#------------------------------------------------------------------------------ #$Date: 2021-10-12 01:12:21 +0300 (Tue, 12 Oct 2021) $ #$Revision: 269887 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/48/1564899.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1564899 loop_ _publ_author_name 'Cooper, Alasdair K.' 'Greaves, Megan E.' 'Donohoe, William' 'Burton, Paul Matthew' 'Ronson, Thomas Oliver' 'Kennedy, Alan' 'Nelson, David James' _publ_section_title ; Inhibition of (dppf)nickel-catalysed Suzuki-Miyaura cross-coupling reactions by \a-halo-N-heterocycles ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC04582B _journal_year 2021 _chemical_formula_sum 'C52 H40 Cl2 Fe N2 Ni2 P2' _chemical_formula_weight 998.97 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2021-08-17 deposited with the CCDC. 2021-10-11 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 106.3800(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 23.0991(3) _cell_length_b 10.33270(10) _cell_length_c 18.9251(3) _cell_measurement_reflns_used 18200 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 72.5400 _cell_measurement_theta_min 2.4150 _cell_volume 4333.64(10) _computing_cell_refinement CrysalisPro _computing_data_collection CrysalisPro _computing_data_reduction CrysalisPro _computing_publication_material 'SHELXL in WINGX' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'Rigaku Synergy-i' _diffrn_measurement_method 'omega scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0626 _diffrn_reflns_av_unetI/netI 0.0253 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 28 _diffrn_reflns_limit_h_min -26 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 32177 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 70.000 _diffrn_reflns_theta_max 72.764 _diffrn_reflns_theta_min 3.989 _diffrn_source 'microsource tube' _exptl_absorpt_coefficient_mu 5.797 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.37498 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.99a (Rigaku Oxford Diffraction, 2021) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour red _exptl_crystal_density_diffrn 1.531 _exptl_crystal_description 'plate fragment' _exptl_crystal_F_000 2048 _exptl_crystal_size_max 0.37 _exptl_crystal_size_mid 0.14 _exptl_crystal_size_min 0.03 _refine_diff_density_max 0.835 _refine_diff_density_min -0.433 _refine_diff_density_rms 0.080 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.054 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 276 _refine_ls_number_reflns 4296 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.054 _refine_ls_R_factor_all 0.0428 _refine_ls_R_factor_gt 0.0408 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0683P)^2^+7.4687P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1085 _refine_ls_wR_factor_ref 0.1098 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4059 _reflns_number_total 4296 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1sc04582b3.cif _cod_data_source_block 1clquin_nidimer _cod_original_cell_volume 4333.63(10) _cod_original_sg_symbol_H-M 'C 2/c' _cod_database_code 1564899 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL 1clquin_nidimer_auto_a.res in C2/c shelx.res created by SHELXL-2018/3 at 22:15:20 on 23-Jun-2021 CELL 1.54184 23.0991 10.3327 18.9251 90.000 106.380 90.000 ZERR 4.00 0.0003 0.0001 0.0003 0.000 0.001 0.000 LATT 7 SYMM - X, Y, 1/2 - Z SFAC NI FE P CL N C H UNIT 8 4 8 8 8 208 160 MERG 2 OMIT -3.00 180.00 FMAP 2 PLAN 20 ACTA 140.00 BOND $H CONF L.S. 4 TEMP -173.00 WGHT 0.068300 7.468700 FVAR 0.15369 NI1 1 0.436882 0.814396 0.764531 11.00000 0.01431 0.02071 = 0.01908 -0.00026 0.00561 -0.00041 FE1 2 0.500000 0.403143 0.750000 10.50000 0.01681 0.01888 = 0.02701 0.00000 0.01214 0.00000 P1 3 0.386045 0.658924 0.696170 11.00000 0.01336 0.02241 = 0.02092 -0.00160 0.00670 -0.00118 CL1 4 0.409517 0.743284 0.862170 11.00000 0.01874 0.02705 = 0.02265 0.00024 0.00950 0.00058 N1 5 0.501336 0.921081 0.673790 11.00000 0.01828 0.02002 = 0.01948 -0.00163 0.00479 -0.00073 C1 6 0.446272 0.909295 0.682665 11.00000 0.01777 0.01864 = 0.02095 -0.00393 0.00479 -0.00115 C2 6 0.511074 0.993882 0.617042 11.00000 0.02130 0.02377 = 0.02381 -0.00039 0.00815 -0.00390 AFIX 43 H2 7 0.550893 0.999431 0.612407 11.00000 -1.20000 AFIX 0 C3 6 0.466090 1.057923 0.567548 11.00000 0.02901 0.02493 = 0.02175 0.00166 0.00892 -0.00130 AFIX 43 H3 7 0.474415 1.107452 0.529261 11.00000 -1.20000 AFIX 0 C4 6 0.406558 1.049623 0.573977 11.00000 0.02485 0.02246 = 0.02164 -0.00226 0.00369 0.00203 C5 6 0.357312 1.114322 0.524496 11.00000 0.03344 0.03169 = 0.02549 0.00294 0.00403 0.00501 AFIX 43 H5 7 0.363588 1.164012 0.485065 11.00000 -1.20000 AFIX 0 C6 6 0.300953 1.104964 0.533710 11.00000 0.02790 0.03572 = 0.03284 0.00205 -0.00125 0.01015 AFIX 43 H6 7 0.267897 1.145426 0.499237 11.00000 -1.20000 AFIX 0 C7 6 0.291054 1.036549 0.593274 11.00000 0.01811 0.03463 = 0.03824 -0.00257 0.00213 0.00637 AFIX 43 H7 7 0.251900 1.034402 0.600198 11.00000 -1.20000 AFIX 0 C8 6 0.337878 0.972772 0.641507 11.00000 0.02033 0.02601 = 0.02959 -0.00012 0.00491 0.00120 AFIX 43 H8 7 0.330810 0.925807 0.681428 11.00000 -1.20000 AFIX 0 C9 6 0.396653 0.976171 0.632444 11.00000 0.01980 0.02091 = 0.02287 -0.00245 0.00289 0.00109 C10 6 0.417554 0.500293 0.725310 11.00000 0.01226 0.02280 = 0.03010 -0.00032 0.00944 -0.00062 C11 6 0.414920 0.390869 0.677688 11.00000 0.01966 0.02906 = 0.03405 -0.00692 0.01198 -0.00292 AFIX 43 H11 7 0.405610 0.393548 0.625506 11.00000 -1.20000 AFIX 0 C12 6 0.428607 0.278239 0.721996 11.00000 0.02207 0.02342 = 0.04742 -0.00505 0.01781 -0.00708 AFIX 43 H12 7 0.429639 0.192281 0.704580 11.00000 -1.20000 AFIX 0 C13 6 0.440556 0.316020 0.797135 11.00000 0.02377 0.02406 = 0.04162 0.00417 0.01949 -0.00080 AFIX 43 H13 7 0.451101 0.259497 0.838381 11.00000 -1.20000 AFIX 0 C14 6 0.434051 0.452325 0.799982 11.00000 0.01915 0.02573 = 0.02969 0.00149 0.01447 -0.00015 AFIX 43 H14 7 0.439565 0.502956 0.843281 11.00000 -1.20000 AFIX 0 C15 6 0.382741 0.662139 0.598942 11.00000 0.01719 0.02373 = 0.02272 -0.00240 0.00724 -0.00260 C16 6 0.437298 0.650972 0.580588 11.00000 0.01802 0.03123 = 0.02457 -0.00093 0.00665 -0.00098 AFIX 43 H16 7 0.473928 0.638060 0.618300 11.00000 -1.20000 AFIX 0 C17 6 0.438023 0.658651 0.508027 11.00000 0.02282 0.04552 = 0.03090 0.00009 0.01419 0.00337 AFIX 43 H17 7 0.475030 0.649678 0.495908 11.00000 -1.20000 AFIX 0 C18 6 0.384993 0.679382 0.452906 11.00000 0.03194 0.05353 = 0.02465 0.00158 0.01229 0.00491 AFIX 43 H18 7 0.385564 0.684485 0.402987 11.00000 -1.20000 AFIX 0 C19 6 0.331318 0.692623 0.470532 11.00000 0.02380 0.04874 = 0.02439 0.00262 0.00499 0.00399 AFIX 43 H19 7 0.295051 0.708079 0.432651 11.00000 -1.20000 AFIX 0 C20 6 0.329835 0.683569 0.543077 11.00000 0.01833 0.03586 = 0.02604 0.00014 0.00758 0.00223 AFIX 43 H20 7 0.292573 0.692030 0.554635 11.00000 -1.20000 AFIX 0 C21 6 0.307354 0.634202 0.696180 11.00000 0.01567 0.02887 = 0.02190 0.00306 0.00725 -0.00048 C22 6 0.278828 0.720815 0.731445 11.00000 0.01745 0.03203 = 0.02531 -0.00076 0.00772 -0.00086 AFIX 43 H22 7 0.300400 0.793612 0.756248 11.00000 -1.20000 AFIX 0 C23 6 0.219042 0.702284 0.730896 11.00000 0.01913 0.03795 = 0.02899 0.00100 0.01052 0.00099 AFIX 43 H23 7 0.199791 0.762785 0.754609 11.00000 -1.20000 AFIX 0 C24 6 0.187827 0.595776 0.695804 11.00000 0.01470 0.04460 = 0.03142 0.00522 0.00816 -0.00292 AFIX 43 H24 7 0.147183 0.582195 0.695943 11.00000 -1.20000 AFIX 0 C25 6 0.215765 0.508277 0.660232 11.00000 0.02212 0.03330 = 0.02841 0.00261 0.00522 -0.00775 AFIX 43 H25 7 0.194038 0.435435 0.635700 11.00000 -1.20000 AFIX 0 C26 6 0.274977 0.526915 0.660451 11.00000 0.02196 0.02938 = 0.02547 -0.00058 0.00810 -0.00292 AFIX 43 H26 7 0.293879 0.466591 0.636215 11.00000 -1.20000 AFIX 0 HKLF 4 REM 1clquin_nidimer_auto_a.res in C2/c REM wR2 = 0.1098, GooF = S = 1.054, Restrained GooF = 1.054 for all data REM R1 = 0.0408 for 4059 Fo > 4sig(Fo) and 0.0428 for all 4296 data REM 276 parameters refined using 0 restraints END WGHT 0.0683 7.4686 REM Highest difference peak 0.835, deepest hole -0.433, 1-sigma level 0.080 Q1 1 0.5000 0.3159 0.7500 10.50000 0.05 0.84 Q2 1 0.4375 0.7220 0.7588 11.00000 0.05 0.66 Q3 1 0.3900 0.5759 0.7001 11.00000 0.05 0.63 Q4 1 0.4301 0.7555 0.7152 11.00000 0.05 0.57 Q5 1 0.4388 0.9038 0.7536 11.00000 0.05 0.56 Q6 1 0.3939 0.7252 0.7360 11.00000 0.05 0.50 Q7 1 0.3919 0.7413 0.7198 11.00000 0.05 0.46 Q8 1 0.4105 0.6639 0.8330 11.00000 0.05 0.45 Q9 1 0.3813 0.6537 0.6445 11.00000 0.05 0.45 Q10 1 0.4383 0.7397 0.8063 11.00000 0.05 0.43 Q11 1 0.4997 0.4788 0.7770 11.00000 0.05 0.42 Q12 1 0.4378 0.7966 0.8262 11.00000 0.05 0.42 Q13 1 0.3383 0.6393 0.6967 11.00000 0.05 0.40 Q14 1 0.4112 0.6710 0.9028 11.00000 0.05 0.40 Q15 1 0.4102 0.8353 0.8693 11.00000 0.05 0.39 Q16 1 0.3874 0.6958 0.6524 11.00000 0.05 0.38 Q17 1 0.4113 0.3209 0.7017 11.00000 0.05 0.38 Q18 1 0.4591 0.2955 0.7383 11.00000 0.05 0.37 Q19 1 0.3871 0.6066 0.6557 11.00000 0.05 0.36 Q20 1 0.4165 0.5633 0.7073 11.00000 0.05 0.35 ; _shelx_res_checksum 34661 _shelx_hkl_file ; 0 0 -1 5.38 0.33 0 0 1 5.56 0.32 0 0 -1 5.42 0.30 0 0 -1 4.13 0.26 0 0 -1 4.59 0.27 0 0 -1 4.97 0.28 0 0 -2 5112.36 143.99 0 0 2 5680.85 144.18 0 0 2 5583.34 144.18 0 0 -2 5791.32 144.16 0 0 -2 5218.50 144.07 0 0 2 5686.20 144.14 0 0 -2 5089.84 144.09 0 0 2 5298.03 143.98 0 0 -2 5394.41 144.11 0 0 2 5398.66 144.11 0 0 -3 0.88 0.43 0 0 3 1.49 0.67 0 0 3 1.79 0.70 0 0 3 1.62 0.72 0 0 -3 1.01 0.59 0 0 -3 0.60 0.58 0 0 -3 1.00 0.54 0 0 3 0.98 0.38 0 0 3 1.54 0.65 0 0 3 2.47 0.68 0 0 -3 1.36 0.53 0 0 -4 922.86 26.99 0 0 4 1033.32 27.35 0 0 4 1046.44 27.39 0 0 4 1012.16 27.49 0 0 -4 1099.53 27.33 0 0 -4 991.65 27.19 0 0 4 985.57 26.92 0 0 -4 1022.53 27.24 0 0 4 1005.46 27.26 0 0 -4 966.26 27.17 0 0 4 986.49 27.13 0 0 -5 0.08 0.72 0 0 -5 0.64 0.81 0 0 5 0.31 1.16 0 0 -5 0.72 0.89 0 0 5 0.47 1.11 0 0 -5 1.05 1.00 0 0 5 0.51 1.16 0 0 5 0.86 1.14 0 0 5 0.73 1.13 0 0 -6 87.06 3.23 0 0 6 81.04 3.19 0 0 6 84.96 3.41 0 0 -6 86.60 3.18 0 0 6 84.56 3.60 0 0 -6 96.24 3.34 0 0 6 89.86 3.47 0 0 6 91.48 3.52 0 0 7 0.89 1.26 0 0 -7 0.43 1.01 0 0 -7 -0.05 1.06 0 0 7 3.39 1.45 0 0 -7 -0.14 1.05 0 0 7 -0.03 1.34 0 0 7 0.10 1.32 0 0 8 119.50 4.34 0 0 -8 118.41 4.40 0 0 -8 123.33 4.35 0 0 8 113.68 4.83 0 0 8 124.43 4.78 0 0 8 126.71 4.74 0 0 -9 0.71 1.29 0 0 -9 0.44 1.17 0 0 9 -0.05 1.46 0 0 9 1.58 1.57 0 0 9 0.83 1.61 0 0 -10 191.13 6.44 0 0 -10 183.28 6.52 0 0 10 176.35 7.06 0 0 10 189.15 7.03 0 0 10 191.03 6.96 0 0 -11 0.62 1.39 0 0 -11 1.74 1.58 0 0 11 3.42 2.02 0 0 11 1.26 1.89 0 0 11 0.43 1.90 0 0 -12 5.65 1.81 0 0 -12 4.28 1.59 0 0 12 2.56 2.09 0 0 12 5.24 2.33 0 0 12 1.04 2.32 0 0 -13 1.23 1.64 0 0 -13 1.40 1.74 0 0 13 1.48 2.59 0 0 13 0.62 3.70 0 0 13 0.56 2.37 0 0 13 0.57 2.15 0 0 13 0.27 2.52 0 0 -14 22.81 2.57 0 0 14 22.17 4.33 0 0 14 24.80 3.23 0 0 14 22.30 3.18 0 0 14 26.33 2.86 0 0 14 24.97 3.61 0 0 -15 -0.31 1.92 0 0 15 -0.76 2.55 0 0 15 -0.72 2.51 0 0 15 0.84 2.90 0 0 15 2.75 3.26 0 0 15 0.23 4.49 0 0 16 91.52 6.15 0 0 16 97.00 5.06 0 0 16 99.07 4.87 0 0 -16 111.24 4.48 0 0 17 -2.56 4.84 0 0 17 0.04 3.41 0 0 17 -0.18 2.82 0 0 -17 0.66 2.15 0 0 18 340.34 11.59 0 0 18 327.31 10.90 0 0 18 352.45 11.15 0 0 -18 358.28 10.84 0 0 19 1.27 3.18 0 0 19 3.38 4.50 0 0 19 2.40 2.60 0 0 -19 0.04 2.05 0 0 20 10.87 2.86 0 0 20 11.85 4.04 0 0 20 11.26 2.47 0 0 -20 8.32 1.97 0 0 21 0.57 2.24 0 0 -21 -0.47 1.48 0 0 21 0.64 1.91 0 0 -22 19.02 1.51 0 0 22 17.33 1.78 0 -2 0 160.15 4.44 0 2 0 160.23 4.58 0 -2 0 173.80 4.72 0 2 0 146.81 4.71 0 -2 0 170.90 4.95 0 2 0 150.94 4.74 0 -2 0 182.04 4.85 0 2 0 154.41 4.62 0 2 0 155.91 4.81 0 2 0 151.56 4.71 0 -2 0 166.04 4.98 0 -2 -1 297.51 7.26 0 -2 1 276.30 6.77 0 2 -1 239.02 7.00 0 -2 1 274.18 6.97 0 2 1 241.57 6.96 0 2 -1 260.31 6.87 0 -2 -1 267.65 6.89 0 2 1 253.47 6.87 0 2 -1 206.96 6.92 0 -2 1 253.77 6.85 0 2 1 234.37 6.88 0 -2 1 272.92 7.06 0 -2 -1 263.07 7.17 0 -2 1 238.79 7.02 0 -2 -1 249.01 6.98 0 -2 1 181.00 6.59 0 2 -1 252.93 6.62 0 2 1 213.20 6.59 0 2 -1 255.82 6.94 0 -2 -1 267.59 7.24 0 -2 1 262.65 7.12 0 2 1 272.53 6.97 0 -2 -2 180.44 5.63 0 2 -2 183.65 5.38 0 -2 -2 187.77 5.29 0 2 2 175.89 5.36 0 -2 2 203.65 5.43 0 -2 2 200.32 5.27 0 2 -2 158.25 5.07 0 2 2 182.53 5.32 0 -2 2 197.64 5.47 0 -2 2 154.32 5.08 0 -2 -2 142.48 4.94 0 -2 2 201.82 5.44 0 2 -2 182.06 5.33 0 -2 -2 200.32 5.59 0 -2 -2 205.59 5.42 0 2 2 169.74 5.14 0 -2 2 177.34 5.25 0 2 -2 198.67 5.28 0 -2 -2 196.98 5.65 0 -2 2 193.00 5.44 0 2 2 200.79 5.42 0 2 2 191.37 5.37 0 -2 2 195.47 5.47 0 2 -3 2074.34 52.28 0 2 3 1850.57 52.22 0 -2 3 2123.75 52.26 0 2 3 1896.08 52.23 0 -2 -3 2059.73 52.60 0 2 -3 2066.31 52.33 0 2 -3 1878.39 52.16 0 -2 3 1699.10 51.92 0 -2 -3 2055.75 52.49 0 -2 -3 1783.83 52.22 0 2 3 1805.15 