 2.98 0 -5 -20 31.07 3.95 0 5 21 87.20 7.73 0 5 21 84.58 4.78 0 5 -21 85.37 5.42 0 5 -21 73.32 3.33 0 5 -21 74.86 3.34 0 5 -21 69.49 3.32 0 5 -21 64.30 3.25 0 -5 -21 85.32 6.35 0 -5 -21 86.46 5.95 0 5 22 4.43 3.86 0 5 22 0.15 1.72 0 5 -22 2.67 2.10 0 5 -22 0.56 0.56 0 5 -22 0.86 0.86 0 5 -22 0.47 0.95 0 5 -22 -0.15 0.91 0 -5 -22 0.74 0.61 0 -5 -22 0.41 1.84 0 -5 -22 2.22 2.58 0 5 23 57.70 5.25 0 5 23 57.64 4.07 0 5 -23 63.26 6.29 0 5 -23 41.57 2.68 0 5 -23 44.21 2.15 0 5 -23 48.11 2.67 0 -5 -23 54.54 5.62 0 -5 -23 58.88 7.22 0 5 24 403.01 16.48 0 5 24 369.63 15.84 0 5 -24 403.13 15.98 0 -5 -24 414.15 18.68 0 -5 -24 367.46 14.88 0 5 25 57.53 5.50 0 5 25 61.89 4.42 0 5 -25 52.18 4.94 0 5 -25 44.63 2.91 0 5 -25 51.20 3.61 0 -5 -25 51.65 7.30 0 -5 -25 59.66 4.73 0 5 26 97.10 6.65 0 5 26 87.42 5.29 0 5 -26 91.62 6.24 0 5 -26 67.50 3.81 0 5 -26 69.84 4.24 0 -5 -26 95.10 6.79 0 -5 -26 86.13 7.26 0 5 27 78.90 6.24 0 5 27 74.39 5.05 0 5 -27 79.76 5.76 0 5 -27 53.85 3.95 0 5 -27 59.30 3.33 0 -5 -27 79.28 6.40 0 -5 -27 73.24 5.25 0 5 28 67.16 8.51 0 5 28 61.26 4.80 0 5 -28 69.52 7.63 0 5 -28 51.34 3.84 0 5 -28 49.91 3.05 0 -5 -28 73.88 6.09 0 -5 -28 63.40 5.11 0 5 29 177.41 12.31 0 5 29 167.62 10.17 0 5 -29 180.56 11.74 0 5 -29 143.09 6.90 0 -5 -29 178.11 10.82 0 -5 -29 178.10 9.86 0 5 30 314.02 14.34 0 5 30 295.59 12.92 0 5 -30 331.15 16.86 0 -5 -30 331.30 14.76 0 -5 -30 290.70 13.34 0 5 31 82.57 6.86 0 5 31 87.40 5.98 0 5 -31 79.33 6.53 0 -5 -31 90.12 6.39 0 5 32 7.04 3.80 0 5 32 11.35 4.61 0 5 -32 8.21 3.62 0 5 -32 6.45 2.06 0 -5 -32 8.73 3.22 0 5 33 9.41 3.67 0 5 33 6.03 2.99 0 5 -33 4.02 3.54 0 5 -33 3.28 2.01 0 -5 -33 5.03 4.58 0 5 34 34.55 7.52 0 5 34 30.98 4.24 0 5 -34 33.61 5.04 0 -5 -34 27.05 6.32 0 5 35 39.98 7.93 0 5 35 41.50 6.26 0 5 -35 41.07 5.36 0 5 -35 25.28 3.29 0 -5 -35 40.61 4.84 0 5 36 23.41 4.65 0 5 36 18.41 3.88 0 5 -36 18.21 4.69 0 5 -36 13.43 2.02 0 -5 -36 19.67 4.12 0 5 37 1.61 3.24 0 5 37 1.63 2.69 0 5 -37 0.68 3.33 0 5 -37 0.58 1.85 0 -5 -37 -0.02 2.85 0 5 38 38.32 5.65 0 5 38 41.99 6.98 0 5 -38 37.83 5.70 0 5 -38 24.25 2.63 0 -5 -38 38.57 5.11 0 5 39 6.35 5.81 0 5 39 2.27 3.28 0 5 -39 8.28 3.93 0 5 -39 2.28 2.29 0 -5 -39 2.92 3.49 0 5 40 29.66 5.14 0 5 40 23.96 4.57 0 5 -40 27.90 5.48 0 5 -40 16.77 