#------------------------------------------------------------------------------ #$Date: 2022-03-18 12:32:04 +0200 (Fri, 18 Mar 2022) $ #$Revision: 273808 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/51/1565118.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1565118 loop_ _publ_author_name 'Wu, Ni' 'Xiao, Hui' 'Lou, Yuheng' 'Han, Mingxi' 'Guo, Zhiyong' 'Zhan, Hongbing' _publ_section_title ; Manipulating the Position of Triplet Chromophores To Achieve a Dynamic Photoactivated Ultralong Organic Phosphorescence Effect ; _journal_issue 41 _journal_name_full 'The Journal of Physical Chemistry C' _journal_page_first 22848 _journal_page_last 22855 _journal_paper_doi 10.1021/acs.jpcc.1c06860 _journal_volume 125 _journal_year 2021 _chemical_formula_moiety 'C30 H19 Cl N2' _chemical_formula_sum 'C30 H19 Cl N2' _chemical_formula_weight 442.92 _chemical_melting_point ? _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2017/1 _cell_angle_alpha 89.128(2) _cell_angle_beta 88.531(2) _cell_angle_gamma 81.574(2) _cell_formula_units_Z 6 _cell_length_a 9.2641(5) _cell_length_b 14.4485(8) _cell_length_c 25.7528(14) _cell_measurement_reflns_used 12027 _cell_measurement_temperature 200(2) _cell_measurement_theta_max 25.071 _cell_measurement_theta_min 1.425 _cell_volume 3408.5(3) _computing_structure_refinement 'SHELXL-2017/1 (Sheldrick, 2017)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 200(2) _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'SuperNova, Dual, Mo at zero, Atlas' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0968 _diffrn_reflns_av_unetI/netI 0.1062 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 30 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_number 45806 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.071 _diffrn_reflns_theta_max 25.071 _diffrn_reflns_theta_min 1.425 _exptl_absorpt_coefficient_mu 0.189 _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.295 _exptl_crystal_description lump _exptl_crystal_F_000 1380 _exptl_crystal_size_max 0.130 _exptl_crystal_size_mid 0.120 _exptl_crystal_size_min 0.100 _refine_diff_density_max 0.215 _refine_diff_density_min -0.289 _refine_diff_density_rms 0.046 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.021 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 892 _refine_ls_number_reflns 12027 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.022 _refine_ls_R_factor_all 0.1530 _refine_ls_R_factor_gt 0.0671 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0476P)^2^+1.2482P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1218 _refine_ls_wR_factor_ref 0.1488 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6401 _reflns_number_total 12027 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file jp1c06860_si_005.cif _cod_data_source_block gzy26a_0m_a _cod_depositor_comments ; The following automatic conversions were performed: data item '_chemical_melting_point' value 'not measured' was changed to '?' -- the value is undefined or not given. Automatic conversion script Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas 2022-03-18 Z value and formula fixed to values more according to usual chemical conventions. miguel ; _cod_original_formula_sum 'C90 H57 Cl3 N6' _cod_original_formula_weight 1328.76 _cod_original_formula_moiety 'C90 H57 Cl3 N6' _cod_original_formula_units_Z 2 _cod_database_code 1565118 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.976 _shelx_estimated_absorpt_t_max 0.981 _shelx_res_file ; TITL gzy26a_0m_a.res in P-1 gzy26a_0m_a.res created by SHELXL-2017/1 at 09:40:39 on 28-Sep-2020 CELL 0.71073 9.2641 14.4485 25.7528 89.128 88.531 81.574 ZERR 2.000 0.0005 0.0008 0.0014 0.002 0.002 0.002 LATT 1 SFAC C H Cl N UNIT 180 114 6 12 OMIT 0 -1 1 OMIT 0 1 1 OMIT 0 0 2 OMIT -1 -1 1 OMIT -2 -5 7 OMIT 0 3 0 OMIT -1 -2 2 OMIT 1 1 1 OMIT 0 0 1 OMIT 0 -1 4 OMIT 0 -2 1 OMIT 1 0 0 OMIT 1 1 0 L.S. 10 ACTA BOND $H FMAP 2 PLAN 5 SIZE 0.10 0.12 0.13 DELU 0.01 0.01 C54 C55 TEMP 23 WGHT 0.047600 1.248200 FVAR 0.33256 CL1 3 0.322815 0.630641 0.658837 11.00000 0.06007 0.04085 = 0.06172 0.01063 -0.01494 -0.01247 CL2 3 0.716547 0.303773 0.881784 11.00000 0.13938 0.07293 = 0.06063 0.00927 -0.04189 -0.03717 CL3 3 0.333370 0.208073 0.606083 11.00000 0.09465 0.04735 = 0.06787 0.00317 -0.01743 -0.02011 N1 4 0.236751 0.437419 0.664341 11.00000 0.05482 0.04391 = 0.06345 -0.00158 -0.00958 -0.02352 N2 4 0.540807 0.647554 0.739549 11.00000 0.03545 0.02757 = 0.06213 -0.00241 -0.00388 -0.00964 N3 4 0.861568 0.444458 0.934945 11.00000 0.05298 0.03253 = 0.05302 0.00723 0.00114 -0.01034 N4 4 0.690517 0.142604 0.951866 11.00000 0.05017 0.03936 = 0.07073 -0.00404 -0.00388 -0.01766 N5 4 0.398780 0.076118 0.694092 11.00000 0.05502 0.06277 = 0.04519 0.00030 -0.01363 -0.01983 N6 4 0.152676 0.125753 0.528774 11.00000 0.05542 0.06136 = 0.04637 0.00469 -0.01554 -0.00287 C1 1 0.393331 0.541497 0.700525 11.00000 0.03844 0.02858 = 0.04822 0.00364 0.00012 -0.00392 C2 1 0.346624 0.454134 0.698608 11.00000 0.04140 0.03290 = 0.06020 -0.00170 -0.00203 -0.01107 C3 1 0.406457 0.384352 0.732108 11.00000 0.04942 0.02902 = 0.07743 0.00262 -0.00155 -0.01319 AFIX 43 H3 2 0.376597 0.325709 0.731077 11.00000 -1.20000 AFIX 0 C4 1 0.509148 0.400266 0.766830 11.00000 0.05309 0.03551 = 0.07479 0.01205 -0.01226 -0.01040 AFIX 43 H4 2 0.548730 0.352468 0.789102 11.00000 -1.20000 AFIX 0 C5 1 0.553960 0.486554 0.768906 11.00000 0.04179 0.04241 = 0.06024 0.00572 -0.01084 -0.00987 AFIX 43 H5 2 0.623174 0.497105 0.792804 11.00000 -1.20000 AFIX 0 C6 1 0.497124 0.557415 0.735873 11.00000 0.03328 0.02713 = 0.05412 -0.00036 -0.00166 -0.00799 C7 1 0.104245 0.407658 0.679989 11.00000 0.04990 0.03334 = 0.08661 -0.00688 -0.01177 -0.00793 C8 1 0.051181 0.391511 0.729207 11.00000 0.05555 0.04743 = 0.09824 0.00411 0.00144 -0.01623 AFIX 43 H8 2 0.102835 0.402156 0.758489 11.00000 -1.20000 AFIX 0 C9 1 -0.081748 0.358881 0.733513 11.00000 0.05809 0.06475 = 0.14889 -0.00199 0.01206 -0.01650 AFIX 43 H9 2 -0.120279 0.346882 0.766212 11.00000 -1.20000 AFIX 0 C10 1 -0.157284 0.344047 0.690057 11.00000 0.05801 0.07299 = 0.19519 -0.03173 0.00605 -0.01878 AFIX 43 H10 2 -0.246019 0.321604 0.694206 11.00000 -1.20000 AFIX 0 C11 1 -0.107610 0.360868 0.640916 11.00000 0.06181 0.07527 = 0.16426 -0.04498 -0.03274 -0.01452 AFIX 43 H11 2 -0.161119 0.350845 0.611989 11.00000 -1.20000 AFIX 0 C12 1 0.027084 0.393811 0.635746 11.00000 0.06117 0.04820 = 0.09858 -0.02078 -0.02287 -0.00724 C13 1 0.114964 0.413070 0.592165 11.00000 0.09826 0.04256 = 0.07537 -0.01754 -0.03787 -0.00751 C14 1 0.098715 0.407257 0.538742 11.00000 0.13942 0.07349 = 0.11245 -0.02064 -0.04736 -0.01382 AFIX 43 H14 2 0.011604 0.393969 0.525555 11.00000 -1.20000 AFIX 0 C15 1 0.210596 0.421089 0.506243 11.00000 0.20293 0.10187 = 0.08302 -0.03428 -0.02887 -0.04664 AFIX 43 H15 2 0.199132 0.416976 0.470621 11.00000 -1.20000 AFIX 0 C16 1 0.340804 0.441049 0.524258 11.00000 0.18789 0.10442 = 0.08125 -0.02087 0.02195 -0.06351 AFIX 43 H16 2 0.416347 0.448442 0.500783 11.00000 -1.20000 AFIX 0 C17 1 0.361312 0.450447 0.577751 11.00000 0.12550 0.07616 = 0.07608 -0.01567 0.00605 -0.04706 AFIX 43 H17 2 0.448402 0.464813 0.590409 11.00000 -1.20000 AFIX 0 C18 1 0.246004 0.437308 0.610377 11.00000 0.08465 0.04036 = 0.06658 -0.00831 -0.01380 -0.01698 C19 1 0.682006 0.667770 0.730430 11.00000 0.03911 0.03505 = 0.04707 0.00829 -0.00895 -0.01322 C20 1 0.804793 0.610599 0.712316 11.00000 0.04267 0.04478 = 0.06893 0.00890 -0.00645 -0.00873 AFIX 43 H20 2 0.801796 0.548536 0.703939 11.00000 -1.20000 AFIX 0 C21 1 0.931726 0.648979 0.707139 11.00000 0.04193 0.06402 = 0.08025 0.01754 -0.00405 -0.01306 AFIX 43 H21 2 1.016482 0.612023 0.695266 11.00000 -1.20000 AFIX 0 C22 1 0.935919 0.741412 0.719228 11.00000 0.04415 0.07403 = 0.07903 0.02448 -0.01743 -0.02854 AFIX 43 H22 2 1.023457 0.765355 0.715201 11.00000 -1.20000 AFIX 0 C23 1 0.814413 0.798439 0.736959 11.00000 0.06708 0.04933 = 0.05530 0.01609 -0.01981 -0.02942 AFIX 43 H23 2 0.818583 0.860682 0.744596 11.00000 -1.20000 AFIX 0 C24 1 0.684282 0.761648 0.743380 11.00000 0.04524 0.03639 = 0.04075 0.01198 -0.01359 -0.01514 C25 1 0.540488 0.798877 0.761728 11.00000 0.05339 0.02807 = 0.04372 0.00689 -0.01378 -0.00962 C26 1 0.475987 0.884331 0.782492 11.00000 0.07684 0.03427 = 0.04895 0.00612 -0.01682 -0.01439 AFIX 43 H26 2 0.530220 0.933341 0.784897 11.00000 -1.20000 AFIX 0 C27 1 0.334302 0.895894 0.799152 11.00000 0.08275 0.03668 = 0.05140 -0.00550 -0.00377 0.00196 AFIX 43 H27 2 0.292530 0.952755 0.813231 11.00000 -1.20000 AFIX 0 C28 1 0.250985 0.823952 0.795443 11.00000 0.05495 0.05288 = 0.06124 -0.00405 0.00700 -0.00002 AFIX 43 H28 2 0.153969 0.833651 0.806878 11.00000 -1.20000 AFIX 0 C29 1 0.309326 0.738165 0.775092 11.00000 0.05170 0.04066 = 0.05740 0.00030 0.00136 -0.00906 AFIX 43 H29 2 0.253362 0.690086 0.772426 11.00000 -1.20000 AFIX 0 C30 1 0.453577 0.726786 0.758935 11.00000 0.04683 0.03374 = 0.04355 0.00672 -0.00989 -0.01030 C31 1 0.778092 0.293103 0.943970 11.00000 0.04809 0.03999 = 0.03847 -0.00088 -0.00725 -0.01076 C32 1 0.847243 0.362560 0.964431 11.00000 0.04621 0.03283 = 0.04342 0.00245 0.00098 -0.01132 C33 1 0.901722 0.351221 1.013451 11.00000 0.07419 0.04194 = 0.05536 -0.00329 -0.02146 -0.01720 AFIX 43 H33 2 0.948294 0.397516 1.027525 11.00000 -1.20000 AFIX 0 C34 1 0.887745 0.271713 1.041846 11.00000 0.11212 0.04783 = 0.04844 0.01040 -0.02971 -0.01567 AFIX 43 H34 2 0.926565 0.263809 1.074838 11.00000 -1.20000 AFIX 0 C35 1 0.816822 0.203897 1.021797 11.00000 0.08238 0.04117 = 0.05283 0.01000 -0.00724 -0.01763 AFIX 43 H35 2 0.806634 0.150687 1.041521 11.00000 -1.20000 AFIX 0 C36 1 0.760850 0.213807 0.972991 11.00000 0.04584 0.03406 = 0.04732 -0.00186 -0.00326 -0.00959 C37 1 0.748033 0.513678 0.921493 11.00000 0.05625 0.03496 = 0.05044 0.00155 -0.00095 -0.01202 C38 1 0.603546 0.523926 0.937570 11.00000 0.06419 0.05200 = 0.07291 0.00585 0.00502 -0.00796 AFIX 43 H38 2 0.568996 0.480496 0.959885 11.00000 -1.20000 AFIX 0 C39 1 0.512074 0.600850 0.919389 11.00000 0.07025 0.06169 = 0.09180 -0.00174 -0.00161 0.00455 AFIX 43 H39 2 0.414090 0.609463 0.929651 11.00000 -1.20000 AFIX 0 C40 1 0.563408 0.665537 0.886126 11.00000 0.09107 0.04885 = 0.07000 0.00298 -0.02258 0.00625 AFIX 43 H40 2 0.499976 0.717410 0.874821 11.00000 -1.20000 AFIX 0 C41 1 0.706170 0.653908 0.869774 11.00000 0.09179 0.04345 = 0.04768 0.00376 -0.00986 -0.01016 AFIX 43 H41 2 0.739587 0.697132 0.847039 11.00000 -1.20000 AFIX 0 C42 1 0.801171 0.577137 0.887299 11.00000 0.06792 0.03445 = 0.03463 -0.00031 -0.00934 -0.01157 C43 1 0.953076 0.543656 0.878182 11.00000 0.06326 0.03573 = 0.04079 -0.00287 0.00056 -0.01567 C44 1 1.063159 0.575325 0.848122 11.00000 0.08561 0.05283 = 0.06350 0.00539 0.01119 -0.01972 AFIX 43 H44 2 1.043419 0.628775 0.827429 11.00000 -1.20000 AFIX 0 C45 1 1.200935 0.526345 0.849590 11.00000 0.09216 0.06955 = 0.09245 0.00353 0.02932 -0.02563 AFIX 43 H45 2 1.274987 0.547868 0.829878 11.00000 -1.20000 AFIX 0 C46 1 1.234054 0.446066 0.879296 11.00000 0.06052 0.06571 = 0.10276 -0.00462 0.01823 -0.01109 AFIX 43 H46 2 1.329119 0.414608 0.879297 11.00000 -1.20000 AFIX 0 C47 1 1.126325 0.412196 0.909085 11.00000 0.06635 0.04088 = 0.07904 0.00079 0.00005 -0.01368 AFIX 43 H47 2 1.146765 0.357888 0.929043 11.00000 -1.20000 AFIX 0 C48 1 0.987739 0.461965 0.908047 11.00000 0.05219 0.03389 = 0.04845 -0.00665 -0.00244 -0.01641 C49 1 0.760743 0.068671 0.922431 11.00000 0.06337 0.03604 = 0.05196 -0.00006 -0.01410 -0.01826 C50 1 0.904188 0.051988 0.905633 11.00000 0.06545 0.05913 = 0.07353 -0.01276 -0.00919 -0.01000 AFIX 43 H50 2 0.969039 0.093249 0.912845 11.00000 -1.20000 AFIX 0 C51 1 0.947894 -0.027844 0.877835 11.00000 0.09618 0.07849 = 0.08790 -0.02769 -0.00318 0.00103 AFIX 43 H51 2 1.044234 -0.040670 0.865878 11.00000 -1.20000 AFIX 0 C52 1 0.853933 -0.088720 0.867314 11.00000 0.13879 0.06981 = 0.08483 -0.02462 -0.01566 -0.00825 AFIX 43 H52 2 0.888041 -0.142573 0.848768 11.00000 -1.20000 AFIX 0 C53 1 0.710902 -0.072910 0.883242 11.00000 0.12878 0.05157 = 0.06127 -0.00205 -0.03687 -0.03407 AFIX 43 H53 2 0.647879 -0.115125 0.875656 11.00000 -1.20000 AFIX 0 C54 1 0.660750 0.009051 0.911519 11.00000 0.07299 0.05193 = 0.04994 0.01078 -0.02055 -0.02390 C55 1 0.525408 0.047640 0.934470 11.00000 0.07248 0.05666 = 0.05071 0.02607 -0.03014 -0.03909 C56 1 0.386468 0.022083 0.937400 11.00000 0.09387 0.10505 = 0.07778 0.04396 -0.03652 -0.05541 AFIX 43 H56 2 0.368542 -0.032204 0.921364 11.00000 -1.20000 AFIX 0 C57 1 0.277554 0.075715 0.963410 11.00000 0.07483 0.14260 = 0.09284 0.05917 -0.03292 -0.05727 AFIX 43 H57 2 0.185640 0.057044 0.965226 11.00000 -1.20000 AFIX 0 C58 1 0.298265 0.158295 0.987682 11.00000 0.06404 0.12983 = 0.07466 0.04488 0.00299 -0.00119 AFIX 43 H58 2 0.220710 0.193828 1.005167 11.00000 -1.20000 AFIX 0 C59 1 0.435906 0.187693 0.985714 11.00000 0.05681 0.08080 = 0.07653 0.02734 -0.00714 -0.01257 AFIX 43 H59 2 0.452582 0.242542 1.001445 11.00000 -1.20000 AFIX 0 C60 1 0.545453 0.130958 0.959197 11.00000 0.04927 0.05735 = 0.05406 0.02075 -0.00770 -0.01482 C61 1 0.274067 0.101465 0.612104 11.00000 0.04930 0.03872 = 0.04217 -0.00462 -0.00404 -0.00687 C62 1 0.310487 0.045530 0.655443 11.00000 0.04585 0.04827 = 0.03728 -0.00530 -0.00388 -0.00686 C63 1 0.259387 -0.038873 0.661310 11.00000 0.06614 0.05311 = 0.03885 0.00699 -0.00453 -0.01292 AFIX 43 H63 2 0.283031 -0.076101 0.690523 11.00000 -1.20000 AFIX 0 C64 1 0.172985 -0.068223 0.623781 11.00000 0.07446 0.05133 = 0.05220 -0.00301 -0.00945 -0.02650 AFIX 43 H64 2 0.138095 -0.125120 0.627878 11.00000 -1.20000 AFIX 0 C65 1 0.138494 -0.014024 0.580632 11.00000 0.06126 0.05926 = 0.04301 -0.00599 -0.01161 -0.01599 AFIX 43 H65 2 0.080556 -0.034618 0.555531 11.00000 -1.20000 AFIX 0 C66 1 0.188497 0.070856 0.573811 11.00000 0.05068 0.04753 = 0.03672 -0.00138 -0.00745 -0.00140 C67 1 0.551178 0.062492 0.692498 11.00000 0.06580 0.05966 = 0.06396 0.02103 -0.02031 -0.02596 C68 1 0.645542 0.022039 0.654320 11.00000 0.05588 0.09406 = 0.09655 0.03099 0.00169 -0.01545 AFIX 43 H68 2 0.611044 0.000645 0.623795 11.00000 -1.20000 AFIX 0 C69 