#------------------------------------------------------------------------------ #$Date: 2021-11-06 01:12:47 +0200 (Sat, 06 Nov 2021) $ #$Revision: 270329 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/51/1565131.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1565131 loop_ _publ_author_name 'He, Weiying' 'Beattie, D. Dawson' 'Zhou, Hao' 'Bowes, Eric G.' 'Schafer, Laurel L.' 'Love, Jennifer' 'Kennepohl, Pierre' _publ_section_title ; Direct metal-carbon bonding in symmetric bis(C-H) agostic Nickel(I) complexes ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC03578A _journal_year 2021 _chemical_formula_moiety 'C30 H24 Cl4 Cu N3' _chemical_formula_sum 'C30 H24 Cl4 Cu N3' _chemical_formula_weight 631.86 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _audit_block_doi 10.5517/ccdc.csd.cc239b1t _audit_creation_method SHELXL-2017/1 _audit_update_record ; 2019-08-03 deposited with the CCDC. 2021-10-29 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 108.036(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.8807(5) _cell_length_b 15.5610(5) _cell_length_c 14.8263(6) _cell_measurement_reflns_used 9977 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 25.49 _cell_measurement_theta_min 2.25 _cell_volume 2825.71(19) _computing_cell_refinement 'SAINT V8.37A (Bruker, 2005)' _computing_data_collection 'APEX3 V2016.5-0 (Bruker, 2016)' _computing_data_reduction ; SAINT V8.37A, XPREP v2014/2, SADABS V2016/2 (Bruker, 2016) ; _computing_molecular_graphics 'SHELXLE v932 (Hubschle, 2011)' _computing_publication_material 'XCIF V2014-2 (Bruker, 2014)' _computing_structure_refinement 'SHELX-2018-1 (Sheldrick, 2015)' _computing_structure_solution 'SHELX-2014-5 (Sheldrick, 2015)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.991 _diffrn_measurement_device 'Bruker APEX DUO/ApexII CCD' _diffrn_measurement_method 'profile data from \f and \w scans' _diffrn_radiation_monochromator 'multilayer mirrors' _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0285 _diffrn_reflns_av_unetI/netI 0.0210 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.991 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 26800 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.991 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.487 _diffrn_reflns_theta_min 1.834 _exptl_absorpt_coefficient_mu 1.176 _exptl_absorpt_correction_T_max 0.7452 _exptl_absorpt_correction_T_min 0.5892 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS V2016/2 (Bruker, 2016)' _exptl_crystal_density_diffrn 1.485 _exptl_crystal_density_method 'not measured' _exptl_crystal_description prism _exptl_crystal_F_000 1288 _exptl_crystal_size_max 0.310 _exptl_crystal_size_mid 0.276 _exptl_crystal_size_min 0.118 _refine_diff_density_max 0.289 _refine_diff_density_min -0.285 _refine_diff_density_rms 0.047 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.038 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 348 _refine_ls_number_reflns 5209 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.038 _refine_ls_R_factor_all 0.0260 _refine_ls_R_factor_gt 0.0222 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0248P)^2^+1.6714P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0552 _refine_ls_wR_factor_ref 0.0570 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4723 _reflns_number_total 5209 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1sc03578a2.cif _cod_data_source_block P21n_a _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 1565131 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.712 _shelx_estimated_absorpt_t_max 0.874 _shelx_res_file ; TITL P21n_a.res in P2(1)/n P21n_a.res created by SHELXL-2017/1 at 12:58:06 on 08-May-2019 CELL 0.71073 12.8807 15.5610 14.8263 90.000 108.036 90.000 ZERR 4.0000 0.0005 0.0005 0.0006 0.000 0.002 0.000 LATT 1 SYMM 0.5-X, 0.5+Y, 0.5-Z SFAC C H CL CU N UNIT 120 96 16 4 12 BOND $H FMAP 2 1 53 PLAN 20 LIST 4 TEMP -173 SIZE 0.310 0.276 0.118 HTAB EQIV $1 x+1/2, -y+3/2, z+1/2 HTAB N3 Cl2_$1 ACTA L.S. 20 WGHT 0.024800 1.671400 FVAR 0.37289 CU1 4 0.285823 0.741205 0.533189 11.00000 0.01389 0.01338 = 0.01222 0.00134 0.00671 0.00390 CL1 3 0.463182 0.884256 0.498320 11.00000 0.01847 0.02411 = 0.03298 -0.00603 0.00345 -0.00534 CL2 3 0.068713 0.809600 0.247750 11.00000 0.02023 0.02953 = 0.01727 -0.00023 0.00157 -0.00001 CL3 3 0.366364 0.803491 0.790831 11.00000 0.02076 0.02434 = 0.02496 -0.00563 0.00703 -0.00465 CL4 3 0.051650 0.597706 0.571858 11.00000 0.02008 0.02414 = 0.02141 -0.00497 0.00828 -0.00485 N1 5 0.227538 0.838937 0.445553 11.00000 0.01430 0.01294 = 0.01184 0.00051 0.00546 0.00062 N2 5 0.194735 0.754302 0.611918 11.00000 0.01485 0.01294 = 0.01252 0.00215 0.00628 0.00243 N3 5 0.402454 0.681411 0.508950 11.00000 0.01377 0.01649 = 0.01331 0.00266 0.00474 0.00336 H3 2 0.467260 0.690503 0.544873 11.00000 -1.50000 C1 1 0.152528 0.891258 0.458487 11.00000 0.01389 0.01132 = 0.01345 -0.00009 0.00321 -0.00014 C2 1 0.103480 0.879975 0.530464 11.00000 0.01481 0.01174 = 0.01567 -0.00006 0.00594 0.00366 AFIX 43 H2 2 0.049423 0.921350 0.530949 11.00000 -1.20000 AFIX 0 C3 1 0.122077 0.817331 0.601229 11.00000 0.01317 0.01247 = 0.01215 -0.00286 0.00465 -0.00063 C4 1 0.116603 0.970659 0.397693 11.00000 0.02453 0.01571 = 0.02170 0.00456 0.01261 0.00568 AFIX 137 H4A 2 0.158224 0.975179 0.352636 11.00000 -1.50000 H4B 2 0.129783 1.021760 0.438305 11.00000 -1.50000 H4C 2 0.038563 0.966403 0.362810 11.00000 -1.50000 AFIX 0 C5 1 0.056419 0.823537 0.669465 11.00000 0.02028 0.01802 = 0.01764 0.00289 0.01088 0.00594 AFIX 137 H5A 2 0.014062 0.770685 0.666295 11.00000 -1.50000 H5B 2 0.006659 0.872725 0.652321 11.00000 -1.50000 H5C 2 0.105904 0.831232 0.734087 11.00000 -1.50000 AFIX 0 C6 1 0.268671 0.847993 0.368971 11.00000 0.01712 0.00945 = 0.01557 0.00323 0.00830 0.00306 C7 1 0.380124 0.863091 0.383854 11.00000 0.01898 0.01256 = 0.02234 0.00322 0.00908 0.00064 C8 1 0.426577 0.863674 0.311470 11.00000 0.02343 0.01963 = 0.03979 0.00856 0.02099 0.00372 AFIX 43 H8 2 0.502850 0.872600 0.325067 11.00000 -1.20000 AFIX 0 C9 1 0.361396 0.851211 0.219475 11.00000 0.04290 0.02837 = 0.03078 0.01041 0.02961 0.00954 AFIX 43 H9 2 0.392298 0.852694 0.169038 11.00000 -1.20000 AFIX 0 C10 1 0.251350 0.836594 0.200692 11.00000 0.03757 0.02769 = 0.01649 0.00462 0.01288 0.00729 AFIX 43 H10 2 0.206166 0.828318 0.137186 11.00000 -1.20000 AFIX 0 C11 1 0.206398 0.833935 0.274304 11.00000 0.01878 0.01780 = 0.01647 0.00319 0.00741 0.00289 C12 1 0.211052 0.695787 0.687459 11.00000 0.01533 0.01326 = 0.01501 0.00116 0.01044 0.00534 C13 1 0.292396 0.708498 