#------------------------------------------------------------------------------ #$Date: 2021-11-06 01:12:47 +0200 (Sat, 06 Nov 2021) $ #$Revision: 270329 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/51/1565132.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1565132 loop_ _publ_author_name 'He, Weiying' 'Beattie, D. Dawson' 'Zhou, Hao' 'Bowes, Eric G.' 'Schafer, Laurel L.' 'Love, Jennifer' 'Kennepohl, Pierre' _publ_section_title ; Direct metal-carbon bonding in symmetric bis(C-H) agostic Nickel(I) complexes ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC03578A _journal_year 2021 _chemical_formula_moiety 'C27 H38 Cu N2 O' _chemical_formula_sum 'C27 H38 Cu N2 O' _chemical_formula_weight 470.13 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_block_doi 10.5517/ccdc.csd.cc23453k _audit_creation_method SHELXL-2017/1 _audit_update_record ; 2019-08-03 deposited with the CCDC. 2021-10-29 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 101.785(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 15.755(4) _cell_length_b 9.051(2) _cell_length_c 18.592(4) _cell_measurement_reflns_used 7383 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 25.49 _cell_measurement_theta_min 2.24 _cell_volume 2595.3(10) _computing_cell_refinement 'SAINT V8.37A (Bruker, 2005)' _computing_data_collection 'APEX3 V2016.5-0 (Bruker, 2016)' _computing_data_reduction ; SAINT V8.37A, XPREP v2014/2, SADABS V2016/2 (Bruker, 2016) ; _computing_molecular_graphics 'SHELXLE v932 (Hubschle, 2011)' _computing_publication_material 'XCIF V2014-2 (Bruker, 2014)' _computing_structure_refinement 'SHELX-2018-1 (Sheldrick, 2015)' _computing_structure_solution 'SHELX-2014-5 (Sheldrick, 2015)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device 'Bruker APEX DUO/ApexII CCD' _diffrn_measurement_method 'profile data from \f and \w scans' _diffrn_radiation_monochromator 'multilayer mirrors' _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0689 _diffrn_reflns_av_unetI/netI 0.0450 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_h_min -19 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 27153 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.586 _diffrn_reflns_theta_min 1.897 _exptl_absorpt_coefficient_mu 0.861 _exptl_absorpt_correction_T_max 0.7452 _exptl_absorpt_correction_T_min 0.4795 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS V2016/2 (Bruker, 2016)' _exptl_crystal_density_diffrn 1.203 _exptl_crystal_density_method 'not measured' _exptl_crystal_description prism _exptl_crystal_F_000 1004 _exptl_crystal_size_max 0.288 _exptl_crystal_size_mid 0.206 _exptl_crystal_size_min 0.121 _refine_diff_density_max 0.615 _refine_diff_density_min -0.672 _refine_diff_density_rms 0.066 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.042 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 331 _refine_ls_number_reflns 4841 _refine_ls_number_restraints 109 _refine_ls_restrained_S_all 1.048 _refine_ls_R_factor_all 0.0508 _refine_ls_R_factor_gt 0.0372 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0507P)^2^+2.0075P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0948 _refine_ls_wR_factor_ref 0.1031 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3963 _reflns_number_total 4841 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1sc03578a2.cif _cod_data_source_block P21n_a_CCDC1 _cod_original_cell_volume 2595.5(10) _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 1565132 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.790 _shelx_estimated_absorpt_t_max 0.903 _shelx_res_file ; TITL P21n_a.res in P2(1)/n P21n_a.res created by SHELXL-2017/1 at 13:14:40 on 08-May-2019 CELL 0.71073 15.7551 9.0514 18.5921 90.000 101.785 90.000 ZERR 4.0000 0.0037 0.0021 0.0043 0.000 0.003 0.000 LATT 1 SYMM 0.5-X, 0.5+Y, 0.5-Z SFAC C H CU N O UNIT 108 152 4 8 4 BOND $H FMAP 2 1 53 PLAN 20 SIZE 0.288 0.206 0.121 ACTA LIST 4 TEMP -173.000 SADI 0.01 O1 C24 O1 C24B SIMU 0.01 0.02 C24 > C27B OMIT -1 0 1 L.S. 10 WGHT 0.050700 2.007500 FVAR 0.31486 0.50841 CU1 3 0.508715 0.664202 0.711768 11.00000 0.01539 0.01788 = 0.01655 0.00004 0.00153 0.00062 O1 5 0.396984 0.618868 0.680160 11.00000 0.01629 0.02074 = 0.02517 -0.00083 0.00085 0.00171 N1 4 0.612988 0.680542 0.677657 11.00000 0.02016 0.01870 = 0.01745 0.00249 0.00221 0.00228 N2 4 0.558708 0.680804 0.813114 11.00000 0.01860 0.02184 = 0.01753 0.00006 0.00454 -0.00156 C1 1 0.691414 0.684986 0.720608 11.00000 0.01803 0.01787 = 0.02137 0.00158 0.00176 0.00337 C2 1 0.705392 0.678568 0.796964 11.00000 0.01517 0.02541 = 0.01973 0.00014 -0.00134 0.00116 AFIX 43 H2 2 0.764135 0.673180 0.822280 11.00000 -1.20000 AFIX 0 C3 1 0.643359 0.679136 0.840357 11.00000 0.02161 0.02041 = 0.01750 0.00051 0.00056 -0.00145 C4 1 0.769510 0.700456 0.686375 11.00000 0.01930 0.03890 = 0.02292 0.00236 0.00409 0.00155 AFIX 137 H4A 2 0.769104 0.621833 0.650067 11.00000 -1.50000 H4B 2 0.822307 0.692792 0.724603 11.00000 -1.50000 H4C 2 0.768047 0.796830 0.662131 11.00000 -1.50000 AFIX 0 C5 1 0.675191 0.677490 0.922492 11.00000 0.02498 0.04367 = 0.01963 0.00308 -0.00046 -0.00310 AFIX 137 H5A 2 0.664504 0.774053 0.942774 11.00000 -1.50000 H5B 2 0.737511 0.656409 0.933940 11.00000 -1.50000 H5C 2 0.644258 0.600939 0.944176 11.00000 -1.50000 AFIX 0 C6 1 0.604696 0.696466 0.599563 11.00000 0.01468 0.02017 = 0.01574 0.00293 0.00225 0.00094 C7 1 0.606099 0.572416 0.555634 11.00000 0.01646 0.01897 = 0.02043 0.00070 0.00206 0.00131 C8 1 0.598857 0.592200 0.480440 11.00000 0.02199 0.01751 = 0.02084 -0.00210 0.00400 0.00163 AFIX 43 H8 2 0.598971 0.508041 0.449928 11.00000 -1.20000 AFIX 0 C9 1 0.591454 0.732020 0.448779 11.00000 0.02032 0.02134 = 0.01992 0.00105 0.00407 -0.00009 C10 1 0.588997 0.853427 0.493966 11.00000 0.02000 0.01629 = 0.02014 0.00337 0.00156 0.00005 AFIX 43 H10 2 0.583136 0.949396 0.472843 11.00000 -1.20000 AFIX 0 C11 1 0.594870 0.838506 0.569235 11.00000 0.01472 0.01736 = 0.01915 -0.00077 0.00049 0.00008 C12 1 0.618372 0.420435 0.588688 11.00000 0.03225 0.01864 = 0.02761 0.00353 0.00409 0.00519 AFIX 137 H12A 2 0.605284 0.346297 0.549575 11.00000 -1.50000 H12B 2 0.579290 0.407090 0.622974 11.00000 -1.50000 H12C 2 0.678544 0.408821 0.615068 11.00000 -1.50000 AFIX 0 C13 1 0.588247 0.749716 0.367498 11.00000 0.04355 0.02543 = 0.02133 0.00209 0.01014 0.00267 AFIX 137 H13A 2 0.591087 0.652239 0.345168 11.00000 -1.50000 H13B 2 0.637551 0.809689 0.360120 11.00000 -1.50000 H13C 2 0.534024 0.798702 0.344462 11.00000 -1.50000 AFIX 0 C14 1 0.592616 0.970486 0.617876 11.00000 0.02867 0.01680 = 0.02283 -0.00137 0.00116 -0.00043 AFIX 137 H14A 2 0.542587 0.962814 0.641499 11.00000 -1.50000 H14B 2 0.587746 1.060791 0.588237 11.00000 -1.50000 H14C 2 0.646044 0.973900 0.655606 11.00000 -1.50000 AFIX 0 C15 1 0.500082 0.697307 0.862107 11.00000 0.01838 0.02673 = 0.01269 -0.00154 0.00069 0.00085 C16 1 0.483898 0.838498 0.886300 11.00000 0.02432 0.02647 = 0.02137 -0.00245 0.00359 -0.00245 C17 1 0.426703 0.852482 0.933625 11.00000 0.02680 0.03250 = 0.02258 -0.00715 0.00208 0.00462 AFIX 43 H17 2 0.416219 0.947664 0.951508 11.00000 -1.20000 AFIX 0 C18 1 0.384378 0.731105 0.955550 11.00000 0.01984 0.04785 = 0.01709 0.00149 0.00092 0.00232 C19 1 0.400729 0.593278 0.929074 11.00000 0.02083 0.03441 = 0.02068 0.00741 0.00226 -0.00416 AFIX 43 H19 2 0.371781 0.509592 0.943412 11.00000 -1.20000 AFIX 0 C20 1 0.457976 0.573449 0.882321 11.00000 0.02162 0.02493 = 0.01641 0.00300 -0.00125 -0.00137 C21 1 0.525846 0.972836 0.860834 11.00000 0.04253 0.02446 = 0.03997 -0.00666 0.01297 -0.00676 AFIX 137 H21A 2 0.588883 0.966374 0.877577 11.00000 -1.50000 H21B 2 0.504388 1.061830 0.881294 11.00000 -1.50000 H21C 2 0.511569 0.977736 0.807055 11.00000 -1.50000 AFIX 0 C22 1 0.323292 0.750233 1.007248 11.00000 0.02808 0.06148 = 0.03008 0.00285 0.01089 0.00720 AFIX 137 H22A 2 0.355482 0.740871 1.058036 11.00000 -1.50000 H22B 2 0.278171 0.674123 0.997326 11.00000 -1.50000 H22C 2 0.296382 0.848182 1.000098 11.00000 -1.50000 AFIX 0 C23 1 0.472595 0.423512 0.853385 11.00000 0.03342 0.02481 = 0.03380 0.00447 0.00944 -0.00307 AFIX 137 H23A 2 0.448904 0.348326 0.881725 11.00000 -1.50000 H23B 2 0.534930 0.406983 0.857872 11.00000 -1.50000 H23C 2 0.443534 0.416937 0.801590 11.00000 -1.50000 AFIX 0 PART 1 21 C24 1 0.321884 0.708645 0.665046 21.00000 0.01651 0.02279 = 0.02207 0.00159 0.00488 0.00693 C25 1 0.338575 0.838023 0.617728 21.00000 0.02906 0.03809 = 0.08337 0.02387 -0.00749 0.00286 AFIX 137 H25A 2 0.387832 0.895703 0.644149 21.00000 -1.50000 H25B 2 0.286922 0.900947 0.606802 21.00000 -1.50000 H25C 2 0.351736 0.800859 0.571717 21.00000 -1.50000 AFIX 0 C26 1 0.249664 0.616282 0.620402 21.00000 0.01734 0.03173 = 0.05263 -0.00963 -0.00532 -0.00469 AFIX 137 H26A 2 0.265925 0.585439 0.574523 21.00000 -1.50000 H26B 2 0.196322 0.674964 0.609121 21.00000 -1.50000 H26C 2 0.240042 0.528715 0.648691 21.00000 -1.50000 AFIX 0 C27 1 0.299855 0.759445 0.735266 21.00000 0.05082 0.07782 = 0.03872 -0.01616 -0.00479 0.04415 AFIX 137 H27A 2 0.292630 0.673538 0.765533 21.00000 -1.50000 H27B 2 0.245752 0.816164 0.724625 21.00000 -1.50000 H27C 2 0.346698 0.822033 0.761812 21.00000 -1.50000 AFIX 0 PART 2 -21 SAME 0.01 C24 > C27 C24B 1 0.321395 0.706860 0.673111 -21.00000 0.01671 0.02345 = 0.03048 -0.00094 -0.00355 -0.00240 C25B 1 0.343264 0.867551 0.661948 -21.00000 0.03624 0.02624 = 0.10174 0.01491 0.00783 0.00880 AFIX 137 H25D 2 0.378016 0.907089 0.707671 -21.00000 -1.50000 H25E 2 0.289564 0.924699 0.648184 -21.00000 -1.50000 H25F 2 0.376322 0.874555 0.622783 -21.00000 -1.50000 AFIX 0 C26B 1 0.258332 0.654856 0.605027 -21.00000 0.04221 0.07552 = 0.05080 -0.02167 -0.01079 0.02634 AFIX 137 H26D 2 0.283441 0.671616 0.561645 -21.00000 -1.50000 H26E 2 0.203943 0.710129 0.599928 -21.00000 -1.50000 H26F 2 0.246838 0.549199 0.609487 -21.00000 -1.50000 AFIX 0 C27B 1 0.282454 0.690415 0.739621 -21.00000 0.03561 0.06999 = 0.04348 0.01981 0.01588 0.02128 AFIX 137 H27D 2 0.268358 0.586331 0.745784 -21.00000 -1.50000 H27E 2 0.229478 0.749862 0.733533 -21.00000 -1.50000 H27F 2 0.324015 0.724276 0.783118 -21.00000 -1.50000 PART 0 AFIX 0 HKLF 4 REM P21n_a.res in P2(1)/n REM R1 = 0.0372 for 3963 Fo > 4sig(Fo) and 0.0508 for all 4841 data REM 331 parameters refined using 109 restraints END WGHT 0.0507 2.0074 REM Highest difference peak 0.615, deepest hole -0.672, 1-sigma level 0.066 Q1 1 0.4803 0.6922 0.7576 11.00000 0.05 0.62 Q2 1 0.5485 0.6378 0.6727 11.00000 0.05 0.51 Q3 1 0.5266 0.7229 0.6599 11.00000 0.05 0.51 Q4 1 0.5199 0.6896 0.8398 11.00000 0.05 0.38 Q5 1 0.4626 0.8375 0.9122 11.00000 0.05 0.37 Q6 1 0.4246 0.6946 0.7163 11.00000 0.05 0.36 Q7 1 0.4357 0.5876 0.9037 11.00000 0.05 0.34 Q8 1 0.6744 0.6808 0.8164 11.00000 0.05 0.33 Q9 1 0.2619 0.6141 0.7013 11.00000 0.05 0.31 Q10 1 0.4351 0.6040 0.7196 11.00000 0.05 0.31 Q11 1 0.4302 0.6556 0.6415 11.00000 0.05 0.31 Q12 1 0.3474 0.8601 0.7158 11.00000 0.05 0.30 Q13 1 0.3592 0.7357 0.9778 11.00000 0.05 0.30 Q14 1 