#------------------------------------------------------------------------------ #$Date: 2021-11-10 01:16:51 +0200 (Wed, 10 Nov 2021) $ #$Revision: 270546 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/51/1565153.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1565153 loop_ _publ_author_name 'Wang, Lele' 'Han, Hua-Bin' 'Gu, Lijie' 'Zhang, Wenjing' 'Zhao, Junwei' 'Wang, Qi-Lin' _publ_section_title ; Skeletal remodeling of chalcone-based pyridinium salts to access isoindoline polycycles and their bridged derivatives ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC05741C _journal_year 2021 _chemical_formula_moiety 'C26 H26 N4 O3' _chemical_formula_sum 'C26 H26 N4 O3' _chemical_formula_weight 442.51 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _audit_creation_date 2020-06-24 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-05-28 deposited with the CCDC. 2021-11-08 downloaded from the CCDC. ; _cell_angle_alpha 106.178(4) _cell_angle_beta 93.800(3) _cell_angle_gamma 114.614(3) _cell_formula_units_Z 2 _cell_length_a 9.5216(3) _cell_length_b 10.7823(4) _cell_length_c 12.6332(5) _cell_measurement_reflns_used 2433 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 67.7780 _cell_measurement_theta_min 4.7750 _cell_volume 1107.48(8) _computing_cell_refinement 'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.53 (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXS (Sheldrick, 2008)' _diffrn_ambient_temperature 293(2) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 16.2312 _diffrn_detector_type Eos _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -52.00 35.00 0.50 1.50 -- -33.50 57.00 -60.00 174 2 \w -108.00 -32.00 0.50 1.50 -- -33.50 178.00 120.00 152 3 \w -102.00 -15.00 0.50 1.50 -- -33.50 -57.00 150.00 174 4 \w -34.00 59.00 0.50 1.50 -- 36.47 -37.00-120.00 186 5 \w 57.00 110.00 0.50 1.50 -- 36.47 178.00-180.00 106 6 \w 57.00 110.00 0.50 1.50 -- 36.47 178.00 150.00 106 7 \w 14.00 107.00 0.50 1.50 -- 36.47 37.00 60.00 186 8 \w -4.00 53.00 0.50 1.50 -- 36.47 -99.00 30.00 114 9 \w 11.00 40.00 0.50 1.50 -- 36.47 77.00 60.00 58 10 \w -32.00 19.00 0.50 1.50 -- 36.47 -77.00 120.00 102 11 \w 40.00 65.00 0.50 1.50 -- 36.47 -77.00 120.00 50 12 \w 31.00 105.00 0.50 1.50 -- 36.47 57.00 -30.00 148 13 \w 19.00 72.00 0.50 1.50 -- 36.47 -99.00 120.00 106 14 \w 5.00 75.00 0.50 1.50 -- 36.47 -99.00 -90.00 140 15 \w 61.00 105.00 0.50 1.50 -- 36.47 77.00 60.00 88 16 \w 152.00 178.00 0.50 6.50 -- 108.00 111.00 150.00 52 17 \w 44.00 99.00 0.50 6.50 -- 108.00-111.00 150.00 110 18 \w 38.00 127.00 0.50 6.50 -- 108.00 -45.00 0.00 178 19 \w 80.00 132.00 0.50 6.50 -- 108.00 -77.00 90.00 104 20 \w 76.00 108.00 0.50 6.50 -- 108.00 -94.00 -60.00 64 21 \w 45.00 123.00 0.50 6.50 -- 108.00 -45.00-180.00 156 22 \w 97.00 149.00 0.50 6.50 -- 108.00 30.00 30.00 104 23 \w 37.00 122.00 0.50 6.50 -- 108.00 -30.00 90.00 170 24 \w 76.00 109.00 0.50 6.50 -- 108.00 -94.00-180.00 66 25 \w 68.00 109.00 0.50 6.50 -- 108.00-111.00 90.00 82 26 \w 40.00 127.00 0.50 6.50 -- 108.00 -45.00 -90.00 174 27 \w 60.00 101.00 0.50 6.50 -- 108.00 -94.00 -90.00 82 28 \w 38.00 178.00 0.50 6.50 -- 108.00 0.00 150.00 280 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Xcalibur, Eos, Gemini' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0063998000 _diffrn_orient_matrix_UB_12 0.0251273000 _diffrn_orient_matrix_UB_13 0.1253772000 _diffrn_orient_matrix_UB_21 -0.1810276000 _diffrn_orient_matrix_UB_22 -0.0903974000 _diffrn_orient_matrix_UB_23 -0.0325428000 _diffrn_orient_matrix_UB_31 0.0174674000 _diffrn_orient_matrix_UB_32 -0.1381035000 _diffrn_orient_matrix_UB_33 -0.0088731000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0229 _diffrn_reflns_av_unetI/netI 0.0326 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 7986 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 67.068 _diffrn_reflns_theta_max 67.068 _diffrn_reflns_theta_min 3.725 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.715 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.86956 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.53 (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.327 _exptl_crystal_description prism _exptl_crystal_F_000 468 _exptl_crystal_size_max 0.22 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.09 _refine_diff_density_max 0.334 _refine_diff_density_min -0.206 _refine_diff_density_rms 0.041 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.047 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 326 _refine_ls_number_reflns 3949 _refine_ls_number_restraints 40 _refine_ls_restrained_S_all 1.063 _refine_ls_R_factor_all 0.0763 _refine_ls_R_factor_gt 0.0570 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1040P)^2^+0.0918P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1642 _refine_ls_wR_factor_ref 0.1847 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2883 _reflns_number_total 3949 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1sc05741c2.cif _cod_data_source_block zzy119 _cod_original_cell_volume 1107.47(8) _cod_database_code 1565153 _shelx_shelxl_version_number 2014/7 _chemical_oxdiff_formula C14H15N2O4 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.938 _shelx_estimated_absorpt_t_min 0.859 _reflns_odcompleteness_completeness 99.92 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All N(H) groups 2. Restrained distances C21A-N4 1.45 with sigma of 0.02 C25A-C24A 1.52 with sigma of 0.02 C24A-C23A 1.52 with sigma of 0.02 C26A-C25A 1.52 with sigma of 0.02 3. Uiso/Uaniso restraints and constraints Uanis(N4) \\sim Ueq, Uanis(C22) \\sim Ueq, Uanis(C26) \\sim Ueq, Uanis(C25) \\sim Ueq, Uanis(C24) \\sim Ueq, Uanis(C23) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C20) = Uanis(C20A) Uanis(C21) = Uanis(C21A) Uanis(N4) = Uanis(N4A) Uanis(C22) = Uanis(C22A) Uanis(C23) = Uanis(C23A) Uanis(C24) = Uanis(C24A) Uanis(C25) = Uanis(C25A) Uanis(C26) = Uanis(C26A) 4. Others Sof(N4A)=Sof(C20A)=Sof(H20A)=Sof(C21A)=Sof(H21A)=Sof(C22A)=Sof(H22C)= Sof(H22D)=Sof(C23A)=Sof(H23C)=Sof(H23D)=Sof(C24A)=Sof(H24C)=Sof(H24D)= Sof(C25A)=Sof(H25C)=Sof(H25D)=Sof(C26A)=Sof(H26C)=Sof(H26D)=1-FVAR(1) Sof(N4)=Sof(C20)=Sof(H20)=Sof(C21)=Sof(H21)=Sof(C22)=Sof(H22A)=Sof(H22B)= Sof(C23)=Sof(H23A)=Sof(H23B)=Sof(C24)=Sof(H24A)=Sof(H24B)=Sof(C25)=Sof(H25A)= Sof(H25B)=Sof(C26)=Sof(H26A)=Sof(H26B)=FVAR(1) 5.a Ternary CH refined with riding coordinates: C9(H9) 5.b Secondary CH2 refined with riding coordinates: C10(H10A,H10B), C22(H22A,H22B), C22A(H22C,H22D), C23(H23A,H23B), C23A(H23C, H23D), C24(H24A,H24B), C24A(H24C,H24D), C25(H25A,H25B), C25A(H25C,H25D), C26(H26A,H26B), C26A(H26C,H26D) 5.c Aromatic/amide H refined with riding coordinates: N1(H1), C5(H5), C6(H6), C7(H7), C8(H8), C13(H13), C14(H14), C15(H15), C16(H16), C17(H17), C20(H20), C20A(H20A), C21(H21), C21A(H21A) ; _shelx_res_file ; zzy119.res created by SHELXL-2014/7 TITL zzy119 in P-1 #2 REM reset to P-1 #2 CELL 