0.774119 11.00000 0.01700 0.01723 = 0.01743 -0.00082 0.00753 0.00279 C14 1 0.317101 0.647868 0.846038 11.00000 0.02255 0.02858 = 0.01730 0.00431 0.00468 0.00938 AFIX 43 H14 2 0.373718 0.658321 0.903668 11.00000 -1.20000 AFIX 0 C15 1 0.258349 0.571770 0.833050 11.00000 0.03383 0.02179 = 0.02408 0.01121 0.01499 0.01149 AFIX 43 H15 2 0.274852 0.529677 0.881851 11.00000 -1.20000 AFIX 0 C16 1 0.175877 0.557078 0.749276 11.00000 0.02800 0.01434 = 0.02730 0.00306 0.01731 0.00264 AFIX 43 H16 2 0.134883 0.505295 0.740491 11.00000 -1.20000 AFIX 0 C17 1 0.153420 0.618342 0.678253 11.00000 0.01641 0.01625 = 0.01644 -0.00082 0.00896 0.00310 C18 1 0.405227 0.638541 0.435040 11.00000 0.01754 0.01158 = 0.01377 0.00357 0.00760 0.00285 C19 1 0.300411 0.613812 0.364678 11.00000 0.01662 0.01039 = 0.01646 -0.00032 0.00557 0.00436 C20 1 0.288570 0.611738 0.267949 11.00000 0.01988 0.02114 = 0.01913 -0.00157 0.00911 0.00343 AFIX 43 H20 2 0.349474 0.623375 0.246579 11.00000 -1.20000 AFIX 0 C21 1 0.188200 0.592749 0.203133 11.00000 0.02527 0.02828 = 0.01691 -0.00419 0.00421 0.00261 AFIX 43 H21 2 0.180231 0.592146 0.137256 11.00000 -1.20000 AFIX 0 C22 1 0.099395 0.574639 0.233572 11.00000 0.01969 0.02218 = 0.02620 -0.00396 0.00141 -0.00060 AFIX 43 H22 2 0.030612 0.561778 0.188711 11.00000 -1.20000 AFIX 0 C23 1 0.110886 0.575281 0.329525 11.00000 0.01654 0.02034 = 0.02874 0.00182 0.00844 -0.00109 AFIX 43 H23 2 0.050126 0.562120 0.350538 11.00000 -1.20000 AFIX 0 C24 1 0.210368 0.594989 0.394739 11.00000 0.02017 0.01491 = 0.01877 0.00104 0.00826 0.00276 AFIX 43 H24 2 0.217646 0.595756 0.460484 11.00000 -1.20000 AFIX 0 C25 1 0.510138 0.613894 0.420538 11.00000 0.01631 0.01798 = 0.01019 0.00393 0.00600 0.00485 C26 1 0.598255 0.670629 0.445896 11.00000 0.01898 0.01976 = 0.01202 0.00002 0.00705 0.00378 AFIX 43 H26 2 0.589321 0.726377 0.468547 11.00000 -1.20000 AFIX 0 C27 1 0.698724 0.646368 0.438328 11.00000 0.01770 0.02862 = 0.01691 0.00122 0.00805 0.00044 AFIX 43 H27 2 0.758412 0.685330 0.455904 11.00000 -1.20000 AFIX 0 C28 1 0.712046 0.564983 0.405001 11.00000 0.01954 0.02876 = 0.01967 0.00653 0.01116 0.00981 AFIX 43 H28 2 0.781327 0.547771 0.401191 11.00000 -1.20000 AFIX 0 C29 1 0.624498 0.509033 0.377379 11.00000 0.02730 0.01724 = 0.02094 0.00469 0.01419 0.00899 AFIX 43 H29 2 0.633418 0.453887 0.353295 11.00000 -1.20000 AFIX 0 C30 1 0.523733 0.533040 0.384667 11.00000 0.02138 0.01669 = 0.01708 0.00293 0.00934 0.00347 AFIX 43 H30 2 0.463775 0.494438 0.365230 11.00000 -1.20000 REM ##### AFIX 0 HKLF 4 REM P21n_a.res in P2(1)/n REM R1 = 0.0222 for 4723 Fo > 4sig(Fo) and 0.0260 for all 5209 data REM 348 parameters refined using 0 restraints END WGHT 0.0248 1.6714 REM Instructions for potential hydrogen bonds HTAB N3 Cl2_$1 REM Highest difference peak 0.289, deepest hole -0.285, 1-sigma level 0.047 Q1 1 0.2563 0.6975 0.7258 11.00000 0.05 0.29 Q2 1 0.3511 0.6319 0.3995 11.00000 0.05 0.27 Q3 1 0.2990 0.6046 0.3199 11.00000 0.05 0.25 Q4 1 0.2057 0.7240 0.6529 11.00000 0.05 0.25 Q5 1 0.1976 0.6492 0.6763 11.00000 0.05 0.25 Q6 1 0.3248 0.8516 0.3741 11.00000 0.05 0.24 Q7 1 0.1335 0.8827 0.5023 11.00000 0.05 0.24 Q8 1 0.0926 0.8218 0.6396 11.00000 0.05 0.24 Q9 1 0.2574 0.6129 0.3783 11.00000 0.05 0.23 Q10 1 0.1376 0.8613 0.5782 11.00000 0.05 0.23 Q11 1 0.3022 0.6006 0.8270 11.00000 0.05 0.23 Q12 1 0.0737 0.7837 0.7237 11.00000 0.05 0.23 Q13 1 0.2405 0.8432 0.3211 11.00000 0.05 0.23 Q14 1 0.1761 0.8565 0.4456 11.00000 0.05 0.23 Q15 1 0.5590 0.6373 0.4355 11.00000 0.05 0.22 Q16 1 0.4523 0.6317 0.4198 11.00000 0.05 0.22 Q17 1 0.1606 0.6028 0.3579 11.00000 0.05 0.22 Q18 1 0.5191 0.5793 0.4001 11.00000 0.05 0.22 Q19 1 0.1136 0.8491 0.5611 11.00000 0.05 0.22 Q20 1 0.2332 0.8340 0.2411 11.00000 0.05 0.21 ; _shelx_res_checksum 86537 _shelx_hkl_file ; 1 0 0 2.40 0.50 1 0 0 2.40 0.50 2 0 0 3035.40 74.49 2 0 0 2986.50 73.59 2 0 0 2952.50 74.39 -2 0 0 2862.61 73.59 3 0 0 -0.70 1.00 3 0 0 0.50 1.10 3 0 0 0.80 0.40 -3 0 0 1.20 0.40 4 0 0 30.20 2.70 4 0 0 31.20 2.60 -4 0 0 29.60 1.20 4 0 0 28.80 1.30 -5 0 0 0.10 0.40 5 0 0 -0.50 1.30 5 0 0 -0.50 0.50 5 0 0 0.60 1.70 6 0 0 950.80 26.50 6 0 0 926.21 26.50 7 0 0 1.90 2.10 7 0 0 -0.60 1.60 8 0 0 225.38 9.70 8 0 0 245.68 9.90 9 0 0 -2.20 2.00 9 0 0 0.70 2.60 10 0 0 186.88 9.60 10 0 0 201.48 9.80 11 0 0 -1.10 2.60 11 0 0 4.10 3.50 12 0 0 1831.62 52.79 13 0 0 5.70 3.80 14 0 0 244.88 13.50 0 -1 0 3.60 0.50 0 -1 0 2.70 0.40 0 1 0 0.50 0.20 1 -1 0 3.80 0.70 1 -1 0 4.50 0.50 -1 -1 0 5.10 0.50 1 1 0 4.70 0.60 1 1 0 3.60 0.80 1 1 0 3.40 0.70 -1 1 0 5.10 0.50 1 1 0 3.80 0.50 2 -1 0 14.40 1.50 2 -1 0 12.80 1.20 2 1 0 14.30 1.10 2 1 0 9.90 1.20 3 -1 0 247.18 7.60 3 -1 0 251.07 7.90 3 1 0 245.98 6.80 3 1 0 245.68 7.80 3 1 0 259.17 7.90 -3 1 0 240.98 6.70 4 -1 0 1247.78 32.50 4 -1 0 1211.88 32.20 4 1 0 1209.08 32.40 4 1 0 1293.57 32.60 -4 1 0 1225.88 30.90 4 1 0 1138.29 30.90 5 -1 0 27.30 2.60 5 -1 0 30.60 3.10 5 1 0 26.20 2.90 -5 1 0 36.00 1.50 5 1 0 29.00 2.90 5 1 0 30.20 1.60 6 -1 0 1.50 2.00 6 -1 0 3.50 1.60 6 1 0 5.50 1.90 6 1 0 5.70 1.90 6 1 0 4.90 0.90 7 -1 0 40.40 3.80 7 -1 0 43.20 4.00 7 1 0 42.40 4.10 7 1 0 48.00 4.30 7 1 0 39.80 1.80 8 -1 0 164.18 7.70 8 -1 0 154.88 7.70 8 1 0 152.98 7.80 8 1 0 157.08 7.80 9 -1 0 463.65 16.30 9 -1 0 480.05 16.70 9 1 0 475.85 16.60 10 -1 0 1093.19 32.50 10 -1 0 1084.49 32.20 10 1 0 1047.30 32.30 11 -1 0 145.79 9.10 11 -1 0 161.18 9.10 11 1 0 150.48 9.20 12 -1 0 0.80 3.60 12 -1 0 2.30 3.30 12 1 0 15.50 4.30 13 -1 0 62.09 7.10 13 -1 0 51.49 6.60 -13 -1 0 71.39 6.80 13 1 0 67.19 7.60 -14 -1 0 11.50 4.10 14 -1 0 9.40 4.50 14 1 0 10.40 4.40 0 -2 0 4557.24 110.29 0 -2 0 4453.45 109.99 0 -2 0 4299.77 109.69 0 2 0 4303.37 110.49 0 2 0 4449.55 109.69 -1 -2 0 225.38 6.10 1 -2 0 215.18 5.80 1 -2 0 209.98 6.40 1 -2 0 233.38 6.50 1 2 0 222.28 6.80 -1 2 0 217.88 5.80 1 2 0 217.28 6.30 -2 -2 0 2702.73 66.29 2 -2 0 2554.24 66.19 2 -2 0 2607.64 66.79 2 2 0 2670.73 66.69 2 2 0 2645.64 66.39 2 2 0 2653.73 67.29 -3 -2 0 1389.06 35.20 3 -2 0 1332.27 35.20 3 -2 0 1373.76 35.80 3 2 0 1392.76 36.50 3 2 0 1326.07 35.70 3 2 0 1394.96 35.00 -4 -2 0 142.19 5.20 4 -2 0 150.78 5.90 4 -2 0 140.79 5.30 4 2 0 146.99 5.80 4 2 0 142.09 4.70 5 -2 0 129.29 5.50 5 -2 0 148.09 6.20 5 2 0 130.29 4.50 5 2 0 139.29 6.00 6 -2 0 405.06 12.80 6 -2 0 415.66 13.30 6 2 0 406.86 13.30 6 2 0 380.86 11.10 7 -2 0 104.69 5.60 7 -2 0 113.89 6.30 7 2 0 107.09 6.10 7 2 0 109.29 4.00 8 -2 0 113.79 6.20 8 -2 0 117.29 6.80 8 2 0 115.89 6.70 8 2 0 107.89 4.00 9 -2 0 671.73 21.70 9 -2 0 647.24 21.00 9 2 0 678.33 21.70 10 -2 0 211.78 10.60 10 -2 0 215.08 10.00 10 2 0 209.18 