2.41 0 -5 -40 24.85 4.81 0 5 41 100.65 8.11 0 5 41 89.40 9.74 0 5 -41 96.91 8.28 0 5 -41 66.47 5.31 0 -5 -41 91.33 10.20 0 5 42 9.56 4.30 0 5 42 10.90 3.93 0 5 -42 6.08 4.67 0 5 -42 4.76 1.85 0 -5 -42 9.37 6.22 0 5 43 1.68 6.13 0 5 43 3.86 3.63 0 5 -43 5.61 4.38 0 5 -43 2.64 2.43 0 -5 -43 5.20 5.89 0 6 0 1.91 1.47 0 6 0 2.09 2.07 0 -6 0 0.15 1.34 0 6 -1 4.40 1.64 0 6 1 5.29 2.37 0 6 1 3.88 1.19 0 6 -1 3.47 3.38 0 -6 -1 5.08 2.12 0 -6 1 4.38 1.56 0 6 -2 14.46 1.55 0 6 2 25.77 3.18 0 6 2 16.91 2.43 0 6 -2 22.38 2.90 0 6 -2 15.95 2.31 0 -6 -2 21.43 2.80 0 -6 2 19.46 2.22 0 6 -3 37.36 2.86 0 6 3 46.94 4.06 0 6 3 37.90 2.55 0 6 -3 42.40 3.61 0 6 -3 33.87 2.31 0 -6 -3 40.13 3.42 0 -6 3 43.47 4.08 0 6 -4 19.68 2.24 0 6 4 25.70 4.80 0 6 4 24.28 2.77 0 6 -4 26.73 2.97 0 6 -4 18.86 2.31 0 -6 -4 22.97 2.11 0 -6 4 25.66 3.49 0 6 -5 0.89 0.79 0 6 5 -1.38 3.46 0 6 5 1.30 1.06 0 6 -5 -1.22 2.62 0 6 -5 0.92 0.84 0 -6 -5 0.63 1.08 0 -6 5 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-12 1 -5 18.86 5.14 -12 -1 -5 13.20 5.56 12 -1 5 23.41 7.26 -12 -1 -5 15.75 5.53 -12 -1 -5 18.33 5.02 12 1 6 0.46 3.30 -12 1 -6 -3.34 3.53 -12 1 -6 -0.54 3.08 -12 -1 -6 -3.82 5.49 -12 -1 -6 -0.94 2.70 -12 -1 -6 -0.26 2.57 12 -1 6 1.27 3.25 12 1 7 7.06 4.01 -12 1 -7 6.22 5.79 -12 1 -7 4.52 4.25 -12 1 -7 7.24 4.26 -12 -1 -7 8.51 4.94 12 -1 7 4.71 4.06 -12 -1 -7 8.03 4.83 -12 -1 -7 5.90 4.19 12 1 8 -0.59 3.05 -12 1 -8 0.44 3.07 -12 1 -8 0.72 3.28 -12 -1 -8 2.14 3.16 -12 -1 -8 -0.93 2.46 12 -1 8 0.21 3.02 -12 -1 -8 -1.35 2.39 12 1 9 71.68 9.96 -12 1 -9 72.88 6.97 -12 1 -9 65.44 7.35 -12 1 -9 68.94 10.43 -12 -1 -9 64.31 6.23 12 -1 9 67.49 9.58 -12 -1 -9 61.98 7.82 -12 -1 -9 71.08 10.07 12 1 10 -0.15 5.46 -12 1 -10 -0.12 5.27 -12 1 -10 -2.66 3.74 -12 1 -10 -3.00 4.16 -12 -1 -10 -1.27 3.11 12 -1 10 0.82 5.54 -12 -1 -10 -3.21 2.96 -12 -1 -10 -0.35 3.67 12 1 11 12.29 4.48 -12 1 -11 12.55 4.34 -12 1 -11 12.24 4.55 -12 1 -11 8.43 7.21 -12 -1 -11 9.38 3.83 12 -1 11 12.28 4.39 -12 -1 -11 9.55 5.41 -12 -1 -11 14.59 4.47 12 1 12 3.04 3.13 -12 1 -12 1.48 2.93 -12 -1 -12 -0.43 4.89 12 -1 12 0.49 3.17 -12 -1 -12 -3.53 4.09 -12 -1 -12 -1.66 2.58 12 1 13 84.88 7.46 -12 1 -13 84.05 7.38 -12 1 -13 85.74 11.42 -12 -1 -13 85.47 7.88 -12 -1 -13 81.61 7.04 12 2 -5 16.74 