52.16 0 -2 3 2003.79 52.37 0 2 3 1913.97 52.27 0 -2 3 2045.03 52.40 0 -2 -3 2041.69 52.51 0 2 3 1980.01 52.28 0 -2 3 1957.35 52.29 0 -2 3 1969.30 52.32 0 2 4 1633.99 46.18 0 -2 -4 1888.27 46.64 0 2 4 1641.07 46.23 0 -2 4 1798.40 46.32 0 2 -4 1758.28 46.23 0 2 -4 1770.16 46.31 0 -2 -4 1810.10 46.50 0 2 -4 1537.77 46.05 0 -2 -4 1755.20 46.20 0 -2 4 1753.85 46.52 0 2 4 1580.04 46.23 0 -2 4 1645.30 46.27 0 -2 -4 1715.78 46.48 0 2 4 1668.57 46.26 0 -2 4 1742.62 46.42 0 2 -5 15.65 1.37 0 -2 -5 13.19 1.55 0 2 -5 13.92 1.34 0 2 5 14.62 1.34 0 2 5 14.45 1.72 0 -2 -5 12.92 1.54 0 -2 5 14.14 1.58 0 -2 -5 13.04 1.63 0 2 -5 15.25 1.23 0 -2 5 13.16 1.51 0 2 -5 14.41 1.38 0 2 5 11.63 1.48 0 -2 5 14.58 1.68 0 2 5 14.09 1.53 0 2 5 13.26 1.42 0 -2 -5 13.50 1.74 0 -2 5 13.19 1.43 0 2 -6 238.69 7.79 0 -2 -6 273.83 8.22 0 2 6 247.84 7.91 0 2 6 259.97 7.75 0 2 -6 260.33 7.84 0 -2 -6 260.79 8.20 0 2 -6 265.23 7.95 0 -2 6 272.88 8.11 0 2 -6 269.39 7.68 0 -2 6 255.71 7.99 0 2 6 241.71 8.09 0 2 6 250.72 8.00 0 -2 -6 258.25 8.15 0 -2 6 267.56 8.48 0 -2 6 257.97 8.13 0 2 6 251.06 8.08 0 2 -7 455.15 13.88 0 2 -7 489.88 14.05 0 2 -7 493.78 13.95 0 -2 7 505.72 14.28 0 2 7 462.04 13.98 0 -2 -7 487.95 14.29 0 -2 -7 502.42 14.29 0 -2 7 511.54 14.81 0 2 7 437.82 14.13 0 -2 7 482.82 14.29 0 -2 7 486.71 14.18 0 2 7 467.44 14.30 0 -2 -7 485.57 14.30 0 2 7 483.90 14.20 0 2 -8 282.48 8.85 0 -2 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92.11 4.90 0 2 12 95.21 5.01 0 2 12 87.10 4.88 0 -2 13 98.36 5.37 0 2 13 134.94 4.84 0 2 13 107.78 5.00 0 -2 13 105.18 5.18 0 -2 -13 112.73 4.55 0 -2 -13 103.60 5.20 0 -2 -13 96.25 5.20 0 2 -13 111.40 5.16 0 -2 13 115.24 6.41 0 2 13 106.57 5.67 0 2 13 107.07 4.46 0 -2 13 126.03 5.07 0 -2 13 115.01 5.76 0 2 13 120.46 5.96 0 2 13 121.55 5.94 0 2 14 15.07 2.44 0 2 14 15.30 3.51 0 -2 14 16.27 4.29 0 -2 14 13.54 3.61 0 2 -14 19.80 2.16 0 -2 -14 13.43 2.25 0 2 -14 14.01 2.42 0 -2 -14 12.74 2.43 0 2 14 17.26 3.05 0 -2 14 12.67 2.94 0 2 14 12.04 2.99 0 2 14 11.62 2.91 0 2 14 16.11 2.50 0 -2 14 16.87 3.01 0 -2 14 13.63 3.51 0 2 14 12.55 3.15 0 2 -15 154.69 5.44 0 -2 -15 134.60 5.57 0 -2 15 131.06 6.26 0 2 -15 129.17 6.22 0 2 -15 152.18 5.35 0 -2 -15 145.46 5.38 0 -2 15 156.30 6.26 0 2 15 146.97 5.66 0 2 15 116.02 6.75 0 -2 15 135.77 6.71 0 2 15 167.82 5.95 0 2 15 145.81 6.20 0 -2 -16 -0.39 2.14 0 -2 16 0.04 3.79 0 2 -16 0.71 1.90 0 -2 -16 2.43 1.95 0 -2 16 -1.42 3.06 0 2 16 -0.56 2.44 0 -2 16 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717.71 22.18 0 4 -5 709.77 22.12 0 4 -6 7.24 1.43 0 -4 6 3.45 1.80 0 -4 -6 7.03 1.91 0 -4 -6 6.12 2.11 0 -4 6 6.43 1.61 0 4 6 9.62 1.75 0 -4 6 6.50 1.69 0 4 6 7.09 1.66 0 4 -6 8.42 1.65 0 4 -6 6.45 1.55 0 4 6 8.65 1.95 0 -4 -6 7.20 2.24 0 4 -7 91.38 3.81 0 -4 7 96.30 4.88 0 -4 -7 105.42 4.58 0 -4 7 101.67 4.36 0 -4 -7 104.10 4.73 0 4 7 106.83 4.51 0 -4 7 96.98 4.35 0 4 -7 96.00 4.12 0 -4 -7 94.98 4.87 0 4 7 104.48 4.36 0 4 7 81.01 3.87 0 4 -7 106.23 4.27 0 -4 -8 488.46 14.35 0 -4 8 495.19 14.92 0 4 -8 407.12 13.41 0 4 8 516.17 14.49 0 -4 8 469.94 14.21 0 -4 -8 497.34 14.59 0 -4 8 451.43 14.13 0 -4 -8 439.48 14.67 0 4 -8 486.55 14.00 0 4 8 498.58 14.03 0 4 -8 511.25 14.01 0 -4 9 81.95 4.65 0 -4 9 76.50 4.14 0 4 9 78.37 4.32 0 -4 -9 79.99 4.54 0 -4 9 83.83 4.29 0 4 -9 80.50 3.94 0 4 9 79.06 4.19 0 -4 -9 71.92 4.43 0 4 -9 86.53 4.02 0 -4 10 285.21 10.74 0 4 -10 302.88 10.05 0 -4 -10 252.53 10.42 0 4 -10 316.38 10.06 0 4 10 290.42 10.02 0 -4 -10 308.68 10.72 0 -4 10 299.22 10.43 0 4 10 330.48 10.76 0 4 10 283.52 10.64 0 4 11 72.58 4.78 0 -4 -11 65.25 3.43 0 -4 11 65.26 4.07 0 -4 11 60.87 4.37 0 4 11 82.17 3.35 0 4 -11 63.59 3.85 0 -4 -11 61.42 4.29 0 4 11 67.39 4.19 0 -4 -11 64.85 3.48 0 4 11 69.98 3.28 0 4 11 80.07 4.64 0 -4 -11 73.72 4.70 0 -4 11 70.58 4.40 0 4 12 50.82 4.32 0 -4 12 50.37 4.09 0 -4 -12 47.93 3.06 0 -4 12 47.63 3.15 0 4 -12 49.42 3.51 0 -4 -12 38.19 3.64 0 4 12 50.13 3.78 0 4 12 60.44 4.27 0 4 12 48.50 2.94 0 4 12 58.40 3.08 0 4 13 1.74 3.02 0 -4 -13 1.80 2.11 0 -4 13 2.46 3.64 0 4 -13 2.00 2.03 0 -4 -13 1.68 2.33 0 4 13 1.05 1.99 0 4 13 1.50 2.61 0 4 13 0.75 2.63 0 4 13 2.59 1.99 0 4 14 339.03 10.39 0 -4 14 329.20 10.85 0 -4 -14 297.55 10.36 0 4 14 288.92 10.07 0 4 15 45.23 4.49 0 4 15 37.23 3.13 0 -4 -15 34.96 3.09 0 -4 15 41.45 4.56 0 4 15 38.44 2.89 0 -4 16 70.02 5.46 0 4 16 76.80 4.89 0 4 16 65.20 3.64 0 -4 16 65.06 5.09 0 4 -16 63.53 3.56 0 -4 -16 57.92 3.68 0 4 16 62.95 3.46 0 -4 17 58.93 5.26 0 4 17 52.22 3.35 0 4 17 67.42 4.52 0 -4 -17 43.95 3.32 0 -4 17 49.69 4.82 0 4 -17 55.67 3.31 0 4 17 51.62 3.11 0 4 -18 42.42 2.92 0 -4 18 48.38 4.42 0 -4 -18 38.84 2.95 0 -4 18 35.73 2.98 0 -4 18 45.84 4.90 0 4 18 39.84 2.90 0 4 18 50.64 4.00 0 4 -19 47.44 2.78 0 -4 -19 46.74 2.83 0 4 19 47.67 2.87 0 -4 19 44.54 2.90 0 4 19 49.93 3.49 0 -4 -20 33.17 2.21 0 4 -20 36.70 2.21 0 4 20 34.81 2.30 0 4 20 38.44 2.76 0 -4 -21 5.29 1.15 0 4 21 6.70 1.66 0 4 21 4.94 1.20 0 -6 0 268.21 9.30 0 -6 0 248.19 8.81 0 6 0 257.04 8.23 0 6 0 277.39 8.69 0 -6 -1 123.37 5.64 0 -6 1 116.01 5.45 0 -6 1 122.29 5.55 0 -6 -1 111.26 5.21 0 -6 1 115.73 5.22 0 6 1 126.76 4.79 0 6 -1 125.71 4.72 0 6 1 140.46 4.90 0 6 1 131.30 5.18 0 6 -1 125.79 5.05 0 -6 2 6.52 2.05 0 6 -2 7.23 1.63 0 -6 -2 7.73 2.14 0 -6 -2 6.44 2.42 0 -6 2 7.74 2.06 0 -6 2 8.56 2.20 0 6 -2 8.76 2.03 0 6 2 7.78 1.87 0 6 2 5.58 1.89 0 -6 3 78.52 4.51 0 -6 -3 84.76 4.80 0 -6 3 106.51 4.87 0 -6 -3 92.60 4.64 0 6 -3 109.07 4.18 0 6 -3 111.22 4.55 0 6 3 99.00 4.45 0 6 3 92.19 4.20 0 -6 -4 81.35 4.85 0 -6 4 97.43 4.80 0 -6 4 86.38 4.62 0 6 -4 104.12 4.15 0 -6 -4 89.55 4.65 0 -6 4 84.93 4.95 0 6 -4 104.92 4.50 0 6 -4 95.92 4.34 0 6 4 94.06 4.28 0 6 -5 30.71 2.41 0 -6 -5 22.68 2.78 0 -6 5 21.40 3.02 0 -6 5 28.12 2.83 0 -6 -5 23.12 3.22 0 -6 5 26.07 2.77 0 6 5 26.03 2.81 0 6 5 25.86 2.60 0 6 -5 32.41 2.72 0 6 -5 29.28 2.47 0 6 6 66.84 3.71 0 6 -6 77.00 3.96 0 6 -6 69.59 3.75 0 6 -6 75.67 3.58 0 -6 6 52.15 4.43 0 -6 6 62.83 4.08 0 -6 6 65.93 4.13 0 -6 -6 54.48 4.31 0 -6 7 8.99 2.45 0 -6 -7 12.18 2.31 0 -6 7 9.54 2.84 0 6 -7 12.60 2.09 0 6 7 12.10 1.84 0 6 -7 12.46 2.19 0 6 -7 12.30 2.46 0 6 7 12.56 2.25 0 -6 -7 13.53 2.20 0 -6 7 12.53 2.56 0 6 7 9.84 2.24 0 -6 -7 12.17 2.98 0 -6 -8 5.99 2.92 0 -6 8 8.08 2.53 0 6 8 5.81 2.23 0 -6 8 6.02 2.86 0 6 -8 8.30 1.99 0 6 8 6.48 1.80 0 6 8 9.17 2.15 0 6 -8 7.20 2.37 0 6 -8 5.84 1.99 0 -6 -8 7.70 2.20 0 -6 8 6.91 2.45 0 -6 9 9.91 2.65 0 -6 9 10.25 3.49 0 6 -9 8.99 2.13 0 -6 9 5.63 2.93 0 6 9 9.07 1.92 0 6 9 12.76 2.27 0 6 -9 9.13 2.15 0 6 -9 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442.24 11.97 -1 -1 2 460.24 11.97 1 1 -1 1998.02 52.82 1 -1 -1 1972.98 52.91 -1 -1 1 1936.40 52.78 -1 1 1 1767.15 52.81 -1 1 1 1838.60 52.78 -1 -1 1 2118.11 52.87 1 1 -1 1994.17 52.75 1 1 -1 1916.40 52.80 1 -1 -1 2108.92 52.73 -1 -1 1 2041.40 52.81 -1 -1 1 2152.67 52.87 1 -1 -1 2136.32 52.97 1 -1 -1 1678.61 52.72 1 1 -1 1759.71 52.70 1 1 -1 2046.65 52.87 1 -1 -1 2026.74 52.74 1 1 -1 2002.98 52.77 -1 -1 1 2070.54 52.86 -1 1 1 2131.95 52.76 1 -1 -1 1997.86 52.87 -1 -1 1 2188.01 52.91 -1 1 1 1817.97 52.73 -1 -1 0 16.81 0.71 -1 1 0 13.25 0.56 1 1 0 13.80 0.66 1 1 0 11.81 0.64 1 -1 0 18.92 0.61 -1 1 0 13.62 0.63 -1 -1 0 17.46 0.77 1 -1 0 18.24 0.70 1 -1 0 15.97 0.77 1 1 0 12.59 0.61 1 -1 0 17.22 0.70 -1 -1 0 16.00 0.70 -1 -1 0 17.55 0.79 1 1 0 10.31 0.56 1 1 0 10.40 0.53 1 -1 0 15.95 0.59 1 -1 0 15.63 0.59 1 1 0 11.88 0.73 1 1 0 14.56 0.74 1 1 0 12.59 0.72 -1 -1 0 15.65 0.75 1 -1 0 16.61 0.75 -1 1 -1 311.18 9.03 1 1 1 346.02 9.06 -1 -1 -1 337.09 9.12 -1 1 -1 292.35 8.89 1 1 1 310.54 9.05 -1 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2.18 5 -5 -8 0.80 1.69 5 5 -8 3.53 1.84 5 -5 -8 0.08 2.38 5 5 -8 3.10 2.14 -5 -5 8 0.50 2.11 5 5 -7 20.72 2.41 -5 -5 7 17.56 2.99 -5 5 7 22.88 2.79 -5 -5 7 21.31 2.66 -5 -5 7 20.51 2.54 5 -5 -7 18.49 2.54 5 -5 -7 19.65 2.96 5 -5 -7 11.84 2.23 5 5 -7 21.90 2.29 5 5 -7 21.22 2.66 5 5 -6 13.47 2.12 -5 -5 6 8.87 2.60 -5 5 6 16.45 2.66 5 -5 -6 14.93 2.25 -5 -5 6 12.68 2.17 5 5 -6 12.24 1.89 5 -5 -6 7.37 1.89 5 -5 -6 13.41 2.69 -5 -5 6 14.71 2.38 5 5 -5 507.15 14.73 -5 -5 5 503.23 15.62 -5 5 5 536.52 15.27 5 -5 -5 510.50 14.99 -5 -5 5 453.01 15.14 -5 -5 5 431.20 14.98 5 -5 -5 487.83 15.60 5 -5 -5 407.83 15.30 5 5 -5 550.36 14.66 -5 -5 5 475.31 15.48 5 5 -5 495.19 14.95 -5 -5 4 81.23 4.36 5 5 -4 78.81 3.51 -5 5 4 80.75 4.01 -5 -5 4 68.90 3.89 5 5 -4 72.57 3.59 -5 -5 4 67.69 3.78 -5 -5 4 78.93 4.40 5 -5 -4 67.54 3.91 5 5 -4 82.88 3.41 5 -5 -4 66.41 4.14 5 5 -4 75.41 3.72 5 5 -3 424.33 12.50 -5 -5 3 420.72 13.38 -5 5 3 423.09 12.97 5 5 -3 418.93 12.78 -5 -5 3 411.20 13.21 -5 -5 3 408.25 13.08 -5 5 3 424.99 12.93 5 -5 -3 408.99 13.32 5 -5 -3 380.73 13.20 5 5 -3 424.59 12.36 -5 -5 3 414.92 13.49 5 5 -3 427.70 12.92 5 5 -2 4.59 1.45 -5 -5 2 2.15 2.11 -5 -5 2 2.36 2.25 -5 5 2 4.05 1.94 5 5 -2 3.40 1.44 5 5 -2 5.20 1.54 -5 -5 2 2.78 1.67 5 -5 -2 4.54 1.47 5 -5 -2 4.31 2.07 -5 5 2 4.13 1.76 5 5 -2 3.30 1.24 5 5 -2 5.42 1.71 -5 -5 2 3.49 1.88 -5 -5 1 2.16 2.04 -5 -5 1 2.10 2.23 -5 5 1 3.61 1.78 5 5 -1 2.05 1.42 -5 -5 1 2.25 1.71 5 5 -1 2.97 1.47 5 -5 -1 1.65 1.81 5 -5 -1 2.86 1.36 -5 5 1 1.61 1.73 5 5 -1 2.22 1.62 -5 -5 0 33.78 2.89 5 5 0 35.94 2.31 -5 5 0 40.29 2.79 -5 -5 0 35.89 2.77 5 5 0 41.51 2.47 5 -5 0 33.78 2.35 -5 5 0 39.62 2.70 -5 -5 0 33.82 3.11 5 -5 0 35.93 2.73 5 5 0 39.02 2.69 5 5 1 131.87 4.85 -5 5 -1 142.23 5.28 5 5 1 135.32 5.08 5 5 1 133.25 4.99 -5 -5 -1 117.45 5.61 -5 5 -1 140.10 5.28 5 -5 1 130.62 5.29 5 -5 1 116.35 5.22 5 5 1 130.77 5.27 -5 5 -2 304.22 9.15 5 5 2 275.25 8.75 5 5 2 283.23 9.06 -5 -5 -2 282.50 9.75 5 5 2 280.87 8.94 -5 -5 -2 270.45 9.58 -5 5 -2 255.28 8.98 5 -5 2 247.25 9.01 5 -5 2 273.25 9.44 5 5 2 284.93 9.27 -5 5 -3 18.33 2.17 5 5 3 19.79 1.98 5 5 3 17.42 2.06 -5 -5 -3 19.00 2.81 5 5 3 18.56 2.07 -5 -5 -3 17.70 2.59 -5 5 -3 12.38 2.06 5 -5 3 17.21 2.29 5 5 3 18.36 2.31 -5 5 -4 118.46 4.91 -5 5 -4 111.72 5.12 5 5 4 127.86 4.84 -5 -5 -4 114.51 5.68 5 5 4 120.57 5.07 5 5 4 125.09 5.07 -5 -5 -4 127.74 5.57 -5 5 -4 130.60 5.01 5 -5 4 136.57 5.77 5 5 4 122.02 5.32 -5 5 -5 4.41 1.86 5 5 5 5.22 1.74 5 5 5 1.48 1.75 -5 -5 -5 2.60 2.51 5 5 5 2.37 1.83 -5 5 -5 3.98 1.69 5 -5 5 3.76 2.12 5 5 5 2.36 2.03 5 5 5 5.27 2.14 -5 -5 -6 215.10 8.90 5 5 6 269.47 8.32 -5 5 -6 263.07 8.82 -5 -5 -6 219.05 9.08 5 5 6 235.28 8.79 5 5 6 247.62 8.72 5 5 6 241.83 8.95 5 5 6 233.84 8.95 5 -5 6 283.37 9.69 5 5 7 122.16 6.02 5 5 7 122.09 6.08 5 -5 7 136.13 5.27 5 -5 7 129.59 5.22 5 -5 7 160.27 6.70 -5 -5 -7 144.27 5.07 -5 -5 -7 115.33 5.98 5 5 7 139.76 5.37 -5 5 -7 147.65 5.94 5 5 7 142.65 4.97 -5 -5 -7 134.43 5.28 5 5 7 132.16 5.80 -5 -5 -7 126.51 6.31 5 5 7 129.21 5.97 5 5 8 208.31 8.93 5 5 8 214.92 8.86 5 -5 8 217.76 7.83 5 -5 8 253.25 9.47 -5 -5 -8 239.12 7.71 -5 5 -8 261.61 8.91 -5 -5 -8 180.91 8.66 -5 5 -8 260.30 8.81 5 5 8 247.88 7.67 -5 -5 -8 245.08 7.98 5 5 8 226.69 8.89 5 5 8 235.68 8.73 5 5 9 193.63 8.57 5 5 9 193.25 8.75 5 -5 9 224.21 9.01 5 -5 9 224.75 7.62 -5 -5 -9 230.19 7.43 -5 5 -9 249.51 8.68 -5 -5 -9 168.01 8.33 -5 5 -9 241.85 8.51 5 5 9 236.92 7.45 -5 -5 -9 212.01 7.69 5 5 9 232.25 8.70 5 5 9 222.02 8.79 5 5 10 70.70 5.11 5 5 10 69.03 4.86 -5 -5 -10 90.34 3.88 5 -5 10 80.86 4.11 5 -5 10 83.97 4.17 5 -5 10 82.24 5.08 -5 -5 -10 61.96 4.61 -5 5 -10 88.95 4.66 -5 5 -10 82.67 4.59 5 5 10 85.35 3.92 -5 -5 -10 77.23 4.16 5 5 10 83.83 5.10 5 5 11 10.92 2.10 5 5 11 10.06 3.53 -5 -5 -11 16.10 2.54 5 -5 11 14.39 3.73 -5 -5 -11 14.09 2.20 5 5 11 13.36 2.32 5 -5 11 9.95 2.67 5 5 12 141.96 6.55 5 5 12 156.92 6.02 5 -5 12 165.70 6.81 -5 -5 -12 184.10 6.39 5 5 12 165.97 6.07 5 -5 12 154.45 6.23 5 5 13 115.10 5.06 5 5 13 112.44 5.73 5 -5 13 129.92 6.14 -5 -5 -13 128.49 5.32 5 5 13 125.10 5.01 5 -5 13 123.10 5.34 5 5 14 62.56 3.75 5 5 14 65.09 4.61 5 -5 14 79.75 5.11 -5 -5 -14 81.22 4.06 5 5 14 67.34 3.64 5 -5 14 73.43 4.13 5 -5 15 25.19 3.04 5 5 15 22.76 3.71 5 5 15 18.25 2.47 -5 -5 -15 27.75 2.81 5 5 15 22.31 2.36 5 -5 15 17.74 2.82 5 5 16 108.71 4.45 5 5 16 127.67 5.25 5 -5 16 112.84 4.88 5 5 16 109.54 4.72 -5 -5 -16 137.66 4.96 -5 5 -16 121.54 4.51 5 5 17 16.15 1.81 5 5 17 20.12 2.07 5 -5 17 20.25 2.35 -5 -5 -17 22.80 2.16 -5 -5 -18 87.89 3.31 5 -5 18 83.58 3.47 5 5 19 2.29 1.04 5 -5 19 3.87 1.27 -5 7 19 3.29 1.19 5 7 -19 3.52 1.16 -5 -7 19 6.05 2.64 -5 7 19 2.18 1.21 -5 7 18 4.16 1.58 5 -7 -18 1.06 1.51 -5 -7 18 3.96 3.23 5 7 -18 4.97 1.44 -5 7 18 2.65 1.47 -5 -7 17 7.85 3.89 5 7 -17 3.52 1.71 -5 7 17 7.28 2.03 5 -7 -17 2.44 1.90 5 7 -17 6.67 1.83 -5 7 17 5.79 1.79 5 7 -16 26.32 2.26 -5 -7 16 28.02 4.67 -5 7 16 26.62 2.41 5 -7 -16 26.16 2.75 -5 7 16 28.68 2.76 5 7 -16 24.65 2.54 -5 -7 15 80.43 5.83 -5 7 15 75.16 3.71 5 -7 -15 72.76 3.90 -5 7 15 75.15 4.03 5 -7 -15 68.35 4.11 5 7 -15 78.19 3.98 -5 -7 14 27.87 5.26 -5 7 