1.54184 9.52155 10.782304 12.633213 106.1775 93.8002 114.6144 ZERR 2 0.000264 0.000403 0.000527 0.0035 0.0028 0.0031 LATT 1 SFAC C H N O UNIT 52 52 8 6 EQIV $1 2-X,1-Y,1-Z DFIX 1.45 C21A N4 DFIX 1.52 C25A C24A DFIX 1.52 C24A C23A DFIX 1.52 C26A C25A ISOR 0.01 0.02 N4 C22 C26 C25 C24 C23 EADP C20 C20A EADP C21 C21A EADP N4 N4A EADP C22 C22A EADP C23 C23A EADP C24 C24A EADP C25 C25A EADP C26 C26A L.S. 19 0 0 PLAN 20 SIZE 0.22 0.1 0.09 MPLA C1 C2 C3 C4 C5 C6 C7 C8 N1 MPLA C11 C12 C13 C14 C15 C16 HTAB N1 O1_$1 BOND $h conf fmap 2 ACTA REM REM REM WGHT 0.104000 0.091800 FVAR 8.78794 0.76261 O1 4 0.897379 0.312074 0.506916 11.00000 0.05014 0.05212 = 0.09270 0.03287 -0.00441 0.01348 O2 4 0.590068 -0.333300 0.141119 11.00000 0.19853 0.06381 = 0.09388 0.00842 0.01972 0.07958 O3 4 0.833474 -0.179854 0.224268 11.00000 0.14591 0.08901 = 0.13025 0.06168 0.07947 0.08705 N1 3 0.837313 0.406851 0.378492 11.00000 0.05033 0.03995 = 0.08213 0.02619 0.01166 0.01649 AFIX 43 H1 2 0.903880 0.496365 0.411983 11.00000 -1.20000 AFIX 0 N2 3 0.442767 -0.055882 0.316259 11.00000 0.05648 0.04061 = 0.05940 0.01470 0.00526 0.01485 N3 3 0.691262 -0.211893 0.200523 11.00000 0.15322 0.06633 = 0.07265 0.03933 0.04912 0.07394 PART 1 N4 3 1.108041 0.204570 0.150846 21.00000 0.09553 0.10321 = 0.12236 0.06827 0.06156 0.06476 PART 0 PART 2 N4A 3 1.056673 0.168523 0.108190 -21.00000 0.09553 0.10321 = 0.12236 0.06827 0.06156 0.06476 PART 0 C1 1 0.821366 0.299582 0.418993 11.00000 0.04060 0.04450 = 0.07547 0.02678 0.01336 0.01891 C2 1 0.691707 0.156339 0.334951 11.00000 0.05288 0.03959 = 0.05733 0.02143 0.01779 0.02275 C3 1 0.640637 0.205488 0.245924 11.00000 0.06871 0.04219 = 0.05358 0.02026 0.02339 0.03126 C4 1 0.732729 0.355323 0.275494 11.00000 0.05814 0.04589 = 0.06308 0.02359 0.02505 0.02972 C5 1 0.717418 0.432515 0.209294 11.00000 0.07837 0.04719 = 0.07755 0.03269 0.03238 0.03652 AFIX 43 H5 2 0.779777 0.532156 0.230971 11.00000 -1.20000 AFIX 0 C6 1 0.606642 0.357385 0.109780 11.00000 0.11909 0.06836 = 0.06148 0.03488 0.03029 0.05912 AFIX 43 H6 2 0.593593 0.406838 0.063280 11.00000 -1.20000 AFIX 0 C7 1 0.514579 0.209289 0.078168 11.00000 0.13042 0.06464 = 0.04876 0.01786 0.00969 0.05099 AFIX 43 H7 2 0.440991 0.160499 0.010293 11.00000 -1.20000 AFIX 0 C8 1 0.529911 0.131508 0.146156 11.00000 0.10554 0.04311 = 0.05275 0.01212 0.01290 0.03271 AFIX 43 H8 2 0.466815 0.031994 0.124604 11.00000 -1.20000 AFIX 0 C9 1 0.560482 0.084360 0.395091 11.00000 0.04537 0.03951 = 0.04778 0.01704 0.00711 0.01673 AFIX 13 H9 2 0.608411 0.067321 0.457201 11.00000 -1.20000 AFIX 0 C10 1 0.279286 -0.082299 0.318259 11.00000 0.04855 0.06776 = 0.08051 0.02965 -0.00436 0.01157 AFIX 23 H10A 2 0.223989 -0.162595 0.344557 11.00000 -1.20000 H10B 2 0.221899 -0.101663 0.244433 11.00000 -1.20000 AFIX 0 C11 1 0.301530 0.057860 0.399984 11.00000 0.05109 0.07176 = 0.06759 0.04086 0.00962 0.02778 C12 1 0.459790 0.155128 0.439770 11.00000 0.05056 0.05479 = 0.05042 0.02619 0.01385 0.02716 C13 1 0.504749 0.291434 0.516482 11.00000 0.06902 0.06358 = 0.05929 0.01713 0.01847 0.03394 AFIX 43 H13 2 0.611082 0.357500 0.542326 11.00000 -1.20000 AFIX 0 C14 1 0.389910 0.328510 0.554391 11.00000 0.10403 0.09154 = 0.07906 0.03192 0.03751 0.06560 AFIX 43 H14 2 0.419096 0.420316 0.605500 11.00000 -1.20000 AFIX 0 C15 1 0.232524 0.230191 0.516855 11.00000 0.09350 0.12097 = 0.10691 0.06229 0.04760 0.07765 AFIX 43 H15 2 0.156430 0.255602 0.544167 11.00000 -1.20000 AFIX 0 C16 1 0.186426 0.094746 0.439401 11.00000 0.05318 0.11140 = 0.11095 0.06601 0.02390 0.04547 AFIX 43 H16 2 0.079963 0.028975 0.413858 11.00000 -1.20000 AFIX 0 C17 1 0.491529 -0.144570 0.252792 11.00000 0.08978 0.03687 = 0.05396 0.01536 0.00676 0.02450 AFIX 43 H17 2 0.418103 -0.238856 0.210234 11.00000 -1.20000 AFIX 0 C18 1 0.645298 -0.100557 0.248891 11.00000 0.10553 0.04867 = 0.05736 0.02699 0.03006 0.04805 C19 1 0.769357 0.052077 0.295245 11.00000 0.07671 0.05481 = 0.08711 0.03998 0.04115 0.04239 H19 2 0.833689 0.068823 0.362906 11.00000 -1.20000 PART 1 C20 1 0.855202 0.087775 0.199671 21.00000 0.07282 0.05156 = 0.06001 0.02161 0.02501 0.03510 AFIX 43 H20 2 0.798120 0.055849 0.126686 21.00000 -1.20000 AFIX 0 PART 0 PART 2 C20A 1 0.930913 0.139477 0.270636 -21.00000 0.07282 0.05156 = 0.06001 0.02161 0.02501 0.03510 AFIX 43 H20A 2 1.016848 0.206857 0.328801 -21.00000 -1.20000 AFIX 0 PART 0 PART 1 C21 1 1.008137 0.162979 0.222909 21.00000 0.08672 0.09161 = 0.09555 0.05969 0.04332 0.05936 AFIX 43 H21 2 1.057029 0.192858 0.297916 21.00000 -1.20000 AFIX 0 PART 0 PART 2 C21A 1 0.942901 0.116353 0.167810 -21.00000 0.08672 0.09161 = 0.09555 0.05969 0.04332 0.05936 AFIX 43 H21A 2 0.848467 0.044117 0.119701 -21.00000 -1.20000 AFIX 0 PART 0 PART 1 C22 1 1.042803 0.188627 0.036507 21.00000 0.11863 0.08889 = 0.10081 0.04310 0.05849 0.04948 AFIX 23 H22A 2 0.952416 0.093918 0.003250 21.00000 -1.20000 H22B 2 1.121758 0.192889 -0.008993 21.00000 -1.20000 AFIX 0 PART 0 PART 2 C22A 1 0.986439 0.170124 0.000328 -21.00000 0.11863 0.08889 = 0.10081 0.04310 0.05849 0.04948 AFIX 23 H22C 2 1.032836 0.139154 -0.061547 -21.00000 -1.20000 H22D 2 0.872482 0.112913 -0.019489 -21.00000 -1.20000 AFIX 0 PART 0 PART 1 C23 1 0.989862 0.308455 0.032663 21.00000 0.12559 0.09986 = 0.11025 0.04855 0.03075 0.05910 AFIX 23 H23A 2 0.960606 0.301123 -0.044672 21.00000 -1.20000 H23B 2 0.899931 0.297060 0.067978 21.00000 -1.20000 AFIX 0 PART 0 PART 2 C23A 1 1.031939 0.314793 0.034373 -21.00000 0.12559 0.09986 = 0.11025 0.04855 0.03075 0.05910 AFIX 23 H23C 2 0.970929 0.328446 0.091132 -21.00000 -1.20000 H23D 2 0.984888 0.327102 -0.029993 -21.00000 -1.20000 AFIX 0 PART 0 PART 1 C24 1 1.129504 0.452339 0.095999 21.00000 0.13828 0.08787 = 0.13063 0.06669 0.04120 0.03874 AFIX 23 H24A 2 1.097744 0.528490 0.103848 21.00000 -1.20000 H24B 2 1.211462 0.468567 0.052339 21.00000 -1.20000 AFIX 0 PART 0 PART 2 C24A 1 1.187952 0.450534 0.079692 -21.00000 0.13828 0.08787 = 0.13063 0.06669 0.04120 0.03874 AFIX 23 H24C 2 1.262508 0.447237 0.031575 -21.00000 -1.20000 H24D 2 1.174093 0.536446 0.086727 -21.00000 -1.20000 AFIX 0 PART 0 PART 1 C25 1 1.197573 0.462749 0.212931 21.00000 0.13158 0.10561 = 0.12173 0.06165 0.03247 0.03765 AFIX 23 H25A 2 1.289978 0.555785 0.247520 21.00000 -1.20000 H25B 2 1.119903 0.457970 0.259645 21.00000 -1.20000 AFIX 0 PART 0 PART 2 C25A 1 1.241846 0.447837 0.193035 -21.00000 0.13158 0.10561 = 0.12173 0.06165 0.03247 0.03765 AFIX 23 H25C 2 1.172391 0.458169 0.243925 -21.00000 -1.20000 H25D 2 1.349518 0.521314 0.227660 -21.00000 -1.20000 AFIX 0 PART 0 PART 1 C26 1 1.243149 0.343555 0.209083 21.00000 0.09616 0.13387 = 0.12942 0.07598 0.04979 0.04829 AFIX 23 H26A 2 1.329600 0.354130 0.170036 21.00000 -1.20000 H26B 2 1.277926 0.349633 0.285100 21.00000 -1.20000 AFIX 0 PART 0 PART 2 C26A 1 1.228427 0.296528 0.155696 -21.00000 0.09616 0.13387 = 0.12942 0.07598 0.04979 0.04829 AFIX 23 H26C 2 1.276233 0.283635 0.219410 -21.00000 -1.20000 