4.67 -12 2 5 16.75 4.68 -12 2 5 8.99 6.33 12 -2 -5 15.22 7.71 -12 -2 5 13.89 6.94 12 2 -4 35.35 7.81 -12 2 4 33.83 5.42 -12 2 4 42.23 10.24 -12 2 4 28.83 6.62 12 -2 -4 29.19 5.73 -12 -2 4 23.40 3.34 -12 -2 4 20.47 4.53 -12 -2 4 35.37 5.42 12 2 -3 9.20 4.39 -12 2 3 14.07 6.63 -12 2 3 18.24 5.98 -12 2 3 33.27 9.19 12 -2 -3 10.32 4.57 -12 -2 3 4.49 2.54 -12 -2 3 4.81 2.46 -12 -2 3 10.49 4.39 12 2 -2 114.09 8.51 -12 2 2 109.85 13.23 -12 2 2 110.64 9.74 -12 2 2 120.98 8.72 -12 -2 2 113.77 8.69 -12 -2 2 71.05 7.22 12 -2 -2 101.88 8.76 12 2 -1 -0.52 5.13 -12 2 1 2.15 3.33 -12 2 1 -0.18 4.01 12 -2 -1 2.47 5.48 -12 -2 1 1.73 5.18 -12 -2 1 0.26 2.97 -12 -2 1 0.30 1.85 12 2 0 11.23 4.22 -12 2 0 11.90 6.15 -12 2 0 5.42 7.74 -12 2 0 9.69 4.86 12 -2 0 4.05 6.50 -12 -2 0 3.69 2.40 -12 -2 0 4.97 3.43 -12 -2 0 14.08 6.71 12 2 1 18.62 4.88 -12 2 -1 19.13 4.65 -12 2 -1 28.23 6.94 -12 2 -1 14.34 6.19 12 -2 1 19.20 5.04 -12 -2 -1 12.43 2.93 -12 -2 -1 10.33 2.81 -12 -2 -1 19.81 5.00 12 2 2 72.37 9.73 -12 2 -2 69.55 6.68 -12 2 -2 76.30 11.97 -12 2 -2 62.49 8.07 -12 -2 -2 51.31 6.21 12 -2 2 57.28 6.93 -12 -2 -2 45.86 5.95 -12 -2 -2 70.05 7.21 12 2 3 11.37 4.45 -12 2 -3 8.71 6.33 -12 -2 -3 9.56 4.72 12 -2 3 8.07 4.53 -12 -2 -3 3.73 4.25 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 87620 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 +X,+Y,+Z 2 1/2-X,1/2+Y,1/2-Z 3 -X,-Y,-Z 4 -1/2+X,-1/2-Y,-1/2+Z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Se1 Se 0.38682(2) 0.01952(3) 0.36159(2) 0.02064(6) Uani 1 1 d . . . . . Se2 Se 0.22818(2) 0.43684(3) 0.32280(2) 0.02065(6) Uani 1 1 d . . . . . O1 O 0.29283(13) 0.3313(2) 0.41230(3) 0.0219(3) Uani 1 1 d . . . . . O2 O 0.49896(15) 0.5022(2) 0.40135(3) 0.0272(3) Uani 1 1 d . . . . . O3 O 0.43048(15) 0.0800(2) 0.45219(3) 0.0291(3) Uani 1 1 d . . . . . C1 C 0.27378(18) 0.2947(3) 0.35983(4) 0.0187(3) Uani 1 1 d . . . . . C2 C 0.23270(18) 0.3996(3) 0.38463(4) 0.0202(4) Uani 1 1 d . . . . . C3 C 0.11940(19) 0.5712(3) 0.38855(4) 0.0197(4) Uani 1 1 d . . . . . C4 C 0.13886(19) 0.7698(3) 0.40598(4) 0.0223(4) Uani 1 1 d . . . . . H4 H 0.2270 0.7997 0.4151 0.027 Uiso 1 1 calc R U . . . C5 C 0.0297(2) 0.9236(3) 0.41002(4) 0.0235(4) Uani 1 1 d . . . . . H5 H 0.0451 1.0599 0.4216 0.028 Uiso 1 