10.40 -11 -2 0 3.60 2.80 11 -2 0 -0.20 2.90 11 -2 0 -2.70 2.50 11 2 0 3.10 3.00 12 -2 0 234.48 11.70 12 -2 0 217.38 12.00 -12 -2 0 245.78 11.10 12 2 0 233.38 12.20 13 -2 0 10.30 4.70 -13 -2 0 9.40 3.70 13 -2 0 13.30 4.40 13 2 0 2.60 3.50 14 -2 0 587.64 22.90 -14 -2 0 600.34 21.50 14 -2 0 602.64 23.00 14 2 0 608.04 23.60 0 -3 0 0.10 0.50 0 -3 0 -0.70 0.90 0 -3 0 0.50 0.90 0 3 0 0.30 0.50 0 3 0 1.20 1.10 -1 -3 0 81.69 2.90 1 -3 0 83.09 3.30 1 -3 0 73.89 3.30 1 3 0 77.79 3.00 1 3 0 78.79 3.80 -1 3 0 71.69 3.70 -2 -3 0 2598.74 66.39 2 -3 0 2605.44 67.09 2 -3 0 2508.05 66.09 2 -3 0 2793.12 67.19 2 3 0 2636.14 66.89 2 3 0 2678.63 66.89 2 3 0 2664.13 67.69 3 -3 0 124.39 5.00 3 -3 0 118.89 4.20 -3 -3 0 129.19 4.40 3 3 0 113.89 4.90 3 3 0 129.89 5.60 3 3 0 124.09 4.60 4 -3 0 1031.90 28.50 4 -3 0 1022.40 27.50 -4 -3 0 1043.90 27.50 4 3 0 1049.40 28.40 4 3 0 1077.69 27.60 4 3 0 1032.30 29.30 5 -3 0 35.20 2.80 5 -3 0 30.60 3.30 -5 -3 0 42.90 2.80 5 3 0 32.20 2.40 5 3 0 31.60 3.20 6 -3 0 212.38 8.00 -6 -3 0 223.48 7.80 6 -3 0 229.18 8.80 6 3 0 222.18 8.80 6 3 0 213.18 7.10 7 -3 0 1664.03 44.80 7 -3 0 1736.83 45.80 -7 -3 0 1674.83 44.30 7 3 0 1700.83 45.60 7 3 0 1574.94 43.00 -8 -3 0 324.27 11.10 8 -3 0 332.87 12.40 8 -3 0 322.27 11.60 -8 3 0 298.77 8.60 8 3 0 315.67 9.60 8 3 0 323.57 12.30 9 -3 0 22.80 4.20 9 -3 0 12.00 2.90 -9 -3 0 19.50 3.10 9 3 0 15.60 3.50 -10 -3 0 362.46 13.00 10 -3 0 373.56 14.00 10 -3 0 368.16 14.50 10 3 0 331.97 14.20 -11 -3 0 490.85 16.80 11 -3 0 489.85 17.80 11 -3 0 480.35 18.40 11 3 0 473.55 18.30 -12 -3 0 64.39 6.00 12 -3 0 55.99 6.50 12 -3 0 71.09 6.90 12 3 0 79.59 7.90 13 -3 0 54.99 6.70 -13 -3 0 59.59 6.20 13 -3 0 57.19 7.20 13 3 0 53.69 6.90 14 -3 0 2.10 4.50 -14 -3 0 6.70 3.70 14 -3 0 1.10 3.60 14 3 0 5.80 4.20 0 -4 0 5933.41 150.98 0 -4 0 6018.00 150.58 0 4 0 5971.70 149.88 0 4 0 6175.38 151.68 1 -4 0 3921.61 98.79 -1 -4 0 3948.90 98.89 -1 -4 0 3974.50 98.29 1 -4 0 3917.11 98.59 1 4 0 3906.41 98.19 1 4 0 3853.51 99.39 -1 4 0 3891.11 99.49 2 -4 0 1275.67 34.10 2 -4 0 1352.56 34.10 2 -4 0 1222.08 32.60 -2 -4 0 1305.07 33.30 2 4 0 1295.07 34.70 2 4 0 1292.07 33.70 2 4 0 1313.17 34.00 -2 4 0 1299.47 34.80 -3 -4 0 1066.09 27.80 3 -4 0 1089.29 28.90 3 -4 0 1035.20 27.50 3 4 0 1051.59 29.50 3 4 0 1087.59 28.60 3 4 0 1077.79 28.50 4 -4 0 45.90 3.70 -4 -4 0 38.90 2.50 4 -4 0 37.70 2.40 4 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524.55 15.80 -3 6 0 552.04 17.00 3 6 0 530.75 16.90 -4 -6 0 1513.25 39.80 4 -6 0 1483.65 39.10 4 -6 0 1556.94 41.30 4 6 0 1563.44 41.00 -4 6 0 1509.35 42.30 4 6 0 1520.25 40.80 4 6 0 1533.55 42.40 -5 -6 0 180.88 6.60 5 -6 0 185.18 6.30 5 -6 0 185.68 8.10 5 6 0 200.58 8.00 -5 6 0 159.68 8.40 5 6 0 195.48 7.70 5 6 0 182.98 8.90 6 -6 0 138.69 7.00 -6 -6 0 132.89 5.70 6 -6 0 137.59 5.60 6 6 0 140.39 8.20 6 6 0 149.79 7.20 6 6 0 134.09 6.30 7 -6 0 0.40 1.40 -7 -6 0 0.30 1.50 7 -6 0 -0.70 2.30 -7 6 0 0.60 1.20 7 6 0 1.20 1.60 7 6 0 -0.90 2.00 -8 -6 0 466.55 14.80 8 -6 0 461.05 15.00 8 -6 0 477.35 16.90 8 6 0 473.65 16.70 8 6 0 477.45 15.00 -8 6 0 463.55 13.90 -9 -6 0 5.60 2.20 9 -6 0 3.10 2.10 9 -6 0 -0.20 2.70 9 6 0 0.10 1.70 9 6 0 2.30 2.90 -9 6 0 3.40 3.50 10 -6 0 93.39 6.30 10 -6 0 94.69 8.10 -10 -6 0 89.79 5.80 10 6 0 80.89 7.50 -11 -6 0 117.49 7.00 11 -6 0 120.59 7.70 11 -6 0 122.79 9.20 11 6 0 126.99 9.00 12 -6 0 322.67 13.80 12 -6 0 328.97 15.30 12 6 0 317.07 15.10 13 -6 0 106.59 8.80 13 -6 0 104.19 9.80 13 6 0 101.59 9.70 -14 6 0 22.00 7.20 0 -7 0 1.40 1.60 0 -7 0 1.70 1.50 0 7 0 0.80 0.90 0 7 0 -0.10 1.80 -1 -7 0 171.38 6.20 1 -7 0 163.08 6.80 1 -7 0 165.78 6.50 -1 -7 0 161.18 6.90 -1 7 0 172.18 7.80 1 7 0 158.28 6.80 1 7 0 164.18 5.60 1 7 0 174.98 7.90 2 -7 0 179.68 7.20 -2 -7 0 176.68 7.30 2 -7 0 179.78 7.30 -2 -7 0 187.88 6.60 -2 7 0 180.78 8.30 2 7 0 174.18 7.40 2 7 0 183.08 6.60 2 7 0 182.18 8.30 3 -7 0 269.47 9.90 -3 -7 0 286.97 9.00 3 -7 0 284.37 10.20 3 7 0 272.97 10.10 -3 7 0 287.37 11.10 3 7 0 286.77 11.10 3 7 0 283.47 9.50 4 -7 0 12.40 2.50 4 -7 0 14.50 1.40 -4 -7 0 11.80 1.80 4 7 0 12.30 2.40 4 7 0 12.60 2.40 -4 7 0 18.00 3.50 4 7 0 16.20 3.30 -5 -7 0 104.99 4.80 5 -7 0 103.89 6.00 5 -7 0 105.89 4.30 -5 7 0 112.89 7.10 5 7 0 111.49 6.00 5 7 0 114.79 6.00 5 7 0 109.59 6.90 6 -7 0 1786.22 49.20 -6 -7 0 1851.31 49.70 6 -7 0 1922.71 51.89 6 7 0 1940.51 53.29 6 7 0 1973.80 51.19 6 7 0 1929.21 51.49 7 -7 0 161.88 8.40 7 -7 0 149.19 6.30 -7 -7 0 153.28 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120.89 8.80 -10 8 0 127.59 10.00 11 -8 0 118.49 9.30 11 8 0 128.39 9.50 -11 8 0 118.39 10.10 12 -8 0 267.47 13.90 -12 8 0 253.37 15.30 12 8 0 244.98 13.60 13 -8 0 195.48 12.60 13 8 0 203.18 12.80 -13 8 0 182.08 13.30 0 -9 0 1.30 2.00 0 -9 0 -0.80 1.60 0 9 0 2.40 2.40 0 9 0 0.90 1.00 0 9 0 1.50 2.00 -1 -9 0 407.96 12.70 1 -9 0 384.46 13.50 -1 -9 0 416.76 13.80 1 -9 0 402.06 13.10 -1 9 0 399.36 14.60 1 9 0 411.26 14.90 1 9 0 392.46 11.70 1 9 0 384.16 13.70 2 -9 0 782.52 22.90 -2 -9 0 784.02 22.10 2 -9 0 790.62 23.40 -2 -9 0 811.32 23.50 -2 9 0 790.72 24.60 2 9 0 744.73 23.40 2 9 0 766.92 21.70 2 9 0 785.82 24.70 3 -9 0 444.86 15.10 -3 -9 0 461.35 13.90 3 -9 0 450.85 14.80 -3 -9 0 437.66 15.10 3 9 0 444.06 16.50 3 9 0 449.76 15.30 3 9 0 451.45 14.20 -3 9 0 452.65 16.40 -4 -9 0 29.30 3.00 4 -9 0 28.20 3.80 4 9 0 28.20 3.40 4 9 0 23.00 3.40 -4 9 0 30.40 4.60 4 9 0 34.30 4.90 -5 -9 0 123.29 5.60 5 -9 0 109.69 4.10 5 -9 0 121.79 6.90 5 9 0 115.19 8.00 5 9 0 127.19 6.80 5 9 0 127.29 7.00 6 -9 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31.40 5.60 -6 -10 -9 -5.70 3.30 6 -10 9 5.10 4.00 6 10 9 3.00 4.10 -6 10 -9 -4.10 3.50 7 -10 9 295.27 14.50 -7 -10 -9 278.97 14.20 -7 10 -9 298.17 16.40 7 10 9 297.77 15.20 11 -11 -9 136.89 10.10 11 -11 -9 142.39 10.40 11 11 -9 138.19 10.80 11 11 -9 144.39 12.20 -11 11 9 145.99 11.60 11 11 -9 174.08 11.30 10 -11 -9 46.80 6.50 10 -11 -9 68.69 7.20 10 11 -9 65.79 8.10 10 11 -9 55.79 7.30 10 11 -9 63.99 9.10 -10 11 9 54.69 7.30 -9 -11 9 371.86 16.40 9 -11 -9 362.76 15.00 9 -11 -9 368.66 16.10 9 11 -9 360.46 16.10 9 11 -9 356.66 16.60 -9 11 9 360.06 16.50 9 11 -9 353.76 18.30 -8 -11 9 105.39 8.30 8 -11 -9 104.79 7.50 8 -11 -9 94.79 8.70 8 11 -9 106.39 8.90 8 11 -9 85.49 7.90 -8 11 9 102.09 8.70 8 11 -9 107.09 10.00 7 -11 -9 77.89 6.60 -7 -11 9 73.49 7.30 7 -11 -9 85.69 8.00 -7 11 9 71.59 7.40 7 11 -9 78.59 8.20 7 11 -9 88.29 9.70 6 -11 -9 27.90 5.20 6 -11 -9 27.40 3.90 -6 -11 9 24.50 4.80 6 11 -9 23.20 5.60 6 11 -9 29.20 5.60 -6 11 9 21.80 4.40 -5 -11 9 2.50 3.40 5 -11 -9 5.40 3.30 5 11 -9 0.70 3.60 -5 11 9 2.20 3.40 5 11 -9 2.40 3.30 4 -11 -9 136.49 