0.6542 0.7066 0.6997 11.00000 0.05 0.28 Q15 1 0.3942 0.7877 0.9220 11.00000 0.05 0.28 Q16 1 0.2886 0.7502 0.5962 11.00000 0.05 0.28 Q17 1 0.4816 0.7700 0.8596 11.00000 0.05 0.27 Q18 1 0.3776 0.6710 0.9269 11.00000 0.05 0.27 Q19 1 0.4847 0.6356 0.8758 11.00000 0.05 0.26 Q20 1 0.6037 0.6843 0.6447 11.00000 0.05 0.26 ; _shelx_res_checksum 20189 _shelx_hkl_file ; 1 0 0 0.00 0.10 1 0 0 0.10 0.10 -1 0 0 0.00 0.10 -2 0 0 3101.49 199.48 2 0 0 2759.32 199.58 3 0 0 -1.10 1.20 -3 0 0 -0.10 0.90 3 0 0 -1.00 1.20 4 0 0 46.10 4.40 -4 0 0 62.49 4.30 4 0 0 51.69 4.60 5 0 0 -1.60 1.60 5 0 0 -0.50 1.70 -5 0 0 1.70 1.30 6 0 0 5.80 1.80 6 0 0 4.30 2.00 -6 0 0 5.70 1.50 7 0 0 0.10 1.90 -7 0 0 -0.80 1.40 7 0 0 1.10 2.10 8 0 0 732.83 54.99 -8 0 0 837.42 54.99 8 0 0 833.32 55.19 9 0 0 -1.50 2.40 -9 0 0 0.70 1.80 9 0 0 4.90 2.40 10 0 0 1934.61 139.99 10 0 0 2212.88 140.29 -10 0 0 2000.50 139.99 -11 0 0 4.30 2.20 11 0 0 -2.70 2.80 11 0 0 -1.70 3.00 12 0 0 490.45 35.80 12 0 0 543.95 36.10 -12 0 0 498.25 35.60 -13 0 0 -2.40 2.40 13 0 0 -2.10 3.40 13 0 0 -1.30 3.50 14 0 0 14.50 5.10 14 0 0 19.80 4.50 -14 0 0 17.00 3.40 15 0 0 -3.90 5.00 15 0 0 2.50 4.20 -15 0 0 1.30 3.30 16 0 0 11.00 5.10 -16 0 0 5.10 4.00 16 0 0 6.60 5.80 -17 0 0 -0.40 4.20 17 0 0 2.60 6.30 17 0 0 12.00 5.50 18 0 0 72.09 9.70 -18 0 0 72.19 7.90 18 0 0 84.39 9.50 0 -1 0 1.20 0.60 0 1 0 0.30 0.40 0 1 0 1.30 0.60 1 -1 0 1524.85 107.99 -1 -1 0 1755.02 107.99 1 -1 0 1502.15 107.99 -1 1 0 1537.35 107.99 -1 1 0 1467.45 107.99 1 1 0 1551.04 107.99 1 1 0 1764.72 107.99 2 -1 0 425.76 33.20 2 -1 0 458.35 33.30 2 1 0 508.25 33.20 2 1 0 467.65 33.30 -2 1 0 512.05 33.30 -2 1 0 546.65 33.30 -3 -1 0 0.90 0.80 3 -1 0 2.10 1.50 -3 -1 0 1.20 0.90 3 -1 0 1.20 1.40 -3 1 0 0.20 1.10 3 1 0 1.40 1.00 3 1 0 0.20 1.40 -4 -1 0 1116.39 69.59 -4 -1 0 869.51 69.49 4 -1 0 896.51 69.59 4 -1 0 1015.70 69.79 4 1 0 949.71 69.69 -4 1 0 1179.28 69.59 4 1 0 1115.79 69.59 5 -1 0 12.50 2.40 -5 -1 0 14.90 1.80 5 -1 0 15.20 2.20 5 1 0 12.70 2.00 5 1 0 12.00 2.20 -5 1 0 19.10 1.90 6 -1 0 0.60 1.80 -6 -1 0 0.30 1.30 6 -1 0 -1.60 1.90 6 1 0 1.60 1.80 6 1 0 1.30 1.70 -6 1 0 0.60 1.30 7 -1 0 136.39 11.20 7 -1 0 146.59 11.50 -7 -1 0 170.08 11.10 7 1 0 134.39 11.20 -7 1 0 157.88 11.10 7 1 0 172.58 11.30 8 -1 0 1.60 2.30 -8 -1 0 -0.30 1.60 8 -1 0 0.80 2.30 8 1 0 -1.90 2.10 -8 1 0 0.70 1.60 8 1 0 3.10 2.20 -9 -1 0 342.27 23.60 9 -1 0 341.17 24.00 9 -1 0 307.17 23.80 -9 1 0 340.67 23.60 9 1 0 398.76 24.00 9 1 0 299.47 23.80 -10 -1 0 12.10 2.50 10 -1 0 12.10 3.10 10 -1 0 14.80 3.40 -10 1 0 14.30 2.40 10 1 0 10.90 3.00 10 1 0 19.90 3.30 -11 -1 0 47.40 4.90 11 -1 0 60.69 6.00 -11 1 0 52.89 5.00 11 1 0 56.49 5.60 12 -1 0 189.88 15.40 12 -1 0 215.98 15.90 -12 -1 0 205.68 15.00 12 1 0 191.68 15.30 -12 1 0 190.88 15.00 12 1 0 233.58 15.60 13 -1 0 25.20 4.80 -13 -1 0 19.50 3.60 13 1 0 27.00 4.20 -13 1 0 20.00 3.40 13 1 0 25.10 4.40 14 -1 0 54.69 6.50 -14 -1 0 56.99 5.70 14 -1 0 72.99 7.40 14 1 0 55.79 6.70 14 1 0 50.69 6.30 -14 1 0 48.80 5.40 -15 -1 0 -0.70 3.50 15 -1 0 14.10 4.40 15 -1 0 0.20 5.40 15 1 0 3.30 4.10 -15 1 0 5.30 3.20 15 1 0 1.30 5.00 -16 -1 0 151.98 13.30 16 -1 0 155.78 15.20 16 -1 0 160.58 13.90 16 1 0 166.58 14.40 -16 1 0 152.18 13.10 16 1 0 164.68 14.70 -17 -1 0 41.40 6.30 17 -1 0 37.30 7.90 17 -1 0 60.19 7.60 -17 1 0 52.39 6.30 17 1 0 50.29 7.80 17 1 0 54.59 7.70 18 -1 0 -2.30 5.80 -18 -1 0 5.40 4.90 18 -1 0 -1.20 6.70 18 1 0 3.10 6.00 -18 1 0 -6.40 4.50 18 1 0 -11.90 6.40 0 -2 0 4601.94 311.07 0 2 0 4533.85 310.97 1 -2 0 213.68 16.30 1 -2 0 222.88 16.30 -1 -2 0 262.77 16.40 -1 2 0 208.78 16.20 1 2 0 256.17 16.30 1 2 0 217.48 16.20 -1 2 0 266.47 16.30 2 -2 0 162.38 11.50 2 -2 0 148.09 11.40 -2 -2 0 185.78 11.50 -2 2 0 168.28 11.40 2 2 0 149.09 11.40 2 2 0 175.78 11.50 -2 2 0 150.18 11.30 3 -2 0 15.30 1.80 -3 -2 0 20.40 2.00 3 -2 0 21.90 2.40 3 2 0 15.10 2.10 3 2 0 19.70 2.00 -3 2 0 20.30 2.00 -3 2 0 16.00 2.20 -4 -2 0 51.39 4.00 4 -2 0 44.40 3.80 4 -2 0 43.80 4.50 -4 2 0 48.10 4.00 4 2 0 55.79 4.10 -4 2 0 43.50 4.30 4 2 0 41.20 4.20 -5 -2 0 0.00 1.20 -5 -2 0 0.70 1.20 5 -2 0 1.70 2.00 -5 2 0 0.90 1.80 5 2 0 -0.70 1.70 -5 2 0 1.10 1.30 6 -2 0 300.77 21.70 -6 -2 0 321.37 21.40 -6 -2 0 302.07 21.20 6 2 0 305.27 21.50 6 2 0 324.87 21.20 -6 2 0 282.17 21.30 -7 -2 0 604.64 38.90 -7 -2 0 553.84 38.70 7 -2 0 566.84 39.20 7 -2 0 540.85 39.00 7 2 0 628.44 38.90 7 2 0 515.65 39.00 -7 2 0 539.15 38.90 8 -2 0 13.90 2.80 8 -2 0 15.30 3.00 -8 -2 0 9.80 2.10 8 2 0 13.30 2.70 8 2 0 7.30 2.10 -8 2 0 12.30 2.10 -9 -2 0 118.49 9.00 9 -2 0 124.39 9.40 9 -2 0 110.59 9.60 9 2 0 109.69 9.30 9 2 0 132.19 9.10 -9 2 0 108.09 8.90 -10 -2 0 249.18 18.80 10 -2 0 273.57 19.40 10 -2 0 286.27 19.10 10 2 0 277.57 18.90 10 2 0 248.28 19.00 -10 2 0 251.57 18.80 11 -2 0 74.19 7.10 -11 -2 0 70.59 6.40 11 -2 0 75.69 7.20 11 2 0 72.99 6.80 11 2 0 68.19 6.60 -11 2 0 64.59 6.30 12 -2 0 154.68 12.20 -12 -2 0 123.99 10.90 12 -2 0 172.28 11.70 12 2 0 143.19 11.30 -12 2 0 128.49 10.90 12 2 0 137.79 11.50 13 -2 0 17.80 4.80 -13 -2 0 14.20 3.20 13 -2 0 22.80 4.40 -13 2 0 16.50 3.20 13 2 0 15.60 3.90 13 2 0 21.80 4.30 14 -2 0 47.50 5.80 14 -2 0 39.70 6.30 -14 -2 0 31.80 4.50 14 2 0 39.40 5.30 -14 2 0 37.60 4.60 14 2 0 43.40 5.70 15 -2 0 105.39 10.90 -15 -2 0 109.79 10.30 15 -2 0 118.99 10.90 15 2 0 95.69 10.00 15 2 0 126.39 10.70 -15 2 0 116.19 10.00 16 -2 0 68.69 8.80 -16 -2 0 48.20 6.70 16 -2 0 73.49 7.90 -16 2 0 49.90 6.40 16 2 0 46.30 7.40 16 2 0 67.39 7.90 17 -2 0 132.49 11.30 -17 -2 0 90.09 9.90 17 -2 0 128.29 12.00 -17 2 0 99.39 9.80 17 2 0 96.09 10.80 17 2 0 129.19 11.50 -18 -2 0 28.40 6.00 18 -2 0 39.80 8.30 18 -2 0 33.90 7.30 -18 2 0 37.80 5.80 18 2 0 26.60 7.20 18 2 0 50.79 9.50 0 -3 0 0.50 1.60 0 3 0 -0.80 1.20 0 3 0 -0.60 1.60 1 -3 0 2820.52 201.98 -1 -3 0 3320.77 201.98 1 -3 0 2680.73 201.88 1 3 0 3290.17 201.98 -1 3 0 2834.02 201.88 1 3 0 2837.22 201.88 2 -3 0 82.89 7.20 2 -3 0 82.79 7.10 -2 -3 0 106.79 7.30 -2 3 0 90.39 6.90 -2 3 0 110.39 7.20 2 3 0 102.09 7.10 2 3 0 87.19 6.90 -3 -3 0 232.08 15.30 3 -3 0 209.38 15.20 3 -3 0 203.38 15.30 3 3 0 206.28 15.20 -3 3 0 204.98 15.10 3 3 0 231.48 15.20 -3 3 0 226.18 15.20 4 -3 0 152.08 11.60 -4 -3 0 177.88 11.80 4 -3 0 150.68 11.90 -4 3 0 175.88 11.80 -4 3 0 158.58 11.70 4 3 0 154.38 11.70 4 3 0 176.88 11.80 5 -3 0 701.43 51.29 -5 -3 0 794.02 51.39 5 -3 0 734.23 51.59 5 3 0 752.62 51.39 -5 3 0 773.72 51.39 5 3 0 753.32 51.39 -5 3 0 733.13 51.39 6 -3 0 45.80 4.60 -6 -3 0 50.39 4.30 6 -3 0 41.20 4.00 6 3 0 43.50 4.10 -6 3 0 46.50 4.30 6 3 0 49.70 4.70 -6 3 0 53.29 4.40 7 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112.59 9.90 -15 3 0 120.99 9.80 16 -3 0 -7.90 6.10 -16 -3 0 1.10 4.60 -16 3 0 -1.20 5.40 -16 3 0 0.00 3.80 16 3 0 -8.90 4.90 -17 -3 0 98.29 9.00 17 -3 0 76.79 10.00 17 3 0 77.99 9.20 -17 3 0 88.29 9.30 -17 3 0 71.79 8.00 18 -3 0 3.60 7.50 0 -4 0 756.12 55.99 0 4 0 908.81 55.99 0 4 0 783.42 55.99 1 -4 0 501.85 39.30 1 -4 0 558.64 39.50 -1 -4 0 618.44 39.60 1 4 0 541.75 39.40 1 4 0 622.74 39.50 -1 4 0 649.54 39.50 -1 4 0 524.35 39.40 -2 -4 0 359.36 22.70 2 -4 0 288.37 22.60 2 -4 0 292.07 22.50 -2 4 0 309.17 22.50 2 4 0 342.07 22.60 -2 4 0 369.96 22.60 2 4 0 309.37 22.50 -3 -4 0 201.68 13.30 3 -4 0 176.18 13.20 3 -4 0 173.08 13.20 -3 4 0 193.48 13.20 3 4 0 191.18 13.20 3 4 0 174.98 13.10 -3 4 0 177.98 13.10 4 -4 0 67.99 6.20 4 -4 0 73.89 6.50 -4 -4 0 82.99 6.50 -4 4 0 77.99 6.40 4 4 0 73.49 6.20 4 4 0 80.69 6.40 -4 4 0 79.19 6.10 -5 -4 0 78.09 5.90 5 -4 0 59.99 6.10 5 -4 0 59.99 5.60 -5 4 0 68.39 5.60 5 4 0 62.59 5.60 -5 4 0 68.99 5.90 5 4 0 70.69 5.90 -6 -4 0 5.00 2.10 6 -4 0 5.80 2.50 6 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29.00 4.70 15 4 0 21.60 6.20 -15 4 0 29.70 5.40 16 -4 0 4.40 6.60 -16 -4 0 1.80 4.60 16 4 0 4.90 5.50 -16 4 0 5.90 5.00 -16 4 0 1.20 3.90 -17 -4 0 44.00 6.80 17 -4 0 54.79 8.90 17 4 0 39.60 7.40 -17 4 0 41.70 6.30 -17 4 0 48.80 7.00 0 -5 0 3.90 2.10 0 5 0 3.20 1.70 0 5 0 0.00 1.90 -1 -5 0 43.10 4.30 1 -5 0 44.90 4.30 1 5 0 42.90 4.00 -1 5 0 49.00 4.70 -1 5 0 46.10 4.30 1 5 0 46.40 4.20 2 -5 0 35.90 3.60 2 -5 0 29.40 3.00 -2 -5 0 29.60 3.40 2 5 0 32.90 3.20 -2 5 0 32.30 3.40 2 5 0 32.50 3.40 -2 5 0 30.30 3.20 3 -5 0 -0.70 1.90 -3 -5 0 -0.30 2.00 3 -5 0 0.50 1.70 -3 5 0 1.40 2.10 -3 5 0 -1.20 1.60 3 5 0 -0.40 1.90 3 5 0 -1.30 1.70 -4 -5 0 40.00 4.00 4 -5 0 37.50 4.00 4 -5 0 33.60 3.90 4 5 0 48.60 4.00 -4 5 0 37.50 3.90 -4 5 0 42.00 3.90 4 5 0 42.10 4.00 5 -5 0 317.77 24.30 5 -5 0 333.97 24.50 -5 -5 0 387.56 24.50 5 5 0 377.66 24.50 -5 5 0 359.36 24.40 -5 5 0 320.27 24.30 5 5 0 340.37 24.40 6 -5 0 26.90 3.90 -6 -5 0 33.60 3.70 6 -5 0 27.50 3.40 6 5 0 26.10 3.60 -6 5 0 37.00 3.60 6 5 0 34.50 3.60 -6 5 0 36.60 3.70 7 -5 0 66.89 6.10 7 -5 0 68.89 6.70 -7 -5 0 81.89 6.60 7 5 0 79.19 6.70 -7 5 0 65.39 6.50 7 5 0 73.69 6.40 -7 5 0 66.39 6.30 8 -5 0 52.69 5.80 -8 -5 0 56.79 5.10 8 -5 0 42.40 4.60 -8 5 0 56.79 5.20 8 5 0 59.19 5.50 -8 5 0 56.19 5.10 8 5 0 57.69 5.10 9 -5 0 1.10 1.80 9 -5 0 -1.80 3.50 -9 -5 0 -1.60 2.50 -9 -5 0 1.60 2.50 -9 5 0 4.00 2.70 -9 5 0 -2.30 2.40 9 5 0 2.40 3.00 10 -5 0 28.60 3.70 -10 -5 0 48.90 4.80 -10 -5 0 39.90 4.30 10 -5 0 43.60 5.80 -10 5 0 41.70 4.50 -10 5 0 35.60 4.50 10 5 0 39.50 4.90 11 -5 0 34.80 5.70 -11 -5 0 35.80 4.80 -11 -5 0 33.00 4.20 -11 5 0 38.80 4.50 11 5 0 42.40 5.40 -11 5 0 37.90 4.90 -12 -5 0 44.40 5.70 -12 -5 0 48.00 4.90 12 -5 0 40.50 6.40 12 5 0 46.80 6.30 -12 5 0 50.89 5.30 -12 5 0 48.40 5.60 13 -5 0 15.60 5.90 -13 -5 0 16.80 4.70 -13 5 0 26.90 4.90 -13 5 0 21.00 3.90 13 5 0 16.20 5.40 14 -5 0 -0.40 6.10 -14 -5 0 -5.20 4.40 -14 5 0 -2.10 3.60 -14 5 0 7.20 4.50 14 5 0 0.90 5.30 15 -5 0 145.89 13.20 -15 -5 0 135.29 12.70 -15 5 0 137.89 12.10 15 5 0 113.79 12.00 -15 5 0 140.99 12.50 16 -5 0 9.00 7.30 -16 -5 0 18.40 5.70 -16 5 0 17.10 4.80 -16 5 0 20.70 5.70 16 5 0 17.60 6.50 0 -6 0 744.53 51.79 0 6 0 731.73 51.59 0 6 0 769.42 51.59 -1 -6 0 50.49 4.90 1 -6 0 41.40 4.70 1 6 0 47.80 4.40 1 6 0 54.59 4.60 -1 6 0 44.50 4.60 -1 6 0 44.20 4.40 2 -6 0 234.58 17.50 2 -6 0 238.58 18.00 -2 -6 0 285.47 18.10 -2 6 0 243.88 17.70 2 6 0 259.67 17.80 2 6 0 243.88 17.80 -2 6 0 241.38 17.70 -3 -6 0 12.80 2.80 3 -6 0 7.20 2.20 3 -6 0 5.10 2.50 3 6 0 6.20 2.40 3 6 0 8.60 2.30 -3 6 0 5.70 2.20 -3 6 0 0.80 2.40 -4 -6 0 602.94 38.50 4 -6 0 520.75 38.30 4 -6 0 513.55 38.40 -4 6 0 529.85 38.30 4 6 0 556.34 38.30 4 6 0 560.04 38.30 -4 6 0 584.24 38.40 5 -6 0 -1.90 2.50 5 -6 0 -2.90 2.30 -5 -6 0 3.30 2.60 -5 6 0 0.80 2.20 5 6 0 0.10 2.60 -5 6 0 -2.40 2.30 5 6 0 -2.20 2.10 6 -6 0 474.65 33.60 6 -6 0 440.86 33.30 -6 -6 0 517.25 33.40 6 6 0 495.15 33.40 6 6 0 487.95 33.40 -6 6 0 414.06 33.20 -6 6 0 513.65 33.40 7 -6 0 90.69 8.60 -7 -6 0 117.79 9.00 7 -6 0 111.59 9.60 7 6 0 111.79 8.90 -7 6 0 93.89 8.90 -7 6 0 109.39 8.80 7 6 0 113.29 9.10 8 -6 0 131.19 11.30 8 -6 0 118.89 10.20 -8 -6 0 136.99 10.60 8 6 0 125.59 10.80 -8 6 0 138.49 10.40 8 6 0 150.98 10.80 -8 6 0 120.69 10.50 -9 -6 0 11.40 3.40 9 -6 0 12.10 2.60 -9 -6 0 12.10 