1 0.792026 0.014480 0.662963 11.00000 0.05773 0.11174 = 0.17961 0.05168 0.00973 -0.01762 AFIX 43 H69 2 0.858397 -0.013441 0.638127 11.00000 -1.20000 AFIX 0 C70 1 0.842215 0.047362 0.707558 11.00000 0.08351 0.10905 = 0.22980 0.06310 -0.04962 -0.05591 AFIX 43 H70 2 0.942527 0.041943 0.711742 11.00000 -1.20000 AFIX 0 C71 1 0.751732 0.087880 0.746330 11.00000 0.09986 0.07300 = 0.16193 0.04602 -0.07424 -0.04970 AFIX 43 H71 2 0.788262 0.109119 0.776534 11.00000 -1.20000 AFIX 0 C72 1 0.599221 0.095913 0.738181 11.00000 0.08660 0.05213 = 0.08805 0.03077 -0.03612 -0.03700 C73 1 0.472571 0.130796 0.768828 11.00000 0.12294 0.03212 = 0.05066 0.01096 -0.04491 -0.03171 C74 1 0.448395 0.168500 0.817715 11.00000 0.19566 0.04177 = 0.06786 0.01009 -0.05890 -0.03099 AFIX 43 H74 2 0.526910 0.175986 0.838248 11.00000 -1.20000 AFIX 0 C75 1 0.310744 0.194449 0.835635 11.00000 0.23396 0.04261 = 0.04404 -0.00953 -0.02574 -0.00451 AFIX 43 H75 2 0.296627 0.219969 0.868632 11.00000 -1.20000 AFIX 0 C76 1 0.187946 0.184663 0.806725 11.00000 0.16170 0.04874 = 0.06862 0.00165 0.01474 0.00378 AFIX 43 H76 2 0.094645 0.203610 0.820448 11.00000 -1.20000 AFIX 0 C77 1 0.206728 0.146062 0.756905 11.00000 0.10251 0.04846 = 0.05614 -0.00267 -0.00070 -0.00435 AFIX 43 H77 2 0.127861 0.139398 0.736365 11.00000 -1.20000 AFIX 0 C78 1 0.347643 0.118837 0.740333 11.00000 0.09078 0.03390 = 0.03583 0.00198 -0.01321 -0.01631 C79 1 0.252312 0.145734 0.489336 11.00000 0.07118 0.05689 = 0.03813 0.00228 -0.01240 -0.01133 C80 1 0.400168 0.118358 0.485852 11.00000 0.07042 0.07937 = 0.05419 -0.00350 -0.00115 -0.00336 AFIX 43 H80 2 0.449117 0.081108 0.511510 11.00000 -1.20000 AFIX 0 C81 1 0.474080 0.148055 0.442848 11.00000 0.08556 0.11153 = 0.05951 -0.00634 0.01039 -0.01939 AFIX 43 H81 2 0.574513 0.130474 0.439512 11.00000 -1.20000 AFIX 0 C82 1 0.401721 0.203052 0.404992 11.00000 0.11912 0.10298 = 0.06206 0.00174 0.00578 -0.03260 AFIX 43 H82 2 0.454331 0.222242 0.376581 11.00000 -1.20000 AFIX 0 C83 1 0.253774 0.230309 0.408116 11.00000 0.11136 0.07970 = 0.04133 0.01081 -0.01361 -0.03108 AFIX 43 H83 2 0.205870 0.267221 0.382111 11.00000 -1.20000 AFIX 0 C84 1 0.175823 0.201215 0.451560 11.00000 0.07541 0.05569 = 0.04837 -0.00309 -0.01831 -0.01671 C85 1 0.026731 0.217711 0.468501 11.00000 0.07760 0.04919 = 0.04871 0.00053 -0.03714 -0.01401 C86 1 -0.098561 0.270754 0.449544 11.00000 0.10055 0.07573 = 0.07817 0.00816 -0.04868 -0.01584 AFIX 43 H86 2 -0.094155 0.303991 0.418473 11.00000 -1.20000 AFIX 0 C87 1 -0.227620 0.274182 0.476319 11.00000 0.08032 0.08997 = 0.10650 -0.01066 -0.04520 0.00835 AFIX 43 H87 2 -0.310818 0.309880 0.463249 11.00000 -1.20000 AFIX 0 C88 1 -0.237478 0.225122 0.523035 11.00000 0.06757 0.10529 = 0.09319 -0.02195 -0.01499 -0.02001 AFIX 43 H88 2 -0.327108 0.227505 0.540455 11.00000 -1.20000 AFIX 0 C89 1 -0.113195 0.172398 0.543769 11.00000 0.06189 0.07103 = 0.07786 -0.01141 -0.02857 -0.00592 AFIX 43 H89 2 -0.117594 0.140094 0.575147 11.00000 -1.20000 AFIX 0 C90 1 0.015788 0.170211 0.515920 11.00000 0.05147 0.05615 = 0.05653 -0.01277 -0.01694 -0.01084 HKLF 4 REM gzy26a_0m_a.res in P-1 REM R1 = 0.0671 for 6401 Fo > 4sig(Fo) and 0.1530 for all 12027 data REM 892 parameters refined using 1 restraints END WGHT 0.0459 1.3743 REM Highest difference peak 0.215, deepest hole -0.289, 1-sigma level 0.046 Q1 1 -0.3096 0.2200 0.5611 11.00000 0.05 0.22 Q2 1 0.6777 0.1225 0.7743 11.00000 0.05 0.19 Q3 1 0.5059 0.4431 0.5996 11.00000 0.05 0.18 Q4 1 0.2289 0.2042 0.5922 11.00000 0.05 0.17 Q5 1 0.2644 0.2197 1.0088 11.00000 0.05 0.17 ; _shelx_res_checksum 56981 _shelx_hkl_file ; -1 0 0 275.57 17.60 1 0 0 260.57 17.60 1 0 0 298.47 17.70 -2 0 0 1926.71 112.29 -2 0 0 1818.92 112.49 -2 0 0 1740.53 112.19 2 0 0 1821.82 112.19 2 0 0 1777.52 112.19 2 0 0 1733.73 112.39 -3 0 0 56.69 5.20 -3 0 0 52.59 6.40 -3 0 0 67.49 5.50 3 0 0 63.49 6.00 3 0 0 59.39 5.60 3 0 0 65.99 5.20 -4 0 0 38.90 5.40 -4 0 0 30.90 4.40 -4 0 0 31.50 4.50 4 0 0 34.60 4.70 4 0 0 38.40 4.40 4 0 0 33.90 5.20 -5 0 0 150.78 11.60 -5 0 0 140.99 12.10 -5 0 0 121.49 12.20 5 0 0 140.49 12.00 5 0 0 147.49 12.00 5 0 0 159.48 11.20 5 0 0 152.08 11.60 -6 0 0 14.60 4.20 -6 0 0 16.90 4.50 6 0 0 18.20 4.10 6 0 0 22.80 5.20 6 0 0 13.50 4.90 6 0 0 13.80 3.90 -7 0 0 1.60 4.10 -7 0 0 4.20 3.90 7 0 0 4.90 3.70 7 0 0 -8.20 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12.20 -3 -6 0 14.10 4.40 -3 -6 0 13.60 3.10 3 6 0 12.60 1.90 3 6 0 15.00 2.20 3 6 0 15.80 2.90 3 6 0 16.50 4.30 -4 -6 0 8.10 3.10 4 6 0 18.70 4.50 4 6 0 14.50 2.70 4 6 0 8.60 2.20 4 6 0 14.50 4.90 4 6 0 13.00 3.20 -5 -6 0 20.60 5.00 5 6 0 25.30 4.00 5 6 0 26.80 5.90 5 6 0 27.90 4.20 5 6 0 28.80 5.90 5 6 0 30.00 4.80 -6 -6 0 32.60 5.90 6 6 0 34.40 7.30 6 6 0 38.90 7.00 6 6 0 45.00 5.60 6 6 0 43.40 6.30 6 6 0 37.00 5.70 -7 -6 0 9.40 5.10 7 6 0 -0.60 6.50 7 6 0 8.10 4.80 7 6 0 2.50 3.60 7 6 0 -4.90 4.00 7 6 0 0.60 5.30 8 6 0 29.30 8.50 8 6 0 21.30 6.70 8 6 0 20.10 5.60 8 6 0 20.80 7.40 9 6 0 18.80 7.00 9 6 0 33.90 9.50 9 6 0 36.10 8.80 10 6 0 -4.70 8.60 10 6 0 7.50 9.50 9 -7 0 -2.50 8.90 -9 7 0 2.60 8.20 -9 7 0 2.80 8.70 8 -7 0 3.80 7.50 -8 7 0 2.40 7.30 -8 7 0 2.90 6.00 7 -7 0 19.20 6.00 -7 7 0 5.90 5.60 -7 7 0 2.50 6.30 6 -7 0 8.70 6.20 6 -7 0 -5.00 4.60 -6 7 0 6.10 5.20 -6 7 0 5.10 4.30 5 -7 0 1.80 4.50 5 -7 0 4.80 5.90 5 -7 0 0.90 3.90 -5 7 0 3.10 4.00 -5 7 0 -1.40 4.20 4 -7 0 30.80 5.30 4 -7 0 35.60 5.70 4 -7 0 40.80 6.30 -4 7 0 17.40 5.00 -4 7 0 28.00 5.40 -4 7 0 40.30 6.20 3 -7 0 66.59 8.10 3 -7 0 52.39 6.30 3 -7 0 54.19 6.50 -3 7 0 54.29 7.20 -3 7 0 42.50 6.60 -3 7 0 52.69 6.40 2 -7 0 179.78 12.50 2 -7 0 146.19 11.70 2 -7 0 176.48 12.80 -2 7 0 144.59 12.20 -2 7 0 158.68 12.00 1 -7 0 7.60 3.50 1 -7 0 7.20 2.70 1 -7 0 6.30 2.70 -1 7 0 3.50 2.40 -1 7 0 5.10 3.10 -1 7 0 8.50 2.90 0 -7 0 76.49 7.80 0 -7 0 75.09 6.40 0 -7 0 81.29 5.70 0 7 0 67.59 5.70 0 7 0 72.19 7.50 0 7 0 75.29 6.60 -1 -7 0 82.09 7.70 -1 -7 0 84.49 5.30 -1 -7 0 80.09 6.40 1 7 0 63.49 5.40 1 7 0 80.09 6.50 1 7 0 72.09 7.30 -2 -7 0 600.34 43.30 -2 -7 0 648.84 42.00 -2 -7 0 660.43 41.00 2 7 0 619.54 43.20 2 7 0 648.64 40.90 2 7 0 755.12 42.00 -3 -7 0 33.00 4.30 -3 -7 0 26.30 5.70 3 7 0 34.60 6.00 3 7 0 33.60 3.10 3 7 0 30.30 2.70 3 7 0 30.60 4.00 -4 -7 0 1.80 3.30 -4 -7 0 3.50 2.60 4 7 0 -2.00 3.60 4 7 0 1.40 1.40 4 7 0 -6.80 3.80 4 7 0 0.10 2.30 4 7 0 1.80 1.90 -5 -7 0 5.10 3.60 5 7 0 8.10 2.60 5 7 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499.45 31.00 1 -8 0 106.19 8.00 1 -8 0 109.39 8.90 1 -8 0 105.89 9.80 -1 8 0 101.79 9.50 -1 8 0 117.59 8.40 -1 8 0 88.89 8.90 0 -8 0 91.19 6.40 0 -8 0 97.19 7.40 0 -8 0 76.69 8.70 0 8 0 85.99 7.50 0 8 0 81.09 8.30 0 8 0 76.49 6.40 -1 -8 0 29.90 4.30 -1 -8 0 32.90 2.70 -1 -8 0 32.40 5.80 1 8 0 28.70 2.90 1 8 0 32.60 5.60 1 8 0 29.50 4.20 -2 -8 0 9.10 3.90 -2 -8 0 11.40 1.60 -2 -8 0 14.20 3.10 2 8 0 14.50 2.90 2 8 0 8.00 4.20 2 8 0 10.10 1.50 -3 -8 0 -0.30 4.20 -3 -8 0 2.40 2.60 3 8 0 2.50 1.30 3 8 0 1.70 4.10 3 8 0 2.20 1.00 3 8 0 3.90 2.20 -4 -8 0 -0.80 2.80 -4 -8 0 7.00 4.60 4 8 0 -1.50 1.20 4 8 0 2.00 1.80 4 8 0 0.60 2.60 4 8 0 0.30 3.90 -5 -8 0 24.70 5.40 5 8 0 27.70 4.00 5 8 0 38.20 5.60 5 8 0 24.60 6.90 5 8 0 27.30 4.00 5 8 0 24.60 6.40 -6 -8 0 1.90 4.10 6 8 0 -4.50 6.30 6 8 0 2.90 3.50 6 8 0 6.20 3.00 6 8 0 -1.50 4.90 6 8 0 7.30 4.40 -7 -8 0 19.30 6.00 7 8 0 18.30 4.60 7 8 0 18.30 6.70 7 8 0 10.90 4.80 -8 -8 0 22.40 7.20 8 8 0 28.30 8.10 8 8 0 33.00 6.30 8 8 0 43.80 7.50 9 8 0 3.00 8.90 9 8 0 10.90 8.60 9 8 0 5.20 5.60 10 8 0 5.50 7.50 10 8 0 -7.50 9.70 8 -9 0 12.20 10.10 -8 9 0 16.30 7.60 7 -9 0 10.30 7.70 -7 9 0 16.20 6.80 -7 9 0 0.70 6.70 6 -9 0 31.20 8.40 6 -9 0 28.20 7.30 -6 9 0 28.40 7.60 -6 9 0 23.20 6.70 5 -9 0 33.80 7.20 5 -9 0 44.50 8.70 -5 9 0 50.99 8.20 -5 9 0 44.70 7.60 4 -9 0 10.70 4.60 4 -9 0 14.10 5.20 -4 9 0 6.30 5.30 -4 9 0 8.80 4.90 3 -9 0 8.20 3.90 3 -9 0 7.00 3.80 3 -9 0 9.50 4.50 -3 9 0 -2.40 3.60 -3 9 0 5.40 4.50 2 -9 0 43.10 5.90 2 -9 0 42.50 6.20 2 -9 0 44.70 7.40 -2 9 0 47.60 5.80 -2 9 0 52.19 7.50 -2 9 0 36.30 6.40 1 -9 0 232.98 16.10 1 -9 0 275.97 17.20 1 -9 0 228.58 18.10 -1 9 0 242.98 16.50 -1 9 0 233.68 17.90 -1 9 0 212.98 17.30 0 -9 0 24.10 3.00 0 -9 0 17.70 5.00 0 -9 0 29.80 4.20 0 9 0 18.50 3.00 0 9 0 25.50 5.20 0 9 0 22.20 4.50 -1 -9 0 55.39 5.30 -1 -9 0 43.40 3.60 -1 -9 0 41.90 7.20 1 9 0 52.09 7.00 1 9 0 39.10 3.80 1 9 0 54.59 5.50 -2 -9 0 14.40 3.60 -2 -9 0 10.50 1.50 -2 -9 0 10.00 4.20 2 9 0 12.30 1.70 2 9 0 12.30 3.80 2 9 0 13.60 3.40 -3 -9 0 203.38 14.90 -3 -9 0 182.88 16.80 3 9 0 204.28 13.00 3 9 0 181.68 16.10 3 9 0 223.98 13.20 -4 -9 0 15.20 4.10 -4 -9 0 20.40 6.00 4 9 0 17.20 2.50 4 9 0 14.00 3.60 4 9 0 16.40 4.90 4 9 0 12.80 1.90 -5 -9 0 41.20 6.70 5 9 0 60.09 5.10 5 9 0 55.49 6.00 5 9 0 50.39 8.70 5 9 0 74.89 6.90 -6 -9 0 -1.50 4.10 6 9 0 0.10 4.90 6 9 0 -2.50 2.40 6 9 0 -0.10 5.40 6 9 0 0.30 3.50 -7 -9 0 -3.30 4.70 7 9 0 -1.00 4.60 7 9 0 1.90 3.50 7 9 0 5.40 6.60 -8 -9 0 -5.00 5.60 8 9 0 6.10 7.40 8 9 0 1.60 5.60 8 9 0 -1.30 4.20 9 9 0 -2.70 10.80 9 9 0 6.60 10.20 9 9 0 -10.90 5.20 10 9 0 5.80 10.00 10 9 0 -15.90 6.70 10 9 0 22.00 10.90 7 -10 0 -2.50 7.40 -7 10 0 22.10 8.60 -7 10 0 -0.50 6.50 6 -10 0 13.70 7.60 6 -10 0 -4.80 6.90 -6 10 0 6.30 6.90 -6 10 0 2.20 5.50 5 -10 0 3.60 7.20 5 -10 0 2.60 5.70 -5 10 0 1.50 5.50 -5 10 0 -5.90 4.90 4 -10 0 4.80 6.00 4 -10 0 13.80 5.60 -4 10 0 18.20 5.30 -4 10 0 7.90 5.50 3 -10 0 0.50 5.30 3 -10 0 3.30 4.20 3 -10 0 -1.40 5.20 -3 10 0 4.50 4.10 -3 10 0 5.60 4.90 2 -10 0 3.80 4.20 2 -10 0 7.00 3.90 2 -10 0 3.80 5.20 -2 10 0 3.50 4.70 -2 10 0 0.40 3.50 1 -10 0 79.89 7.50 1 -10 0 57.79 6.70 1 -10 0 56.89 8.90 -1 10 0 62.99 6.30 -1 10 0 57.69 7.30 -1 10 0 57.39 8.00 0 -10 0 8.90 5.30 0 -10 0 0.60 2.80 0 10 0 -6.40 3.20 0 10 0 2.20 3.80 0 10 0 2.80 2.20 -1 -10 0 193.78 12.70 -1 -10 0 184.48 16.40 -1 -10 0 199.88 14.20 1 10 0 188.78 14.50 1 10 0 213.98 13.00 1 10 0 171.98 15.60 -2 -10 0 12.60 1.80 -2 -10 0 14.80 3.90 -2 -10 0 11.30 5.40 2 10 0 23.30 4.00 2 10 0 20.10 6.40 2 10 0 13.90 2.00 -3 -10 0 3.40 3.20 -3 -10 0 -3.80 5.90 3 10 0 5.60 4.70 3 10 0 4.00 1.30 3 10 0 -0.70 2.80 3 10 0 3.80 1.00 -4 -10 0 9.00 3.80 4 10 0 9.00 4.60 4 10 0 10.80 2.20 4 10 0 12.50 1.80 4 10 0 1.30 3.40 -5 -10 0 82.59 9.60 5 10 0 102.09 8.80 5 10 0 73.99 10.90 5 10 0 95.89 6.70 5 10 0 91.69 7.40 -6 -10 0 13.90 5.00 6 10 0 -3.50 5.90 6 10 0 3.70 3.60 6 10 0 7.00 2.70 -7 -10 0 -3.30 5.20 7 10 0 0.80 7.00 7 10 0 0.50 3.20 7 10 0 7.10 4.60 -8 -10 0 11.60 6.90 8 10 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11 0 60.89 5.00 5 11 0 68.99 10.60 -6 -11 0 -4.30 5.10 6 11 0 3.20 6.80 6 11 0 3.90 3.40 -7 -11 0 -3.00 6.10 7 11 0 1.30 7.50 7 11 0 -1.70 2.90 8 11 0 7.80 8.20 8 11 0 0.40 4.00 -9 -11 0 8.10 7.50 9 11 0 5.90 5.10 9 11 0 -14.00 9.30 6 -12 0 -9.80 8.00 -6 12 0 -2.70 7.70 -6 12 0 11.20 7.90 5 -12 0 5.50 6.60 -5 12 0 2.00 6.30 -5 12 0 9.50 6.60 4 -12 0 -4.20 6.20 -4 12 0 -3.30 5.20 -4 12 0 11.50 7.10 3 -12 0 47.90 7.50 3 -12 0 59.29 9.10 -3 12 0 57.39 8.40 2 -12 0 9.80 5.10 2 -12 0 6.60 4.40 -2 12 0 7.20 6.20 -2 12 0 4.10 4.40 1 -12 0 3.60 3.90 1 -12 0 5.40 3.30 -1 12 0 8.10 5.90 -1 12 0 6.00 3.60 0 -12 0 100.69 7.80 0 -12 0 116.89 9.70 0 12 0 87.99 8.50 0 12 0 99.79 11.20 -1 -12 0 50.29 4.30 -1 -12 0 55.09 6.80 1 12 0 53.69 4.80 1 12 0 50.99 8.70 -2 -12 0 30.20 5.60 -2 -12 0 33.90 2.60 2 12 0 36.60 7.90 2 12 0 31.40 2.60 -3 -12 0 3.10 4.20 3 12 0 7.30 5.60 -4 -12 0 11.40 4.90 4 12 0 11.20 6.70 -5 -12 0 34.20 6.90 5 12 0 28.90 2.80 5 12 0 28.30 3.20 5 12 0 35.40 8.80 -6 -12 0 48.50 8.60 6 12 0 48.30 5.20 6 12 0 47.50 4.50 -7 -12 0 3.40 6.10 7 12 0 -8.60 8.00 -8 -12 0 1.70 7.30 8 12 0 3.30 3.80 8 12 0 2.50 8.90 5 -13 0 3.80 7.70 -5 13 0 -5.90 8.80 -5 13 0 2.80 7.30 4 -13 0 10.30 6.80 -4 13 0 8.90 6.50 -4 13 0 11.80 8.30 3 -13 0 22.20 6.60 3 -13 0 42.80 8.00 -3 13 0 33.90 9.80 -3 13 0 36.40 6.70 2 -13 0 2.60 4.90 -2 13 0 12.00 4.80 -2 13 0 7.50 7.30 1 -13 0 13.70 5.20 1 -13 0 14.00 4.00 -1 13 0 8.80 4.10 -1 13 0 35.70 8.40 0 -13 0 7.80 4.60 0 -13 0 9.20 2.90 0 13 0 4.50 6.70 0 13 0 4.60 3.30 -1 -13 0 14.20 4.60 -1 -13 0 6.10 1.90 1 13 0 7.10 6.60 1 13 0 8.40 2.40 -2 -13 0 72.19 8.30 2 13 0 67.79 11.30 -3 -13 0 17.60 5.30 3 13 0 20.10 7.80 -4 -13 0 -0.10 4.80 4 13 0 2.40 8.00 -5 -13 0 10.70 6.10 5 13 0 17.60 8.20 -6 -13 0 12.00 6.30 6 13 0 17.80 8.80 -7 -13 0 5.40 7.20 7 13 0 -8.00 8.00 -8 -13 0 3.20 8.30 8 13 0 -14.40 8.60 5 -14 0 -1.60 8.30 -5 14 0 -0.40 9.40 -5 14 0 22.90 9.00 4 -14 0 5.20 6.70 -4 14 0 -0.90 16.50 -4 14 0 0.80 7.10 3 -14 0 3.90 6.40 -3 14 0 14.40 6.00 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6.10 2 -11 3 6.90 4.30 -3 11 -3 9.20 5.20 -3 11 -3 9.40 6.00 3 -11 3 7.40 5.10 3 -11 3 9.60 6.10 3 -11 3 9.20 5.10 -4 11 -3 22.00 6.20 4 -11 3 30.70 7.40 4 -11 3 16.00 6.90 -5 11 -3 16.90 7.20 -5 11 -3 8.30 6.10 5 -11 3 18.10 7.20 5 -11 3 21.80 7.40 -6 11 -3 13.60 8.20 -6 11 -3 -1.30 6.00 6 -11 3 6.20 7.70 -7 11 -3 13.20 7.30 -7 11 -3 -0.20 8.50 7 -11 3 4.90 9.10 9 10 -3 -5.40 9.20 9 10 -3 1.20 5.20 9 10 -3 3.90 10.10 8 10 -3 6.00 4.60 8 10 -3 -1.80 8.10 8 10 -3 16.50 6.10 -8 -10 3 7.50 6.40 7 10 -3 17.40 4.50 7 10 -3 27.10 5.90 7 10 -3 23.50 8.80 -7 -10 3 16.80 6.30 6 10 -3 4.20 3.80 6 10 -3 4.80 4.30 6 10 -3 0.10 6.80 6 10 -3 5.80 3.00 -6 -10 3 0.00 4.20 5 10 -3 198.78 14.80 5 10 -3 231.58 18.90 5 10 -3 213.18 15.20 -5 -10 3 195.38 16.00 4 10 -3 3.80 2.40 4 10 -3 2.50 5.50 4 10 -3 -1.80 2.70 -4 -10 3 11.60 3.80 3 10 -3 26.10 4.50 3 10 -3 37.10 7.40 3 10 -3 36.40 3.60 -3 -10 3 30.90 5.20 -3 -10 3 37.30 4.00 2 10 -3 43.60 5.90 2 10 -3 52.59 4.40 2 10 -3 44.20 7.30 -2 -10 3 45.30 4.20 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9 -3 3.10 3.70 7 9 -3 10.00 7.30 7 9 -3 13.00 5.50 -7 -9 3 5.30 4.70 6 9 -3 53.69 5.70 6 9 -3 55.99 7.00 6 9 -3 46.20 6.40 6 9 -3 51.09 9.60 -6 -9 3 38.00 6.90 5 9 -3 34.90 7.60 5 9 -3 36.40 5.30 5 9 -3 32.50 4.20 5 9 -3 36.20 5.20 -5 -9 3 26.80 5.40 4 9 -3 62.39 6.00 4 9 -3 64.09 5.70 4 9 -3 56.79 9.40 4 9 -3 57.99 9.10 -4 -9 3 50.99 6.40 3 9 -3 8.20 2.90 3 9 -3 10.00 1.90 3 9 -3 7.40 4.90 3 9 -3 1.60 5.40 -3 -9 3 8.50 3.00 -3 -9 3 16.60 5.80 -3 -9 3 11.30 2.40 2 9 -3 106.39 7.20 