H26D 2 1.289799 0.289316 0.098033 -21.00000 -1.20000 AFIX 0 HKLF 4 REM zzy119 in P-1 #2 REM R1 = 0.0570 for 2883 Fo > 4sig(Fo) and 0.0763 for all 3949 data REM 326 parameters refined using 40 restraints END WGHT 0.1037 0.0896 REM Highest difference peak 0.334, deepest hole -0.206, 1-sigma level 0.041 Q1 1 1.1057 0.3514 0.3521 11.00000 0.05 0.33 Q2 1 0.7005 0.2846 0.2537 11.00000 0.05 0.20 Q3 1 1.0000 0.5000 0.0000 10.50000 0.05 0.18 Q4 1 0.6489 0.1323 0.3671 11.00000 0.05 0.16 Q5 1 0.6790 -0.2661 0.1225 11.00000 0.05 0.15 Q6 1 0.3873 0.1348 0.3998 11.00000 0.05 0.15 Q7 1 0.3966 0.0247 0.1484 11.00000 0.05 0.15 Q8 1 0.9180 0.3615 0.5594 11.00000 0.05 0.14 Q9 1 0.4776 0.2039 0.4843 11.00000 0.05 0.14 Q10 1 0.7197 0.1031 0.3047 11.00000 0.05 0.14 Q11 1 0.7458 0.2032 0.3815 11.00000 0.05 0.14 Q12 1 0.6288 0.1754 0.1868 11.00000 0.05 0.14 Q13 1 0.8560 0.2241 0.5036 11.00000 0.05 0.14 Q14 1 0.9211 -0.1257 0.2114 11.00000 0.05 0.13 Q15 1 0.2413 0.0654 0.4032 11.00000 0.05 0.13 Q16 1 0.5196 0.3191 0.1290 11.00000 0.05 0.13 Q17 1 0.9676 0.3514 0.4730 11.00000 0.05 0.12 Q18 1 0.3974 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352.920 83.8967 23 0 -8 13 968.325 161.273 26 0 -8 12 72.3166 103.915 26 0 -8 11 2151.62 249.146 26 0 -8 10 1020.58 190.587 26 0 -8 9 60.7435 105.198 26 0 -8 9 402.936 209.433 20 0 -8 8 2333.96 298.851 20 0 -8 8 1964.39 248.228 26 0 -8 7 10348.9 555.673 20 0 -8 6 85.6998 86.3471 18 0 -8 6 436.144 191.652 20 0 -8 5 5980.65 387.411 18 0 -8 5 6684.89 454.881 20 0 -8 4 3826.23 339.004 16 0 -8 4 3687.86 369.922 20 0 -8 3 1120.27 200.763 16 0 -8 3 1703.82 283.454 20 0 -8 2 4552.40 368.649 16 0 -8 2 4750.08 366.976 17 0 -8 1 3290.53 320.532 17 0 -8 1 4300.90 357.320 16 0 -8 0 22850.4 796.560 25 0 -8 0 23661.2 834.406 17 0 -8 -1 398.405 130.652 17 0 -8 -1 438.385 139.293 25 0 -8 -2 12.0746 87.4013 18 0 -8 -2 226.432 122.550 17 0 -8 -3 707.728 167.665 17 0 -8 -3 793.383 153.919 18 0 -8 -4 55.5382 92.3129 17 0 -8 -4-100.973 78.5909 18 0 -8 -5 440.780 130.436 17 0 -8 -6 130.502 85.0585 17 0 -9 12 217.592 105.675 26 0 -9 12 241.137 85.3124 18 0 -9 11 1675.57 203.550 26 0 -9 11 1680.38 188.591 18 0 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115.057 17 1 -8 -2 458.163 143.918 25 1 -8 -1-83.2480 137.615 25 1 -8 -1 48.1433 96.7998 17 1 -8 0 9804.73 522.625 25 1 -8 0 10632.0 548.282 17 1 -8 1 1864.01 237.946 17 1 -8 1 1560.51 223.705 16 1 -8 2 4942.25 359.637 17 1 -8 2 4410.00 359.399 16 1 -8 3 12524.5 1172.71 13 1 -8 3 13214.2 589.926 20 1 -8 3 12296.8 588.630 16 1 -8 4 11852.5 556.628 27 1 -8 4 11596.9 570.050 16 1 -8 5 1593.46 241.546 20 1 -8 6 2531.93 288.579 20 1 -8 7 1717.57 246.188 20 1 -8 8 136.972 148.084 20 1 -8 8-32.2886 112.904 26 1 -8 9 123.499 113.117 26 1 -8 9 284.213 165.388 20 1 -8 10 1211.00 207.247 26 1 -8 11 1977.48 256.571 26 1 -8 12 556.187 152.380 26 1 -8 13 8136.45 411.994 26 1 -7 -8 344.896 98.3492 23 1 -7 -7 1740.55 215.760 19 1 -7 -7 1988.98 216.490 23 1 -7 -6 442.076 141.235 17 1 -7 -6 490.429 135.618 23 1 -7 -5 7682.07 464.610 17 1 -7 -4 7330.22 462.211 17 1 -7 -3 4546.91 368.310 17 1 -7 -2 281.388 116.298 25 1 -7 -2 193.810 109.520 17 1 -7 -1 5007.97 732.418 5 1 -7 -1 3016.80 579.734 13 1 -7 0 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442.499 17 1 -6 -6 7317.79 443.001 23 1 -6 -5 27533.1 860.145 17 1 -6 -4 119.913 86.3338 17 1 -6 -3 917.424 334.220 13 1 -6 -2 9344.79 959.611 13 1 -6 -1 1052.64 299.769 5 1 -6 -1 1535.00 408.754 13 1 -6 0 135.476 176.432 13 1 -6 0 157.013 144.205 6 1 -6 0 221.522 214.753 5 1 -6 1 2693.39 467.077 13 1 -6 1 3163.18 521.996 5 -1 6 -1 3345.38 528.892 9 1 -6 1 3456.91 527.373 6 1 -6 2-321.380 201.756 6 -1 6 -2 380.796 203.998 9 1 -6 2-40.8590 144.781 5 1 -6 2 145.122 145.455 13 1 -6 3 221.853 179.489 13 1 -6 3 680.615 254.812 5 -1 6 -3 687.833 283.121 9 1 -6 3 237.119 183.765 8 1 -6 3 604.099 237.154 6 -1 6 -4 20471.4 1373.17 9 1 -6 4 19389.1 1231.72 5 1 -6 4 19742.1 1273.06 6 1 -6 4 20737.8 1294.89 8 1 -6 4 19710.7 1105.20 13 1 -6 5 389.210 224.698 8 1 -6 5 127.995 160.410 6 -1 6 -5 54.2282 231.427 9 1 -6 5 225.587 157.354 5 -1 6 -5-5.66246 140.296 7 -1 6 -6 2018.10 444.034 7 -1 6 -6 2058.73 540.373 9 1 -6 6 1791.58 422.743 6 1 -6 6 2135.95 463.892 8 -1 6 -7 558.714 285.218 7 1 -6 7 100.081 165.983 6 1 -6 7 247.384 216.290 8 1 -6 8 3444.52 581.416 6 1 -6 8 3535.91 650.903 8 -1 6 -8 3751.73 670.394 7 -1 6 -8 1938.74 522.011 9 1 -6 9 6404.23 422.645 26 1 -6 10 29489.0 922.055 26 1 -6 11 16830.8 704.167 26 1 -6 12 32.2381 103.182 26 1 -6 13 467.703 146.267 26 1 -6 14 77.1061 93.5295 26 1 -5 -11 483.211 104.328 23 1 -5 -10 279.721 102.186 23 1 -5 -9-34.8878 82.3342 23 1 -5 -8 11039.9 554.392 23 1 -5 -7 979.610 184.330 23 1 -5 -7 954.473 168.181 18 1 -5 -6 182.221 103.025 18 1 -5 -5 330.301 245.694 13 -1 5 5 337.442 274.229 3 -1 5 4 9006.05 962.322 3 1 -5 -4 6221.09 776.435 13 1 -5 -3 2087.12 441.918 13 -1 5 3 2050.98 456.631 3 -1 5 2 7482.73 750.377 3 1 -5 -2 7583.09 704.424 5 1 -5 -2 6890.19 736.934 13 1 -5 -1 44668.2 1766.98 13 -1 5 1 43744.1 1612.19 3 1 -5 -1 41944.8 1609.68 5 1 -5 0 2475.99 412.914 13 1 -5 0 2421.77 409.542 5 -1 5 0 2299.45 352.344 3 -1 5 0 2585.65 410.613 9 1 -5 0 3007.76 432.498 6 1 -5 1 7110.07 655.949 13 1 -5 1 6902.07 649.908 6 1 -5 1 6809.78 649.470 5 -1 5 -1 6510.69 627.472 9 1 -5 2 2096.17 385.255 6 -1 5 -2 2010.61 395.168 9 1 -5 2 2038.85 356.819 13 1 -5 2 1579.73 354.912 8 1 -5 2 1664.90 339.026 5 1 -5 3 3911.65 507.632 6 1 -5 3 3210.57 469.898 8 1 -5 3 3714.94 491.196 5 -1 5 -3 3723.88 424.208 7 1 -5 3 3433.14 422.598 13 1 -5 4 11479.5 877.181 6 -1 5 -4 10569.4 779.074 7 1 -5 4 10264.0 831.007 8 1 -5 4 10453.8 684.327 13 1 -5 4 9423.62 771.154 5 1 -5 5 6768.05 696.579 6 1 -5 5 5842.66 656.294 8 -1 5 -5 6719.93 690.641 7 1 -5 6 957.310 283.425 6 -1 5 -6 816.386 323.861 7 1 -5 6 1643.95 405.739 8 -1 5 -7 24549.6 1520.44 7 1 -5 7 22283.1 1451.67 8 1 -5 7 22781.8 1329.83 6 1 -5 8-2.31407 152.982 8 -1 5 -8 275.592 256.007 7 -1 5 -9 11210.4 1170.99 9 1 -5 9 12069.2 565.080 26 1 -5 10 31.9707 109.250 26 1 -5 11 623.591 173.738 26 1 -5 12 255.941 134.339 26 1 -5 13 160.880 113.940 26 1 -5 14 386.941 113.716 26 1 -4 -12 426.467 97.6057 23 1 -4 -11 280.446 106.038 23 1 -4 -10 8666.29 475.302 23 1 -4 -9 1143.07 194.673 23 1 -4 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6 1 -4 2 2167.57 328.606 5 -1 4 -2 1947.00 224.700 12 1 -4 3 72.8058 121.278 5 -1 4 -3 260.625 132.490 12 1 -4 3 327.976 190.733 6 1 -4 3 202.914 167.965 8 -1 4 -3 297.954 173.116 7 1 -4 3 111.215 77.0319 11 1 -4 3 246.762 134.528 13 -1 4 -4 97452.8 2072.17 12 -1 4 -4 99108.2 2238.10 7 1 -4 4 96875.9 2235.02 6 1 -4 4 97668.3 2296.94 8 1 -4 4 89724.8 2090.15 5 -1 4 -5 83875.0 2275.54 7 -1 4 -5 84789.9 2229.38 12 1 -4 5 82810.7 2274.14 8 1 -4 5 79674.9 2085.15 6 -1 4 -6 59286.6 2102.37 7 1 -4 6 60792.2 2111.19 8 1 -4 6 59230.6 1862.14 6 -1 4 -6 61630.0 2132.62 12 -1 4 -7 142884. 