3.70 9 -6 0 10.50 4.10 -9 6 0 11.20 3.20 9 6 0 18.00 4.20 -9 6 0 14.90 3.30 9 6 0 8.60 3.10 -10 -6 0 121.09 9.70 10 -6 0 101.99 9.50 -10 -6 0 114.89 10.20 10 -6 0 112.99 10.80 -10 6 0 121.99 9.60 10 6 0 116.99 10.70 -10 6 0 99.29 9.80 -11 -6 0 -0.30 4.20 11 -6 0 -3.50 4.30 -11 -6 0 2.20 3.10 -11 6 0 -1.20 3.00 -11 6 0 6.20 3.70 11 6 0 6.70 4.80 12 -6 0 160.18 14.70 -12 -6 0 164.28 12.70 -12 -6 0 153.98 13.70 -12 6 0 176.18 13.00 12 6 0 163.38 14.20 -12 6 0 145.69 13.40 -13 -6 0 11.50 4.90 13 -6 0 -0.20 5.90 -13 6 0 5.90 4.30 -13 6 0 8.00 4.10 13 6 0 2.10 5.60 14 -6 0 210.18 18.70 -14 -6 0 197.18 17.00 14 6 0 180.58 17.30 -14 6 0 220.78 16.60 -14 6 0 234.78 19.60 -15 -6 0 9.90 5.50 15 -6 0 5.60 7.10 15 6 0 -0.30 5.90 -15 6 0 1.90 4.40 0 -7 0 2.00 2.80 0 7 0 -1.20 2.50 0 7 0 0.60 2.30 -1 -7 0 98.99 8.20 1 -7 0 92.19 8.20 1 7 0 78.59 7.50 -1 7 0 76.79 7.40 -1 7 0 86.39 7.60 1 7 0 78.19 7.50 2 -7 0 294.57 22.10 -2 -7 0 350.96 22.20 -2 7 0 287.87 21.80 2 7 0 298.57 21.80 -2 7 0 307.87 21.80 2 7 0 300.87 21.80 3 -7 0 95.29 8.50 3 -7 0 112.19 9.50 -3 -7 0 135.89 9.40 -3 7 0 96.49 9.00 -3 7 0 120.79 8.90 3 7 0 113.69 9.10 3 7 0 98.19 8.80 4 -7 0 8.30 3.20 -4 -7 0 8.10 3.30 4 -7 0 7.20 2.60 -4 7 0 8.80 3.10 -4 7 0 10.80 2.90 4 7 0 7.40 3.00 4 7 0 9.30 2.80 5 -7 0 181.58 15.60 5 -7 0 197.08 15.90 -5 -7 0 228.88 15.90 5 7 0 221.18 15.80 5 7 0 235.08 16.00 -5 7 0 199.78 15.70 -5 7 0 224.38 15.80 6 -7 0 -3.90 2.80 -6 -7 0 1.30 3.10 6 -7 0 -2.70 3.00 -6 7 0 4.40 3.20 6 7 0 2.20 3.50 -6 7 0 7.40 2.90 6 7 0 0.90 2.70 -7 -7 0 82.09 7.50 7 -7 0 63.09 6.90 7 -7 0 69.79 6.70 -7 7 0 78.49 7.10 7 7 0 64.39 7.10 -7 7 0 70.69 6.60 7 7 0 78.69 6.80 8 -7 0 -1.00 3.10 -8 -7 0 6.80 3.40 8 -7 0 0.50 3.60 -8 7 0 4.00 3.60 -8 7 0 1.00 2.90 8 7 0 6.40 4.30 8 7 0 4.80 3.00 9 -7 0 8.00 4.20 9 -7 0 2.00 3.20 -9 -7 0 7.80 3.60 9 7 0 3.90 4.60 -9 7 0 6.40 3.70 -9 7 0 12.20 3.50 9 7 0 13.30 3.70 10 -7 0 31.60 5.50 -10 -7 0 25.10 5.60 -10 -7 0 28.10 4.70 -10 7 0 31.90 4.80 -10 7 0 35.60 4.60 10 7 0 27.40 5.90 11 -7 0 5.20 5.10 -11 -7 0 -2.50 5.00 -11 -7 0 -1.20 3.40 11 7 0 -2.70 5.20 -11 7 0 2.90 4.30 -11 7 0 -0.70 3.50 -12 -7 0 125.39 10.80 -12 -7 0 126.89 10.50 12 -7 0 116.99 11.50 -12 7 0 129.59 10.90 12 7 0 80.79 10.50 13 -7 0 57.49 8.50 -13 -7 0 53.69 7.50 -13 7 0 57.39 6.60 13 7 0 36.90 7.30 -14 -7 0 4.70 5.60 14 -7 0 -8.70 6.70 -14 7 0 0.50 4.60 14 7 0 4.60 6.00 0 -8 0 284.37 19.80 0 8 0 260.87 19.30 0 8 0 252.77 19.30 -1 -8 0 9.00 3.60 1 -8 0 11.30 3.90 -1 8 0 -5.50 3.40 1 8 0 3.10 3.50 -1 8 0 -1.60 2.70 1 8 0 -0.40 2.80 2 -8 0 47.70 5.40 -2 -8 0 29.20 4.60 2 8 0 32.30 4.20 -2 8 0 30.90 4.20 -2 8 0 26.90 4.50 2 8 0 28.00 4.70 3 -8 0 -3.60 2.30 3 -8 0 0.50 3.90 -3 -8 0 4.20 3.40 3 8 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481.65 35.60 5 -7 -4 112.89 9.60 5 -7 -4 93.39 8.90 -5 -7 4 106.19 9.40 5 7 -4 101.39 9.60 5 7 -4 110.59 9.00 -5 7 4 109.49 8.90 4 -7 -4 125.99 11.00 4 -7 -4 122.99 10.50 -4 -7 4 150.38 11.10 4 7 -4 136.59 10.60 4 7 -4 134.49 11.10 -4 7 4 133.09 10.50 -3 -7 4 12.40 3.60 3 -7 -4 2.40 2.50 3 -7 -4 5.50 3.00 3 7 -4 3.40 3.40 3 7 -4 10.80 2.80 -3 7 4 8.10 2.50 -2 -7 4 5.10 3.30 2 -7 -4 6.30 3.10 2 7 -4 -0.10 2.40 -2 7 4 0.50 2.30 2 7 -4 9.20 3.50 -1 -7 4 52.39 5.80 1 -7 -4 53.19 5.50 1 7 -4 52.69 5.00 1 7 -4 47.20 5.60 -1 7 4 63.59 5.40 0 -7 4 6.60 3.20 0 -7 -4 0.40 2.70 0 7 -4 6.30 2.40 0 7 4 3.10 2.20 0 7 -4 0.90 3.30 0 7 4 3.40 2.30 -1 -7 -4 247.68 17.00 1 -7 4 228.08 17.20 -1 7 -4 233.38 16.50 1 7 4 238.38 16.70 1 7 4 228.98 16.40 -1 7 -4 193.48 17.00 -2 -7 -4 69.09 6.50 2 -7 4 74.09 6.80 2 -7 4 67.49 6.60 -2 7 -4 69.39 6.70 2 7 4 64.29 6.40 2 7 4 76.39 6.60 -2 7 -4 69.29 6.30 3 -7 4 229.88 16.80 -3 -7 -4 234.98 16.60 3 -7 4 201.38 16.30 3 7 4 221.78 16.20 -3 7 -4 231.58 16.10 3 7 4 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3.10 6 8 -4 -0.90 3.00 5 -8 -4 223.08 17.50 -5 -8 4 227.68 17.90 5 -8 -4 248.68 18.50 5 8 -4 245.08 17.60 5 8 -4 235.98 18.50 -5 8 4 238.38 17.60 4 -8 -4 8.60 3.20 -4 -8 4 16.40 4.50 4 -8 -4 12.50 4.50 -4 8 4 14.50 3.20 4 8 -4 16.10 5.00 4 8 -4 12.80 3.40 -3 -8 4 96.49 9.10 3 -8 -4 87.59 8.30 3 -8 -4 104.39 9.10 3 8 -4 96.19 9.10 3 8 -4 112.39 8.90 -3 8 4 105.69 8.80 -2 -8 4 -3.40 3.60 2 -8 -4 -0.90 3.60 2 8 -4 -1.50 2.60 -2 8 4 -4.40 2.50 2 8 -4 0.60 4.40 1 -8 -4 21.00 4.50 -1 -8 4 18.70 4.80 1 8 -4 15.10 3.20 1 8 -4 14.70 4.80 -1 8 4 22.10 3.60 -1 8 4 18.60 3.30 0 -8 4 0.70 4.10 0 -8 -4 1.70 3.40 0 8 -4 2.70 2.50 0 8 -4 5.90 4.40 0 8 4 1.20 2.90 0 8 4 3.00 2.80 1 -8 4 83.09 8.00 -1 -8 -4 70.69 7.00 -1 8 -4 62.79 7.40 1 8 4 73.99 6.70 1 8 4 76.09 6.60 -1 8 -4 65.59 6.30 2 -8 4 6.00 4.50 -2 -8 -4 7.10 3.30 -2 8 -4 3.80 2.70 2 8 4 5.80 2.90 2 8 4 -0.50 3.10 -2 8 -4 -0.70 4.30 -3 -8 -4 156.88 12.60 3 -8 4 145.39 12.20 3 -8 4 167.68 13.60 -3 8 -4 138.39 13.40 3 8 4 158.88 12.30 3 8 4 166.78 12.50 -3 8 -4 164.78 12.10 4 -8 4 14.80 5.00 -4 -8 -4 16.80 3.70 4 -8 4 13.70 3.40 4 8 4 10.10 3.50 -4 8 -4 15.60 3.20 -4 8 -4 10.70 4.90 4 8 4 7.80 3.90 -5 -8 -4 63.39 6.50 5 -8 4 72.29 7.40 5 -8 4 56.29 6.30 5 8 4 66.39 6.60 -5 8 -4 63.89 7.60 5 8 4 67.89 6.70 -5 8 -4 61.59 6.00 -6 -8 -4 -9.20 3.10 6 -8 4 1.10 3.40 6 -8 4 -0.90 4.50 -6 8 -4 3.40 3.00 6 8 4 -2.30 3.70 -6 8 -4 -2.80 5.30 6 8 4 3.70 4.50 -7 -8 -4 38.70 5.20 7 -8 4 50.49 6.00 7 -8 4 47.40 5.90 -7 8 -4 43.00 4.90 7 8 4 41.40 5.60 -7 8 -4 33.40 6.60 7 8 4 36.00 6.10 8 -8 4 3.00 4.40 8 -8 4 8.80 4.60 -8 -8 -4 0.70 3.90 8 8 4 5.20 5.20 -8 8 -4 6.70 3.30 8 8 4 8.80 4.50 -8 8 -4 13.30 5.70 -9 -8 -4 19.30 4.50 9 -8 4 30.10 6.00 9 8 4 25.20 5.20 -9 8 -4 16.50 6.40 -9 8 -4 19.70 4.10 9 8 4 10.20 5.50 10 -8 4 5.00 6.10 -10 -8 -4 3.30 4.20 -10 8 -4 7.30 3.90 10 8 4 6.30 4.80 10 8 4 11.50 5.90 -10 8 -4 11.60 6.20 11 -8 4 -4.10 6.20 -11 -8 -4 -1.50 4.30 -11 -8 -4 7.00 5.70 11 8 4 -0.10 5.60 -11 8 -4 6.10 4.10 -11 8 -4 -5.80 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12.10 4.20 -11 -5 7 14.10 3.60 11 -5 -7 12.60 3.20 -11 -5 7 14.10 3.10 -11 5 7 13.10 3.20 11 5 -7 7.50 4.00 -10 -5 7 52.59 5.20 -10 -5 7 47.40 5.00 10 5 -7 41.00 5.70 -10 5 7 50.39 5.00 -9 -5 7 11.80 2.70 9 -5 -7 15.00 3.10 -9 -5 7 10.20 3.00 9 -5 -7 16.00 3.80 9 5 -7 14.90 4.10 -9 5 7 15.40 2.90 -8 -5 7 159.68 13.40 -8 -5 7 165.88 13.10 8 -5 -7 211.68 14.00 8 -5 -7 200.58 13.50 8 5 -7 163.38 13.80 -8 5 7 175.98 13.30 7 -5 -7 1.50 2.40 -7 -5 7 3.20 2.00 7 -5 -7 2.10 2.90 -7 -5 7 0.90 2.40 7 5 -7 3.50 3.20 -7 5 7 6.70 2.20 6 -5 -7 59.09 5.70 -6 -5 7 52.39 5.50 -6 -5 7 56.79 5.30 6 -5 -7 70.29 5.70 6 5 -7 58.59 5.90 -6 5 7 64.59 5.70 -5 -5 7 2.30 1.60 -5 -5 7 -0.60 2.20 5 -5 -7 3.60 2.50 5 5 -7 -2.30 2.80 -5 5 7 -1.20 1.80 4 -5 -7 1.30 2.30 -4 -5 7 1.40 2.40 4 5 -7 -3.90 2.70 4 5 -7 1.00 1.70 -4 5 7 -1.90 1.70 3 -5 -7 37.10 4.40 3 -5 -7 47.80 4.30 -3 -5 7 43.30 4.60 3 5 -7 42.80 4.80 -3 5 7 44.10 4.10 3 5 -7 41.70 4.00 -2 -5 7 12.90 2.90 2 -5 -7 15.20 2.60 2 -5 -7 12.90 2.70 2 5 -7 13.30 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188.08 14.10 5 -6 -7 182.18 14.10 5 -6 -7 185.08 14.10 -5 6 7 185.88 13.80 5 6 -7 191.18 13.60 5 6 -7 175.68 14.20 4 -6 -7 -2.30 2.50 -4 -6 7 1.50 2.60 4 -6 -7 -3.10 2.50 -4 6 7 1.30 2.10 4 6 -7 -2.90 3.00 4 6 -7 -0.90 2.00 3 -6 -7 180.78 14.70 3 -6 -7 210.38 14.60 -3 -6 7 193.28 14.70 3 6 -7 206.48 14.20 3 6 -7 183.18 14.80 -3 6 7 194.58 14.30 2 -6 -7 -0.20 2.20 -2 -6 7 1.90 2.70 2 -6 -7 1.80 2.40 -2 6 7 -1.80 1.90 2 6 -7 -1.90 1.80 2 6 -7 -2.50 3.10 -1 -6 7 116.49 9.80 1 -6 -7 126.09 10.20 -1 -6 7 141.09 10.40 1 -6 -7 134.09 9.80 1 6 -7 131.49 9.50 -1 6 7 134.09 9.80 1 6 -7 100.39 10.40 0 -6 7 14.30 3.50 0 -6 -7 12.50 2.40 0 -6 7 8.70 2.70 0 -6 -7 8.00 2.90 0 6 -7 13.20 2.20 0 6 7 9.90 2.50 0 6 -7 9.90 3.70 -1 -6 -7 477.65 33.40 1 -6 7 469.45 33.50 1 -6 7 476.75 33.60 -1 6 -7 470.95 33.00 1 6 7 482.45 33.10 -1 6 -7 439.56 33.70 1 6 7 522.15 33.40 -2 -6 -7 72.89 6.60 2 -6 7 62.99 6.40 2 -6 7 68.99 6.40 -2 6 -7 60.29 5.70 2 6 7 67.29 6.40 2 6 7 75.19 6.30 -2 6 -7 61.49 6.90 -3 -6 -7 508.95 35.40 3 -6 7 486.35 35.60 3 -6 7 529.95 35.70 3 6 7 541.15 35.40 -3 6 -7 483.15 35.90 -3 6 -7 456.15 35.00 3 6 7 547.15 35.40 4 -6 7 5.00 3.10 -4 -6 -7 2.90 2.70 4 -6 7 0.80 3.10 -4 6 -7 -0.60 1.90 -4 6 -7 0.70 4.50 4 6 7 -4.50 2.70 4 6 7 -2.80 2.20 5 -6 7 146.79 13.00 5 -6 7 156.18 12.90 -5 -6 -7 168.28 12.70 -5 6 -7 160.68 14.10 -5 6 -7 143.89 11.90 5 6 7 184.48 12.80 5 6 7 193.18 12.90 6 -6 7 11.80 3.80 6 -6 7 2.70 3.80 -6 -6 -7 16.30 3.40 -6 6 -7 10.80 2.50 6 6 7 23.10 4.30 6 6 7 10.80 3.40 -6 6 -7 19.10 5.80 7 -6 7 156.98 13.90 7 -6 7 171.48 13.40 -7 -6 -7 165.68 13.00 7 6 7 196.18 13.40 7 6 7 187.38 13.80 -7 6 -7 173.08 15.00 -7 6 -7 140.79 12.30 8 -6 7 -3.90 3.50 -8 -6 -7 3.30 3.20 8 -6 7 -0.80 4.30 -8 6 -7 2.20 3.60 8 6 7 1.50 4.60 8 6 7 2.10 3.70 -8 6 -7 2.70 5.80 9 -6 7 374.86 27.00 -9 -6 -7 351.56 25.60 9 6 7 362.76 26.50 9 6 7 360.46 26.20 -9 6 -7 339.97 27.30 10 -6 7 8.90 6.20 -10 -6 -7 -0.70 3.30 -10 -6 -7 -2.70 4.60 -10 6 -7 6.80 6.70 10 6 7 0.90 5.20 11 -6 7 198.68 18.80 -11 -6 -7 225.88 16.80 11 6 7 187.08 17.10 -11 6 -7 201.38 18.30 12 -6 7 -2.90 7.40 -12 -6 -7 4.30 5.20 12 6 7 -3.80 5.70 -12 6 -7 2.90 6.90 -13 -6 -7 76.79 8.30 13 -6 7 70.69 10.80 -13 6 -7 70.49 9.60 13 6 7 60.99 8.80 14 -7 -7 6.10 6.40 -14 -7 7 22.90 5.80 -14 -7 7 17.60 4.70 14 7 -7 21.90 7.10 -14 7 7 20.40 5.10 -13 -7 7 38.20 6.50 -13 -7 7 45.30 5.90 13 -7 -7 35.90 7.20 13 7 -7 35.70 7.80 -13 7 7 44.00 5.90 -12 -7 7 47.50 6.10 12 -7 -7 46.50 7.20 -12 -7 7 47.10 6.50 12 7 -7 42.90 7.50 -12 7 7 41.80 5.90 -11 -7 7 9.50 4.20 11 -7 -7 11.60 4.30 -11 -7 7 14.50 4.70 11 -7 -7 15.60 5.30 11 7 -7 19.10 6.30 -11 7 7 15.50 4.40 -10 -7 7 27.30 4.90 10 -7 -7 32.70 5.10 10 -7 -7 26.20 5.40 -10 -7 7 31.00 5.20 -10 7 7 36.90 5.10 10 7 -7 35.00 6.60 9 -7 -7 12.60 4.30 -9 -7 7 -1.90 3.60 -9 -7 7 5.60 3.80 9 -7 -7 7.20 3.90 -9 7 7 -1.30 3.50 9 7 -7 -0.20 5.40 -8 -7 7 28.40 4.90 8 -7 -7 29.30 5.00 8 -7 -7 25.80 4.60 -8 -7 7 23.70 4.50 8 7 -7 31.30 5.80 -8 7 7 34.20 4.70 -7 -7 7 26.80 4.40 7 -7 -7 25.60 4.40 -7 -7 7 26.70 4.20 7 -7 -7 24.20 4.80 -7 7 7 35.90 4.30 7 7 -7 20.00 5.10 6 -7 -7 65.19 6.40 6 -7 -7 61.79 6.00 -6 -7 7 38.00 5.70 6 7 -7 59.19 5.50 -6 7 7 62.09 5.80 6 7 -7 51.09 6.40 5 -7 -7 17.00 3.40 5 -7 -7 12.60 3.90 -5 -7 7 7.90 3.40 5 7 -7 15.00 3.10 5 7 -7 9.90 4.20 -5 7 7 15.20 3.10 4 -7 -7 44.30 5.60 4 -7 -7 46.00 5.10 -4 -7 7 51.89 5.60 -4 7 7 50.29 5.00 4 7 -7 42.30 5.80 4 7 -7 49.50 4.80 3 -7 -7 23.10 4.10 -3 -7 7 22.50 4.10 3 -7 -7 25.10 3.70 -3 7 7 29.20 3.70 3 7 -7 14.90 4.50 3 7 -7 29.30 3.50 2 -7 -7 17.00 3.50 -2 -7 7 15.50 3.70 2 -7 -7 12.30 3.00 -2 7 7 15.20 3.00 2 7 -7 11.90 2.80 2 7 -7 8.70 4.10 1 -7 -7 7.90 3.00 -1 -7 7 3.90 3.50 1 -7 -7 3.00 2.50 1 7 -7 5.30 4.20 1 7 -7 6.90 2.40 -1 7 7 5.40 2.50 0 -7 7 38.40 5.10 0 -7 -7 35.80 4.40 0 -7 7 34.90 4.10 0 7 -7 24.40 5.20 0 7 7 37.40 4.20 0 7 -7 35.00 3.70 1 -7 7 8.60 3.90 -1 -7 -7 -0.30 3.00 1 -7 7 3.40 2.90 -1 7 -7 6.40 4.50 -1 7 -7 7.40 2.30 1 7 7 3.60 2.60 1 7 7 3.80 2.60 2 -7 7 105.89 9.80 2 -7 