8.50 -4 -11 9 131.49 8.60 4 11 -9 145.49 9.60 4 11 -9 118.79 9.70 -3 -11 9 281.07 12.80 3 -11 -9 301.27 13.30 3 11 -9 305.37 14.90 3 11 -9 286.77 13.60 2 -11 -9 4.80 3.40 -2 -11 9 -0.10 2.80 2 11 -9 1.30 3.50 2 11 -9 9.60 3.80 -1 -11 9 10.80 3.80 1 -11 -9 17.00 4.20 -1 11 9 15.30 3.30 1 11 -9 12.80 4.50 1 11 -9 14.50 4.50 0 -11 9 79.89 7.20 0 -11 -9 80.69 7.30 0 11 9 74.19 6.10 0 11 -9 79.09 8.40 0 11 -9 88.29 7.90 -1 -11 -9 1.90 3.10 1 -11 9 -0.70 3.10 -1 11 -9 -0.10 2.90 1 11 9 -0.20 2.70 -1 11 -9 1.10 3.40 2 -11 9 109.79 8.20 -2 -11 -9 79.99 7.50 2 11 9 94.39 7.40 -2 11 -9 108.79 9.20 -2 11 -9 95.29 8.30 3 -11 9 237.88 12.60 -3 -11 -9 265.07 12.90 3 -11 9 244.88 12.50 -3 11 -9 283.77 12.70 3 11 9 243.68 11.90 -3 11 -9 242.48 14.00 -4 -11 -9 29.90 5.20 4 -11 9 20.70 5.00 -4 11 -9 31.50 6.40 -4 11 -9 36.00 5.40 4 11 9 26.40 5.20 5 -11 9 282.97 14.10 -5 -11 -9 285.47 14.00 -5 11 -9 302.27 16.00 5 11 9 286.67 14.00 -6 -11 -9 54.19 7.20 6 -11 9 45.70 6.70 6 11 9 48.10 6.90 -6 11 -9 52.19 8.00 -7 11 -9 49.50 8.20 -11 12 9 88.09 9.60 11 12 -9 78.99 9.70 11 12 -9 101.99 9.70 11 12 -9 95.29 9.90 10 -12 -9 -0.80 3.70 -10 -12 9 7.80 4.80 10 -12 -9 -0.60 3.50 -10 12 9 1.90 4.40 10 12 -9 -2.80 4.00 10 12 -9 -1.30 3.70 10 12 -9 4.50 4.50 9 -12 -9 -1.90 3.00 9 -12 -9 2.70 3.80 -9 -12 9 5.30 4.50 9 12 -9 4.90 4.00 9 12 -9 13.70 5.50 -9 12 9 4.10 4.10 9 12 -9 7.40 4.20 8 -12 -9 29.10 5.70 -8 -12 9 20.50 5.30 8 -12 -9 16.90 4.10 -8 12 9 15.10 4.90 8 12 -9 30.50 6.00 8 12 -9 13.00 4.40 8 12 -9 11.50 5.20 7 -12 -9 5.80 3.60 7 -12 -9 4.50 3.70 -7 -12 9 4.00 4.00 -7 12 9 1.70 3.70 7 12 -9 6.80 4.00 7 12 -9 6.90 4.60 -6 -12 9 33.10 5.40 6 -12 -9 42.50 5.70 6 12 -9 23.30 5.60 6 12 -9 42.20 6.20 -6 12 9 32.50 6.00 5 -12 -9 135.39 9.40 -5 -12 9 144.19 9.50 5 12 -9 167.18 11.60 5 12 -9 166.48 10.50 4 -12 -9 222.98 11.40 -4 -12 9 247.28 12.00 4 12 -9 222.78 13.50 4 12 -9 217.88 11.90 3 -12 -9 198.18 10.90 -3 -12 9 191.48 10.70 3 12 -9 194.18 11.10 3 12 -9 195.68 12.40 -2 -12 9 645.34 22.30 2 -12 -9 607.44 22.20 2 12 -9 638.04 24.60 2 12 -9 645.24 23.10 1 -12 -9 361.16 15.40 -1 -12 9 382.96 15.50 1 12 -9 420.96 16.80 1 12 -9 356.36 17.30 0 -12 -9 90.79 7.90 0 -12 9 63.89 6.70 0 12 -9 80.79 8.00 0 12 -9 79.59 8.70 1 -12 9 197.08 11.20 -1 -12 -9 232.58 11.80 -1 12 -9 217.28 11.70 1 12 9 200.98 13.80 -1 12 -9 215.78 13.20 -2 -12 -9 101.79 8.30 2 -12 9 107.29 8.60 -2 12 -9 110.79 8.90 2 12 9 95.19 7.50 -2 12 -9 98.99 9.30 -3 -12 -9 150.48 9.90 3 -12 9 136.29 9.80 -3 12 -9 154.68 11.50 -3 12 -9 130.79 9.50 3 12 9 139.49 9.20 -4 -12 -9 86.59 8.50 4 -12 9 88.59 8.70 -4 12 -9 97.49 8.40 4 12 9 79.29 7.80 -4 12 -9 100.79 10.40 5 -12 9 158.18 11.00 -5 -12 -9 172.48 10.90 -5 12 -9 160.28 12.40 5 12 9 156.38 10.30 -6 -12 -9 23.40 5.40 6 -12 9 17.50 5.60 6 12 9 17.40 5.20 -6 12 -9 20.10 6.40 10 -13 -9 81.79 8.50 10 -13 -9 88.19 9.10 -10 -13 9 90.19 9.30 10 13 -9 75.99 10.00 10 13 -9 88.69 9.00 -10 13 9 87.29 9.70 10 13 -9 92.49 9.90 9 -13 -9 20.10 5.40 -9 -13 9 22.80 5.40 9 -13 -9 27.60 6.20 9 13 -9 24.60 6.10 9 13 -9 24.10 5.60 9 13 -9 29.10 7.10 -9 13 9 27.70 6.40 -8 -13 9 149.69 10.90 8 -13 -9 151.28 10.60 -8 13 9 139.29 11.00 8 13 -9 189.28 13.00 8 13 -9 169.98 11.50 7 -13 -9 247.98 13.00 -7 -13 9 245.58 13.30 7 13 -9 241.08 13.30 7 13 -9 232.38 14.80 -6 -13 9 200.78 11.80 6 -13 -9 213.58 11.50 6 13 -9 205.18 13.70 6 13 -9 206.28 12.40 -5 -13 9 1.50 3.80 5 -13 -9 5.60 3.70 5 13 -9 5.50 4.00 5 13 -9 -2.70 3.50 4 -13 -9 100.79 8.10 -4 -13 9 108.39 8.80 4 13 -9 110.39 9.10 4 13 -9 104.09 10.60 -3 -13 9 18.30 4.70 3 -13 -9 21.10 4.90 3 13 -9 9.20 4.40 3 13 -9 19.20 4.90 -2 -13 9 1.40 3.70 2 -13 -9 -1.80 3.50 2 13 -9 1.90 3.80 2 13 -9 0.20 3.70 1 -13 -9 94.39 8.40 -1 -13 9 112.09 8.70 1 13 -9 102.99 8.70 1 13 -9 94.09 9.80 0 -13 9 1.70 3.50 0 -13 -9 6.90 4.10 0 13 -9 8.70 4.40 0 13 -9 5.20 3.90 -1 -13 -9 46.80 6.20 1 -13 9 38.10 5.70 -1 13 -9 44.60 6.50 -1 13 -9 45.50 7.30 -2 -13 -9 97.29 8.70 2 -13 9 96.79 8.80 -2 13 -9 92.49 9.90 -2 13 -9 101.39 9.00 3 -13 9 35.90 6.30 -3 -13 -9 32.40 5.90 -3 13 -9 28.40 6.20 -3 13 -9 26.80 5.40 -4 -13 -9 21.80 5.40 4 -13 9 19.10 5.40 -4 13 -9 27.30 6.60 4 13 9 22.00 5.90 -4 13 -9 18.30 5.00 5 -13 9 135.39 10.60 -5 -13 -9 97.39 9.00 -5 13 -9 105.49 11.20 5 13 9 104.19 9.40 8 -14 -9 7.80 4.50 -8 -14 9 2.90 4.10 8 14 -9 8.40 5.40 8 14 -9 7.00 4.40 -7 -14 9 44.80 7.00 7 -14 -9 48.10 6.60 7 14 -9 52.39 7.50 7 14 -9 66.09 8.80 6 -14 -9 25.30 5.50 -6 -14 9 24.90 5.40 6 14 -9 32.90 6.90 6 14 -9 29.80 6.20 5 -14 -9 2.90 4.20 -5 -14 9 -0.30 4.00 5 14 -9 -3.10 3.20 5 14 -9 0.70 4.00 4 -14 -9 416.76 17.40 -4 -14 9 424.46 17.80 4 14 -9 401.56 19.90 4 14 -9 425.66 18.40 3 -14 -9 648.74 23.70 -3 -14 9 662.33 23.80 3 14 -9 667.23 26.50 3 14 -9 647.24 24.40 2 -14 -9 336.77 15.40 -2 -14 9 331.47 15.00 2 14 -9 323.27 15.60 2 14 -9 330.77 17.30 1 -14 -9 1.40 4.00 -1 -14 9 0.00 3.80 1 14 -9 4.60 3.80 1 14 -9 -1.00 3.90 0 -14 9 -0.30 3.40 0 -14 -9 0.00 3.60 0 14 -9 1.40 3.80 0 14 -9 -1.10 4.00 1 -14 9 116.19 9.50 -1 -14 -9 128.79 9.60 -1 14 -9 122.69 9.60 -1 14 -9 106.59 10.90 -2 -14 -9 300.97 14.60 2 -14 9 297.97 14.90 -2 14 -9 313.87 17.10 -2 14 -9 286.77 14.60 3 -14 9 7.40 4.50 -3 -14 -9 5.80 4.30 -3 14 -9 1.20 4.30 -3 14 -9 14.00 4.70 -4 -14 -9 8.30 4.40 -4 14 -9 1.70 3.90 -4 14 -9 2.40 4.80 -7 -15 9 48.30 7.20 7 -15 -9 57.09 7.80 7 15 -9 50.29 8.40 7 15 -9 34.20 6.80 -6 -15 9 319.17 15.60 6 -15 -9 273.07 14.90 6 15 -9 313.87 17.70 6 15 -9 281.87 15.40 -5 -15 9 88.29 8.80 5 -15 -9 71.39 7.80 5 15 -9 67.39 9.20 5 15 -9 90.79 9.20 -4 -15 9 4.50 4.40 4 -15 -9 2.40 3.90 4 15 -9 6.90 4.20 4 15 -9 0.60 4.30 3 -15 -9 17.00 5.00 -3 -15 9 18.40 5.20 3 15 -9 7.70 4.80 3 15 -9 15.90 5.10 2 -15 -9 5.50 4.00 -2 -15 9 8.10 4.60 2 15 -9 -0.80 4.20 2 15 -9 6.50 5.00 -1 -15 9 22.00 5.50 1 -15 -9 21.30 5.50 1 15 -9 19.90 5.40 1 15 -9 8.20 5.10 0 -15 -9 37.90 6.20 0 -15 9 30.00 6.00 0 15 -9 28.40 5.80 0 15 -9 26.90 6.50 -1 -15 -9 24.30 5.80 1 -15 9 29.90 6.00 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2.50 8 -1 -10 248.38 9.70 8 -1 -10 276.97 11.70 8 1 -10 240.08 8.90 8 1 -10 256.17 11.40 7 -1 -10 518.45 16.70 7 -1 -10 566.54 18.90 7 1 -10 544.25 18.80 7 1 -10 533.95 16.10 6 -1 -10 595.24 18.10 6 -1 -10 603.34 20.00 6 1 -10 576.14 17.40 6 1 -10 597.34 19.90 5 -1 -10 7.30 2.10 5 -1 -10 5.40 2.40 5 1 -10 4.80 2.40 5 1 -10 8.00 1.90 4 -1 -10 1936.11 52.19 4 -1 -10 2014.30 53.99 -4 -1 10 1909.71 50.59 4 1 -10 1979.60 53.89 4 1 -10 1976.60 51.69 3 -1 -10 5.80 2.60 3 -1 -10 9.80 2.40 -3 -1 10 11.60 1.60 3 1 -10 15.90 3.40 3 1 -10 12.50 1.90 3 1 -10 7.40 2.00 2 -1 -10 3.40 1.90 -2 -1 10 7.20 1.30 2 -1 -10 5.00 2.70 2 1 -10 6.30 1.40 2 1 -10 6.30 2.00 2 1 -10 5.20 2.40 -1 -1 10 183.88 5.90 1 -1 -10 190.08 8.30 1 -1 -10 184.98 8.70 1 1 -10 187.48 8.10 1 1 -10 174.58 6.20 1 1 -10 163.48 8.40 0 -1 10 116.09 4.50 0 -1 -10 123.29 7.00 0 -1 -10 114.89 6.70 0 1 -10 119.59 6.80 0 1 -10 119.89 6.50 0 1 -10 114.39 5.00 -1 -1 -10 120.29 6.90 1 -1 10 100.79 4.50 -1 -1 -10 107.29 6.40 -1 1 -10 104.49 6.50 -1 1 -10 109.49 5.20 1 1 10 116.19 7.60 -1 1 -10 107.09 6.30 2 -1 10 777.32 24.80 -2 -1 -10 735.83 23.20 2 -1 10 718.93 21.00 -2 -1 -10 817.42 24.20 -2 1 -10 783.52 23.90 -2 1 -10 760.12 23.30 2 1 10 754.92 24.70 3 -1 10 14.80 2.40 -3 -1 -10 18.50 3.60 3 -1 10 14.70 4.00 -3 -1 -10 18.50 3.20 -3 1 -10 16.90 3.20 -3 1 -10 17.10 3.50 -3 1 -10 11.60 3.30 3 1 10 13.30 3.80 4 -1 10 416.56 14.80 -4 -1 -10 412.06 16.00 4 -1 10 452.85 17.20 -4 -1 -10 422.06 14.80 -4 1 -10 455.05 16.30 -4 1 -10 442.06 14.90 4 1 10 440.86 17.10 5 -1 10 162.28 9.80 -5 -1 -10 141.69 8.80 -5 1 -10 160.88 9.10 5 1 10 153.08 9.70 -6 -1 -10 7.60 3.70 6 -1 10 9.00 4.10 6 1 10 6.70 3.80 -6 1 -10 7.30 3.30 -7 -1 -10 11.60 3.80 7 -1 10 14.90 4.60 7 1 10 16.40 4.70 -7 1 -10 11.30 3.70 -8 -1 -10 113.99 8.60 8 -1 10 124.29 10.00 8 1 10 114.39 9.50 -8 1 -10 108.59 8.70 9 -1 10 65.69 8.10 -9 -1 -10 40.40 6.30 9 1 10 55.69 7.60 -9 1 -10 46.60 6.70 14 -2 -10 187.98 11.40 14 2 -10 175.58 11.40 13 -2 -10 -2.60 3.10 13 -2 -10 -0.50 2.90 13 2 -10 3.80 3.30 13 2 -10 5.80 4.00 12 -2 -10 44.10 5.60 12 -2 -10 63.59 6.70 12 2 -10 57.39 7.00 12 2 -10 58.39 6.20 11 -2 -10 292.87 13.00 11 -2 -10 311.87 13.50 11 2 -10 302.97 13.80 11 2 -10 314.07 13.50 10 -2 -10 246.38 11.50 10 -2 -10 245.38 11.40 10 -2 -10 264.67 10.50 10 2 -10 261.67 11.90 10 2 -10 243.48 11.90 9 -2 -10 298.27 12.70 9 -2 -10 290.17 11.20 9 2 -10 289.47 12.60 9 2 -10 287.77 12.70 8 -2 -10 1387.86 40.20 8 -2 -10 1367.96 38.30 8 2 -10 1391.76 40.20 7 -2 -10 94.39 6.60 7 -2 -10 98.69 5.80 7 2 -10 106.89 7.00 7 2 -10 84.19 4.40 6 -2 -10 54.69 4.50 6 -2 -10 47.70 5.00 6 2 -10 60.19 3.60 6 2 -10 65.09 5.40 5 -2 -10 2.20 1.90 5 -2 -10 3.10 2.60 5 2 -10 -0.60 2.00 5 2 -10 0.70 1.40 -4 -2 10 12.50 2.00 4 -2 -10 7.20 2.70 4 -2 -10 8.60 2.40 4 2 -10 10.50 2.00 4 2 -10 10.40 3.10 3 -2 -10 8.40 2.40 3 -2 -10 13.00 3.20 -3 -2 10 8.70 1.80 3 2 -10 8.50 2.70 3 2 -10 9.30 2.10 3 2 -10 10.30 2.00 2 -2 -10 -0.10 1.80 -2 -2 10 -0.40 1.20 2 -2 -10 1.50 2.30 2 2 -10 3.50 1.80 2 2 -10 -1.10 2.10 2 2 -10 2.20 1.40 1 -2 -10 114.49 6.90 -1 -2 10 119.69 4.90 1 -2 -10 128.59 6.80 1 2 -10 121.19 5.40 1 2 -10 125.09 7.00 1 2 -10 113.49 6.20 0 -2 -10 152.88 7.80 0 -2 10 148.09 5.80 0 -2 -10 163.38 8.00 0 2 -10 166.18 8.00 0 2 -10 154.38 7.40 0 2 -10 135.89 6.30 -1 -2 -10 413.06 14.70 -1 -2 -10 419.26 15.00 1 -2 10 398.56 12.60 -1 2 -10 425.46 14.80 1 2 10 414.76 15.70 -1 2 -10 431.76 14.80 -2 -2 -10 12.90 3.10 -2 -2 -10 12.60 3.20 2 -2 10 12.70 3.60 2 -2 10 14.40 2.40 -2 2 -10 9.80 2.40 -2 2 -10 16.40 3.40 -2 2 -10 14.70 3.10 2 2 10 11.60 3.30 -3 -2 -10 34.20 4.50 3 -2 10 32.40 4.90 -3 -2 -10 39.20 4.30 3 -2 10 34.60 3.50 -3 2 -10 43.20 4.30 -3 2 -10 46.50 4.50 3 2 10 50.79 6.00 -3 2 -10 42.20 4.80 4 -2 10 618.54 22.00 4 -2 10 611.94 19.10 -4 -2 -10 642.44 21.40 -4 2 -10 638.04 19.80 4 2 10 670.63 22.40 -4 2 -10 593.34 20.00 -4 2 -10 612.74 20.90 -5 -2 -10 9.40 3.20 5 -2 10 4.20 2.70 5 -2 10 1.50 3.40 -5 2 -10 9.00 3.10 5 2 10 1.40 3.30 6 -2 10 425.86 17.80 -6 -2 -10 430.16 17.20 6 -2 10 431.86 19.70 6 2 10 472.45 18.30 -6 2 -10 461.85 17.50 -7 -2 -10 13.00 3.70 7 -2 10 10.00 4.10 -7 2 -10 7.20 3.80 7 2 10 5.30 3.70 -8 -2 -10 24.30 5.10 8 -2 10 16.70 4.70 -8 2 -10 25.80 5.20 8 2 10 30.30 6.00 9 -2 10 174.88 12.20 -9 -2 -10 152.38 10.80 -9 2 -10 177.18 10.90 9 2 10 170.98 11.70 14 -3 -10 124.79 9.20 14 3 -10 135.59 10.10 13 -3 -10 4.10 3.70 13 -3 -10 -2.90 3.10 13 3 -10 0.80 3.10 13 3 -10 0.20 3.60 12 -3 -10 418.06 16.60 12 -3 -10 449.46 17.20 12 3 -10 424.86 17.70 12 3 -10 425.26 16.80 11 -3 -10 80.89 7.20 11 -3 -10 83.99 7.20 11 -3 -10 71.89 6.10 11 3 -10 76.49 7.10 11 3 -10 82.59 7.80 10 -3 -10 82.09 6.80 10 -3 -10 60.49 5.50 10 3 -10 79.89 7.20 10 3 -10 82.49 6.70 9 -3 -10 0.80 2.40 9 -3 -10 1.00 2.60 9 3 -10 0.20 2.60 9 3 -10 -1.00 2.90 8 -3 -10 414.36 15.80 8 -3 -10 421.86 14.60 8 3 -10 413.56 16.00 8 3 -10 420.86 15.70 7 -3 -10 329.87 12.20 7 -3 -10 328.97 13.50 7 3 -10 342.27 13.60 6 -3 -10 279.27 10.60 6 -3 -10 283.27 11.90 6 3 -10 279.37 11.20 6 3 -10 266.97 11.60 6 3 -10 248.68 8.60 5 -3 -10 2.70 2.70 5 -3 -10 4.20 2.20 5 3 -10 3.20 1.40 5 3 -10 4.90 2.70 5 3 -10 3.30 2.10 -5 3 10 3.10 1.70 -4 -3 10 517.55 15.00 4 -3 -10 499.15 17.10 4 -3 -10 473.25 15.90 4 3 -10 476.95 16.90 4 3 -10 475.15 14.60 -4 3 10 493.15 13.70 4 3 -10 482.25 15.90 3 -3 -10 206.98 9.60 -3 -3 10 207.98 7.50 3 -3 -10 196.88 8.70 3 3 -10 163.78 7.70 3 3 -10 210.28 7.80 3 3 -10 226.48 9.80 -2 -3 10 304.47 10.00 2 -3 -10 317.67 12.30 2 -3 -10 303.57 11.60 2 3 -10 309.57 12.30 2 3 -10 302.17 10.80 1 -3 -10 841.12 24.90 -1 -3 10 791.52 22.50 1 -3 -10 810.72 25.10 1 3 -10 815.42 25.10 1 3 -10 818.62 24.00 0 -3 10 568.84 17.00 0 -3 -10 622.94 19.50 0 -3 -10 578.64 19.20 0 3 -10 607.74 19.50 0 3 -10 567.44 18.50 -1 -3 -10 770.42 24.00 1 -3 10 775.62 22.00 -1 -3 -10 805.12 24.40 1 3 10 768.52 24.70 -1 3 -10 759.32 23.80 -1 3 -10 767.82 23.70 -1 3 -10 782.22 23.40 -2 -3 -10 100.99 6.30 -2 -3 -10 93.59 6.50 2 -3 10 105.49 5.50 2 -3 10 104.69 7.50 -2 3 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-15 11.90 4.10 4 7 -15 12.70 4.80 3 -7 -15 476.75 19.00 3 7 -15 467.75 19.80 -3 7 15 497.45 19.80 2 -7 -15 24.90 5.30 -2 7 15 32.30 6.10 2 7 -15 35.10 6.40 1 -7 -15 311.77 14.80 -1 7 15 306.87 15.20 1 7 -15 295.27 15.00 0 -7 -15 12.90 4.30 0 7 -15 8.70 4.50 0 7 15 -0.60 4.20 -1 -7 -15 20.90 5.40 1 -7 15 28.80 6.10 1 7 15 24.70 6.30 -1 7 -15 18.50 5.10 -1 7 -15 19.30 4.50 9 -8 -15 89.59 8.80 9 8 -15 103.09 9.90 8 -8 -15 24.00 5.20 8 8 -15 25.90 5.40 7 -8 -15 154.68 10.30 7 8 -15 175.58 11.60 6 -8 -15 243.78 13.00 6 8 -15 245.48 13.60 5 -8 -15 97.59 8.80 5 8 -15 96.99 9.50 4 -8 -15 -5.70 3.10 4 8 -15 2.20 4.00 3 -8 -15 126.39 9.80 -3 8 15 138.19 10.60 3 8 -15 125.59 10.20 2 -8 -15 4.70 3.80 -2 8 15 -4.90 4.30 2 8 -15 -0.20 3.90 1 -8 -15 111.29 9.70 -1 8 15 106.09 9.70 1 8 -15 100.89 9.60 0 -8 -15 14.40 4.50 0 8 15 7.10 4.90 0 8 -15 5.50 4.60 -1 -8 -15 -4.40 3.20 7 -9 -15 130.39 9.90 7 9 -15 126.19 10.50 6 -9 -15 22.20 5.50 6 9 -15 9.10 4.70 5 -9 -15 112.39 9.80 5 9 -15 107.49 10.50 4 -9 -15 51.89 7.00 4 9 -15 50.89 7.50 -4 9 15 47.20 6.80 3 -9 -15 268.77 14.00 -3 9 15 239.78 13.40 3 9 -15 255.07 14.40 2 -9 -15 38.90 6.60 -2 9 15 38.30 6.50 2 9 -15 60.89 8.00 1 -9 -15 12.50 4.70 1 9 -15 0.80 4.50 -1 9 15 10.20 5.00 5 -10 -15 150.88 10.90 5 10 -15 159.08 11.80 4 -10 -15 59.19 7.80 4 10 -15 56.89 7.80 3 -10 -15 205.48 12.50 3 10 -15 218.18 13.50 10 0 -16 32.70 6.30 9 0 -16 -3.80 3.40 8 0 -16 109.09 10.00 7 0 -16 2.40 3.80 6 0 -16 5.60 3.80 5 0 -16 -1.50 3.70 5 0 -16 -1.00 2.80 4 0 -16 17.50 5.20 4 0 -16 29.90 4.90 3 0 -16 -6.00 3.30 3 0 -16 -1.50 2.80 2 0 -16 1155.98 37.30 2 0 -16 1190.28 36.50 1 0 -16 -4.70 3.30 1 0 -16 2.10 3.40 0 0 -16 1.80 4.00 0 0 16 2.80 4.80 0 0 -16 8.00 4.00 -1 0 -16 2.70 3.80 -1 0 -16 4.90 3.70 1 0 16 1.30 4.80 -2 0 -16 213.08 12.20 -2 0 -16 214.98 13.80 2 0 16 192.08 13.40 10 -1 -16 32.70 6.30 10 1 -16 27.50 5.90 9 -1 -16 7.80 4.30 9 1 -16 9.10 4.30 8 -1 -16 142.39 10.10 8 1 -16 143.09 10.50 7 -1 -16 -0.10 3.70 7 1 -16 -1.30 3.60 6 -1 -16 634.54 23.80 6 -1 -16 621.04 21.40 6 1 -16 630.74 23.80 5 -1 -16 205.28 12.20 5 -1 -16 195.38 10.30 5 1 -16 193.68 12.00 4 -1 -16 361.66 16.30 4 -1 -16 334.77 14.70 4 1 -16 339.37 14.20 4 1 -16 345.57 15.90 3 -1 -16 4.50 3.40 3 -1 -16 9.30 4.40 3 1 -16 13.20 3.80 3 1 -16 5.60 4.20 2 -1 -16 225.28 12.40 2 -1 -16 204.78 11.40 2 1 -16 191.58 11.90 2 1 -16 199.48 11.00 1 -1 -16 33.90 5.50 1 -1 -16 37.10 6.30 1 1 -16 35.80 6.00 1 1 -16 36.40 5.70 0 -1 16 9.10 5.10 0 -1 -16 7.90 4.30 0 -1 -16 11.30 4.30 0 1 -16 5.60 4.20 0 1 16 -0.30 4.60 0 1 -16 5.50 3.60 -1 -1 -16 6.00 3.90 1 -1 16 6.40 5.00 -1 -1 -16 1.20 4.00 -1 1 -16 5.90 3.90 1 1 16 9.80 5.90 -1 1 -16 5.40 4.10 -2 -1 -16 91.29 9.10 -2 -1 -16 88.49 9.10 2 -1 16 97.79 10.40 -2 1 -16 90.79 8.60 2 1 16 101.89 10.40 10 -2 -16 0.00 3.90 10 2 -16 4.90 4.20 9 -2 -16 96.09 9.50 9 2 -16 94.09 9.40 8 -2 -16 18.50 5.10 8 2 -16 18.00 5.20 7 -2 -16 4.40 4.30 7 -2 -16 3.50 3.20 7 2 -16 4.40 3.40 6 -2 -16 106.59 9.60 6 -2 -16 105.89 7.80 6 2 -16 117.19 9.60 5 -2 -16 208.08 12.60 5 -2 -16 218.58 11.10 5 2 -16 227.58 12.90 4 -2 -16 134.19 10.00 4 -2 -16 136.09 9.00 4 2 -16 130.59 10.10 3 -2 -16 21.90 4.80 3 -2 -16 17.50 4.80 3 2 -16 13.00 3.80 3 2 -16 14.40 4.70 2 -2 -16 108.59 9.60 2 -2 -16 107.99 8.60 2 2 -16 112.39 9.50 2 2 -16 114.99 8.30 1 -2 -16 19.20 4.80 1 -2 -16 26.40 5.60 1 2 -16 19.40 5.00 1 2 -16 13.20 4.20 -1 2 16 8.80 5.30 0 -2 -16 132.99 9.50 0 -2 -16 123.79 9.60 0 2 -16 127.49 10.00 0 2 16 93.99 9.90 0 2 -16 110.69 8.90 -1 -2 -16 0.40 3.60 1 -2 16 7.80 5.10 -1 -2 -16 4.30 4.20 1 2 16 3.20 5.10 -1 2 -16 5.20 3.90 -1 2 -16 2.30 3.90 -2 -2 -16 145.99 10.70 2 -2 16 157.98 12.40 -2 -2 -16 164.48 10.70 -2 2 -16 179.68 10.90 2 2 16 157.58 12.60 10 -3 -16 129.99 10.50 10 3 -16 122.39 10.10 9 -3 -16 50.39 7.30 9 3 -16 34.50 6.30 8 -3 -16 586.54 22.80 8 -3 -16 557.54 20.10 8 3 -16 565.94 22.40 7 -3 -16 -0.20 3.80 7 -3 -16 0.10 3.10 7 3 -16 4.80 3.70 6 -3 -16 186.28 11.80 6 -3 -16 178.58 10.20 6 3 -16 200.88 12.10 5 -3 -16 127.79 10.00 5 -3 -16 145.29 9.20 5 3 -16 123.99 9.50 4 -3 -16 86.59 7.90 4 -3 -16 79.99 8.20 4 3 -16 85.59 8.40 3 -3 -16 121.59 9.00 3 -3 -16 127.09 10.00 3 3 -16 140.29 10.20 2 -3 -16 58.79 7.10 2 -3 -16 68.79 7.80 2 3 -16 62.69 6.60 2 3 -16 63.99 7.80 1 -3 -16 -1.30 3.90 1 -3 -16 2.30 3.60 1 3 -16 1.20 3.10 1 3 -16 0.70 3.90 -1 3 16 3.40 4.80 0 -3 -16 261.47 13.60 0 -3 -16 223.88 13.20 0 3 -16 258.67 13.80 0 3 -16 236.28 12.60 0 3 16 245.98 14.60 -1 -3 -16 5.00 4.30 1 -3 16 13.00 5.40 -1 -3 -16 8.20 3.90 -1 3 -16 6.40 4.40 -1 3 -16 7.10 3.90 1 3 16 6.70 5.00 10 -4 -16 8.10 4.60 10 4 -16 12.10 4.90 9 -4 -16 177.18 10.50 9 -4 -16 209.78 12.70 9 4 -16 180.48 11.60 8 -4 -16 72.79 7.10 8 -4 -16 61.69 7.90 8 4 -16 61.89 7.70 7 -4 -16 31.80 6.10 7 -4 -16 31.80 5.30 7 4 -16 29.40 5.50 6 -4 -16 0.40 3.80 6 -4 -16 2.50 3.30 6 4 -16 -4.20 3.50 5 -4 -16 91.79 8.20 5 -4 -16 95.39 9.10 5 4 -16 95.49 8.90 4 -4 -16 182.48 11.70 4 -4 -16 172.48 10.50 4 4 -16 172.98 11.40 3 -4 -16 19.10 4.80 3 -4 -16 14.50 5.10 3 4 -16 7.30 4.40 2 -4 -16 23.40 5.40 2 -4 -16 29.10 5.40 2 4 -16 20.60 5.40 1 -4 -16 16.90 5.10 1 -4 -16 5.50 4.00 1 4 -16 9.50 4.60 1 4 -16 4.40 3.40 -1 4 16 10.30 5.40 0 -4 -16 405.96 18.00 0 -4 -16 414.76 18.00 0 4 16 441.66 19.60 0 4 -16 414.46 17.20 0 4 -16 416.26 18.10 1 -4 16 65.99 9.00 -1 -4 -16 93.99 9.30 1 4 16 91.49 9.90 -1 4 -16 74.89 8.20 -1 4 -16 71.19 7.60 9 -5 -16 194.08 11.10 9 -5 -16 187.38 12.30 9 5 -16 177.48 11.90 8 -5 -16 215.98 12.90 8 -5 -16 184.68 10.90 8 5 -16 206.28 12.60 7 -5 -16 64.29 7.20 7 -5 -16 86.89 8.90 7 5 -16 65.79 8.20 6 -5 -16 152.18 10.80 6 -5 -16 142.09 9.70 6 5 -16 131.39 10.40 5 -5 -16 7.70 4.50 5 -5 -16 7.00 3.80 5 5 -16 0.00 3.90 4 -5 -16 25.60 5.90 4 -5 -16 16.50 4.70 4 5 -16 17.90 5.10 3 -5 -16 3.00 4.30 3 -5 -16 4.40 3.80 3 5 -16 1.40 4.10 2 -5 -16 0.60 4.00 2 -5 -16 -2.40 3.10 -2 5 16 -6.10 4.20 2 5 -16 2.70 4.30 1 -5 -16 202.78 12.20 -1 5 16 232.68 13.80 1 5 -16 212.48 12.90 0 -5 -16 2.40 4.10 0 5 16 6.80 5.10 0 5 -16 -0.90 3.00 0 5 -16 7.30 4.40 -1 -5 -16 266.17 14.10 -1 5 -16 236.28 12.60 -1 5 -16 255.77 13.90 8 -6 -16 2.20 4.20 8 -6 -16 17.20 4.70 8 6 -16 19.80 5.20 7 -6 -16 28.20 5.60 7 -6 -16 26.90 5.90 7 6 -16 27.80 6.10 6 -6 -16 362.16 17.10 6 -6 -16 352.06 15.80 6 6 -16 343.67 16.60 5 -6 -16 28.10 6.00 5 -6 -16 43.30 6.30 5 6 -16 37.00 6.10 4 -6 -16 13.40 4.50 4 6 -16 16.60 5.20 3 -6 -16 6.50 4.00 3 6 -16 6.00 4.10 2 -6 -16 322.57 15.30 -2 6 16 281.77 15.80 2 6 -16 326.17 15.70 1 -6 -16 17.70 5.10 -1 6 16 24.10 6.50 1 6 -16 17.20 5.30 0 -6 -16 281.97 14.10 0 6 -16 250.07 14.00 0 6 16 236.58 14.40 7 -7 -16 58.99 7.20 7 7 -16 74.19 9.00 6 -7 -16 111.89 8.60 6 7 -16 87.69 9.10 5 -7 -16 74.59 8.00 5 7 -16 64.49 8.10 4 -7 -16 51.19 7.10 4 7 -16 52.19 7.30 3 -7 -16 13.50 4.50 -3 7 16 11.70 5.40 3 7 -16 15.10 5.20 2 -7 -16 58.89 7.70 -2 7 16 57.09 7.90 2 7 -16 62.69 8.10 1 -7 -16 75.09 8.20 1 7 -16 63.39 7.90 -1 7 16 59.29 8.30 6 -8 -16 152.78 10.40 6 8 -16 153.68 11.60 5 -8 -16 21.30 5.00 5 8 -16 27.30 6.50 4 -8 -16 -0.40 4.10 4 8 -16 1.90 3.90 -4 8 16 6.30 4.90 3 -8 -16 -0.60 4.00 3 8 -16 7.10 4.40 -3 8 16 6.70 4.70 9 0 -17 186.68 12.30 8 0 -17 -0.30 3.70 7 0 -17 259.77 14.40 6 0 -17 2.30 4.00 5 0 -17 294.37 15.30 4 0 -17 3.80 4.30 4 0 -17 2.80 3.40 3 0 -17 3.60 3.70 3 0 -17 10.40 4.70 2 0 -17 4.80 4.30 2 0 -17 2.50 3.50 1 0 -17 275.37 14.80 1 0 -17 273.07 13.90 0 0 -17 -0.50 3.20 0 0 -17 -4.60 3.90 0 0 17 -1.70 4.80 9 -1 -17 18.90 5.40 9 1 -17 28.80 6.00 8 -1 -17 5.30 4.50 8 1 -17 6.80 4.10 7 -1 -17 92.89 9.40 7 1 -17 92.39 9.50 6 -1 -17 108.59 10.10 6 1 -17 97.49 9.60 5 -1 -17 531.65 19.60 5 -1 -17 496.85 21.20 5 1 -17 518.65 