3552.42 12 -1 4 -7 139560. 3480.20 7 1 -4 7 137070. 2913.62 6 1 -4 7 143758. 3484.39 8 -1 4 -8 970.594 336.428 7 -1 4 -8 517.079 307.086 12 1 -4 8 1136.85 369.618 8 1 -4 9 1385.81 422.300 8 -1 4 -9 126.817 226.461 7 -1 4 -9 1165.68 407.468 12 1 -4 10 6505.26 426.168 26 1 -4 10 6599.78 410.025 28 1 -4 11 2997.05 292.154 28 1 -4 11 2656.55 292.339 26 1 -4 12 173.297 117.570 26 1 -4 12 222.770 123.287 28 1 -4 13 17.8724 90.9238 26 1 -4 13 21.5038 82.9019 28 1 -4 14-76.6375 92.3666 28 -1 3 12 767.256 126.066 28 1 -3 -12 843.538 146.511 23 1 -3 -11 247.731 106.849 23 -1 3 11 357.678 112.068 28 -1 3 10 2639.60 263.319 28 1 -3 -10 2328.40 268.508 23 -1 3 9-117.362 121.921 28 1 -3 -9 60.2944 85.3746 23 -1 3 8 193.718 105.524 28 1 -3 -8 75.7063 79.1104 23 1 -3 -7 983.643 322.972 11 -1 3 7 1809.16 497.542 3 -1 3 6 1600.31 451.110 3 1 -3 -5 179.942 185.311 13 -1 3 5-46.9569 176.476 3 1 -3 -4 2094.30 321.859 2 1 -3 -4 1614.44 319.328 13 -1 3 4 2111.68 430.502 3 1 -3 -3 214.221 162.222 13 -1 3 3-18.4710 164.094 3 1 -3 -3 117.075 122.498 2 1 -3 -3-73.1538 99.9608 5 1 -3 -2 71879.5 1293.18 14 1 -3 -2 67289.8 1711.15 13 -1 3 2 67774.0 1763.62 3 1 -3 -2 69458.5 1584.71 2 1 -3 -2 66341.8 1458.05 5 1 -3 -1 31102.3 1093.59 13 -1 3 1 33604.6 1077.97 3 1 -3 -1 33817.2 1070.18 2 -1 3 1 30160.6 839.228 9 1 -3 -1 31323.8 996.438 5 1 -3 0 135697. 2058.62 5 1 -3 0 140920. 2117.27 6 1 -3 0 141280. 2148.23 2 -1 3 0 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10 14549.3 609.705 28 1 -3 10 14807.7 625.148 26 1 -3 11 917.632 179.497 28 1 -3 11 738.995 163.065 26 1 -3 12 17740.3 683.598 26 1 -3 12 16579.7 663.722 28 1 -3 13 289.558 122.954 28 1 -3 14 536.159 127.548 28 1 -2 -13 214.499 79.9578 23 -1 2 13 215.703 87.8006 28 1 -2 -12 713.954 144.731 23 -1 2 12 816.840 155.649 28 1 -2 -11 527.797 138.563 23 -1 2 11 322.055 117.373 28 -1 2 10 194.838 112.031 28 1 -2 -10 232.693 105.623 23 1 -2 -9 27.1332 79.4923 23 -1 2 9 104.698 102.177 28 -1 2 8 3659.46 735.728 3 -1 2 7 1785.62 468.367 3 -1 2 6 45986.5 2019.09 3 1 -2 -6 48380.5 1818.69 11 -1 2 5 6183.26 693.391 3 1 -2 -5 5321.52 522.989 2 1 -2 -5 5933.47 530.322 13 -1 2 4 21355.0 1140.94 3 1 -2 -4 23831.8 984.518 13 1 -2 -4 23730.6 1000.58 2 1 -2 -3 15338.5 728.122 2 -1 2 3 14257.9 823.085 3 1 -2 -3 15093.2 523.414 14 1 -2 -3 14776.8 519.958 5 1 -2 -3 14537.0 725.592 13 1 -2 -3 15932.1 513.004 7 1 -2 -2 104.313 89.5775 5 -1 2 2 101.237 150.567 3 1 -2 -2 148.952 52.6747 7 1 -2 -2 92.8422 71.1286 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224.623 7 -1 2 -9 519.864 358.362 12 1 -2 10 427.053 134.094 28 1 -2 11 8330.11 480.980 28 1 -2 12 999.635 189.068 28 1 -2 13 210.711 106.221 28 1 -2 14 288.777 96.0069 28 -1 1 13 336.361 107.760 28 1 -1 -13 481.479 112.905 23 -1 1 12 1982.90 240.603 28 1 -1 -12 2330.29 252.602 23 -1 1 11 46.0013 88.3245 28 1 -1 -11 71.5019 80.5262 23 -1 1 10-101.823 95.3073 28 1 -1 -10-90.6747 82.0899 23 1 -1 -9 201.769 109.075 23 -1 1 9-84.8241 96.8687 28 -1 1 8 1094.37 404.724 3 -1 1 7 10289.7 999.925 3 1 -1 -6-508.506 196.379 11 1 -1 -6 63.4280 169.372 2 1 -1 -6 38.4309 181.379 7 -1 1 6-245.143 216.250 3 1 -1 -5 11340.4 694.009 7 1 -1 -5 11471.4 723.354 11 -1 1 5 10869.8 826.844 3 1 -1 -5 11445.5 770.970 2 -1 1 4 16949.7 920.555 3 1 -1 -4 18679.3 883.183 2 1 -1 -4 17874.0 707.448 13 1 -1 -3 40196.5 1143.56 2 1 -1 -3 40176.7 977.893 13 -1 1 3 38911.1 1216.05 3 1 -1 -3 41586.7 956.514 7 1 -1 -2 46926.5 964.231 13 1 -1 -2 48838.8 819.369 7 -1 1 2 48196.6 1119.28 3 1 -1 -2 50092.4 1110.59 2 1 -1 -1 2089.20 203.689 1 1 -1 -1 2203.18 138.754 7 1 -1 -1 2419.43 220.020 2 1 -1 0 69032.2 954.073 1 1 -1 0 70434.6 983.425 2 1 -1 1 392331. 2254.29 2 1 -1 1 390838. 2041.28 8 1 -1 1 388696. 2371.56 1 1 -1 2 166139. 1835.06 3 1 -1 2 164100. 1630.07 14 1 -1 3 816623. 3985.46 14 -1 1 -3 819317. 3809.15 10 1 -1 3 829245. 4960.50 3 -1 1 -4 8177.62 660.581 12 1 -1 4 8406.65 595.772 3 -1 1 -4 8325.23 439.770 10 1 -1 4 8508.84 592.199 4 1 -1 5 57218.4 1710.21 4 -1 1 -5 58001.7 1280.36 10 -1 1 -5 58059.9 1942.89 12 1 -1 5 56100.1 1709.08 3 1 -1 6 12299.4 898.260 4 1 -1 6 12020.6 896.646 3 -1 1 -6 12891.0 1024.96 12 -1 1 -7 6621.81 823.508 12 1 -1 7 6904.09 750.884 3 -1 1 -8 3687.78 683.645 12 1 -1 8 3808.17 631.998 3 -1 1 -8 4123.49 633.983 7 -1 1 -9 10609.0 1055.93 7 1 -1 9 10988.2 1114.21 3 1 -1 9 10755.0 514.283 28 1 -1 10 192.116 111.966 28 1 -1 11 2199.31 259.505 28 1 -1 12 1859.16 234.782 28 1 -1 13 12.5727 80.4354 28 1 -1 14 85.2104 79.3581 28 -1 0 14 1043.85 155.204 28 -1 0 13 341.320 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7 -1 -1 7 4629.96 575.908 3 -1 -1 6-1.12475 134.293 3 1 1 -6 117.664 160.531 7 1 1 -6-142.870 241.232 12 1 1 -6 397.082 161.722 9 -1 -1 5 26392.1 1035.84 3 1 1 -5 27138.1 1166.08 7 1 1 -5 29715.0 1054.11 9 1 1 -5 28724.0 1257.78 12 1 1 -4 17738.6 868.147 12 -1 -1 4 18587.3 533.373 5 1 1 -4 18087.4 855.621 7 -1 -1 4 18576.8 742.926 3 1 1 -3 153028. 2147.54 12 -1 -1 3 156313. 1689.18 5 -1 -1 3 154414. 1731.76 3 -1 -1 2 89189.7 1334.04 8 1 1 -2 91520.1 1537.09 9 1 1 -1 23613.7 478.630 1 -1 -1 1 23561.8 600.145 8 1 1 0 97935.8 1359.05 7 1 1 0 98920.7 1295.73 3 1 1 1 19403.3 731.523 3 1 1 1 19031.9 592.315 4 -1 -1 -1 20364.7 628.856 12 1 1 1 19700.5 706.955 15 1 1 2 39993.2 1008.61 15 -1 -1 -2 38564.2 1177.76 10 1 1 2 40281.8 1233.33 3 -1 -1 -2 37369.5 623.863 6 1 1 2 40027.7 978.737 4 1 1 3 162.773 105.354 15 1 1 3 53.1011 156.367 3 -1 -1 -3 127.056 46.5536 2 -1 -1 -3 81.8132 133.045 12 -1 -1 -3 126.600 142.355 10 1 1 3 126.118 124.732 4 -1 -1 -4 4348.24 480.028 10 -1 -1 -4 5204.23 448.151 13 -1 -1 -4 5176.13 566.435 12 1 1 4 5132.89 470.695 4 1 1 4 4140.06 533.763 3 1 1 5 5451.57 648.007 3 -1 -1 -5 5197.41 629.677 12 -1 -1 -5 5706.61 582.605 10 1 1 5 5644.61 543.656 4 1 1 6 2083.34 483.907 3 -1 -1 -6 2087.55 452.129 12 -1 -1 -6 1779.19 371.430 10 1 1 7 1999.72 491.592 3 -1 -1 -7 2718.23 564.039 12 -1 -1 -8 2216.81 251.980 18 -1 -1 -8 2396.93 574.301 12 1 1 9 280.990 122.466 28 -1 -1 -10 1.73730 71.8122 23 1 1 10-50.3624 94.5048 28 -1 -1 -11 87.5856 81.1412 23 1 1 11 23.7174 86.1137 28 1 1 12 11.6706 68.8190 28 -1 -1 -12 11.6256 77.2384 23 1 1 13 717.421 127.312 28 -1 -1 -13 489.765 101.352 23 -1 -2 14 211.383 102.809 28 1 2 -14 215.366 109.038 22 -1 -2 13 3305.30 298.907 28 -1 -2 12 1558.31 230.744 28 -1 -2 11 1719.42 235.735 28 -1 -2 10 76.9029 95.8154 28 1 2 -9 350.473 247.613 7 1 2 -8 38373.1 1890.26 7 1 2 -7 1715.30 411.610 7 1 2 -7 1377.54 381.802 12 1 2 -6 6068.07 647.631 7 -1 -2 6 6423.97 572.194 6 1 2 -6 6324.11 615.548 9 1 2 -6 5683.21 633.957 12 1 2 -5 248.235 180.236 7 -1 -2 5 379.263 146.324 3 1 2 -5 392.013 194.147 12 1 2 -5 218.631 162.567 9 1 2 -4 8719.47 642.401 9 -1 -2 4 8254.08 396.585 3 1 2 -4 8313.35 575.744 12 1 2 -4 8005.70 619.126 7 -1 -2 4 8274.60 591.472 8 -1 -2 3 109922. 1006.40 3 1 2 -3 112675. 2120.89 9 1 2 -3 109082. 2002.93 7 -1 -2 3 111719. 