7 99.79 9.10 -2 -7 -7 105.29 9.00 -2 7 -7 86.49 7.80 -2 7 -7 86.79 9.30 2 7 7 107.19 8.60 2 7 7 102.59 8.50 3 -7 7 13.50 4.40 -3 -7 -7 5.80 3.20 -3 7 -7 7.20 5.30 3 7 7 8.60 3.30 3 7 7 10.00 3.00 -3 7 -7 9.90 2.50 4 -7 7 8.80 4.40 -4 -7 -7 8.30 3.30 4 -7 7 6.40 3.40 -4 7 -7 7.20 5.70 4 7 7 7.30 3.20 -4 7 -7 8.60 2.60 4 7 7 12.10 3.90 -5 -7 -7 -0.90 3.20 5 -7 7 11.30 3.60 5 7 7 -2.50 3.90 -5 7 -7 0.40 5.90 5 7 7 0.80 3.50 6 -7 7 9.70 4.00 6 -7 7 23.30 4.80 -6 -7 -7 15.00 3.80 6 7 7 16.50 4.40 -6 7 -7 11.60 6.70 6 7 7 22.60 4.80 -7 -7 -7 21.40 4.20 7 -7 7 27.40 5.10 7 -7 7 30.90 5.20 7 7 7 22.80 4.70 7 7 7 27.20 5.50 -7 7 -7 11.10 6.80 8 -7 7 -2.80 4.70 -8 -7 -7 -0.40 3.40 8 -7 7 2.70 4.40 8 7 7 -0.70 4.30 -8 7 -7 -4.10 6.60 8 7 7 3.40 4.80 -9 -7 -7 51.59 5.90 9 -7 7 58.39 7.90 -9 7 -7 54.99 8.60 9 7 7 48.50 6.60 9 7 7 50.09 7.10 10 -7 7 3.90 6.60 -10 -7 -7 2.00 3.80 10 7 7 1.60 5.30 -10 7 -7 14.50 7.30 10 7 7 10.70 4.80 -11 -7 -7 59.09 7.40 11 -7 7 50.49 9.00 11 7 7 45.90 7.70 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11.10 2.70 -9 3 -9 13.40 4.80 9 3 9 9.90 5.10 -9 3 -9 16.30 2.70 9 3 9 11.60 3.80 -10 -3 -9 117.99 9.70 10 -3 9 118.39 11.80 10 3 9 125.49 11.90 -10 3 -9 111.19 9.20 -10 3 -9 114.49 10.70 10 3 9 110.09 10.40 11 -3 9 1.40 5.60 -11 -3 -9 3.50 3.20 11 3 9 0.80 4.20 -11 3 -9 10.10 5.90 -11 3 -9 4.20 3.80 11 3 9 1.10 5.80 -12 -3 -9 130.49 11.20 12 -3 9 144.69 13.30 12 3 9 125.79 12.00 -12 3 -9 131.39 12.70 12 3 9 137.39 12.90 13 -3 9 3.70 7.20 -13 -3 -9 0.80 4.00 13 3 9 2.70 6.80 -13 3 -9 9.10 7.00 13 3 9 2.40 4.80 14 -3 9 36.00 8.60 -14 -3 -9 15.10 4.80 14 3 9 13.00 7.50 14 3 9 17.00 6.30 -14 3 -9 27.20 8.10 17 -4 -9 4.40 6.60 -17 -4 9 -6.00 4.70 -17 4 9 3.90 4.20 17 4 -9 -6.00 5.40 -16 -4 9 138.29 11.80 16 -4 -9 110.79 11.70 16 4 -9 123.59 11.80 -16 4 9 120.19 11.40 -15 -4 9 -3.80 4.00 15 -4 -9 -1.00 5.80 15 4 -9 0.60 5.20 -15 4 9 5.20 3.80 -14 -4 9 65.99 7.10 14 -4 -9 66.59 8.60 -14 -4 9 72.09 6.80 14 4 -9 79.59 8.00 -14 4 9 60.29 6.90 13 -4 -9 3.70 5.30 -13 -4 9 22.30 4.10 -13 -4 9 12.20 3.10 13 4 -9 14.40 4.40 -13 4 9 8.50 3.70 -13 4 9 12.20 3.00 -12 -4 9 60.09 5.90 -12 -4 9 62.49 5.60 12 -4 -9 56.29 7.00 -12 4 9 51.69 5.70 12 4 -9 53.09 6.40 -12 4 9 55.79 5.20 11 -4 -9 26.20 4.90 -11 -4 9 23.80 3.80 -11 -4 9 27.10 3.70 -11 4 9 30.70 3.40 -11 4 9 26.40 3.90 11 4 -9 35.80 4.90 11 4 -9 22.00 3.80 10 -4 -9 9.20 3.70 -10 -4 9 5.70 2.60 -10 -4 9 4.50 2.30 -10 4 9 4.00 2.20 10 4 -9 1.60 3.70 10 4 -9 1.40 2.40 -10 4 9 4.10 2.50 -9 -4 9 22.90 2.90 -9 -4 9 16.40 3.20 9 -4 -9 21.00 4.00 9 4 -9 24.20 4.20 9 4 -9 24.40 3.20 -9 4 9 26.50 3.20 -9 4 9 24.70 3.40 -8 -4 9 26.60 3.60 8 -4 -9 28.80 4.30 -8 -4 9 25.00 3.10 -8 4 9 32.00 3.60 8 4 -9 35.30 3.50 -8 4 9 34.40 3.60 8 4 -9 27.70 4.30 7 -4 -9 7.30 3.10 -7 -4 9 11.70 2.70 -7 -4 9 5.00 1.80 7 4 -9 7.60 2.10 -7 4 9 6.20 2.30 7 4 -9 7.60 3.20 -7 4 9 7.30 2.10 6 -4 -9 53.09 5.50 -6 -4 9 52.39 4.80 -6 -4 9 62.59 5.70 -6 4 9 57.99 5.50 6 4 -9 56.99 5.60 6 4 -9 52.09 5.20 -6 4 9 69.69 5.30 -5 -4 9 79.59 6.40 5 -4 -9 85.89 7.70 -5 -4 9 83.09 7.20 -5 4 9 92.99 7.10 5 4 -9 89.89 7.60 -5 4 9 85.79 6.90 5 4 -9 79.39 6.80 -4 -4 9 35.20 3.10 4 -4 -9 44.50 4.20 -4 -4 9 40.10 4.00 4 4 -9 25.30 3.40 4 4 -9 34.20 4.20 -4 4 9 39.00 3.80 -4 4 9 36.00 3.50 -3 -4 9 59.29 5.10 -3 -4 9 71.99 6.00 -3 -4 9 75.69 6.20 3 -4 -9 80.09 6.40 3 4 -9 69.29 6.20 -3 4 9 73.29 6.10 -3 4 9 64.79 5.80 -2 -4 9 66.69 5.90 2 -4 -9 95.49 7.20 -2 -4 9 89.39 7.00 -2 -4 9 90.29 7.10 -2 4 9 93.69 7.00 -2 4 9 85.69 6.60 2 4 -9 85.49 7.50 -1 -4 9 71.49 6.60 -1 -4 9 75.49 6.60 1 -4 -9 86.89 6.60 -1 4 9 69.29 6.40 -1 4 9 71.79 6.20 1 4 -9 69.89 6.70 0 -4 9 143.49 11.00 0 -4 -9 152.88 10.80 0 -4 9 147.09 11.20 0 4 9 145.29 10.80 0 4 9 133.89 10.60 0 4 -9 136.89 11.40 -1 -4 -9 62.39 5.50 1 -4 9 49.10 5.20 1 -4 9 58.69 5.70 1 4 9 63.69 5.70 1 4 9 56.59 5.40 -1 4 -9 64.09 6.10 -2 -4 -9 75.79 6.40 2 -4 9 70.39 6.60 2 -4 9 79.19 7.30 2 4 9 69.49 6.20 2 4 9 75.29 6.50 -2 4 -9 72.39 7.00 2 4 9 70.29 6.20 3 -4 9 35.60 4.60 -3 -4 -9 39.70 3.90 3 -4 9 30.80 3.90 3 4 9 36.00 3.80 3 4 9 35.90 3.80 -3 4 -9 32.70 4.80 3 4 9 31.80 3.60 4 -4 9 90.59 7.40 4 -4 9 86.29 8.40 -4 4 -9 70.69 6.30 4 4 9 91.79 7.40 4 4 9 91.09 7.30 -4 4 -9 90.19 8.50 4 4 9 89.99 7.30 4 4 9 90.99 7.20 5 -4 9 120.59 10.50 5 -4 9 116.39 9.50 5 4 9 128.29 9.50 -5 4 -9 98.59 9.10 5 4 9 135.39 9.80 5 4 9 127.89 9.50 -5 4 -9 115.19 10.80 6 -4 9 31.30 4.70 -6 -4 -9 21.20 3.30 -6 4 -9 28.50 4.90 6 4 9 33.40 4.30 6 4 9 22.50 3.50 6 4 9 20.90 3.30 7 -4 9 142.69 10.80 7 -4 9 135.69 11.90 -7 -4 -9 143.59 10.80 7 4 9 135.69 11.00 -7 4 -9 123.79 12.40 7 4 9 164.98 11.90 7 4 9 136.09 11.10 8 -4 9 7.10 3.20 8 -4 9 -4.50 3.50 -8 -4 -9 -1.10 2.40 8 4 9 -1.30 2.80 8 4 9 -4.40 3.00 -8 4 -9 -0.20 4.60 8 4 9 -1.00 4.50 9 -4 9 16.40 4.90 -9 -4 -9 23.10 3.80 -9 -4 -9 15.60 3.20 -9 4 -9 24.30 6.00 9 4 9 20.70 3.80 9 4 9 22.80 5.70 -10 -4 -9 5.60 3.40 10 -4 9 3.20 5.50 10 4 9 3.40 3.70 10 4 9 7.50 5.90 -10 4 -9 12.60 6.00 -11 -4 -9 69.09 7.20 11 -4 9 82.29 10.00 -11 4 -9 76.59 9.20 11 4 9 69.79 9.10 12 -4 9 17.90 7.50 -12 -4 -9 30.90 5.20 12 4 9 33.60 7.40 13 -4 9 82.69 11.60 -13 -4 -9 101.49 9.30 13 4 9 97.19 11.00 -13 4 -9 102.09 10.90 14 -4 9 7.60 8.50 -14 -4 -9 12.40 4.90 14 4 9 3.50 7.10 16 -5 -9 -1.50 6.40 -16 -5 9 1.20 4.80 16 5 -9 3.40 6.00 -16 5 9 5.50 4.40 15 -5 -9 109.09 11.50 -15 -5 9 117.09 10.60 -15 5 9 130.99 11.30 15 5 -9 114.49 11.30 14 -5 -9 2.40 5.90 -14 -5 9 13.10 4.60 -14 -5 9 7.90 3.20 14 5 -9 10.00 5.80 -14 5 9 2.20 3.90 -13 -5 9 60.99 6.30 -13 -5 9 50.29 5.60 13 -5 -9 50.99 7.50 -13 5 9 52.79 6.20 13 5 -9 52.89 7.30 -12 -5 9 19.00 4.00 12 -5 -9 16.30 5.30 12 -5 -9 10.20 3.90 -12 -5 9 16.40 3.40 -12 5 9 15.50 4.00 12 5 -9 21.40 5.30 -11 -5 9 214.78 16.30 -11 -5 9 207.58 16.20 11 -5 -9 215.68 17.30 11 5 -9 226.98 17.20 -11 5 9 230.78 16.60 10 -5 -9 11.50 4.10 -10 -5 9 12.50 3.20 -10 -5 9 12.00 3.20 10 5 -9 9.00 4.30 -10 5 9 16.50 3.40 -10 5 9 14.00 3.00 -9 -5 9 190.68 15.10 9 -5 -9 219.98 16.00 -9 -5 9 183.88 14.80 -9 5 9 214.28 15.00 -9 5 9 212.68 15.20 9 5 -9 202.58 15.70 -8 -5 9 31.20 3.70 -8 -5 9 35.60 4.40 8 -5 -9 37.90 4.90 8 5 -9 35.20 4.90 -8 5 9 34.20 3.90 -8 5 9 36.60 4.10 -7 -5 9 25.40 3.90 7 -5 -9 32.30 4.60 -7 -5 9 34.00 3.50 -7 5 9 41.50 4.10 7 5 -9 29.80 4.60 -7 5 9 36.60 4.10 6 -5 -9 19.20 3.60 -6 -5 9 9.70 2.80 -6 -5 9 17.90 2.30 -6 5 9 21.80 3.10 -6 5 9 22.90 3.00 6 5 -9 18.50 3.90 -5 -5 9 31.00 3.30 -5 -5 9 35.70 4.40 5 -5 -9 35.60 4.30 -5 5 9 45.50 4.10 5 5 -9 31.40 4.50 -5 5 9 44.60 4.10 -4 -5 9 0.30 2.30 4 -5 -9 3.70 2.70 -4 -5 9 4.50 1.50 4 5 -9 4.80 2.00 4 5 -9 4.40 3.10 -4 5 9 5.20 2.30 -4 5 9 7.60 2.20 3 -5 -9 175.88 11.10 -3 -5 9 115.89 10.00 -3 -5 9 138.89 10.60 -3 -5 9 154.78 11.10 -3 5 9 143.99 10.90 3 5 -9 128.69 11.20 -3 5 9 152.28 10.70 -2 -5 9 7.40 2.80 -2 -5 9 5.40 2.30 2 -5 -9 13.10 2.80 -2 5 9 9.60 2.20 2 5 -9 1.80 3.30 -2 5 9 10.30 2.60 2 5 -9 3.20 1.50 1 -5 -9 352.96 22.20 -1 -5 9 296.87 22.20 -1 -5 9 301.57 22.30 1 5 -9 285.77 21.60 1 5 -9 304.97 22.50 -1 5 9 320.87 22.20 -1 5 9 329.17 22.10 0 -5 9 78.69 6.90 0 -5 -9 78.89 6.50 0 -5 9 76.69 7.00 0 5 -9 71.79 6.90 0 5 9 69.39 6.60 0 5 -9 67.49 5.50 0 5 9 73.59 6.50 1 -5 9 187.38 14.70 -1 -5 -9 223.78 14.30 1 -5 9 196.18 14.60 -1 5 -9 153.58 13.90 -1 5 -9 188.58 15.10 1 5 9 210.88 14.40 1 5 9 207.68 14.30 2 -5 9 216.58 16.00 -2 -5 -9 223.18 15.50 2 -5 9 209.08 16.20 2 5 9 218.88 15.60 -2 5 -9 206.78 16.60 2 5 9 211.98 15.50 -3 -5 -9 -0.70 2.00 3 -5 9 1.00 3.20 3 -5 9 10.60 3.00 -3 -5 -9 2.30 2.70 -3 5 -9 6.00 4.30 3 5 9 0.80 2.40 3 5 9 -4.10 2.00 -4 -5 -9 60.99 5.70 4 -5 9 52.19 6.20 4 -5 9 56.49 5.80 -4 -5 -9 62.49 5.60 -4 5 -9 56.09 6.80 4 5 9 57.09 5.40 4 5 9 57.39 5.60 -5 -5 -9 19.80 3.40 -5 -5 -9 24.00 3.30 5 5 9 13.60 3.30 5 5 9 17.40 3.80 -5 5 -9 16.30 5.00 6 -5 9 73.49 6.50 -6 -5 -9 59.89 5.90 6 -5 9 52.19 6.70 6 5 9 74.29 6.80 -6 5 -9 70.39 7.70 6 5 9 61.19 6.20 -7 -5 -9 5.20 2.90 7 -5 9 10.40 4.00 7 5 9 5.30 3.50 7 5 9 0.60 3.40 7 5 9 -0.80 4.30 -7 5 -9 3.70 5.40 -8 -5 -9 12.80 3.30 8 -5 9 19.50 4.80 8 -5 9 10.90 4.40 8 5 9 15.60 5.10 8 5 9 12.20 4.00 -8 5 -9 20.50 6.20 -9 -5 -9 7.00 3.10 9 -5 9 8.30 5.40 9 5 9 6.30 5.60 -9 5 -9 10.40 6.40 9 5 9 5.50 4.10 10 -5 9 18.30 6.60 -10 -5 -9 12.50 4.50 -10 5 -9 6.30 6.70 10 5 9 9.80 6.10 -11 -5 -9 14.00 5.00 11 -5 9 6.90 7.00 11 5 9 12.60 6.50 -11 5 -9 12.30 7.00 12 -5 9 7.80 7.70 -12 -5 -9 10.60 5.10 12 5 9 20.50 7.00 -12 5 -9 21.20 7.50 13 -5 9 11.90 8.20 -13 -5 -9 12.10 5.20 -13 5 -9 16.80 7.80 13 5 9 17.30 7.50 15 -6 -9 8.70 6.50 -15 -6 9 4.80 5.20 15 6 -9 7.90 6.40 -15 6 9 5.40 4.50 14 -6 -9 11.40 6.20 -14 -6 9 7.20 3.80 -14 -6 9 6.10 4.80 -14 6 9 14.10 4.40 14 6 -9 3.40 6.30 -13 -6 9 25.00 5.10 13 -6 -9 30.40 6.70 -13 -6 9 21.40 4.50 13 6 -9 33.10 6.90 -13 6 9 25.80 4.90 12 -6 -9 1.70 3.90 -12 -6 9 -1.00 3.30 12 -6 -9 -3.00 5.30 -12 -6 9 4.30 4.00 12 6 -9 6.00 5.90 -12 6 9 0.90 3.70 -11 -6 9 38.70 5.10 11 -6 -9 36.00 6.20 11 -6 -9 47.10 5.50 -11 -6 9 31.70 4.90 11 6 -9 43.40 7.00 -11 6 9 37.40 5.20 -10 -6 9 26.50 4.20 -10 -6 9 22.40 4.10 10 -6 -9 25.60 4.50 10 -6 -9 18.60 4.80 -10 6 9 20.40 4.30 10 6 -9 32.90 6.00 -9 -6 9 20.40 3.70 9 -6 -9 15.80 4.30 -9 -6 9 19.80 3.60 9 -6 -9 23.10 4.50 9 6 -9 11.20 4.60 -9 6 9 22.40 3.90 -8 -6 9 -1.40 2.60 8 -6 -9 3.80 3.70 8 -6 -9 -3.00 3.40 -8 -6 9 6.30 3.30 -8 6 9 -2.30 2.80 8 6 -9 1.40 3.70 7 -6 -9 20.60 4.30 7 -6 -9 18.70 3.90 -7 -6 9 14.00 2.80 -7 -6 9 14.80 3.60 -7 6 9 19.70 3.50 7 6 -9 15.50 4.20 6 -6 -9 1.40 3.10 -6 -6 9 1.70 2.10 6 -6 -9 -3.60 3.20 -6 -6 9 -3.70 3.00 -6 6 9 1.10 2.40 6 6 -9 2.50 3.50 -5 -6 9 107.99 8.70 5 -6 -9 111.99 9.80 -5 -6 9 110.59 9.70 5 -6 -9 120.29 10.00 -5 6 9 124.19 9.30 5 6 -9 105.09 10.00 -4 -6 9 11.80 3.50 4 -6 -9 22.10 3.70 -4 -6 9 13.40 2.30 4 -6 -9 13.80 3.30 -4 6 9 20.40 3.10 4 6 -9 14.90 4.00 3 -6 -9 152.68 10.90 3 -6 -9 140.09 11.10 -3 -6 9 137.39 11.10 3 6 -9 135.89 10.20 3 6 -9 121.59 11.30 -3 6 9 131.49 10.50 2 -6 -9 13.40 2.90 -2 -6 9 11.40 2.60 -2 -6 9 10.10 3.30 2 -6 -9 5.80 2.90 2 6 -9 14.50 3.90 2 6 -9 9.80 2.00 -2 6 9 7.90 2.60 -1 -6 9 167.28 12.70 1 -6 -9 170.88 12.90 1 -6 -9 188.88 12.70 -1 -6 9 171.88 13.10 1 6 -9 141.29 12.70 -1 6 9 173.28 12.60 1 6 -9 151.38 13.30 0 -6 9 1.70 3.20 0 -6 -9 9.00 2.90 0 -6 -9 4.60 2.40 0 -6 9 10.70 3.10 0 6 9 5.90 2.50 0 6 -9 5.00 3.90 -1 -6 -9 362.96 25.60 1 -6 9 336.17 25.60 1 -6 9 351.46 25.80 -1 -6 -9 357.26 25.20 -1 6 -9 361.76 26.20 1 6 9 384.26 25.50 2 -6 9 3.10 3.50 2 -6 9 5.20 3.30 -2 -6 -9 -0.30 2.90 -2 -6 -9 -2.60 2.00 -2 6 -9 -3.80 4.50 2 6 9 1.10 2.60 -3 -6 -9 78.79 7.80 3 -6 9 76.29 7.60 3 -6 9 96.39 8.20 3 6 9 84.99 7.60 -3 6 -9 80.19 8.50 3 6 9 78.79 7.50 -4 -6 -9 34.00 4.40 4 -6 9 32.30 5.00 4 -6 9 28.70 5.20 4 6 9 31.70 4.50 4 6 9 31.60 4.30 -4 6 -9 35.80 6.60 5 -6 9 173.68 15.00 -5 -6 -9 185.38 14.40 5 -6 9 196.88 15.00 5 6 9 206.28 14.70 5 6 9 182.38 14.60 -5 6 -9 174.98 16.50 6 -6 9 55.59 7.10 6 -6 9 57.89 6.90 -6 -6 -9 71.69 6.40 6 6 