2 9 -3 112.09 10.50 2 9 -3 95.69 8.10 -2 -9 3 81.09 10.30 -2 -9 3 95.29 8.00 -2 -9 3 91.79 7.00 1 9 -3 21.80 4.80 1 9 -3 24.80 3.30 1 9 -3 25.90 4.20 -1 -9 3 25.80 5.50 -1 -9 3 23.10 3.20 -1 -9 3 26.40 4.00 0 9 -3 25.40 5.40 0 9 -3 22.60 4.30 0 9 -3 18.50 3.50 0 -9 3 27.80 4.00 0 -9 3 21.80 5.80 0 -9 3 22.60 3.30 -1 9 -3 4.20 2.90 -1 9 -3 4.70 3.80 -1 9 -3 0.50 3.80 1 -9 3 9.20 4.40 1 -9 3 7.80 2.90 1 -9 3 2.10 2.80 -2 9 -3 48.50 7.00 -2 9 -3 58.09 6.60 -2 9 -3 42.90 6.70 2 -9 3 51.59 6.30 2 -9 3 61.69 6.80 2 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-1.50 4.30 3 8 -3 -4.40 4.10 3 8 -3 0.30 1.30 3 8 -3 -4.70 1.80 -3 -8 3 0.10 1.80 -3 -8 3 -0.30 2.30 -3 -8 3 0.80 4.30 2 8 -3 175.68 12.50 2 8 -3 178.78 11.90 2 8 -3 183.78 14.60 -2 -8 3 176.38 11.90 -2 -8 3 176.18 14.40 -2 -8 3 180.58 12.60 1 8 -3 20.50 5.00 1 8 -3 22.50 3.60 1 8 -3 20.70 3.00 -1 -8 3 22.70 3.40 -1 -8 3 26.40 5.40 -1 -8 3 25.60 2.80 0 8 -3 76.99 7.90 0 8 -3 75.19 6.80 0 -8 3 70.69 5.80 0 -8 3 75.09 8.40 0 -8 3 74.29 6.50 -1 8 -3 32.70 4.60 -1 8 -3 26.90 4.90 -1 8 -3 33.30 5.00 1 -8 3 25.90 5.50 1 -8 3 32.80 3.90 1 -8 3 30.70 4.60 -2 8 -3 177.88 14.60 -2 8 -3 186.08 14.50 -2 8 -3 187.98 14.00 2 -8 3 174.28 14.90 2 -8 3 220.68 14.80 2 -8 3 203.68 14.00 -3 8 -3 43.70 7.00 -3 8 -3 47.30 7.00 -3 8 -3 50.89 6.40 3 -8 3 41.40 6.70 3 -8 3 52.09 6.20 3 -8 3 46.80 6.90 -4 8 -3 14.50 4.90 -4 8 -3 18.00 5.10 4 -8 3 25.20 4.90 4 -8 3 26.60 5.90 4 -8 3 23.20 5.20 -5 8 -3 8.70 4.30 -5 8 -3 8.40 5.20 5 -8 3 15.00 4.90 5 -8 3 7.30 5.60 -6 8 -3 7.90 6.20 -6 8 -3 -6.00 4.50 6 -8 3 8.40 4.90 -7 8 -3 28.20 5.90 -7 8 -3 27.00 7.80 7 -8 3 18.10 5.50 7 -8 3 10.10 8.20 -8 8 -3 9.00 8.10 -8 8 -3 -0.60 5.70 8 -8 3 -3.50 8.40 10 7 -3 15.00 7.20 10 7 -3 7.60 11.00 10 7 -3 14.20 11.10 9 7 -3 4.90 8.70 9 7 -3 -6.50 5.40 9 7 -3 -0.50 8.10 8 7 -3 16.00 7.90 8 7 -3 33.10 6.10 8 7 -3 34.80 8.20 7 7 -3 150.28 13.10 7 7 -3 152.08 12.60 7 7 -3 165.38 16.30 7 7 -3 149.39 13.10 -7 -7 3 140.49 13.50 6 7 -3 4.10 5.50 6 7 -3 -1.40 3.30 6 7 -3 1.30 3.80 6 7 -3 3.90 3.10 6 7 -3 -8.70 5.90 -6 -7 3 2.50 3.50 5 7 -3 77.89 7.10 5 7 -3 77.59 6.90 5 7 -3 69.69 10.20 5 7 -3 68.79 6.20 5 7 -3 80.99 9.50 -5 -7 3 51.89 7.20 4 7 -3 11.70 2.60 4 7 -3 7.70 2.20 4 7 -3 1.20 4.20 4 7 -3 5.30 2.40 4 7 -3 13.10 5.10 -4 -7 3 7.60 2.80 3 7 -3 5.80 4.40 3 7 -3 -3.20 3.20 3 7 -3 -0.40 1.70 3 7 -3 -1.00 1.20 -3 -7 3 1.80 1.80 -3 -7 3 0.50 2.00 2 7 -3 25.90 9.20 2 7 -3 21.50 2.50 2 7 -3 29.50 3.60 -2 -7 3 25.10 5.20 -2 -7 3 25.60 3.80 -2 -7 3 17.60 2.70 1 7 -3 436.96 29.40 1 7 -3 408.46 27.90 1 7 -3 430.66 27.50 -1 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7.20 9 6 -3 1.40 5.60 9 6 -3 -0.90 8.40 8 6 -3 4.40 7.20 8 6 -3 4.40 6.70 8 6 -3 5.30 5.10 7 6 -3 13.90 5.30 7 6 -3 13.80 5.50 7 6 -3 15.50 7.20 7 6 -3 6.80 5.80 7 6 -3 5.20 7.20 7 6 -3 3.00 3.80 6 6 -3 11.30 3.50 6 6 -3 1.40 3.40 6 6 -3 4.60 5.40 6 6 -3 1.60 3.20 6 6 -3 1.70 6.20 -6 -6 3 -0.50 3.60 5 6 -3 26.30 4.20 5 6 -3 12.80 5.70 5 6 -3 22.00 6.00 5 6 -3 22.10 3.60 5 6 -3 24.50 4.10 -5 -6 3 23.40 4.30 4 6 -3 24.90 3.30 4 6 -3 32.10 6.00 4 6 -3 28.70 4.00 4 6 -3 22.30 5.80 4 6 -3 34.80 3.90 -4 -6 3 31.30 4.50 3 6 -3 208.18 13.20 3 6 -3 193.18 15.50 3 6 -3 216.08 15.70 3 6 -3 187.98 12.80 -3 -6 3 180.68 13.10 -3 -6 3 184.78 13.40 2 6 -3 16.90 4.10 2 6 -3 18.80 2.70 2 6 -3 12.50 3.90 2 6 -3 16.90 2.10 -2 -6 3 14.70 2.20 -2 -6 3 13.90 4.20 -2 -6 3 14.50 3.20 1 6 -3 955.10 57.19 1 6 -3 889.81 55.69 1 6 -3 892.11 55.39 -1 -6 3 788.02 55.89 -1 -6 3 914.31 55.29 -1 -6 3 869.11 57.09 0 6 -3 1.10 1.60 0 6 -3 1.40 2.00 0 6 -3 0.10 2.70 0 -6 3 -0.40 1.80 0 -6 3 3.20 3.10 0 -6 3 -0.20 1.40 -1 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5.50 5.20 4 13 -4 3.90 7.30 4 13 -4 -2.50 3.00 -4 -13 4 -1.10 4.60 3 13 -4 11.50 6.40 -3 -13 4 26.30 3.80 -3 -13 4 15.00 5.40 2 13 -4 1.60 3.10 2 13 -4 -3.70 6.50 -2 -13 4 2.80 2.70 -2 -13 4 4.20 4.00 1 13 -4 3.70 6.60 1 13 -4 2.90 3.50 -1 -13 4 -3.80 2.80 -1 -13 4 -1.20 4.00 0 13 -4 0.50 3.70 0 13 -4 7.30 6.00 0 -13 4 4.70 4.00 0 -13 4 3.90 3.40 -1 13 -4 0.70 5.70 -1 13 -4 11.60 4.70 1 -13 4 11.40 4.10 1 -13 4 0.10 4.60 -2 13 -4 2.30 6.10 -2 13 -4 6.30 5.30 2 -13 4 6.40 5.80 2 -13 4 6.10 4.90 -3 13 -4 4.10 7.50 -3 13 -4 8.00 5.30 3 -13 4 9.10 6.00 -4 13 -4 25.70 8.80 -4 13 -4 18.60 7.90 4 -13 4 16.30 7.60 -5 13 -4 -13.00 7.50 -5 13 -4 2.90 8.00 5 -13 4 15.80 8.60 8 12 -4 0.10 4.30 8 12 -4 2.70 9.70 -8 -12 4 20.60 7.80 7 12 -4 -0.10 8.70 7 12 -4 -8.60 3.40 -7 -12 4 7.50 6.30 6 12 -4 5.10 3.10 6 12 -4 20.10 4.70 6 12 -4 20.70 8.90 -6 -12 4 -0.20 5.30 5 12 -4 45.70 11.60 5 12 -4 29.00 5.10 5 12 -4 36.60 4.80 -5 -12 4 34.20 6.50 4 12 -4 40.70 6.50 4 12 -4 51.49 5.30 4 12 -4 39.40 5.50 4 12 -4 58.59 10.20 -4 -12 4 43.70 6.70 3 12 -4 83.89 11.90 3 12 -4 74.19 8.50 -3 -12 4 81.49 8.90 -3 -12 4 94.09 7.20 2 12 -4 12.40 6.10 2 12 -4 13.00 3.30 2 12 -4 9.70 4.40 -2 -12 4 6.60 2.60 -2 -12 4 11.50 4.20 1 12 -4 82.89 7.60 1 12 -4 87.99 10.90 -1 -12 4 74.79 6.80 -1 -12 4 83.49 8.40 0 12 -4 1.40 3.30 0 12 -4 6.20 5.80 0 -12 4 2.60 3.30 0 -12 4 3.40 3.00 -1 12 -4 54.99 8.90 -1 12 -4 55.39 7.20 1 -12 4 59.99 7.90 1 -12 4 45.50 6.40 -2 12 -4 -5.60 5.60 -2 12 -4 1.90 4.80 2 -12 4 2.20 4.40 2 -12 4 1.90 4.40 -3 12 -4 204.38 16.00 -3 12 -4 167.08 17.50 3 -12 4 226.58 17.20 -4 12 -4 0.60 6.40 -4 12 -4 -0.60 6.30 4 -12 4 -7.50 5.70 -5 12 -4 25.80 7.80 -5 12 -4 23.50 8.30 5 -12 4 22.30 7.90 -6 12 -4 6.10 8.90 -6 12 -4 -4.90 6.70 6 -12 4 -7.00 7.40 9 11 -4 -2.60 5.50 9 11 -4 -0.80 10.10 -9 -11 4 1.40 9.60 8 11 -4 -2.80 4.60 8 11 -4 13.80 9.70 -8 -11 4 -3.50 6.70 7 11 -4 5.80 3.50 7 11 -4 11.80 8.40 7 11 -4 -2.20 5.00 -7 -11 4 10.30 6.00 6 11 -4 10.50 4.50 6 11 -4 12.00 8.20 -6 -11 4 9.30 4.80 5 11 -4 0.20 2.50 5 11 -4 -5.30 6.40 5 11 -4 4.20 3.60 5 11 -4 11.10 4.00 -5 -11 4 5.80 4.10 4 11 -4 1.20 2.20 4 11 -4 -8.30 5.40 4 11 -4 -2.80 2.80 4 11 -4 -0.60 3.20 -4 -11 4 3.00 3.80 3 11 -4 4.10 3.70 3 11 -4 2.70 4.70 -3 -11 4 1.00 3.40 -3 -11 4 4.90 2.60 2 11 -4 2.60 4.40 2 11 -4 1.30 5.10 2 11 -4 1.10 3.50 -2 -11 4 5.50 3.20 -2 -11 4 5.00 2.30 1 11 -4 19.60 6.10 1 11 -4 14.90 3.60 1 11 -4 14.20 4.40 -1 -11 4 15.80 3.90 -1 -11 4 19.90 3.20 0 11 -4 -1.60 2.90 0 11 -4 5.10 5.00 0 11 -4 -0.10 3.80 0 -11 4 4.50 6.00 0 -11 4 7.20 3.20 0 -11 4 5.10 2.70 -1 11 -4 -0.60 3.60 -1 11 -4 -3.20 4.70 1 -11 4 3.70 3.70 1 -11 4 -3.30 3.20 1 -11 4 1.50 5.70 -2 11 -4 16.10 5.70 -2 11 -4 19.50 5.40 2 -11 4 21.60 4.60 2 -11 4 21.90 5.30 2 -11 4 28.90 6.50 -3 11 -4 5.90 4.90 -3 11 -4 9.30 6.00 3 -11 4 1.10 4.40 3 -11 4 9.50 6.70 3 -11 4 0.20 4.90 -4 11 -4 25.30 6.60 -4 11 -4 1.90 5.10 4 -11 4 15.00 6.80 4 -11 4 5.70 5.90 -5 11 -4 11.00 6.30 -5 11 -4 28.00 7.80 5 -11 4 3.80 6.50 5 -11 4 28.80 7.80 -6 11 -4 4.50 6.00 -6 11 -4 11.90 8.10 6 -11 4 -2.90 7.50 -7 11 -4 8.50 9.10 -7 11 -4 15.50 8.00 9 10 -4 -7.20 5.20 9 10 -4 14.20 9.60 9 10 -4 1.40 9.10 8 10 -4 13.50 6.90 8 10 -4 2.10 8.70 8 10 -4 10.50 4.60 -8 -10 4 -4.00 6.30 7 10 -4 -4.30 5.10 7 10 -4 3.70 3.70 7 10 -4 6.10 8.10 -7 -10 4 -5.60 4.90 6 10 -4 3.00 2.80 6 10 -4 11.20 7.50 6 10 -4 4.60 4.20 6 10 -4 -4.50 4.00 -6 -10 4 1.60 4.20 5 10 -4 65.69 5.90 5 10 -4 65.99 7.00 5 10 -4 67.79 11.10 5 10 -4 85.09 7.60 -5 -10 4 50.89 8.00 4 10 -4 55.99 6.20 4 10 -4 58.19 9.50 4 10 -4 49.60 4.90 4 10 -4 48.10 5.40 -4 -10 4 53.39 6.70 3 10 -4 289.37 20.30 3 10 -4 324.17 29.30 -3 -10 4 296.97 20.70 -3 -10 4 297.87 19.70 2 10 -4 10.80 3.70 2 10 -4 14.70 5.90 -2 -10 4 14.80 5.90 -2 -10 4 15.50 2.70 -2 -10 4 15.40 3.60 1 10 -4 38.40 5.90 1 10 -4 36.00 4.60 1 10 -4 36.00 6.80 -1 -10 4 41.20 7.50 -1 -10 4 41.30 5.00 0 10 -4 87.89 9.10 0 10 -4 100.99 8.50 0 10 -4 112.49 10.60 0 -10 4 80.29 11.60 0 -10 4 116.59 8.90 0 -10 4 104.29 7.90 -1 10 -4 0.00 4.50 -1 10 -4 2.50 3.30 -1 10 -4 2.20 4.10 1 -10 4 0.10 4.70 1 -10 4 6.10 3.30 1 -10 4 7.60 2.90 -2 10 -4 77.29 8.40 -2 10 -4 89.99 9.50 2 -10 4 77.69 10.50 2 -10 4 78.19 8.20 2 -10 4 98.49 9.40 -3 10 -4 11.40 5.50 -3 10 -4 10.60 4.60 3 -10 4 6.10 5.50 3 -10 4 6.10 4.20 3 -10 4 11.70 4.90 -4 10 -4 4.90 4.90 -4 10 -4 2.50 5.50 4 -10 4 7.50 6.00 4 -10 4 2.90 4.90 -5 10 -4 31.30 7.60 -5 10 -4 38.90 7.00 5 -10 4 17.60 6.70 -6 10 -4 14.20 9.50 -6 10 -4 36.50 6.80 6 -10 4 37.80 8.80 6 -10 4 26.70 7.80 -7 10 -4 4.70 6.20 -7 10 -4 5.70 7.90 7 -10 4 13.20 8.30 9 9 -4 16.50 9.00 9 9 -4 -1.50 8.70 9 9 -4 11.60 5.50 8 9 -4 21.80 5.00 8 9 -4 8.80 8.70 -8 -9 4 22.90 7.20 7 9 -4 6.50 5.40 7 9 -4 -1.00 5.10 7 9 -4 0.90 3.70 7 9 -4 14.40 7.90 -7 -9 4 2.50 4.70 6 9 -4 81.49 8.40 6 9 -4 87.29 7.40 6 9 -4 77.89 11.90 6 9 -4 78.69 8.20 -6 -9 4 70.59 9.30 5 9 -4 11.20 2.70 5 9 -4 7.20 3.10 5 9 -4 23.90 6.10 5 9 -4 13.70 3.70 -5 -9 4 14.00 4.50 4 9 -4 29.00 4.00 4 9 -4 37.00 7.10 4 9 -4 21.40 7.80 4 9 -4 25.60 3.40 4 9 -4 24.30 4.10 -4 -9 4 24.50 4.70 3 9 -4 60.99 8.20 3 9 -4 73.89 9.80 3 9 -4 67.69 6.30 -3 -9 4 66.99 5.70 -3 -9 4 56.89 6.40 2 9 -4 6.10 4.00 2 9 -4 11.60 2.50 2 9 -4 11.20 3.10 -2 -9 4 14.00 3.20 -2 -9 4 10.70 5.20 -2 -9 4 9.30 2.40 1 9 -4 103.59 8.90 1 9 -4 104.89 10.50 -1 -9 4 107.39 11.10 -1 -9 4 111.69 7.80 -1 -9 4 101.59 8.40 0 9 -4 3.10 2.70 0 9 -4 1.30 3.80 0 9 -4 0.90 3.00 0 -9 4 5.60 2.70 0 -9 4 5.40 2.30 0 -9 4 -2.90 4.00 -1 9 -4 9.90 4.00 -1 9 -4 10.80 4.00 -1 9 -4 14.30 3.50 1 -9 4 8.40 4.60 1 -9 4 13.80 3.80 1 -9 4 13.90 3.40 -2 9 -4 -4.30 3.90 -2 9 -4 -1.70 3.30 -2 9 -4 -1.70 3.80 2 -9 4 -4.90 2.80 2 -9 4 0.80 3.30 2 -9 4 -7.70 3.70 -3 9 -4 12.70 4.40 -3 9 -4 11.00 4.70 3 -9 4 13.70 4.70 3 -9 4 16.00 4.90 3 -9 4 8.10 4.40 -4 9 -4 10.90 5.50 -4 9 -4 19.80 5.60 4 -9 4 17.10 5.40 4 -9 4 26.60 6.60 4 -9 4 22.60 8.70 -5 9 -4 3.00 5.30 -5 9 -4 -3.80 4.60 5 -9 4 17.70 6.80 5 -9 4 -3.10 4.90 -6 9 -4 4.50 4.70 -6 9 -4 5.40 6.40 6 -9 4 7.40 6.60 6 -9 4 19.60 5.90 -7 9 -4 2.50 5.00 -7 9 -4 1.50 7.20 7 -9 4 -5.10 7.20 -8 9 -4 9.40 6.30 8 -9 4 -2.30 8.40 10 8 -4 -4.30 10.90 10 8 -4 4.40 10.90 10 8 -4 6.70 7.70 9 8 -4 4.10 15.50 9 8 -4 7.80 8.70 9 8 -4 -0.10 5.60 8 8 -4 16.40 7.20 8 8 -4 -0.10 4.10 8 8 -4 -8.50 7.00 7 8 -4 27.50 5.50 7 8 -4 29.70 5.80 7 8 -4 34.90 9.20 7 8 -4 34.30 6.20 -7 -8 4 21.50 5.80 6 8 -4 41.60 5.70 6 8 -4 44.80 6.10 6 8 -4 52.69 9.30 6 8 -4 50.59 6.80 -6 -8 4 38.20 6.70 5 8 -4 -0.50 3.10 5 8 -4 4.30 5.90 5 8 -4 2.00 2.30 5 8 -4 2.40 4.70 5 8 -4 1.50 2.80 -5 -8 4 2.50 3.30 4 8 -4 3.10 2.60 4 8 -4 5.90 4.10 4 8 -4 4.10 5.50 4 8 -4 -1.50 1.80 4 8 -4 0.30 2.10 -4 -8 4 1.60 2.70 3 8 -4 0.90 1.80 3 8 -4 2.00 3.30 3 8 -4 10.80 4.80 3 8 -4 2.00 2.10 -3 -8 4 -0.50 2.30 -3 -8 4 1.10 2.00 2 8 -4 30.50 3.40 2 8 -4 32.70 6.40 2 8 -4 39.30 4.40 -2 -8 4 31.70 6.30 -2 -8 4 41.70 4.40 1 8 -4 115.39 9.10 1 8 -4 129.89 11.00 1 8 -4 113.09 8.50 -1 -8 4 130.49 9.00 -1 -8 4 114.59 10.60 -1 -8 4 105.99 8.70 0 8 -4 130.39 10.70 0 8 -4 135.59 10.10 0 8 -4 135.89 11.60 0 -8 4 140.29 9.80 0 -8 4 133.79 11.90 0 -8 4 146.89 10.30 -1 8 -4 281.47 20.50 -1 8 -4 268.77 20.70 -1 8 -4 295.97 20.00 1 -8 4 306.27 19.80 1 -8 4 309.57 21.60 1 -8 4 313.67 20.40 -2 8 -4 4.60 3.20 -2 8 -4 0.80 2.80 -2 8 -4 3.40 3.50 2 -8 4 5.50 3.60 2 -8 4 5.60 3.00 2 -8 4 7.30 3.50 -3 8 -4 101.39 10.70 -3 8 -4 96.59 9.50 -3 8 -4 112.69 10.00 3 -8 4 109.79 9.40 3 -8 4 102.49 9.90 3 -8 4 122.69 10.40 -4 8 -4 42.90 6.50 -4 8 -4 31.50 6.10 4 -8 4 39.70 6.90 4 -8 4 37.60 5.90 4 -8 4 35.10 5.70 -5 8 -4 9.30 5.50 -5 8 -4 4.50 3.90 5 -8 4 3.30 4.30 5 -8 4 3.00 5.50 -6 8 -4 0.80 6.00 6 -8 4 -1.70 4.60 6 -8 4 11.90 6.70 -7 8 -4 3.80 7.00 -7 8 -4 0.60 4.30 7 -8 4 2.10 8.40 -8 8 -4 -11.90 7.50 -8 8 -4 8.60 6.70 8 -8 4 -0.80 8.00 10 7 -4 13.70 7.30 10 7 -4 10.40 11.20 9 7 -4 19.00 8.80 9 7 -4 3.30 8.90 9 7 -4 6.20 5.50 8 7 -4 -1.10 6.20 8 7 -4 3.80 4.70 8 7 -4 9.40 7.40 7 7 -4 2.90 5.80 7 7 -4 11.10 4.50 7 7 -4 17.30 5.30 7 7 -4 9.10 4.40 7 7 -4 17.10 7.40 -7 -7 4 11.80 5.40 6 7 -4 21.60 4.00 6 7 -4 11.30 6.00 6 7 -4 32.10 9.60 6 7 -4 21.00 4.30 6 7 -4 29.70 5.00 -6 -7 4 15.50 5.10 5 7 -4 55.69 9.60 5 7 -4 59.89 5.50 5 7 -4 52.39 8.90 5 7 -4 67.29 6.00 5 7 -4 55.79 6.00 -5 -7 4 59.79 6.80 4 7 -4 -2.40 2.00 4 7 -4 -3.80 3.90 4 7 -4 1.60 2.40 4 7 -4 3.20 1.90 4 7 -4 9.60 5.10 -4 -7 4 1.10 2.40 3 7 -4 355.36 21.50 3 7 -4 325.17 24.00 3 7 -4 338.57 21.20 3 7 -4 299.27 23.60 -3 -7 4 315.07 21.70 -3 -7 4 321.07 21.40 2 7 -4 49.80 7.30 2 7 -4 38.40 6.60 2 7 -4 45.10 4.40 2 7 -4 43.90 3.80 -2 -7 4 43.40 6.80 -2 -7 4 41.30 4.50 -2 -7 4 39.70 3.90 1 7 -4 160.48 13.10 1 7 -4 164.38 11.10 1 7 -4 154.28 11.40 -1 -7 4 169.88 10.90 -1 -7 4 154.18 13.20 0 7 -4 3.90 2.50 0 7 -4 4.60 3.30 0 -7 4 4.90 3.70 0 -7 4 4.50 2.00 0 -7 4 3.00 2.00 -1 7 -4 178.38 13.90 -1 7 -4 162.08 13.00 -1 7 -4 167.08 13.50 1 -7 4 199.48 14.30 1 -7 4 219.18 13.60 1 -7 4 193.38 13.00 -2 7 -4 13.70 4.00 -2 7 -4 18.20 4.00 -2 7 -4 19.90 3.80 2 -7 4 17.00 4.10 2 -7 4 15.10 3.90 2 -7 4 13.90 3.40 -3 7 -4 7.80 4.10 -3 7 -4 11.60 3.90 -3 7 -4 12.20 3.90 3 -7 4 13.10 3.80 3 -7 4 16.40 3.80 3 -7 4 11.40 4.00 -4 7 -4 45.80 6.80 -4 7 -4 28.50 6.50 -4 7 -4 51.69 6.80 4 -7 4 52.19 6.20 4 -7 4 49.50 6.80 4 -7 4 54.99 7.50 -5 7 -4 -0.40 4.30 -5 7 -4 -5.80 3.10 5 -7 4 6.00 5.30 5 -7 4 0.60 3.50 -6 7 -4 0.30 3.30 -6 7 -4 -2.60 5.10 6 -7 4 0.50 3.90 6 -7 4 1.70 5.80 -7 7 -4 0.10 4.00 7 -7 4 13.00 6.80 7 -7 4 -1.60 4.10 -8 7 -4 14.40 7.90 -8 7 -4 4.10 4.80 8 -7 4 -4.80 7.60 -9 7 -4 4.00 8.80 9 -7 4 1.70 10.00 10 6 -4 -0.60 6.80 9 6 -4 52.79 8.80 9 6 -4 48.40 10.70 9 6 -4 64.79 12.50 8 6 -4 0.60 5.90 8 6 -4 4.10 4.60 8 6 -4 2.30 7.00 7 6 -4 26.60 6.40 7 6 -4 35.90 6.90 7 6 -4 18.60 7.60 7 6 -4 26.60 5.60 7 6 -4 24.20 5.70 6 6 -4 40.40 6.10 6 6 -4 43.20 5.70 6 6 -4 31.20 7.60 6 6 -4 29.60 7.70 6 6 -4 45.00 6.30 -6 -6 4 33.20 5.80 5 6 -4 129.79 10.10 5 6 -4 146.79 10.00 5 6 -4 132.39 12.90 5 6 -4 136.89 10.10 5 6 -4 110.89 12.10 -5 -6 4 106.69 10.20 4 6 -4 242.48 17.20 4 6 -4 279.97 17.30 4 6 -4 251.57 19.50 4 6 -4 253.57 19.60 4 6 -4 262.57 17.10 -4 -6 4 238.48 17.50 3 6 -4 79.29 6.20 3 6 -4 78.99 9.00 3 6 -4 88.19 6.30 3 6 -4 76.99 8.80 -3 -6 4 68.99 6.50 -3 -6 4 84.59 6.50 2 6 -4 117.79 8.00 2 6 -4 115.09 8.30 2 6 -4 121.69 10.40 -2 -6 4 116.39 8.90 -2 -6 4 109.39 8.10 1 6 -4 370.16 23.80 1 6 -4 368.16 25.30 1 6 -4 366.36 23.50 -1 -6 4 350.96 