21.50 4 -1 -17 6.90 4.50 4 -1 -17 9.90 4.10 4 1 -17 4.00 4.30 3 -1 -17 327.17 16.00 3 -1 -17 338.67 15.20 3 1 -17 324.07 16.20 3 1 -17 339.17 15.00 2 -1 -17 38.80 6.70 2 -1 -17 44.30 6.60 2 1 -17 39.40 6.70 2 1 -17 41.20 6.20 1 -1 -17 6.30 4.40 1 -1 -17 5.90 3.90 1 1 -17 0.70 3.60 1 1 -17 1.90 4.30 -1 1 17 9.20 5.50 8 -2 -17 198.38 12.60 8 2 -17 186.78 12.00 7 -2 -17 301.47 15.80 7 2 -17 309.77 15.90 6 -2 -17 129.19 10.60 6 -2 -17 130.29 9.10 6 2 -17 129.09 10.50 5 -2 -17 193.38 10.90 5 -2 -17 196.18 12.50 5 2 -17 188.68 12.40 4 -2 -17 15.90 5.30 4 -2 -17 4.20 3.80 4 2 -17 3.80 4.50 3 -2 -17 104.29 9.70 3 -2 -17 88.89 8.50 3 2 -17 85.09 9.00 2 -2 -17 3.50 4.30 2 -2 -17 1.00 3.70 2 2 -17 3.90 4.40 2 2 -17 3.30 3.50 1 -2 -17 116.99 9.40 1 -2 -17 119.59 10.60 1 2 -17 131.59 10.30 1 2 -17 116.69 9.00 -1 2 17 106.19 10.60 8 -3 -17 122.69 11.00 8 3 -17 117.59 10.60 7 -3 -17 51.29 7.50 7 -3 -17 43.10 5.90 7 3 -17 32.20 6.40 6 -3 -17 -0.50 4.10 6 -3 -17 2.20 3.70 6 3 -17 2.30 4.10 5 -3 -17 286.67 14.90 5 -3 -17 241.08 12.80 5 3 -17 260.47 14.40 4 -3 -17 7.90 4.00 4 -3 -17 4.80 4.70 4 3 -17 14.60 5.30 3 -3 -17 191.18 12.30 3 -3 -17 198.48 11.80 3 3 -17 218.28 13.00 2 -3 -17 86.29 9.00 2 -3 -17 93.39 8.90 2 3 -17 84.69 9.30 1 -3 -17 5.20 4.00 1 -3 -17 -1.10 4.40 -1 3 17 10.80 5.50 1 3 -17 -0.10 3.90 1 3 -17 4.20 3.70 7 -4 -17 623.24 24.30 7 -4 -17 633.04 22.60 7 4 -17 600.74 24.20 6 -4 -17 18.70 5.70 6 -4 -17 19.00 4.90 6 4 -17 14.10 5.20 5 -4 -17 52.59 7.80 5 -4 -17 48.60 6.70 5 4 -17 42.10 7.00 4 -4 -17 3.90 4.50 4 -4 -17 7.50 4.00 4 4 -17 5.50 4.40 3 -4 -17 47.60 6.80 3 -4 -17 44.70 7.00 3 4 -17 35.00 6.50 2 -4 -17 -2.60 3.40 2 -4 -17 12.00 5.30 2 4 -17 -2.30 3.90 -2 4 17 0.30 4.80 6 -5 -17 -0.40 3.60 6 -5 -17 -2.60 4.10 6 5 -17 0.90 4.00 5 -5 -17 32.70 5.80 5 -5 -17 26.50 6.10 5 5 -17 26.50 6.30 4 -5 -17 7.00 4.40 4 -5 -17 8.60 4.10 4 5 -17 11.80 5.10 3 -5 -17 84.89 8.60 3 -5 -17 92.09 9.40 3 5 -17 87.39 9.10 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 35231 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.28582(2) 0.74121(2) 0.53319(2) 0.01256(6) Uani 1 1 d . . . . . Cl1 Cl 0.46318(3) 0.88426(3) 0.49832(3) 0.02622(11) Uani 1 1 d . . . . . Cl2 Cl 0.06871(3) 0.80960(3) 0.24775(3) 0.02331(10) Uani 1 1 d . . . . . Cl3 Cl 0.36636(3) 0.80349(3) 0.79083(3) 0.02336(10) Uani 1 1 d . . . . . Cl4 Cl 0.05165(3) 0.59771(3) 0.57186(3) 0.02145(10) Uani 1 1 d . . . . . N1 N 0.22754(11) 0.83894(8) 0.44555(9) 0.0127(3) Uani 1 1 d . . . . . N2 N 0.19474(11) 0.75430(8) 0.61192(9) 0.0130(3) Uani 1 1 d . . . . . N3 N 0.40245(12) 0.68141(8) 0.50895(10) 0.0144(3) Uani 1 1 d . . . . . H3 H 0.4673(17) 0.6905(12) 0.5449(14) 0.022 Uiso 1 1 d . U . . . C1 C 0.15253(13) 0.89126(10) 0.45849(11) 0.0131(3) Uani 1 1 d . . . . . C2 C 0.10348(13) 0.87998(10) 0.53046(11) 0.0138(3) Uani 1 1 d . . . . . H2 H 0.049423 0.921350 0.530949 0.017 Uiso 1 1 calc R U . . . C3 C 0.12208(13) 0.81733(9) 0.60123(11) 0.0124(3) Uani 1 1 d . . . . . C4 C 0.11660(14) 0.97066(10) 0.39769(12) 0.0194(4) Uani 1 1 d . . . . . H4A H 0.158224 0.975179 0.352636 0.029 Uiso 1 1 calc R U . . . H4B H 0.129783 1.021760 0.438305 0.029 Uiso 1 1 calc R U . . . H4C H 0.038563 0.966403 0.362810 0.029 Uiso 1 1 calc R U . . . C5 C 0.05642(14) 0.82354(10) 0.66947(12) 0.0175(3) Uani 1 1 d . . . . . H5A H 0.014062 0.770685 0.666295 0.026 Uiso 1 1 calc R U . . . H5B H 0.006659 0.872725 0.652321 0.026 Uiso 1 1 calc R U . . . H5C H 0.105904 0.831232 0.734087 0.026 Uiso 1 1 calc R U . . . C6 C 0.26867(13) 0.84799(9) 0.36897(11) 0.0133(3) Uani 1 1 d . . . . . C7 C 0.38012(14) 0.86309(10) 0.38385(12) 0.0174(3) Uani 1 1 d . . . . . C8 C 0.42658(15) 0.86367(11) 0.31147(14) 0.0251(4) Uani 1 1 d . . . . . H8 H 0.502850 0.872600 0.325067 0.030 Uiso 1 1 calc R U . . . C9 C 0.36140(17) 0.85121(12) 0.21948(14) 0.0299(4) Uani 1 1 d . . . . . H9 H 0.392298 0.852694 0.169038 0.036 Uiso 1 1 calc R U . . . C10 C 0.25135(16) 0.83659(12) 0.20069(13) 0.0262(4) Uani 1 1 d . . . . . H10 H 0.206166 0.828318 0.137186 0.031 Uiso 1 1 calc R U . . . C11 C 0.20640(14) 0.83393(10) 0.27430(11) 0.0172(3) Uani 1 1 d . . . . . C12 C 0.21105(13) 0.69579(10) 0.68746(11) 0.0132(3) Uani 1 1 d . . . . . C13 C 0.29240(13) 0.70850(10) 0.77412(11) 0.0167(3) Uani 1 1 d . . . . . C14 C 0.31710(15) 0.64787(11) 0.84604(12) 0.0232(4) Uani 1 1 d . . . . . H14 H 0.373718 0.658321 0.903668 0.028 Uiso 1 1 calc R U . . . C15 C 0.25835(16) 0.57177(11) 0.83305(13) 0.0252(4) Uani 1 1 d . . . . . H15 H 0.274852 0.529677 0.881851 0.030 Uiso 1 1 calc R U . . . C16 C 0.17588(15) 0.55708(11) 0.74928(13) 0.0212(4) Uani 1 1 d . . . . . H16 H 0.134883 0.505295 0.740491 0.025 Uiso 1 1 calc R U . . . C17 C 0.15342(13) 0.61834(10) 0.67825(11) 0.0155(3) Uani 1 1 d . . . . . C18 C 0.40523(13) 0.63854(10) 0.43504(11) 0.0137(3) Uani 1 1 d . . . . . C19 C 0.30041(13) 0.61381(9) 0.36468(11) 0.0144(3) Uani 1 1 d . . . . . C20 C 0.28857(14) 0.61174(11) 0.26795(12) 0.0193(4) Uani 1 1 d . . . . . H20 H 0.349474 0.623375 0.246579 0.023 Uiso 1 1 calc R U . . . C21 C 0.18820(15) 0.59275(11) 0.20313(12) 0.0240(4) Uani 1 1 d . . . . . H21 H 0.180231 0.592146 0.137256 0.029 Uiso 1 1 calc R U . . . C22 C 0.09940(15) 0.57464(11) 0.23357(13) 0.0240(4) Uani 1 1 d . . . . . H22 H 0.030612 0.561778 0.188711 0.029 Uiso 1 1 calc R U . . . C23 C 0.11089(14) 0.57528(11) 0.32952(13) 0.0215(4) Uani 1 1 d . . . . . H23 H 0.050126 0.562120 0.350538 0.026 Uiso 1 1 calc R U . . . C24 C 0.21037(14) 0.59499(10) 0.39474(12) 0.0174(3) Uani 1 1 d . . . . . H24 H 0.217646 0.595756 0.460484 0.021 Uiso 1 1 calc R U . . . C25 C 0.51014(13) 0.61389(10) 0.42054(11) 0.0144(3) Uani 1 1 d . . . . . C26 C 0.59826(13) 0.67063(11) 0.44590(11) 0.0164(3) Uani 1 1 d . . . . . H26 H 0.589321 0.726377 0.468547 0.020 Uiso 1 1 calc R U . . . C27 C 0.69872(14) 0.64637(11) 0.43833(12) 0.0205(4) Uani 1 1 d . . . . . H27 H 0.758412 0.685330 0.455904 0.025 Uiso 1 1 calc R U . . . C28 C 0.71205(14) 0.56498(11) 0.40500(12) 0.0215(4) Uani 1 1 d . . . . . H28 H 0.781327 0.547771 0.401191 0.026 Uiso 1 1 calc R U . . . C29 C 0.62450(14) 0.50903(11) 0.37738(12) 0.0203(4) Uani 1 1 d . . . . . H29 H 0.633418 0.453887 0.353295 0.024 Uiso 1 1 calc R U . . . C30 C 0.52373(14) 0.53304(10) 0.38467(11) 0.0176(3) Uani 1 1 d . . . . . H30 H 0.463775 0.494438 0.365230 0.021 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.01389(11) 0.01338(10) 0.01222(10) 0.00134(7) 0.00671(8) 0.00390(7) Cl1 0.0185(2) 0.0241(2) 0.0330(2) -0.00603(18) 0.00345(18) -0.00534(17) Cl2 0.0202(2) 0.0295(2) 0.0173(2) -0.00023(17) 0.00157(17) -0.00001(17) Cl3 