9 75.59 7.10 6 6 9 66.79 6.60 -6 6 -9 58.59 8.70 7 -6 9 155.08 13.00 -7 -6 -9 164.18 12.60 7 -6 9 146.69 13.60 -7 6 -9 139.29 13.90 7 6 9 166.18 13.60 7 6 9 172.38 13.40 -8 -6 -9 77.99 7.00 8 -6 9 64.09 8.30 8 6 9 76.99 8.20 8 6 9 75.69 7.60 -8 6 -9 74.89 9.40 -9 -6 -9 8.80 3.70 9 -6 9 16.30 6.20 9 6 9 13.00 4.90 -9 6 -9 12.50 7.40 9 6 9 10.80 5.90 -10 -6 -9 -4.50 4.80 10 -6 9 0.10 6.20 -10 -6 -9 -5.70 3.40 -10 6 -9 -1.90 7.20 10 6 9 2.90 5.80 -11 -6 -9 95.99 9.70 11 -6 9 98.19 11.40 11 6 9 102.39 10.80 -11 6 -9 95.89 11.40 -12 -6 -9 -5.00 5.40 12 -6 9 -0.20 7.50 12 6 9 4.10 6.40 -13 -7 9 30.20 5.60 13 -7 -9 25.30 6.70 -13 -7 9 21.90 5.30 13 7 -9 29.10 7.10 -13 7 9 21.30 5.10 -12 -7 9 27.00 5.20 12 -7 -9 24.20 5.10 -12 -7 9 23.60 5.10 12 -7 -9 24.30 6.40 -12 7 9 27.00 5.10 12 7 -9 37.40 7.10 -11 -7 9 39.50 5.70 -11 -7 9 40.30 5.50 11 -7 -9 25.20 5.30 11 -7 -9 35.10 6.40 11 7 -9 30.40 7.00 -11 7 9 38.00 5.50 -10 -7 9 8.90 3.90 10 -7 -9 6.60 4.90 -10 -7 9 2.90 4.20 10 -7 -9 11.10 4.50 10 7 -9 12.20 6.20 -10 7 9 4.60 4.10 9 -7 -9 34.10 5.50 9 -7 -9 31.00 5.60 -9 -7 9 45.90 5.90 -9 -7 9 33.20 4.90 9 7 -9 26.50 6.30 -9 7 9 34.00 5.20 8 -7 -9 5.60 3.90 -8 -7 9 9.40 3.50 -8 -7 9 3.80 3.90 8 -7 -9 9.60 4.70 -8 7 9 12.80 4.10 8 7 -9 6.00 5.10 7 -7 -9 73.69 7.10 7 -7 -9 77.19 7.50 -7 -7 9 58.59 6.20 -7 -7 9 63.69 7.20 -7 7 9 73.49 7.00 7 7 -9 68.69 7.80 6 -7 -9 27.20 4.40 -6 -7 9 25.30 3.70 -6 -7 9 16.40 4.40 6 -7 -9 24.00 4.90 -6 7 9 25.10 4.20 6 7 -9 27.30 5.40 -5 -7 9 81.09 8.50 -5 -7 9 81.39 7.80 5 -7 -9 90.39 8.60 5 -7 -9 104.39 8.60 -5 7 9 89.49 8.50 5 7 -9 86.59 8.60 -4 -7 9 138.19 11.50 4 -7 -9 119.69 11.50 4 -7 -9 132.89 10.90 -4 7 9 124.69 10.70 4 7 -9 134.39 10.20 4 7 -9 127.49 11.70 3 -7 -9 29.00 4.70 3 -7 -9 27.30 4.10 -3 -7 9 22.10 4.70 3 7 -9 31.30 5.30 -3 7 9 31.90 4.20 2 -7 -9 84.09 8.10 -2 -7 9 103.99 9.00 2 7 -9 73.09 8.50 -2 7 9 96.69 8.30 1 -7 -9 34.40 4.70 1 -7 -9 33.50 4.20 -1 -7 9 40.40 4.50 -1 -7 9 32.50 5.60 -1 7 9 41.50 4.70 1 7 -9 33.10 6.00 0 -7 9 42.90 6.20 0 -7 -9 47.70 5.00 0 -7 -9 53.49 5.80 0 -7 9 52.59 5.50 0 7 -9 47.10 6.70 0 7 9 51.79 5.40 1 -7 9 5.10 4.40 1 -7 9 6.00 3.40 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332.97 22.00 7 2 10 296.17 21.40 7 2 10 326.07 22.00 -7 2 -10 296.57 21.20 8 -2 10 6.30 2.60 -8 -2 -10 10.60 2.60 8 -2 10 10.40 3.70 8 2 10 7.10 4.10 8 2 10 10.40 2.50 -8 2 -10 9.60 3.80 -8 2 -10 10.50 2.30 8 2 10 8.90 3.50 -9 -2 -10 73.89 6.60 9 -2 10 68.59 7.50 9 2 10 71.89 7.10 -9 2 -10 66.29 6.20 -9 2 -10 64.09 7.10 9 2 10 63.69 7.60 -10 -2 -10 -0.40 2.60 10 -2 10 -5.70 4.90 10 2 10 -4.60 4.10 10 2 10 -1.50 5.20 -10 2 -10 -3.10 2.60 -10 2 -10 1.30 4.90 11 -2 10 163.08 14.70 -11 -2 -10 141.39 11.70 11 2 10 139.49 13.20 11 2 10 151.78 14.30 -11 2 -10 147.49 14.00 -12 -2 -10 2.70 3.10 12 -2 10 5.40 6.50 -12 2 -10 0.20 6.20 12 2 10 -5.10 5.00 12 2 10 -8.10 6.40 13 -2 10 100.99 11.40 -13 -2 -10 106.09 9.50 13 2 10 103.39 11.30 -13 2 -10 108.19 11.10 13 2 10 82.19 9.80 14 -2 10 11.30 7.80 -14 -2 -10 2.40 4.10 -14 2 -10 2.90 7.50 14 2 10 -0.40 5.80 14 2 10 3.30 7.40 -17 -3 10 97.19 9.70 17 -3 -10 122.09 11.60 17 3 -10 102.89 10.40 16 -3 -10 -11.50 6.00 -16 -3 10 0.60 4.20 -16 3 10 -0.10 4.00 16 3 -10 -0.20 4.60 15 -3 -10 107.49 11.00 -15 -3 10 100.49 9.40 -15 3 10 112.39 10.30 15 3 -10 107.89 9.80 15 3 -10 104.69 10.20 -14 -3 10 5.80 3.70 -14 -3 10 6.80 2.80 14 -3 -10 -7.20 5.40 -14 3 10 10.60 3.80 14 3 -10 6.70 3.90 14 3 -10 3.70 3.80 -13 -3 10 133.39 11.10 -13 -3 10 141.29 10.40 13 -3 -10 131.79 12.90 -13 3 10 133.89 10.10 13 3 -10 141.49 11.40 13 3 -10 114.09 11.10 -13 3 10 122.69 11.20 -12 -3 10 49.40 5.00 12 -3 -10 65.29 7.00 -12 -3 10 49.40 5.30 12 3 -10 46.10 5.80 12 3 -10 49.30 5.60 -12 3 10 53.49 5.10 -12 3 10 46.60 5.30 11 -3 -10 121.09 10.90 -11 -3 10 117.59 9.80 -11 -3 10 116.79 9.60 -11 3 10 131.49 10.10 -11 3 10 123.39 9.40 11 3 -10 111.29 10.00 11 3 -10 133.49 10.50 -10 -3 10 97.09 7.60 10 -3 -10 98.09 8.70 -10 -3 10 75.49 7.20 10 3 -10 82.79 7.80 -10 3 10 79.69 7.20 -10 3 10 95.99 7.70 10 3 -10 89.89 8.30 -9 -3 10 25.70 3.40 -9 -3 10 20.30 2.90 9 -3 -10 27.50 4.40 9 3 -10 22.90 3.40 9 3 -10 23.00 3.90 -9 3 10 24.90 3.10 -9 3 10 24.40 3.30 -8 -3 10 52.09 4.70 8 -3 -10 52.69 5.50 -8 -3 10 48.10 4.80 -8 3 10 47.80 4.50 8 3 -10 52.59 5.20 8 3 -10 43.30 4.70 -8 3 10 52.39 4.70 -7 -3 10 169.48 12.40 -7 -3 10 175.08 12.80 7 -3 -10 176.28 13.50 -7 3 10 177.38 12.60 7 3 -10 182.58 13.00 7 3 -10 161.58 12.70 -7 3 10 168.98 12.70 -6 -3 10 8.10 1.60 6 -3 -10 6.50 2.80 -6 -3 10 10.90 2.40 6 3 -10 7.70 2.30 -6 3 10 4.00 1.90 -6 3 10 9.20 2.20 6 3 -10 4.90 2.80 5 -3 -10 89.99 8.20 -5 -3 10 107.19 7.80 -5 -3 10 89.99 7.00 -5 3 10 90.39 7.30 5 3 -10 94.79 7.70 -5 3 10 92.99 7.60 5 3 -10 109.69 8.10 -4 -3 10 5.60 2.30 -4 -3 10 3.20 1.20 4 -3 -10 5.40 2.50 4 3 -10 -1.40 2.50 4 3 -10 4.00 2.10 -4 3 10 6.50 1.80 -4 3 10 5.00 2.00 3 -3 -10 429.26 31.50 -3 -3 10 461.75 31.50 -3 3 10 454.75 31.30 3 3 -10 443.96 31.50 -3 3 10 467.75 31.40 -2 -3 10 12.30 2.60 2 -3 -10 10.10 2.60 -2 -3 10 10.70 2.50 -2 3 10 8.20 1.90 2 3 -10 8.40 3.00 -2 3 10 11.00 2.40 -1 -3 10 574.44 40.70 -1 -3 10 591.84 40.80 1 -3 -10 641.54 40.80 1 3 -10 560.04 40.80 -1 3 10 567.14 40.50 -1 3 10 592.74 40.70 0 -3 -10 2.70 2.20 0 -3 10 2.90 2.10 0 -3 10 -0.80 2.40 0 3 -10 1.40 3.10 0 3 10 0.00 1.70 0 3 10 2.70 2.10 1 -3 10 27.90 3.40 1 -3 10 32.80 4.00 -1 -3 -10 28.20 3.60 -1 3 -10 31.20 4.30 1 3 10 33.00 3.20 1 3 10 27.00 3.40 1 3 10 29.40 3.10 2 -3 10 23.90 3.80 2 -3 10 21.60 3.00 2 3 10 19.60 2.60 -2 3 -10 24.40 3.90 2 3 10 23.10 3.00 2 3 10 16.60 2.50 3 -3 10 8.60 2.40 3 -3 10 6.70 3.00 3 3 10 5.00 2.20 -3 3 -10 4.50 3.40 3 3 10 3.40 1.90 3 3 10 1.90 2.40 3 3 10 8.00 2.30 4 -3 10 1.20 2.20 4 -3 10 -2.10 2.90 -4 3 -10 6.60 3.50 4 3 10 -1.20 2.30 4 3 10 2.70 2.20 4 3 10 4.60 2.50 4 3 10 0.90 1.90 5 -3 10 77.29 7.70 5 -3 10 80.49 6.90 5 3 10 85.99 7.40 5 3 10 65.19 6.70 -5 3 -10 89.19 7.70 5 3 10 85.29 6.90 5 3 10 81.19 7.20 6 -3 10 4.60 3.50 6 -3 10 2.50 2.10 6 3 10 -1.80 2.10 6 3 10 1.70 3.00 6 3 10 0.50 2.70 -6 3 -10 0.50 3.60 6 3 10 -3.90 2.00 7 -3 10 -1.90 3.40 7 -3 10 4.10 2.20 -7 3 -10 -0.80 3.70 7 3 10 -0.20 2.80 7 3 10 1.00 2.20 7 3 10 4.10 2.40 7 3 10 1.00 3.40 -8 -3 -10 6.00 2.60 8 -3 10 -0.20 3.60 8 3 10 -1.70 3.40 8 3 10 11.50 4.60 -8 3 -10 4.50 4.10 9 -3 10 139.09 13.40 -9 -3 -10 158.78 11.70 9 3 10 144.69 12.40 -9 3 -10 130.69 13.10 9 3 10 162.58 13.30 10 -3 10 36.50 6.70 -10 -3 -10 31.70 4.30 -10 3 -10 30.70 6.50 10 3 10 27.80 5.20 10 3 10 34.00 6.80 -11 -3 -10 60.49 6.20 11 -3 10 47.30 8.20 11 3 10 58.09 8.40 11 3 10 54.09 6.70 -11 3 -10 75.79 8.60 12 -3 10 9.50 6.80 -12 -3 -10 -0.50 3.50 12 3 10 6.50 4.80 12 3 10 6.00 6.60 -12 3 -10 4.60 6.70 -13 -3 -10 12.10 4.60 13 3 10 15.60 7.10 13 3 10 18.20 5.40 14 -3 10 32.20 8.90 -14 -3 -10 31.00 5.40 -14 3 -10 36.50 8.70 14 3 10 20.70 7.90 14 3 10 24.10 8.60 17 -4 -10 -2.20 6.60 -16 -4 10 36.60 5.80 16 -4 -10 36.10 7.70 -16 4 10 27.90 5.20 16 4 -10 30.50 6.50 15 -4 -10 -5.90 6.00 -15 -4 10 3.60 4.10 15 4 -10 -2.00 5.00 -15 4 10 1.10 3.90 -14 -4 10 18.00 3.50 14 -4 -10 16.40 6.60 -14 -4 10 23.80 4.60 14 4 -10 23.40 5.50 -14 4 10 25.80 4.80 -13 -4 10 -0.30 3.60 -13 -4 10 2.30 2.60 13 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55.29 5.90 -6 4 10 81.09 6.40 6 4 -10 68.69 6.40 -5 -4 10 21.00 3.20 -5 -4 10 22.80 2.30 5 -4 -10 19.60 3.50 5 4 -10 25.10 3.80 5 4 -10 21.00 3.00 -5 4 10 23.90 3.00 -5 4 10 25.90 3.30 -4 -4 10 32.20 3.10 4 -4 -10 37.60 4.30 -4 -4 10 32.70 3.90 -4 4 10 43.70 4.00 -4 4 10 39.20 3.70 4 4 -10 29.50 3.60 4 4 -10 38.00 4.40 -3 -4 10 17.60 1.90 3 -4 -10 23.90 3.30 -3 -4 10 30.00 3.60 -3 -4 10 25.30 3.10 -3 4 10 25.20 3.10 3 4 -10 18.40 3.60 -3 4 10 23.00 2.80 -2 -4 10 94.39 8.10 -2 -4 10 100.19 8.20 2 -4 -10 113.39 8.30 -2 4 10 97.29 7.70 -2 4 10 98.89 8.10 2 4 -10 86.09 8.50 1 -4 -10 34.80 3.80 -1 -4 10 32.70 3.80 -1 -4 10 34.40 4.00 -1 4 10 25.70 3.30 1 4 -10 28.50 4.40 -1 4 10 34.50 3.70 0 -4 -10 300.67 19.00 0 -4 10 266.17 19.20 0 -4 10 250.57 19.10 0 4 10 251.17 18.80 0 4 10 264.47 19.00 0 4 -10 252.87 19.40 1 -4 10 609.94 41.50 1 -4 10 560.74 41.20 -1 -4 -10 634.04 41.20 -1 4 -10 580.04 41.50 1 4 10 617.64 41.20 1 4 10 556.14 41.00 2 -4 10 151.28 12.00 -2 -4 -10 166.88 11.90 2 -4 10 164.88 12.50 -2 4 -10 162.68 12.90 2 4 10 147.29 11.40 2 4 10 140.29 11.50 2 4 10 169.58 11.90 3 -4 10 226.98 16.80 3 -4 10 214.58 16.20 -3 -4 -10 252.77 16.20 -3 4 -10 222.88 16.90 3 4 10 203.58 15.90 3 4 10 207.78 15.90 3 4 10 221.78 16.10 4 -4 10 46.10 5.40 4 -4 10 34.20 4.40 -4 4 -10 36.60 5.40 4 4 10 36.20 4.20 4 4 10 37.40 4.50 4 4 10 42.90 4.30 4 4 10 44.20 4.20 5 -4 10 213.38 16.70 5 -4 10 225.78 17.60 -5 4 -10 213.98 17.60 5 4 10 228.18 16.70 5 4 10 244.28 16.70 5 4 10 226.98 16.80 5 4 10 252.57 17.00 6 -4 10 7.00 3.70 6 -4 10 1.70 2.60 6 4 10 0.90 3.70 6 4 10 8.70 2.90 6 4 10 -0.30 2.60 -6 4 -10 -1.40 4.10 -7 -4 -10 37.20 4.30 7 -4 10 35.60 5.40 7 4 10 38.10 4.70 7 4 10 39.30 4.60 -7 4 -10 30.90 5.70 7 4 10 45.50 5.90 8 -4 10 10.30 4.30 -8 -4 -10 -4.60 2.50 8 4 10 -2.30 4.70 -8 4 -10 6.50 5.00 8 4 10 4.00 3.40 8 4 10 -2.40 3.30 9 -4 10 59.99 7.70 -9 -4 -10 50.69 5.70 -9 -4 -10 50.79 5.40 9 4 10 68.39 7.90 -9 4 -10 62.09 7.90 9 4 10 50.19 5.90 -10 -4 -10 14.10 3.90 10 -4 10 10.70 6.10 10 4 10 10.90 6.20 10 4 10 15.60 4.30 -10 4 -10 16.60 6.50 11 -4 10 336.47 23.50 -11 -4 -10 267.07 21.00 -11 4 -10 272.17 22.60 11 4 10 264.57 22.60 12 -4 10 6.90 7.10 -12 -4 -10 2.40 4.30 -12 4 -10 -0.60 6.80 12 4 10 3.90 6.70 -13 -4 -10 77.79 8.30 13 -4 10 100.99 11.50 13 4 10 90.59 10.60 -13 4 -10 70.89 10.10 16 -5 -10 4.10 6.80 -16 -5 10 3.20 4.70 -16 5 10 3.20 4.40 16 5 -10 -3.20 6.00 -15 -5 10 -0.90 4.40 15 -5 -10 -3.40 6.20 15 5 -10 1.40 5.70 -15 5 10 4.10 4.20 -14 -5 10 -7.70 3.90 -14 -5 10 -0.50 3.00 14 -5 -10 -6.70 5.80 -14 5 10 -4.00 3.90 14 5 -10 1.20 5.50 -13 -5 10 10.20 4.10 13 -5 -10 -0.80 5.90 -13 -5 10 10.70 3.30 13 5 -10 13.40 5.70 -13 5 10 18.30 4.30 -12 -5 10 3.40 3.00 12 -5 -10 3.30 5.40 -12 -5 10 1.30 3.50 12 5 -10 6.30 5.00 -12 5 10 1.90 2.70 -12 5 10 -1.30 3.70 -11 -5 10 17.30 3.60 -11 -5 10 17.60 3.60 11 -5 -10 11.00 5.10 -11 5 10 19.20 4.20 -11 5 10 16.20 3.30 11 5 -10 16.00 4.80 -10 -5 10 -2.90 2.50 10 -5 -10 2.00 4.00 -10 -5 10 -1.10 2.80 -10 5 10 -2.60 2.50 -10 5 10 6.30 3.20 10 5 -10 5.10 4.00 9 -5 -10 0.60 3.60 -9 -5 10 5.50 2.40 -9 -5 10 -5.30 2.80 -9 5 10 0.80 2.80 -9 5 10 4.30 2.60 9 5 -10 0.90 3.80 -8 -5 10 3.00 2.10 -8 -5 10 -5.00 2.60 8 -5 -10 1.70 3.40 8 5 -10 3.90 3.60 -8 5 10 3.50 2.50 -8 5 10 -0.60 2.50 -7 -5 10 36.60 4.00 -7 -5 10 52.79 5.20 7 -5 -10 43.30 5.30 -7 5 10 44.60 4.80 7 5 -10 49.60 5.50 -7 5 10 44.20 4.60 -6 -5 10 10.90 2.10 -6 -5 10 9.80 3.00 6 -5 -10 17.90 3.60 6 5 -10 13.60 3.70 -6 5 10 17.90 3.10 -6 5 10 14.00 2.70 6 5 -10 9.30 2.40 -5 -5 10 7.60 1.80 5 -5 -10 14.60 3.40 -5 -5 10 12.50 3.30 -5 5 10 11.70 3.00 5 5 -10 13.20 3.70 -5 5 10 15.20 2.60 5 5 -10 12.50 2.50 -4 -5 10 