1 calc R U . . . C6 C -0.1017(2) 0.8840(3) 0.39761(4) 0.0232(4) Uani 1 1 d . . . . . C7 C -0.1206(2) 0.6828(4) 0.38048(4) 0.0256(4) Uani 1 1 d . . . . . H7 H -0.2096 0.6507 0.3719 0.031 Uiso 1 1 calc R U . . . C8 C -0.0119(2) 0.5296(3) 0.37580(4) 0.0234(4) Uani 1 1 d . . . . . H8 H -0.0267 0.3952 0.3638 0.028 Uiso 1 1 calc R U . . . C9 C -0.2207(2) 1.0501(4) 0.40222(5) 0.0312(5) Uani 1 1 d . . . . . H9A H -0.3060 0.9612 0.4055 0.037 Uiso 1 1 calc R U . . . H9B H -0.2331 1.1488 0.3846 0.037 Uiso 1 1 calc R U . . . H9C H -0.2004 1.1482 0.4196 0.037 Uiso 1 1 calc R U . . . C10 C 0.52189(19) 0.1020(3) 0.33281(4) 0.0213(4) Uani 1 1 d . . . . . C11 C 0.5519(2) -0.0583(3) 0.31098(4) 0.0272(4) Uani 1 1 d . . . . . H11 H 0.5012 -0.2002 0.3095 0.033 Uiso 1 1 calc R U . . . C12 C 0.6570(2) -0.0103(4) 0.29108(5) 0.0311(5) Uani 1 1 d . . . . . H12 H 0.6799 -0.1216 0.2764 0.037 Uiso 1 1 calc R U . . . C13 C 0.7278(2) 0.1984(4) 0.29270(4) 0.0296(4) Uani 1 1 d . . . . . H13 H 0.7994 0.2306 0.2791 0.036 Uiso 1 1 calc R U . . . C14 C 0.6948(2) 0.3613(4) 0.31410(4) 0.0285(4) Uani 1 1 d . . . . . H14 H 0.7425 0.5063 0.3149 0.034 Uiso 1 1 calc R U . . . C15 C 0.5924(2) 0.3131(3) 0.33441(4) 0.0256(4) Uani 1 1 d . . . . . H15 H 0.5706 0.4236 0.3493 0.031 Uiso 1 1 calc R U . . . C16 C 0.13451(18) 0.1862(3) 0.30253(4) 0.0208(4) Uani 1 1 d . . . . . C17 C 0.0675(2) 0.0101(3) 0.31755(4) 0.0247(4) Uani 1 1 d . . . . . H17 H 0.0675 0.0089 0.3386 0.030 Uiso 1 1 calc R U . . . C18 C 0.0002(2) -0.1650(4) 0.30154(5) 0.0298(4) Uani 1 1 d . . . . . H18 H -0.0456 -0.2866 0.3118 0.036 Uiso 1 1 calc R U . . . C19 C -0.0010(2) -0.1642(4) 0.27097(5) 0.0346(5) Uani 1 1 d . . . . . H19 H -0.0456 -0.2866 0.2602 0.042 Uiso 1 1 calc R U . . . C20 C 0.0629(2) 0.0150(4) 0.25603(5) 0.0341(5) Uani 1 1 d . . . . . H20 H 0.0600 0.0180 0.2350 0.041 Uiso 1 1 calc R U . . . C21 C 0.1317(2) 0.1917(4) 0.27170(4) 0.0280(4) Uani 1 1 d . . . . . H21 H 0.1762 0.3145 0.2614 0.034 Uiso 1 1 calc R U . . . C22 C 0.42871(19) 0.3872(3) 0.41727(4) 0.0212(4) Uani 1 1 d . . . . . C23 C 0.48032(19) 0.2684(3) 0.44622(4) 0.0221(4) Uani 1 1 d . . . . . C24 C 0.58978(19) 0.3832(3) 0.46446(4) 0.0217(4) Uani 1 1 d . . . . . C25 C 0.6493(2) 0.5973(4) 0.45730(4) 0.0302(4) Uani 1 1 d . . . . . H25 