25.20 -1 -6 4 374.26 23.40 0 6 -4 51.29 4.90 0 6 -4 41.60 4.30 0 6 -4 45.90 5.80 0 -6 4 51.09 4.50 0 -6 4 42.20 4.40 0 -6 4 49.30 6.10 -1 6 -4 -1.20 2.30 -1 6 -4 -1.00 2.40 -1 6 -4 -0.10 2.00 1 -6 4 0.90 2.80 1 -6 4 1.20 2.50 1 -6 4 1.80 2.10 -2 6 -4 61.59 7.00 -2 6 -4 72.29 6.70 -2 6 -4 69.59 6.60 2 -6 4 78.99 6.60 2 -6 4 73.09 7.00 2 -6 4 75.19 7.00 -3 6 -4 44.90 5.50 -3 6 -4 31.00 5.50 -3 6 -4 36.00 5.80 3 -6 4 34.20 5.60 3 -6 4 43.60 5.40 3 -6 4 45.60 5.20 -4 6 -4 -0.40 3.40 -4 6 -4 3.50 4.50 -4 6 -4 7.20 3.20 4 -6 4 5.50 3.40 4 -6 4 0.90 2.70 4 -6 4 7.00 4.10 -5 6 -4 -4.40 3.60 -5 6 -4 3.50 3.00 5 -6 4 11.50 3.70 5 -6 4 4.10 3.10 5 -6 4 8.90 4.80 -6 6 -4 0.20 3.30 -6 6 -4 -3.10 4.90 6 -6 4 2.90 3.30 6 -6 4 11.50 6.00 -7 6 -4 -7.90 3.70 -7 6 -4 3.10 6.00 7 -6 4 2.30 3.50 7 -6 4 1.70 6.40 -8 6 -4 19.90 5.30 -8 6 -4 27.50 8.10 8 -6 4 28.20 8.80 -9 6 -4 7.90 8.10 9 -6 4 17.40 9.90 10 5 -4 -2.90 6.40 10 5 -4 1.00 11.50 10 5 -4 21.20 10.80 9 5 -4 33.50 9.70 9 5 -4 30.60 7.40 9 5 -4 48.30 9.50 8 5 -4 -0.60 4.30 8 5 -4 -2.40 6.50 8 5 -4 0.10 6.10 7 5 -4 10.10 6.60 7 5 -4 20.30 4.90 7 5 -4 24.60 5.70 7 5 -4 14.80 5.40 7 5 -4 21.60 5.40 7 5 -4 15.60 7.20 6 5 -4 27.40 6.70 6 5 -4 20.60 4.70 6 5 -4 10.00 6.00 6 5 -4 17.80 4.10 6 5 -4 13.50 5.30 6 5 -4 17.60 4.30 5 5 -4 14.80 3.60 5 5 -4 11.20 5.40 5 5 -4 16.40 5.40 5 5 -4 18.40 3.70 5 5 -4 18.30 3.40 -5 -5 4 13.60 3.80 4 5 -4 116.59 8.80 4 5 -4 111.79 11.20 4 5 -4 121.09 8.80 4 5 -4 132.99 11.20 4 5 -4 115.39 9.00 -4 -5 4 109.59 9.20 3 5 -4 242.28 18.90 3 5 -4 267.77 16.90 3 5 -4 233.88 18.70 3 5 -4 258.47 17.20 -3 -5 4 247.88 17.00 -3 -5 4 271.67 17.10 2 5 -4 57.69 4.30 2 5 -4 58.99 6.80 2 5 -4 54.19 6.70 2 5 -4 52.79 4.30 -2 -5 4 51.39 4.40 -2 -5 4 49.70 4.50 1 5 -4 385.16 27.60 1 5 -4 394.66 27.60 1 5 -4 407.96 26.10 1 5 -4 401.96 26.20 -1 -5 4 436.46 27.80 -1 -5 4 442.96 26.20 -1 -5 4 405.06 26.10 0 5 -4 589.04 40.60 0 5 -4 638.94 40.50 0 -5 4 680.53 40.60 0 -5 4 675.93 41.60 0 -5 4 619.34 40.30 -1 5 -4 19.10 3.50 -1 5 -4 19.30 3.50 1 -5 4 20.30 4.20 1 -5 4 21.80 3.00 1 -5 4 20.50 3.30 -2 5 -4 6.10 2.20 -2 5 -4 8.70 3.20 -2 5 -4 6.40 2.80 2 -5 4 9.60 3.10 2 -5 4 8.20 2.60 2 -5 4 7.20 2.70 -3 5 -4 19.10 4.20 -3 5 -4 22.90 4.80 -3 5 -4 25.60 4.20 3 -5 4 25.00 4.00 3 -5 4 31.20 4.60 3 -5 4 26.30 4.90 -4 5 -4 126.19 9.20 -4 5 -4 107.39 10.90 -4 5 -4 123.39 10.40 4 -5 4 125.99 11.00 4 -5 4 115.39 9.10 4 -5 4 125.99 9.90 -5 5 -4 29.20 4.40 -5 5 -4 25.10 5.60 -5 5 -4 26.90 5.60 5 -5 4 28.20 4.20 5 -5 4 34.40 4.90 5 -5 4 22.40 6.70 -6 5 -4 26.50 4.50 -6 5 -4 28.50 6.60 6 -5 4 31.30 7.10 -7 5 -4 -3.20 5.70 7 -5 4 5.20 6.50 7 -5 4 7.60 5.20 -8 5 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12.80 7 5 -5 108.59 10.30 7 5 -5 132.49 15.30 7 5 -5 94.89 11.00 7 5 -5 109.19 10.70 7 5 -5 94.99 9.80 6 5 -5 20.10 4.40 6 5 -5 27.50 5.00 6 5 -5 23.10 6.90 6 5 -5 23.50 5.50 6 5 -5 11.70 5.90 6 5 -5 15.70 4.50 -6 -5 5 19.60 6.20 5 5 -5 114.39 8.70 5 5 -5 115.99 8.80 5 5 -5 107.09 8.90 5 5 -5 108.39 11.20 5 5 -5 112.99 11.30 -5 -5 5 87.39 10.70 -5 -5 5 84.39 8.70 4 5 -5 58.79 7.90 4 5 -5 49.80 7.70 4 5 -5 51.49 5.20 4 5 -5 50.99 4.90 4 5 -5 51.49 4.90 -4 -5 5 43.20 5.40 3 5 -5 78.49 6.10 3 5 -5 81.89 5.80 3 5 -5 59.79 8.30 3 5 -5 72.79 8.40 -3 -5 5 68.79 6.10 -3 -5 5 80.09 6.30 2 5 -5 219.68 15.00 2 5 -5 194.28 12.60 2 5 -5 189.28 12.60 -2 -5 5 184.78 12.60 -2 -5 5 171.58 13.20 1 5 -5 53.49 6.50 1 5 -5 48.80 6.50 1 5 -5 56.79 4.50 1 5 -5 57.69 4.60 -1 -5 5 63.89 4.60 -1 -5 5 58.99 4.60 0 5 -5 610.74 40.60 0 5 -5 668.03 40.60 0 5 -5 627.54 42.30 0 -5 5 666.03 41.60 0 -5 5 628.04 40.50 -1 5 -5 328.77 21.80 -1 5 -5 346.17 21.90 -1 5 -5 325.07 21.50 1 -5 5 320.27 21.30 1 -5 5 295.37 22.60 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2.00 5.40 6 11 -6 46.40 6.20 6 11 -6 43.30 5.70 6 11 -6 42.10 6.70 -6 -11 6 37.20 6.90 5 11 -6 173.48 12.50 5 11 -6 173.18 17.80 5 11 -6 191.48 13.30 5 11 -6 173.78 13.30 -5 -11 6 150.08 13.70 4 11 -6 -5.10 3.20 4 11 -6 4.70 2.60 4 11 -6 7.00 6.70 -4 -11 6 0.40 3.40 -4 -11 6 -0.30 3.50 3 11 -6 0.20 5.90 3 11 -6 -0.70 2.50 3 11 -6 3.90 3.40 -3 -11 6 -0.20 2.90 -3 -11 6 -5.40 3.30 2 11 -6 52.09 9.20 2 11 -6 42.60 6.40 2 11 -6 59.69 5.90 -2 -11 6 55.39 5.70 -2 -11 6 64.69 6.80 1 11 -6 -1.80 3.90 1 11 -6 -4.20 4.80 1 11 -6 -1.30 2.90 -1 -11 6 -2.00 2.60 -1 -11 6 -2.00 2.50 0 11 -6 26.80 5.40 0 11 -6 28.00 6.70 0 11 -6 34.50 5.40 0 -11 6 37.10 4.90 0 -11 6 25.90 7.20 0 -11 6 39.00 5.40 -1 11 -6 88.99 9.80 -1 11 -6 85.79 8.70 1 -11 6 87.29 8.50 1 -11 6 72.29 10.60 1 -11 6 78.19 7.60 -2 11 -6 3.50 4.70 -2 11 -6 10.40 4.90 2 -11 6 18.20 6.80 2 -11 6 5.70 4.40 2 -11 6 6.90 4.70 -3 11 -6 21.20 5.90 -3 11 -6 27.60 6.30 3 -11 6 27.70 7.90 3 -11 6 24.80 6.30 -4 11 -6 9.90 5.80 -4 11 -6 -0.30 6.00 4 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4.10 -1 -10 6 19.00 6.40 0 10 -6 138.59 12.30 0 10 -6 122.89 12.90 0 10 -6 140.49 11.50 0 -10 6 158.68 11.10 0 -10 6 156.58 14.20 0 -10 6 184.08 12.10 -1 10 -6 104.49 10.30 -1 10 -6 82.09 9.20 -1 10 -6 86.09 8.60 1 -10 6 78.19 10.40 1 -10 6 103.39 8.60 1 -10 6 82.59 7.70 -2 10 -6 3.80 4.20 -2 10 -6 -4.30 5.40 -2 10 -6 4.40 4.40 2 -10 6 -0.60 4.20 2 -10 6 2.20 5.00 2 -10 6 7.20 4.00 -3 10 -6 94.89 10.50 -3 10 -6 102.29 10.20 3 -10 6 85.49 11.40 3 -10 6 116.59 11.40 3 -10 6 103.29 10.00 -4 10 -6 -4.20 4.60 -4 10 -6 6.20 5.20 4 -10 6 -1.30 5.50 4 -10 6 3.50 5.60 -5 10 -6 36.30 7.30 -5 10 -6 46.00 8.20 5 -10 6 33.60 7.30 -6 10 -6 10.60 7.10 -6 10 -6 4.40 4.90 6 -10 6 -5.40 6.90 -7 10 -6 -2.60 7.20 -7 10 -6 -19.30 7.70 7 -10 6 -2.20 7.90 9 9 -6 4.70 10.00 9 9 -6 5.20 9.00 9 9 -6 10.30 6.20 8 9 -6 -11.20 7.10 8 9 -6 -1.60 8.60 7 9 -6 45.30 7.00 7 9 -6 43.20 6.40 7 9 -6 41.80 6.30 7 9 -6 50.79 11.10 -7 -9 6 29.60 6.50 6 9 -6 9.20 3.80 6 9 -6 14.50 7.50 6 9 -6 16.50 3.90 6 9 -6 14.30 5.00 -6 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15.80 3.90 5 -5 6 25.40 5.90 5 -5 6 21.40 3.20 -6 5 -6 -9.80 4.20 -6 5 -6 4.60 2.40 6 -5 6 10.00 5.60 6 -5 6 -1.50 2.30 -7 5 -6 67.59 8.70 -7 5 -6 53.69 5.40 7 -5 6 66.69 11.70 7 -5 6 54.69 5.40 -8 5 -6 46.50 9.60 8 -5 6 58.49 10.80 8 -5 6 51.19 5.10 -9 5 -6 7.70 7.60 9 -5 6 -19.80 8.10 10 4 -6 4.20 6.80 10 4 -6 -13.20 9.20 10 4 -6 5.00 11.00 9 4 -6 7.70 6.10 9 4 -6 3.90 6.70 -9 -4 6 -6.80 7.70 8 4 -6 1.80 5.90 8 4 -6 -4.20 5.60 8 4 -6 -0.30 4.90 -8 -4 6 -8.70 6.80 7 4 -6 10.00 4.60 7 4 -6 26.50 7.40 7 4 -6 10.30 5.40 7 4 -6 7.00 5.40 -7 -4 6 17.30 7.20 6 4 -6 -3.30 5.40 6 4 -6 5.60 3.70 6 4 -6 -1.50 3.80 6 4 -6 2.30 3.50 6 4 -6 -3.00 3.60 -6 -4 6 -4.30 4.50 5 4 -6 144.09 10.40 5 4 -6 138.49 11.00 5 4 -6 146.49 10.60 5 4 -6 125.79 10.70 5 4 -6 128.99 12.50 -5 -4 6 117.39 12.30 4 4 -6 -2.60 2.40 4 4 -6 1.10 4.00 4 4 -6 -2.20 2.20 4 4 -6 -1.40 2.00 -4 -4 6 -1.80 2.40 -4 -4 6 -2.80 3.60 -4 -4 6 1.90 2.30 3 4 -6 847.82 49.80 3 4 -6 733.53 47.70 3 4 -6 786.52 47.20 -3 -4 6 700.43 50.39 -3 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10.10 2.10 -7 4 -6 23.00 6.40 7 -4 6 9.70 6.60 7 -4 6 11.90 2.10 -8 4 -6 6.00 6.40 8 -4 6 4.80 7.30 -9 4 -6 17.50 8.20 9 -4 6 20.70 9.60 -10 4 -6 -1.30 8.20 10 -4 6 -9.80 9.80 10 3 -6 -1.30 9.00 10 3 -6 -1.30 7.20 -10 -3 6 2.50 8.70 9 3 -6 14.30 7.40 -9 -3 6 17.60 8.30 8 3 -6 12.90 5.70 8 3 -6 15.00 5.80 8 3 -6 3.10 5.70 -8 -3 6 19.00 7.30 7 3 -6 11.40 5.00 7 3 -6 -0.30 3.90 7 3 -6 2.20 6.40 7 3 -6 11.20 5.30 -7 -3 6 11.80 6.10 6 3 -6 71.49 7.70 6 3 -6 82.49 8.20 6 3 -6 60.39 8.20 6 3 -6 83.49 8.00 6 3 -6 85.29 10.20 -6 -3 6 73.79 9.60 5 3 -6 1.00 4.50 5 3 -6 0.10 2.80 5 3 -6 -0.30 2.60 5 3 -6 3.30 3.00 5 3 -6 12.40 3.70 -5 -3 6 4.90 4.30 4 3 -6 335.67 21.70 4 3 -6 340.17 21.20 4 3 -6 308.37 23.00 4 3 -6 324.47 21.50 4 3 -6 306.17 21.40 -4 -3 6 303.87 23.00 3 3 -6 139.49 9.70 3 3 -6 120.39 11.40 3 3 -6 145.19 9.50 3 3 -6 150.88 10.00 -3 -3 6 119.49 11.50 -3 -3 6 141.39 10.20 2 3 -6 108.69 6.90 2 3 -6 93.09 8.70 2 3 -6 106.39 7.60 -2 -3 6 94.19 7.00 -2 -3 6 123.49 9.50 -2 -3 6 111.09 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7.80 -7 10 -7 12.30 8.80 7 -10 7 8.00 8.90 9 9 -7 4.30 10.90 9 9 -7 13.50 9.00 9 9 -7 4.20 6.30 8 9 -7 5.10 7.30 8 9 -7 -11.10 8.60 8 9 -7 6.60 5.00 7 9 -7 102.09 14.90 7 9 -7 97.79 9.40 7 9 -7 107.89 11.00 7 9 -7 101.39 9.50 -7 -9 7 77.89 10.50 6 9 -7 -3.50 7.10 6 9 -7 1.80 3.40 6 9 -7 -3.80 4.30 6 9 -7 -1.20 3.60 -6 -9 7 -3.60 4.00 5 9 -7 9.40 3.10 5 9 -7 2.60 6.00 5 9 -7 -3.00 3.70 5 9 -7 3.30 2.90 -5 -9 7 4.00 3.50 4 9 -7 0.90 5.30 4 9 -7 4.60 2.70 4 9 -7 4.00 2.40 -4 -9 7 1.50 2.80 -4 -9 7 4.00 3.30 3 9 -7 26.00 3.70 3 9 -7 22.80 3.60 3 9 -7 19.30 6.90 3 9 -7 19.60 6.60 -3 -9 7 26.20 4.00 -3 -9 7 25.10 4.00 2 9 -7 38.80 7.00 2 9 -7 41.60 7.90 2 9 -7 41.20 5.10 2 9 -7 40.30 4.60 -2 -9 7 39.20 4.80 -2 -9 7 41.80 4.40 1 9 -7 0.50 2.40 1 9 -7 1.40 3.00 1 9 -7 0.90 5.30 1 9 -7 -6.40 4.10 -1 -9 7 2.80 2.50 -1 -9 7 1.30 2.20 0 9 -7 51.69 6.80 0 9 -7 52.79 8.30 0 9 -7 57.89 8.60 0 9 -7 54.69 5.70 0 -9 7 55.69 5.60 0 -9 7 53.99 8.30 0 -9 7 63.59 6.10 -1 9 -7 16.60 4.00 -1 9 -7 18.40 4.70 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34.10 4.20 4 8 -7 39.50 8.30 4 8 -7 38.40 4.50 -4 -8 7 45.90 5.50 -4 -8 7 32.40 4.80 3 8 -7 152.78 13.70 3 8 -7 144.39 13.90 3 8 -7 120.19 10.00 3 8 -7 154.68 10.20 -3 -8 7 145.09 10.50 -3 -8 7 131.79 10.30 2 8 -7 11.80 2.50 2 8 -7 9.10 2.60 2 8 -7 15.80 5.80 2 8 -7 13.10 5.20 -2 -8 7 10.30 2.50 -2 -8 7 5.90 2.50 1 8 -7 437.86 30.50 1 8 -7 431.76 28.20 1 8 -7 413.36 28.40 -1 -8 7 465.75 28.20 -1 -8 7 422.16 28.00 0 8 -7 187.18 15.70 0 8 -7 213.98 14.00 0 8 -7 173.18 13.90 0 8 -7 201.68 15.40 0 -8 7 185.68 13.40 0 -8 7 191.18 15.80 0 -8 7 205.38 13.80 -1 8 -7 7.40 3.60 -1 8 -7 5.40 3.80 -1 8 -7 7.40 3.00 1 -8 7 6.10 2.80 1 -8 7 5.10 2.70 1 -8 7 6.00 3.90 -2 8 -7 14.60 4.10 -2 8 -7 12.10 4.50 -2 8 -7 13.60 3.90 2 -8 7 18.10 3.70 2 -8 7 12.70 4.70 2 -8 7 10.20 4.10 -3 8 -7 114.09 10.20 -3 8 -7 115.29 9.50 -3 8 -7 107.99 11.00 3 -8 7 105.59 9.80 3 -8 7 115.59 10.60 3 -8 7 112.69 10.50 -4 8 -7 10.70 5.10 4 -8 7 17.10 4.60 4 -8 7 19.60 5.90 -5 8 -7 7.00 3.80 -5 8 -7 2.90 5.60 5 -8 7 9.20 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6.70 9 8 -9 1.10 8.20 9 8 -9 -9.10 10.40 8 8 -9 34.60 5.60 8 8 -9 16.30 11.30 8 8 -9 33.10 6.80 8 8 -9 19.30 7.70 7 8 -9 21.90 4.60 7 8 -9 19.90 4.90 7 8 -9 16.80 10.10 7 8 -9 17.50 6.10 6 8 -9 5.20 3.90 6 8 -9 -0.80 7.40 6 8 -9 1.90 3.10 6 8 -9 -4.70 4.80 -6 -8 9 -4.30 3.60 5 8 -9 -0.50 2.40 5 8 -9 2.40 2.90 5 8 -9 1.20 6.40 -5 -8 9 4.00 4.00 -5 -8 9 -1.60 3.00 4 8 -9 113.69 9.00 4 8 -9 122.29 8.70 4 8 -9 121.19 12.50 -4 -8 9 108.59 9.20 -4 -8 9 116.69 10.00 3 8 -9 1.70 2.10 3 8 -9 1.10 2.30 3 8 -9 -3.30 3.80 3 8 -9 3.60 6.00 -3 -8 9 1.60 2.20 -3 -8 9 2.50 3.00 2 8 -9 52.29 8.30 2 8 -9 41.90 4.90 2 8 -9 47.50 8.20 2 8 -9 41.10 4.60 -2 -8 9 38.70 4.70 -2 -8 9 44.40 4.60 1 8 -9 156.28 16.10 1 8 -9 197.78 13.90 1 8 -9 218.18 16.70 1 8 -9 192.08 14.10 -1 -8 9 203.28 13.90 -1 -8 9 213.48 13.70 0 8 -9 20.30 4.10 0 8 -9 17.20 5.50 0 8 -9 27.70 5.70 0 8 -9 17.30 3.70 0 -8 9 14.10 3.40 0 -8 9 24.40 3.60 -1 8 -9 6.00 4.30 -1 8 -9 11.30 3.50 -1 8 -9 0.00 3.50 -1 8 -9 6.20 3.90 1 -8 9 7.30 3.00 1 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196.88 14.30 1 -3 9 238.98 14.80 -2 3 -9 254.77 18.90 -2 3 -9 285.27 19.60 -2 3 -9 315.57 19.10 -2 3 -9 277.37 19.90 2 -3 9 301.77 19.40 2 -3 9 294.77 19.90 -3 3 -9 301.07 21.10 -3 3 -9 319.47 21.80 -3 3 -9 309.87 19.40 3 -3 9 302.57 20.70 3 -3 9 294.77 21.50 -4 3 -9 2.30 4.00 -4 3 -9 2.40 3.40 4 -3 9 1.20 3.10 4 -3 9 1.40 3.60 -5 3 -9 23.40 6.10 -5 3 -9 24.50 6.30 5 -3 9 24.20 4.20 5 -3 9 30.10 6.00 -6 3 -9 -1.40 4.60 6 -3 9 2.80 5.20 -7 3 -9 19.90 6.70 7 -3 9 14.30 7.50 -8 3 -9 7.80 7.10 8 -3 9 13.30 8.30 -9 3 -9 0.20 7.40 9 -3 9 6.30 8.60 -10 3 -9 8.50 9.30 10 -3 9 10.40 11.00 10 2 -9 10.40 7.80 10 2 -9 20.90 9.00 -10 -2 9 22.50 11.70 9 2 -9 11.30 6.80 9 2 -9 -3.30 5.90 -9 -2 9 9.20 8.90 8 2 -9 6.40 5.80 8 2 -9 -12.30 5.10 8 2 -9 -4.00 5.40 -8 -2 9 2.50 7.00 7 2 -9 194.98 15.40 7 2 -9 177.88 15.30 7 2 -9 209.58 15.80 -7 -2 9 177.78 17.60 6 2 -9 10.90 4.10 6 2 -9 10.40 4.20 6 2 -9 10.40 5.10 6 2 -9 12.00 5.90 6 2 -9 13.50 4.10 -6 -2 9 18.40 6.50 5 2 -9 9.00 4.00 5 2 -9 8.20 3.30 5 2 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6 -2 9 53.79 8.90 -7 2 -9 8.20 6.00 7 -2 9 11.10 6.80 8 -2 9 30.20 10.00 -9 2 -9 4.40 7.80 9 -2 9 -2.40 8.00 -10 2 -9 1.40 8.30 10 -2 9 25.10 10.60 10 1 -9 3.50 7.20 10 1 -9 6.00 8.70 -10 -1 9 -12.40 9.40 9 1 -9 -1.40 6.10 9 1 -9 11.00 6.90 -9 -1 9 9.00 9.50 8 1 -9 8.20 5.70 8 1 -9 3.10 6.20 8 1 -9 1.90 5.80 -8 -1 9 7.90 7.30 7 1 -9 -0.90 4.90 7 1 -9 5.20 3.90 7 1 -9 5.00 5.20 -7 -1 9 4.20 6.10 6 1 -9 54.99 7.30 6 1 -9 56.49 9.40 6 1 -9 65.89 7.80 6 1 -9 65.99 7.50 -6 -1 9 62.79 9.60 5 1 -9 3.00 4.50 5 1 -9 -1.30 2.90 5 1 -9 3.70 2.90 5 1 -9 3.70 2.60 5 1 -9 -0.90 3.10 -5 -1 9 4.30 4.70 4 1 -9 45.60 4.80 4 1 -9 49.90 5.60 4 1 -9 56.19 5.60 4 1 -9 49.20 7.50 -4 -1 9 53.39 5.60 -4 -1 9 51.39 7.80 -4 -1 9 49.20 5.40 3 1 -9 257.77 16.70 3 1 -9 231.78 15.70 3 1 -9 282.57 18.30 -3 -1 9 241.98 16.90 -3 -1 9 239.48 16.00 -3 -1 9 202.08 18.00 2 1 -9 45.10 4.20 2 1 -9 46.40 6.20 2 1 -9 46.30 3.10 -2 -1 9 44.20 4.40 -2 -1 9 44.60 3.50 -2 -1 9 38.40 6.10 1 1 -9 949.01 60.29 1 1 -9 998.80 61.39 1 1 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5.10 4 12 -10 22.20 9.00 4 12 -10 26.40 4.80 4 12 -10 22.80 5.20 -4 -12 10 17.90 5.60 -4 -12 10 33.90 5.50 3 12 -10 27.80 5.80 3 12 -10 39.10 5.60 3 12 -10 29.40 9.10 -3 -12 10 33.00 5.50 -3 -12 10 30.10 5.50 2 12 -10 12.20 5.30 2 12 -10 8.00 4.10 2 12 -10 5.60 7.50 -2 -12 10 14.90 4.10 -2 -12 10 14.50 4.40 1 12 -10 39.70 8.90 1 12 -10 33.30 6.90 1 12 -10 47.50 6.50 -1 -12 10 41.00 6.00 -1 -12 10 31.90 5.90 0 12 -10 144.59 15.20 0 12 -10 161.68 13.80 0 12 -10 178.58 16.10 0 -12 10 181.98 13.30 0 -12 10 151.68 12.80 -1 12 -10 -0.50 5.00 -1 12 -10 -4.40 5.70 1 -12 10 4.30 4.30 -2 12 -10 7.10 5.60 -2 12 -10 10.80 5.50 2 -12 10 6.10 5.20 -3 12 -10 -5.40 5.80 -3 12 -10 -2.50 5.50 -3 12 -10 17.70 8.50 3 -12 10 -0.80 5.70 -4 12 -10 5.70 6.70 4 -12 10 25.40 7.70 -5 12 -10 21.10 8.30 -5 12 -10 3.10 7.70 5 -12 10 -2.20 