38.50 3.90 4 -5 -10 58.49 5.20 -4 -5 10 54.89 5.40 4 5 -10 44.80 4.30 -4 5 10 45.40 4.50 4 5 -10 41.00 5.10 -4 5 10 49.40 4.90 3 -5 -10 83.09 7.20 -3 -5 10 74.49 6.70 -3 -5 10 82.29 7.10 -3 5 10 75.59 7.00 -3 5 10 72.69 6.50 3 5 -10 70.99 7.00 2 -5 -10 9.70 2.60 -2 -5 10 3.10 2.50 -2 -5 10 5.60 2.70 2 5 -10 3.00 3.40 -2 5 10 4.80 2.20 -2 5 10 1.70 2.20 -1 -5 10 105.89 9.60 1 -5 -10 133.29 9.50 -1 -5 10 101.49 9.60 -1 5 10 123.69 9.20 1 5 -10 110.59 10.30 -1 5 10 122.39 9.40 0 -5 -10 177.38 12.30 0 -5 10 163.98 12.70 0 -5 10 159.98 12.60 0 5 -10 140.69 13.10 0 5 10 162.98 12.10 0 5 10 160.98 12.30 1 -5 10 2.20 2.80 1 -5 10 0.60 2.90 -1 -5 -10 0.90 2.20 -1 5 -10 2.10 4.10 1 5 10 5.70 2.50 1 5 10 1.30 2.30 -2 -5 -10 304.07 20.90 2 -5 10 293.67 21.20 2 -5 10 297.17 21.50 2 5 10 294.77 20.90 2 5 10 275.37 20.70 2 5 10 296.77 21.00 -2 5 -10 291.47 21.80 3 -5 10 25.40 4.50 -3 -5 -10 25.60 3.50 3 -5 10 30.20 4.30 -3 5 -10 25.40 5.40 3 5 10 33.80 3.70 3 5 10 26.60 3.70 -4 -5 -10 361.96 25.00 -4 -5 -10 357.76 25.30 4 -5 10 348.57 25.70 4 -5 10 343.27 25.30 -4 5 -10 344.67 26.10 4 5 10 359.96 25.10 4 5 10 351.56 25.10 -5 -5 -10 44.20 5.20 -5 -5 -10 53.79 5.10 5 -5 10 48.80 5.60 5 -5 10 49.30 6.20 -5 5 -10 47.50 6.80 5 5 10 50.39 5.40 5 5 10 52.59 5.90 6 -5 10 319.57 22.80 6 -5 10 301.77 23.30 -6 5 -10 317.27 23.90 6 5 10 316.97 22.70 6 5 10 311.07 23.10 7 -5 10 9.90 3.70 7 -5 10 17.50 4.90 -7 -5 -10 10.40 3.30 7 5 10 9.90 4.90 7 5 10 10.90 3.90 7 5 10 16.50 4.00 -7 5 -10 18.20 6.20 8 -5 10 20.50 5.70 -8 -5 -10 18.20 3.60 -8 5 -10 5.60 6.70 8 5 10 20.40 4.60 8 5 10 26.90 6.30 -9 -5 -10 6.30 3.30 9 -5 10 13.60 6.00 -9 5 -10 12.30 6.70 9 5 10 8.90 5.90 9 5 10 8.10 4.30 10 -5 10 10.90 6.60 -10 -5 -10 3.70 4.40 10 5 10 8.50 6.60 -10 5 -10 12.70 6.90 11 -5 10 12.80 7.30 -11 -5 -10 9.20 5.00 11 5 10 13.90 6.90 -11 5 -10 8.70 7.10 -12 -5 -10 134.29 11.90 12 -5 10 128.49 13.20 -12 5 -10 88.39 11.80 12 5 10 122.89 12.40 15 -6 -10 -6.20 6.40 -14 -6 10 80.29 7.90 14 -6 -10 73.39 9.50 -14 -6 10 66.99 7.40 -14 6 10 71.59 7.60 14 6 -10 65.49 9.10 -13 -6 10 3.00 3.70 13 -6 -10 -5.20 5.60 -13 -6 10 5.60 4.10 13 6 -10 -8.00 5.90 -13 6 10 -1.40 3.90 12 -6 -10 175.78 15.40 -12 -6 10 162.38 13.50 12 -6 -10 174.38 14.00 -12 -6 10 158.38 13.60 12 6 -10 172.18 15.50 -12 6 10 170.38 14.00 -11 -6 10 10.60 3.80 11 -6 -10 6.40 5.20 -11 -6 10 13.90 3.80 11 -6 -10 12.70 4.30 -11 6 10 9.10 4.00 11 6 -10 14.90 6.00 10 -6 -10 229.58 17.60 -10 -6 10 211.68 16.70 -10 -6 10 204.58 16.50 10 -6 -10 247.98 17.50 -10 6 10 221.18 17.00 10 6 -10 219.68 17.90 9 -6 -10 -6.20 3.60 -9 -6 10 -4.00 2.90 -9 -6 10 -1.80 2.80 9 -6 -10 4.10 4.20 9 6 -10 -1.30 4.60 -9 6 10 -0.30 3.50 -8 -6 10 115.59 10.20 8 -6 -10 134.99 11.80 8 -6 -10 137.09 11.60 -8 -6 10 126.79 10.80 8 6 -10 134.59 11.40 -8 6 10 138.39 11.20 -7 -6 10 7.90 2.50 -7 -6 10 3.40 3.30 7 -6 -10 13.40 3.90 7 6 -10 8.10 3.90 -7 6 10 6.70 3.20 -6 -6 10 93.39 8.20 6 -6 -10 93.59 8.90 -6 -6 10 85.49 7.20 6 6 -10 80.99 8.00 -6 6 10 86.29 8.10 -5 -6 10 8.10 3.20 5 -6 -10 6.90 3.30 5 6 -10 8.90 3.80 -5 6 10 6.50 2.90 -4 -6 10 150.68 11.40 4 -6 -10 139.79 11.40 4 6 -10 143.09 11.60 -4 6 10 149.99 11.00 4 6 -10 124.09 10.60 3 -6 -10 -0.40 2.80 -3 -6 10 3.10 2.90 -3 -6 10 2.80 2.40 -3 6 10 1.70 2.50 3 6 -10 4.70 3.70 2 -6 -10 310.87 22.50 -2 -6 10 332.47 22.60 -2 -6 10 293.97 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2 6 -14 77.19 9.70 -2 6 14 94.39 8.90 -1 -6 14 18.10 5.40 -1 -6 14 15.20 4.30 1 -6 -14 19.30 3.80 -1 6 14 17.60 4.20 -1 6 14 11.50 4.20 1 6 -14 12.10 6.40 0 -6 14 147.19 14.30 0 -6 14 158.88 13.40 0 -6 -14 175.88 12.90 0 6 -14 157.48 14.50 0 6 14 168.58 13.80 0 6 14 144.99 13.00 1 -6 14 12.50 5.50 1 -6 14 12.30 4.60 -1 -6 -14 17.00 3.80 -1 6 -14 21.90 7.60 1 6 14 18.00 4.60 1 6 14 10.90 4.20 -2 -6 -14 137.29 11.10 2 -6 14 112.69 11.70 2 -6 14 146.39 12.50 -2 6 -14 139.39 13.40 2 6 14 141.49 12.50 2 6 14 120.19 11.50 -3 -6 -14 1.90 3.20 3 -6 14 -2.90 5.20 3 -6 14 4.40 4.80 3 6 14 10.10 4.30 -3 6 -14 -15.70 7.50 4 -6 14 169.68 14.10 -4 -6 -14 122.69 13.80 4 -6 14 166.38 14.30 -4 6 -14 139.89 14.70 4 6 14 165.98 13.60 5 -6 14 7.30 5.20 -5 -6 -14 9.70 5.20 5 -6 14 4.20 5.40 -5 6 -14 11.60 8.40 5 6 14 8.80 4.80 6 -6 14 72.99 8.30 6 -6 14 66.99 9.10 6 6 14 82.29 8.10 -6 6 -14 83.89 11.20 -7 -6 -14 2.10 4.90 7 -6 14 3.20 6.30 -7 6 -14 3.40 8.50 7 6 14 -5.70 4.70 8 -6 14 49.80 8.50 8 6 14 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15 16.80 3.70 -10 2 15 7.80 3.00 -10 2 15 20.60 3.80 10 2 -15 16.20 3.70 10 2 -15 4.80 4.70 9 -2 -15 3.00 4.50 -9 -2 15 0.40 2.70 -9 2 15 -1.80 2.70 9 2 -15 -2.40 3.00 -9 2 15 -4.10 2.90 9 2 -15 7.90 4.20 -8 -2 15 -3.10 2.50 8 -2 -15 -4.60 3.60 -8 2 15 -1.20 2.70 8 2 -15 -2.10 3.80 -8 2 15 -0.70 2.60 8 2 -15 -0.80 2.70 -7 -2 15 31.50 4.30 7 -2 -15 36.00 5.00 7 2 -15 40.30 4.60 7 2 -15 41.00 5.20 -7 2 15 39.50 4.10 -7 2 15 33.30 4.40 -6 -2 15 390.36 27.80 6 -2 -15 396.16 28.20 -6 2 15 423.06 27.50 6 2 -15 386.36 28.10 6 2 -15 397.46 27.80 -6 2 15 361.96 27.70 5 -2 -15 33.10 4.60 -5 -2 15 28.90 3.90 -5 2 15 28.70 3.90 5 2 -15 29.00 4.10 -5 2 15 26.50 3.30 5 2 -15 35.60 4.60 4 -2 -15 233.18 18.60 -4 -2 15 251.17 18.40 4 2 -15 245.68 18.40 -4 2 15 260.57 18.30 -4 2 15 259.87 17.90 4 2 -15 259.97 18.80 -3 -2 15 128.39 9.90 3 -2 -15 105.49 10.30 3 2 -15 121.89 10.70 -3 2 15 116.39 9.20 -3 2 15 123.79 9.80 3 2 -15 131.89 10.30 2 -2 -15 146.19 13.20 -2 -2 15 172.18 12.90 -2 2 15 160.28 12.80 2 2 -15 175.18 13.40 -2 2 15 185.68 12.40 1 -2 -15 53.19 6.50 -1 -2 15 79.09 7.10 -1 -2 15 63.39 6.30 -1 2 15 66.89 5.80 1 2 -15 75.69 6.90 -1 2 15 59.19 5.90 0 -2 -15 35.50 5.30 0 -2 15 35.20 4.70 0 -2 -15 38.50 4.30 0 -2 15 40.10 5.30 0 2 15 36.30 4.50 0 2 15 43.10 3.90 0 2 -15 47.30 5.60 -1 -2 -15 -0.80 3.50 1 -2 15 -0.60 2.90 1 -2 15 0.10 3.40 -1 -2 -15 0.60 2.60 1 2 15 -0.20 3.00 -1 2 -15 1.50 3.90 1 2 15 -1.20 2.00 2 -2 15 51.59 6.20 -2 -2 -15 44.90 4.90 2 -2 15 47.30 5.30 -2 2 -15 45.60 5.90 2 2 15 48.30 4.40 2 2 15 46.80 5.40 2 2 15 50.39 6.10 3 -2 15 7.30 3.40 -3 -2 -15 12.30 3.10 3 -2 15 10.60 4.20 3 2 15 9.40 3.60 3 2 15 7.90 2.40 -3 2 -15 10.20 4.10 3 2 15 11.70 4.40 4 -2 15 150.88 11.60 4 -2 15 156.28 13.10 -4 -2 -15 131.79 11.30 4 2 15 136.69 11.90 4 2 15 145.59 12.80 4 2 15 148.19 12.40 -4 2 -15 153.58 12.40 -5 -2 -15 3.10 3.00 5 -2 15 1.10 5.00 5 -2 15 3.00 3.20 -5 2 -15 1.60 4.00 5 2 15 7.80 4.90 5 2 15 -1.90 3.60 6 -2 15 274.97 20.20 -6 -2 -15 238.78 18.60 6 -2 15 240.08 18.50 -6 2 -15 262.57 19.40 6 2 15 253.87 19.70 6 2 15 249.18 18.70 7 -2 15 10.10 5.90 -7 -2 -15 4.70 4.00 7 2 15 5.50 3.50 -7 2 -15 15.80 5.60 7 2 15 7.60 5.50 8 -2 15 123.89 11.40 -8 -2 -15 106.99 10.10 8 2 15 97.29 10.40 -8 2 -15 102.29 10.40 -9 -2 -15 19.00 6.20 9 -2 15 25.10 6.60 9 2 15 17.50 6.20 -9 2 -15 25.30 6.60 -10 -2 -15 154.68 14.20 10 -2 15 156.68 14.70 -10 2 -15 130.69 13.00 10 2 15 129.69 12.70 11 2 15 22.90 6.90 -15 -3 15 35.60 5.50 15 -3 -15 48.40 9.10 -15 -3 15 33.20 4.80 -15 3 15 40.20 6.20 15 3 -15 42.00 5.90 15 3 -15 23.40 6.30 -14 -3 15 208.08 17.10 -14 -3 15 213.58 16.50 14 -3 -15 262.77 20.30 14 3 -15 216.18 17.00 -14 3 15 241.58 17.50 14 3 -15 192.88 17.80 -14 3 15 209.78 16.20 -13 -3 15 1.70 3.40 13 -3 -15 -8.30 6.50 -13 -3 15 -2.10 4.60 13 3 -15 6.10 4.00 -13 3 15 -0.60 2.90 13 3 -15 -5.50 4.60 -13 3 15 7.60 4.50 12 -3 -15 95.09 10.70 -12 -3 15 96.49 9.10 12 3 -15 102.99 9.70 -12 3 15 94.09 8.70 12 3 -15 100.09 9.40 -12 3 15 97.69 9.00 -11 -3 15 12.50 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6 15 77.19 7.70 -9 6 15 79.29 7.90 9 6 -15 76.39 8.60 8 -6 -15 9.70 5.50 -8 -6 15 10.00 4.90 -8 6 15 7.10 4.20 -8 6 15 11.90 4.60 8 6 -15 9.10 5.40 -7 -6 15 185.28 16.20 7 -6 -15 206.58 16.70 -7 6 15 210.78 16.00 -7 6 15 201.78 16.00 7 6 -15 186.68 16.60 -6 -6 15 1.10 4.60 6 -6 -15 11.60 5.10 -6 6 15 1.40 4.20 6 6 -15 5.70 5.50 -6 6 15 2.30 4.10 -5 -6 15 20.10 5.60 5 -6 -15 22.00 4.90 5 6 -15 22.10 4.80 5 6 -15 18.20 6.00 -5 6 15 15.50 4.50 -5 6 15 20.20 4.80 4 -6 -15 19.60 4.60 -4 -6 15 18.80 5.80 4 6 -15 15.50 6.10 4 6 -15 11.30 4.50 -4 6 15 20.30 5.00 -4 6 15 14.70 4.40 3 -6 -15 22.10 4.30 -3 -6 15 8.00 5.50 3 6 -15 13.00 6.30 -3 6 15 8.60 4.60 -3 6 15 10.90 4.30 -2 -6 15 7.00 3.80 -2 -6 15 4.40 5.00 2 -6 -15 5.40 3.60 2 6 -15 -1.00 6.20 -2 6 15 0.20 4.30 -2 6 15 2.70 3.90 1 -6 -15 18.70 4.30 -1 -6 15 22.50 4.80 -1 -6 15 26.70 6.00 -1 6 15 23.40 4.90 -1 6 15 29.80 4.80 1 6 -15 20.70 7.50 0 -6 15 -9.40 3.70 0 -6 -15 1.10 3.30 0 -6 15 -4.70 5.30 0 6 15 2.30 4.30 0 6 -15 -9.90 7.30 0 6 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6.00 10 0 -20 20.70 6.50 -10 0 20 19.10 4.50 -9 0 20 0.00 3.80 9 0 -20 -0.60 5.70 8 0 -20 27.90 6.40 -8 0 20 18.10 4.60 -7 0 20 -2.80 3.70 7 0 -20 3.80 5.40 -6 0 20 117.79 11.50 6 0 -20 156.78 13.40 -5 0 20 2.30 3.90 5 0 -20 1.80 5.50 4 0 -20 140.19 12.90 -4 0 20 112.09 10.90 -3 0 20 -2.60 3.80 3 0 -20 -1.40 5.50 -2 0 20 7.30 4.10 2 0 -20 13.10 6.40 1 0 -20 1.80 4.60 -1 0 20 -2.90 4.00 1 0 -20 1.70 6.20 0 0 -20 13.20 6.80 0 0 -20 -3.10 4.10 0 0 20 -5.20 4.10 -1 0 -20 2.30 4.50 1 0 20 3.30 4.20 -2 0 -20 13.20 4.70 2 0 20 7.50 4.40 2 0 20 10.30 6.10 3 0 20 -1.40 6.20 -3 0 -20 5.00 4.70 3 0 20 3.00 4.20 -4 0 -20 23.10 5.40 4 0 20 16.60 4.90 4 0 20 20.30 7.00 5 0 20 1.90 6.60 5 0 20 0.00 4.30 -11 -1 20 2.90 4.00 11 -1 -20 5.10 6.30 -11 1 20 1.30 3.80 11 1 -20 -5.40 5.90 10 -1 -20 33.20 7.60 -10 -1 20 41.60 5.80 10 1 -20 62.09 7.80 -10 1 20 49.20 5.90 9 -1 -20 7.40 6.00 -9 -1 20 3.90 4.10 -9 1 20 8.00 4.20 9 1 -20 7.90 5.90 -8 -1 20 44.30 5.70 8 -1 -20 43.50 7.10 8 1 -20 34.70 6.90 -8 1 20 40.60 5.50 7 -1 -20 18.90 5.90 -7 -1 20 12.10 4.60 7 1 -20 15.10 6.00 -7 1 20 13.50 4.40 -6 -1 20 112.89 9.90 6 -1 -20 91.99 9.70 -6 1 20 100.19 9.00 6 1 -20 79.79 9.80 -5 -1 20 8.20 4.30 5 -1 -20 9.20 5.50 -5 1 20 9.10 3.90 5 1 -20 6.20 6.00 4 -1 -20 25.40 6.30 -4 -1 20 23.60 4.90 4 1 -20 21.80 5.30 4 1 -20 31.00 6.80 -4 1 20 35.90 5.20 3 -1 -20 12.10 5.60 -3 -1 20 5.30 4.00 3 1 -20 -7.00 4.20 3 1 -20 4.20 6.20 -3 1 20 8.10 4.20 -2 -1 20 91.89 8.70 2 -1 -20 75.49 9.40 2 1 -20 115.49 9.40 -2 1 20 82.19 8.20 2 1 -20 81.09 10.00 1 -1 -20 0.80 5.80 -1 -1 20 -0.20 4.10 -1 1 20 5.60 4.10 1 1 -20 0.60 6.70 1 1 -20 -1.70 4.60 0 -1 20 78.99 8.70 0 -1 -20 95.29 10.40 0 1 -20 105.89 9.80 0 1 -20 113.69 11.40 0 1 20 92.79 8.90 1 -1 20 2.00 6.00 -1 -1 -20 -2.20 6.40 1 -1 20 -2.20 4.20 -1 1 -20 3.20 5.00 1 1 20 -0.10 4.30 2 -1 20 106.59 9.40 -2 -1 -20 118.69 10.10 -2 -1 -20 86.59 10.80 2 -1 20 78.59 10.50 -2 1 -20 108.49 10.10 2 1 20 102.69 9.30 -3 -1 -20 8.20 4.30 3 -1 20 -0.30 6.10 3 -1 20 0.00 4.10 3 1 20 -2.70 6.10 3 1 20 2.20 4.40 -3 1 -20 3.70 5.30 -4 -1 -20 90.79 8.70 4 -1 20 76.99 8.30 4 -1 20 105.59 10.80 4 1 20 73.89 8.30 4 1 20 84.09 10.00 -4 1 -20 103.39 9.60 5 -1 20 5.20 6.80 5 -1 20 4.40 4.30 5 1 20 3.00 4.50 5 1 20 7.30 6.80 -11 -2 20 26.80 5.10 11 -2 -20 21.00 7.20 11 2 -20 23.10 6.60 -11 2 20 23.40 4.70 10 -2 -20 5.10 6.40 -10 -2 20 19.70 5.00 10 