H 0.6210 0.6755 0.4396 0.036 Uiso 1 1 calc R U . . . C26 C 0.7493(2) 0.6961(4) 0.47580(5) 0.0329(5) Uani 1 1 d . . . . . H26 H 0.7902 0.8404 0.4704 0.039 Uiso 1 1 calc R U . . . C27 C 0.7915(2) 0.5892(4) 0.50211(4) 0.0277(4) Uani 1 1 d . . . . . C28 C 0.7310(2) 0.3763(4) 0.50928(4) 0.0280(4) Uani 1 1 d . . . . . H28 H 0.7583 0.2999 0.5272 0.034 Uiso 1 1 calc R U . . . C29 C 0.6319(2) 0.2744(4) 0.49082(4) 0.0261(4) Uani 1 1 d . . . . . H29 H 0.5922 0.1291 0.4961 0.031 Uiso 1 1 calc R U . . . C30 C 0.8966(2) 0.7035(4) 0.52248(5) 0.0351(5) Uani 1 1 d . . . . . H30A H 0.9731 0.7653 0.5108 0.042 Uiso 1 1 calc R U . . . H30B H 0.9329 0.5885 0.5367 0.042 Uiso 1 1 calc R U . . . H30C H 0.8523 0.8312 0.5332 0.042 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Se1 0.02029(10) 0.01862(10) 0.02301(10) 0.00226(7) 0.00073(7) 0.00113(7) Se2 0.02249(10) 0.01964(10) 0.01973(10) 0.00262(7) -0.00162(7) -0.00056(7) O1 0.0188(6) 0.0274(7) 0.0193(6) 0.0020(5) -0.0026(5) 0.0002(5) O2 0.0286(7) 0.0312(7) 0.0218(6) 0.0040(6) -0.0035(6) -0.0079(6) O3 0.0333(8) 0.0246(7) 0.0289(7) 0.0065(6) -0.0062(6) -0.0058(6) C1 0.0170(8) 0.0171(8) 0.0219(8) 0.0024(7) -0.0012(7) 0.0000(7) C2 0.0179(9) 0.0212(9) 0.0212(8) 0.0026(7) -0.0035(7) -0.0014(7) C3 0.0188(9) 0.0218(9) 0.0185(8) 0.0026(7) 0.0008(7) 0.0002(7) C4 0.0218(9) 0.0255(9) 0.0195(8) -0.0002(7) -0.0011(7) -0.0019(8) C5 0.0279(10) 0.0232(9) 0.0193(8) -0.0014(7) 0.0003(7) -0.0006(8) C6 0.0231(9) 0.0237(9) 0.0230(9) 0.0048(7) 0.0034(7) 0.0017(8) C7 0.0184(9) 0.0290(10) 0.0295(9) -0.0011(8) -0.0014(7) -0.0009(8) C8 0.0224(9) 0.0226(9) 0.0251(9) -0.0027(7) -0.0011(7) -0.0020(8) C9 0.0280(11) 0.0301(11) 0.0357(11) 0.0016(9) 0.0055(9) 0.0072(9) C10 0.0191(9) 0.0231(9) 0.0215(8) 0.0026(7) -0.0011(7) 0.0031(7) C11 0.0293(11) 0.0240(10) 0.0283(10) -0.0017(8) -0.0001(8) 0.0021(8) C12 0.0348(12) 0.0327(11) 0.0260(10) -0.0021(8) 0.0054(9) 0.0067(9) C13 0.0244(10) 0.0384(12) 0.0261(9) 0.0080(9) 0.0044(8) 0.0066(9) C14 0.0230(10) 0.0297(10) 0.0329(10) 0.0044(9) 0.0003(8) -0.0030(8) C15 0.0240(10) 0.0256(10) 0.0272(9) -0.0025(8) 0.0004(8) -0.0019(8) C16 0.0176(8) 0.0231(9) 0.0217(8) -0.0017(7) -0.0035(7) 0.0040(7) C17 0.0214(9) 0.0258(10) 0.0266(9) 0.0015(8) -0.0057(7) 0.0018(8) C18 0.0228(10) 