7.30 8 11 -10 14.80 8.10 8 11 -10 14.40 5.80 8 11 -10 10.60 10.30 7 11 -10 8.50 5.00 7 11 -10 21.00 9.80 -7 -11 10 4.20 5.70 6 11 -10 27.00 9.60 6 11 -10 28.10 4.90 6 11 -10 12.50 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11.70 -1 10 -10 141.89 13.20 -1 10 -10 139.69 14.00 1 -10 10 159.58 11.90 1 -10 10 137.09 11.20 -2 10 -10 10.50 6.50 -2 10 -10 3.50 4.30 -2 10 -10 7.80 4.70 -2 10 -10 11.60 5.70 2 -10 10 7.70 4.40 -3 10 -10 5.50 4.50 -3 10 -10 9.50 6.20 -3 10 -10 13.20 5.40 3 -10 10 8.60 5.50 -4 10 -10 51.99 8.80 -4 10 -10 51.09 8.70 -4 10 -10 69.69 9.90 4 -10 10 68.39 9.90 -5 10 -10 -3.20 4.80 -5 10 -10 -0.60 7.60 -5 10 -10 8.00 8.70 5 -10 10 5.70 7.30 -6 10 -10 33.40 9.00 -6 10 -10 31.60 6.20 6 -10 10 33.30 9.20 -7 10 -10 1.40 6.60 7 -10 10 -8.20 8.40 9 9 -10 13.70 12.00 9 9 -10 2.30 8.10 9 9 -10 5.40 6.70 8 9 -10 -2.30 10.60 8 9 -10 -0.10 5.00 8 9 -10 9.10 7.30 7 9 -10 6.80 3.80 7 9 -10 7.40 4.70 7 9 -10 12.30 8.90 7 9 -10 18.70 6.50 6 9 -10 23.00 6.70 6 9 -10 7.50 8.20 6 9 -10 6.00 3.50 6 9 -10 8.80 3.70 -6 -9 10 9.10 4.20 5 9 -10 25.00 9.90 5 9 -10 31.30 4.70 5 9 -10 41.40 5.30 -5 -9 10 30.40 4.90 -5 -9 10 29.50 6.40 4 9 -10 3.30 2.60 4 9 -10 7.70 3.50 4 9 -10 -6.20 5.80 -4 -9 10 0.70 2.80 -4 -9 10 -1.10 5.10 3 9 -10 62.29 6.20 3 9 -10 62.09 9.20 3 9 -10 60.39 6.00 -3 -9 10 53.89 5.70 -3 -9 10 51.99 6.20 2 9 -10 12.70 6.30 2 9 -10 14.80 3.30 2 9 -10 7.90 6.40 2 9 -10 7.40 3.20 -2 -9 10 15.60 3.40 -2 -9 10 13.00 2.90 1 9 -10 3.00 5.00 1 9 -10 7.00 6.10 1 9 -10 0.10 2.70 1 9 -10 0.40 3.30 -1 -9 10 6.00 3.20 -1 -9 10 4.90 2.40 0 9 -10 42.30 6.10 0 9 -10 48.90 8.70 0 9 -10 43.50 7.90 0 9 -10 41.60 6.20 0 -9 10 35.60 5.50 -1 9 -10 1.40 4.50 -1 9 -10 5.90 3.70 -1 9 -10 10.70 4.60 -1 9 -10 10.70 6.00 1 -9 10 9.90 3.50 1 -9 10 14.20 3.80 -2 9 -10 -0.60 4.10 -2 9 -10 -2.10 4.60 -2 9 -10 8.50 5.60 -2 9 -10 0.40 3.80 2 -9 10 7.90 3.70 2 -9 10 -5.20 3.80 -3 9 -10 47.30 8.00 -3 9 -10 55.59 7.90 -3 9 -10 45.60 6.90 3 -9 10 66.29 8.80 -4 9 -10 0.40 5.20 -4 9 -10 4.90 4.10 -4 9 -10 -0.50 5.40 4 -9 10 -0.10 5.30 -5 9 -10 21.80 7.20 -5 9 -10 25.00 6.30 5 -9 10 15.90 7.30 -6 9 -10 11.30 7.20 6 -9 10 2.70 7.20 -7 9 -10 16.80 8.40 7 -9 10 -5.50 7.60 9 8 -10 -1.70 8.00 9 8 -10 4.20 6.20 9 8 -10 -16.40 11.40 8 8 -10 13.80 10.40 8 8 -10 19.90 6.00 8 8 -10 10.70 7.10 7 8 -10 7.60 4.50 7 8 -10 14.60 6.00 7 8 -10 11.10 3.90 6 8 -10 4.00 4.60 6 8 -10 0.10 3.40 6 8 -10 2.40 6.00 6 8 -10 5.50 2.90 6 8 -10 11.10 7.80 5 8 -10 3.50 2.40 5 8 -10 -2.20 2.80 5 8 -10 -5.90 6.50 -5 -8 10 -2.00 4.30 -5 -8 10 2.40 3.20 4 8 -10 1.70 2.70 4 8 -10 -1.10 7.00 4 8 -10 -1.90 1.90 -4 -8 10 -2.90 3.40 -4 -8 10 0.30 2.40 3 8 -10 63.19 10.10 3 8 -10 69.09 5.80 3 8 -10 55.79 5.30 3 8 -10 62.29 9.40 -3 -8 10 53.89 6.20 -3 -8 10 57.19 6.50 2 8 -10 30.00 4.40 2 8 -10 43.80 7.90 2 8 -10 27.60 7.30 2 8 -10 29.80 4.30 -2 -8 10 33.80 4.70 -2 -8 10 35.10 4.00 1 8 -10 26.60 4.20 1 8 -10 30.30 6.80 1 8 -10 23.70 4.00 1 8 -10 18.00 6.20 -1 -8 10 23.70 3.40 -1 -8 10 25.40 4.20 0 8 -10 203.78 15.10 0 8 -10 210.48 16.80 0 8 -10 208.28 15.40 0 -8 10 225.18 14.70 0 -8 10 199.68 14.60 -1 8 -10 111.19 10.70 -1 8 -10 95.59 10.00 -1 8 -10 133.09 11.70 -1 8 -10 101.59 9.40 1 -8 10 116.19 9.40 1 -8 10 106.09 8.90 -2 8 -10 19.20 4.50 -2 8 -10 17.70 5.50 -2 8 -10 14.40 5.00 -2 8 -10 19.10 4.50 2 -8 10 16.30 4.30 2 -8 10 23.50 4.70 -3 8 -10 15.60 5.20 -3 8 -10 21.40 4.20 -3 8 -10 11.80 5.10 3 -8 10 16.20 5.20 3 -8 10 16.90 5.70 -4 8 -10 24.60 4.90 -4 8 -10 27.60 6.20 -4 8 -10 22.40 5.70 4 -8 10 36.30 6.90 -5 8 -10 31.90 5.70 -5 8 -10 40.20 8.10 5 -8 10 27.80 7.60 -6 8 -10 34.60 7.80 -6 8 -10 19.80 3.40 -6 8 -10 13.40 4.60 6 -8 10 10.50 7.80 -7 8 -10 1.30 7.30 7 -8 10 4.60 7.60 -8 8 -10 -2.80 8.10 8 -8 10 2.60 9.50 9 7 -10 -2.60 10.80 9 7 -10 3.40 5.90 9 7 -10 -6.20 7.50 8 7 -10 2.10 4.90 8 7 -10 -2.40 8.90 8 7 -10 1.10 6.20 8 7 -10 -0.90 4.50 7 7 -10 -4.10 4.20 7 7 -10 1.10 3.60 7 7 -10 -9.20 4.80 7 7 -10 3.70 8.20 6 7 -10 10.30 4.20 6 7 -10 16.50 5.80 6 7 -10 21.20 8.60 6 7 -10 9.70 4.80 6 7 -10 11.10 3.20 5 7 -10 4.90 3.10 5 7 -10 6.90 6.50 5 7 -10 4.70 2.30 -5 -7 10 0.80 4.00 -5 -7 10 5.70 3.10 4 7 -10 9.60 3.10 4 7 -10 8.80 6.50 4 7 -10 9.20 6.20 -4 -7 10 8.40 3.80 -4 -7 10 10.70 2.80 3 7 -10 17.50 2.50 3 7 -10 20.10 3.50 3 7 -10 14.40 5.70 3 7 -10 13.80 5.50 -3 -7 10 19.30 3.80 -3 -7 10 14.00 2.60 2 7 -10 30.00 6.10 2 7 -10 19.50 2.90 2 7 -10 21.60 6.60 2 7 -10 18.40 3.50 -2 -7 10 18.40 2.60 -2 -7 10 26.40 3.90 1 7 -10 154.68 11.20 1 7 -10 164.08 13.80 1 7 -10 141.09 10.90 1 7 -10 146.59 13.50 -1 -7 10 149.49 11.00 0 7 -10 18.40 5.40 0 7 -10 24.80 5.80 0 7 -10 18.10 3.80 0 7 -10 27.20 4.20 0 -7 10 21.50 3.60 0 -7 10 22.00 3.30 -1 7 -10 5.60 4.70 -1 7 -10 5.30 3.00 -1 7 -10 8.90 4.20 -1 7 -10 1.40 3.40 1 -7 10 5.90 3.00 1 -7 10 8.90 3.00 -2 7 -10 2.40 3.90 -2 7 -10 4.00 3.20 -2 7 -10 3.70 3.30 -2 7 -10 -2.70 4.00 2 -7 10 -4.90 3.10 2 -7 10 -2.70 2.90 -3 7 -10 -0.20 4.50 -3 7 -10 4.40 3.90 -3 7 -10 6.60 4.00 -3 7 -10 -0.50 2.60 3 -7 10 1.80 4.10 3 -7 10 -5.50 3.40 -4 7 -10 13.00 4.40 -4 7 -10 -2.30 4.40 4 -7 10 -2.30 4.50 -5 7 -10 -3.60 5.10 -5 7 -10 5.10 3.40 5 -7 10 6.80 5.90 -6 7 -10 0.80 2.10 -6 7 -10 -5.00 6.10 -6 7 -10 4.40 1.70 6 -7 10 17.90 8.10 -7 7 -10 -5.30 6.90 7 -7 10 -9.40 6.80 -8 7 -10 -7.80 7.80 8 -7 10 -13.60 7.60 10 6 -10 -10.00 9.00 10 6 -10 2.80 7.00 10 6 -10 16.20 12.20 9 6 -10 18.90 11.50 9 6 -10 -15.50 7.00 9 6 -10 5.20 6.00 8 6 -10 0.50 4.90 8 6 -10 -8.00 5.60 8 6 -10 0.30 4.90 7 6 -10 3.80 3.90 7 6 -10 -0.20 4.20 7 6 -10 -2.80 4.50 -7 -6 10 -3.20 7.10 6 6 -10 50.09 7.20 6 6 -10 42.90 6.20 6 6 -10 46.00 6.40 6 6 -10 44.20 5.50 -6 -6 10 29.70 8.50 5 6 -10 1.40 1.90 5 6 -10 1.80 2.90 -5 -6 10 -0.40 4.00 -5 -6 10 6.90 4.60 4 6 -10 14.90 2.10 4 6 -10 16.00 5.30 4 6 -10 15.40 3.40 -4 -6 10 11.20 2.60 -4 -6 10 14.70 3.80 -4 -6 10 17.60 6.00 3 6 -10 185.28 15.60 3 6 -10 183.58 12.40 3 6 -10 179.98 11.50 -3 -6 10 172.78 15.20 -3 -6 10 158.88 11.60 -3 -6 10 164.48 12.70 2 6 -10 18.90 3.20 2 6 -10 20.90 5.80 2 6 -10 15.00 4.90 2 6 -10 17.30 2.50 -2 -6 10 20.50 2.40 -2 -6 10 17.40 5.40 -2 -6 10 20.50 3.50 1 6 -10 9.50 4.50 1 6 -10 5.70 4.40 1 6 -10 10.40 2.70 1 6 -10 9.00 2.50 -1 -6 10 11.40 2.00 -1 -6 10 9.20 2.80 0 6 -10 82.69 8.50 0 6 -10 65.79 8.80 0 6 -10 74.29 6.80 0 6 -10 76.49 6.70 0 -6 10 83.29 6.60 -1 6 -10 16.50 4.80 -1 6 -10 7.40 4.10 -1 6 -10 14.50 3.40 -1 6 -10 8.50 3.50 1 -6 10 6.50 2.70 1 -6 10 14.00 3.10 -2 6 -10 67.79 6.80 -2 6 -10 56.99 7.60 -2 6 -10 77.09 7.60 -2 6 -10 63.99 6.80 2 -6 10 73.59 7.30 2 -6 10 52.19 5.80 -3 6 -10 31.30 4.50 -3 6 -10 37.70 5.90 -3 6 -10 33.10 6.30 3 -6 10 38.30 5.50 3 -6 10 42.50 6.50 -4 6 -10 123.69 11.60 -4 6 -10 136.89 12.60 -4 6 -10 121.79 9.70 -4 6 -10 137.19 10.20 4 -6 10 142.69 12.40 -5 6 -10 100.09 10.60 -5 6 -10 99.69 7.50 -5 6 -10 100.49 7.10 5 -6 10 101.79 11.80 -6 6 -10 9.90 6.40 6 -6 10 10.50 6.80 -7 6 -10 -6.40 4.60 7 -6 10 -12.10 6.80 -8 6 -10 5.40 7.40 -9 6 -10 -13.00 8.30 9 -6 10 -2.60 10.70 10 5 -10 25.20 9.60 10 5 -10 13.00 7.80 10 5 -10 20.80 12.70 -10 -5 10 -9.90 11.40 9 5 -10 1.60 6.00 9 5 -10 1.80 6.90 -9 -5 10 -2.60 9.30 8 5 -10 4.80 5.40 8 5 -10 10.60 6.30 8 5 -10 0.90 5.20 -8 -5 10 16.80 9.30 7 5 -10 7.70 4.50 7 5 -10 0.70 4.50 7 5 -10 9.20 4.30 -7 -5 10 1.70 7.30 6 5 -10 13.30 3.50 6 5 -10 13.20 4.20 6 5 -10 13.40 6.10 6 5 -10 10.70 4.00 -6 -5 10 -1.70 6.20 5 5 -10 3.30 2.90 5 5 -10 -1.70 5.70 5 5 -10 0.70 2.90 -5 -5 10 7.20 5.60 -5 -5 10 2.10 4.10 4 5 -10 20.20 6.00 4 5 -10 26.80 3.70 4 5 -10 30.30 4.30 4 5 -10 21.30 2.60 -4 -5 10 24.30 6.50 -4 -5 10 22.50 4.60 3 5 -10 6.30 2.40 3 5 -10 7.50 4.10 3 5 -10 5.80 1.20 -3 -5 10 5.70 1.50 -3 -5 10 8.20 3.00 -3 -5 10 3.70 4.60 2 5 -10 250.97 19.80 2 5 -10 250.47 17.60 2 5 -10 291.07 17.00 -2 -5 10 272.97 20.00 -2 -5 10 242.98 16.80 -2 -5 10 273.07 17.90 1 5 -10 6.00 1.90 1 5 -10 7.30 4.20 1 5 -10 9.20 2.40 -1 -5 10 8.80 4.00 -1 -5 10 6.40 1.40 -1 -5 10 9.00 2.50 0 5 -10 5.70 3.70 0 5 -10 7.40 3.70 0 5 -10 3.70 2.20 0 5 -10 0.80 2.00 0 -5 10 1.30 2.10 0 -5 10 4.10 1.80 -1 5 -10 26.70 4.40 -1 5 -10 34.90 5.30 -1 5 -10 34.70 4.60 -1 5 -10 36.50 5.70 1 -5 10 37.20 4.00 1 -5 10 35.10 4.70 -2 5 -10 32.20 5.50 -2 5 -10 35.00 5.00 -2 5 -10 32.20 5.00 -2 5 -10 31.60 5.40 2 -5 10 41.00 5.60 2 -5 10 33.40 4.70 -3 5 -10 108.89 9.20 -3 5 -10 113.39 10.20 -3 5 -10 105.59 7.60 -3 5 -10 83.89 7.90 3 -5 10 84.09 8.50 3 -5 10 102.49 9.40 -4 5 -10 14.50 2.60 -4 5 -10 19.70 5.50 -4 5 -10 19.40 4.80 4 -5 10 16.00 4.40 4 -5 10 8.70 5.00 -5 5 -10 6.50 3.90 5 -5 10 1.80 4.50 -6 5 -10 18.60 5.60 6 -5 10 17.30 6.90 -7 5 -10 11.90 8.10 -8 5 -10 6.80 7.20 8 -5 10 1.80 8.80 -9 5 -10 26.60 9.30 9 -5 10 -9.10 9.30 10 4 -10 0.00 7.20 10 4 -10 -9.40 8.40 -10 -4 10 3.70 10.10 9 4 -10 -14.20 5.30 9 4 -10 -7.10 6.80 -9 -4 10 14.10 10.40 8 4 -10 3.40 5.60 8 4 -10 9.20 5.90 8 4 -10 15.60 5.90 -8 -4 10 2.50 8.70 7 4 -10 1.00 4.50 7 4 -10 2.90 4.50 7 4 -10 10.50 4.50 6 4 -10 19.70 4.60 6 4 -10 15.90 4.30 6 4 -10 21.10 4.00 -6 -4 10 21.80 7.00 5 4 -10 66.19 8.60 5 4 -10 53.59 6.30 5 4 -10 66.79 6.30 5 4 -10 55.89 7.10 -5 -4 10 49.30 7.30 -5 -4 10 59.99 9.50 4 4 -10 83.09 5.80 4 4 -10 80.39 6.30 4 4 -10 76.89 7.00 4 4 -10 69.69 8.80 -4 -4 10 69.19 7.60 -4 -4 10 94.29 9.80 3 4 -10 5.20 2.30 3 4 -10 3.90 1.30 3 4 -10 0.00 4.00 3 4 -10 4.20 0.90 -3 -4 10 0.40 3.20 -3 -4 10 9.50 3.10 2 4 -10 1.10 1.90 2 4 -10 11.20 4.70 2 4 -10 3.10 0.70 -2 -4 10 3.40 1.90 -2 -4 10 5.70 3.90 -2 -4 10 1.10 0.60 1 4 -10 8.60 1.60 1 4 -10 6.20 3.80 1 4 -10 9.20 2.50 -1 -4 10 11.20 2.60 -1 -4 10 10.10 1.40 -1 -4 10 4.50 3.80 0 4 -10 10.60 4.00 0 4 -10 12.10 2.50 0 4 -10 17.50 3.10 0 -4 10 13.00 2.20 0 -4 10 9.70 3.50 0 -4 10 12.90 2.80 -1 4 -10 345.97 22.10 -1 4 -10 331.67 23.40 -1 4 -10 304.37 22.10 -1 4 -10 318.67 22.50 1 -4 10 358.76 22.00 1 -4 10 320.57 22.10 -2 4 -10 120.89 9.40 -2 4 -10 127.39 9.30 -2 4 -10 113.39 9.30 -2 4 -10 120.89 10.20 2 -4 10 114.09 9.80 2 -4 10 119.69 9.30 -3 4 -10 23.60 4.70 -3 4 -10 25.30 3.00 -3 4 -10 20.50 3.20 -3 4 -10 32.10 5.50 3 -4 10 25.70 4.10 3 -4 10 25.10 5.00 -4 4 -10 23.50 5.80 -4 4 -10 32.50 5.70 4 -4 10 28.50 6.00 4 -4 10 32.20 5.30 -5 4 -10 13.90 5.50 -5 4 -10 2.60 4.10 5 -4 10 9.00 5.30 -6 4 -10 29.40 7.00 6 -4 10 25.30 6.80 -7 4 -10 23.10 7.10 7 -4 10 -1.00 6.90 -8 4 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2.00 5 5 -11 5.00 2.80 5 5 -11 -0.50 2.90 -5 -5 11 18.20 6.40 -5 -5 11 2.50 3.90 4 5 -11 -1.40 2.60 4 5 -11 2.10 1.80 4 5 -11 1.80 1.10 4 5 -11 7.50 5.80 -4 -5 11 2.00 5.00 -4 -5 11 3.60 3.50 3 5 -11 38.20 7.20 3 5 -11 32.70 4.60 3 5 -11 34.20 3.20 3 5 -11 39.00 2.80 -3 -5 11 29.50 6.60 -3 -5 11 33.30 5.00 2 5 -11 2.80 2.10 2 5 -11 0.70 1.10 2 5 -11 1.10 4.10 -2 -5 11 1.20 4.00 -2 -5 11 -0.30 2.20 -2 -5 11 0.50 0.90 1 5 -11 56.89 5.50 1 5 -11 56.99 7.80 1 5 -11 58.69 4.90 -1 -5 11 58.59 5.60 -1 -5 11 54.69 7.40 -1 -5 11 62.89 4.40 0 5 -11 270.17 17.10 0 5 -11 257.97 18.50 0 5 -11 239.88 16.80 0 5 -11 209.38 18.00 0 -5 11 264.47 16.90 0 -5 11 227.68 18.10 0 -5 11 258.97 16.40 -1 5 -11 91.79 9.20 -1 5 -11 83.69 8.40 -1 5 -11 109.99 8.50 -1 5 -11 109.39 9.30 1 -5 11 109.69 8.20 1 -5 11 101.49 8.40 -2 5 -11 7.50 4.00 -2 5 -11 9.80 3.60 -2 5 -11 14.10 3.80 -2 5 -11 11.20 3.70 2 -5 11 11.30 3.30 2 -5 11 16.10 3.90 -3 5 -11 2.10 3.40 -3 5 -11 6.40 2.70 -3 5 -11 -1.20 2.00 -3 5 -11 5.20 4.20 3 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6 6 -12 18.90 4.80 -6 -6 12 25.20 7.80 5 6 -12 0.30 2.50 5 6 -12 -0.20 1.60 5 6 -12 3.00 3.40 -5 -6 12 -6.10 4.00 -5 -6 12 4.00 6.60 4 6 -12 14.80 2.00 4 6 -12 16.30 2.60 4 6 -12 22.70 4.00 -4 -6 12 22.00 4.70 -4 -6 12 19.00 6.40 3 6 -12 8.20 1.60 3 6 -12 13.80 3.10 3 6 -12 5.30 4.90 -3 -6 12 14.80 2.10 -3 -6 12 6.20 5.20 -3 -6 12 10.60 3.40 2 6 -12 125.89 12.20 2 6 -12 116.79 8.20 2 6 -12 127.79 9.20 -2 -6 12 104.69 9.00 -2 -6 12 119.19 7.90 -2 -6 12 111.29 11.70 1 6 -12 -1.30 4.30 1 6 -12 -2.50 4.50 1 6 -12 0.50 2.10 1 6 -12 1.40 2.10 -1 -6 12 0.50 3.90 -1 -6 12 2.60 1.40 -1 -6 12 0.70 2.50 0 6 -12 83.49 9.00 0 6 -12 65.59 6.30 0 6 -12 75.79 8.90 0 6 -12 59.19 6.40 0 -6 12 59.29 7.80 0 -6 12 62.49 6.10 -1 6 -12 138.09 11.90 -1 6 -12 137.29 10.80 -1 6 -12 136.19 11.00 -1 6 -12 140.69 12.10 1 -6 12 130.89 10.50 1 -6 12 135.19 10.40 -2 6 -12 10.00 4.10 -2 6 -12 -0.20 3.40 -2 6 -12 1.10 3.30 -2 6 -12 0.70 4.20 2 -6 12 2.50 2.60 2 -6 12 1.40 3.50 -3 6 -12 100.19 8.80 -3 6 -12 87.89 9.20 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14 4.40 7.40 4 7 -14 111.29 7.60 4 7 -14 123.39 9.90 4 7 -14 112.69 7.80 -4 -7 14 114.89 13.60 3 7 -14 53.49 4.40 3 7 -14 63.39 6.40 -3 -7 14 57.99 4.30 -3 -7 14 64.19 7.30 -3 -7 14 61.89 10.30 2 7 -14 1.20 2.80 2 7 -14 -4.60 5.60 2 7 -14 0.40 2.00 2 7 -14 0.50 5.40 -2 -7 14 -5.60 4.90 -2 -7 14 3.50 3.40 -2 -7 14 0.50 1.40 1 7 -14 36.70 5.20 1 7 -14 46.40 8.60 1 7 -14 42.40 5.50 1 7 -14 62.59 9.20 -1 -7 14 50.89 5.60 -1 -7 14 49.99 5.80 0 7 -14 8.50 3.50 0 7 -14 12.80 6.00 0 7 -14 5.50 5.50 0 7 -14 8.80 3.50 0 -7 14 3.80 3.20 0 -7 14 5.90 2.60 -1 7 -14 5.60 5.30 -1 7 -14 2.50 4.30 -1 7 -14 4.30 3.60 -1 7 -14 -4.90 3.80 1 -7 14 1.10 3.00 1 -7 14 2.60 2.50 -2 7 -14 77.79 8.90 -2 7 -14 90.39 10.00 -2 7 -14 90.99 8.90 -2 7 -14 68.39 9.20 2 -7 14 76.09 8.70 -3 7 -14 4.00 4.40 -3 7 -14 11.40 6.10 -3 7 -14 -4.40 3.80 -3 7 -14 0.10 3.30 3 -7 14 4.10 4.40 -4 7 -14 52.79 6.00 -4 7 -14 60.89 8.90 4 -7 14 56.59 8.70 -5 7 -14 7.20 4.90 5 -7 14 10.20 7.20 -6 7 -14 15.30 7.00 6 -7 14 3.60 6.90 -7 7 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77.19 7.90 -2 6 -14 79.29 12.40 -2 6 -14 92.19 9.50 2 -6 14 81.09 8.00 2 -6 14 83.49 8.70 -3 6 -14 31.10 4.80 -3 6 -14 18.40 5.40 -3 6 -14 40.80 7.10 -3 6 -14 24.50 5.00 3 -6 14 25.70 5.70 -4 6 -14 19.80 3.50 -4 6 -14 9.80 4.30 -4 6 -14 15.60 8.50 -4 6 -14 15.70 2.80 4 -6 14 16.30 5.90 -5 6 -14 4.40 5.70 5 -6 14 -5.00 6.20 -6 6 -14 -8.10 6.20 6 -6 14 1.70 6.80 -7 6 -14 0.40 5.30 7 -6 14 3.30 7.90 -8 6 -14 16.90 8.60 8 -6 14 4.20 8.90 9 5 -14 6.00 6.20 9 5 -14 6.00 5.90 -9 -5 14 8.20 10.80 8 5 -14 -12.30 4.80 8 5 -14 1.60 5.40 -8 -5 14 -3.70 8.50 7 5 -14 10.90 4.30 7 5 -14 15.40 3.50 7 5 -14 20.90 5.30 6 5 -14 9.10 4.20 6 5 -14 3.40 2.70 6 5 -14 4.20 2.20 -6 -5 14 10.10 6.40 5 5 -14 -0.70 1.40 5 5 -14 1.90 3.50 5 5 -14 1.20 1.10 -5 -5 14 -1.50 4.80 4 5 -14 27.60 4.60 -4 -5 14 31.10 5.20 -4 -5 14 9.20 6.70 3 5 -14 4.50 4.30 3 5 -14 1.20 2.70 -3 -5 14 0.10 4.60 -3 -5 14 5.50 3.50 2 5 -14 173.28 13.00 2 5 -14 152.18 15.30 -2 -5 14 179.08 13.40 -2 -5 14 222.08 16.00 1 5 -14 54.79 7.90 1 5 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20.60 3.60 6 4 -14 19.30 4.00 -6 -4 14 24.80 9.20 5 4 -14 24.00 2.70 5 4 -14 27.30 4.60 5 4 -14 24.50 2.90 -5 -4 14 37.40 8.60 4 4 -14 32.20 5.10 -4 -4 14 31.20 7.70 -4 -4 14 33.10 5.30 3 4 -14 14.00 6.40 -3 -4 14 16.40 5.20 -3 -4 14 12.00 4.10 2 4 -14 9.90 2.80 2 4 -14 6.20 5.10 -2 -4 14 2.80 4.70 -2 -4 14 4.00 3.20 1 4 -14 130.09 10.40 -1 -4 14 155.98 9.10 -1 -4 14 129.69 9.10 -1 -4 14 149.09 13.20 -1 -4 14 146.99 10.60 0 4 -14 9.60 4.10 0 4 -14 1.00 1.90 0 -4 14 2.40 1.90 0 -4 14 1.80 2.70 0 -4 14 0.90 1.70 0 -4 14 -3.00 3.90 -1 4 -14 87.79 8.90 -1 4 -14 93.79 8.00 1 -4 14 117.69 9.60 1 -4 14 108.49 8.20 1 -4 14 97.19 8.30 1 -4 14 77.19 7.90 -2 4 -14 1.00 3.00 -2 4 -14 6.80 3.50 -2 4 -14 5.00 3.40 2 -4 14 0.80 2.90 2 -4 14 -1.90 3.10 2 -4 14 -1.40 3.30 -3 4 -14 3.00 2.60 -3 4 -14 2.60 2.50 -3 4 -14 4.60 3.70 3 -4 14 0.40 3.70 3 -4 14 -3.10 3.90 3 -4 14 -5.70 2.20 -4 4 -14 27.40 2.90 -4 4 -14 25.30 5.80 -4 4 -14 28.70 2.70 4 -4 14 32.10 6.50 4 -4 14 27.40 6.70 -5 4 -14 42.90 7.30 5 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2.60 -2 3 -14 6.30 3.00 -2 3 -14 5.70 3.30 2 -3 14 8.70 3.30 2 -3 14 7.70 3.00 2 -3 14 4.30 3.40 2 -3 14 10.80 3.60 -3 3 -14 -0.80 2.30 -3 3 -14 1.40 3.40 -3 3 -14 3.80 2.80 3 -3 14 4.40 3.30 3 -3 14 2.60 4.00 3 -3 14 2.10 3.60 -4 3 -14 49.70 6.00 -4 3 -14 39.20 3.00 -4 3 -14 44.00 3.00 4 -3 14 41.40 7.10 4 -3 14 51.89 7.60 -5 3 -14 30.10 6.40 5 -3 14 31.50 7.00 -6 3 -14 -7.40 5.40 6 -3 14 4.10 6.80 -7 3 -14 -1.30 5.90 -8 3 -14 3.80 7.20 8 -3 14 -5.50 8.30 -9 3 -14 -10.00 7.90 9 -3 14 -12.40 9.00 9 2 -14 3.00 6.50 9 2 -14 -1.90 6.20 -9 -2 14 2.10 9.60 8 2 -14 -3.40 4.90 8 2 -14 5.70 5.60 8 2 -14 5.40 5.80 -8 -2 14 2.50 8.80 7 2 -14 3.00 3.90 7 2 -14 5.60 4.00 7 2 -14 3.90 4.70 -7 -2 14 4.40 7.70 6 2 -14 98.69 9.80 6 2 -14 81.99 8.40 6 2 -14 102.39 8.20 -6 -2 14 75.59 12.60 5 2 -14 -0.10 2.40 5 2 -14 -0.50 2.30 5 2 -14 0.50 1.90 -5 -2 14 3.00 5.90 4 2 -14 0.60 3.00 4 2 -14 0.40 0.90 4 2 -14 -1.60 4.80 4 2 -14 -0.80 1.30 -4 -2 14 -2.00 3.70 -4 -2 14 1.20 5.30 3 2 -14 109.49 8.70 3 2 -14 116.79 11.60 -3 -2 14 106.69 9.50 -3 -2 14 100.29 10.70 2 2 -14 62.19 8.00 2 2 -14 46.80 5.00 -2 -2 14 55.49 7.90 -2 -2 14 53.09 5.90 1 2 -14 44.80 6.70 1 2 -14 44.10 4.60 -1 -2 14 35.80 4.30 -1 -2 14 40.30 2.80 -1 -2 14 35.60 3.00 -1 -2 14 41.00 6.70 0 2 -14 230.38 15.80 0 2 -14 192.08 16.60 0 -2 14 270.97 17.50 0 -2 14 212.28 15.20 0 -2 14 230.78 14.90 0 -2 14 235.98 15.80 1 -2 14 553.44 37.80 1 -2 14 592.24 37.90 1 -2 14 534.85 38.30 1 -2 14 655.33 37.90 -2 2 -14 71.29 7.20 2 -2 14 77.39 7.40 2 -2 14 77.99 7.30 2 -2 14 82.19 7.00 2 -2 14 74.69 7.60 -3 2 -14 104.39 9.10 -3 2 -14 87.89 7.60 3 -2 14 112.59 9.50 3 -2 14 97.99 7.80 3 -2 14 105.19 8.30 3 -2 14 102.59 9.60 -4 2 -14 92.99 6.20 -4 2 -14 91.59 8.60 4 -2 14 88.79 9.80 4 -2 14 86.39 8.30 4 -2 14 96.99 10.30 -5 2 -14 6.90 3.90 5 -2 14 9.60 5.80 5 -2 14 -0.10 6.20 -6 2 -14 354.16 25.40 6 -2 14 348.07 27.10 -7 2 -14 21.80 6.90 7 -2 14 28.60 8.30 -8 2 -14 7.00 7.00 8 -2 14 18.50 8.10 -9 2 -14 3.70 6.20 9 -2 14 3.20 9.20 9 1 -14 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-10.10 4.60 -1 -3 -27 2.10 5.70 1 3 27 6.60 8.00 1 3 27 4.60 5.50 -2 -3 -27 10.60 6.60 -2 -3 -27 -1.70 5.30 2 3 27 7.00 7.70 -3 -3 -27 -2.40 5.70 -3 -3 -27 3.10 7.10 3 3 27 -10.10 8.00 -4 -3 -27 30.80 7.40 4 3 27 12.70 8.20 -5 -3 -27 25.00 7.80 5 3 27 3.70 9.90 4 -4 -27 1.00 6.40 3 -4 -27 18.20 6.10 3 -4 -27 8.60 4.80 -3 4 27 14.30 10.40 2 -4 -27 22.00 5.70 2 -4 -27 30.70 6.70 -2 4 27 14.20 9.80 1 -4 -27 -0.30 5.40 1 -4 -27 8.30 5.20 -1 4 27 5.70 8.70 0 -4 -27 12.40 5.90 0 -4 -27 -3.00 5.30 0 4 27 8.60 8.80 -1 -4 -27 8.80 5.30 -1 -4 -27 8.40 6.20 -2 -4 -27 -11.20 6.10 -2 -4 -27 4.90 6.60 2 4 27 1.50 8.50 -3 -4 -27 6.30 6.00 -3 -4 -27 6.30 6.50 3 4 27 19.70 8.60 -4 -4 -27 4.60 7.40 -4 -4 -27 5.80 6.60 4 4 27 11.60 8.30 -5 -4 -27 22.00 8.10 -5 -4 -27 15.60 8.70 5 4 27 -13.90 7.20 5 4 27 7.50 9.10 3 -5 -27 -12.00 5.70 3 -5 -27 15.10 5.30 -3 5 27 15.60 10.80 2 -5 -27 9.90 5.30 2 -5 -27 9.20 5.60 -2 5 27 -2.90 9.60 1 -5 -27 4.50 5.10 1 -5 -27 12.20 5.80 -1 5 27 8.60 8.70 0 -5 -27 -0.20 5.30 0 -5 -27 21.40 6.20 0 5 27 4.80 8.90 -1 -5 -27 13.90 6.80 1 5 27 13.00 8.20 -2 -5 -27 5.60 7.30 2 5 27 12.20 9.10 -3 -5 -27 8.10 7.20 3 5 27 3.10 8.40 -4 -5 -27 4.00 6.90 -4 -5 -27 3.10 8.20 4 5 27 -0.10 8.10 2 -6 -27 12.90 6.30 2 -6 -27 10.00 5.60 -2 6 27 13.60 9.90 1 -6 -27 -0.70 5.70 1 -6 -27 9.40 6.40 -1 6 27 -3.70 9.30 0 -6 -27 -5.00 5.70 0 -6 -27 -2.90 6.30 0 6 27 10.20 8.90 -1 -6 -27 0.50 5.20 -1 -6 -27 16.00 7.20 1 6 27 5.10 8.70 -2 -6 -27 -6.30 5.50 -2 -6 -27 23.00 7.90 2 6 27 5.80 8.70 -3 -6 -27 20.40 8.50 -3 -6 -27 12.40 7.20 -4 -6 -27 1.80 7.70 4 6 27 3.90 8.90 2 -7 -27 -1.80 5.50 2 -7 -27 8.20 7.10 -2 7 27 9.10 10.30 1 -7 -27 2.70 6.00 1 -7 -27 9.80 6.80 -1 7 27 2.40 8.90 0 -7 -27 -2.70 6.90 0 7 27 18.30 10.20 -1 -7 -27 -11.10 7.60 -1 -7 -27 -0.20 6.00 1 7 27 7.90 8.60 -2 -7 -27 7.10 6.70 -2 -7 -27 -9.60 7.80 2 7 27 11.90 9.20 -3 -7 -27 20.30 8.50 -3 -7 -27 5.60 7.10 3 7 27 29.10 10.10 0 -8 -27 10.10 11.40 0 -8 -27 9.80 7.60 0 8 27 -8.20 9.20 -1 -8 -27 -5.00 5.70 -1 -8 -27 -5.90 7.00 1 8 27 9.20 9.40 -2 -8 -27 6.30 6.30 -2 -8 -27 10.90 8.30 2 8 27 5.80 9.30 2 6 -28 1.10 6.70 1 6 -28 3.90 6.50 -1 -6 28 23.70 10.70 0 6 -28 3.00 6.70 0 -6 28 16.00 13.10 -1 6 -28 1.40 6.70 1 -6 28 13.10 10.10 3 5 -28 -7.60 6.30 -3 -5 28 24.70 12.10 2 5 -28 -3.70 6.30 -2 -5 28 -3.20 10.30 1 5 -28 9.10 6.60 -1 -5 28 12.10 11.50 0 5 -28 29.30 7.50 0 -5 28 14.10 18.40 -1 5 -28 10.60 5.10 1 -5 28 -2.50 9.60 -2 5 -28 5.70 7.20 2 -5 28 16.00 8.50 3 4 -28 7.20 4.80 -3 -4 28 -1.80 11.40 2 4 -28 -4.20 5.80 -2 -4 28 23.00 11.30 1 4 -28 11.20 6.30 -1 -4 28 23.80 11.30 0 -4 28 12.60 10.50 -1 4 -28 -2.40 6.60 1 -4 28 -6.00 8.80 -2 4 -28 14.40 7.10 2 -4 28 15.40 8.70 2 -4 28 9.80 7.80 -3 4 -28 15.60 7.80 3 -4 28 -10.90 7.40 4 3 -28 13.20 5.20 -3 -3 28 36.50 12.20 2 3 -28 1.60 5.70 -2 -3 28 -7.10 10.00 1 3 -28 8.80 6.30 -1 -3 28 5.30 10.50 0 3 -28 0.80 6.00 0 -3 28 -14.70 9.70 1 -3 28 0.60 9.50 -2 3 -28 16.40 7.30 2 -3 28 30.30 10.10 2 -3 28 33.50 7.60 -3 3 -28 36.40 8.80 3 -3 28 51.49 9.50 3 -3 28 81.09 11.80 4 2 -28 1.60 6.20 -4 -2 28 6.40 11.80 3 2 -28 4.80 5.90 -3 -2 28 -6.50 11.20 2 2 -28 -1.80 5.50 -2 -2 28 -2.00 11.20 1 2 -28 0.80 5.50 -1 -2 28 -15.40 9.70 0 2 -28 6.20 5.50 0 -2 28 4.20 10.40 -1 2 -28 9.10 6.30 1 -2 28 0.70 8.40 1 -2 28 8.10 5.50 -2 2 -28 18.10 7.10 2 -2 28 7.80 8.60 2 -2 28 -3.40 6.50 -3 2 -28 9.10 6.90 3 -2 28 -1.00 8.00 3 -2 28 -1.40 7.20 -4 2 -28 20.10 8.20 4 -2 28 -5.90 8.90 4 1 -28 -1.50 5.80 -4 -1 28 3.00 11.40 3 1 -28 15.20 4.70 -3 -1 28 -3.80 10.30 2 1 -28 5.10 5.70 -2 -1 28 3.60 10.00 1 1 -28 -1.20 5.30 -1 -1 28 3.00 9.10 0 1 -28 10.30 6.00 0 -1 28 -0.40 5.90 0 -1 28 3.00 9.90 -1 1 -28 6.00 6.00 1 -1 28 2.20 5.80 1 -1 28 0.70 8.90 -2 1 -28 5.60 6.30 2 -1 28 2.20 6.80 2 -1 28 -6.50 8.20 -3 1 -28 22.40 7.60 3 -1 28 -6.30 7.60 3 -1 28 -0.70 8.00 -4 1 -28 7.20 7.40 4 -1 28 20.50 9.60 4 0 -28 -3.20 5.90 -4 0 28 17.70 12.70 3 0 -28 14.30 6.00 -3 0 28 8.70 10.10 2 0 -28 -2.70 5.30 -2 0 28 15.00 10.20 1 0 -28 11.60 5.90 -1 0 28 14.60 10.00 0 0 -28 23.80 6.50 0 0 28 45.50 13.30 0 0 28 23.50 6.30 -1 0 -28 6.20 6.00 1 0 28 -4.40 6.00 1 0 28 -7.10 9.30 -2 0 -28 6.20 6.50 2 0 28 18.60 7.40 2 0 28 17.30 9.00 -3 0 -28 -1.30 6.10 3 0 28 -6.70 7.90 3 0 28 -10.30 7.50 -4 0 -28 -6.10 6.90 4 0 28 -7.60 8.90 4 0 28 11.90 9.80 4 -1 -28 0.50 6.30 -4 1 28 -0.20 11.10 3 -1 -28 -3.60 5.70 -3 1 28 -12.90 10.20 2 -1 -28 8.70 5.50 -2 1 28 7.30 9.90 1 -1 -28 6.70 5.50 -1 1 28 6.10 9.60 0 -1 -28 2.20 5.40 0 1 28 2.40 5.70 -1 -1 -28 16.70 6.10 1 1 28 14.60 7.30 1 1 28 32.50 10.60 -2 -1 -28 1.00 5.60 2 1 28 16.40 9.50 2 1 28 -16.10 6.70 -3 -1 -28 11.50 6.70 3 1 28 18.00 8.30 3 1 28 15.20 8.70 -4 -1 -28 4.50 6.90 4 1 28 15.40 7.80 4 1 28 8.20 8.80 3 -2 -28 9.90 6.00 -3 2 28 19.40 10.70 2 -2 -28 -6.30 5.00 -2 2 28 12.00 10.50 1 -2 -28 3.70 4.80 1 -2 -28 -5.10 5.20 -1 2 28 -4.10 9.60 0 -2 -28 5.20 5.50 0 -2 -28 -8.10 5.20 0 2 28 -8.90 8.80 -1 -2 -28 3.90 6.20 -1 -2 -28 0.80 5.40 1 2 28 3.60 8.60 -2 -2 -28 18.40 6.60 -2 -2 -28 25.50 7.10 2 2 28 24.50 10.00 2 2 28 6.60 7.40 -3 -2 -28 10.80 7.20 3 2 28 10.70 8.70 3 2 28 22.30 9.40 -4 -2 -28 5.90 7.30 4 2 28 12.10 8.20 4 2 28 -9.30 9.70 3 -3 -28 0.50 5.90 -3 3 28 -0.20 10.20 2 -3 -28 8.50 5.60 -2 3 28 4.00 9.80 1 -3 -28 14.20 5.50 1 -3 -28 2.30 5.30 -1 3 28 9.30 10.10 0 -3 -28 6.80 5.40 0 -3 -28 6.90 5.90 0 3 28 11.20 9.70 -1 -3 -28 9.10 5.60 -1 -3 -28 4.60 6.30 -2 -3 -28 5.70 6.40 -2 -3 -28 -5.60 5.60 2 3 28 11.80 8.80 -3 -3 -28 0.10 7.50 -3 -3 -28 -3.60 6.30 3 3 28 19.50 9.00 -4 -3 -28 0.90 6.70 4 3 28 4.90 8.30 4 3 28 -2.10 9.50 3 -4 -28 2.90 5.90 -3 4 28 0.60 10.50 2 -4 -28 5.10 5.20 2 -4 -28 -4.80 5.40 -2 4 28 11.10 9.90 1 -4 -28 2.00 5.50 1 -4 -28 -1.90 5.20 -1 4 28 7.80 9.40 0 -4 -28 11.40 6.20 0 -4 -28 4.40 5.30 0 4 28 6.00 8.90 -1 -4 -28 6.30 5.70 -1 -4 -28 4.40 6.40 1 4 28 -6.50 8.50 -2 -4 -28 5.50 6.20 -2 -4 -28 -11.60 6.70 2 4 28 3.90 9.40 -3 -4 -28 8.10 6.30 -3 -4 -28 15.60 8.50 3 4 28 5.00 9.20 -4 -4 -28 6.50 8.60 -4 -4 -28 11.80 7.10 4 4 28 -9.70 8.30 2 -5 -28 11.20 5.70 2 -5 -28 6.50 5.70 -2 5 28 6.30 10.80 1 -5 -28 -5.40 6.00 1 -5 -28 11.10 5.90 -1 5 28 25.20 9.90 0 -5 -28 0.20 5.40 0 -5 -28 21.60 6.90 0 5 28 4.50 9.10 -1 -5 -28 14.40 7.10 -1 -5 -28 4.80 5.90 1 5 28 7.30 9.80 -2 -5 -28 12.10 7.70 -2 -5 -28 -5.20 5.50 2 5 28 3.80 9.10 -3 -5 -28 5.10 9.70 -3 -5 -28 7.90 7.20 3 5 28 15.20 9.80 1 -6 -28 1.30 5.70 1 -6 -28 -16.10 6.40 -1 6 28 -8.70 9.10 0 -6 -28 7.10 7.10 0 -6 -28 9.70 5.70 0 6 28 34.10 10.70 -1 -6 -28 -5.80 5.50 -1 -6 -28 6.20 7.30 1 6 28 -10.00 8.50 -2 -6 -28 -0.80 6.80 2 6 28 16.30 9.30 -3 -6 -28 1.60 8.50 -3 -6 -28 16.90 7.00 3 6 28 12.30 9.50 0 -7 -28 9.20 7.80 0 -7 -28 5.20 6.50 0 7 28 7.50 9.90 -1 -7 -28 -5.70 6.50 -1 -7 -28 11.90 9.60 1 7 28 13.50 10.20 -2 -7 -28 14.60 8.70 -2 -7 -28 -9.30 7.20 2 7 28 18.00 9.80 1 5 -29 2.50 6.70 -1 -5 29 23.70 11.20 0 5 -29 11.60 6.60 0 -5 29 -1.50 11.20 -1 5 -29 15.70 7.50 2 4 -29 26.20 7.60 -2 -4 29 18.80 11.90 1 4 -29 5.30 6.80 -1 -4 29 31.80 11.30 0 4 -29 -14.90 6.20 0 -4 29 5.50 10.30 -1 4 -29 3.10 6.40 1 -4 29 5.60 10.50 -2 4 -29 17.50 7.90 2 -4 29 14.40 9.40 2 3 -29 0.00 6.50 -2 -3 29 -13.50 10.70 1 3 -29 -3.00 6.20 -1 -3 29 20.20 10.90 0 3 -29 3.10 4.70 0 -3 29 19.20 11.10 -1 3 -29 0.10 6.40 1 -3 29 1.60 9.30 -2 3 -29 11.60 7.10 2 -3 29 8.10 9.20 3 2 -29 -7.90 5.90 -3 -2 29 -17.90 11.70 2 2 -29 7.20 6.40 -2 -2 29 16.00 11.80 1 2 -29 -4.20 5.50 -1 -2 29 13.70 11.30 0 2 -29 0.50 5.80 0 -2 29 -9.90 9.40 -1 2 -29 14.70 6.60 1 -2 29 31.20 11.30 -2 2 -29 -8.10 4.80 2 -2 29 5.20 9.90 2 -2 29 -3.70 7.50 -3 2 -29 14.60 7.50 3 -2 29 20.10 8.60 3 -2 29 17.00 8.40 3 1 -29 -4.50 5.90 -3 -1 29 8.00 11.80 2 1 -29 1.00 5.60 -2 -1 29 -4.70 11.30 1 1 -29 23.90 7.10 -1 -1 29 -8.60 9.90 0 1 -29 0.20 6.00 0 -1 29 13.90 11.30 -1 1 -29 -5.90 4.30 1 -1 29 -3.50 7.90 1 -1 29 13.90 10.50 -2 1 -29 7.70 5.20 2 -1 29 25.70 10.10 2 -1 29 7.90 7.50 -3 1 -29 23.40 8.00 3 -1 29 21.90 8.70 3 -1 29 24.50 9.30 3 0 -29 10.30 5.00 -3 0 29 8.40 11.50 2 0 -29 -11.20 5.50 -2 0 29 19.70 12.00 1 0 -29 -1.90 5.70 -1 0 29 20.60 10.30 0 0 -29 9.40 6.00 0 0 29 1.70 10.00 -1 0 -29 9.70 5.00 1 0 29 -6.30 9.50 1 0 29 -2.80 6.80 -2 0 -29 6.40 6.30 2 0 29 4.50 9.00 2 0 29 -0.70 7.20 -3 0 -29 -0.10 6.40 3 0 29 -8.40 8.00 3 0 29 2.20 8.90 3 -1 -29 8.20 6.10 -3 1 29 10.80 12.20 2 -1 -29 11.30 6.00 -2 1 29 -1.70 10.20 1 -1 -29 -3.50 5.50 -1 1 29 10.90 11.30 0 -1 -29 -2.70 5.40 0 1 29 -4.10 7.00 0 1 29 17.30 10.30 -1 -1 -29 -7.00 5.40 1 1 29 0.60 7.00 1 1 29 17.40 11.00 -2 -1 -29 13.40 6.70 2 1 29 2.00 7.70 2 1 29 11.50 9.70 -3 -1 -29 -13.50 6.80 3 1 29 -1.00 8.70 3 1 29 20.80 9.50 2 -2 -29 5.20 6.30 -2 2 29 7.50 10.50 1 -2 -29 10.60 6.10 -1 2 29 -7.70 9.50 0 -2 -29 2.00 5.40 0 -2 -29 1.90 5.70 0 2 29 23.80 10.70 -1 -2 -29 10.10 6.00 -1 -2 -29 5.10 6.40 1 2 29 -3.60 12.00 -2 -2 -29 -11.60 5.80 2 2 29 0.20 7.90 2 2 29 -1.20 9.00 -3 -2 -29 -2.80 6.70 3 2 29 -2.50 8.70 3 2 29 10.20 9.50 2 -3 -29 8.20 5.90 -2 3 29 15.00 11.20 1 -3 -29 -3.50 5.40 -1 3 29 -5.50 9.80 0 -3 -29 -10.50 5.50 0 -3 -29 -0.60 5.70 0 3 29 -4.70 9.00 -1 -3 -29 1.40 5.80 -1 -3 -29 -6.00 6.40 1 3 29 12.70 10.00 -2 -3 -29 0.40 6.20 -2 -3 -29 -0.10 7.50 2 3 29 18.00 11.00 -3 -3 -29 2.70 6.70 -3 -3 -29 -1.30 8.20 3 3 29 12.20 9.50 3 3 29 7.30 9.30 2 -4 -29 10.30 6.20 1 -4 -29 -6.10 5.50 1 -4 -29 -1.50 5.80 -1 4 29 23.10 11.40 0 -4 -29 14.50 6.40 0 -4 -29 -5.90 5.60 0 4 29 1.20 9.40 -1 -4 -29 -13.30 5.60 -1 -4 -29 -2.10 6.80 1 4 29 -9.70 9.80 -2 -4 -29 -6.30 7.60 -2 -4 -29 -11.20 6.00 2 4 29 -7.80 9.40 -3 -4 -29 10.80 7.60 -3 -4 -29 12.20 9.90 3 4 29 10.50 10.30 1 -5 -29 5.70 6.50 1 -5 -29 -14.10 5.90 -1 5 29 8.10 10.10 0 -5 -29 9.50 7.10 0 -5 -29 2.80 6.80 0 5 29 -2.20 9.30 -1 -5 -29 0.10 6.00 -1 -5 -29 4.30 7.50 1 5 29 0.20 9.20 -2 -5 -29 2.20 6.10 -2 -5 -29 8.90 8.40 2 5 29 13.90 10.50 1 3 -30 -13.10 6.30 0 3 -30 -10.20 6.30 0 -3 30 27.70 12.70 1 2 -30 -6.80 6.10 -1 -2 30 6.60 11.00 0 2 -30 6.50 6.30 0 -2 30 -17.30 10.10 -1 2 -30 5.10 6.80 1 -2 30 -2.70 12.40 2 1 -30 -10.10 4.60 1 1 -30 -6.50 5.90 -1 -1 30 0.00 11.60 0 1 -30 15.10 6.70 0 -1 30 6.30 11.40 -1 1 -30 16.10 6.80 -2 1 -30 2.90 7.30 2 -1 30 -0.70 10.60 2 0 -30 12.50 6.40 1 0 -30 12.90 6.50 -1 0 30 15.50 10.90 0 0 -30 -1.00 5.40 0 0 30 1.80 10.10 -1 0 -30 -1.30 6.30 1 0 30 5.90 13.50 -2 0 -30 -9.50 6.60 2 0 30 16.60 8.70 2 0 30 -7.80 10.70 1 -1 -30 13.20 6.90 -1 1 30 23.20 11.30 0 -1 -30 21.20 6.90 0 1 30 15.50 10.60 -1 -1 -30 -3.40 6.00 1 1 30 10.10 11.00 1 1 30 -3.80 8.80 -2 -1 -30 5.70 6.50 2 1 30 34.60 11.20 2 1 30 0.10 