0.0208(2) 0.0243(2) 0.0250(2) -0.00563(17) 0.00703(17) -0.00465(17) Cl4 0.0201(2) 0.0241(2) 0.0214(2) -0.00497(16) 0.00828(17) -0.00485(16) N1 0.0143(7) 0.0129(6) 0.0118(6) 0.0005(5) 0.0055(5) 0.0006(5) N2 0.0148(7) 0.0129(6) 0.0125(7) 0.0021(5) 0.0063(5) 0.0024(5) N3 0.0138(7) 0.0165(7) 0.0133(7) 0.0027(5) 0.0047(6) 0.0034(5) C1 0.0139(8) 0.0113(7) 0.0134(8) -0.0001(6) 0.0032(6) -0.0001(6) C2 0.0148(8) 0.0117(7) 0.0157(8) -0.0001(6) 0.0059(6) 0.0037(6) C3 0.0132(8) 0.0125(7) 0.0121(8) -0.0029(6) 0.0047(6) -0.0006(6) C4 0.0245(9) 0.0157(8) 0.0217(9) 0.0046(7) 0.0126(7) 0.0057(7) C5 0.0203(9) 0.0180(8) 0.0176(8) 0.0029(6) 0.0109(7) 0.0059(7) C6 0.0171(8) 0.0094(7) 0.0156(8) 0.0032(6) 0.0083(6) 0.0031(6) C7 0.0190(9) 0.0126(7) 0.0223(9) 0.0032(7) 0.0091(7) 0.0006(6) C8 0.0234(10) 0.0196(9) 0.0398(11) 0.0086(8) 0.0210(9) 0.0037(7) C9 0.0429(12) 0.0284(10) 0.0308(11) 0.0104(8) 0.0296(9) 0.0095(9) C10 0.0376(11) 0.0277(9) 0.0165(9) 0.0046(7) 0.0129(8) 0.0073(8) C11 0.0188(9) 0.0178(8) 0.0165(8) 0.0032(7) 0.0074(7) 0.0029(7) C12 0.0153(8) 0.0133(7) 0.0150(8) 0.0012(6) 0.0104(6) 0.0053(6) C13 0.0170(8) 0.0172(8) 0.0174(8) -0.0008(7) 0.0075(7) 0.0028(6) C14 0.0226(9) 0.0286(10) 0.0173(9) 0.0043(7) 0.0047(7) 0.0094(7) C15 0.0338(11) 0.0218(9) 0.0241(9) 0.0112(7) 0.0150(8) 0.0115(8) C16 0.0280(10) 0.0143(8) 0.0273(9) 0.0031(7) 0.0173(8) 0.0026(7) C17 0.0164(8) 0.0162(8) 0.0164(8) -0.0008(6) 0.0090(7) 0.0031(6) C18 0.0175(8) 0.0116(7) 0.0138(8) 0.0036(6) 0.0076(6) 0.0029(6) C19 0.0166(8) 0.0104(7) 0.0165(8) -0.0003(6) 0.0056(7) 0.0044(6) C20 0.0199(9) 0.0211(8) 0.0191(9) -0.0016(7) 0.0091(7) 0.0034(7) C21 0.0253(10) 0.0283(9) 0.0169(9) -0.0042(7) 0.0042(7) 0.0026(8) C22 0.0197(9) 0.0222(9) 0.0262(10) -0.0040(7) 0.0014(7) -0.0006(7) C23 0.0165(9) 0.0203(9) 0.0287(10) 0.0018(7) 0.0084(7) -0.0011(7) C24 0.0202(9) 0.0149(8) 0.0188(8) 0.0010(6) 0.0083(7) 0.0028(6) C25 0.0163(8) 0.0180(8) 0.0102(7) 0.0039(6) 0.0060(6) 0.0048(6) C26 0.0190(9) 0.0198(8) 0.0120(8) 0.0000(6) 0.0070(7) 0.0038(7) C27 0.0177(9) 0.0286(9) 0.0169(8) 0.0012(7) 0.0080(7) 0.0004(7) C28 0.0195(9) 0.0288(9) 0.0197(9) 0.0065(7) 0.0112(7) 0.0098(7) C29 0.0273(10) 0.0172(8) 0.0209(9) 0.0047(7) 0.0142(7) 0.0090(7) C30 0.0214(9) 0.0167(8) 0.0171(8) 0.0029(6) 0.0093(7) 0.0035(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3 Cu1 N2 147.58(6) . . ? N3 Cu1 N1 114.37(6) . . ? N2 Cu1 N1 97.98(5) . . ? C1 N1 C6 122.17(13) . . ? C1 N1 Cu1 121.39(11) . . ? C6 N1 Cu1 116.43(10) . . ? C3 N2 C12 119.85(13) . . ? C3 N2 Cu1 123.35(11) . . ? C12 N2 Cu1 116.73(10) . . ? C18 N3 Cu1 130.25(12) . . ? C18 N3 H3 109.7(13) . . ? Cu1 N3 H3 118.8(13) . . ? N1 C1 C2 123.52(14) . . ? N1 C1 C4 121.22(14) . . ? C2 C1 C4 115.23(14) . . ? C3 C2 C1 129.98(15) . . ? C3 C2 H2 115.0 . . ? C1 C2 H2 115.0 . . ? N2 C3 C2 123.66(14) . . ? N2 C3 C5 119.12(14) . . ? C2 C3 C5 117.21(14) . . ? C1 C4 H4A 109.5 . . ? C1 C4 H4B 109.5 . . ? H4A C4 H4B 109.5 . . ? C1 C4 H4C 109.5 . . ? H4A C4 H4C 109.5 . . ? H4B C4 H4C 109.5 . . ? C3 C5 H5A 109.5 . . ? C3 C5 H5B 109.5 . . ? H5A C5 H5B 109.5 . . ? C3 C5 H5C 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? N1 C6 C11 123.59(14) . . ? N1 C6 C7 120.98(14) . . ? C11 C6 C7 115.09(15) . . ? C8 C7 C6 123.18(16) . . ? C8 C7 Cl1 118.34(14) . . ? C6 C7 Cl1 118.47(13) . . ? C9 C8 C7 119.41(17) . . ? C9 C8 H8 120.3 . . ? C7 C8 H8 120.3 . . ? C8 C9 C10 119.86(17) . . ? C8 C9 H9 120.1 . . ? C10 C9 H9 120.1 . . ? C9 C10 C11 120.07(17) . . ? C9 C10 H10 120.0 . . ? C11 C10 H10 120.0 . . ? C10 C11 C6 122.35(16) . . ? C10 C11 Cl2 118.35(14) . . ? C6 C11 Cl2 119.28(13) . . ? C13 C12 C17 115.81(14) . . ? C13 C12 N2 121.63(14) . . ? C17 C12 N2 122.36(14) . . ? C14 C13 C12 122.64(16) . . ? C14 C13 Cl3 119.04(13) . . ? C12 C13 Cl3 118.31(12) . . ? C13 C14 C15 119.31(16) . . ? C13 C14 H14 120.3 . . ? C15 C14 H14 120.3 . . ? C16 C15 C14 120.08(16) . . ? C16 C15 H15 120.0 . . ? C14 C15 H15 120.0 . . ? C15 C16 C17 119.48(16) . . ? C15 C16 H16 120.3 . . ? C17 C16 H16 120.3 . . ? C16 C17 C12 122.66(15) . . ? C16 C17 Cl4 118.96(13) . . ? C12 C17 Cl4 118.37(12) . . ? N3 C18 C19 118.26(14) . . ? N3 C18 C25 121.46(15) . . ? C19 C18 C25 120.28(14) . . ? C20 C19 C24 119.09(15) . . ? C20 C19 C18 121.11(15) . . ? C24 C19 C18 119.77(14) . . ? C21 C20 C19 120.03(16) . . ? C21 C20 H20 120.0 . . ? C19 C20 H20 120.0 . . ? C22 C21 C20 120.44(17) . . ? C22 C21 H21 119.8 . . ? C20 C21 H21 119.8 . . ? C21 C22 C23 119.88(16) . . ? C21 C22 H22 120.1 . . ? C23 C22 H22 120.1 . . ? C24 C23 C22 120.16(16) . . ? C24 C23 H23 119.9 . . ? C22 C23 H23 119.9 . . ? C23 C24 C19 120.39(16) . . ? C23 C24 H24 119.8 . . ? C19 C24 H24 119.8 . . ? C26 C25 C30 119.01(15) . . ? C26 C25 C18 119.95(14) . . ? C30 C25 C18 121.00(15) . . ? C27 C26 C25 120.55(15) . . ? C27 C26 H26 119.7 . . ? C25 C26 H26 119.7 . . ? C26 C27 C28 119.90(16) . . ? C26 C27 H27 120.0 . . ? C28 C27 H27 120.0 . . ? C29 C28 C27 120.01(16) . . ? C29 C28 H28 120.0 . . ? C27 C28 H28 120.0 . . ? C28 C29 C30 120.30(16) . . ? C28 C29 H29 119.8 . . ? C30 C29 H29 119.8 . . ? C29 C30 C25 120.18(16) . . ? C29 C30 H30 119.9 . . ? C25 C30 H30 119.9 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1 N3 1.8937(14) . ? Cu1 N2 1.9049(13) . ? Cu1 N1 1.9901(13) . ? Cl1 C7 1.7346(17) . ? Cl2 C11 1.7353(17) . ? Cl3 C13 1.7344(17) . ? Cl4 C17 1.7405(17) . ? N1 C1 1.322(2) . ? N1 C6 1.401(2) . ? N2 C3 1.331(2) . ? N2 C12 1.408(2) . ? N3 C18 1.293(2) . ? N3 H3 0.85(2) . ? C1 C2 1.409(2) . ? C1 C4 1.515(2) . ? C2 C3 1.397(2) . ? C2 H2 0.9500 . ? C3 C5 1.509(2) . ? C4 H4A 0.9800 . ? C4 H4B 0.9800 . ? C4 H4C 0.9800 . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 C11 1.401(2) . ? C6 C7 1.403(2) . ? C7 C8 1.381(2) . ? C8 C9 1.376(3) . ? C8 H8 0.9500 . ? C9 C10 1.376(3) . ? C9 H9 0.9500 . ? C10 C11 1.385(2) . ? C10 H10 0.9500 . ? C12 C13 1.398(2) . ? C12 C17 1.400(2) . ? C13 C14 1.385(2) . ? C14 C15 1.386(3) . ? C14 H14 0.9500 . ? C15 C16 1.381(3) . ? C15 H15 0.9500 . ? C16 C17 1.383(2) . ? C16 H16 0.9500 . ? C18 C19 1.479(2) . ? C18 C25 1.483(2) . ? C19 C20 1.395(2) . ? C19 C24 1.396(2) . ? C20 C21 1.383(2) . ? C20 H20 0.9500 . ? C21 C22 1.382(3) . ? C21 H21 0.9500 . ? C22 C23 1.384(3) . ? C22 H22 0.9500 . ? C23 C24 1.380(2) . ? C23 H23 0.9500 . ? C24 H24 0.9500 . ? C25 C26 1.395(2) . ? C25 C30 1.398(2) . ? C26 C27 1.386(2) . ? C26 H26 0.9500 . ? C27 C28 1.389(2) . ? C27 H27 0.9500 . ? C28 C29 1.383(3) . ? C28 H28 0.9500 . ? C29 C30 1.387(2) . ? C29 H29 0.9500 . ? C30 H30 0.9500 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag N3 H3 Cl2 0.85(2) 2.88(2) 3.5279(14) 133.8(16) 4_676 yes