14 32.93 2.72 -5 7 14 27.59 2.70 5 -7 -14 26.32 3.06 -5 7 14 25.89 3.01 5 -7 -14 26.80 3.20 5 7 -14 30.62 2.96 -5 -7 13 91.61 6.29 -5 7 13 88.96 4.24 -5 7 13 90.50 4.15 5 -7 -13 81.98 4.45 -5 7 13 69.96 4.29 5 -7 -13 70.97 4.41 5 7 -13 94.31 4.35 -5 -7 12 11.25 5.04 -5 7 12 7.39 2.59 5 -7 -12 9.43 2.74 -5 7 12 10.32 2.65 5 7 -12 17.62 2.58 5 -7 -12 11.38 2.88 5 -7 -11 5.91 2.90 5 7 -11 7.84 2.32 5 -7 -11 6.34 2.72 -5 -7 11 4.46 4.90 5 -7 -11 3.69 2.64 5 -7 -10 12.06 3.04 5 -7 -10 6.54 2.55 5 -7 -10 10.08 2.94 5 7 -10 14.41 2.36 -5 -7 10 15.74 4.97 5 -7 -9 89.72 4.67 5 -7 -9 73.90 5.24 5 7 -9 80.89 4.52 -5 -7 9 52.59 5.86 -5 -7 9 71.18 5.31 5 7 -9 84.78 4.73 -5 7 9 72.09 4.92 5 -7 -9 73.15 4.26 5 7 -9 94.33 3.91 -5 -7 9 103.95 6.04 5 -7 -9 73.90 4.38 5 7 -8 53.12 3.90 -5 7 8 56.05 4.27 5 -7 -8 46.45 4.41 5 -7 -8 52.99 3.86 5 -7 -8 43.91 4.32 5 7 -8 51.03 3.51 -5 -7 8 34.19 4.61 -5 -7 8 63.51 5.27 5 7 -8 50.63 3.02 5 -7 -8 49.40 3.69 -5 -7 8 45.19 4.47 -5 -7 8 49.38 4.33 5 -7 -7 41.18 3.38 -5 -7 7 44.32 4.91 5 7 -7 34.72 2.65 5 7 -7 38.84 3.38 -5 7 7 47.03 4.01 5 -7 -7 30.15 2.93 5 -7 -7 25.57 3.55 5 -7 -7 41.83 4.15 5 -7 -7 41.29 3.52 5 7 -7 38.32 3.17 -5 -7 7 34.50 4.25 -5 -7 7 39.78 4.11 -5 -7 7 37.81 3.80 5 7 -6 134.74 5.11 5 -7 -6 151.87 5.82 5 -7 -6 156.79 5.98 5 -7 -6 148.12 7.19 5 7 -6 139.58 5.74 5 7 -6 151.68 6.10 -5 7 6 174.59 6.94 -5 -7 6 152.43 7.09 -5 -7 6 145.39 7.07 -5 -7 6 131.70 6.73 5 -7 -5 8.23 2.49 5 7 -5 9.50 1.85 5 -7 -5 4.04 2.22 5 -7 -5 9.32 2.77 5 7 -5 8.43 2.10 -5 -7 5 8.10 2.86 5 7 -5 8.92 2.22 -5 7 5 7.79 2.88 -5 -7 5 12.94 3.58 -5 -7 5 8.67 2.65 -5 -7 4 113.27 5.92 5 7 -4 102.38 4.14 -5 -7 4 99.64 5.57 5 7 -4 112.57 4.08 5 -7 -4 109.46 4.76 5 -7 -4 108.71 5.90 5 7 -4 103.16 4.56 -5 7 4 113.82 5.46 5 7 -4 106.02 4.76 -5 7 4 127.13 5.61 -5 -7 4 115.33 5.84 5 -7 -4 100.25 4.37 5 -7 -3 11.38 1.92 5 -7 -3 8.81 2.43 5 -7 -3 9.86 2.69 -5 7 3 12.15 2.47 -5 -7 3 10.45 2.85 -5 7 3 7.50 2.60 -5 -7 3 4.59 3.27 -5 -7 3 17.92 3.19 5 7 -3 10.70 1.76 -5 -7 3 11.87 2.70 5 -7 -2 0.95 1.99 5 -7 -2 2.55 2.29 5 -7 -2 3.31 2.42 -5 7 2 1.35 2.26 -5 -7 2 4.22 2.57 -5 7 2 2.72 2.47 -5 -7 2 2.26 3.12 5 -7 -2 3.24 1.78 5 -7 -2 2.64 2.26 -5 -7 2 7.37 2.88 -5 -7 2 1.63 2.28 5 7 -2 2.95 1.55 5 7 -1 28.17 2.75 5 7 -1 30.54 2.11 -5 -7 1 28.21 3.45 -5 -7 1 27.11 3.03 -5 -7 1 21.07 2.64 5 -7 -1 29.54 2.84 5 -7 -1 27.82 2.62 5 -7 -1 31.13 3.34 -5 7 1 19.23 2.78 -5 -7 1 20.23 3.85 -5 7 1 33.96 3.23 -5 -7 1 27.24 3.24 5 -7 -1 21.91 3.02 5 -7 -1 27.49 2.33 5 7 0 60.75 3.58 5 7 0 60.36 2.84 -5 -7 0 53.66 4.32 -5 -7 0 58.60 4.51 -5 -7 0 58.57 3.72 -5 -7 0 47.92 3.42 -5 7 0 49.50 3.64 5 -7 0 56.78 4.06 -5 -7 0 49.42 4.66 5 -7 0 61.83 3.49 5 -7 0 50.77 2.98 -5 7 0 69.56 4.00 5 7 0 51.56 3.27 5 -7 0 48.28 3.90 -5 -7 0 58.51 3.84 5 -7 0 58.80 3.07 5 7 1 35.27 2.32 -5 -7 -1 31.22 3.74 5 7 1 35.98 3.21 -5 -7 -1 34.38 3.01 -5 -7 -1 38.48 3.29 -5 7 -1 35.05 3.05 5 -7 1 37.97 3.41 -5 -7 -1 33.22 3.94 5 -7 1 44.52 3.06 5 -7 1 30.43 2.52 5 7 1 35.51 2.35 -5 7 -1 44.68 3.40 5 7 1 32.25 2.74 5 -7 1 36.27 3.42 5 -7 1 37.07 2.54 5 7 2 60.24 4.04 -5 -7 -2 60.77 3.83 -5 -7 -2 59.33 3.67 -5 7 -2 75.98 4.02 5 -7 2 73.90 3.84 5 7 2 64.92 3.14 -5 7 -2 73.36 4.13 5 7 2 56.73 3.53 5 -7 2 64.38 3.35 5 -7 2 61.57 4.21 5 7 2 67.88 3.07 -5 -7 -2 59.38 4.66 5 7 3 52.87 3.16 5 7 3 44.82 2.59 -5 -7 -3 44.42 4.25 5 7 3 43.14 3.63 -5 -7 -3 47.90 3.47 -5 -7 -3 46.58 3.26 -5 7 -3 55.25 3.51 5 -7 3 51.39 3.37 5 7 3 44.02 2.72 -5 7 -3 50.32 3.58 -5 7 -3 51.37 3.64 5 7 3 39.93 3.08 -5 -7 -3 43.99 3.15 5 -7 3 44.42 3.64 5 -7 3 48.42 2.96 5 7 4 5.07 1.66 5 7 4 5.63 2.11 -5 -7 -4 1.64 2.92 5 7 4 3.12 2.39 -5 -7 -4 2.97 2.47 5 -7 4 6.00 2.43 -5 -7 -4 5.46 2.20 -5 7 -4 6.70 2.10 5 7 4 4.46 1.81 -5 7 -4 4.53 2.29 -5 7 -4 5.76 2.16 5 7 4 3.42 2.10 -5 -7 -4 2.75 2.18 5 -7 4 1.02 2.53 5 -7 4 5.72 2.01 5 7 5 8.42 2.17 -5 -7 -5 5.26 3.10 5 7 5 6.19 2.59 -5 -7 -5 3.75 2.64 -5 -7 -5 4.95 2.38 -5 7 -5 7.92 2.11 5 -7 5 2.34 2.45 5 -7 5 7.34 2.58 5 7 5 5.77 1.86 -5 7 -5 4.01 2.22 5 7 5 2.02 2.16 -5 -7 -5 4.86 2.44 5 -7 5 -0.25 2.38 5 7 6 9.69 2.78 -5 -7 -6 8.76 2.74 5 -7 6 13.63 2.76 -5 -7 -6 7.52 2.47 5 -7 6 5.04 2.65 5 7 6 10.53 2.09 -5 7 -6 12.09 2.47 5 7 6 6.54 2.19 -5 -7 -6 9.27 2.57 5 7 6 10.82 2.49 5 7 6 11.08 2.36 -5 -7 -6 8.56 3.29 5 7 7 65.02 4.62 -5 -7 -7 72.91 3.97 5 -7 7 79.89 4.31 5 -7 7 66.03 4.48 5 7 7 73.07 3.59 5 7 7 59.09 3.79 -5 7 -7 62.94 4.26 -5 -7 -7 73.18 4.16 5 7 7 73.40 3.93 5 7 8 12.97 2.22 5 7 8 12.18 2.48 -5 -7 -8 11.73 2.84 5 7 8 11.07 2.31 5 -7 8 18.86 2.96 -5 -7 -8 12.24 2.48 5 -7 8 11.55 3.23 5 -7 9 254.58 9.54 -5 -7 -9 280.10 9.13 5 7 9 268.64 8.86 5 7 9 268.64 8.98 -5 -7 -9 285.69 9.42 5 7 9 269.72 9.26 5 7 10 44.64 2.98 -5 -7 -10 49.38 3.28 5 -7 10 45.84 3.93 5 -7 10 45.82 3.61 5 7 10 54.99 3.36 -5 -7 -10 48.11 3.66 -5 -7 -11 149.52 5.65 -5 -7 -11 151.80 6.08 5 7 11 137.16 5.67 5 -7 11 144.18 6.01 5 -7 11 143.09 6.16 -5 -7 -12 4.03 2.58 5 7 12 1.35 2.28 5 -7 12 0.86 2.77 -5 -7 -12 3.48 1.97 5 -7 12 5.26 2.76 5 7 13 8.18 2.33 -5 -7 -13 5.98 2.46 5 -7 13 6.25 2.70 5 7 14 1.60 1.99 -5 -7 -14 0.96 2.02 5 -7 14 3.52 2.38 5 7 15 62.17 3.09 5 -7 15 70.36 3.50 -5 -7 -15 71.35 2.95 -5 -7 -16 5.89 1.27 -5 7 -16 6.46 1.42 5 7 16 5.50 1.47 5 -7 16 1.53 1.77 5 7 17 45.32 2.03 5 -7 17 49.71 2.43 -5 7 -17 50.38 2.06 5 -9 -16 5.09 1.25 5 9 -16 4.58 1.29 -5 -9 16 6.61 2.67 -5 9 15 126.28 4.54 5 -9 -15 142.40 4.80 5 9 -15 132.82 4.67 -5 -9 15 147.25 5.82 -5 9 14 2.45 1.69 5 -9 -14 1.67 1.86 5 9 -14 2.30 1.79 -5 -9 14 3.46 3.87 -5 9 13 216.41 7.01 5 -9 -13 213.95 7.18 5 9 -13 201.61 6.87 -5 -9 13 199.25 8.22 -5 9 12 5.70 2.32 5 -9 -12 5.89 2.31 5 9 -12 3.35 2.05 5 -9 -12 4.36 2.44 -5 -9 12 4.80 4.54 -5 9 11 85.27 4.06 5 -9 -11 80.50 4.07 5 9 -11 71.23 3.61 -5 -9 11 69.86 5.82 5 -9 -11 73.23 4.19 5 9 -11 67.27 3.61 5 9 -10 49.47 3.22 5 -9 -10 50.19 3.91 5 9 -10 53.98 3.11 -5 9 10 55.72 3.54 5 -9 -9 22.84 3.48 5 9 -9 19.05 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45.76 3.68 -7 -7 11 57.28 5.78 7 7 -11 41.73 3.27 7 -7 -11 44.51 3.48 7 7 -11 53.46 3.27 7 -7 -11 49.94 4.02 7 7 -10 13.14 2.49 7 -7 -10 11.22 2.94 -7 -7 10 17.98 5.05 7 -7 -10 12.42 3.32 7 -7 -10 11.94 2.65 7 7 -10 15.10 2.37 7 7 -9 14.89 2.73 7 -7 -9 23.27 3.48 7 -7 -9 18.04 3.48 -7 -7 9 15.92 3.49 7 7 -9 17.80 2.88 7 -7 -9 18.96 2.73 -7 7 9 22.36 3.64 -7 -7 9 24.83 5.13 7 7 -9 20.25 2.54 7 -7 -9 17.99 3.12 7 7 -9 23.98 2.46 -7 -7 8 83.01 5.49 -7 -7 8 72.79 5.13 7 -7 -8 80.42 4.37 -7 -7 8 92.40 5.98 7 7 -8 78.71 3.75 7 -7 -8 87.40 4.79 7 -7 -8 55.86 4.96 7 -7 -8 73.85 5.37 7 7 -8 76.22 4.30 7 7 -8 65.11 4.90 7 7 -8 82.92 4.55 -7 7 8 97.52 5.49 7 -7 -8 71.47 3.99 -7 -7 8 63.83 5.36 7 -7 -8 63.55 3.85 7 7 -7 4.27 2.00 7 -7 -7 2.70 2.62 -7 -7 7 4.98 4.49 7 -7 -7 -0.89 2.44 7 7 -7 3.40 2.13 7 -7 -7 5.95 3.01 7 -7 -7 2.40 2.85 -7 -7 7 4.98 2.82 7 7 -7 1.95 2.58 -7 -7 7 6.38 3.61 -7 7 7 0.84 3.03 7 -7 -7 1.51 2.30 7 -7 -7 1.39 2.05 -7 -7 7 8.25 3.73 7 7 -7 2.36 2.37 -7 -7 7 0.40 2.56 -7 -7 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1.11 8 -4 18 3.39 1.37 -8 6 20 4.79 1.29 -8 -6 20 6.07 3.17 8 -6 -20 3.21 1.34 -8 6 20 4.53 1.28 8 6 -20 2.28 1.20 -8 -6 19 12.53 3.86 -8 6 19 6.26 1.63 8 -6 -19 7.10 1.77 -8 6 19 7.10 1.71 8 -6 -19 5.97 1.60 8 6 -19 8.88 1.61 -8 -6 19 5.81 3.05 8 6 -18 3.91 1.74 -8 -6 18 -1.95 3.58 -8 -6 18 2.46 4.37 -8 6 18 1.71 1.82 8 -6 -18 0.64 2.02 8 -6 -18 -0.72 1.87 -8 6 18 1.97 1.95 8 6 -18 2.04 1.81 -8 -6 17 -1.86 4.18 -8 6 17 3.98 2.09 -8 -6 17 5.59 4.98 8 -6 -17 5.11 2.40 -8 6 17 3.40 2.32 8 -6 -17 2.45 2.18 8 6 -17 7.91 2.18 -8 -6 16 85.80 5.88 8 -6 -16 94.76 4.52 -8 6 16 98.39 4.55 8 6 -16 96.89 4.44 -8 -6 16 94.61 6.54 -8 6 16 93.04 4.27 -8 -6 15 14.82 4.84 8 -6 -15 17.24 2.88 -8 6 15 17.64 2.87 8 6 -15 12.17 2.67 -8 -6 15 15.45 5.54 -8 -6 14 7.86 4.78 8 -6 -14 14.93 2.83 -8 6 14 15.40 2.79 8 6 -14 11.04 2.70 -8 -6 14 15.00 5.48 8 6 -13 -3.20 2.51 -8 -6 13 1.52 4.72 8 -6 -13 1.22 2.63 -8 6 13 3.00 2.58 8 6 -13 2.05 2.35 -8 -6 13 3.34 5.36 8 -6 -12 231.94 8.47 -8 -6 12 239.65 9.63 8 6 -12 213.93 8.30 -8 6 12 286.86 8.82 8 -6 -12 259.54 8.78 8 6 -12 284.49 8.63 8 -6 -11 85.71 4.43 -8 -6 11 83.41 5.95 8 6 -11 77.91 4.17 8 -6 -11 83.09 5.67 8 6 -11 79.30 4.89 -8 -6 11 73.27 5.32 8 6 -11 79.42 4.90 -8 6 11 97.23 5.39 8 -6 -11 94.18 4.56 -8 6 11 108.09 4.59 8 6 -11 103.12 4.34 -8 -6 10 369.33 15.10 -8 -6 10 492.65 14.61 8 -6 -10 437.83 13.72 8 6 -10 439.10 13.55 8 -6 -10 495.17 14.50 8 -6 -10 449.88 15.86 8 -6 -10 298.59 14.85 8 6 -10 433.57 14.69 8 6 -10 372.12 15.07 -8 -6 10 396.84 15.21 8 6 -10 430.64 14.63 8 -6 -10 479.00 13.84 -8 6 10 503.27 15.42 8 -6 -10 501.81 14.06 8 6 -10 540.85 13.76 -8 -6 9 52.03 4.42 -8 -6 9 69.80 5.29 8 6 -9 58.66 3.37 8 -6 -9 67.79 3.77 8 -6 -9 70.59 4.44 8 -6 -9 34.30 3.86 8 -6 -9 58.80 4.91 8 6 -9 58.67 4.00 8 6 -9 51.34 4.35 -8 -6 9 52.66 4.48 8 6 -9 66.41 4.16 -8 6 9 77.63 4.90 8 -6 -9 69.40 3.68 8 -6 -9 73.33 3.69 8 6 -9 78.66 3.40 8 6 -8 255.31 10.69 8 -6 -8 282.28 11.26 8 -6 -8 318.94 10.14 8 -6 -8 180.23 10.19 8 6 -8 296.78 10.13 8 6 -8 279.18 9.10 -8 -6 8 328.37 10.36 8 -6 -8 301.38 9.44 8 6 -8 289.58 10.06 -8 -6 8 291.60 11.50 -8 6 8 330.90 11.15 8 -6 -8 304.27 9.47 -8 -6 8 250.00 10.60 -8 -6 8 250.44 10.64 8 6 -8 304.00 10.59 8 6 -8 325.96 9.24 8 -6 -7 94.64 4.72 8 -6 -7 87.73 5.53 8 6 -7 93.56 4.49 8 6 -7 80.92 3.65 -8 -6 7 89.03 5.24 8 -6 -7 84.89 4.01 -8 -6 7 89.14 5.77 -8 6 7 96.25 5.33 8 -6 -7 86.00 4.02 -8 -6 7 78.44 5.01 -8 -6 7 78.65 4.93 8 6 -7 94.52 4.88 8 6 -7 76.94 4.98 8 -6 -6 105.27 5.09 8 -6 -6 82.94 5.28 -8 6 6 111.80 5.54 8 -6 -6 99.88 5.87 8 6 -6 117.24 4.94 -8 -6 6 95.42 5.88 -8 -6 6 113.03 5.52 8 6 -6 108.15 4.12 8 -6 -6 111.82 4.54 8 -6 -6 108.23 4.55 -8 -6 6 104.15 6.15 -8 6 6 118.96 5.97 8 6 -6 100.65 4.30 -8 -6 6 107.42 5.61 8 6 -6 118.35 5.38 -8 -6 6 105.59 5.68 8 -6 -6 113.92 4.30 8 6 -5 296.38 9.76 8 -6 -5 261.48 8.89 8 -6 -5 216.16 9.57 -8 6 5 297.03 9.82 8 -6 -5 267.23 10.11 -8 -6 5 242.84 10.11 8 6 -5 278.37 8.97 -8 -6 5 257.15 9.08 8 6 -5 262.54 8.08 8 -6 -5 266.38 8.45 -8 -6 5 247.51 10.25 8 -6 -5 256.23 8.52 -8 6 5 292.82 10.05 -8 -6 5 269.94 9.98 8 6 -5 262.22 8.33 -8 -6 5 263.33 9.74 8 6 -5 294.71 9.48 8 -6 -5 279.82 8.40 8 -6 -5 205.14 8.36 -8 -6 4 622.93 22.25 -8 6 4 792.08 22.14 8 -6 -4 661.59 22.13 -8 -6 4 620.84 22.28 -8 6 4 792.90 21.98 8 -6 -4 705.12 22.21 -8 -6 4 712.02 22.22 8 6 -4 766.29 21.59 8 6 -4 782.07 21.96 -8 -6 3 305.79 10.25 -8 -6 3 285.81 11.50 8 -6 -3 305.92 11.25 -8 6 3 376.71 11.40 -8 -6 3 272.71 11.52 8 -6 -3 329.78 11.44 -8 -6 3 319.61 11.46 8 6 -3 351.08 10.80 8 6 -3 357.10 11.24 -8 -6 2 473.71 15.22 -8 -6 2 438.33 16.45 -8 6 2 555.67 16.19 8 -6 -2 483.59 16.18 -8 6 2 588.46 16.36 8 -6 -2 550.61 16.51 -8 -6 2 419.94 16.50 -8 -6 2 493.29 16.52 8 6 -2 565.05 15.86 8 6 -2 558.30 16.30 -8 -6 1 286.11 9.54 -8 -6 1 261.44 10.62 -8 6 1 327.46 10.24 8 -6 -1 265.39 10.03 -8 6 1 327.04 10.35 8 -6 -1 299.60 10.33 -8 -6 1 258.96 10.85 8 6 -1 282.10 9.87 -8 -6 1 276.66 10.58 8 6 -1 310.20 9.90 8 6 -1 313.74 10.34 -8 -6 0 61.40 3.79 -8 6 0 84.36 4.42 -8 -6 0 60.07 4.72 8 -6 0 73.30 4.13 -8 6 0 81.65 4.20 8 6 0 67.36 3.86 8 6 0 73.05 3.86 8 6 0 66.48 4.09 8 6 1 271.74 9.67 -8 -6 -1 243.95 8.78 -8 6 -1 295.36 9.77 -8 -6 -1 249.36 10.14 8 -6 1 268.02 9.54 8 6 1 264.29 8.55 8 -6 1 274.47 8.61 8 6 1 274.75 9.41 -8 -6 -1 266.30 10.19 8 6 1 278.89 9.30 8 -6 1 278.27 8.67 8 -6 1 295.91 9.27 8 6 2 3.65 2.25 -8 -6 -2 1.30 2.37 -8 -6 -2 2.16 1.88 8 -6 2 5.05 1.93 -8 6 -2 0.38 2.31 8 -6 2 3.47 2.14 8 -6 2 3.48 1.60 8 6 2 3.77 1.68 -8 -6 -2 3.84 2.74 8 6 2 2.87 1.91 8 6 2 4.93 1.88 8 6 2 2.56 1.90 -8 -6 -2 4.07 2.85 8 -6 2 3.70 1.71 8 -6 2 2.66 1.92 8 6 3 258.61 9.45 -8 -6 -3 244.29 8.53 -8 -6 -3 234.25 8.40 -8 -6 -3 249.21 9.85 8 -6 3 247.68 8.49 -8 6 -3 247.46 9.08 8 -6 3 262.94 9.90 8 -6 3 254.95 8.48 8 -6 3 252.08 8.34 8 6 3 265.51 8.34 -8 6 -3 243.18 9.26 8 -6 3 269.42 8.86 8 -6 3 281.61 8.42 8 6 3 279.35 8.87 8 6 3 267.50 9.23 -8 -6 -3 259.42 10.02 8 6 3 278.38 9.21 8 6 4 182.90 6.73 8 6 4 189.43 7.21 8 6 4 195.85 7.18 8 6 4 169.04 7.29 -8 -6 -4 180.79 6.46 -8 -6 -4 179.76 6.53 8 -6 4 184.60 6.54 -8 -6 -4 178.89 7.68 8 -6 4 175.60 6.57 8 -6 4 186.59 7.86 8 6 4 182.14 6.25 8 -6 4 156.77 6.23 -8 6 -4 171.40 7.10 -8 -6 -4 159.72 6.44 8 -6 4 186.18 6.71 8 -6 4 186.95 6.30 8 6 5 112.41 5.73 -8 -6 -5 123.60 4.94 8 -6 5 115.67 4.98 8 -6 5 111.15 5.06 8 -6 5 122.32 6.24 8 6 5 122.97 4.74 -8 6 -5 109.00 5.43 -8 -6 -5 116.84 5.06 8 6 5 120.35 4.67 8 6 5 126.54 5.24 8 6 5 127.17 5.66 8 6 5 116.54 5.61 8 6 6 319.67 11.95 -8 -6 -6 363.54 10.97 8 -6 6 343.02 11.11 8 -6 6 358.82 12.84 8 6 6 345.69 10.72 -8 6 -6 311.50 11.67 -8 -6 -6 355.32 11.13 8 6 6 329.31 10.67 8 6 6 374.27 11.39 8 6 6 357.03 11.95 8 6 6 331.89 11.88 8 6 7 67.87 4.59 -8 -6 -7 81.87 3.95 8 -6 7 67.60 3.67 8 -6 7 68.06 4.16 8 6 7 72.89 3.61 -8 6 -7 71.04 4.52 -8 6 -7 70.62 4.29 8 6 7 73.82 3.72 -8 -6 -7 76.41 4.11 8 6 7 78.29 4.22 8 -6 8 162.42 6.45 8 -6 8 170.63 6.79 -8 -6 -8 186.57 6.87 8 6 8 178.72 6.45 8 6 8 175.83 6.96 -8 -6 -8 194.16 6.65 8 -6 9 11.80 2.58 8 -6 9 16.50 3.00 8 6 9 17.19 2.50 -8 -6 -9 18.38 2.92 8 6 9 15.00 2.67 -8 -6 -9 20.23 2.51 -8 -6 -10 79.30 3.93 -8 -6 -10 76.15 3.91 8 -6 10 68.27 4.01 8 -6 10 69.06 4.19 -8 -6 -10 75.20 4.15 8 6 10 72.76 3.86 -8 -6 -11 1.18 2.14 -8 -6 -11 2.64 2.12 8 -6 11 2.03 2.51 8 -6 11 -0.09 2.71 -8 -6 -11 2.71 2.41 8 6 11 1.27 2.27 -8 -6 -12 159.98 5.78 -8 -6 -12 168.81 5.97 8 6 12 144.46 5.83 8 -6 12 166.31 6.15 8 -6 12 144.73 6.02 8 -6 13 25.49 2.75 -8 -6 -13 28.88 2.39 -8 -6 -13 30.75 2.58 8 6 13 24.69 2.52 8 -6 13 29.64 2.88 8 -6 14 53.63 3.28 8 6 14 51.48 2.96 -8 -6 -14 65.75 3.17 -8 -6 -14 61.93 2.93 8 6 14 52.39 2.98 8 -6 14 68.26 3.46 8 6 15 6.72 1.62 -8 -6 -15 8.50 1.71 8 6 15 5.80 1.59 8 -6 15 6.58 1.95 8 6 16 31.61 1.95 8 6 16 32.19 1.89 8 -6 16 39.97 2.30 -8 -6 -16 39.83 2.03 -8 -8 18 3.23 2.31 8 -8 -18 2.86 1.08 -8 8 18 2.97 0.96 8 8 -18 1.52 1.12 -8 -8 17 90.57 4.33 -8 8 17 74.76 2.97 8 -8 -17 66.47 2.94 -8 8 17 78.01 3.02 8 -8 -17 81.42 3.21 8 8 -17 76.68 3.13 -8 -8 16 62.46 4.46 -8 8 16 53.43 2.59 -8 8 16 50.30 2.62 8 -8 -16 47.34 2.71 8 -8 -16 58.58 2.94 -8 8 16 54.56 2.70 8 8 -16 53.59 2.81 -8 -8 15 86.05 5.43 -8 8 15 86.75 3.65 8 -8 -15 75.47 3.69 8 -8 -15 80.39 3.85 8 8 -15 78.00 3.64 -8 -8 14 6.93 4.72 -8 8 14 6.92 2.21 8 -8 -14 6.86 2.41 8 -8 -14 3.64 2.30 8 8 -14 1.58 2.11 8 8 -13 11.11 2.47 8 -8 -13 8.37 2.56 -8 -8 13 11.90 5.19 -8 8 13 10.44 2.57 8 -8 -13 10.48 2.81 8 -8 -13 10.18 2.59 8 8 -13 11.36 2.40 -8 -8 12 16.15 5.42 8 -8 -12 6.04 2.76 8 8 -12 10.14 2.51 -8 8 12 9.20 2.71 8 -8 -12 12.81 2.98 8 -8 -12 11.61 2.63 8 8 -12 15.51 2.42 8 -8 -11 1.23 2.76 -8 -8 11 3.20 5.31 8 8 -11 3.05 2.51 8 -8 -11 6.92 3.05 -8 8 11 -2.96 2.87 8 -8 -11 4.89 2.43 8 8 -11 4.80 2.20 8 -8 -10 41.06 3.25 -8 -8 10 43.07 5.79 8 8 -10 42.67 3.26 8 -8 -10 32.56 3.63 8 -8 -10 45.94 3.91 8 -8 -10 39.15 3.06 8 8 -10 42.67 2.93 8 -8 -9 1.69 2.48 8 -8 -9 0.10 3.06 -8 -8 9 2.43 5.16 8 8 -9 3.31 2.29 8 -8 -9 3.60 3.09 8 -8 -9 -0.09 2.15 -8 -8 9 7.25 3.96 8 -8 -8 10.39 2.67 8 -8 -8 10.24 3.04 -8 -8 8 13.88 5.26 8 8 -8 14.51 2.41 8 -8 -8 12.92 3.37 -8 -8 8 10.49 4.29 8 -8 -8 13.77 2.50 8 -8 -7 1.36 2.51 8 -8 -7 1.41 2.89 8 8 -7 4.84 2.25 -8 -8 7 3.74 4.96 8 -8 -7 3.97 2.22 -8 -8 7 0.65 4.04 8 -8 -7 1.11 3.12 8 -8 -6 8.34 3.14 8 8 -6 9.96 2.15 8 -8 -6 7.45 2.89 -8 -8 6 11.04 4.99 8 -8 -6 3.87 2.56 -8 -8 6 9.15 4.19 8 -8 -6 8.81 2.42 8 8 -6 8.89 2.18 8 8 -5 2.19 2.10 8 -8 -5 5.55 3.17 8 -8 -5 2.97 2.76 8 8 -5 3.05 2.03 8 -8 -5 0.92 2.62 -8 -8 5 5.57 3.90 8 -8 -5 2.76 2.29 8 8 -4 152.34 5.91 8 -8 -4 169.52 6.79 8 8 -4 166.37 5.68 -8 -8 4 168.54 7.69 8 -8 -4 178.50 6.39 -8 -8 3 12.81 3.29 -8 8 3 8.11 2.89 8 -8 -3 17.16 2.56 -8 -8 3 18.46 3.77 8 8 -3 13.20 2.23 -8 -8 2 138.05 7.59 8 8 -2 165.14 5.97 -8 -8 2 169.25 6.86 -8 8 2 132.85 6.78 -8 -8 2 118.48 7.88 8 -8 -2 147.05 7.45 8 -8 -2 179.00 6.25 -8 8 2 195.42 7.38 -8 -8 2 180.09 7.47 8 -8 -2 172.67 6.33 8 -8 -2 166.28 6.94 8 8 -1 35.94 2.73 -8 -8 1 35.69 3.79 -8 8 1 29.95 3.38 8 -8 -1 30.86 3.67 8 -8 -1 34.51 2.86 -8 8 1 38.98 3.49 -8 -8 1 45.20 3.97 8 -8 -1 40.73 3.80 8 -8 -1 36.13 3.04 8 -8 0 109.22 5.17 -8 -8 0 101.54 5.24 8 8 0 95.20 4.39 8 8 0 100.32 4.28 8 -8 0 104.27 5.53 8 -8 0 106.15 4.71 8 -8 1 285.44 9.35 -8 -8 -1 266.43 9.14 -8 -8 -1 233.05 8.92 8 8 1 242.57 8.47 8 8 1 250.88 8.76 8 8 1 258.87 8.34 8 -8 1 264.71 8.78 8 -8 1 275.05 9.79 -8 -8 -2 13.47 2.82 8 -8 2 15.53 2.96 -8 -8 -2 14.62 3.11 8 8 2 11.97 2.38 8 -8 2 15.65 3.28 8 -8 2 15.65 2.55 8 8 2 15.77 2.53 8 8 2 14.10 2.13 8 8 3 233.35 8.45 8 8 3 236.89 7.86 8 -8 3 236.86 8.99 -8 -8 -3 246.10 8.62 -8 -8 -3 234.31 8.59 8 8 3 229.13 8.19 -8 -8 -3 248.77 8.49 8 -8 3 256.31 8.49 8 -8 3 241.19 9.28 8 8 4 92.47 4.65 8 -8 4 107.23 5.14 8 -8 4 91.18 5.23 -8 -8 -4 102.79 4.84 -8 -8 -4 98.73 4.99 8 8 4 96.07 4.47 -8 -8 -4 100.89 4.72 8 -8 4 89.58 5.25 8 8 5 15.83 2.68 -8 -8 -5 17.56 2.90 8 -8 5 16.91 3.43 8 -8 5 24.04 3.32 -8 -8 -5 18.47 3.04 8 8 5 13.07 2.50 -8 -8 -5 18.93 2.89 8 -8 5 15.21 3.07 8 -8 6 241.91 9.33 -8 -8 -6 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98.58 4.76 10 4 5 99.17 4.86 10 4 5 97.13 5.07 -10 -4 -5 93.48 5.43 10 -4 5 104.76 4.40 -10 -4 -5 97.07 5.32 10 -4 5 121.15 5.43 10 4 5 121.46 4.43 10 4 5 107.72 5.36 10 4 5 110.44 5.05 10 4 6 14.91 2.51 10 4 6 10.30 2.39 -10 -4 -6 10.43 2.80 -10 4 -6 12.82 2.26 -10 -4 -6 10.10 2.73 10 -4 6 13.69 2.37 10 -4 6 13.64 2.43 10 4 6 14.40 2.07 10 4 6 13.83 2.83 10 4 7 107.22 5.57 10 4 7 103.04 5.20 10 -4 7 110.44 4.76 -10 -4 -7 106.64 5.67 10 -4 7 116.85 5.62 -10 4 -7 120.90 5.49 10 4 7 127.85 4.76 10 4 7 101.99 5.66 10 4 8 193.17 8.17 10 4 8 234.24 9.04 10 -4 8 228.69 7.55 10 -4 8 223.77 7.72 10 -4 8 215.58 8.65 10 4 8 208.41 7.66 -10 4 -8 241.22 8.70 10 4 8 245.42 7.73 10 4 8 209.58 8.88 10 4 9 111.86 4.82 10 4 9 98.71 5.03 10 -4 9 111.57 4.70 10 -4 9 102.57 4.80 10 4 9 112.54 4.71 10 -4 10 24.07 2.69 10 4 10 32.22 2.89 10 4 10 26.15 3.60 10 -4 10 30.82 2.91 10 -4 10 27.51 3.07 10 4 10 27.15 2.72 10 4 11 114.10 4.81 10 -4 11 95.98 4.53 10 4 11 98.77 4.47 10 -4 11 106.51 4.72 10 -4 11 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6.86 1.77 10 -6 -6 4.56 2.07 -10 -6 6 3.86 3.24 -10 6 6 3.77 2.96 -10 -6 6 3.91 3.00 10 6 -6 4.71 2.38 10 6 -6 5.82 2.00 10 -6 -6 3.97 1.48 10 6 -5 3.98 2.35 10 -6 -5 0.89 1.97 -10 -6 5 3.75 3.73 10 -6 -5 0.36 2.58 10 6 -5 4.89 1.68 10 -6 -5 0.09 2.45 10 -6 -5 1.49 2.57 10 -6 -5 0.92 1.75 -10 6 5 -0.45 2.39 10 -6 -5 0.16 1.96 -10 -6 5 2.99 3.20 -10 6 5 -0.40 2.87 -10 -6 5 3.17 2.99 10 6 -5 1.64 2.08 10 6 -5 -0.64 1.90 10 -6 -5 1.02 1.37 10 -6 -5 -0.24 1.98 10 6 -4 2.52 2.26 -10 -6 4 -0.08 3.60 10 -6 -4 1.55 2.47 10 -6 -4 0.17 2.41 10 -6 -4 1.27 2.48 10 -6 -4 1.71 1.65 -10 6 4 1.39 2.41 10 -6 -4 4.55 1.53 -10 -6 4 3.88 3.03 10 -6 -4 1.68 1.93 -10 6 4 5.59 2.87 -10 -6 4 1.36 2.91 10 6 -4 -0.12 1.96 10 6 -4 0.04 1.86 10 -6 -4 2.79 1.44 10 -6 -4 3.73 2.03 10 -6 -3 34.75 2.80 10 -6 -3 32.74 2.97 10 -6 -3 35.65 3.03 10 -6 -3 43.75 3.35 -10 6 3 43.92 3.63 -10 -6 3 31.38 3.94 10 -6 -3 39.33 2.48 -10 -6 3 36.31 3.96 10 -6 -3 34.23 2.67 10 6 -3 31.35 2.94 10 6 -3 36.17 2.58 10 6 -3 39.20 3.04 10 6 -3 36.85 3.36 10 6 -2 120.75 5.68 -10 -6 2 107.03 5.07 10 -6 -2 112.35 5.42 10 -6 -2 126.79 5.25 -10 6 2 135.57 5.89 -10 -6 2 97.58 6.03 10 -6 -2 136.78 4.76 10 6 -2 119.35 4.76 -10 -6 2 101.38 6.05 10 6 -2 110.40 5.28 10 6 -2 120.73 4.65 10 6 -2 125.62 5.38 10 -6 -2 122.10 4.86 10 -6 -2 115.91 5.23 10 6 -1 123.68 5.66 -10 -6 1 110.41 5.09 10 -6 -1 106.01 5.23 -10 6 1 129.93 5.72 -10 -6 1 96.25 5.96 10 6 -1 118.05 4.69 10 -6 -1 125.46 4.64 -10 -6 1 95.95 5.82 10 6 -1 109.86 5.22 10 6 -1 116.01 4.48 10 6 -1 114.54 5.16 10 -6 -1 116.11 4.67 10 -6 -1 111.13 5.11 10 6 0 236.74 8.72 -10 -6 0 198.22 7.80 10 -6 0 221.88 8.47 -10 6 0 268.13 8.92 -10 -6 0 199.87 9.11 10 -6 0 245.04 7.61 10 6 0 229.87 7.66 -10 -6 0 198.85 8.92 10 6 0 223.90 8.33 10 6 0 224.59 7.42 10 6 0 231.50 8.30 10 -6 0 248.20 7.69 10 -6 0 231.56 8.22 10 6 1 132.46 6.02 -10 -6 -1 112.70 5.29 -10 -6 -1 109.41 6.30 -10 6 -1 149.54 6.15 10 6 1 132.66 5.05 10 -6 1 133.37 4.97 -10 -6 -1 112.81 6.15 10 6 1 121.53 5.28 10 6 1 124.74 5.62 10 6 1 133.59 5.63 10 -6 1 134.10 4.96 10 -6 1 130.37 5.44 10 6 2 33.56 3.27 -10 -6 -2 32.06 3.13 10 -6 2 41.63 2.83 -10 -6 -2 30.37 3.84 10 -6 2 40.95 3.65 10 6 2 39.88 2.74 10 -6 2 38.43 2.63 -10 6 -2 30.74 2.99 10 6 2 34.84 3.03 10 6 2 32.71 3.03 10 6 2 38.41 3.11 10 -6 2 39.95 2.59 10 -6 2 39.57 3.09 10 6 3 41.08 3.58 -10 -6 -3 43.56 3.03 -10 -6 -3 43.82 3.37 10 -6 3 46.72 3.05 -10 -6 -3 42.21 4.04 10 -6 3 44.13 3.19 10 -6 3 42.22 3.81 10 6 3 48.50 2.95 10 -6 3 42.91 2.80 -10 6 -3 41.21 3.23 10 -6 3 45.28 2.80 10 -6 3 44.05 3.23 10 6 3 41.06 3.25 10 6 3 50.30 3.45 10 6 3 47.69 3.41 10 6 4 227.01 7.98 10 6 4 229.71 8.34 10 6 4 214.31 8.19 10 6 4 225.11 8.20 10 6 4 195.65 8.28 -10 -6 -4 209.35 7.39 -10 -6 -4 208.20 8.75 10 -6 4 213.01 7.50 10 -6 4 222.13 9.06 10 6 4 216.96 7.30 10 -6 4 213.46 7.31 -10 6 -4 203.95 8.10 -10 -6 -4 197.37 7.49 10 6 4 206.67 7.21 10 -6 4 207.90 7.20 10 -6 4 216.89 7.72 -10 -6 -5 250.11 8.44 10 -6 5 242.02 8.48 10 -6 5 262.43 10.23 10 6 5 225.47 9.28 10 6 5 251.85 8.33 -10 -6 -5 243.20 8.57 10 6 5 255.32 8.35 10 6 5 265.25 9.03 10 6 5 259.84 9.41 10 6 5 242.63 9.25 10 -6 6 174.34 6.77 -10 -6 -6 186.17 6.63 10 6 6 177.88 6.44 10 6 6 175.73 6.52 -10 -6 -6 172.17 6.80 10 6 6 188.04 7.17 10 -6 7 167.49 6.69 -10 -6 -7 180.23 6.57 10 6 7 170.51 6.38 -10 -6 -7 178.40 6.83 10 6 7 178.83 6.54 10 6 7 193.71 7.14 10 -6 8 423.49 13.47 10 6 8 419.51 13.28 -10 -6 -8 427.60 13.56 10 6 8 448.17 13.94 -10 -6 -8 451.89 13.39 10 -6 9 84.23 4.18 10 -6 9 84.13 4.52 10 6 9 84.61 4.27 -10 -6 -9 87.96 4.48 10 6 9 92.97 4.69 -10 -6 -9 91.52 4.32 10 -6 10 131.10 5.30 10 -6 10 125.82 5.53 -10 -6 -10 140.79 5.33 10 6 10 121.53 5.26 10 -6 11 49.69 3.31 10 -6 11 48.22 3.55 -10 -6 -11 59.02 3.33 -10 -6 -11 53.09 3.25 10 6 11 43.36 3.20 10 -6 12 5.58 2.28 -10 -6 -12 3.87 2.00 10 -6 12 5.24 2.49 -10 -6 -12 4.22 2.03 10 6 12 0.50 2.01 -10 -6 -13 2.27 1.73 10 -6 13 6.39 2.19 -10 -6 -13 4.03 1.82 10 6 13 4.02 1.76 -10 -6 -14 2.82 1.48 -10 -6 -14 3.56 1.60 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10 -8 -11 3.09 3.05 10 -8 -11 1.60 2.18 10 8 -11 1.45 2.08 10 -8 -10 11.58 2.67 10 -8 -10 12.54 3.08 -10 -8 10 22.59 5.58 10 8 -10 14.75 2.71 10 -8 -10 16.02 3.44 10 -8 -10 14.52 2.59 10 -8 -9 15.87 2.82 10 -8 -9 17.11 3.26 -10 -8 9 16.80 5.39 10 8 -9 18.88 2.67 10 -8 -9 21.90 3.69 10 -8 -9 19.72 2.75 -10 -8 9 19.23 4.39 10 -8 -8 -1.84 2.58 10 -8 -8 1.91 2.78 -10 -8 8 -0.30 5.15 10 8 -8 0.71 2.36 10 -8 -8 0.81 2.32 -10 -8 8 0.53 3.78 10 -8 -8 2.20 3.26 10 -8 -7 7.21 3.49 10 -8 -7 9.68 2.96 -10 -8 7 8.75 5.11 10 8 -7 8.70 2.27 10 -8 -7 5.99 2.70 -10 -8 7 10.63 3.91 10 -8 -7 9.01 2.57 10 8 -7 8.46 2.40 10 8 -6 31.50 2.77 10 -8 -6 28.68 3.84 -10 -8 6 34.98 5.24 10 8 -6 32.00 2.70 10 -8 -6 33.81 3.26 10 -8 -6 25.77 3.13 -10 -8 6 34.68 4.65 10 -8 -6 33.70 3.15 -10 -8 5 15.58 4.86 10 8 -5 15.96 2.25 10 -8 -5 11.90 2.75 10 -8 -5 14.48 3.41 10 8 -5 14.73 2.44 10 -8 -5 16.64 2.75 -10 -8 5 13.36 3.98 -10 -8 4 13.94 3.37 -10 -8 4 10.58 4.59 10 -8 -4 5.96 2.62 -10 -8 4 13.46 3.78 10 -8 -4 11.71 2.57 10 8 -4 4.44 2.25 10 8 -3 100.40 4.62 -10 -8 3 100.50 6.18 -10 -8 3 101.75 5.43 10 -8 -3 97.25 4.97 -10 -8 3 107.21 5.90 10 -8 -3 112.48 5.03 10 -8 -3 104.48 5.42 10 8 -2 73.67 3.85 10 -8 -2 86.95 4.00 -10 -8 2 71.95 4.76 10 -8 -2 68.02 4.21 -10 -8 2 83.81 5.08 10 -8 -2 74.60 4.18 10 -8 -2 79.66 4.74 10 8 -1 82.49 4.06 10 8 -1 83.26 4.21 10 -8 -1 100.96 4.42 -10 -8 1 81.08 4.91 10 -8 -1 81.63 4.45 -10 -8 1 86.49 5.06 10 -8 -1 90.38 4.44 10 -8 -1 96.28 5.13 -10 -8 0 239.40 8.75 10 8 0 223.39 8.17 10 -8 0 248.48 8.42 10 -8 0 251.24 8.47 10 8 0 234.56 8.01 10 8 1 57.03 3.66 10 8 1 62.02 3.41 10 -8 1 78.25 4.20 -10 -8 -1 62.43 4.33 10 8 1 62.77 3.65 -10 -8 -1 62.22 3.77 10 -8 1 63.33 3.73 10 -8 1 72.98 4.59 10 8 2 151.77 6.20 10 8 2 147.73 5.66 -10 -8 -2 154.95 6.50 -10 -8 -2 142.57 6.14 10 8 2 148.05 6.03 -10 -8 -2 150.98 6.20 10 -8 2 169.96 6.24 10 -8 2 168.12 7.04 10 8 3 30.25 2.98 -10 -8 -3 32.79 3.20 -10 -8 -3 34.74 3.46 10 8 3 33.77 2.94 -10 -8 -3 33.55 3.15 10 -8 3 38.06 3.71 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12.55 2.34 -10 -10 3 12.16 3.13 10 10 -3 11.26 2.11 10 10 -2 69.26 3.60 10 -10 -2 83.66 4.25 -10 -10 2 88.14 4.36 -10 -10 2 78.72 4.62 10 -10 -2 73.16 3.94 10 -10 -2 74.31 4.50 -10 -10 1 2.13 2.72 10 10 -1 2.24 2.00 10 -10 -1 -0.30 2.15 10 -10 -1 -2.10 2.82 10 -10 -1 1.10 2.39 -10 -10 0 17.57 2.97 10 10 0 14.47 2.13 10 -10 0 9.92 2.96 10 -10 1 15.72 2.86 10 10 1 16.67 2.31 -10 -10 -1 19.22 2.88 10 10 1 17.80 2.13 10 -10 1 13.34 3.18 10 10 2 27.97 2.60 -10 -10 -2 37.12 3.16 -10 -10 -2 30.64 2.93 10 10 2 30.83 2.58 10 10 2 29.08 2.33 10 -10 2 30.68 3.55 10 10 3 33.61 2.66 -10 -10 -3 33.67 3.03 -10 -10 -3 31.67 2.85 10 -10 3 25.74 3.42 10 10 3 34.38 2.67 10 10 3 33.27 2.28 10 10 4 73.90 3.67 -10 -10 -4 70.40 3.76 -10 -10 -4 78.04 3.77 10 10 4 69.92 3.59 -10 -10 -4 83.87 3.56 10 -10 4 60.80 4.25 10 10 5 20.04 2.23 -10 -10 -5 15.62 2.34 -10 -10 -5 20.40 2.36 10 10 5 18.52 2.22 -10 -10 -5 22.88 2.20 10 -10 5 12.91 2.67 -10 -10 -6 5.86 1.95 10 -10 6 6.95 2.49 -10 -10 -6 6.88 1.85 10 10 6 5.53 1.79 -10 -10 -6 6.32 1.76 10 10 6 7.74 1.86 10 10 7 1.76 1.54 10 10 7 0.54 1.57 -10 -10 -7 1.30 1.55 -10 -10 -7 0.30 1.70 10 -10 7 1.59 2.24 10 10 8 1.67 1.31 10 10 8 0.77 1.38 -10 -10 -8 2.17 1.46 10 -10 8 5.49 