8.60 1 -2 -30 9.20 6.40 -1 2 30 18.00 11.70 0 -2 -30 2.00 6.10 0 2 30 6.20 10.60 -1 -2 -30 -3.30 6.50 1 2 30 21.70 10.40 1 2 30 12.20 8.70 -2 -2 -30 23.40 7.40 2 2 30 8.80 9.00 1 -3 -30 21.70 6.90 0 -3 -30 -12.80 5.80 0 3 30 0.80 10.30 -1 -3 -30 19.40 6.80 -1 -3 -30 10.90 7.10 1 3 30 31.40 11.00 -2 -3 -30 -5.60 6.90 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 49279 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 0.32282(10) 0.63064(6) 0.65884(3) 0.0536(3) Uani 1 1 d . . . . . Cl2 Cl 0.71655(14) 0.30377(7) 0.88178(4) 0.0882(4) Uani 1 1 d . . . . . Cl3 Cl 0.33337(12) 0.20807(6) 0.60608(4) 0.0688(3) Uani 1 1 d . . . . . N1 N 0.2368(3) 0.43742(18) 0.66434(12) 0.0523(8) Uani 1 1 d . . . . . N2 N 0.5408(3) 0.64755(16) 0.73955(10) 0.0411(7) Uani 1 1 d . . . . . N3 N 0.8616(3) 0.44446(17) 0.93494(10) 0.0459(7) Uani 1 1 d . . . . . N4 N 0.6905(3) 0.14260(18) 0.95187(11) 0.0522(7) Uani 1 1 d . . . . . N5 N 0.3988(3) 0.07612(19) 0.69409(10) 0.0530(8) Uani 1 1 d . . . . . N6 N 0.1527(3) 0.12575(19) 0.52877(11) 0.0548(8) Uani 1 1 d . . . . . C1 C 0.3933(3) 0.54150(19) 0.70052(12) 0.0386(8) Uani 1 1 d . . . . . C2 C 0.3466(3) 0.4541(2) 0.69861(13) 0.0442(8) Uani 1 1 d . . . . . C3 C 0.4065(4) 0.3844(2) 0.73211(14) 0.0512(9) Uani 1 1 d . . . . . H3 H 0.376597 0.325709 0.731077 0.061 Uiso 1 1 calc R U . . . C4 C 0.5091(4) 0.4003(2) 0.76683(14) 0.0540(9) Uani 1 1 d . . . . . H4 H 0.548730 0.352468 0.789102 0.065 Uiso 1 1 calc R U . . . C5 C 0.5540(3) 0.4866(2) 0.76891(13) 0.0477(9) Uani 1 1 d . . . . . H5 H 0.623174 0.497105 0.792804 0.057 Uiso 1 1 calc R U . . . C6 C 0.4971(3) 0.5574(2) 0.73587(12) 0.0378(8) Uani 1 1 d . . . . . C7 C 0.1042(4) 0.4077(2) 0.67999(17) 0.0562(10) Uani 1 1 d . . . . . C8 C 0.0512(4) 0.3915(2) 0.72921(18) 0.0663(11) Uani 1 1 d . . . . . H8 H 0.102835 0.402156 0.758489 0.080 Uiso 1 1 calc R U . . . C9 C -0.0817(5) 0.3589(3) 0.7335(2) 0.0901(15) Uani 1 1 d . . . . . H9 H -0.120279 0.346882 0.766212 0.108 Uiso 1 1 calc R U . . . C10 C -0.1573(6) 0.3440(3) 0.6901(3) 0.108(2) Uani 1 1 d . . . . . H10 H -0.246019 0.321604 0.694206 0.129 Uiso 1 1 calc R U . . . C11 C -0.1076(5) 0.3609(3) 0.6409(3) 0.0990(17) Uani 1 1 d . . . . . H11 H -0.161119 0.350845 0.611989 0.119 Uiso 1 1 calc R U . . . C12 C 0.0271(5) 0.3938(3) 0.63575(19) 0.0688(11) Uani 1 1 d . . . . . C13 C 0.1150(5) 0.4131(2) 0.59217(18) 0.0716(12) Uani 1 1 d . . . . . C14 C 0.0987(7) 0.4073(3) 0.5387(2) 0.1077(18) Uani 1 1 d . . . . . H14 H 0.011604 0.393969 0.525555 0.129 Uiso 1 1 calc R U . . . C15 C 0.2106(9) 0.4211(4) 0.5062(2) 0.126(2) Uani 1 1 d . . . . . H15 H 0.199132 0.416976 0.470621 0.151 Uiso 1 1 calc R U . . . C16 C 0.3408(8) 0.4410(4) 0.5243(2) 0.121(2) Uani 1 1 d . . . . . H16 H 0.416347 0.448442 0.500783 0.145 Uiso 1 1 calc R U . . . C17 C 0.3613(6) 0.4504(3) 0.57775(18) 0.0893(14) Uani 1 1 d . . . . . H17 H 0.448402 0.464813 0.590409 0.107 Uiso 1 1 calc R U . . . C18 C 0.2460(5) 0.4373(2) 0.61038(16) 0.0628(11) Uani 1 1 d . . . . . C19 C 0.6820(4) 0.6678(2) 0.73043(12) 0.0396(8) Uani 1 1 d . . . . . C20 C 0.8048(4) 0.6106(2) 0.71232(13) 0.0519(9) Uani 1 1 d . . . . . H20 H 0.801796 0.548536 0.703939 0.062 Uiso 1 1 calc R U . . . C21 C 0.9317(4) 0.6490(3) 0.70714(14) 0.0617(10) Uani 1 1 d . . . . . H21 H 1.016482 0.612023 0.695266 0.074 Uiso 1 1 calc R U . . . C22 C 0.9359(4) 0.7414(3) 0.71923(15) 0.0637(11) Uani 1 1 d . . . . . H22 H 1.023457 0.765355 0.715201 0.076 Uiso 1 1 calc R U . . . C23 C 0.8144(4) 0.7984(3) 0.73696(13) 0.0550(10) Uani 1 1 d . . . . . H23 H 0.818583 0.860682 0.744596 0.066 Uiso 1 1 calc R U . . . C24 C 0.6843(4) 0.7616(2) 0.74338(12) 0.0398(8) Uani 1 1 d . . . . . C25 C 0.5405(4) 0.7989(2) 0.76173(12) 0.0412(8) Uani 1 1 d . . . . . C26 C 0.4760(4) 0.8843(2) 0.78249(13) 0.0525(9) Uani 1 1 d . . . . . H26 H 0.530220 0.933341 0.784897 0.063 Uiso 1 1 calc R U . . . C27 C 0.3343(5) 0.8959(2) 0.79915(13) 0.0579(10) Uani 1 1 d . . . . . H27 H 0.292530 0.952755 0.813231 0.070 Uiso 1 1 calc R U . . . C28 C 0.2510(4) 0.8240(2) 0.79544(13) 0.0573(10) Uani 1 1 d . . . . . H28 H 0.153969 0.833651 0.806878 0.069 Uiso 1 1 calc R U . . . C29 C 0.3093(4) 0.7382(2) 0.77509(13) 0.0497(9) Uani 1 1 d . . . . . H29 H 0.253362 0.690086 0.772426 0.060 Uiso 1 1 calc R U . . . C30 C 0.4536(4) 0.7268(2) 0.75893(12) 0.0409(8) Uani 1 1 d . . . . . C31 C 0.7781(3) 0.2931(2) 0.94397(11) 0.0416(8) Uani 1 1 d . . . . . C32 C 0.8472(3) 0.3626(2) 0.96443(12) 0.0403(8) Uani 1 1 d . . . . . C33 C 0.9017(4) 0.3512(2) 1.01345(13) 0.0559(10) Uani 1 1 d . . . . . H33 H 0.948294 0.397516 1.027525 0.067 Uiso 1 1 calc R U . . . C34 C 0.8877(5) 0.2717(2) 1.04185(14) 0.0687(12) Uani 1 1 d . . . . . H34 H 0.926565 0.263809 1.074838 0.082 Uiso 1 1 calc R U . . . C35 C 0.8168(4) 0.2039(2) 1.02180(14) 0.0579(10) Uani 1 1 d . . . . . H35 H 0.806634 0.150687 1.041521 0.070 Uiso 1 1 calc R U . . . C36 C 0.7608(3) 0.2138(2) 0.97299(12) 0.0420(8) Uani 1 1 d . . . . . C37 C 0.7480(4) 0.5137(2) 0.92149(13) 0.0467(9) Uani 1 1 d . . . . . C38 C 0.6035(4) 0.5239(3) 0.93757(15) 0.0633(10) Uani 1 1 d . . . . . H38 H 0.568996 0.480496 0.959885 0.076 Uiso 1 1 calc R U . . . C39 C 0.5121(5) 0.6009(3) 0.91939(17) 0.0760(12) Uani 1 1 d . . . . . H39 H 0.414090 0.609463 0.929651 0.091 Uiso 1 1 calc R U . . . C40 C 0.5634(5) 0.6655(3) 0.88613(16) 0.0713(12) Uani 1 1 d . . . . . H40 H 0.499976 0.717410 0.874821 0.086 Uiso 1 1 calc R U . . . C41 C 0.7062(5) 0.6539(2) 0.86977(14) 0.0608(10) Uani 1 1 d . . . . . H41 H 0.739587 0.697132 0.847039 0.073 Uiso 1 1 calc R U . . . C42 C 0.8012(4) 0.5771(2) 0.88730(12) 0.0451(9) Uani 1 1 d . . . . . C43 C 0.9531(4) 0.5437(2) 0.87818(12) 0.0458(9) Uani 1 1 d . . . . . C44 C 1.0632(5) 0.5753(3) 0.84812(14) 0.0666(11) Uani 1 1 d . . . . . H44 H 1.043419 0.628775 0.827429 0.080 Uiso 1 1 calc R U . . . C45 C 1.2009(6) 0.5263(3) 0.84959(17) 0.0839(13) Uani 1 1 d . . . . . H45 H 1.274987 0.547868 0.829878 0.101 Uiso 1 1 calc R U . . . C46 C 1.2341(4) 0.4461(3) 0.87930(17) 0.0765(12) Uani 1 1 d . . . . . H46 H 1.329119 0.414608 0.879297 0.092 Uiso 1 1 calc R U . . . C47 C 1.1263(4) 0.4122(2) 0.90908(15) 0.0616(10) Uani 1 1 d . . . . . H47 H 1.146765 0.357888 0.929043 0.074 Uiso 1 1 calc R U . . . C48 C 0.9877(4) 0.4620(2) 0.90805(12) 0.0437(8) Uani 1 1 d . . . . . C49 C 0.7607(4) 0.0687(2) 0.92243(13) 0.0491(9) Uani 1 1 d . . . . . C50 C 0.9042(5) 0.0520(3) 0.90563(15) 0.0657(11) Uani 1 1 d . . . . . H50 H 0.969039 0.093249 0.912845 0.079 Uiso 1 1 calc R U . . . C51 C 0.9479(5) -0.0278(3) 0.87784(17) 0.0886(14) Uani 1 1 d . . . . . H51 H 1.044234 -0.040670 0.865878 0.106 Uiso 1 1 calc R U . . . C52 C 0.8539(7) -0.0887(3) 0.86731(18) 0.0980(16) Uani 1 1 d . . . . . H52 H 0.888041 -0.142573 0.848768 0.118 Uiso 1 1 calc R U . . . C53 C 0.7109(6) -0.0729(3) 0.88324(16) 0.0778(13) Uani 1 1 d . . . . . H53 H 0.647879 -0.115125 0.875656 0.093 Uiso 1 1 calc R U . . . C54 C 0.6607(5) 0.0091(3) 0.91152(14) 0.0566(10) Uani 1 1 d . U . . . C55 C 0.5254(5) 0.0476(3) 0.93447(14) 0.0568(10) Uani 1 1 d . U . . . C56 C 0.3865(6) 0.0221(4) 0.93740(19) 0.0880(15) Uani 1 1 d . . . . . H56 H 0.368542 -0.032204 0.921364 0.106 Uiso 1 1 calc R U . . . C57 C 0.2776(6) 0.0757(5) 0.9634(2) 0.0994(19) Uani 1 1 d . . . . . H57 H 0.185640 0.057044 0.965226 0.119 Uiso 1 1 calc R U . . . C58 C 0.2983(5) 0.1583(4) 0.98768(18) 0.0914(15) Uani 1 1 d . . . . . H58 H 0.220710 0.193828 1.005167 0.110 Uiso 1 1 calc R U . . . C59 C 0.4359(5) 0.1877(3) 0.98571(16) 0.0713(12) Uani 1 1 d . . . . . H59 H 0.452582 0.242542 1.001445 0.086 Uiso 1 1 calc R U . . . C60 C 0.5455(4) 0.1310(3) 0.95920(14) 0.0530(9) Uani 1 1 d . . . . . C61 C 0.2741(3) 0.1015(2) 0.61210(12) 0.0433(8) Uani 1 1 d . . . . . C62 C 0.3105(3) 0.0455(2) 0.65544(12) 0.0437(8) Uani 1 1 d . . . . . C63 C 0.2594(4) -0.0389(2) 0.66131(12) 0.0523(9) Uani 1 1 d . . . . . H63 H 0.283031 -0.076101 0.690523 0.063 Uiso 1 1 calc R U . . . C64 C 0.1730(4) -0.0682(2) 0.62378(13) 0.0574(10) Uani 1 1 d . . . . . H64 H 0.138095 -0.125120 0.627878 0.069 Uiso 1 1 calc R U . . . C65 C 0.1385(4) -0.0140(2) 0.58063(13) 0.0536(9) Uani 1 1 d . . . . . H65 H 0.080556 -0.034618 0.555531 0.064 Uiso 1 1 calc R U . . . C66 C 0.1885(4) 0.0709(2) 0.57381(12) 0.0454(8) Uani 1 1 d . . . . . C67 C 0.5512(5) 0.0625(3) 0.69250(16) 0.0614(11) Uani 1 1 d . . . . . C68 C 0.6455(5) 0.0220(3) 0.65432(19) 0.0821(13) Uani 1 1 d . . . . . H68 H 0.611044 0.000645 0.623795 0.099 Uiso 1 1 calc R U . . . C69 C 0.7920(6) 0.0145(4) 0.6630(3) 0.117(2) Uani 1 1 d . . . . . H69 H 0.858397 -0.013441 0.638127 0.140 Uiso 1 1 calc R U . . . C70 C 0.8422(8) 0.0474(5) 0.7076(4) 0.136(3) Uani 1 1 d . . . . . H70 H 0.942527 0.041943 0.711742 0.164 Uiso 1 1 calc R U . . . C71 C 0.7517(7) 0.0879(4) 0.7463(3) 0.107(2) Uani 1 1 d . . . . . H71 H 0.788262 0.109119 0.776534 0.129 Uiso 1 1 calc R U . . . C72 C 0.5992(5) 0.0959(3) 0.73818(19) 0.0726(13) Uani 1 1 d . . . . . C73 C 0.4726(6) 0.1308(2) 0.76883(15) 0.0659(12) Uani 1 1 d . . . . . C74 C 0.4484(8) 0.1685(3) 0.8177(2) 0.0995(19) Uani 1 1 d . . . . . H74 H 0.526910 0.175986 0.838248 0.119 Uiso 1 1 calc R U . . . C75 C 0.3107(9) 0.1944(3) 0.83563(19) 0.108(2) Uani 1 1 d . . . . . H75 H 0.296627 0.219969 0.868632 0.130 Uiso 1 1 calc R U . . . C76 C 0.1879(7) 0.1847(3) 0.80672(19) 0.0953(16) Uani 1 1 d . . . . . H76 H 0.094645 0.203610 0.820448 0.114 Uiso 1 1 calc R U . . . C77 C 0.2067(5) 0.1461(2) 0.75691(15) 0.0697(11) Uani 1 1 d . . . . . H77 H 0.127861 0.139398 0.736365 0.084 Uiso 1 1 calc R U . . . C78 C 0.3476(5) 0.1188(2) 0.74033(13) 0.0526(10) Uani 1 1 d . . . . . C79 C 0.2523(5) 0.1457(2) 0.48934(13) 0.0550(10) Uani 1 1 d . . . . . C80 C 0.4002(5) 0.1184(3) 0.48585(15) 0.0687(11) Uani 1 1 d . . . . . H80 H 0.449117 0.081108 0.511510 0.082 Uiso 1 1 calc R U . . . C81 C 0.4741(5) 0.1481(3) 0.44285(18) 0.0852(13) Uani 1 1 d . . . . . H81 H 0.574513 0.130474 0.439512 0.102 Uiso 1 1 calc R U . . . C82 C 0.4017(7) 0.2031(3) 0.40499(18) 0.0932(15) Uani 1 1 d . . . . . H82 H 0.454331 0.222242 0.376581 0.112 Uiso 1 1 calc R U . . . C83 C 0.2538(6) 0.2303(3) 0.40812(15) 0.0757(13) Uani 1 1 d . . . . . H83 H 0.205870 0.267221 0.382111 0.091 Uiso 1 1 calc R U . . . C84 C 0.1758(5) 0.2012(2) 0.45156(14) 0.0588(10) Uani 1 1 d . . . . . C85 C 0.0267(5) 0.2177(2) 0.46850(14) 0.0574(10) Uani 1 1 d . . . . . C86 C -0.0986(6) 0.2708(3) 0.44954(18) 0.0838(14) Uani 1 1 d . . . . . H86 H -0.094155 0.303991 0.418473 0.101 Uiso 1 1 calc R U . . . C87 C -0.2276(6) 0.2742(3) 0.4763(2) 0.0935(15) Uani 1 1 d . . . . . H87 H -0.310818 0.309880 0.463249 0.112 Uiso 1 1 calc R U . . . C88 C -0.2375(5) 0.2251(3) 0.5230(2) 0.0875(14) Uani 1 1 d . . . . . H88 H -0.327108 0.227505 0.540455 0.105 Uiso 1 1 calc R U . . . C89 C -0.1132(5) 0.1724(3) 0.54377(16) 0.0701(11) Uani 1 1 d . . . . . H89 H -0.117594 0.140094 0.575147 0.084 Uiso 1 1 calc R U . . . C90 C 0.0158(4) 0.1702(2) 0.51592(14) 0.0540(10) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0601(6) 0.0408(5) 0.0617(6) 0.0106(4) -0.0149(5) -0.0125(4) Cl2 0.1394(11) 0.0729(7) 0.0606(7) 0.0093(5) -0.0419(7) -0.0372(7) Cl3 0.0946(8) 0.0474(5) 0.0679(6) 0.0032(5) -0.0174(6) -0.0201(5) N1 0.055(2) 0.0439(17) 0.063(2) -0.0016(14) -0.0096(16) -0.0235(15) N2 0.0354(17) 0.0276(15) 0.0621(18) -0.0024(13) -0.0039(14) -0.0096(13) N3 0.0530(19) 0.0325(15) 0.0530(18) 0.0072(13) 0.0011(15) -0.0103(14) N4 0.050(2) 0.0394(17) 0.071(2) -0.0040(15) -0.0039(16) -0.0177(15) N5 0.055(2) 0.063(2) 0.0452(18) 0.0003(15) -0.0136(15) -0.0198(16) N6 0.055(2) 0.0614(19) 0.0464(18) 0.0047(15) -0.0155(17) -0.0029(16) C1 0.038(2) 0.0286(17) 0.048(2) 0.0036(14) 0.0001(16) -0.0039(15) C2 0.041(2) 0.0329(19) 0.060(2) -0.0017(17) -0.0020(18) -0.0111(16) C3 0.049(2) 0.0290(19) 0.077(3) 0.0026(18) -0.002(2) -0.0132(17) C4 0.053(2) 0.036(2) 0.075(3) 0.0120(18) -0.012(2) -0.0104(18) C5 0.042(2) 0.042(2) 0.060(2) 0.0057(17) -0.0108(18) -0.0099(17) C6 0.0333(19) 0.0271(17) 0.054(2) -0.0004(15) -0.0017(16) -0.0080(15) C7 0.050(2) 0.033(2) 0.087(3) -0.0069(19) -0.012(2) -0.0079(18) C8 0.056(3) 0.047(2) 0.098(3) 0.004(2) 0.001(2) -0.016(2) C9 0.058(3) 0.065(3) 0.149(5) -0.002(3) 0.012(3) -0.017(2) C10 0.058(4) 0.073(3) 0.195(7) -0.032(4) 0.006(4) -0.019(3) C11 0.062(4) 0.075(3) 0.164(6) -0.045(4) -0.033(3) -0.015(3) C12 0.061(3) 0.048(2) 0.099(4) -0.021(2) -0.023(3) -0.007(2) C13 0.098(4) 0.043(2) 0.075(3) -0.018(2) -0.038(3) -0.008(2) C14 0.139(5) 0.073(3) 0.112(5) -0.021(3) -0.047(4) -0.014(3) C15 0.203(8) 0.102(4) 0.083(4) -0.034(3) -0.029(5) -0.047(5) C16 0.188(6) 0.104(4) 0.081(4) -0.021(3) 0.022(4) -0.064(4) C17 0.125(4) 0.076(3) 0.076(3) -0.016(2) 0.006(3) -0.047(3) C18 0.085(3) 0.040(2) 0.067(3) -0.0083(19) -0.014(3) -0.017(2) C19 0.039(2) 0.0350(19) 0.047(2) 0.0083(15) -0.0090(17) -0.0132(17) C20 0.043(2) 0.045(2) 0.069(2) 0.0089(18) -0.0064(19) -0.0087(19) C21 0.042(2) 0.064(3) 0.080(3) 0.018(2) -0.004(2) -0.013(2) C22 0.044(3) 0.074(3) 0.079(3) 0.024(2) -0.017(2) -0.029(2) C23 0.067(3) 0.049(2) 0.055(2) 0.0161(18) -0.020(2) -0.029(2) C24 0.045(2) 0.0364(19) 0.0407(19) 0.0120(15) -0.0136(17) -0.0151(17) C25 0.053(2) 0.0281(18) 0.044(2) 0.0069(15) -0.0138(17) -0.0096(17) C26 0.077(3) 0.034(2) 0.049(2) 0.0061(16) -0.017(2) -0.014(2) C27 0.083(3) 0.037(2) 0.051(2) -0.0055(17) -0.004(2) 0.002(2) C28 0.055(2) 0.053(2) 0.061(2) -0.0041(19) 0.0070(19) 0.000(2) C29 0.052(3) 0.041(2) 0.057(2) 0.0003(17) 0.0014(19) -0.0091(18) C30 0.047(2) 0.0337(19) 0.044(2) 0.0067(15) -0.0099(17) -0.0103(17) C31 0.048(2) 0.0400(19) 0.0385(19) -0.0009(15) -0.0072(16) -0.0108(16) C32 0.046(2) 0.0328(18) 0.043(2) 0.0025(15) 0.0010(17) -0.0113(16) C33 0.074(3) 0.042(2) 0.055(2) -0.0033(17) -0.021(2) -0.0172(19) C34 0.112(3) 0.048(2) 0.048(2) 0.0104(18) -0.030(2) -0.016(2) C35 0.082(3) 0.041(2) 0.053(2) 0.0100(17) -0.007(2) -0.018(2) C36 0.046(2) 0.0341(19) 0.047(2) -0.0019(16) -0.0033(17) -0.0096(16) C37 0.056(3) 0.0350(19) 0.050(2) 0.0016(16) -0.0009(19) -0.0120(18) C38 0.064(3) 0.052(2) 0.073(3) 0.006(2) 0.005(2) -0.008(2) C39 0.070(3) 0.062(3) 0.092(3) -0.002(2) -0.002(3) 0.005(2) C40 