1944.22 8 -1 -2 2 13012.1 612.649 8 1 2 -2 13215.0 657.748 7 -1 -2 2 13037.3 579.468 10 1 2 -1 148244. 2006.24 7 1 2 -1 148342. 1286.27 1 -1 -2 1 151178. 2008.78 8 -1 -2 0 10295.7 608.230 10 1 2 0 8778.79 425.763 4 -1 -2 0 9564.45 292.653 12 1 2 0 9684.92 502.770 3 1 2 0 9453.88 495.241 7 -1 -2 -1 1995.63 232.446 6 -1 -2 -1 2434.39 241.461 12 -1 -2 -1 2011.20 321.786 10 1 2 1 2104.59 300.489 3 1 2 1 2093.35 216.382 4 1 2 1 2629.78 339.132 15 1 2 2 37430.6 1148.78 15 -1 -2 -2 36150.2 847.038 6 -1 -2 -2 36355.9 1335.42 10 1 2 2 37350.4 1319.57 3 1 2 2 37186.1 959.738 4 -1 -2 -3 55063.8 1611.90 12 1 2 3 55184.3 1391.72 15 -1 -2 -3 53654.0 1720.70 10 1 2 3 53802.1 1765.51 3 1 2 3 54792.8 1317.90 4 -1 -2 -4 28839.6 1377.16 10 -1 -2 -4 29234.0 1248.21 13 -1 -2 -4 30566.2 1388.91 12 1 2 4 27211.5 1406.33 3 -1 -2 -5 32262.4 1564.91 10 -1 -2 -5 35603.6 1669.58 12 -1 -2 -6 2758.48 551.263 12 1 2 6 2683.22 547.485 3 1 2 7 90.8054 189.495 3 1 2 8-42.0920 91.9821 28 -1 -2 -8-38.3112 96.5050 18 1 2 9 2722.27 278.750 28 1 2 10 2900.82 279.911 28 -1 -2 -10 2486.77 270.474 23 1 2 11 92.8934 91.7519 28 -1 -2 -11 143.413 93.6236 23 -1 -2 -12-22.0761 67.3691 23 1 2 12 42.3938 69.8568 28 1 3 -15 17.5286 58.7416 22 1 3 -14 672.915 141.934 22 -1 -3 13 973.756 180.134 28 -1 -3 12 1568.94 221.438 28 -1 -3 12 2007.07 248.275 26 -1 -3 11 685.332 180.188 26 -1 -3 11 554.696 151.043 28 -1 -3 10 738.626 165.461 28 -1 -3 10 841.567 184.933 26 1 3 -9 2587.70 564.579 7 -1 -3 9 3908.30 663.795 8 1 3 -8 58861.2 2406.56 7 -1 -3 8 52903.8 2203.24 8 -1 -3 7 4167.52 540.449 6 -1 -3 7 4673.77 615.601 8 1 3 -7 4765.01 646.250 9 1 3 -7 5339.44 685.490 7 -1 -3 6 115572. 2670.75 6 1 3 -6 119861. 2906.44 9 -1 -3 6 118298. 2821.98 8 1 3 -6 115735. 2886.60 7 -1 -3 5 1703.79 338.174 6 -1 -3 5 2126.72 366.580 8 -1 -3 5 1983.80 314.491 5 1 3 -5 2162.45 419.529 9 1 3 -5 2275.17 397.179 7 1 3 -4 15030.9 902.164 7 -1 -3 4 15526.1 918.592 6 -1 -3 4 16483.8 864.477 5 1 3 -4 17655.0 1030.30 9 -1 -3 4 16631.4 924.809 8 -1 -3 3 73763.8 1832.83 5 -1 -3 3 75512.5 1808.13 8 1 3 -3 73457.2 1802.55 7 1 3 -3 70991.3 1963.41 9 1 3 -2 44753.2 1316.45 7 -1 -3 2 39928.7 1363.62 6 -1 -3 2 44694.4 1435.18 5 -1 -3 2 45233.5 1281.79 10 -1 -3 2 42959.6 1320.83 8 1 3 -2 43276.8 1528.57 9 1 3 -1 2740.86 320.401 7 -1 -3 1 2422.29 373.695 5 -1 -3 1 2824.78 355.913 6 1 3 -1 2643.87 202.599 1 -1 -3 1 1930.61 317.015 10 1 3 -1 2676.14 248.189 3 1 3 0 35905.1 1070.14 7 -1 -3 0 37121.3 1342.66 10 -1 -3 0 32509.6 1286.95 5 -1 -3 0 34976.6 1169.49 6 1 3 0 35754.3 895.703 4 1 3 0 37535.8 1122.70 3 1 3 1 56516.0 1699.67 15 -1 -3 -1 52152.7 1652.59 5 -1 -3 -1 57039.9 1421.04 6 1 3 1 57785.3 1618.92 3 -1 -3 -1 55416.6 1751.31 10 -1 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522.361 23 2 -5 -6 100.370 84.6429 23 2 -5 -5 1978.76 446.542 13 2 -5 -5 1870.26 457.882 11 -2 5 5 1085.90 389.139 3 -2 5 4 1237.58 378.357 3 2 -5 -4 1630.19 393.542 13 2 -5 -4 813.913 299.553 11 2 -5 -3 149.414 175.198 13 2 -5 -3 282.882 168.953 2 2 -5 -3 608.165 289.954 11 -2 5 3 332.972 234.451 3 2 -5 -2 22251.1 1287.42 13 -2 5 2 22994.2 1288.62 3 2 -5 -2 23608.7 1242.13 2 2 -5 -1 7070.56 600.268 14 2 -5 -1 6053.01 618.881 2 -2 5 1 6962.56 663.063 3 2 -5 -1 8023.56 692.392 5 2 -5 -1 6847.80 675.192 11 2 -5 -1 7541.94 716.514 13 -2 5 0 760.601 228.305 3 2 -5 0 1080.02 291.846 13 2 -5 0 760.145 247.045 5 2 -5 0 490.859 194.671 14 2 -5 0 1087.05 283.451 2 2 -5 0 997.465 261.685 11 -2 5 0 676.724 211.458 9 2 -5 1 7503.42 669.882 5 2 -5 1 7418.44 608.910 11 -2 5 -1 7881.38 560.390 3 2 -5 1 7430.02 657.976 13 2 -5 1 7569.10 681.821 6 2 -5 1 7532.55 647.946 14 2 -5 2 858.228 272.294 6 2 -5 2 852.983 240.343 8 2 -5 2 1117.16 271.429 13 2 -5 2 1160.64 207.809 1 2 -5 2 841.688 218.480 11 -2 5 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531.854 142.825 19 2 -4 -6 683.596 276.288 11 -2 4 6 656.433 379.481 3 2 -4 -5 291.984 191.932 13 2 -4 -5 162.934 182.387 11 2 -4 -4 27780.3 1343.97 2 -2 4 4 26705.5 1495.42 3 2 -4 -4 27427.9 1406.52 13 2 -4 -4 28385.1 1483.25 11 2 -4 -3 99027.6 2523.37 13 -2 4 3 97078.8 2583.27 3 2 -4 -3 95943.6 2371.86 2 2 -4 -3 98568.9 2577.64 11 -2 4 2 2083.00 376.474 3 2 -4 -2 2900.38 352.415 14 2 -4 -2 2914.53 429.032 11 2 -4 -2 2414.45 374.708 2 2 -4 -2 2970.17 429.849 13 2 -4 -1 837.718 246.517 13 -2 4 1 487.100 197.131 3 2 -4 -1 735.318 214.621 2 2 -4 -1 771.278 226.121 11 2 -4 -1 781.516 212.139 14 2 -4 0 271207. 3592.90 2 2 -4 0 276539. 3385.83 14 2 -4 0 272794. 3559.92 13 2 -4 0 273673. 3432.87 11 -2 4 -1 97673.2 1456.73 7 2 -4 1 98817.7 2088.98 14 2 -4 1 97202.7 1767.47 1 2 -4 1 102110. 1449.95 4 2 -4 1 98766.1 1909.28 11 2 -4 1 94841.1 2121.79 2 2 -4 1 98912.5 2032.92 13 2 -4 2 263.919 174.960 6 2 -4 2 267.611 132.746 11 2 -4 2 512.570 180.323 14 2 -4 2 487.938 186.273 8 2 -4 2 256.245 121.175 1 2 -4 2 302.142 145.507 13 2 -4 3 235305. 3250.47 8 2 -4 3 229120. 3358.49 6 2 -4 3 234471. 2733.90 1 -2 4 -3 231553. 3188.24 12 2 -4 3 226039. 3353.01 14 2 -4 3 231651. 3009.69 4 2 -4 3 236284. 2849.94 13 2 -4 4 1819.95 323.511 4 2 -4 4 2148.38 356.159 8 2 -4 4 2009.96 286.509 1 -2 4 -4 2039.05 347.295 12 2 -4 4 1993.52 363.201 14 2 -4 4 2717.95 385.430 6 -2 4 -5 27785.0 1355.51 12 2 -4 5 28078.9 1304.52 4 2 -4 5 29351.3 1249.65 6 2 -4 5 27797.3 1135.72 1 2 -4 5 29569.3 1354.81 8 2 -4 6 4672.56 598.069 8 -2 4 -6 5718.58 710.360 12 2 -4 6 5210.73 622.795 4 2 -4 6 4651.64 531.546 1 -2 4 -7 5159.52 751.966 12 2 -4 7 5471.02 695.140 8 2 -4 8 9566.54 993.325 8 -2 4 -8 10831.0 1135.51 12 -2 4 -8 9933.30 1029.81 7 2 -4 9 4828.30 769.320 8 2 -4 9 4650.90 360.131 26 2 -4 10 6687.74 414.217 28 2 -4 10 6901.72 442.683 26 2 -4 11 1058.12 200.003 26 2 -4 11 810.769 165.908 28 2 -4 12 700.647 162.409 26 2 -4 12 1007.57 174.401 28 2 -4 13 1191.49 179.540 28 2 -4 13 1122.57 182.619 26 2 -4 14 310.366 99.4724 28 2 -3 -13 1379.87 151.627 23 -2 3 12 56.7080 62.0667 28 2 -3 -12 119.786 86.3772 23 -2 3 11 37.4611 85.6589 28 2 -3 -11 80.9593 91.0807 23 -2 3 10 2380.91 254.502 28 2 -3 -10 1830.05 237.585 23 -2 3 9 883.712 161.752 28 2 -3 -9 965.859 191.588 23 2 -3 -8 7580.56 452.367 23 -2 3 7 3320.50 644.238 3 2 -3 -7 3346.61 586.708 11 -2 3 6 19980.6 1423.58 3 2 -3 -6 21214.0 1334.64 11 2 -3 -5 63.1266 116.833 13 2 -3 -5 225.050 165.947 11 2 -3 -5-149.407 151.401 2 -2 3 5-219.156 214.073 3 2 -3 -4 8245.35 699.475 2 2 -3 -4 8910.53 712.821 13 -2 3 4 9114.49 816.097 3 2 -3 -4 9736.50 784.740 11 -2 3 3 6403.96 632.053 3 2 -3 -3 7815.78 518.677 14 2 -3 -3 7138.45 614.187 13 2 -3 -3 6510.87 603.042 11 2 -3 -3 6835.67 585.713 2 2 -3 -2 75565.1 1812.23 2 2 -3 -2 75766.9 1829.70 13 2 -3 -2 72406.7 1801.22 11 2 -3 -2 77401.3 1610.34 14 -2 3 2 74718.8 1857.22 3 2 -3 -2 77236.2 1092.94 4 2 -3 -1 4765.21 443.695 13 2 -3 -1 5061.81 471.610 2 2 -3 -1 5826.31 481.505 11 2 -3 -1 4910.72 420.102 14 2 -3 -1 5418.84 280.610 4 2 -3 -1 5086.71 441.076 1 2 -3 0 4091.44 408.190 2 2 -3 0 4063.05 381.325 14 2 -3 0 4054.11 368.451 