2.19 -10 -10 -8 3.52 1.40 10 10 9 5.08 1.24 -10 -10 -9 5.77 1.16 -10 -10 -9 7.39 1.34 10 -10 9 6.47 1.87 -11 -1 23 18.82 2.01 -11 1 23 19.76 1.96 11 1 -23 12.20 1.24 11 -1 -23 10.16 1.21 -11 -1 23 13.08 1.66 -11 1 23 13.35 1.61 11 1 -23 14.31 1.36 -11 -1 22 14.41 2.71 -11 1 22 15.26 2.55 11 1 -22 9.95 1.55 11 -1 -22 9.13 1.52 -11 1 22 12.24 2.00 -11 -1 22 10.25 2.12 11 1 -22 10.95 1.78 11 -1 -22 9.58 1.65 -11 -1 21 58.16 3.93 -11 1 21 63.34 3.84 11 1 -21 56.33 2.90 11 -1 -21 52.10 2.90 -11 1 21 58.77 3.36 -11 -1 21 56.13 3.48 11 1 -21 56.69 3.13 11 -1 -21 51.83 2.72 11 -1 -21 57.20 3.07 -11 -1 20 6.08 3.63 -11 1 20 3.09 3.55 11 -1 -20 1.96 2.04 11 1 -20 0.65 1.97 -11 1 20 0.04 2.69 -11 -1 20 -0.76 2.69 11 1 -20 1.38 2.42 11 -1 -20 1.48 1.80 11 -1 -20 2.34 2.23 -11 -1 19 94.00 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9 34.60 3.82 11 -5 -9 33.84 2.55 11 -5 -9 37.27 2.33 11 5 -9 33.93 2.73 11 5 -8 114.06 6.43 11 -5 -8 135.31 5.88 11 -5 -8 134.54 6.34 11 -5 -8 140.08 7.07 11 5 -8 142.16 6.26 -11 -5 8 155.16 6.41 11 -5 -8 159.33 6.27 11 5 -8 127.13 5.15 11 -5 -8 133.59 5.20 -11 -5 8 140.96 7.12 11 -5 -8 154.34 5.41 -11 5 8 165.72 7.13 11 5 -8 111.47 5.25 11 5 -8 138.28 6.19 11 -5 -8 152.13 5.13 11 5 -7 45.73 4.13 11 -5 -7 58.67 3.82 11 -5 -7 63.48 4.00 11 5 -7 70.37 4.08 -11 -5 7 68.73 4.61 11 -5 -7 69.30 4.17 11 5 -7 60.85 3.18 11 -5 -7 61.34 3.25 -11 -5 7 68.72 4.94 -11 5 7 76.32 4.78 11 -5 -7 69.66 3.37 11 5 -7 54.41 3.30 11 5 -7 65.93 4.03 11 -5 -7 66.46 3.06 11 5 -6 55.21 4.34 11 -5 -6 79.58 4.31 11 -5 -6 73.36 3.90 -11 -5 6 74.02 4.57 11 -5 -6 67.92 4.06 11 5 -6 73.79 3.28 11 -5 -6 70.59 3.37 -11 -5 6 71.05 4.98 -11 5 6 80.71 4.81 11 -5 -6 75.67 3.44 11 5 -6 64.15 3.44 11 5 -6 72.84 4.08 11 -5 -6 75.58 3.20 11 -5 -5 296.68 9.95 11 -5 -5 268.34 8.97 11 -5 -5 318.00 10.52 -11 -5 5 269.54 10.60 11 5 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1 170.69 6.20 11 5 1 183.76 6.90 11 5 1 182.52 7.00 11 5 1 185.01 6.88 11 5 2 8.94 2.48 11 5 2 11.71 2.37 11 -5 2 10.56 2.04 11 -5 2 10.07 1.85 11 -5 2 12.67 2.50 11 -5 2 10.48 1.73 11 5 2 16.04 2.04 -11 -5 -2 14.67 3.01 -11 -5 -2 11.46 2.80 11 5 2 11.18 1.93 11 5 2 11.56 2.24 11 5 2 10.35 2.42 11 5 2 13.44 2.26 11 5 3 37.19 3.37 11 5 3 35.67 3.18 11 -5 3 32.76 2.74 -11 -5 -3 39.80 3.81 11 -5 3 35.23 2.71 11 -5 3 41.40 3.57 11 5 3 40.86 2.71 -11 -5 -3 42.66 3.77 11 5 3 36.83 2.71 11 5 3 42.16 3.25 11 5 3 42.29 3.21 11 5 3 39.58 3.12 11 5 4 1.61 2.32 11 5 4 6.85 2.21 11 5 4 4.66 2.14 -11 -5 -4 7.29 1.98 11 -5 4 6.79 2.23 11 -5 4 4.89 2.24 11 5 4 7.41 1.88 -11 -5 -4 5.34 2.62 -11 -5 -4 5.75 2.73 11 5 4 2.58 1.89 11 5 4 5.03 2.45 11 5 4 5.35 2.27 11 5 5 6.50 2.38 11 5 5 1.14 2.03 11 -5 5 3.86 2.31 11 -5 5 4.26 2.39 11 5 5 6.68 1.85 -11 -5 -5 1.89 2.60 11 5 5 2.76 2.04 11 5 5 4.95 2.54 11 5 5 1.03 2.15 11 -5 6 19.91 2.81 11 -5 6 22.31 3.06 11 5 6 29.29 2.98 11 5 6 17.34 2.76 -11 5 -6 22.83 2.79 -11 -5 -6 19.40 3.23 -11 -5 -6 17.70 2.74 11 5 6 20.45 2.52 11 5 6 18.22 3.10 -11 -5 -7 166.99 6.51 11 5 7 176.21 6.40 11 -5 7 153.85 6.35 11 5 8 27.24 2.80 11 -5 8 24.45 3.03 11 5 8 34.10 3.38 11 -5 9 93.97 4.35 11 -5 9 94.28 4.65 11 5 9 95.20 4.49 11 5 9 105.36 5.17 -11 -5 -9 97.39 4.46 -11 -5 -10 45.13 3.12 11 5 10 36.38 3.02 11 -5 10 38.36 3.00 11 -5 10 35.22 3.28 11 5 11 2.93 2.18 -11 -5 -11 3.06 2.24 11 -5 11 7.59 2.43 11 -5 11 3.48 2.64 11 5 12 11.65 2.22 -11 -5 -12 19.11 2.39 -11 -5 -12 19.05 2.60 11 5 12 16.43 2.25 11 -5 12 18.29 2.65 11 5 13 64.82 3.48 11 5 13 67.78 3.39 -11 -5 -13 86.30 3.54 -11 -5 -13 84.71 3.77 -11 -5 -14 3.05 1.60 -11 -5 -14 1.83 1.75 11 5 14 3.38 1.50 11 -5 14 3.57 1.82 11 5 14 1.39 1.58 -11 -5 -15 10.98 1.59 -11 -5 -15 11.95 1.47 11 5 15 7.16 1.62 11 5 15 8.46 1.50 11 5 16 0.60 0.98 11 5 16 -0.12 1.03 -11 -5 -16 0.96 1.00 -11 7 19 32.30 1.69 11 -7 -19 24.86 1.60 -11 7 19 31.11 1.63 11 7 -19 25.54 1.69 -11 -7 18 17.97 2.99 -11 -7 18 21.17 3.57 -11 7 18 16.97 1.65 11 -7 -18 15.95 1.77 11 -7 -18 13.99 1.69 -11 7 18 13.35 1.61 11 7 -18 12.73 1.78 -11 -7 17 47.32 3.96 -11 7 17 41.02 2.38 -11 -7 17 51.23 4.54 11 -7 -17 40.22 2.61 11 -7 -17 30.49 2.40 -11 7 17 31.78 2.30 11 -7 -17 27.70 1.97 11 7 -17 39.25 2.52 11 7 -16 8.79 2.15 -11 -7 16 13.74 4.14 -11 7 16 11.13 2.01 -11 7 16 6.58 1.85 -11 -7 16 12.06 4.64 11 -7 -16 10.58 2.38 11 -7 -16 5.33 2.09 -11 7 16 6.67 1.96 11 -7 -16 6.26 1.64 11 7 -16 8.63 2.15 -11 -7 15 312.69 10.02 11 7 -15 263.02 8.73 -11 -7 15 302.96 10.18 11 -7 -15 269.95 9.00 11 -7 -15 230.17 8.69 -11 7 15 265.32 8.64 11 7 -15 275.13 8.75 -11 -7 14 19.30 5.03 11 7 -14 20.13 2.69 -11 -7 14 19.44 5.49 11 -7 -14 16.25 3.17 11 -7 -14 14.94 2.63 11 7 -14 20.25 2.64 -11 -7 13 97.13 6.47 11 7 -13 87.73 4.31 -11 -7 13 92.29 6.71 11 -7 -13 81.51 4.82 11 -7 -13 74.81 4.24 11 7 -13 84.42 4.10 11 7 -12 2.70 2.63 11 -7 -12 4.83 2.70 -11 -7 12 1.67 5.26 11 -7 -12 3.01 3.24 -11 -7 12 1.96 5.55 11 -7 -12 3.88 2.39 11 7 -12 3.97 2.23 11 -7 -11 49.40 4.28 -11 -7 11 58.30 6.03 11 7 -11 45.51 3.52 11 -7 -11 49.23 3.74 11 -7 -11 51.22 3.51 11 -7 -11 50.36 3.42 11 7 -11 46.17 3.22 11 -7 -10 21.79 2.96 -11 -7 10 21.10 5.41 11 -7 -10 20.30 3.04 11 7 -10 17.92 2.85 11 -7 -10 22.47 3.81 11 7 -10 14.39 2.40 11 -7 -10 13.72 2.73 11 -7 -9 4.17 2.57 11 -7 -9 5.47 2.72 -11 -7 9 3.34 5.02 11 7 -9 2.77 2.36 11 -7 -9 -2.24 2.55 11 -7 -9 1.39 3.27 11 -7 -8 19.81 3.65 -11 -7 8 20.88 5.18 11 7 -8 18.03 2.62 11 -7 -8 22.23 3.04 11 -7 -8 20.55 2.85 11 7 -8 17.29 2.67 11 -7 -8 15.54 2.82 11 -7 -7 43.65 4.13 -11 -7 7 44.89 5.37 11 7 -7 46.90 3.07 11 -7 -7 41.38 3.92 11 -7 -7 48.35 3.50 11 -7 -7 50.47 3.51 11 7 -7 46.55 3.23 11 -7 -7 44.91 3.58 11 -7 -6 0.74 3.09 -11 7 6 -0.25 2.58 11 -7 -6 4.08 2.49 -11 -7 6 2.52 4.70 11 7 -6 3.01 2.03 -11 7 6 3.73 2.99 11 -7 -6 3.44 2.51 -11 -7 6 2.78 3.30 11 7 -6 3.15 2.18 11 -7 -6 3.31 2.50 11 7 -5 154.93 7.56 -11 -7 5 162.27 7.55 -11 -7 5 161.13 6.88 11 -7 -5 173.66 7.00 -11 7 5 198.61 7.76 -11 -7 5 119.91 7.67 -11 -7 5 130.35 7.85 11 -7 -5 189.84 6.60 11 7 -5 179.45 6.33 11 -7 -5 175.79 6.69 11 7 -4 29.43 3.44 -11 -7 4 31.52 3.67 -11 -7 4 31.81 4.76 11 -7 -4 35.02 3.63 -11 7 4 42.52 3.84 11 -7 -4 34.80 2.60 -11 -7 4 25.36 4.15 11 -7 -4 34.42 3.03 -11 -7 4 22.44 4.04 11 7 -4 37.10 2.80 11 -7 -4 35.08 3.12 11 7 -3 154.06 6.92 -11 -7 3 135.08 6.33 -11 -7 3 133.96 6.76 11 -7 -3 114.67 6.39 -11 -7 3 109.59 7.09 -11 7 3 172.53 7.09 11 -7 -3 171.99 5.83 11 -7 -3 162.10 5.96 -11 -7 3 110.55 7.03 11 7 -3 148.74 5.68 11 7 -3 155.55 6.54 11 -7 -3 166.13 6.46 11 -7 -3 158.02 6.03 11 7 -2 42.51 3.72 -11 -7 2 38.31 3.81 -11 -7 2 30.74 4.24 11 -7 -2 26.57 3.09 -11 7 2 48.03 3.84 11 7 -2 39.25 3.04 11 -7 -2 47.50 2.94 -11 -7 2 34.46 4.22 11 7 -2 39.72 2.94 11 7 -2 40.53 3.40 11 -7 -2 48.60 3.69 11 -7 -2 39.82 3.05 11 7 -1 3.13 2.51 -11 -7 1 3.49 3.10 -11 7 1 -1.26 2.31 11 7 -1 3.36 2.19 11 -7 -1 2.10 1.93 -11 -7 1 3.45 3.20 11 7 -1 -0.34 1.99 11 -7 -1 3.48 2.54 11 -7 -1 1.26 2.15 11 7 0 14.56 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1.25 2.20 12 4 11 183.47 7.00 12 4 11 195.51 6.83 12 -4 11 200.14 6.98 12 4 12 109.25 4.85 -12 -4 -12 126.09 5.09 12 -4 12 114.89 4.87 12 -4 12 112.95 4.66 -12 -4 -13 230.05 7.25 -12 -4 -13 209.16 6.92 12 -4 13 209.82 6.95 -12 -4 -14 111.35 4.12 -12 -4 -14 112.71 4.31 12 -4 14 112.36 4.21 12 4 15 65.64 3.11 12 4 15 66.38 3.15 -12 -4 -15 80.84 3.00 -12 -4 -15 82.63 3.18 12 4 16 1.78 1.06 12 4 16 1.06 1.09 -12 -4 -16 1.13 0.94 12 4 16 0.12 1.12 -12 -4 -16 1.31 1.01 -12 6 20 6.72 1.17 -12 6 20 8.11 1.18 12 -6 -20 7.43 1.26 -12 6 19 2.24 1.42 12 -6 -19 2.51 1.56 -12 6 19 -0.09 1.41 12 6 -19 1.04 1.53 -12 -6 18 31.78 4.48 -12 6 18 28.20 2.15 12 -6 -18 28.00 2.40 -12 6 18 20.24 2.15 12 -6 -18 23.26 2.16 12 6 -18 21.53 2.29 12 -6 -17 7.65 2.36 12 -6 -17 8.03 2.11 -12 6 17 9.07 2.13 12 6 -17 6.41 2.25 -12 -6 16 45.10 4.62 12 6 -16 35.68 3.03 -12 -6 16 47.29 5.78 12 -6 -16 39.69 3.31 12 -6 -16 42.06 3.09 -12 6 16 40.73 2.95 12 6 -16 37.99 3.08 12 6 -15 10.03 2.74 -12 -6 15 12.83 4.63 -12 -6 15 15.82 5.78 12 -6 -15 12.78 3.05 -12 6 15 14.92 2.61 12 -6 -15 13.60 2.66 12 6 -15 11.76 2.66 12 6 -14 5.44 2.65 -12 -6 14 4.90 4.78 -12 -6 14 6.63 5.75 12 -6 -14 2.70 3.02 -12 6 14 2.85 2.43 12 -6 -14 5.09 2.64 12 6 -14 5.09 2.48 12 6 -13 3.40 2.66 -12 -6 13 1.47 4.82 -12 -6 13 6.09 5.80 12 -6 -13 1.13 3.18 12 -6 -13 0.58 2.43 -12 6 13 1.22 2.39 12 6 -13 4.71 2.48 12 6 -12 5.28 2.65 -12 -6 12 1.92 4.89 -12 -6 12 -0.51 5.78 12 -6 -12 0.65 3.22 12 -6 -12 1.43 2.33 12 6 -12 6.38 2.36 -12 -6 11 26.59 5.16 12 -6 -11 22.95 3.39 12 6 -11 18.20 3.01 12 -6 -11 23.82 3.04 12 -6 -11 20.10 3.67 -12 -6 11 26.93 5.93 12 -6 -11 24.33 2.68 12 6 -11 26.91 2.70 12 -6 -10 37.19 4.04 -12 -6 10 38.91 5.89 12 -6 -10 43.81 3.24 -12 -6 10 42.28 5.27 12 -6 -10 40.09 3.85 12 6 -10 34.92 3.21 12 -6 -10 38.48 3.28 12 6 -10 45.87 3.03 12 -6 -10 45.64 2.79 -12 -6 9 20.98 4.85 12 -6 -9 21.35 3.41 12 -6 -9 21.51 2.87 12 6 -9 15.65 2.73 12 -6 -9 19.12 3.57 -12 -6 9 17.80 5.51 12 -6 -9 25.72 2.83 12 6 -9 18.66 2.81 12 -6 -9 20.31 2.23 12 6 -8 22.44 3.50 12 -6 -8 32.37 3.68 -12 -6 8 33.55 4.89 12 -6 -8 30.88 3.70 12 6 -8 29.97 2.81 12 -6 -8 30.81 2.97 12 -6 -8 33.13 2.93 -12 -6 8 19.35 4.03 -12 6 8 31.53 3.91 12 6 -8 30.04 2.96 12 -6 -8 34.05 2.49 12 6 -7 18.44 3.32 -12 -6 7 22.53 4.55 12 -6 -7 22.02 3.42 12 6 -7 23.82 2.59 12 -6 -7 24.87 2.67 12 -6 -7 17.82 2.62 12 -6 -7 20.97 3.32 -12 -6 7 20.77 3.98 12 -6 -7 28.51 2.73 -12 6 7 22.41 3.61 12 6 -7 24.75 2.72 12 6 -7 23.09 2.99 12 -6 -7 16.22 2.82 12 -6 -7 23.73 2.10 12 6 -6 122.65 6.52 -12 -6 6 127.18 6.55 12 -6 -6 129.01 6.08 12 -6 -6 125.11 5.06 12 -6 -6 124.99 6.27 12 -6 -6 121.70 5.66 12 -6 -6 146.39 5.10 -12 -6 6 109.28 6.78 -12 6 6 132.22 6.56 12 -6 -6 134.02 5.25 12 6 -6 136.39 5.39 12 6 -6 131.94 5.89 12 -6 -6 112.90 5.40 12 -6 -6 138.67 4.96 12 6 -5 42.21 4.01 12 6 -5 54.74 4.09 -12 -6 5 46.32 4.68 12 -6 -5 43.95 4.05 12 -6 -5 48.96 3.69 12 -6 -5 53.89 3.74 -12 -6 5 32.40 4.12 -12 6 5 56.41 4.08 12 -6 -5 58.74 3.04 -12 -6 5 35.80 4.35 -12 6 5 54.02 4.37 12 -6 -5 48.79 3.14 12 6 -5 54.02 3.31 12 6 -5 48.79 3.53 12 -6 -5 45.89 3.35 12 -6 -5 59.87 2.85 12 -6 -4 512.72 14.72 12 -6 -4 435.50 14.34 -12 -6 4 376.56 15.65 12 -6 -4 461.40 15.58 12 -6 -4 486.73 14.54 -12 6 4 511.00 15.68 12 -6 -4 541.72 14.28 -12 -6 4 390.28 15.82 12 -6 -4 462.60 14.17 12 6 -4 415.36 14.85 12 6 -4 494.51 14.35 12 6 -4 483.56 15.03 12 6 -4 505.52 15.75 12 -6 -3 96.85 4.42 12 -6 -3 101.33 4.74 12 -6 -3 96.42 5.04 12 -6 -3 104.19 4.72 -12 6 3 107.73 5.36 -12 -6 3 79.30 5.64 12 6 -3 105.83 4.66 12 -6 -3 106.60 4.34 -12 -6 3 72.73 5.54 12 6 -3 82.43 4.70 12 6 -3 110.80 4.49 12 6 -3 99.46 4.91 12 6 -3 106.84 5.47 12 -6 -2 3.95 2.33 12 -6 -2 7.19 2.04 12 -6 -2 5.31 1.94 -12 6 2 6.46 2.46 12 -6 -2 4.72 1.86 12 6 -2 8.06 2.28 -12 -6 2 4.54 2.94 -12 -6 2 6.63 3.22 12 6 -2 3.61 2.16 12 6 -2 2.41 2.07 12 6 -2 8.00 2.04 12 6 -2 4.96 2.53 12 6 -1 4.03 2.40 -12 -6 1 5.04 2.79 12 -6 -1 5.09 1.79 -12 6 1 6.13 2.43 12 -6 -1 5.70 1.98 12 6 -1 2.54 2.04 -12 -6 1 4.57 2.83 -12 -6 1 3.76 3.10 12 6 -1 2.53 2.13 12 6 -1 0.94 1.94 12 6 -1 2.13 1.91 12 -6 -1 4.13 2.03 12 -6 -1 8.02 1.83 12 -6 -1 2.72 2.33 12 6 0 255.88 9.75 -12 -6 0 227.07 8.92 12 -6 0 263.78 9.70 -12 6 0 316.94 10.11 -12 -6 0 223.61 10.11 -12 -6 0 228.05 10.08 12 -6 0 288.20 8.74 12 -6 0 273.95 9.30 12 6 0 244.07 9.33 12 6 0 259.56 9.36 12 6 0 271.32 8.93 12 -6 0 300.39 8.78 12 6 1 4.38 2.46 -12 -6 -1 3.66 2.76 12 -6 1 5.16 1.97 12 6 1 4.54 2.15 -12 -6 -1 5.16 2.79 -12 -6 -1 2.64 2.83 12 -6 1 3.20 2.34 12 6 1 5.30 2.18 12 6 1 1.94 2.25 12 6 1 2.30 1.99 12 6 2 425.74 13.71 12 6 2 408.91 13.90 12 6 2 441.34 13.93 -12 -6 -2 387.75 13.19 -12 -6 -2 383.24 14.62 12 -6 2 497.60 15.35 12 6 2 408.06 14.13 12 -6 2 468.92 13.21 12 6 2 440.47 13.27 12 6 2 415.18 13.01 12 -6 2 441.70 13.60 12 -6 3 123.42 5.49 -12 -6 -3 110.77 6.37 12 -6 3 125.76 5.27 12 6 3 121.92 5.98 12 -6 3 133.25 5.16 12 6 3 122.85 5.25 12 6 3 130.91 5.20 12 6 4 148.29 6.03 12 -6 4 139.22 5.59 -12 -6 -4 134.05 5.47 12 6 4 134.59 5.48 12 6 4 133.38 5.42 12 -6 4 134.60 5.71 12 -6 5 68.02 4.10 -12 -6 -5 75.08 3.88 12 6 5 74.74 3.80 -12 -6 -5 63.08 4.08 12 6 5 71.40 3.80 12 6 5 79.75 4.37 12 -6 6 14.15 2.93 -12 -6 -6 17.96 2.54 12 6 6 14.96 2.34 12 6 6 15.94 2.51 -12 -6 -6 13.21 2.81 12 6 6 16.37 2.81 12 6 7 2.94 2.29 -12 -6 -7 1.56 2.43 -12 -6 -7 3.51 2.27 12 -6 7 0.87 2.71 12 6 7 2.95 2.53 12 -6 8 48.67 3.68 -12 -6 -8 51.56 3.56 12 6 8 52.87 3.42 12 6 8 53.22 3.83 -12 -6 -8 58.74 3.52 12 -6 9 25.42 3.12 12 6 9 25.29 2.72 12 6 9 23.71 2.94 -12 -6 -9 31.27 2.86 12 -6 10 58.36 3.72 12 6 10 53.89 3.31 12 6 10 55.40 3.59 -12 -6 -10 65.69 3.46 -12 -6 -10 58.53 3.33 -12 -6 -11 16.10 2.22 12 -6 11 16.12 2.59 -12 -6 -11 16.41 2.25 12 6 11 12.97 2.17 12 -6 12 29.95 2.55 -12 -6 -12 30.28 2.30 -12 -6 -12 28.14 2.26 12 6 12 22.28 2.15 12 6 12 24.23 2.29 -12 -6 -13 0.02 1.48 12 -6 13 -1.67 1.89 12 6 13 0.63 1.42 12 6 13 0.45 1.51 -12 -6 -13 -0.57 1.43 12 6 14 1.78 1.23 -12 -6 -14 3.46 1.17 12 6 14 1.60 1.11 12 6 14 1.42 1.14 -12 -6 -14 1.53 1.12 -12 8 17 14.44 1.24 -12 8 17 15.36 1.29 12 -8 -17 12.30 1.42 -12 -8 17 14.96 2.60 12 8 -17 12.39 1.46 12 8 -16 4.25 1.53 -12 -8 16 5.05 3.08 -12 8 16 5.79 1.38 -12 8 16 4.11 1.33 12 -8 -16 4.15 1.63 12 -8 -16 5.60 1.55 12 8 -16 3.86 1.46 12 -8 -16 4.60 1.17 12 8 -15 1.71 1.78 -12 -8 15 2.99 3.56 -12 8 15 3.23 1.50 -12 8 15 1.09 1.64 12 -8 -15 1.80 1.96 12 -8 -15 1.78 1.71 12 -8 -15 1.05 1.36 12 8 -15 -0.42 1.66 -12 -8 14 127.19 6.05 12 8 -14 118.79 4.52 -12 8 14 97.95 4.33 12 -8 -14 111.43 4.50 12 8 -14 106.38 4.28 12 -8 -14 107.54 4.25 12 -8 -14 116.90 4.69 12 8 -13 2.32 2.15 -12 -8 13 1.32 4.54 12 -8 -13 2.50 1.87 12 8 -13 1.71 1.86 12 -8 -13 5.24 2.67 -12 -8 12 155.47 7.45 12 8 -12 157.12 5.74 12 8 -12 138.01 5.33 12 -8 -12 143.56 5.60 12 -8 -12 155.90 6.18 -12 -8 11 45.72 5.68 12 8 -11 47.87 3.29 12 -8 -11 44.95 3.89 12 -8 -11 44.88 3.25 12 -8 -10 64.68 3.82 -12 -8 10 63.53 6.14 12 8 -10 59.07 3.63 12 -8 -10 63.02 3.99 12 -8 -10 63.30 3.83 12 -8 -10 71.55 4.62 12 8 -9 69.46 3.95 12 -8 -9 72.31 4.76 -12 -8 9 75.42 6.25 12 8 -9 68.90 3.74 12 -8 -9 71.09 4.17 12 -8 -9 65.65 4.01 -12 -8 9 55.84 5.16 12 -8 -9 73.51 4.12 12 -8 -8 8.51 3.55 12 -8 -8 13.70 2.81 -12 -8 8 5.26 5.12 12 8 -8 8.81 2.40 12 -8 -8 8.11 2.71 -12 -8 8 8.36 3.85 12 -8 -8 8.67 2.77 12 8 -8 5.42 2.51 12 8 -7 49.90 3.49 12 -8 -7 52.27 4.32 -12 -8 7 55.07 5.72 12 8 -7 55.09 3.28 12 -8 -7 58.13 3.74 12 -8 -7 54.80 3.73 -12 -8 7 47.19 4.96 12 -8 -7 61.30 3.83 -12 -8 6 8.63 4.87 12 -8 -6 8.98 2.75 12 -8 -6 6.56 3.36 12 8 -6 8.93 2.36 12 -8 -6 10.51 2.71 -12 -8 6 9.34 3.92 -12 -8 5 150.04 6.55 -12 -8 5 145.97 7.44 12 -8 -5 154.75 6.18 12 8 -5 148.37 5.97 12 -8 -5 171.17 6.46 12 -8 -4 94.93 4.10 -12 -8 4 80.98 4.93 -12 -8 4 75.25 5.88 12 -8 -4 86.87 4.46 12 8 -4 78.43 4.11 12 -8 -4 88.87 4.56 -12 -8 3 92.37 5.32 -12 -8 3 99.99 6.12 12 -8 -3 104.29 4.80 12 8 -3 93.86 4.47 12 -8 -3 99.08 4.86 12 -8 -3 93.75 5.27 12 -8 -2 11.56 2.39 12 8 -2 4.22 2.39 -12 -8 2 7.60 3.45 -12 -8 2 12.08 4.49 12 8 -2 9.48 2.39 12 -8 -2 9.74 2.51 12 -8 -2 9.20 3.05 12 -8 -1 0.40 2.08 12 8 -1 -0.10 2.26 -12 -8 1 -2.12 3.29 -12 -8 1 3.39 4.12 12 -8 -1 0.70 2.31 12 -8 -1 0.48 2.89 12 8 -1 2.90 2.06 12 8 0 37.72 2.80 12 8 0 36.85 3.13 12 -8 0 32.90 3.13 -12 -8 0 36.24 3.85 -12 -8 0 34.47 3.23 12 -8 0 41.20 3.16 12 -8 0 40.07 3.96 12 8 1 3.12 2.20 12 8 1 4.21 1.93 12 8 1 0.76 2.30 -12 -8 -1 0.15 3.03 -12 -8 -1 3.12 2.53 12 -8 1 -0.34 2.99 12 -8 1 1.88 2.28 12 8 2 105.75 4.98 -12 -8 -2 107.77 5.19 12 8 2 107.86 4.93 -12 -8 -2 108.53 5.08 12 -8 2 108.05 5.74 12 -8 2 125.41 5.03 12 8 3 11.97 2.44 -12 -8 -3 9.48 2.47 -12 -8 -3 11.19 2.84 12 8 3 9.61 2.53 -12 -8 -3 11.05 2.74 12 -8 3 6.39 2.84 12 8 4 3.79 2.27 -12 -8 -4 0.95 2.30 12 -8 4 -1.68 2.72 -12 -8 -4 2.26 2.60 12 8 4 1.89 2.24 -12 -8 -4 4.45 2.60 12 -8 4 -0.68 2.55 12 8 5 58.93 3.70 12 -8 5 55.68 4.00 -12 -8 -5 62.88 3.61 12 8 5 54.93 3.42 -12 -8 -5 64.02 3.82 12 -8 5 54.16 3.85 12 -8 6 24.32 3.30 -12 -8 -6 32.89 2.87 12 8 6 31.03 2.71 -12 -8 -6 32.75 3.07 12 8 6 31.70 2.89 12 8 7 1.70 1.91 12 8 7 1.35 2.20 12 8 7 2.14 1.98 -12 -8 -7 2.74 2.23 -12 -8 -7 2.47 2.14 12 -8 7 0.04 2.64 12 -8 8 126.30 5.26 -12 -8 -8 138.34 4.91 12 8 8 104.50 4.49 -12 -8 -8 135.53 4.92 12 8 8 116.67 4.69 12 8 8 111.81 4.93 -12 -8 -9 41.63 2.60 -12 -8 -9 42.47 2.65 12 8 9 33.89 2.44 12 8 9 32.15 2.58 12 -8 9 37.04 3.08 -12 -8 -10 66.51 2.98 -12 -8 -10 65.27 2.94 12 8 10 54.59 2.83 12 8 10 56.00 2.94 12 -8 10 60.21 3.29 12 8 11 36.46 2.09 12 -8 11 38.93 2.52 12 8 11 33.89 2.22 -12 -8 -12 15.76 1.30 -12 10 13 25.72 1.37 -12 -10 13 26.12 2.46 12 10 -13 21.59 1.52 -12 -10 12 158.92 5.65 12 10 -12 141.84 4.86 -12 10 12 171.14 4.83 -12 10 12 139.90 4.71 12 -10 -12 151.95 4.71 -12 10 11 9.55 1.31 12 -10 -11 10.94 1.32 -12 -10 11 11.62 3.11 12 10 -11 10.85 1.58 -12 -10 10 6.52 2.40 12 -10 -10 10.98 1.49 12 10 -10 9.17 1.67 -12 -10 10 9.72 3.33 12 10 -9 21.95 1.98 -12 -10 9 20.41 3.04 12 -10 -9 25.07 1.96 12 -10 -8 12.64 2.16 12 10 -8 8.96 1.76 -12 -10 8 15.34 3.82 -12 -10 8 8.25 2.85 12 -10 -8 11.88 1.79 12 10 -8 8.48 1.88 12 10 -7 30.10 2.46 12 -10 -7 36.84 2.72 12 10 -7 28.19 2.22 -12 -10 7 35.99 4.20 -12 -10 7 27.73 3.51 12 -10 -7 38.74 2.53 12 -10 -6 7.07 2.25 -12 -10 6 5.43 2.97 12 -10 -6 4.63 1.89 12 10 -6 3.21 1.96 12 -10 -5 5.72 2.31 -12 -10 5 6.04 2.91 12 -10 -5 4.02 1.96 12 10 -5 1.89 1.94 12 -10 -4 38.24 2.95 12 -10 -4 34.61 2.74 -12 -10 4 33.17 3.47 12 10 -4 28.68 2.51 12 -10 -3 4.98 2.21 -12 -10 3 1.30 2.49 -12 -10 3 3.45 2.59 12 -10 -3 0.88 2.04 12 -10 -3 2.56 2.29 12 10 -3 1.61 1.93 12 10 -2 13.10 2.13 12 -10 -2 18.66 2.42 -12 -10 2 19.33 2.79 12 -10 -2 14.79 2.41 12 -10 -2 19.94 2.77 -12 -10 2 22.38 2.88 -12 -10 1 3.41 2.59 12 10 -1 5.02 1.85 12 -10 -1 2.71 2.46 12 10 0 21.09 2.34 -12 -10 0 28.48 2.99 12 10 0 23.45 2.20 12 -10 0 28.09 3.14 12 10 1 9.20 1.98 -12 -10 -1 14.65 2.56 12 10 1 9.88 1.78 12 -10 1 11.16 2.67 12 10 2 25.13 2.41 12 -10 2 32.35 3.14 12 10 3 2.13 1.83 -12 -10 -3 4.40 2.11 12 -10 3 2.66 2.36 12 10 3 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29.18 3.17 15 -5 -12 32.65 2.78 15 5 -12 31.10 3.08 15 -5 -12 30.65 2.23 -15 -5 12 32.76 6.07 15 5 -11 100.97 5.36 15 -5 -11 147.09 6.48 15 5 -11 120.28 5.43 15 -5 -11 119.77 5.04 -15 -5 11 133.50 7.54 15 -5 -11 139.12 4.88 15 5 -11 133.87 5.44 -15 -5 10 60.88 6.30 15 -5 -10 60.86 4.62 15 5 -10 64.26 3.79 15 -5 -10 64.39 3.10 15 5 -10 49.64 3.75 -15 -5 9 129.90 6.61 15 -5 -9 145.38 6.57 15 5 -9 128.73 5.42 15 -5 -9 135.17 5.69 15 -5 -9 136.17 4.97 15 5 -8 124.59 7.28 -15 -5 8 172.30 7.36 15 -5 -8 169.07 7.40 -15 -5 8 138.62 7.74 -15 5 8 167.17 7.48 15 -5 -8 179.09 6.21 15 5 -8 150.40 6.62 15 -5 -8 199.72 6.95 15 -5 -8 174.65 5.93 -15 -5 7 2.02 4.13 15 -5 -7 3.94 3.29 15 -5 -7 1.41 1.91 -15 -5 7 1.78 3.15 15 -5 -7 4.58 2.08 -15 5 7 1.51 2.72 15 5 -7 -1.90 2.59 15 -5 -7 1.18 1.53 15 -5 -7 4.80 2.66 -15 -5 6 209.30 8.28 15 -5 -6 199.82 8.22 15 -5 -6 187.27 8.12 15 -5 -6 232.15 7.59 15 5 -6 215.87 7.98 -15 -5 6 178.94 8.94 -15 5 6 207.27 8.49 15 5 -6 208.91 7.86 15 5 -6 190.45 7.77 15 -5 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3.39 20 2 -8 49.16 3.20 20 -2 -8 60.57 3.13 20 2 -8 53.65 3.24 20 -2 -8 58.56 3.62 20 2 -8 48.80 3.24 20 2 -8 56.37 3.92 20 2 -7 35.52 3.21 20 -2 -7 43.53 2.89 20 2 -7 37.72 3.60 20 -2 -7 37.61 3.57 20 -2 -7 41.08 2.89 20 -2 -7 41.12 3.58 20 2 -7 39.03 2.87 20 -2 -7 38.32 3.26 20 2 -7 39.23 3.13 20 2 -7 35.03 2.72 20 -2 -7 39.84 3.07 20 -2 -7 43.40 2.79 20 -2 -7 42.28 3.27 20 2 -7 37.23 2.97 20 2 -7 40.96 2.95 20 2 -7 37.68 2.90 20 2 -7 41.02 3.54 20 -2 -6 160.00 6.88 20 2 -6 170.40 6.57 20 2 -6 161.52 6.15 20 -2 -6 172.78 6.52 20 -2 -6 188.34 6.35 20 2 -6 201.32 6.60 20 -2 -6 196.29 6.60 20 -2 -6 182.62 6.77 20 2 -6 161.76 6.33 20 2 -6 180.60 6.52 20 2 -6 177.66 6.38 20 -2 -6 176.04 7.12 20 2 -6 166.24 6.87 20 -2 -6 182.17 6.46 20 2 -6 187.55 7.62 20 -2 -6 166.96 6.99 20 -2 -6 164.65 6.48 20 -2 -6 189.71 6.56 20 2 -6 178.56 6.31 20 -2 -5 89.80 4.79 20 2 -5 100.80 4.73 20 2 -5 96.59 4.34 20 -2 -5 103.26 4.70 20 2 -5 124.47 4.77 20 -2 -5 116.20 4.65 20 -2 -5 112.65 4.92 20 2 -5 100.73 4.60 20 2 -5 114.22 4.75 20 2 -5 113.46 4.61 20 -2 -5 114.37 5.44 20 2 -5 100.56 5.05 20 2 -5 107.50 5.75 20 -2 -5 99.23 5.00 20 -2 -5 100.63 4.62 20 -2 -5 107.15 4.63 20 2 -5 104.60 4.49 20 2 -4 15.79 2.66 20 2 -4 13.96 2.16 20 -2 -4 15.11 2.40 20 2 -4 17.55 2.43 20 -2 -4 17.57 2.43 20 2 -4 18.59 2.54 20 -2 -4 19.60 2.71 20 2 -4 18.01 2.47 20 2 -4 18.88 2.54 20 2 -4 14.93 2.35 20 -2 -4 17.85 3.20 20 -2 -4 18.26 2.43 20 -2 -4 16.58 2.22 20 2 -4 15.59 3.16 20 2 -4 15.50 2.92 20 2 -3 9.12 2.76 20 -2 -3 12.93 3.10 20 -2 -3 11.93 2.18 20 2 -3 8.94 2.87 20 2 -3 8.45 2.16 20 2 -3 10.98 2.55 20 2 -3 10.28 2.05 20 -2 -3 9.59 2.18 20 2 -3 9.38 2.33 20 -2 -3 9.42 2.19 20 2 -3 11.92 2.51 20 2 -3 10.24 2.40 20 -2 -3 11.22 2.27 20 2 -2 56.32 4.18 20 2 -2 67.77 4.66 20 -2 -2 72.54 3.94 20 -2 -2 67.74 4.37 20 2 -2 65.89 3.58 20 2 -2 54.08 4.07 20 2 -2 70.90 3.94 20 2 -2 67.40 3.33 20 -2 -2 55.84 3.39 20 2 -2 77.10 3.76 20 -2 -2 59.30 3.56 20 2 -2 77.88 4.00 20 2 -2 78.89 3.78 20 -2 -2 71.95 3.97 20 2 -1 -0.86 2.55 20 -2 -1 5.59 2.85 20 -2 -1 4.90 2.21 20 2 -1 -0.18 2.35 20 2 -1 0.44 2.14 20 2 -1 2.32 2.36 20 2 -1 3.85 1.81 20 -2 -1 1.77 1.93 20 2 -1 3.35 2.19 20 2 -1 2.47 2.12 20 -2 -1 -0.14 2.16 20 2 -1 1.66 2.33 20 2 -1 2.71 2.55 20 -2 -1 2.66 2.26 20 -2 0 59.37 4.03 20 2 0 43.05 3.99 20 -2 0 57.95 3.69 20 2 0 62.31 3.32 20 2 0 39.23 3.60 20 2 0 60.85 3.68 20 2 0 65.95 3.10 20 -2 0 49.17 3.07 20 2 0 62.02 3.51 20 2 0 70.59 3.80 20 -2 0 43.29 3.26 20 2 0 63.28 4.31 20 -2 0 58.26 3.87 20 -2 1 248.06 8.80 20 2 1 179.90 9.07 20 -2 1 244.19 8.86 20 2 1 273.53 8.20 20 2 1 253.74 8.59 20 2 1 277.06 8.00 20 -2 1 210.27 7.96 20 2 1 280.81 8.40 20 2 1 287.41 8.77 20 -2 1 194.61 8.14 20 2 1 239.38 9.44 20 -2 1 246.72 9.09 20 -2 2 100.72 4.90 20 2 2 105.37 4.39 20 2 2 111.20 4.15 20 -2 2 98.19 4.28 20 2 2 101.07 4.73 20 2 2 101.82 4.80 20 -2 2 87.51 4.49 20 2 2 111.63 4.52 20 2 2 91.44 5.38 20 -2 2 104.96 5.22 20 2 3 122.38 7.25 20 -2 3 185.95 7.23 20 2 3 198.88 6.60 20 -2 3 180.37 6.70 20 2 3 215.95 6.40 20 -2 3 175.26 6.43 20 2 3 197.95 7.01 20 2 3 205.43 6.75 20 2 3 205.72 7.12 20 -2 3 168.68 6.80 20 2 3 157.98 7.57 20 -2 3 196.90 7.62 20 2 4 27.25 3.52 20 2 4 51.15 3.10 20 -2 4 54.67 3.55 20 2 4 61.86 2.89 20 -2 4 53.60 3.01 20 2 4 51.42 3.46 20 2 4 50.34 3.38 20 -2 4 53.92 3.41 20 2 4 55.20 3.55 20 2 4 53.75 3.17 20 2 4 35.20 3.80 20 -2 4 57.58 3.92 20 2 5 57.90 4.34 20 2 5 90.33 3.94 20 -2 5 85.57 4.28 20 2 5 102.59 3.73 20 -2 5 90.62 3.83 20 2 5 87.52 4.32 20 2 5 91.61 4.22 20 -2 5 89.59 4.24 20 2 5 91.46 4.37 20 2 5 96.87 4.04 20 2 5 56.88 4.51 20 -2 5 84.03 4.62 20 -2 6 1.93 2.40 20 2 6 1.50 2.14 20 2 6 1.31 1.83 20 2 6 0.23 2.08 20 2 6 1.12 2.03 20 2 6 3.35 1.88 20 -2 6 1.52 2.00 20 2 6 -0.04 2.20 20 2 6 -2.70 2.56 20 -2 6 2.31 2.16 20 -2 7 135.57 5.11 20 2 7 136.21 4.79 20 2 7 130.20 5.18 20 2 7 140.07 5.02 20 2 7 141.28 5.14 20 2 7 139.35 4.87 20 -2 7 142.36 5.19 20 -2 8 10.11 2.13 20 2 8 7.59 1.92 20 2 8 7.96 1.65 20 2 8 8.14 1.63 20 -2 8 9.25 1.84 20 2 8 5.86 1.85 20 2 8 6.91 1.89 20 2 9 28.92 2.08 20 2 9 26.14 1.84 20 -2 9 27.95 2.05 20 2 9 28.72 2.19 20 2 9 29.52 1.83 20 2 10 5.25 1.11 20 -2 10 3.97 1.20 20 2 10 3.89 1.19 20 2 10 4.97 1.42 20 2 10 5.33 1.12 20 2 11 10.25 1.14 20 2 11 9.94 0.92 20 -4 -19 25.64 1.59 -20 4 19 29.09 1.54 20 4 -18 4.41 1.28 20 4 -18 4.91 1.42 20 -4 -18 7.50 1.64 -20 4 18 8.11 1.40 20 4 -18 6.81 1.47 -20 -4 17 38.49 3.45 20 -4 -17 42.52 2.60 20 4 -17 38.78 2.36 20 4 -17 32.81 1.97 -20 4 17 33.46 2.17 20 4 -17 37.19 2.37 -20 -4 16 4.53 3.40 20 4 -16 5.77 1.97 20 -4 -16 5.78 2.14 20 4 -16 2.10 1.57 20 4 -16 4.62 1.89 -20 -4 15 19.58 3.96 20 -4 -15 26.66 2.75 20 4 -15 23.34 2.47 20 4 -15 19.65 2.39 20 4 -15 17.59 2.10 20 -4 -14 33.65 3.13 20 4 -14 33.93 2.85 20 4 -14 28.35 2.49 20 4 -14 29.74 2.74 20 -4 -14 35.93 2.72 20 -4 -14 37.79 2.10 -20 -4 13 102.09 6.20 20 -4 -13 89.50 4.67 20 4 -13 95.25 4.28 20 4 -13 83.74 4.05 20 4 -13 87.34 4.24 20 -4 -13 97.96 4.40 20 -4 -13 95.61 3.71 20 4 -12 3.62 2.50 20 -4 -12 7.74 1.86 -20 -4 12 8.38 5.16 20 4 -12 12.18 2.39 20 -4 -12 9.04 2.88 20 4 -12 6.29 2.29 20 -4 -12 7.36 1.63 20 -4 -12 11.70 2.64 20 4 -11 152.58 6.98 20 -4 -11 185.08 6.63 -20 -4 11 210.23 8.44 20 -4 -11 171.39 7.21 20 4 -11 195.98 6.73 20 -4 -11 203.04 7.33 20 -4 -11 198.79 6.40 20 4 -10 2.93 2.58 20 -4 -10 8.23 2.21 -20 -4 10 11.11 5.38 20 -4 -10 7.15 2.87 20 4 -10 6.64 2.49 20 -4 -10 7.26 1.78 20 -4 -10 11.22 2.96 20 4 -9 99.14 5.25 20 -4 -9 119.46 4.98 20 -4 -9 109.43 5.32 20 4 -9 127.41 4.97 20 4 -9 84.16 5.06 20 -4 -9 139.50 5.84 20 -4 -9 118.12 4.56 20 4 -8 68.44 4.36 20 -4 -8 87.52 4.26 20 -4 -8 74.33 4.42 20 4 -8 93.05 4.22 20 4 -8 82.72 4.17 20 4 -8 63.37 4.36 20 -4 -8 104.19 5.09 20 -4 -8 81.64 3.65 20 -4 -7 88.85 4.64 20 4 -7 87.56 4.47 20 4 -7 62.34 4.59 20 -4 -7 84.99 3.79 20 -4 -7 101.42 4.14 20 4 -7 94.53 4.29 20 4 -7 69.62 4.49 20 -4 -7 91.37 4.46 20 4 -7 100.11 4.32 20 4 -6 158.92 6.63 20 -4 -6 159.03 6.72 20 -4 -6 166.77 6.09 20 -4 -6 195.28 6.44 20 4 -6 187.14 6.50 20 4 -6 145.23 6.67 20 -4 -6 177.95 6.67 20 4 -6 161.66 7.14 20 4 -6 186.95 6.45 20 4 -5 34.76 3.22 20 -4 -5 29.49 3.33 20 -4 -5 35.57 2.74 20 4 -5 32.85 2.63 20 4 -5 28.93 3.13 20 -4 -5 36.57 3.05 20 4 -5 32.19 3.61 20 4 -5 34.17 2.95 20 4 -4 195.96 6.69 20 -4 -4 162.38 6.90 20 -4 -4 183.03 6.51 20 4 -4 171.28 6.15 20 4 -4 163.08 6.90 