2 -20 19.80 6.20 -10 2 20 18.80 4.60 -9 -2 20 41.50 6.00 9 -2 -20 31.00 7.10 9 2 -20 40.70 6.90 -9 2 20 36.40 5.50 8 -2 -20 -3.40 5.40 -8 -2 20 3.60 4.40 8 2 -20 1.60 5.50 -8 2 20 -1.40 3.80 -7 -2 20 66.59 7.60 7 -2 -20 91.69 9.10 -7 2 20 83.89 7.80 7 2 -20 65.59 8.70 -6 -2 20 -2.40 4.10 6 -2 -20 5.60 5.40 6 2 -20 14.10 5.90 -6 2 20 3.80 4.20 6 2 -20 -2.10 3.70 -5 -2 20 86.29 8.80 5 -2 -20 83.19 9.80 5 2 -20 107.79 10.40 -5 2 20 93.49 8.60 5 2 -20 109.89 9.80 -4 -2 20 2.80 4.40 4 -2 -20 1.60 5.20 4 2 -20 1.30 6.10 4 2 -20 -12.30 4.10 -4 2 20 -4.10 4.00 3 -2 -20 69.29 8.70 -3 -2 20 86.29 8.40 -3 2 20 73.49 7.70 3 2 -20 83.99 8.70 3 2 -20 72.89 9.90 2 -2 -20 9.50 5.50 -2 -2 20 3.10 4.40 -2 2 20 1.50 4.10 2 2 -20 -5.30 5.20 2 2 -20 -2.10 6.80 -1 -2 20 76.29 8.60 1 -2 -20 85.79 9.60 1 2 -20 97.89 11.00 1 2 -20 102.69 9.70 -1 2 20 90.09 8.50 0 -2 -20 4.40 6.00 0 -2 20 -6.00 5.80 0 -2 20 -2.70 4.40 0 2 -20 -2.20 5.90 0 2 20 10.30 4.40 -1 -2 -20 120.49 12.40 1 -2 20 139.89 12.70 1 -2 20 121.29 11.80 -1 2 -20 130.19 12.20 1 2 20 117.49 10.90 2 -2 20 15.40 6.50 2 -2 20 6.10 4.60 -2 -2 -20 10.20 6.50 2 2 20 8.60 4.70 -2 2 -20 -0.60 6.20 3 -2 20 129.99 12.60 3 -2 20 164.28 15.40 -3 2 -20 146.79 14.20 3 2 20 137.49 13.00 4 -2 20 3.40 6.50 4 -2 20 1.30 4.40 4 2 20 7.50 4.90 -4 2 -20 1.20 6.10 -10 -3 20 7.70 4.70 10 -3 -20 1.40 6.30 10 3 -20 8.70 5.60 -10 3 20 10.00 4.40 9 -3 -20 14.70 6.50 -9 -3 20 10.80 4.70 9 3 -20 20.30 4.70 9 3 -20 15.40 6.00 -9 3 20 18.20 4.80 8 -3 -20 0.80 5.70 -8 -3 20 7.90 4.60 8 3 -20 5.80 5.70 8 3 -20 0.50 4.20 -8 3 20 -3.70 4.00 -7 -3 20 37.40 6.10 7 -3 -20 28.80 6.50 7 3 -20 33.00 6.50 -7 3 20 25.10 5.10 7 3 -20 34.20 5.60 -6 -3 20 -5.10 4.40 6 -3 -20 7.40 5.40 6 3 -20 -5.00 4.40 6 3 -20 4.90 5.90 -6 3 20 -3.30 4.00 5 -3 -20 33.80 6.40 -5 -3 20 25.90 5.60 5 3 -20 27.10 6.80 5 3 -20 34.60 5.90 -5 3 20 23.10 4.90 -4 -3 20 4.30 4.60 4 -3 -20 1.50 5.30 4 3 -20 -9.50 5.00 -4 3 20 -0.50 4.00 4 3 -20 -0.30 6.40 3 -3 -20 39.10 6.60 -3 -3 20 31.30 6.20 3 3 -20 25.80 6.60 3 3 -20 34.40 8.00 -3 3 20 32.30 5.30 -2 -3 20 36.80 6.10 2 -3 -20 34.70 6.80 -2 3 20 30.10 5.50 2 3 -20 28.50 7.20 2 3 -20 48.80 8.70 1 -3 -20 6.90 5.60 -1 -3 20 -2.90 4.80 -1 3 20 3.50 4.50 1 3 -20 -6.20 6.30 0 -3 20 8.70 5.00 0 -3 20 7.80 6.20 0 -3 -20 15.70 5.90 0 3 20 6.20 4.70 0 3 -20 -5.00 6.70 -1 -3 -20 -0.60 5.80 1 -3 20 1.10 4.80 1 -3 20 6.00 6.30 -1 3 -20 -2.50 7.00 1 3 20 -1.00 4.90 -2 -3 -20 5.90 6.20 2 -3 20 -3.20 6.30 2 -3 20 2.40 4.70 2 3 20 -5.30 4.70 -2 3 -20 0.70 6.90 3 -3 20 0.60 6.50 3 -3 20 5.20 4.80 -3 -3 -20 8.90 6.30 3 3 20 -3.50 4.90 8 -4 -20 0.90 6.00 -8 -4 20 7.20 5.50 8 4 -20 -4.10 5.00 -8 4 20 5.50 4.40 8 4 -20 5.50 5.50 -7 -4 20 29.10 6.00 7 -4 -20 36.30 7.10 7 4 -20 30.60 6.40 -7 4 20 40.80 5.70 7 4 -20 33.60 6.70 6 -4 -20 18.00 6.00 -6 -4 20 24.70 5.80 6 4 -20 13.40 6.20 -6 4 20 19.30 4.90 6 4 -20 17.50 6.00 5 -4 -20 148.79 14.60 -5 -4 20 145.99 14.00 -5 4 20 161.08 13.30 5 4 -20 146.29 15.00 5 4 -20 164.38 14.60 -4 -4 20 18.50 5.50 4 -4 -20 22.10 6.00 4 4 -20 10.50 6.40 -4 4 20 17.30 5.00 4 4 -20 28.50 7.30 -3 -4 20 186.58 16.00 3 -4 -20 174.38 16.20 3 4 -20 194.98 17.10 -3 4 20 182.38 15.50 3 4 -20 201.28 18.10 -2 -4 20 2.20 5.10 2 -4 -20 5.60 5.40 2 4 -20 5.10 7.70 2 4 -20 -11.00 6.80 -2 4 20 0.10 4.50 -1 -4 20 255.77 19.50 -1 -4 20 194.28 17.90 1 -4 -20 203.28 18.30 1 4 -20 237.88 20.00 0 -4 -20 20.60 6.20 0 -4 20 9.80 6.60 0 -4 20 18.00 5.60 0 4 20 6.60 4.90 0 4 -20 15.90 8.10 1 -4 20 158.48 12.80 1 -4 20 104.89 10.60 -1 -4 -20 113.89 11.30 1 4 20 86.79 9.90 -1 4 -20 115.49 12.60 5 -5 -20 7.10 5.50 -5 5 20 0.60 4.40 4 -5 -20 131.39 12.30 -4 -5 20 141.49 12.90 -4 5 20 124.09 12.20 4 5 -20 119.89 12.50 -3 -5 20 0.20 5.50 3 -5 -20 4.20 5.40 -3 5 20 -2.50 4.50 3 5 -20 3.00 7.30 -2 5 20 29.00 5.70 -10 0 21 -1.40 4.00 10 0 -21 -2.00 5.90 9 0 -21 65.89 8.30 -9 0 21 46.20 6.30 8 0 -21 0.70 5.70 -8 0 21 5.20 4.40 -7 0 21 92.29 8.50 7 0 -21 83.09 9.60 -6 0 21 3.10 4.10 6 0 -21 6.90 5.80 -5 0 21 220.78 17.20 -4 0 21 -2.40 4.00 4 0 -21 -6.70 6.00 3 0 -21 90.79 9.90 -3 0 21 82.89 8.20 -2 0 21 -3.30 4.30 2 0 -21 -2.50 6.50 1 0 -21 76.49 9.90 -1 0 21 77.89 7.90 0 0 -21 7.80 7.20 0 0 21 8.60 4.50 -1 0 -21 86.29 8.80 1 0 21 73.19 8.00 -1 0 -21 76.89 10.40 -2 0 -21 12.50 5.20 2 0 21 -0.30 4.30 3 0 21 75.19 8.30 3 0 21 102.69 10.60 10 -1 -21 -5.20 6.20 -10 -1 21 5.10 4.40 -10 1 21 1.40 3.90 10 1 -21 10.90 6.00 -9 -1 21 49.80 6.40 9 -1 -21 37.70 7.30 -9 1 21 41.10 5.70 9 1 -21 43.70 7.40 -8 -1 21 7.00 4.20 8 -1 -21 15.60 6.30 8 1 -21 7.30 6.00 -8 1 21 12.20 4.40 7 -1 -21 35.00 7.20 -7 -1 21 56.59 6.50 7 1 -21 33.50 7.30 -7 1 21 36.90 5.60 -6 -1 21 38.40 5.90 6 -1 -21 29.00 6.80 6 1 -21 45.30 7.40 -6 1 21 30.80 5.50 -5 -1 21 63.89 7.20 -5 1 21 69.39 7.10 5 1 -21 69.99 9.00 4 -1 -21 41.40 7.40 -4 -1 21 44.10 6.10 -4 1 21 36.90 5.90 4 1 -21 47.10 7.90 3 -1 -21 38.10 7.10 -3 -1 21 30.70 5.50 3 1 -21 39.70 7.90 -3 1 21 27.40 5.30 -2 -1 21 11.00 4.80 2 -1 -21 20.40 6.70 -2 1 21 9.80 4.40 2 1 -21 10.60 5.60 2 1 -21 10.50 7.20 -1 -1 21 2.30 4.40 1 -1 -21 3.40 6.20 -1 1 21 -4.60 4.10 1 1 -21 -2.40 5.40 1 1 -21 -4.50 7.00 0 -1 -21 3.50 6.70 0 -1 21 5.40 4.50 0 1 -21 8.40 7.70 0 1 -21 -2.20 5.60 0 1 21 3.00 4.40 1 -1 21 2.60 4.40 -1 -1 -21 5.10 7.00 1 1 21 4.00 4.50 -1 1 -21 7.30 6.00 -2 -1 -21 39.60 8.30 2 -1 21 31.90 7.60 2 -1 21 29.10 5.60 -2 1 -21 43.00 7.20 2 1 21 28.20 5.50 9 -2 -21 -3.00 6.00 -9 -2 21 8.20 4.80 9 2 -21 10.40 6.10 -9 2 21 3.10 4.20 8 -2 -21 29.80 6.80 -8 -2 21 25.90 5.40 8 2 -21 34.40 6.90 -8 2 21 24.80 5.00 7 -2 -21 15.50 6.00 -7 -2 21 11.80 5.00 -7 2 21 8.80 4.30 7 2 -21 11.20 6.20 6 -2 -21 51.09 7.60 -6 -2 21 46.50 6.40 -6 2 21 33.90 5.70 6 2 -21 53.49 7.80 5 -2 -21 55.99 7.80 -5 -2 21 53.89 6.70 5 2 -21 47.10 6.80 5 2 -21 50.69 8.00 -5 2 21 39.70 6.00 -4 -2 21 27.30 5.40 4 -2 -21 39.50 6.80 -4 2 21 24.00 5.00 4 2 -21 36.20 7.90 4 2 -21 27.40 6.00 -3 -2 21 3.90 4.50 3 -2 -21 11.60 6.00 3 2 -21 2.60 5.50 -3 2 21 10.10 4.50 3 2 -21 8.00 7.20 -2 -2 21 5.10 4.70 2 -2 -21 8.60 6.00 2 2 -21 -6.70 5.70 2 2 -21 4.90 7.40 -2 2 21 5.10 4.50 1 -2 -21 16.30 6.50 -1 -2 21 12.50 5.00 1 2 -21 9.90 6.40 -1 2 21 12.70 4.80 1 2 -21 30.20 8.60 0 -2 -21 0.20 6.30 0 -2 21 5.90 4.70 0 2 -21 -7.70 6.20 0 2 21 -0.60 4.50 1 -2 21 18.10 5.30 -1 -2 -21 24.70 7.30 1 -2 21 29.00 7.40 1 2 21 20.30 5.30 -1 2 -21 21.80 7.20 -2 -2 -21 0.60 6.70 2 -2 21 -1.00 4.50 2 -2 21 2.50 6.70 2 2 21 -0.10 4.60 8 -3 -21 30.00 7.10 8 3 -21 36.30 7.00 -8 3 21 32.90 5.60 7 -3 -21 12.00 5.90 -7 -3 21 0.30 4.60 -7 3 21 -1.30 4.40 7 3 -21 -2.20 4.90 7 3 -21 2.20 5.70 6 -3 -21 78.19 9.20 -6 -3 21 65.89 7.90 6 3 -21 75.79 9.40 6 3 -21 76.79 8.30 -6 3 21 73.09 7.80 5 -3 -21 2.30 5.50 -5 -3 21 -2.00 4.70 5 3 -21 -9.60 5.00 -5 3 21 -0.40 4.20 5 3 -21 -0.70 6.40 4 -3 -21 92.39 10.30 -4 -3 21 87.59 9.50 4 3 -21 110.99 10.30 -4 3 21 97.59 9.20 4 3 -21 97.69 11.10 3 -3 -21 23.20 6.40 -3 -3 21 18.00 5.70 -3 3 21 21.60 5.10 3 3 -21 20.70 6.80 3 3 -21 37.50 8.20 2 -3 -21 143.99 13.00 -2 -3 21 127.39 12.00 -2 3 21 133.19 12.50 2 3 -21 138.99 13.30 1 -3 -21 25.30 6.70 -1 -3 21 20.30 5.70 1 3 -21 24.90 8.70 -1 3 21 21.60 5.30 1 3 -21 19.70 7.60 0 -3 21 153.38 13.50 0 -3 21 123.59 11.70 0 -3 -21 145.49 12.90 0 3 21 114.39 11.30 -4 4 21 7.80 4.80 -3 4 21 43.00 6.40 -7 0 22 -2.50 4.50 7 0 -22 9.00 6.10 -6 0 22 118.09 10.60 -5 0 22 1.30 4.30 5 0 -22 2.50 6.20 4 0 -22 68.89 9.70 -4 0 22 80.59 8.10 3 0 -22 -2.50 6.50 -3 0 22 -1.30 4.30 -2 0 22 45.50 6.20 2 0 -22 48.60 8.70 -1 0 22 -2.70 4.30 1 0 -22 3.50 7.30 0 0 22 4.00 4.50 0 0 -22 9.50 7.50 7 -1 -22 15.10 6.70 -7 -1 22 20.10 4.90 -7 1 22 16.40 4.60 7 1 -22 15.00 6.70 -6 -1 22 35.00 5.80 6 -1 -22 31.80 7.50 6 1 -22 40.80 7.50 -6 1 22 36.80 5.70 -5 -1 22 35.60 5.70 5 -1 -22 38.70 7.30 5 1 -22 36.80 7.90 -5 1 22 20.20 5.00 -4 -1 22 107.39 9.80 4 1 -22 100.59 11.30 -4 1 22 97.89 9.50 -3 -1 22 3.20 4.60 3 -1 -22 6.30 6.80 3 1 -22 0.20 7.40 -3 1 22 -0.20 4.40 -2 -1 22 60.59 6.90 2 -1 -22 55.19 8.60 -2 1 22 45.40 6.40 2 1 -22 51.89 9.40 1 -1 -22 0.30 6.80 -1 -1 22 1.20 4.50 1 1 -22 7.80 7.90 -1 1 22 4.40 4.50 -6 2 22 75.39 7.90 5 -2 -22 58.39 8.90 -5 -2 22 60.79 7.70 -5 2 22 82.59 7.70 5 2 -22 99.89 10.20 4 -2 -22 21.20 6.80 -4 -2 22 15.10 5.30 4 2 -22 13.30 7.40 -4 2 22 11.20 4.80 -3 -2 22 30.80 5.80 3 -2 -22 26.10 6.90 -3 2 22 24.00 5.30 3 2 -22 34.50 8.60 -2 -2 22 1.00 4.60 2 -2 -22 -4.10 6.20 -2 2 22 -1.70 4.30 2 2 -22 0.30 7.80 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 30433 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.50871(2) 0.66420(3) 0.71177(2) 0.01685(11) Uani 1 1 d . . . . . O1 O 0.39698(10) 0.61887(18) 0.68016(9) 0.0212(4) Uani 1 1 d D . . . . N1 N 0.61299(13) 0.6805(2) 0.67766(10) 0.0190(4) Uani 1 1 d . . . . . N2 N 0.55871(12) 0.6808(2) 0.81311(10) 0.0192(4) Uani 1 1 d . . . . . C1 C 0.69141(15) 0.6850(3) 0.72061(13) 0.0194(5) Uani 1 1 d . . . . . C2 C 0.70539(15) 0.6786(3) 0.79696(13) 0.0208(5) Uani 1 1 d . . . . . H2 H 0.764135 0.673180 0.822280 0.025 Uiso 1 1 calc R U . . . C3 C 0.64336(15) 0.6791(3) 0.84036(13) 0.0203(5) Uani 1 1 d . . . . . C4 C 0.76951(16) 0.7005(3) 0.68637(14) 0.0271(6) Uani 1 1 d . . . . . H4A H 0.769104 0.621833 0.650067 0.041 Uiso 1 1 calc R U . . . H4B H 0.822307 0.692792 0.724603 0.041 Uiso 1 1 calc R U . . . H4C H 0.768047 0.796830 0.662131 0.041 Uiso 1 1 calc R U . . . C5 C 0.67519(17) 0.6775(3) 0.92249(14) 0.0301(6) Uani 1 1 d . . . . . H5A H 0.664504 0.774053 0.942774 0.045 Uiso 1 1 calc R U . . . H5B H 0.737511 0.656409 0.933940 0.045 Uiso 1 1 calc R U . . . H5C H 0.644258 0.600939 0.944176 0.045 Uiso 1 1 calc R U . . . C6 C 0.60470(14) 0.6965(3) 0.59956(12) 0.0170(5) Uani 1 1 d . . . . . C7 C 0.60610(14) 0.5724(3) 0.55563(12) 0.0189(5) Uani 1 1 d . . . . . C8 C 0.59886(15) 0.5922(3) 0.48044(13) 0.0202(5) Uani 1 1 d . . . . . H8 H 0.598971 0.508041 0.449928 0.024 Uiso 1 1 calc R U . . . C9 C 0.59145(15) 0.7320(3) 0.44878(13) 0.0205(5) Uani 1 1 d . . . . . C10 C 0.58900(15) 0.8534(3) 0.49397(13) 0.0192(5) Uani 1 1 d . . . . . H10 H 0.583136 0.949396 0.472843 0.023 Uiso 1 1 calc R U . . . C11 C 0.59487(14) 0.8385(3) 0.56923(12) 0.0175(5) Uani 1 1 d . . . . . C12 C 0.61837(17) 0.4204(3) 0.58869(14) 0.0265(6) Uani 1 1 d . . . . . H12A H 0.605284 0.346297 0.549575 0.040 Uiso 1 1 calc R U . . . H12B H 0.579290 0.407090 0.622974 0.040 Uiso 1 1 calc R U . . . H12C H 0.678544 0.408821 0.615068 0.040 Uiso 1 1 calc R U . . . C13 C 0.58825(18) 0.7497(3) 0.36750(13) 0.0296(6) Uani 1 1 d . . . . . H13A H 0.591087 0.652239 0.345168 0.044 Uiso 1 1 calc R U . . . H13B H 0.637551 0.809689 0.360120 0.044 Uiso 1 1 calc R U . . . H13C H 0.534024 0.798702 0.344462 0.044 Uiso 1 1 calc R U . . . C14 C 0.59262(16) 0.9705(3) 0.61788(13) 0.0233(5) Uani 1 1 d . . . . . H14A H 0.542587 0.962814 0.641499 0.035 Uiso 1 1 calc R U . . . H14B H 0.587746 1.060791 0.588237 0.035 Uiso 1 1 calc R U . . . H14C H 0.646044 0.973900 0.655606 0.035 Uiso 1 1 calc R U . . . C15 C 0.50008(15) 