1 2 -3 0 4469.23 395.143 11 2 -3 0 4310.84 275.230 4 2 -3 1 76242.3 1667.06 2 2 -3 1 76233.2 1491.90 1 2 -3 1 77362.2 1321.31 4 2 -3 1 76138.6 1569.11 13 2 -3 2 32288.7 1099.69 14 2 -3 2 33600.9 997.523 1 2 -3 3 13602.2 744.220 14 2 -3 3 14117.3 724.309 8 -2 3 -3 12945.2 751.974 12 2 -3 3 12633.9 700.007 4 2 -3 3 13590.6 686.699 1 2 -3 4 7577.45 587.239 8 2 -3 4 7223.06 560.691 1 2 -3 4 6799.91 556.665 14 -2 3 -4 7449.92 638.706 12 2 -3 4 7433.88 607.240 4 2 -3 5 81471.0 2109.03 8 2 -3 5 80832.4 2175.48 4 2 -3 5 81401.0 2035.40 1 -2 3 -5 80988.2 2333.35 12 2 -3 6 56108.1 1960.74 8 2 -3 6 59368.3 1935.57 1 2 -3 6 57689.8 2019.65 4 -2 3 -6 56955.6 2166.91 12 2 -3 7 26322.1 1467.16 8 2 -3 7 27018.0 1443.61 1 -2 3 -7 25472.3 1613.97 12 2 -3 7 26034.6 1484.59 4 -2 3 -8 1506.75 419.471 7 2 -3 8 995.187 326.076 8 -2 3 -8 942.753 355.110 12 2 -3 8 608.377 261.920 1 2 -3 9 11040.0 1119.75 8 2 -3 10 6237.22 422.477 26 2 -3 10 6083.75 405.529 28 2 -3 11 8109.05 468.648 28 2 -3 11 8013.14 475.682 26 2 -3 12 2371.53 258.830 26 2 -3 12 2256.63 250.100 28 2 -3 13 265.823 109.457 28 2 -3 14 206.491 97.1166 28 -2 2 13 1167.39 153.745 28 2 -2 -13 1051.93 150.370 23 -2 2 12 853.379 164.083 28 2 -2 -12 739.099 155.398 23 2 -2 -11 2422.15 271.536 23 -2 2 11 2422.66 264.797 28 -2 2 10 430.264 146.380 28 2 -2 -10 303.361 119.957 23 2 -2 -9 342.999 117.462 23 -2 2 9 292.838 132.236 28 -2 2 8-114.592 239.190 3 2 -2 -7 409.761 244.450 2 -2 2 7 221.584 255.053 3 -2 2 6 14385.0 1131.54 3 2 -2 -6 14100.4 983.617 11 2 -2 -6 13528.8 991.380 2 -2 2 5 10915.6 911.916 3 2 -2 -5 10032.2 772.815 11 2 -2 -5 11088.8 838.537 2 2 -2 -4 608.229 221.873 2 2 -2 -4 405.504 174.952 11 -2 2 4 755.563 276.295 3 2 -2 -3 552.819 190.722 2 2 -2 -3 649.780 137.856 7 -2 2 3 445.310 209.827 3 2 -2 -3 648.030 195.614 11 2 -2 -2 26763.0 645.553 7 2 -2 -2 26324.7 990.783 2 2 -2 -2 26170.1 962.268 11 2 -2 -1 999999. 5530.87 1 2 -2 -1 989352. 5642.37 2 2 -2 0 239.683 94.0292 4 2 -2 0 286.966 127.333 2 2 -2 0 111.328 129.161 1 2 -2 1 15573.6 648.719 2 2 -2 1 14297.0 629.510 1 2 -2 1 15947.3 533.776 8 2 -2 2 48354.9 1204.91 14 2 -2 2 50429.6 1232.61 1 2 -2 2 49868.7 1060.76 8 2 -2 3 881.727 197.476 14 -2 2 -3 755.509 226.762 12 2 -2 3 1131.65 233.463 1 2 -2 3 840.479 209.741 4 2 -2 4 109464. 1956.33 14 2 -2 4 110460. 2194.08 3 -2 2 -4 112529. 2457.84 12 2 -2 4 114110. 2335.36 4 -2 2 -4 106832. 1715.74 10 -2 2 -5 6713.21 701.710 12 2 -2 5 6102.36 604.935 4 2 -2 5 7023.49 628.457 3 2 -2 6 13682.8 971.580 3 -2 2 -6 13853.8 1111.89 12 2 -2 6 16276.2 1078.14 4 2 -2 7 6614.49 742.994 3 2 -2 7 6953.04 779.447 4 -2 2 -7 7104.99 878.119 12 -2 2 -8 991.858 404.728 12 2 -2 8 89.2220 189.255 3 2 -2 9 126.961 101.090 28 2 -2 10 1152.87 191.394 28 2 -2 11 584.624 153.021 28 2 -2 12 17.2743 89.2074 28 2 -2 13-3.35677 78.0078 28 2 -2 14 54.7896 81.2668 28 2 -1 -14 731.758 111.637 23 2 -1 -13 2641.16 238.066 23 -2 1 13 2728.41 250.120 28 2 -1 -12 113.973 90.8776 23 -2 1 12 40.1873 83.6929 28 -2 1 11 1600.89 226.841 28 2 -1 -11 1735.49 233.974 23 2 -1 -10 3579.00 326.965 23 -2 1 10 3767.52 330.657 28 -2 1 9 8988.41 478.943 28 2 -1 -9 8928.25 484.159 23 -2 1 8 10106.8 1055.23 3 2 -1 -8 8013.39 876.134 2 -2 1 7 16286.6 1219.94 3 2 -1 -7 14784.9 1114.79 2 -2 1 6 14173.3 1047.31 3 2 -1 -6 13544.3 866.068 7 2 -1 -6 14562.8 894.140 11 2 -1 -6 12319.9 956.341 2 2 -1 -5 159.469 208.665 2 2 -1 -5 138.515 143.726 11 2 -1 -5 76.3414 132.216 7 -2 1 5-6.53258 173.469 3 2 -1 -4 1111.72 297.291 2 2 -1 -4 956.535 218.927 7 -2 1 4 889.858 262.859 3 2 -1 -4 832.122 205.292 11 2 -1 -3 6729.77 315.712 15 2 -1 -3 6938.68 494.756 11 2 -1 -3 6264.11 547.951 2 2 -1 -2 764662. 3589.28 15 2 -1 -2 762596. 4163.80 7 2 -1 -2 757358. 4781.89 1 2 -1 -2 754611. 5038.03 2 2 -1 -1 77574.6 1244.84 15 2 -1 -1 78380.4 1431.67 1 2 -1 -1 81769.5 1296.19 7 2 -1 -1 80284.1 1448.27 2 2 -1 0 54953.1 1065.42 2 2 -1 0 53012.4 1142.19 1 2 -1 1 295443. 1653.60 8 2 -1 1 287111. 2612.46 14 2 -1 1 290276. 2265.40 2 2 -1 1 293482. 2824.49 1 2 -1 2 3959.61 316.464 14 2 -1 2 4473.85 400.151 1 -2 1 -3 19205.3 920.044 12 2 -1 3 17458.6 652.038 14 2 -1 3 17523.4 857.836 3 2 -1 3 18205.9 843.289 4 2 -1 4 8625.37 460.028 14 2 -1 4 8145.41 662.092 3 2 -1 4 8027.26 640.536 4 -2 1 -4 8820.35 714.235 12 -2 1 -4 8992.17 598.772 10 -2 1 -5 2474.66 464.726 12 2 -1 5 2283.89 406.352 3 -2 1 -5 2201.39 327.471 10 2 -1 5 2019.96 374.515 4 2 -1 6 10761.6 883.163 4 -2 1 -6 11035.7 1007.35 12 2 -1 6 9580.08 856.214 3 -2 1 -7 3367.23 632.425 12 2 -1 7 4036.33 631.081 3 2 -1 7 2893.53 513.014 4 2 -1 8 1571.78 445.097 3 -2 1 -8 832.898 389.406 12 2 -1 9 1156.30 186.191 28 2 -1 10 74.9023 96.5463 28 2 -1 11 327.232 126.900 28 2 -1 12 174.371 108.748 28 2 -1 13 57.9698 83.1240 28 2 0 -14 126.228 72.0256 23 2 0 -13 1777.22 204.774 22 -2 0 13 1462.19 205.995 28 2 0 -13 1369.35 182.974 23 2 0 -12 965.483 168.917 23 -2 0 12 946.538 180.769 28 2 0 -11 1597.52 225.621 23 -2 0 11 1454.70 216.327 28 -2 0 10 3228.53 301.637 28 2 0 -10 3511.66 314.510 23 2 0 -9 3737.62 675.785 2 2 0 -8 1114.12 348.603 2 2 0 -8 1883.20 423.423 7 -2 0 8 1037.16 335.951 3 2 0 -7 2006.09 418.013 7 -2 0 7 1331.03 364.524 3 -2 0 6 11762.4 888.683 3 2 0 -6 11407.7 842.054 7 2 0 -5 9579.73 701.546 7 -2 0 5 10583.4 742.804 3 -2 0 4 10584.6 660.872 3 2 0 -4 10404.3 662.693 7 2 0 -3 10217.9 604.446 7 2 0 -2 919729. 4797.09 1 2 0 -1 341330. 2822.95 1 -2 0 1 335224. 1650.50 8 2 0 0 13119.1 469.379 2 2 0 0 12756.9 572.255 1 2 0 1 2451.56 148.337 2 2 0 1 2227.29 288.028 1 2 0 1 2530.37 289.456 4 2 0 2 7961.07 530.393 4 2 0 2 7672.39 393.348 14 2 0 2 7911.80 533.702 15 2 0 2 7428.82 559.826 3 -2 0 -2 8371.87 554.621 12 2 0 3 14331.9 769.660 4 2 0 3 13816.5 469.705 14 -2 0 -3 14693.8 840.485 12 2 0 3 14188.0 845.641 3 -2 0 -3 14509.6 809.141 10 -2 0 -4 107.016 179.101 12 2 0 4 130.808 193.620 3 -2 0 -4-12.9208 140.155 10 2 0 4 171.516 151.019 4 -2 0 -5 22126.0 1122.66 10 -2 0 -5 22060.0 1313.16 12 2 0 5 22809.8 1180.00 4 2 0 5 22099.6 1276.23 3 2 0 6 9006.40 826.470 4 2 0 6 8114.25 857.330 3 -2 0 -6 9060.00 940.733 12 2 0 7 6618.59 842.406 3 -2 0 -7 6539.88 875.898 12 2 0 7 5555.59 708.783 4 2 0 8 5233.06 372.133 28 -2 0 -8 4511.58 811.660 12 -2 0 -8 5001.86 358.625 18 2 0 9 5166.76 383.447 28 2 0 10 1431.49 216.511 28 -2 0 -10 1515.71 208.595 23 2 0 11 100.775 98.5709 28 -2 0 -11-11.6563 69.9518 23 2 0 12 14.1489 75.5921 28 -2 0 -12 191.675 93.5361 23 2 0 13 46.4563 68.2014 28 2 1 -14 3053.06 238.907 22 -2 -1 13 45.6568 92.4061 28 2 1 -13 81.9065 93.9140 22 -2 -1 12 1050.28 190.444 28 2 1 -12 1352.83 194.060 23 2 1 -11-21.1822 86.0563 23 -2 -1 11-203.569 114.508 28 2 1 -10 56.1267 87.8912 23 -2 -1 10 24.1391 109.818 28 2 1 -9-483.809 270.678 7 2 1 -8 329.149 237.534 7 2 1 -7 276.869 229.482 7 -2 -1 7 186.498 207.057 3 -2 -1 6 12599.2 827.472 3 2 1 -6 13639.8 958.258 7 -2 -1 5 61846.6 1610.62 3 2 1 -5 61731.7 1838.93 7 2 1 -4 11.3876 143.958 7 -2 -1 4 58.6424 