0.0228(10) 0.0432(11) 0.0020(9) -0.0100(8) 0.0018(8) C19 0.0284(11) 0.0304(11) 0.0444(12) -0.0132(10) -0.0149(9) 0.0079(9) C20 0.0286(11) 0.0497(14) 0.0237(10) -0.0117(9) -0.0056(8) 0.0110(10) C21 0.0246(10) 0.0355(11) 0.0241(9) 0.0002(8) 0.0010(7) 0.0034(9) C22 0.0216(9) 0.0211(9) 0.0208(8) -0.0032(7) -0.0016(7) 0.0016(7) C23 0.0205(9) 0.0242(9) 0.0216(8) 0.0011(7) 0.0004(7) 0.0032(7) C24 0.0211(9) 0.0239(9) 0.0201(8) -0.0002(7) -0.0007(7) 0.0021(8) C25 0.0376(12) 0.0265(10) 0.0262(9) 0.0028(8) -0.0072(8) -0.0042(9) C26 0.0383(12) 0.0270(10) 0.0332(10) -0.0004(9) -0.0047(9) -0.0085(9) C27 0.0223(9) 0.0360(11) 0.0249(9) -0.0069(8) 0.0008(7) 0.0001(8) C28 0.0266(10) 0.0359(11) 0.0213(9) 0.0028(8) -0.0032(7) -0.0001(9) C29 0.0242(10) 0.0296(10) 0.0243(9) 0.0044(8) -0.0014(7) 0.0001(8) C30 0.0312(11) 0.0436(13) 0.0301(10) -0.0086(10) -0.0046(9) -0.0041(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; H H 0.0000 0.0000 ; International Tables for Crystallography (Vol. C, Table 6.1.1.4) ; O O 0.0106 0.0060 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; Se Se -0.0929 2.2259 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C10 Se1 C1 99.28(8) . . ? C1 Se2 C16 101.23(8) . . ? C22 O1 C2 116.88(14) . . ? C2 C1 Se2 118.37(13) . . ? C2 C1 Se1 120.89(13) . . ? Se2 C1 Se1 120.60(9) . . ? C1 C2 O1 119.30(16) . . ? C1 C2 C3 129.04(16) . . ? O1 C2 C3 111.41(14) . . ? C4 C3 C8 118.76(17) . . ? C4 C3 C2 121.29(17) . . ? C8 C3 C2 119.87(17) . . ? C5 C4 C3 120.06(17) . . ? C5 C4 H4 120.0 . . ? C3 C4 H4 120.0 . . ? C4 C5 C6 121.85(18) . . ? C4 C5 H5 119.1 . . ? C6 C5 H5 119.1 . . ? C5 C6 C7 117.65(17) . . ? C5 C6 C9 121.89(18) . . ? C7 C6 C9 120.47(18) . . ? C8 C7 C6 121.18(18) . . ? C8 C7 H7 119.4 . . ? C6 C7 H7 119.4 . . ? C7 C8 C3 120.49(18) . . ? C7 C8 H8 119.8 . . ? C3 C8 H8 119.8 . . ? C6 C9 H9A 109.5 . . ? C6 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C6 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C11 C10 C15 120.52(18) . . ? C11 C10 Se1 118.27(15) . . ? C15 C10 Se1 121.15(14) . . ? C10 C11 C12 119.51(19) . . ? C10 C11 H11 120.2 . . ? C12 C11 H11 120.2 . . ? C13 C12 C11 120.15(19) . . ? C13 C12 H12 119.9 . . ? C11 C12 H12 119.9 . . ? C12 C13 C14 120.13(19) . . ? C12 C13 H13 119.9 . . ? C14 C13 