0.6973(3) 0.86211(12) 0.0196(5) Uani 1 1 d . . . . . C16 C 0.48390(16) 0.8385(3) 0.88630(13) 0.0242(5) Uani 1 1 d . . . . . C17 C 0.42670(17) 0.8525(3) 0.93362(14) 0.0277(6) Uani 1 1 d . . . . . H17 H 0.416219 0.947664 0.951508 0.033 Uiso 1 1 calc R U . . . C18 C 0.38438(16) 0.7311(3) 0.95555(13) 0.0287(6) Uani 1 1 d . . . . . C19 C 0.40073(15) 0.5933(3) 0.92907(13) 0.0256(6) Uani 1 1 d . . . . . H19 H 0.371781 0.509592 0.943412 0.031 Uiso 1 1 calc R U . . . C20 C 0.45798(15) 0.5734(3) 0.88232(12) 0.0217(5) Uani 1 1 d . . . . . C21 C 0.52585(19) 0.9728(3) 0.86083(16) 0.0350(6) Uani 1 1 d . . . . . H21A H 0.588883 0.966374 0.877577 0.053 Uiso 1 1 calc R U . . . H21B H 0.504388 1.061830 0.881294 0.053 Uiso 1 1 calc R U . . . H21C H 0.511569 0.977736 0.807055 0.053 Uiso 1 1 calc R U . . . C22 C 0.32329(18) 0.7502(4) 1.00725(15) 0.0392(7) Uani 1 1 d . . . . . H22A H 0.355482 0.740871 1.058036 0.059 Uiso 1 1 calc R U . . . H22B H 0.278171 0.674123 0.997326 0.059 Uiso 1 1 calc R U . . . H22C H 0.296382 0.848182 1.000098 0.059 Uiso 1 1 calc R U . . . C23 C 0.47259(18) 0.4235(3) 0.85339(15) 0.0303(6) Uani 1 1 d . . . . . H23A H 0.448904 0.348326 0.881725 0.045 Uiso 1 1 calc R U . . . H23B H 0.534930 0.406983 0.857872 0.045 Uiso 1 1 calc R U . . . H23C H 0.443534 0.416937 0.801590 0.045 Uiso 1 1 calc R U . . . C24 C 0.3219(5) 0.7086(9) 0.6650(5) 0.020(2) Uani 0.508(15) 1 d D U P A 1 C25 C 0.3386(5) 0.8380(10) 0.6177(8) 0.053(3) Uani 0.508(15) 1 d D U P A 1 H25A H 0.387832 0.895703 0.644149 0.079 Uiso 0.508(15) 1 calc R U P A 1 H25B H 0.286922 0.900947 0.606802 0.079 Uiso 0.508(15) 1 calc R U P A 1 H25C H 0.351736 0.800859 0.571717 0.079 Uiso 0.508(15) 1 calc R U P A 1 C26 C 0.2497(8) 0.6163(12) 0.6204(6) 0.036(2) Uani 0.508(15) 1 d D U P A 1 H26A H 0.265925 0.585439 0.574523 0.054 Uiso 0.508(15) 1 calc R U P A 1 H26B H 0.196322 0.674964 0.609121 0.054 Uiso 0.508(15) 1 calc R U P A 1 H26C H 0.240042 0.528715 0.648691 0.054 Uiso 0.508(15) 1 calc R U P A 1 C27 C 0.2999(8) 0.7594(16) 0.7353(5) 0.058(3) Uani 0.508(15) 1 d D U P A 1 H27A H 0.292630 0.673538 0.765533 0.087 Uiso 0.508(15) 1 calc R U P A 1 H27B H 0.245752 0.816164 0.724625 0.087 Uiso 0.508(15) 1 calc R U P A 1 H27C H 0.346698 0.822033 0.761812 0.087 Uiso 0.508(15) 1 calc R U P A 1 C24B C 0.3214(5) 0.7069(9) 0.6731(5) 0.025(2) Uani 0.492(15) 1 d D U P A 2 C25B C 0.3433(6) 0.8676(9) 0.6619(9) 0.056(3) Uani 0.492(15) 1 d D U P A 2 H25D H 0.378016 0.907089 0.707671 0.083 Uiso 0.492(15) 1 calc R U P A 2 H25E H 0.289564 0.924699 0.648184 0.083 Uiso 0.492(15) 1 calc R U P A 2 H25F H 0.376322 0.874555 0.622783 0.083 Uiso 0.492(15) 1 calc R U P A 2 C26B C 0.2583(10) 0.6549(18) 0.6050(7) 0.059(4) Uani 0.492(15) 1 d D U P A 2 H26D H 0.283441 0.671616 0.561645 0.089 Uiso 0.492(15) 1 calc R U P A 2 H26E H 0.203943 0.710129 0.599928 0.089 Uiso 0.492(15) 1 calc R U P A 2 H26F H 0.246838 0.549199 0.609487 0.089 Uiso 0.492(15) 1 calc R U P A 2 C27B C 0.2825(7) 0.6904(15) 0.7396(5) 0.049(2) Uani 0.492(15) 1 d D U P A 2 H27D H 0.268358 0.586331 0.745784 0.073 Uiso 0.492(15) 1 calc R U P A 2 H27E H 0.229478 0.749862 0.733533 0.073 Uiso 0.492(15) 1 calc R U P A 2 H27F H 0.324015 0.724276 0.783118 0.073 Uiso 0.492(15) 1 calc R U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.01539(16) 0.01788(17) 0.01655(16) 0.00004(11) 0.00153(11) 0.00062(11) O1 0.0163(8) 0.0207(9) 0.0252(9) -0.0008(7) 0.0009(7) 0.0017(7) N1 0.0202(10) 0.0187(10) 0.0174(10) 0.0025(8) 0.0022(8) 0.0023(8) N2 0.0186(10) 0.0218(10) 0.0175(10) 0.0001(8) 0.0045(8) -0.0016(8) C1 0.0180(11) 0.0179(12) 0.0214(12) 0.0016(9) 0.0018(9) 0.0034(9) C2 0.0152(11) 0.0254(13) 0.0197(12) 0.0001(10) -0.0013(9) 0.0012(9) C3 0.0216(12) 0.0204(12) 0.0175(11) 0.0005(9) 0.0006(9) -0.0015(10) C4 0.0193(12) 0.0389(16) 0.0229(13) 0.0024(11) 0.0041(10) 0.0016(11) C5 0.0250(13) 0.0437(17) 0.0196(13) 0.0031(11) -0.0005(10) -0.0031(12) C6 0.0147(11) 0.0202(12) 0.0157(11) 0.0029(9) 0.0022(9) 0.0009(9) C7 0.0165(11) 0.0190(12) 0.0204(12) 0.0007(9) 0.0021(9) 0.0013(9) C8 0.0220(12) 0.0175(12) 0.0208(12) -0.0021(10) 0.0040(9) 0.0016(9) C9 0.0203(12) 0.0213(12) 0.0199(12) 0.0011(10) 0.0041(9) -0.0001(10) C10 0.0200(12) 0.0163(12) 0.0201(12) 0.0034(9) 0.0016(9) 0.0000(9) C11 0.0147(11) 0.0174(11) 0.0191(11) -0.0008(9) 0.0005(9) 0.0001(9) C12 0.0322(14) 0.0186(13) 0.0276(13) 0.0035(10) 0.0041(11) 0.0052(10) C13 0.0435(16) 0.0254(14) 0.0213(13) 0.0021(11) 0.0101(11) 0.0027(12) C14 0.0287(13) 0.0168(12) 0.0228(12) -0.0014(10) 0.0012(10) -0.0004(10) C15 0.0184(11) 0.0267(13) 0.0127(11) -0.0015(9) 0.0007(9) 0.0009(10) C16 0.0243(13) 0.0265(13) 0.0214(12) -0.0024(10) 0.0036(10) -0.0024(10) C17 0.0268(13) 0.0325(15) 0.0226(13) -0.0072(11) 0.0021(10) 0.0046(11) C18 0.0198(12) 0.0478(17) 0.0171(12) 0.0015(12) 0.0009(10) 0.0023(12) C19 0.0208(12) 0.0344(15) 0.0207(12) 0.0074(11) 0.0023(10) -0.0042(11) C20 0.0216(12) 0.0249(13) 0.0164(11) 0.0030(10) -0.0012(9) -0.0014(10) C21 0.0425(17) 0.0245(15) 0.0400(16) -0.0067(12) 0.0130(13) -0.0068(12) C22 0.0281(15) 0.061(2) 0.0301(15) 0.0029(14) 0.0109(12) 0.0072(14) C23 0.0334(14) 0.0248(14) 0.0338(14) 0.0045(11) 0.0094(11) -0.0031(11) C24 0.017(4) 0.023(4) 0.022(3) 0.002(3) 0.005(3) 0.007(3) C25 0.029(3) 0.038(4) 0.083(6) 0.024(4) -0.007(4) 0.003(3) C26 0.017(3) 0.032(4) 0.053(5) -0.010(4) -0.005(4) -0.005(3) C27 0.051(5) 0.078(7) 0.039(4) -0.016(5) -0.005(4) 0.044(5) C24B 0.017(4) 0.023(4) 0.030(4) -0.001(3) -0.004(3) -0.002(3) C25B 0.036(4) 0.026(4) 0.102(7) 0.015(4) 0.008(5) 0.009(3) C26B 0.042(6) 0.076(8) 0.051(5) -0.022(5) -0.011(4) 0.026(5) C27B 0.036(4) 0.070(6) 0.043(4) 0.020(5) 0.016(3) 0.021(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Cu1 N1 140.89(8) . . ? O1 Cu1 N2 121.82(8) . . ? N1 Cu1 N2 96.58(8) . . ? C24 O1 Cu1 131.4(4) . . ? C24B O1 Cu1 130.9(4) . . ? C1 N1 C6 119.05(19) . . ? C1 N1 Cu1 124.63(16) . . ? C6 N1 Cu1 116.24(14) . . ? C3 N2 C15 119.17(19) . . ? C3 N2 Cu1 124.08(16) . . ? C15 N2 Cu1 116.75(15) . . ? N1 C1 C2 123.1(2) . . ? N1 C1 C4 119.3(2) . . ? C2 C1 C4 117.6(2) . . ? C3 C2 C1 127.5(2) . . ? C3 C2 H2 116.3 . . ? C1 C2 H2 116.3 . . ? N2 C3 C2 123.4(2) . . ? N2 C3 C5 119.2(2) . . ? C2 C3 C5 117.4(2) . . ? C1 C4 H4A 109.5 . . ? C1 C4 H4B 109.5 . . ? H4A C4 H4B 109.5 . . ? C1 C4 H4C 109.5 . . ? H4A C4 H4C 109.5 . . ? H4B C4 H4C 109.5 . . ? C3 C5 H5A 109.5 . . ? C3 C5 H5B 109.5 . . ? H5A C5 H5B 109.5 . . ? C3 C5 H5C 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? C7 C6 C11 121.2(2) . . ? C7 C6 N1 120.2(2) . . ? C11 C6 N1 118.6(2) . . ? C8 C7 C6 118.6(2) . . ? C8 C7 C12 120.4(2) . . ? C6 C7 C12 121.0(2) . . ? C9 C8 C7 121.7(2) . . ? C9 C8 H8 119.2 . . ? C7 C8 H8 119.2 . . ? C10 C9 C8 118.3(2) . . ? C10 C9 C13 121.5(2) . . ? C8 C9 C13 120.2(2) . . ? C9 C10 C11 121.9(2) . . ? C9 C10 H10 119.1 . . ? C11 C10 H10 119.1 . . ? C10 C11 C6 118.3(2) . . ? C10 C11 C14 121.6(2) . . ? C6 C11 C14 120.1(2) . . ? C7 C12 H12A 109.5 . . ? C7 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? C7 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C9 C13 H13A 109.5 . . ? C9 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? C9 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? C11 C14 H14A 109.5 . . ? C11 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C11 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C20 C15 C16 121.4(2) . . ? C20 C15 N2 119.5(2) . . ? C16 C15 N2 119.0(2) . . ? C17 C16 C15 118.2(2) . . ? C17 C16 C21 120.6(2) . . ? C15 C16 C21 121.2(2) . . ? C16 C17 C18 121.8(2) . . ? C16 C17 H17 119.1 . . ? C18 C17 H17 119.1 . . ? C19 C18 C17 118.2(2) . . ? C19 C18 C22 121.4(3) . . ? C17 C18 C22 120.3(3) . . ? C18 C19 C20 122.1(2) . . ? C18 C19 H19 118.9 . . ? C20 C19 H19 118.9 . . ? C19 C20 C15 118.1(2) . . ? C19 C20 C23 120.7(2) . . ? C15 C20 C23 121.1(2) . . ? C16 C21 H21A 109.5 . . ? C16 C21 H21B 109.5 . . ? H21A C21 H21B 109.5 . . ? C16 C21 H21C 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C18 C22 H22A 109.5 . . ? C18 C22 H22B 109.5 . . ? H22A C22 H22B 109.5 . . ? C18 C22 H22C 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? C20 C23 H23A 109.5 . . ? C20 C23 H23B 109.5 . . ? H23A C23 H23B 109.5 . . ? C20 C23 H23C 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? O1 C24 C27 109.8(7) . . ? O1 C24 C26 107.2(8) . . ? C27 C24 C26 111.5(7) . . ? O1 C24 C25 108.7(6) . . ? C27 C24 C25 111.6(7) . . ? C26 C24 C25 107.9(6) . . ? C24 C25 H25A 109.5 . . ? C24 C25 H25B 109.5 . . ? H25A C25 H25B 109.5 . . ? C24 C25 H25C 109.5 . . ? H25A C25 H25C 109.5 . . ? H25B C25 H25C 109.5 . . ? C24 C26 H26A 109.5 . . ? C24 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C24 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C24 C27 H27A 109.5 . . ? C24 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C24 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? O1 C24B C27B 110.3(7) . . ? O1 C24B C26B 107.3(9) . . ? C27B C24B C26B 110.5(7) . . ? O1 C24B C25B 110.0(6) . . ? C27B C24B C25B 110.6(7) . . ? C26B C24B C25B 108.2(7) . . ? C24B C25B H25D 109.5 . . ? C24B C25B H25E 109.5 . . ? H25D C25B H25E 109.5 . . ? C24B C25B H25F 109.5 . . ? H25D C25B H25F 109.5 . . ? H25E C25B H25F 109.5 . . ? C24B C26B H26D 109.5 . . ? C24B C26B H26E 109.5 . . ? H26D C26B H26E 109.5 . . ? C24B C26B H26F 109.5 . . ? H26D C26B H26F 109.5 . . ? H26E C26B H26F 109.5 . . ? C24B C27B H27D 109.5 . . ? C24B C27B H27E 109.5 . . ? H27D C27B H27E 109.5 . . ? C24B C27B H27F 109.5 . . ? H27D C27B H27F 109.5 . . ? H27E C27B H27F 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1 O1 1.7860(16) . ? Cu1 N1 1.884(2) . ? Cu1 N2 1.894(2) . ? O1 C24 1.415(6) . ? O1 C24B 1.416(6) . ? N1 C1 1.328(3) . ? N1 C6 1.438(3) . ? N2 C3 1.326(3) . ? N2 C15 1.431(3) . ? C1 C2 1.393(3) . ? C1 C4 1.503(3) . ? C2 C3 1.389(3) . ? C2 H2 0.9500 . ? C3 C5 1.507(3) . ? C4 H4A 0.9800 . ? C4 H4B 0.9800 . ? C4 H4C 0.9800 . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 C7 1.391(3) . ? C6 C11 1.400(3) . ? C7 C8 1.391(3) . ? C7 C12 1.503(3) . ? C8 C9 1.391(3) . ? C8 H8 0.9500 . ? C9 C10 1.389(3) . ? C9 C13 1.510(3) . ? C10 C11 1.390(3) . ? C10 H10 0.9500 . ? C11 C14 1.503(3) . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 C20 1.393(3) . ? C15 C16 1.395(3) . ? C16 C17 1.388(4) . ? C16 C21 1.506(4) . ? C17 C18 1.389(4) . ? C17 H17 0.9500 . ? C18 C19 1.384(4) . ? C18 C22 1.503(4) . ? C19 C20 1.386(3) . ? C19 H19 0.9500 . ? C20 C23 1.495(4) . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C22 H22C 0.9800 . ? C23 H23A 0.9800 . ? C23 H23B 0.9800 . ? C23 H23C 0.9800 . ? C24 C27 1.490(7) . ? C24 C26 1.516(7) . ? C24 C25 1.520(7) . ? C25 H25A 0.9800 . ? C25 H25B 0.9800 . ? C25 H25C 0.9800 . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C24B C27B 1.496(8) . ? C24B C26B 1.516(7) . ? C24B C25B 1.519(7) . ? C25B H25D 0.9800 . ? C25B H25E 0.9800 . ? C25B H25F 0.9800 . ? C26B H26D 0.9800 . ? C26B H26E 0.9800 . ? C26B H26F 0.9800 . ? C27B H27D 0.9800 . ? C27B H27E 0.9800 . ? C27B H27F 0.9800 . ?