0.091(4) 0.049(2) 0.070(3) 0.003(2) -0.023(3) 0.006(2) C41 0.092(3) 0.043(2) 0.048(2) 0.0038(18) -0.010(2) -0.010(2) C42 0.068(3) 0.0345(19) 0.0346(19) -0.0003(15) -0.0093(18) -0.0116(19) C43 0.063(3) 0.0357(19) 0.041(2) -0.0029(16) 0.0006(18) -0.0157(18) C44 0.086(3) 0.053(2) 0.063(3) 0.005(2) 0.011(2) -0.020(2) C45 0.092(4) 0.070(3) 0.092(3) 0.004(3) 0.029(3) -0.026(3) C46 0.061(3) 0.066(3) 0.103(3) -0.005(3) 0.018(3) -0.011(2) C47 0.066(3) 0.041(2) 0.079(3) 0.0008(19) 0.000(2) -0.014(2) C48 0.052(2) 0.0339(19) 0.048(2) -0.0067(16) -0.0024(18) -0.0164(18) C49 0.063(3) 0.036(2) 0.052(2) -0.0001(17) -0.014(2) -0.018(2) C50 0.065(3) 0.059(3) 0.074(3) -0.013(2) -0.009(2) -0.010(2) C51 0.096(4) 0.078(3) 0.088(3) -0.028(3) -0.003(3) 0.001(3) C52 0.139(5) 0.070(3) 0.085(4) -0.025(3) -0.016(4) -0.008(4) C53 0.129(4) 0.052(3) 0.061(3) -0.002(2) -0.037(3) -0.034(3) C54 0.073(3) 0.052(2) 0.050(2) 0.0108(19) -0.021(2) -0.024(2) C55 0.072(3) 0.057(2) 0.051(2) 0.0261(19) -0.030(2) -0.039(2) C56 0.094(4) 0.105(4) 0.078(3) 0.044(3) -0.037(3) -0.055(3) C57 0.075(4) 0.143(5) 0.093(4) 0.059(4) -0.033(3) -0.057(4) C58 0.064(3) 0.130(5) 0.075(3) 0.045(3) 0.003(3) -0.001(3) C59 0.057(3) 0.081(3) 0.077(3) 0.027(2) -0.007(2) -0.013(3) C60 0.049(3) 0.057(2) 0.054(2) 0.0208(19) -0.008(2) -0.015(2) C61 0.049(2) 0.0387(19) 0.042(2) -0.0046(16) -0.0040(17) -0.0069(16) C62 0.046(2) 0.048(2) 0.037(2) -0.0053(16) -0.0039(16) -0.0069(17) C63 0.066(3) 0.053(2) 0.039(2) 0.0070(17) -0.0045(18) -0.0129(19) C64 0.074(3) 0.051(2) 0.052(2) -0.0030(19) -0.009(2) -0.027(2) C65 0.061(3) 0.059(2) 0.043(2) -0.0060(18) -0.0116(18) -0.016(2) C66 0.051(2) 0.048(2) 0.037(2) -0.0014(16) -0.0075(17) -0.0014(17) C67 0.066(3) 0.060(3) 0.064(3) 0.021(2) -0.020(2) -0.026(2) C68 0.056(3) 0.094(3) 0.097(4) 0.031(3) 0.002(3) -0.015(3) C69 0.058(4) 0.112(5) 0.180(6) 0.052(4) 0.010(4) -0.018(3) C70 0.084(5) 0.109(5) 0.230(10) 0.063(6) -0.050(6) -0.056(4) C71 0.100(5) 0.073(4) 0.162(6) 0.046(4) -0.074(4) -0.050(3) C72 0.087(4) 0.052(3) 0.088(3) 0.031(2) -0.036(3) -0.037(2) C73 0.123(4) 0.032(2) 0.051(3) 0.0110(18) -0.045(3) -0.032(2) C74 0.196(7) 0.042(3) 0.068(4) 0.010(2) -0.059(4) -0.031(3) C75 0.234(8) 0.043(3) 0.044(3) -0.010(2) -0.026(4) -0.005(4) C76 0.162(5) 0.049(3) 0.069(3) 0.002(2) 0.015(3) 0.004(3) C77 0.103(4) 0.048(2) 0.056(3) -0.003(2) -0.001(3) -0.004(2) C78 0.091(3) 0.034(2) 0.036(2) 0.0020(16) -0.013(2) -0.016(2) C79 0.071(3) 0.057(2) 0.038(2) 0.0023(18) -0.012(2) -0.011(2) C80 0.070(3) 0.079(3) 0.054(3) -0.004(2) -0.001(2) -0.003(2) C81 0.086(3) 0.112(4) 0.060(3) -0.006(3) 0.010(3) -0.019(3) C82 0.119(5) 0.103(4) 0.062(3) 0.002(3) 0.006(3) -0.033(3) C83 0.111(4) 0.080(3) 0.041(3) 0.011(2) -0.014(3) -0.031(3) C84 0.075(3) 0.056(2) 0.048(2) -0.0031(19) -0.018(2) -0.017(2) C85 0.078(3) 0.049(2) 0.049(2) 0.0005(18) -0.037(2) -0.014(2) C86 0.101(4) 0.076(3) 0.078(3) 0.008(2) -0.049(3) -0.016(3) C87 0.080(4) 0.090(4) 0.106(4) -0.011(3) -0.045(3) 0.008(3) C88 0.068(3) 0.105(4) 0.093(4) -0.022(3) -0.015(3) -0.020(3) C89 0.062(3) 0.071(3) 0.078(3) -0.011(2) -0.029(3) -0.006(2) C90 0.051(3) 0.056(2) 0.057(3) -0.0128(19) -0.017(2) -0.011(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C18 N1 C7 108.4(3) . . ? C18 N1 C2 126.8(3) . . ? C7 N1 C2 124.5(3) . . ? C30 N2 C19 109.1(2) . . ? C30 N2 C6 125.1(3) . . ? C19 N2 C6 125.4(3) . . ? C37 N3 C48 108.3(3) . . ? C37 N3 C32 125.6(3) . . ? C48 N3 C32 125.4(3) . . ? C60 N4 C49 108.6(3) . . ? C60 N4 C36 126.8(3) . . ? C49 N4 C36 124.5(3) . . ? C78 N5 C67 109.8(3) . . ? C78 N5 C62 125.4(3) . . ? C67 N5 C62 124.6(3) . . ? C90 N6 C79 108.0(3) . . ? C90 N6 C66 126.5(3) . . ? C79 N6 C66 125.5(3) . . ? C6 C1 C2 120.2(3) . . ? C6 C1 Cl1 119.4(2) . . ? C2 C1 Cl1 120.4(2) . . ? C3 C2 C1 118.8(3) . . ? C3 C2 N1 120.0(3) . . ? C1 C2 N1 121.2(3) . . ? C4 C3 C2 120.9(3) . . ? C4 C3 H3 119.6 . . ? C2 C3 H3 119.6 . . ? C3 C4 C5 120.2(3) . . ? C3 C4 H4 119.9 . . ? C5 C4 H4 119.9 . . ? C6 C5 C4 120.4(3) . . ? C6 C5 H5 119.8 . . ? C4 C5 H5 119.8 . . ? C5 C6 C1 119.6(3) . . ? C5 C6 N2 119.9(3) . . ? C1 C6 N2 120.5(3) . . ? C8 C7 C12 122.0(4) . . ? C8 C7 N1 129.5(3) . . ? C12 C7 N1 108.5(4) . . ? C7 C8 C9 117.6(4) . . ? C7 C8 H8 121.2 . . ? C9 C8 H8 121.2 . . ? C10 C9 C8 120.7(5) . . ? C10 C9 H9 119.7 . . ? C8 C9 H9 119.7 . . ? C11 C10 C9 122.7(5) . . ? C11 C10 H10 118.6 . . ? C9 C10 H10 118.6 . . ? C10 C11 C12 117.5(5) . . ? C10 C11 H11 121.3 . . ? C12 C11 H11 121.3 . . ? C7 C12 C11 119.6(5) . . ? C7 C12 C13 107.2(4) . . ? C11 C12 C13 133.1(4) . . ? C14 C13 C18 118.5(5) . . ? C14 C13 C12 133.3(5) . . ? C18 C13 C12 108.2(4) . . ? C15 C14 C13 119.4(5) . . ? C15 C14 H14 120.3 . . ? C13 C14 H14 120.3 . . ? C14 C15 C16 122.0(6) . . ? C14 C15 H15 119.0 . . ? C16 C15 H15 119.0 . . ? C15 C16 C17 120.9(5) . . ? C15 C16 H16 119.6 . . ? C17 C16 H16 119.6 . . ? C18 C17 C16 116.6(5) . . ? C18 C17 H17 121.7 . . ? C16 C17 H17 121.7 . . ? C17 C18 N1 129.5(4) . . ? C17 C18 C13 122.6(4) . . ? N1 C18 C13 107.7(4) . . ? C20 C19 N2 129.5(3) . . ? C20 C19 C24 122.2(3) . . ? N2 C19 C24 108.3(3) . . ? C21 C20 C19 117.4(3) . . ? C21 C20 H20 121.3 . . ? C19 C20 H20 121.3 . . ? C20 C21 C22 121.3(4) . . ? C20 C21 H21 119.3 . . ? C22 C21 H21 119.3 . . ? C23 C22 C21 121.5(3) . . ? C23 C22 H22 119.2 . . ? C21 C22 H22 119.2 . . ? C22 C23 C24 118.8(3) . . ? C22 C23 H23 120.6 . . ? C24 C23 H23 120.6 . . ? C23 C24 C19 118.8(3) . . ? C23 C24 C25 133.9(3) . . ? C19 C24 C25 107.3(3) . . ? C26 C25 C30 117.7(3) . . ? C26 C25 C24 134.8(3) . . ? C30 C25 C24 107.4(3) . . ? C27 C26 C25 120.1(3) . . ? C27 C26 H26 119.9 . . ? C25 C26 H26 119.9 . . ? C26 C27 C28 120.9(3) . . ? C26 C27 H27 119.6 . . ? C28 C27 H27 119.6 . . ? C29 C28 C27 121.3(3) . . ? C29 C28 H28 119.3 . . ? C27 C28 H28 119.3 . . ? C30 C29 C28 117.3(3) . . ? C30 C29 H29 121.3 . . ? C28 C29 H29 121.3 . . ? C29 C30 N2 129.3(3) . . ? C29 C30 C25 122.6(3) . . ? N2 C30 C25 108.0(3) . . ? C36 C31 C32 120.6(3) . . ? C36 C31 Cl2 119.5(2) . . ? C32 C31 Cl2 119.9(2) . . ? C33 C32 C31 119.3(3) . . ? C33 C32 N3 120.4(3) . . ? C31 C32 N3 120.3(3) . . ? C32 C33 C34 120.2(3) . . ? C32 C33 H33 119.9 . . ? C34 C33 H33 119.9 . . ? C35 C34 C33 120.3(3) . . ? C35 C34 H34 119.8 . . ? C33 C34 H34 119.8 . . ? C36 C35 C34 120.6(3) . . ? C36 C35 H35 119.7 . . ? C34 C35 H35 119.7 . . ? C35 C36 C31 119.0(3) . . ? C35 C36 N4 120.5(3) . . ? C31 C36 N4 120.5(3) . . ? C38 C37 N3 128.8(3) . . ? C38 C37 C42 122.0(3) . . ? N3 C37 C42 109.2(3) . . ? C37 C38 C39 117.6(4) . . ? C37 C38 H38 121.2 . . ? C39 C38 H38 121.2 . . ? C38 C39 C40 121.2(4) . . ? C38 C39 H39 119.4 . . ? C40 C39 H39 119.4 . . ? C41 C40 C39 120.7(4) . . ? C41 C40 H40 119.7 . . ? C39 C40 H40 119.7 . . ? C40 C41 C42 119.6(4) . . ? C40 C41 H41 120.2 . . ? C42 C41 H41 120.2 . . ? C41 C42 C37 118.9(4) . . ? C41 C42 C43 134.3(3) . . ? C37 C42 C43 106.8(3) . . ? C44 C43 C48 118.5(4) . . ? C44 C43 C42 134.1(3) . . ? C48 C43 C42 107.4(3) . . ? C45 C44 C43 118.7(4) . . ? C45 C44 H44 120.7 . . ? C43 C44 H44 120.7 . . ? C44 C45 C46 122.3(4) . . ? C44 C45 H45 118.8 . . ? C46 C45 H45 118.8 . . ? C45 C46 C47 120.3(4) . . ? C45 C46 H46 119.9 . . ? C47 C46 H46 119.9 . . ? C48 C47 C46 117.5(3) . . ? C48 C47 H47 121.3 . . ? C46 C47 H47 121.3 . . ? C47 C48 N3 129.0(3) . . ? C47 C48 C43 122.7(3) . . ? N3 C48 C43 108.3(3) . . ? C50 C49 C54 122.6(4) . . ? C50 C49 N4 128.7(3) . . ? C54 C49 N4 108.7(3) . . ? C51 C50 C49 117.4(4) . . ? C51 C50 H50 121.3 . . ? C49 C50 H50 121.3 . . ? C52 C51 C50 121.7(5) . . ? C52 C51 H51 119.2 . . ? C50 C51 H51 119.2 . . ? C51 C52 C53 121.8(4) . . ? C51 C52 H52 119.1 . . ? C53 C52 H52 119.1 . . ? C52 C53 C54 118.5(4) . . ? C52 C53 H53 120.8 . . ? C54 C53 H53 120.8 . . ? C49 C54 C53 118.1(4) . . ? C49 C54 C55 107.2(3) . . ? C53 C54 C55 134.7(4) . . ? C56 C55 C60 117.2(4) . . ? C56 C55 C54 135.0(4) . . ? C60 C55 C54 107.8(3) . . ? C57 C56 C55 120.3(5) . . ? C57 C56 H56 119.9 . . ? C55 C56 H56 119.9 . . ? C56 C57 C58 122.2(5) . . ? C56 C57 H57 118.9 . . ? C58 C57 H57 118.9 . . ? C57 C58 C59 120.0(5) . . ? C57 C58 H58 120.0 . . ? C59 C58 H58 120.0 . . ? C60 C59 C58 116.5(4) . . ? C60 C59 H59 121.8 . . ? C58 C59 H59 121.8 . . ? C59 C60 N4 128.5(4) . . ? C59 C60 C55 123.9(4) . . ? N4 C60 C55 107.7(3) . . ? C62 C61 C66 119.9(3) . . ? C62 C61 Cl3 119.7(2) . . ? C66 C61 Cl3 120.4(2) . . ? C63 C62 C61 120.0(3) . . ? C63 C62 N5 120.1(3) . . ? C61 C62 N5 119.9(3) . . ? C62 C63 C64 119.9(3) . . ? C62 C63 H63 120.0 . . ? C64 C63 H63 120.0 . . ? C65 C64 C63 120.3(3) . . ? C65 C64 H64 119.9 . . ? C63 C64 H64 119.9 . . ? C64 C65 C66 120.9(3) . . ? C64 C65 H65 119.6 . . ? C66 C65 H65 119.6 . . ? C65 C66 C61 119.0(3) . . ? C65 C66 N6 120.2(3) . . ? C61 C66 N6 120.9(3) . . ? C68 C67 C72 122.6(4) . . ? C68 C67 N5 129.0(4) . . ? C72 C67 N5 108.4(4) . . ? C69 C68 C67 117.5(5) . . ? C69 C68 H68 121.2 . . ? C67 C68 H68 121.2 . . ? C70 C69 C68 121.0(7) . . ? C70 C69 H69 119.5 . . ? C68 C69 H69 119.5 . . ? C69 C70 C71 123.1(7) . . ? C69 C70 H70 118.5 . . ? C71 C70 H70 118.5 . . ? C70 C71 C72 116.7(6) . . ? C70 C71 H71 121.6 . . ? C72 C71 H71 121.6 . . ? C67 C72 C71 119.0(5) . . ? C67 C72 C73 107.3(4) . . ? C71 C72 C73 133.7(5) . . ? C74 C73 C78 117.0(5) . . ? C74 C73 C72 135.0(5) . . ? C78 C73 C72 108.0(3) . . ? C75 C74 C73 119.8(5) . . ? C75 C74 H74 120.1 . . ? C73 C74 H74 120.1 . . ? C74 C75 C76 122.9(5) . . ? C74 C75 H75 118.6 . . ? C76 C75 H75 118.6 . . ? C75 C76 C77 119.5(5) . . ? C75 C76 H76 120.2 . . ? C77 C76 H76 120.2 . . ? C78 C77 C76 116.1(4) . . ? C78 C77 H77 121.9 . . ? C76 C77 H77 121.9 . . ? C77 C78 N5 128.8(3) . . ? C77 C78 C73 124.6(4) . . ? N5 C78 C73 106.5(4) . . ? C80 C79 C84 122.6(4) . . ? C80 C79 N6 128.9(3) . . ? C84 C79 N6 108.5(4) . . ? C79 C80 C81 117.7(4) . . ? C79 C80 H80 121.2 . . ? C81 C80 H80 121.2 . . ? C82 C81 C80 121.1(5) . . ? C82 C81 H81 119.4 . . ? C80 C81 H81 119.4 . . ? C83 C82 C81 121.5(4) . . ? C83 C82 H82 119.2 . . ? C81 C82 H82 119.2 . . ? C82 C83 C84 118.6(4) . . ? C82 C83 H83 120.7 . . ? C84 C83 H83 120.7 . . ? C79 C84 C83 118.6(4) . . ? C79 C84 C85 107.2(3) . . ? C83 C84 C85 134.2(4) . . ? C86 C85 C90 118.1(4) . . ? C86 C85 C84 134.4(4) . . ? C90 C85 C84 107.5(3) . . ? C87 C86 C85 120.1(4) . . ? C87 C86 H86 119.9 . . ? C85 C86 H86 119.9 . . ? C86 C87 C88 121.2(5) . . ? C86 C87 H87 119.4 . . ? C88 C87 H87 119.4 . . ? C87 C88 C89 120.3(5) . . ? C87 C88 H88 119.9 . . ? C89 C88 H88 119.9 . . ? C90 C89 C88 117.3(4) . . ? C90 C89 H89 121.3 . . ? C88 C89 H89 121.3 . . ? C89 C90 N6 128.2(4) . . ? C89 C90 C85 123.0(4) . . ? N6 C90 C85 108.8(4) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl1 C1 1.728(3) . ? Cl2 C31 1.711(3) . ? Cl3 C61 1.713(3) . ? N1 C18 1.390(5) . ? N1 C7 1.406(4) . ? N1 C2 1.413(4) . ? N2 C30 1.392(4) . ? N2 C19 1.395(4) . ? N2 C6 1.424(4) . ? N3 C37 1.388(4) . ? N3 C48 1.396(4) . ? N3 C32 1.417(4) . ? N4 C60 1.386(4) . ? N4 C49 1.391(4) . ? N4 C36 1.418(4) . ? N5 C78 1.390(4) . ? N5 C67 1.396(5) . ? N5 C62 1.420(4) . ? N6 C90 1.381(4) . ? N6 C79 1.410(4) . ? N6 C66 1.414(4) . ? C1 C6 1.386(4) . ? C1 C2 1.395(4) . ? C2 C3 1.379(4) . ? C3 C4 1.368(4) . ? C3 H3 0.9300 . ? C4 C5 1.373(4) . ? C4 H4 0.9300 . ? C5 C6 1.374(4) . ? C5 H5 0.9300 . ? C7 C8 1.377(5) . ? C7 C12 1.393(5) . ? C8 C9 1.383(5) . ? C8 H8 0.9300 . ? C9 C10 1.371(7) . ? C9 H9 0.9300 . ? C10 C11 1.366(7) . ? C10 H10 0.9300 . ? C11 C12 1.402(6) . ? C11 H11 0.9300 . ? C12 C13 1.418(6) . ? C13 C14 1.393(6) . ? C13 C18 1.405(5) . ? C14 C15 1.351(7) . ? C14 H14 0.9300 . ? C15 C16 1.374(7) . ? C15 H15 0.9300 . ? C16 C17 1.407(6) . ? C16 H16 0.9300 . ? C17 C18 1.375(5) . ? C17 H17 0.9300 . ? C19 C20 1.379(4) . ? C19 C24 1.405(4) . ? C20 C21 1.374(4) . ? C20 H20 0.9300 . ? C21 C22 1.382(5) . ? C21 H21 0.9300 . ? C22 C23 1.367(5) . ? C22 H22 0.9300 . ? C23 C24 1.392(4) . ? C23 H23 0.9300 . ? C24 C25 1.433(4) . ? C25 C26 1.398(4) . ? C25 C30 1.410(4) . ? C26 C27 1.358(5) . ? C26 H26 0.9300 . ? C27 C28 1.388(5) . ? C27 H27 0.9300 . ? C28 C29 1.383(4) . ? C28 H28 0.9300 . ? C29 C30 1.377(4) . ? C29 H29 0.9300 . ? C31 C36 1.385(4) . ? C31 C32 1.385(4) . ? C32 C33 1.370(4) . ? C33 C34 1.373(4) . ? C33 H33 0.9300 . ? C34 C35 1.371(5) . ? C34 H34 0.9300 . ? C35 C36 1.369(4) . ? C35 H35 0.9300 . ? C37 C38 1.379(5) . ? C37 C42 1.394(4) . ? C38 C39 1.379(5) . ? C38 H38 0.9300 . ? C39 C40 1.385(5) . ? C39 H39 0.9300 . ? C40 C41 1.365(5) . ? C40 H40 0.9300 . ? C41 C42 1.388(5) . ? C41 H41 0.9300 . ? C42 C43 1.434(5) . ? C43 C44 1.391(5) . ? C43 C48 1.401(4) . ? C44 C45 1.367(5) . ? C44 H44 0.9300 . ? C45 C46 1.380(6) . ? C45 H45 0.9300 . ? C46 C47 1.384(5) . ? C46 H46 0.9300 . ? C47 C48 1.377(5) . ? C47 H47 0.9300 . ? C49 C50 1.375(5) . ? C49 C54 1.391(4) . ? C50 C51 1.371(5) . ? C50 H50 0.9300 . ? C51 C52 1.360(6) . ? C51 H51 0.9300 . ? C52 C53 1.365(6) . ? C52 H52 0.9300 . ? C53 C54 1.413(5) . ? C53 H53 0.9300 . ? C54 C55 1.414(5) . ? C55 C56 1.390(6) . ? C55 C60 1.409(5) . ? C56 C57 1.349(7) . ? C56 H56 0.9300 . ? C57 C58 1.395(7) . ? C57 H57 0.9300 . ? C58 C59 1.401(6) . ? C58 H58 0.9300 . ? C59 C60 1.381(5) . ? C59 H59 0.9300 . ? C61 C62 1.387(4) . ? C61 C66 1.397(4) . ? C62 C63 1.376(4) . ? C63 C64 1.381(4) . ? C63 H63 0.9300 . ? C64 C65 1.367(4) . ? C64 H64 0.9300 . ? C65 C66 1.380(4) . ? C65 H65 0.9300 . ? C67 C68 1.377(6) . ? C67 C72 1.387(5) . ? C68 C69 1.369(6) . ? C68 H68 0.9300 . ? C69 C70 1.367(8) . ? C69 H69 0.9300 . ? C70 C71 1.369(8) . ? C70 H70 0.9300 . ? C71 C72 1.421(6) . ? C71 H71 0.9300 . ? C72 C73 1.430(6) . ? C73 C74 1.379(6) . ? C73 C78 1.419(5) . ? C74 C75 1.347(7) . ? C74 H74 0.9300 . ? C75 C76 1.401(7) . ? C75 H75 0.9300 . ? C76 C77 1.403(6) . ? C76 H76 0.9300 . ? C77 C78 1.366(5) . ? C77 H77 0.9300 . ? C79 C80 1.370(5) . ? C79 C84 1.391(5) . ? C80 C81 1.383(5) . ? C80 H80 0.9300 . ? C81 C82 1.373(6) . ? C81 H81 0.9300 . ? C82 C83 1.370(6) . ? C82 H82 0.9300 . ? C83 C84 1.408(5) . ? C83 H83 0.9300 . ? C84 C85 1.425(5) . ? C85 C86 1.389(5) . ? C85 C90 1.400(5) . ? C86 C87 1.360(6) . ? C86 H86 0.9300 . ? C87 C88 1.395(6) . ? C87 H87 0.9300 . ? C88 C89 1.398(6) . ? C88 H88 0.9300 . ? C89 C90 1.374(5) . ? C89 H89 0.9300 . ?