H13 119.9 . . ? C13 C14 C15 120.2(2) . . ? C13 C14 H14 119.9 . . ? C15 C14 H14 119.9 . . ? C14 C15 C10 119.47(18) . . ? C14 C15 H15 120.3 . . ? C10 C15 H15 120.3 . . ? C17 C16 C21 120.49(18) . . ? C17 C16 Se2 122.19(14) . . ? C21 C16 Se2 117.28(15) . . ? C16 C17 C18 119.35(19) . . ? C16 C17 H17 120.3 . . ? C18 C17 H17 120.3 . . ? C19 C18 C17 120.8(2) . . ? C19 C18 H18 119.6 . . ? C17 C18 H18 119.6 . . ? C18 C19 C20 119.8(2) . . ? C18 C19 H19 120.1 . . ? C20 C19 H19 120.1 . . ? C19 C20 C21 120.33(19) . . ? C19 C20 H20 119.8 . . ? C21 C20 H20 119.8 . . ? C16 C21 C20 119.3(2) . . ? C16 C21 H21 120.4 . . ? C20 C21 H21 120.4 . . ? O2 C22 O1 125.79(17) . . ? O2 C22 C23 125.15(17) . . ? O1 C22 C23 109.01(15) . . ? O3 C23 C24 123.58(17) . . ? O3 C23 C22 117.29(17) . . ? C24 C23 C22 119.09(16) . . ? C29 C24 C25 118.53(18) . . ? C29 C24 C23 117.76(17) . . ? C25 C24 C23 123.67(17) . . ? C26 C25 C24 120.31(19) . . ? C26 C25 H25 119.8 . . ? C24 C25 H25 119.8 . . ? C25 C26 C27 121.5(2) . . ? C25 C26 H26 119.3 . . ? C27 C26 H26 119.3 . . ? C26 C27 C28 118.00(19) . . ? C26 C27 C30 120.7(2) . . ? C28 C27 C30 121.30(19) . . ? C29 C28 C27 121.12(18) . . ? C29 C28 H28 119.4 . . ? C27 C28 H28 119.4 . . ? C28 C29 C24 120.56(19) . . ? C28 C29 H29 119.7 . . ? C24 C29 H29 119.7 . . ? C27 C30 H30A 109.5 . . ? C27 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C27 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Se1 C10 1.9164(18) . ? Se1 C1 1.9177(18) . ? Se2 C1 1.9023(17) . ? Se2 C16 1.9188(19) . ? O1 C22 1.360(2) . ? O1 C2 1.420(2) . ? O2 C22 1.196(2) . ? O3 C23 1.215(2) . ? C1 C2 1.338(2) . ? C2 C3 1.482(3) . ? C3 C4 1.395(3) . ? C3 C8 1.398(3) . ? C4 C5 1.387(3) . ? C4 H4 0.9500 . ? C5 C6 1.390(3) . ? C5 H5 0.9500 . ? C6 C7 1.399(3) . ? C6 C9 1.508(3) . ? C7 C8 1.386(3) . ? C7 H7 0.9500 . ? C8 H8 0.9500 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 C11 1.382(3) . ? C10 C15 1.389(3) . ? C11 C12 1.394(3) . ? C11 H11 0.9500 . ? C12 C13 1.379(3) . ? C12 H12 0.9500 . ? C13 C14 1.385(3) . ? C13 H13 0.9500 . ? C14 C15 1.388(3) . ? C14 H14 0.9500 . ? C15 H15 0.9500 . ? C16 C17 1.383(3) . ? C16 C21 1.391(3) . ? C17 C18 1.390(3) . ? C17 H17 0.9500 . ? C18 C19 1.379(3) . ? C18 H18 0.9500 . ? C19 C20 1.381(3) . ? C19 H19 0.9500 . ? C20 C21 1.395(3) . ? C20 H20 0.9500 . ? C21 H21 0.9500 . ? C22 C23 1.546(2) . ? C23 C24 1.478(3) . ? C24 C29 1.396(3) . ? C24 C25 1.396(3) . ? C25 C26 1.382(3) . ? C25 H25 0.9500 . ? C26 C27 1.389(3) . ? C26 H26 0.9500 . ? C27 C28 1.394(3) . ? C27 C30 1.503(3) . ? C28 C29 1.382(3) . ? C28 H28 0.9500 . ? C29 H29 0.9500 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Se2 C1 C2 O1 -164.70(12) . . . . ? Se1 C1 C2 O1 11.0(2) . . . . ? Se2 C1 C2 C3 21.6(3) . . . . ? Se1 C1 C2 C3 -162.70(15) . . . . ? C22 O1 C2 C1 69.1(2) . . . . ? C22 O1 C2 C3 -116.13(17) . . . . ? C1 C2 C3 C4 -135.5(2) . . . . ? O1 C2 C3 C4 50.3(2) . . . . ? C1 C2 C3 C8 47.6(3) . . . . ? O1 C2 C3 C8 -126.55(17) . . . . ? C8 C3 C4 C5 -1.0(3) . . . . ? C2 C3 C4 C5 -177.95(17) . . . . ? C3 C4 C5 C6 1.4(3) . . . . ? C4 C5 C6 C7 -0.5(3) . . . . ? C4 C5 C6 C9 179.44(18) . . . . ? C5 C6 C7 C8 -0.7(3) . . . . ? C9 C6 C7 C8 179.39(18) . . . . ? C6 C7 C8 C3 1.0(3) . . . . ? C4 C3 C8 C7 -0.1(3) . . . . ? C2 C3 C8 C7 176.85(17) . . . . ? C15 C10 C11 C12 2.2(3) . . . . ? Se1 C10 C11 C12 -175.26(15) . . . . ? C10 C11 C12 C13 -1.8(3) . . . . ? C11 C12 C13 C14 0.0(3) . . . . ? C12 C13 C14 C15 1.4(3) . . . . ? C13 C14 C15 C10 -0.9(3) . . . . ? C11 C10 C15 C14 -0.8(3) . . . . ? Se1 C10 C15 C14 176.53(15) . . . . ? C21 C16 C17 C18 1.6(3) . . . . ? Se2 C16 C17 C18 179.23(14) . . . . ? C16 C17 C18 C19 -0.3(3) . . . . ? C17 C18 C19 C20 -1.4(3) . . . . ? C18 C19 C20 C21 1.7(3) . . . . ? C17 C16 C21 C20 -1.3(3) . . . . ? Se2 C16 C21 C20 -179.00(15) . . . . ? C19 C20 C21 C16 -0.4(3) . . . . ? C2 O1 C22 O2 5.5(3) . . . . ? C2 O1 C22 C23 -171.87(14) . . . . ? O2 C22 C23 O3 -144.4(2) . . . . ? O1 C22 C23 O3 32.9(2) . . . . ? O2 C22 C23 C24 33.4(3) . . . . ? O1 C22 C23 C24 -149.20(16) . . . . ? O3 C23 C24 C29 -3.8(3) . . . . ? C22 C23 C24 C29 178.53(16) . . . . ? O3 C23 C24 C25 178.56(19) . . . . ? C22 C23 C24 C25 0.9(3) . . . . ? C29 C24 C25 C26 1.0(3) . . . . ? C23 C24 C25 C26 178.69(19) . . . . ? C24 C25 C26 C27 -1.3(3) . . . . ? C25 C26 C27 C28 0.8(3) . . . . ? C25 C26 C27 C30 -177.8(2) . . . . ? C26 C27 C28 C29 -0.1(3) . . . . ? C30 C27 C28 C29 178.44(19) . . . . ? C27 C28 C29 C24 -0.1(3) . . . . ? C25 C24 C29 C28 -0.3(3) . . . . ? C23 C24 C29 C28 -178.15(17) . . . . ?