20 -4 -4 174.47 6.59 20 4 -4 163.20 7.28 20 4 -4 189.67 6.62 20 4 -3 65.82 3.60 20 -4 -3 58.73 4.01 20 -4 -3 63.67 3.50 20 4 -3 52.99 3.96 20 4 -3 60.17 3.28 20 -4 -3 60.18 3.44 20 4 -3 63.97 4.40 20 4 -3 66.95 3.71 20 4 -2 30.20 2.65 20 4 -2 33.71 2.96 20 -4 -2 30.36 3.43 20 -4 -2 31.37 2.63 20 4 -2 28.56 3.32 20 4 -2 29.22 2.54 20 4 -2 29.44 3.47 20 4 -2 31.68 2.98 20 4 -1 196.23 6.90 20 -4 -1 186.78 7.37 20 -4 -1 200.53 7.11 20 4 -1 184.81 7.34 20 4 -1 198.42 6.66 20 4 -1 187.98 7.67 20 4 -1 197.55 7.10 20 -4 0 45.21 3.53 20 4 0 38.11 3.57 20 -4 0 44.98 3.04 20 4 0 42.43 3.48 20 4 0 41.42 2.77 20 4 0 40.64 3.00 20 4 0 43.28 3.59 20 4 0 39.84 3.59 20 4 0 43.31 3.19 20 -4 1 36.26 3.22 20 4 1 37.62 3.18 20 4 1 32.45 3.48 20 -4 1 36.74 2.81 20 4 1 36.81 2.64 20 4 1 34.87 2.91 20 4 1 38.82 3.56 20 4 1 36.48 3.00 20 4 2 58.05 4.34 20 4 2 67.72 3.93 20 4 2 71.21 3.35 20 4 2 69.05 3.65 20 4 2 69.18 4.35 20 4 2 72.03 3.78 20 4 3 -0.06 2.63 20 4 3 2.55 2.14 20 4 3 1.06 1.82 20 4 3 1.89 2.11 20 4 3 0.08 2.11 20 4 3 2.32 2.44 20 -4 4 67.66 3.58 20 4 4 66.54 4.26 20 4 4 58.92 3.53 20 4 4 72.52 3.21 20 4 4 66.22 3.54 20 4 4 69.01 3.55 20 4 4 71.72 4.19 20 -4 5 55.23 3.20 20 4 5 46.41 3.48 20 4 5 54.49 2.69 20 4 5 52.74 3.01 20 4 5 48.78 3.01 20 4 5 51.28 3.61 20 -4 6 33.93 2.59 20 4 6 26.72 2.74 20 4 6 30.40 2.06 20 4 6 31.05 2.40 20 4 6 29.67 2.39 20 4 6 30.20 2.79 20 -4 7 37.45 2.50 20 4 7 34.33 2.54 20 4 7 30.24 2.22 20 4 7 33.75 2.29 20 4 7 31.45 2.51 20 4 8 35.61 2.28 20 4 8 41.40 2.20 20 4 8 38.72 2.20 20 4 8 35.80 2.37 20 4 9 0.61 1.07 20 4 9 0.36 1.07 -20 -4 -9 1.22 1.11 20 4 9 -0.52 1.06 20 4 9 0.09 1.02 20 6 -16 55.16 2.29 20 6 -16 45.06 2.12 -20 -6 15 42.78 3.91 20 6 -15 30.62 2.01 -20 -6 14 124.94 5.68 20 6 -14 109.13 4.10 -20 -6 13 2.72 4.30 20 6 -13 3.44 1.68 20 6 -12 311.85 10.01 -20 -6 12 332.12 10.94 20 6 -11 50.53 3.24 20 -6 -11 47.09 2.60 -20 -6 11 47.04 5.39 20 6 -10 354.46 11.70 -20 -6 10 338.01 12.46 20 -6 -10 381.66 11.34 20 -6 -10 403.72 11.30 20 6 -9 26.49 2.86 20 -6 -9 25.02 2.28 -20 -6 9 20.87 5.30 20 -6 -9 29.27 2.08 20 6 -8 4.98 2.34 20 -6 -8 2.82 1.91 20 -6 -8 7.07 1.59 20 6 -8 3.37 2.23 20 -6 -7 44.83 2.97 -20 -6 7 32.86 4.33 20 6 -7 35.20 3.09 20 -6 -7 41.37 2.45 20 -6 -6 13.48 2.30 20 6 -6 8.13 2.60 -20 -6 6 12.95 4.07 20 6 -6 14.30 2.49 20 -6 -6 14.82 2.75 20 -6 -5 33.93 2.81 20 6 -5 27.86 3.19 -20 -6 5 30.30 4.04 -20 -6 5 32.37 4.32 20 6 -5 29.33 2.81 20 -6 -5 32.43 3.23 20 6 -5 27.71 2.67 20 -6 -4 56.92 3.33 20 6 -4 46.47 3.61 -20 -6 4 50.83 4.31 -20 -6 4 43.05 4.56 20 -6 -4 53.51 3.74 20 6 -4 42.34 3.10 20 -6 -3 2.29 2.15 20 6 -3 1.83 2.54 -20 -6 3 6.21 3.37 -20 -6 3 3.24 3.88 20 -6 -3 3.66 2.79 20 6 -3 2.40 2.17 20 -6 -2 66.70 3.32 20 6 -2 54.70 3.77 -20 -6 2 47.15 4.05 20 -6 -2 61.02 3.88 20 6 -2 47.37 3.32 20 -6 -1 3.09 1.95 20 6 -1 0.15 2.30 -20 -6 1 3.40 2.83 20 -6 -1 3.83 2.60 20 6 -1 1.21 2.12 20 -6 0 157.91 5.93 20 6 0 144.53 5.73 20 6 1 2.78 2.09 20 -6 1 3.42 2.34 20 6 1 0.56 1.92 20 6 1 -1.73 2.06 20 6 1 0.83 1.73 20 6 2 2.99 1.98 20 6 2 1.76 1.95 20 -6 2 3.42 2.18 -20 -6 -2 3.32 2.19 20 6 2 2.26 1.97 20 6 2 3.52 1.95 20 6 2 0.25 1.78 20 6 3 1.95 1.75 20 6 3 3.80 1.89 -20 -6 -3 4.32 1.97 20 6 3 1.33 1.68 20 6 3 5.52 1.94 20 6 4 2.67 1.57 20 6 4 2.32 1.79 20 6 4 3.75 1.63 20 6 4 1.32 1.71 20 6 5 -0.41 1.40 20 6 5 0.38 1.50 20 6 5 0.98 1.49 20 6 5 1.57 1.35 20 6 6 5.21 1.28 20 6 6 5.38 1.40 20 6 6 5.03 1.21 20 6 6 5.00 1.42 20 -6 6 9.63 1.62 20 -6 7 3.53 1.38 20 6 7 2.71 1.04 -20 -6 -7 2.99 1.11 20 6 7 2.22 1.07 20 6 7 2.01 1.01 -20 -8 12 57.65 3.35 -20 -8 11 5.07 2.89 -20 -8 11 2.46 2.35 20 8 -11 1.28 1.24 -20 -8 10 75.28 3.75 20 8 -10 71.68 2.93 -20 -8 9 26.78 3.56 -20 -8 9 23.44 3.05 -20 -8 9 20.66 2.45 20 8 -9 20.42 1.89 -20 -8 8 40.08 3.77 20 -8 -8 36.27 1.91 -20 -8 8 28.89 2.65 -20 -8 8 30.38 3.36 -20 -8 8 23.69 2.67 20 8 -8 27.64 2.11 -20 -8 7 133.66 5.49 20 -8 -7 143.26 4.40 -20 -8 7 124.17 4.91 -20 -8 7 118.36 5.20 -20 -8 7 94.06 4.88 20 8 -7 109.19 4.33 20 -8 -6 4.69 1.46 -20 -8 6 4.55 3.57 -20 -8 6 5.12 2.38 -20 -8 6 5.36 3.08 -20 -8 6 6.42 2.38 20 8 -6 2.72 1.48 20 8 -6 2.84 1.59 20 8 -5 70.55 3.21 -20 -8 5 80.01 4.00 -20 -8 5 82.19 4.36 -20 -8 5 65.75 3.86 20 -8 -5 67.55 3.64 -20 -8 4 6.70 2.52 -20 -8 4 11.05 3.24 -20 -8 4 3.53 1.93 -20 -8 4 8.82 2.29 20 -8 -4 7.26 2.11 20 -8 -4 4.91 1.59 20 8 -4 4.24 1.67 -20 -8 3 35.00 2.90 -20 -8 3 39.22 3.47 -20 -8 3 37.20 2.63 -20 -8 3 32.83 2.73 20 -8 -3 44.25 2.91 20 8 -3 30.99 2.31 -20 -8 2 8.33 2.28 -20 -8 2 12.78 3.02 -20 -8 2 9.19 2.00 20 -8 -2 9.05 2.17 20 8 -2 5.63 1.66 -20 -8 1 28.76 2.42 -20 -8 1 31.10 3.09 -20 -8 1 25.19 2.25 20 -8 -1 30.37 2.54 20 8 -1 20.06 1.70 20 8 -1 20.16 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1.55 1.17 25 5 -2 0.91 1.00 -25 -5 2 3.05 1.40 25 5 -1 12.91 1.24 25 5 -1 11.39 1.26 25 5 0 12.52 1.12 25 5 0 9.44 1.09 26 0 -15 0.73 0.81 26 0 -15 0.57 1.07 26 0 -15 -0.57 0.88 26 0 -14 148.09 4.34 26 0 -14 136.84 4.13 26 0 -13 1.02 1.07 26 0 -13 -0.19 0.89 26 0 -13 0.21 1.30 26 0 -13 -1.11 1.16 26 0 -12 3.18 1.24 26 0 -12 3.15 1.47 26 0 -12 1.92 1.05 26 0 -12 1.28 1.22 26 0 -11 1.44 1.17 26 0 -11 0.48 1.13 26 0 -11 -0.57 1.33 26 0 -10 48.98 2.40 26 0 -10 55.46 2.48 26 0 -9 0.67 1.26 26 0 -9 0.14 1.33 26 0 -8 8.33 1.69 26 0 -8 7.28 1.51 26 0 -8 4.64 1.56 26 0 -8 7.09 1.53 26 0 -7 1.48 1.51 26 0 -7 0.33 1.51 26 0 -7 0.02 1.36 26 0 -7 -0.55 1.30 26 0 -6 75.80 3.26 26 0 -6 83.67 3.18 26 0 -6 79.43 3.37 26 0 -5 0.25 1.51 26 0 -5 2.15 1.40 26 0 -5 0.47 1.18 26 0 -4 65.15 2.91 26 0 -4 73.86 2.84 26 0 -3 1.29 1.47 26 0 -3 0.50 1.36 26 0 -3 -1.68 1.48 26 0 -2 20.60 1.78 26 0 -2 22.33 1.72 26 0 -2 24.06 1.68 26 0 -1 0.67 1.22 26 0 -1 2.21 1.30 26 0 -1 2.28 1.42 26 0 -1 -1.07 1.41 26 0 -1 3.27 1.22 26 0 -1 -0.69 1.35 26 0 0 1.59 1.12 26 0 0 0.79 1.18 26 0 0 2.54 1.33 26 0 0 -0.28 1.35 26 0 0 3.11 1.16 26 0 0 0.77 1.24 26 0 1 1.11 1.04 26 0 1 0.63 0.99 26 0 1 0.19 1.10 26 0 1 -1.23 1.33 26 0 1 0.55 1.21 26 0 2 74.21 3.09 26 0 2 83.14 3.28 26 0 3 0.84 0.79 26 0 3 1.21 0.88 26 -2 -14 13.99 1.14 26 2 -14 16.26 1.24 26 -2 -14 16.45 1.02 26 2 -13 50.31 2.50 26 -2 -13 61.77 2.56 26 -2 -13 79.17 2.54 26 2 -13 80.97 2.69 26 -2 -13 65.24 2.55 26 2 -12 4.94 1.17 26 -2 -12 6.04 1.15 26 -2 -12 7.50 1.07 26 2 -12 5.04 1.04 26 2 -12 8.19 1.34 26 2 -12 4.89 1.05 26 -2 -12 4.30 1.21 26 -2 -11 92.04 3.60 26 2 -11 85.37 3.53 26 -2 -11 114.19 3.62 26 2 -11 122.34 3.76 26 2 -11 94.76 3.40 26 -2 -11 103.45 3.63 26 -2 -10 77.13 3.29 26 2 -10 73.23 3.32 26 -2 -10 100.33 3.38 26 2 -10 96.21 3.52 26 2 -10 98.55 3.38 26 2 -10 82.28 3.11 26 -2 -10 93.41 3.40 26 -2 -9 111.52 4.53 26 2 -9 154.39 4.86 26 2 -9 112.33 4.64 26 -2 -9 148.77 4.66 26 2 -9 153.89 4.69 26 2 -9 133.98 4.44 26 -2 -9 143.43 4.69 26 -2 -8 18.08 1.65 26 2 -8 26.30 2.04 26 2 -8 17.00 1.87 26 -2 -8 22.67 1.66 26 2 -8 22.39 1.59 26 -2 -8 27.95 1.86 26 2 -8 26.72 1.89 26 2 -8 26.67 1.89 26 2 -7 62.67 2.95 26 -2 -7 57.56 2.67 26 2 -7 71.51 2.87 26 2 -7 66.61 2.77 26 2 -7 62.76 2.56 26 -2 -7 64.92 2.78 26 2 -6 0.75 1.51 26 -2 -6 2.41 1.33 26 2 -6 2.10 1.46 26 2 -6 0.89 1.14 26 -2 -6 1.96 1.33 26 2 -6 0.51 1.43 26 2 -5 60.02 2.87 26 2 -5 55.99 2.42 26 -2 -5 59.90 2.63 26 2 -5 62.77 2.75 26 2 -4 42.70 2.57 26 -2 -4 65.46 2.75 26 2 -4 52.51 2.71 26 2 -4 56.87 2.66 26 2 -4 52.49 2.32 26 -2 -4 56.34 2.56 26 2 -3 4.13 1.46 26 -2 -3 4.01 1.39 26 2 -3 2.46 1.15 26 -2 -3 3.59 1.37 26 2 -3 2.93 1.41 26 2 -2 72.96 3.13 26 -2 -2 74.04 3.21 26 2 -2 80.61 3.01 26 2 -2 86.08 3.20 26 2 -2 80.95 2.86 26 -2 -2 72.75 2.98 26 2 -1 18.43 1.66 26 2 -1 17.61 1.59 26 -2 -1 16.29 1.58 26 2 -1 18.72 1.47 26 2 -1 18.85 1.61 26 2 -1 18.12 1.30 26 -2 -1 17.42 1.45 26 2 0 39.74 2.00 26 2 0 33.37 1.93 26 -2 0 32.43 1.92 26 2 0 36.51 1.79 26 2 0 40.62 1.86 26 -2 0 37.19 1.93 26 2 0 36.01 1.92 26 2 0 36.33 1.65 26 -2 0 33.86 1.80 26 -2 1 56.85 2.24 26 2 1 61.22 2.38 26 2 1 52.35 2.44 26 -2 1 49.07 2.35 26 2 1 60.25 2.26 26 2 1 59.23 2.51 26 2 1 63.10 2.29 26 -2 1 61.67 2.38 26 2 1 57.03 2.35 26 2 2 2.10 0.85 26 2 2 0.92 0.85 26 -2 2 0.17 0.78 26 2 2 0.18 0.89 26 2 2 2.01 0.81 26 2 2 0.14 0.99 26 -4 -12 1.53 0.76 26 -4 -12 2.71 0.73 26 4 -11 7.41 1.04 26 -4 -11 5.63 0.98 26 -4 -11 7.46 0.91 26 4 -10 19.12 1.37 26 -4 -10 16.24 1.29 26 -4 -9 37.77 1.88 26 4 -9 39.63 1.87 26 -4 -8 4.49 1.08 26 4 -8 4.50 1.18 26 4 -8 4.71 1.15 26 -4 -7 4.89 1.11 26 4 -7 4.09 1.22 -26 -4 7 6.55 2.10 26 4 -7 2.69 1.19 -26 -4 6 18.53 2.27 26 4 -6 21.95 1.69 26 4 -6 25.69 1.70 26 4 -5 10.22 1.34 26 4 -5 11.42 1.42 26 4 -4 1.08 1.03 26 4 -4 1.09 1.17 26 4 -3 44.54 1.83 26 4 -3 41.39 2.02 26 4 -2 137.55 4.02 26 4 -2 112.62 4.07 26 4 -1 72.33 2.38 26 4 -1 58.49 2.41 27 -1 -13 13.53 0.93 27 1 -13 12.75 1.02 27 -1 -13 11.09 1.02 27 1 -12 12.53 1.03 27 -1 -12 13.65 1.05 27 1 -12 14.44 1.14 27 -1 -12 15.24 1.21 27 1 -12 12.41 1.09 27 -1 -12 10.83 1.09 27 1 -11 25.99 1.54 27 -1 -11 31.48 1.59 27 1 -11 32.64 1.59 27 -1 -11 32.43 1.67 27 -1 -11 23.01 1.52 27 -1 -10 0.24 0.95 27 1 -10 0.19 0.94 27 1 -10 1.28 0.96 27 -1 -10 2.31 1.12 27 -1 -10 0.49 0.94 27 -1 -9 70.13 2.73 27 1 -9 73.24 2.62 27 -1 -9 76.25 2.74 27 -1 -8 29.41 1.70 27 1 -8 28.74 1.87 27 1 -8 29.23 1.63 27 -1 -8 33.46 1.78 27 1 -7 0.03 1.09 27 -1 -7 0.39 0.98 27 1 -7 1.32 1.29 27 1 -7 1.62 1.05 27 -1 -7 1.72 1.17 27 1 -7 0.64 1.25 27 1 -6 35.11 1.94 27 1 -6 31.71 1.67 27 -1 -6 35.54 1.84 27 -1 -5 6.04 1.15 27 1 -5 4.77 1.08 27 1 -5 8.04 1.37 27 1 -5 5.37 1.16 27 -1 -5 7.24 1.29 27 1 -5 5.99 1.31 27 1 -4 31.72 1.67 27 -1 -4 34.49 1.80 27 1 -4 35.96 1.91 27 1 -3 13.61 1.28 27 1 -3 15.36 1.28 27 -1 -3 17.55 1.38 27 1 -3 15.21 1.42 27 1 -2 105.53 3.74 27 1 -2 126.04 3.60 27 -1 -2 113.07 3.65 27 1 -2 125.23 3.79 27 1 -1 26.87 1.57 27 -1 -1 25.63 1.46 27 1 -1 29.54 1.58 27 1 0 45.99 2.01 27 1 0 49.51 1.96 27 1 0 51.48 1.80 27 -1 0 49.14 1.85 27 -3 -11 4.71 0.75 27 -3 -11 1.87 0.77 27 3 -10 74.80 3.06 27 -3 -10 91.76 3.15 27 -3 -9 3.18 0.80 27 3 -9 2.13 0.91 27 -3 -9 2.42 0.86 27 3 -9 3.02 0.99 27 3 -8 59.03 2.28 27 3 -8 44.02 2.12 27 -3 -8 62.62 2.10 27 -3 -8 42.31 1.97 27 3 -7 19.08 1.28 27 3 -7 16.87 1.41 27 3 -6 -0.32 0.92 27 3 -6 0.95 0.99 27 3 -6 1.17 1.07 27 3 -5 85.42 3.02 27 3 -5 90.65 2.88 27 3 -4 45.88 2.04 27 3 -4 49.00 1.91 27 3 -3 31.43 1.66 27 3 -3 34.12 1.58 27 3 -2 29.38 1.46 28 0 -11 0.40 0.62 28 0 -10 38.80 1.55 28 0 -10 29.23 1.47 28 0 -9 1.77 0.83 28 0 -9 -0.80 0.79 28 0 -8 55.34 1.95 28 0 -8 38.48 1.85 28 0 -7 -1.38 0.99 28 0 -7 0.18 0.74 28 0 -6 264.09 7.64 28 0 -5 -0.33 0.92 28 0 -5 1.02 0.98 28 0 -4 627.80 17.26 28 0 -4 623.68 17.34 28 0 -3 0.62 0.79 28 0 -3 2.15 0.81 28 2 -9 50.71 1.94 28 2 -8 1.86 0.78 28 2 -7 38.58 1.68 28 2 -6 13.12 1.05 28 2 -6 11.92 1.10 28 2 -5 17.60 1.18 28 2 -4 81.54 2.73 0 0 0 0.00 0.00 TITL 1clquin_nidimer_auto in C2/c REM C2/c (#15 in standard setting) CELL 1.54184 23.099128 10.332692 18.925076 90.0000 106.3803 90.0000 ZERR 4.00 0.000260 0.000126 0.000263 0.0000 0.0014 0.0000 LATT 7 SYMM -x, y,-z+1/2 SFAC C H N P Cl Fe Ni UNIT 208.00 160.00 8.00 8.00 8.00 4.00 8.