111.925 3 -2 -1 3 2006.66 254.571 8 2 1 -3 1933.13 306.592 7 2 1 -2 8814.32 443.938 1 -2 -1 2 8035.36 429.579 8 2 1 -1 81606.7 1361.42 1 -2 -1 1 75906.7 1174.15 8 2 1 0 18915.8 795.752 7 2 1 0 20287.1 752.380 1 2 1 0 18995.9 766.044 4 2 1 1 6179.71 512.679 15 2 1 1 6073.44 500.545 3 -2 -1 -1 6455.28 545.155 10 2 1 1 6413.88 464.217 4 2 1 2 1061.11 209.080 4 2 1 2 1246.00 248.673 15 2 1 2 1211.50 274.396 3 -2 -1 -2 1089.16 227.642 12 -2 -1 -2 1017.15 260.874 10 2 1 3 81950.4 1927.16 15 2 1 3 80034.5 2174.33 3 -2 -1 -3 86550.8 2111.17 12 -2 -1 -3 80387.0 2130.12 10 2 1 3 82794.9 1886.49 4 2 1 4 1710.14 378.483 3 -2 -1 -4 2528.69 455.951 12 -2 -1 -4 1809.97 359.403 10 2 1 4 2138.57 358.392 4 2 1 5 7040.59 786.368 3 -2 -1 -5 7498.52 797.174 12 2 1 5 7487.14 687.898 4 -2 -1 -5 7269.12 729.236 10 2 1 6 10021.4 1002.08 3 -2 -1 -6 10575.3 949.316 10 -2 -1 -6 12624.3 1124.88 12 2 1 7 806.543 345.038 3 -2 -1 -7 802.268 389.451 12 2 1 8 74.6781 106.689 28 -2 -1 -8 104.693 120.793 18 2 1 9 1799.73 235.582 28 2 1 10 181.185 111.129 28 -2 -1 -10 71.9543 74.5327 23 2 1 11 305.066 118.282 28 -2 -1 -11 481.371 127.536 23 -2 -1 -12-1.30706 56.1411 23 2 1 12 2.54584 73.3401 28 2 2 -14 164.351 89.4100 22 -2 -2 13 5771.71 385.720 28 2 2 -13 5583.35 385.885 22 -2 -2 12 149.145 107.810 28 -2 -2 11 5059.92 387.672 28 -2 -2 10 1375.40 209.930 26 -2 -2 10 1191.91 203.453 28 -2 -2 9 151.453 132.176 8 2 2 -9 159.327 227.350 7 2 2 -8 3183.67 566.873 7 -2 -2 7 5799.33 681.407 8 2 2 -7 5621.98 716.038 7 -2 -2 6 1380.48 327.192 8 2 2 -6 1061.32 296.447 7 2 2 -6 1511.45 380.212 9 -2 -2 5 42710.0 1518.61 8 2 2 -5 42576.4 1622.48 7 -2 -2 5 44011.1 1349.80 5 2 2 -5 41143.3 1637.33 9 -2 -2 4 54297.6 1537.00 5 2 2 -4 56490.7 1755.48 7 -2 -2 4 55559.7 1569.72 8 2 2 -3 128.139 141.295 7 -2 -2 3 374.690 139.191 8 2 2 -2 5292.63 316.747 1 2 2 -2 4778.87 479.151 7 -2 -2 2 4712.82 395.332 8 2 2 -1 76738.9 1355.35 1 2 2 -1 75430.4 1763.46 7 -2 -2 1 76325.9 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746.111 25 3 -10 2 19667.7 722.924 20 3 -10 3 3835.66 342.077 25 3 -10 3 3981.81 358.482 16 3 -10 3 4253.08 353.724 17 3 -10 3 3799.69 361.685 20 3 -10 4 6718.72 427.646 17 3 -10 4 6120.04 440.910 16 3 -10 4 6094.73 426.057 25 3 -10 4 6910.41 458.475 20 3 -10 4 5688.82 406.625 27 3 -10 5 5634.42 423.877 16 3 -10 5 5620.34 416.032 27 3 -10 5 5348.67 395.953 25 3 -10 5 5212.60 402.306 20 3 -10 6 4600.46 379.371 16 3 -10 6 4376.78 377.864 27 3 -10 6 5139.21 378.721 25 3 -10 6 4333.34 378.922 20 3 -10 7 2921.67 307.796 16 3 -10 7 2505.40 282.639 20 3 -10 8 169.746 109.685 16 3 -10 8 402.455 156.863 20 3 -10 9 35.2581 95.2875 16 3 -10 9 47.0362 140.664 20 3 -10 10 1931.35 229.426 16 3 -10 10 1890.88 230.829 20 3 -10 11-73.0585 83.7807 16 3 -10 11 83.7044 86.7778 26 3 -10 12-6.31214 77.2591 26 3 -9 -7 20.2072 62.9458 19 3 -9 -6-109.790 88.8364 17 3 -9 -6-4.94640 71.7215 19 3 -9 -5 967.084 165.027 17 3 -9 -5 943.409 176.719 19 3 -9 -4 1163.62 191.476 17 3 -9 -4 1553.84 211.657 25 3 -9 -3 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540.339 26 3 -7 10 924.861 184.158 26 3 -7 11 668.498 171.118 26 3 -7 12 3687.19 316.585 26 3 -7 13-84.6618 101.119 26 3 -7 14 581.254 115.335 26 3 -6 -10 799.353 138.630 23 3 -6 -9 3396.53 284.684 23 3 -6 -9 3609.50 289.712 19 3 -6 -8 144.237 98.8856 23 3 -6 -8 155.770 96.6309 19 3 -6 -7 1473.50 211.693 23 3 -6 -7 1493.80 227.184 19 3 -6 -6 16895.1 668.651 23 3 -6 -5 172.429 110.683 25 3 -6 -4 83.4539 128.269 13 -3 6 4 237.804 280.049 3 3 -6 -4 577.526 288.790 11 3 -6 -3 3582.06 614.152 13 -3 6 3 3870.74 666.648 3 3 -6 -3 2729.61 506.234 2 3 -6 -3 2626.09 515.614 11 3 -6 -2 575.931 273.953 13 -3 6 2 106.777 193.347 3 3 -6 -2 966.009 305.969 2 3 -6 -2 509.663 242.373 11 -3 6 1 1719.51 391.519 3 3 -6 -1 1490.11 365.628 13 3 -6 -1 1875.90 372.324 14 3 -6 -1 1508.35 360.729 2 3 -6 -1 1518.27 375.137 11 3 -6 0 1080.67 297.813 14 -3 6 0 1494.37 327.180 3 3 -6 0 1004.97 312.282 13 3 -6 0 1286.44 337.981 2 3 -6 0 1158.69 344.418 11 3 -6 1 3416.09 518.935 14 3 -6 1 3804.57 535.588 13 3 -6 1 4017.61 527.666 11 3 -6 2 37558.7 1677.28 14 3 -6 2 36831.0 1597.59 13 3 -6 3 4500.88 602.829 14 3 -6 3 3834.17 534.178 8 -3 6 -4 26855.3 1379.67 12 3 -6 4 23792.1 1410.33 14 3 -6 4 27064.4 1417.71 8 -3 6 -5 3343.40 532.350 12 3 -6 5 2875.59 502.040 8 -3 6 -5 2525.08 457.750 7 -3 6 -6 1136.08 330.068 7 -3 6 -6 1443.61 413.369 12 3 -6 6 1485.70 372.162 8 -3 6 -7 28.8115 150.546 7 3 -6 7-180.451 206.834 8 -3 6 -7-480.670 305.611 12 3 -6 8 677.502 171.274 26 3 -6 9 5478.46 393.515 26 3 -6 10 3515.79 333.799 26 3 -6 11 81.3392 122.226 26 3 -6 12 757.247 173.863 26 3 -6 13 198.297 103.445 26 3 -6 14 1213.30 154.856 26 3 -5 -11-63.1154 77.7625 23 3 -5 -10 1297.74 190.588 23 3 -5 -9-88.6053 92.8792 23 3 -5 -8 9.48001 89.2297 23 3 -5 -8-85.8476 101.165 19 3 -5 -7 959.850 175.621 23 3 -5 -7 1180.44 202.604 19 3 -5 -6 5533.29 390.422 19 3 -5 -6 5926.48 390.787 23 -3 5 5 171.404 250.393 3 3 -5 -5 512.453 256.519 11 3 -5 -4 2372.36 472.107 2 -3 5 4 2440.42 518.114 3 3 -5 -4 2204.23 478.565 11 -3 5 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14 -3 5 -5 327.138 228.831 12 3 -5 5 50.3611 126.449 8 3 -5 5 115.862 133.936 4 -3 5 -6 1466.32 404.899 12 3 -5 6 1072.95 305.141 8 3 -5 6 1407.43 380.863 4 -3 5 -7-452.430 257.944 7 -3 5 -7-69.3060 212.345 12 3 -5 8-301.147 254.918 8 -3 5 -8 686.008 331.499 7 -3 5 -8 562.804 325.966 12 3 -5 9 543.970 152.401 26 3 -5 10 1311.17 217.757 26 3 -5 11 639.730 166.299 26 3 -5 12 173.327 113.025 26 3 -5 13 1324.69 185.913 26 3 -5 14 634.116 118.559 26 3 -4 -12 731.565 129.987 23 3 -4 -11 64.5889 94.6467 23 3 -4 -10 53.0901 92.9226 23 3 -4 -9 13.0110 88.8260 23 3 -4 -8 102.091 107.135 23 3 -4 -8-16.6494 104.367 19 3 -4 -7 1363.53 202.194 23 3 -4 -7 1284.27 197.526 19 -3 4 6 871.155 322.799 3 3 -4 -6 1956.68 456.461 11 3 -4 -5 5632.99 693.002 2 -3 4 5 6595.64 826.788 3 3 -4 -5 7106.24 806.360 11 3 -4 -4 9852.01 871.873 2 -3 4 4 9908.48 924.660 3 3 -4 -4 10206.6 900.830 11 3 -4 -3 22975.6 1245.06 2 3 -4 -3 25869.3 1157.40 14 3 -4 -3 24346.4 1301.53 11 3 -4 -2 14847.5 875.361 14 3 -4 -2 15313.5 975.051 11 3 -4 -2 14002.4 929.293 13 3 -4 -2 13940.9 946.294 2 -3 4 2 15160.8 972.987 3 3 -4 -1 120937. 2647.68 2 3 -4 -1 123279. 2481.60 14 3 -4 -1 124596. 2624.40 13 3 -4 -1 125068. 2605.61 11 3 -4 -1 132416. 