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 85841 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ni1 Ni 0.43688(2) 0.81440(4) 0.76453(2) 0.01785(13) Uani 1 1 d . . . . . Fe1 Fe 0.500000 0.40314(5) 0.750000 0.01968(15) Uani 1 2 d S T P . . P1 P 0.38604(3) 0.65892(6) 0.69617(3) 0.01851(15) Uani 1 1 d . . . . . Cl1 Cl 0.40952(2) 0.74328(6) 0.86217(3) 0.02207(14) Uani 1 1 d . . . . . N1 N 0.50134(9) 0.9211(2) 0.67379(11) 0.0194(4) Uani 1 1 d . . . . . C1 C 0.44627(11) 0.9093(2) 0.68267(13) 0.0193(5) Uani 1 1 d . . . . . C2 C 0.51107(11) 0.9939(2) 0.61704(14) 0.0226(5) Uani 1 1 d . . . . . H2 H 0.550893 0.999431 0.612407 0.027 Uiso 1 1 calc R U . . . C3 C 0.46609(12) 1.0579(3) 0.56755(14) 0.0249(5) Uani 1 1 d . . . . . H3 H 0.474415 1.107452 0.529261 0.030 Uiso 1 1 calc R U . . . C4 C 0.40656(11) 1.0496(2) 0.57398(13) 0.0236(5) Uani 1 1 d . . . . . C5 C 0.35731(13) 1.1143(3) 0.52450(15) 0.0311(6) Uani 1 1 d . . . . . H5 H 0.363588 1.164012 0.485065 0.037 Uiso 1 1 calc R U . . . C6 C 0.30095(13) 1.1050(3) 0.53371(16) 0.0342(6) Uani 1 1 d . . . . . H6 H 0.267897 1.145426 0.499237 0.041 Uiso 1 1 calc R U . . . C7 C 0.29105(12) 1.0365(3) 0.59327(16) 0.0315(6) Uani 1 1 d . . . . . H7 H 0.251900 1.034402 0.600198 0.038 Uiso 1 1 calc R U . . . C8 C 0.33788(11) 0.9728(3) 0.64151(15) 0.0257(5) Uani 1 1 d . . . . . H8 H 0.330810 0.925807 0.681428 0.031 Uiso 1 1 calc R U . . . C9 C 0.39665(11) 0.9762(2) 0.63244(13) 0.0218(5) Uani 1 1 d . . . . . C10 C 0.41755(10) 0.5003(2) 0.72531(14) 0.0210(5) Uani 1 1 d . . . . . C11 C 0.41492(11) 0.3909(3) 0.67769(16) 0.0267(5) Uani 1 1 d . . . . . H11 H 0.405610 0.393548 0.625506 0.032 Uiso 1 1 calc R U . . . C12 C 0.42861(12) 0.2782(3) 0.72200(17) 0.0293(6) Uani 1 1 d . . . . . H12 H 0.429639 0.192281 0.704580 0.035 Uiso 1 1 calc R U . . . C13 C 0.44056(12) 0.3160(3) 0.79714(16) 0.0277(6) Uani 1 1 d . . . . . H13 H 0.451101 0.259497 0.838381 0.033 Uiso 1 1 calc R U . . . C14 C 0.43405(11) 0.4523(3) 0.79998(14) 0.0233(5) Uani 1 1 d . . . . . H14 H 0.439565 0.502956 0.843281 0.028 Uiso 1 1 calc R U . . . C15 C 0.38274(11) 0.6621(2) 0.59894(13) 0.0209(5) Uani 1 1 d . . . . . C16 C 0.43730(11) 0.6510(3) 0.58059(14) 0.0245(5) Uani 1 1 d . . . . . H16 H 0.473928 0.638060 0.618300 0.029 Uiso 1 1 calc R U . . . C17 C 0.43802(12) 0.6587(3) 0.50803(16) 0.0317(6) Uani 1 1 d . . . . . H17 H 0.475030 0.649678 0.495908 0.038 Uiso 1 1 calc R U . . . C18 C 0.38499(14) 0.6794(3) 0.45291(16) 0.0358(7) Uani 1 1 d . . . . . H18 H 0.385564 0.684485 0.402987 0.043 Uiso 1 1 calc R U . . . C19 C 0.33132(13) 0.6926(3) 0.47053(15) 0.0327(6) Uani 1 1 d . . . . . H19 H 0.295051 0.708079 0.432651 0.039 Uiso 1 1 calc R U . . . C20 C 0.32983(12) 0.6836(3) 0.54308(15) 0.0265(5) Uani 1 1 d . . . . . H20 H 0.292573 0.692030 0.554635 0.032 Uiso 1 1 calc R U . . . C21 C 0.30735(11) 0.6342(3) 0.69618(13) 0.0217(5) Uani 1 1 d . . . . . C22 C 0.27883(11) 0.7208(3) 0.73144(14) 0.0246(5) Uani 1 1 d . . . . . H22 H 0.300400 0.793612 0.756248 0.030 Uiso 1 1 calc R U . . . C23 C 0.21904(12) 0.7023(3) 0.73090(15) 0.0279(6) Uani 1 1 d . . . . . H23 H 0.199791 0.762785 0.754609 0.034 Uiso 1 1 calc R U . . . C24 C 0.18783(11) 0.5958(3) 0.69580(15) 0.0299(6) Uani 1 1 d . . . . . H24 H 0.147183 0.582195 0.695943 0.036 Uiso 1 1 calc R U . . . C25 C 0.21577(12) 0.5083(3) 0.66023(15) 0.0283(6) Uani 1 1 d . . . . . H25 H 0.194038 0.435435 0.635700 0.034 Uiso 1 1 calc R U . . . C26 C 0.27498(11) 0.5269(3) 0.66045(14) 0.0253(5) Uani 1 1 d . . . . . H26 H 0.293879 0.466591 0.636215 0.030 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ni1 0.0143(2) 0.0207(2) 0.0191(2) -0.00026(15) 0.00561(16) -0.00041(15) Fe1 0.0168(3) 0.0189(3) 0.0270(3) 0.000 0.0121(2) 0.000 P1 0.0134(3) 0.0224(3) 0.0209(3) -0.0016(2) 0.0067(2) -0.0012(2) Cl1 0.0187(3) 0.0271(3) 0.0227(3) 0.0002(2) 0.0095(2) 0.0006(2) N1 0.0183(9) 0.0200(10) 0.0195(9) -0.0016(8) 0.0048(7) -0.0007(8) C1 0.0178(11) 0.0186(11) 0.0210(11) -0.0039(9) 0.0048(9) -0.0011(9) C2 0.0213(11) 0.0238(12) 0.0238(12) -0.0004(10) 0.0081(9) -0.0039(10) C3 0.0290(13) 0.0249(13) 0.0218(12) 0.0017(10) 0.0089(10) -0.0013(10) C4 0.0248(12) 0.0225(12) 0.0216(12) -0.0023(10) 0.0037(9) 0.0020(10) C5 0.0334(15) 0.0317(14) 0.0255(13) 0.0029(11) 0.0040(11) 0.0050(12) C6 0.0279(14) 0.0357(15) 0.0328(15) 0.0021(12) -0.0012(11) 0.0102(12) C7 0.0181(12) 0.0346(15) 0.0382(15) -0.0026(12) 0.0021(11) 0.0064(11) C8 0.0203(12) 0.0260(13) 0.0296(13) -0.0001(10) 0.0049(10) 0.0012(10) C9 0.0198(11) 0.0209(11) 0.0229(12) -0.0024(9) 0.0029(9) 0.0011(9) C10 0.0123(10) 0.0228(12) 0.0301(12) -0.0003(10) 0.0094(9) -0.0006(9) C11 0.0197(12) 0.0291(13) 0.0341(14) -0.0069(11) 0.0120(10) -0.0029(10) C12 0.0221(13) 0.0234(13) 0.0474(16) -0.0051(12) 0.0178(12) -0.0071(10) C13 0.0238(13) 0.0241(13) 0.0416(15) 0.0042(11) 0.0195(11) -0.0008(10) C14 0.0191(11) 0.0257(12) 0.0297(13) 0.0015(10) 0.0145(10) -0.0002(10) C15 0.0172(11) 0.0237(12) 0.0227(12) -0.0024(9) 0.0072(9) -0.0026(9) C16 0.0180(11) 0.0312(13) 0.0246(12) -0.0009(10) 0.0067(9) -0.0010(10) C17 0.0228(13) 0.0455(16) 0.0309(14) 0.0001(12) 0.0142(11) 0.0034(12) C18 0.0319(15) 0.0535(19) 0.0247(14) 0.0016(12) 0.0123(11) 0.0049(13) C19 0.0238(13) 0.0487(17) 0.0244(13) 0.0026(12) 0.0050(10) 0.0040(12) C20 0.0183(12) 0.0359(15) 0.0260(13) 0.0001(11) 0.0076(10) 0.0022(10) C21 0.0157(11) 0.0289(13) 0.0219(11) 0.0031(10) 0.0072(9) -0.0005(10) C22 0.0175(11) 0.0320(13) 0.0253(12) -0.0008(11) 0.0077(9) -0.0009(10) C23 0.0191(12) 0.0379(15) 0.0290(13) 0.0010(11) 0.0105(10) 0.0010(11) C24 0.0147(11) 0.0446(16) 0.0314(14) 0.0052(12) 0.0082(10) -0.0029(11) C25 0.0221(12) 0.0333(14) 0.0284(13) 0.0026(11) 0.0052(10) -0.0078(11) C26 0.0220(12) 0.0294(13) 0.0255(12) -0.0006(10) 0.0081(10) -0.0029(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Ni Ni -3.0029 0.5091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe -1.1336 3.1974 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 Ni1 N1 87.89(9) . 2_656 ? C1 Ni1 P1 93.59(7) . . ? N1 Ni1 P1 165.15(7) 2_656 . ? C1 Ni1 Cl1 165.38(8) . . ? N1 Ni1 Cl1 91.21(6) 2_656 . ? P1 Ni1 Cl1 91.01(3) . . ? C12 Fe1 C12 101.64(16) . 2_656 ? C12 Fe1 C13 101.59(11) . 2_656 ? C12 Fe1 C13 40.79(12) 2_656 2_656 ? C12 Fe1 C13 40.79(12) . . ? C12 Fe1 C13 101.59(11) 2_656 . ? C13 Fe1 C13 127.77(15) 2_656 . ? C12 Fe1 C11 40.43(11) . . ? C12 Fe1 C11 133.10(11) 2_656 . ? C13 Fe1 C11 108.39(11) 2_656 . ? C13 Fe1 C11 68.29(11) . . ? C12 Fe1 C11 133.10(11) . 2_656 ? C12 Fe1 C11 40.43(11) 2_656 2_656 ? C13 Fe1 C11 68.29(11) 2_656 2_656 ? C13 Fe1 C11 108.40(11) . 2_656 ? C11 Fe1 C11 172.93(16) . 2_656 ? C12 Fe1 C14 132.90(11) . 2_656 ? C12 Fe1 C14 68.25(10) 2_656 2_656 ? C13 Fe1 C14 40.34(10) 2_656 2_656 ? C13 Fe1 C14 168.06(11) . 2_656 ? C11 Fe1 C14 113.52(10) . 2_656 ? C11 Fe1 C14 68.36(10) 2_656 2_656 ? C12 Fe1 C14 68.25(10) . . ? C12 Fe1 C14 132.90(11) 2_656 . ? C13 Fe1 C14 168.06(11) 2_656 . ? C13 Fe1 C14 40.33(10) . . ? C11 Fe1 C14 68.36(10) . . ? C11 Fe1 C14 113.52(10) 2_656 . ? C14 Fe1 C14 151.58(15) 2_656 . ? C12 Fe1 C10 168.93(10) . 2_656 ? C12 Fe1 C10 68.08(10) 2_656 2_656 ? C13 Fe1 C10 68.08(10) 2_656 2_656 ? C13 Fe1 C10 142.85(11) . 2_656 ? C11 Fe1 C10 144.99(11) . 2_656 ? C11 Fe1 C10 40.56(10) 2_656 2_656 ? C14 Fe1 C10 40.65(10) 2_656 2_656 ? C14 Fe1 C10 121.50(10) . 2_656 ? C12 Fe1 C10 68.08(10) . . ? C12 Fe1 C10 168.93(10) 2_656 . ? C13 Fe1 C10 142.85(11) 2_656 . ? C13 Fe1 C10 68.08(10) . . ? C11 Fe1 C10 40.56(10) . . ? C11 Fe1 C10 144.99(11) 2_656 . ? C14 Fe1 C10 121.50(10) 2_656 . ? C14 Fe1 C10 40.65(10) . . ? C10 Fe1 C10 122.47(14) 2_656 . ? C10 P1 C15 102.86(11) . . ? C10 P1 C21 100.75(11) . . ? C15 P1 C21 104.09(11) . . ? C10 P1 Ni1 112.42(8) . . ? C15 P1 Ni1 116.57(8) . . ? C21 P1 Ni1 117.97(9) . . ? C1 N1 C2 121.2(2) . . ? C1 N1 Ni1 116.30(16) . 2_656 ? C2 N1 Ni1 122.03(16) . 2_656 ? N1 C1 C9 118.8(2) . . ? N1 C1 Ni1 118.85(17) . . ? C9 C1 Ni1 122.22(18) . . ? C3 C2 N1 122.7(2) . . ? C3 C2 H2 118.6 . . ? N1 C2 H2 118.6 . . ? C2 C3 C4 118.9(2) . . ? C2 C3 H3 120.5 . . ? C4 C3 H3 120.5 . . ? C9 C4 C3 118.4(2) . . ? C9 C4 C5 119.5(2) . . ? C3 C4 C5 122.1(2) . . ? C6 C5 C4 119.9(3) . . ? C6 C5 H5 120.1 . . ? C4 C5 H5 120.1 . . ? C5 C6 C7 121.1(2) . . ? C5 C6 H6 119.5 . . ? C7 C6 H6 119.5 . . ? C8 C7 C6 120.0(3) . . ? C8 C7 H7 120.0 . . ? C6 C7 H7 120.0 . . ? C7 C8 C9 120.7(3) . . ? C7 C8 H8 119.6 . . ? C9 C8 H8 119.6 . . ? C4 C9 C8 118.7(2) . . ? C4 C9 C1 120.0(2) . . ? C8 C9 C1 121.3(2) . . ? C11 C10 C14 107.3(2) . . ? C11 C10 P1 125.3(2) . . ? C14 C10 P1 125.45(19) . . ? C11 C10 Fe1 68.67(14) . . ? C14 C10 Fe1 69.10(13) . . ? P1 C10 Fe1 139.93(13) . . ? C12 C11 C10 108.2(2) . . ? C12 C11 Fe1 69.22(15) . . ? C10 C11 Fe1 70.77(14) . . ? C12 C11 H11 125.9 . . ? C10 C11 H11 125.9 . . ? Fe1 C11 H11 125.7 . . ? C11 C12 C13 108.3(2) . . ? C11 C12 Fe1 70.35(15) . . ? C13 C12 Fe1 69.69(15) . . ? C11 C12 H12 125.9 . . ? C13 C12 H12 125.9 . . ? Fe1 C12 H12 125.7 . . ? C14 C13 C12 108.5(2) . . ? C14 C13 Fe1 70.79(14) . . ? C12 C13 Fe1 69.52(15) . . ? C14 C13 H13 125.8 . . ? C12 C13 H13 125.8 . . ? Fe1 C13 H13 125.5 . . ? C13 C14 C10 107.8(2) . . ? C13 C14 Fe1 68.87(14) . . ? C10 C14 Fe1 70.25(13) . . ? C13 C14 H14 126.1 . . ? C10 C14 H14 126.1 . . ? Fe1 C14 H14 126.3 . . ? C20 C15 C16 118.9(2) . . ? C20 C15 P1 123.30(19) . . ? C16 C15 P1 117.66(18) . . ? C17 C16 C15 120.3(2) . . ? C17 C16 H16 119.8 . . ? C15 C16 H16 119.8 . . ? C16 C17 C18 120.2(2) . . ? C16 C17 H17 119.9 . . ? C18 C17 H17 119.9 . . ? C19 C18 C17 119.9(3) . . ? C19 C18 H18 120.1 . . ? C17 C18 H18 120.1 . . ? C18 C19 C20 120.5(3) . . ? C18 C19 H19 119.7 . . ? C20 C19 H19 119.7 . . ? C19 C20 C15 120.1(2) . . ? C19 C20 H20 119.9 . . ? C15 C20 H20 119.9 . . ? C22 C21 C26 118.8(2) . . ? C22 C21 P1 120.96(19) . . ? C26 C21 P1 120.28(19) . . ? C21 C22 C23 120.8(2) . . ? C21 C22 H22 119.6 . . ? C23 C22 H22 119.6 . . ? C24 C23 C22 119.8(3) . . ? C24 C23 H23 120.1 . . ? C22 C23 H23 120.1 . . ? C23 C24 C25 120.1(2) . . ? C23 C24 H24 120.0 . . ? C25 C24 H24 120.0 . . ? C26 C25 C24 120.2(3) . . ? C26 C25 H25 119.9 . . ? C24 C25 H25 119.9 . . ? C25 C26 C21 120.4(2) . . ? C25 C26 H26 119.8 . . ? C21 C26 H26 119.8 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ni1 C1 1.897(2) . ? Ni1 N1 1.917(2) 2_656 ? Ni1 P1 2.1855(7) . ? Ni1 Cl1 2.2389(7) . ? Fe1 C12 2.043(3) . ? Fe1 C12 2.043(3) 2_656 ? Fe1 C13 2.045(2) 2_656 ? Fe1 C13 2.045(3) . ? Fe1 C11 2.058(3) . ? Fe1 C11 2.058(3) 2_656 ? Fe1 C14 2.070(2) 2_656 ? Fe1 C14 2.070(2) . ? Fe1 C10 2.086(2) 2_656 ? Fe1 C10 2.086(2) . ? P1 C10 1.815(3) . ? P1 C15 1.820(2) . ? P1 C21 1.836(2) . ? N1 C1 1.335(3) . ? N1 C2 1.381(3) . ? C1 C9 1.442(3) . ? C2 C3 1.359(4) . ? C2 H2 0.9500 . ? C3 C4 1.417(4) . ? C3 H3 0.9500 . ? C4 C9 1.413(4) . ? C4 C5 1.420(4) . ? C5 C6 1.365(4) . ? C5 H5 0.9500 . ? C6 C7 1.403(4) . ? C6 H6 0.9500 . ? C7 C8 1.371(4) . ? C7 H7 0.9500 . ? C8 C9 1.416(4) . ? C8 H8 0.9500 . ? C10 C11 1.436(4) . ? C10 C14 1.444(4) . ? C11 C12 1.417(4) . ? C11 H11 0.9500 . ? C12 C13 1.425(4) . ? C12 H12 0.9500 . ? C13 C14 1.419(4) . ? C13 H13 0.9500 . ? C14 H14 0.9500 . ? C15 C20 1.390(3) . ? C15 C16 1.403(3) . ? C16 C17 1.380(4) . ? C16 H16 0.9500 . ? C17 C18 1.383(4) . ? C17 H17 0.9500 . ? C18 C19 1.379(4) . ? C18 H18 0.9500 . ? C19 C20 1.386(4) . ? C19 H19 0.9500 . ? C20 H20 0.9500 . ? C21 C22 1.389(4) . ? C21 C26 1.400(4) . ? C22 C23 1.391(3) . ? C22 H22 0.9500 . ? C23 C24 1.379(4) . ? C23 H23 0.9500 . ? C24 C25 1.390(4) . ? C24 H24 0.9500 . ? C25 C26 1.380(4) . ? C25 H25 0.9500 . ? C26 H26 0.9500 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C2 N1 C1 C9 -1.1(3) . . . . ? Ni1 N1 C1 C9 -173.24(17) 2_656 . . . ? C2 N1 C1 Ni1 -177.09(17) . . . . ? Ni1 N1 C1 Ni1 10.8(2) 2_656 . . . ? N1 Ni1 C1 N1 52.71(17) 2_656 . . . ? P1 Ni1 C1 N1 -112.49(18) . . . . ? Cl1 Ni1 C1 N1 139.4(2) . . . . ? N1 Ni1 C1 C9 -123.1(2) 2_656 . . . ? P1 Ni1 C1 C9 71.65(19) . . . . ? Cl1 Ni1 C1 C9 -36.5(4) . . . . ? C1 N1 C2 C3 0.4(4) . . . . ? Ni1 N1 C2 C3 172.1(2) 2_656 . . . ? N1 C2 C3 C4 -0.2(4) . . . . ? C2 C3 C4 C9 0.8(4) . . . . ? C2 C3 C4 C5 179.7(3) . . . . ? C9 C4 C5 C6 -0.1(4) . . . . ? C3 C4 C5 C6 -179.0(3) . . . . ? C4 C5 C6 C7 2.6(4) . . . . ? C5 C6 C7 C8 -3.0(4) . . . . ? C6 C7 C8 C9 0.7(4) . . . . ? C3 C4 C9 C8 176.8(2) . . . . ? C5 C4 C9 C8 -2.1(4) . . . . ? C3 C4 C9 C1 -1.5(4) . . . . ? C5 C4 C9 C1 179.5(2) . . . . ? C7 C8 C9 C4 1.8(4) . . . . ? C7 C8 C9 C1 -179.9(2) . . . . ? N1 C1 C9 C4 1.7(3) . . . . ? Ni1 C1 C9 C4 177.54(18) . . . . ? N1 C1 C9 C8 -176.6(2) . . . . ? Ni1 C1 C9 C8 -0.8(3) . . . . ? C15 P1 C10 C11 -23.3(2) . . . . ? C21 P1 C10 C11 84.0(2) . . . . ? Ni1 P1 C10 C11 -149.52(18) . . . . ? C15 P1 C10 C14 174.8(2) . . . . ? C21 P1 C10 C14 -77.9(2) . . . . ? Ni1 P1 C10 C14 48.6(2) . . . . ? C15 P1 C10 Fe1 75.3(2) . . . . ? C21 P1 C10 Fe1 -177.4(2) . . . . ? Ni1 P1 C10 Fe1 -50.9(2) . . . . ? C14 C10 C11 C12 0.8(3) . . . . ? P1 C10 C11 C12 -163.78(18) . . . . ? Fe1 C10 C11 C12 59.32(17) . . . . ? C14 C10 C11 Fe1 -58.50(16) . . . . ? P1 C10 C11 Fe1 136.89(18) . . . . ? C10 C11 C12 C13 -0.7(3) . . . . ? Fe1 C11 C12 C13 59.59(18) . . . . ? C10 C11 C12 Fe1 -60.30(17) . . . . ? C11 C12 C13 C14 0.3(3) . . . . ? Fe1 C12 C13 C14 60.32(18) . . . . ? C11 C12 C13 Fe1 -60.01(18) . . . . ? C12 C13 C14 C10 0.2(3) . . . . ? Fe1 C13 C14 C10 59.73(16) . . . . ? C12 C13 C14 Fe1 -59.53(18) . . . . ? C11 C10 C14 C13 -0.6(3) . . . . ? P1 C10 C14 C13 163.95(18) . . . . ? Fe1 C10 C14 C13 -58.86(17) . . . . ? C11 C10 C14 Fe1 58.23(16) . . . . ? P1 C10 C14 Fe1 -137.19(18) . . . . ? C10 P1 C15 C20 123.0(2) . . . . ? C21 P1 C15 C20 18.3(3) . . . . ? Ni1 P1 C15 C20 -113.5(2) . . . . ? C10 P1 C15 C16 -61.4(2) . . . . ? C21 P1 C15 C16 -166.1(2) . . . . ? Ni1 P1 C15 C16 62.1(2) . . . . ? C20 C15 C16 C17 -1.3(4) . . . . ? P1 C15 C16 C17 -177.1(2) . . . . ? C15 C16 C17 C18 1.0(4) . . . . ? C16 C17 C18 C19 0.1(5) . . . . ? C17 C18 C19 C20 -0.9(5) . . . . ? C18 C19 C20 C15 0.6(5) . . . . ? C16 C15 C20 C19 0.5(4) . . . . ? P1 C15 C20 C19 176.0(2) . . . . ? C10 P1 C21 C22 130.2(2) . . . . ? C15 P1 C21 C22 -123.5(2) . . . . ? Ni1 P1 C21 C22 7.5(2) . . . . ? C10 P1 C21 C26 -49.7(2) . . . . ? C15 P1 C21 C26 56.6(2) . . . . ? Ni1 P1 C21 C26 -172.43(17) . . . . ? C26 C21 C22 C23 -0.5(4) . . . . ? P1 C21 C22 C23 179.5(2) . . . . ? C21 C22 C23 C24 0.9(4) . . . . ? C22 C23 C24 C25 -0.9(4) . . . . ? C23 C24 C25 C26 0.6(4) . . . . ? C24 C25 C26 C21 -0.3(4) . . . . ? C22 C21 C26 C25 0.2(4) . . . . ? P1 C21 C26 C25 -179.8(2) . . . . ?