2591.73 1 3 -4 0 17050.6 979.035 2 3 -4 0 16877.3 934.393 14 3 -4 0 17342.8 911.527 1 3 -4 0 16380.9 893.593 11 3 -4 1 91131.7 2208.96 2 3 -4 1 88703.8 1998.22 1 3 -4 1 87417.6 2128.17 14 3 -4 1 93300.5 1759.69 4 3 -4 2 58298.6 1544.68 4 3 -4 2 58491.0 1614.03 1 3 -4 2 55439.9 1718.90 14 3 -4 2 58023.0 1533.32 8 3 -4 3 23894.6 1068.75 1 3 -4 3 22226.9 1118.54 14 3 -4 3 23540.8 1080.91 4 3 -4 3 24929.8 1046.53 8 3 -4 4 23088.4 1173.15 14 -3 4 -4 25061.2 1287.79 12 3 -4 4 23200.1 1175.87 4 3 -4 4 24227.7 1116.75 8 3 -4 4 24715.4 1145.59 1 3 -4 5 7488.32 707.234 14 -3 4 -5 7703.45 785.129 12 3 -4 5 7886.36 743.871 4 3 -4 5 8063.73 716.416 1 3 -4 5 8346.87 725.780 8 3 -4 6 3370.82 509.406 1 3 -4 6 3869.04 549.320 8 -3 4 -6 2195.67 489.590 12 3 -4 6 2465.79 471.316 4 -3 4 -7 18176.2 1423.06 12 3 -4 7 18559.5 1338.85 4 3 -4 7 18159.9 1271.22 1 3 -4 7 18040.6 1265.99 8 3 -4 8 573.683 274.363 8 -3 4 -8 929.524 379.381 12 3 -4 9 1028.85 198.241 26 3 -4 9 1217.69 208.081 21 3 -4 10 20967.2 721.551 28 3 -4 10 19440.5 746.101 26 3 -4 11 1865.62 237.450 28 3 -4 11 1641.02 240.274 26 3 -4 12 175.769 106.070 28 3 -4 12 121.796 101.265 26 3 -4 13 30.9458 86.3598 26 3 -4 13-26.9228 81.1917 28 3 -4 14 512.904 101.247 28 3 -3 -13 251.980 83.5385 23 3 -3 -12 1059.36 163.943 23 -3 3 11 1077.08 173.153 28 3 -3 -11 1074.55 183.647 23 -3 3 10 5712.36 385.672 28 3 -3 -10 5440.01 405.395 23 3 -3 -9 4095.93 352.382 23 3 -3 -8 1057.06 187.487 23 3 -3 -7 1034.67 327.589 2 -3 3 7 1016.95 389.426 3 -3 3 6 6889.23 858.709 3 3 -3 -6 7037.21 796.882 11 3 -3 -6 6175.39 747.977 2 3 -3 -5-312.924 190.903 2 -3 3 5 294.151 267.799 3 3 -3 -5-58.3366 155.091 11 -3 3 4 59310.4 2082.26 3 3 -3 -4 59831.3 1725.75 14 3 -3 -4 59051.1 1968.26 11 3 -3 -4 54980.2 1942.88 2 -3 3 3 84330.2 2259.83 3 3 -3 -3 84260.9 2002.57 14 3 -3 -3 83458.6 2203.95 11 3 -3 -3 82135.3 2228.33 2 3 -3 -2 86842.8 1973.80 14 3 -3 -2 83081.4 2050.74 11 3 -3 -2 85813.4 2078.27 1 3 -3 -2 81505.4 2077.63 2 3 -3 -1 26984.9 1139.85 2 3 -3 -1 28651.3 1121.08 14 3 -3 -1 27946.7 1126.99 1 3 -3 0 16588.4 844.910 1 3 -3 0 17715.4 883.196 14 3 -3 0 16149.5 858.431 2 3 -3 0 17229.4 741.351 4 3 -3 1 3377.42 393.951 2 3 -3 1 3558.08 399.264 1 3 -3 1 3905.93 430.574 14 3 -3 1 3374.68 361.196 4 3 -3 2 47431.5 1439.42 1 3 -3 2 48679.0 1421.70 2 3 -3 2 48888.9 1492.59 14 3 -3 2 50919.8 1448.90 4 3 -3 3 2301.22 359.896 14 -3 3 -3 2510.63 377.576 12 3 -3 3 3057.53 403.892 4 3 -3 3 3166.02 409.902 1 3 -3 3 2964.00 330.305 8 3 -3 4 6847.72 594.700 14 -3 3 -4 5983.98 639.491 12 3 -3 4 6237.94 628.176 4 3 -3 4 5563.15 576.062 1 3 -3 4 6648.41 551.524 8 3 -3 5 43591.7 1562.18 8 3 -3 5 42221.6 1495.87 14 -3 3 -5 40992.0 1784.35 12 3 -3 5 44102.2 1742.95 4 3 -3 5 43605.6 1708.95 1 3 -3 6 4961.85 594.289 8 3 -3 6 3874.67 562.840 1 -3 3 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18613.1 822.241 7 3 -2 -4 17582.5 1071.05 2 3 -2 -3 14223.8 671.544 7 3 -2 -3 12910.9 847.726 2 3 -2 -2 243467. 3290.60 1 3 -2 -2 243061. 3350.92 2 3 -2 -1 34104.3 1187.37 1 3 -2 -1 34537.0 1070.49 4 3 -2 -1 33893.8 1169.95 2 3 -2 0 8650.63 558.912 2 3 -2 0 9140.80 609.737 1 3 -2 0 9140.35 602.047 14 3 -2 0 8283.32 538.475 4 3 -2 1 6214.72 516.720 1 3 -2 1 5653.66 478.472 14 3 -2 1 6217.42 461.138 2 3 -2 1 5645.46 465.772 4 3 -2 1 6198.65 294.970 8 3 -2 2 184.729 156.091 1 3 -2 2 197.438 88.9357 8 3 -2 2 86.9858 138.266 4 3 -2 2 156.237 103.455 2 3 -2 2 245.802 149.126 14 3 -2 3 8721.12 602.511 14 -3 2 -3 8386.61 692.018 12 3 -2 3 8491.95 658.106 4 3 -2 3 8843.73 682.055 1 3 -2 4 464.387 167.136 14 -3 2 -4 658.346 238.042 12 3 -2 4 448.523 210.965 1 3 -2 4 524.929 212.933 4 -3 2 -5 19544.7 1255.54 12 3 -2 5 19729.0 1188.48 1 3 -2 5 20627.7 1201.84 4 -3 2 -6 34371.3 1831.78 12 3 -2 6 33128.6 1681.25 1 3 -2 6 31313.7 1601.94 4 -3 2 -7 14771.3 1331.71 12 3 -2 7 15002.3 1194.20 4 3 -2 7 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311.634 8 4 -7 5 1184.15 409.903 14 4 -7 6 264.746 162.370 8 4 -7 7 15513.9 641.424 27 4 -7 7 9719.86 494.253 26 4 -7 8 1505.95 234.972 27 4 -7 8 1777.17 241.401 26 4 -7 9 1509.24 225.369 26 4 -7 10 914.090 188.394 26 4 -7 11 1448.23 229.608 26 4 -7 12 204.513 113.109 26 4 -7 13 148.513 93.1868 26 4 -6 -10 3196.09 249.636 23 4 -6 -9 1273.08 184.394 23 4 -6 -9 1433.08 193.257 19 4 -6 -8 1634.30 216.874 23 4 -6 -8 1560.53 223.569 19 4 -6 -7 1346.77 204.089 23 4 -6 -7 1030.29 198.502 19 4 -6 -6 18.2399 103.665 23 4 -6 -6 31.6624 91.2700 19 4 -6 -5 1177.53 205.159 19 -4 6 4 6046.72 871.450 3 4 -6 -4 5869.47 804.213 2 4 -6 -4 6105.79 843.703 11 -4 6 3 1230.66 380.713 3 4 -6 -3 1753.49 432.469 2 4 -6 -3 2286.89 506.571 11 4 -6 -2 16906.9 1275.10 2 -4 6 2 16794.6 1253.09 3 4 -6 -2 17358.9 1170.33 14 4 -6 -2 17934.8 1303.19 11 4 -6 -1 4945.83 685.447 2 -4 6 1 6501.90 733.135 3 4 -6 -1 6206.45 715.238 14 4 -6 0 21442.4 1382.15 2 4 -6 0 22976.6 1347.62 14 4 -6 1 184.625 203.986 14 4 -6 1 63.2492 150.432 2 4 -6 1-8.72364 128.701 1 4 -6 2 104512. 2917.61 14 4 -6 2 108720. 2671.45 1 4 -6 3 22038.9 1385.25 14 -4 6 -3 23674.7 1363.14 12 4 -6 4 20368.2 1351.54 14 -4 6 -4 20672.6 1339.36 12 4 -6 4 23380.2 1295.65 4 4 -6 4 21995.4 1275.36 8 4 -6 5 8247.54 899.739 14 -4 6 -5 7716.84 872.441 12 4 -6 5 9093.85 885.493 4 4 -6 5 9646.90 881.911 8 -4 6 -6-261.310 216.939 12 4 -6 6 118.564 160.533 4 -4 6 -7 6112.89 809.658 7 -4 6 -7 5972.09 901.798 12 4 -6 8 78.4420 102.471 26 4 -6 9 2638.15 292.652 26 4 -6 10 2856.76 304.067 26 4 -6 11 1870.19 246.648 26 4 -6 12 334.189 128.618 26 4 -6 13 258.066 105.936 26 4 -5 -11-68.3718 80.8018 23 4 -5 -10 93.4404 98.2050 23 4 -5 -9 3823.58 331.059 23 4 -5 -9 3632.44 315.817 19 4 -5 -8 4809.80 373.645 23 4 -5 -8 4690.02 378.180 19 4 -5 -7 2697.49 288.028 23 4 -5 -7 2073.16 256.970 19 4 -5 -6 1099.29 183.626 23 4 -5 -6 1214.89 205.553 19 4 -5 -5 1642.76 437.578 2 -4 5 5 1384.09 451.671 3 4 -5 -4-214.891 201.506 2 -4 5 4-161.700 194.380 3 4 -5 -4-48.8055 153.892 11 4 -5 -3 1739.67 365.658 14 -4 5 3 1259.21 384.731 3 4 -5 -3 1602.78 401.543 2 4 -5 -3 1397.88 367.466 11 4 -5 -2 311.921 175.544 14 -4 5 2 151.994 195.771 3 4 -5 -2 519.153 247.368 2 4 -5 -1 11106.4 941.283 2 4 -5 -1 11170.4 888.040 14 4 -5 -1 12288.9 922.395 1 4 -5 0 47800.8 1882.25 2 4 -5 0 50081.6 1867.99 14 4 -5 0 50711.4 1804.40 1 4 -5 1 54277.7 1978.08 2 4 -5 1 55757.7 1985.78 14 4 -5 1 58157.3 1917.46 1 4 -5 1 56709.2 1606.37 4 4 -5 2 299.221 202.073 14 4 -5 2 241.240 185.121 1 4 -5 2 683.256 208.764 4 4 -5 3 297.956 149.522 8 4 -5 3 349.274 222.882 1 4 -5 3 248.623 165.345 14 4 -5 3 418.627 199.233 4 4 -5 4 1331.42 288.237 8 4 -5 4 1032.06 317.581 14 -4 5 -4 1447.16 385.293 12 4 -5 4 1251.07 320.190 4 4 -5 4 993.209 291.856 1 4 -5 5 8996.36 834.924 1 4 -5 5 7639.72 806.953 14 -4 5 -5 8250.56 889.790 12 4 -5 5 8821.55 865.114 4 4 -5 6 746.997 284.167 14 4 -5 6 955.110 318.637 1 -4 5 -6 435.706 266.413 12 4 -5 6 688.384 263.580 4 -4 5 -7 3101.79 648.968 12 4 -5 7 1962.11 479.016 4 4 -5 8 737.034 164.833 21 4 -5 9 4048.95 348.723 21 4 -5 9 3495.42 322.222 26 4 -5 10 2086.74 262.935 26 4 -5 11 698.416 168.232 26 4 -5 12 33.8106 97.7765 26 4 -5 13 96.8048 78.9805 26 4 -4 -12 345.022 98.1297 23 4 -4 -11 1005.05 173.169 23 4 -4 -10 3078.63 301.213 23 4 -4 -9-16.3882 97.4734 23 4 -4 -9 351.958 130.434 19 4 -4 -8 5725.31 416.173 23 4 -4 -8 5662.95 407.261 19 4 -4 -7 5.92317 85.0505 23 4 -4 -7 83.7382 101.067 19 4 -4 -6 440.138 257.160 2 -4 4 6 720.764 363.086 3 -4 4 5 8956.37 976.375 3 4 -4 -5 7278.32 854.578 2 4 -4 -4 105.387 147.090 2 4 -4 -4-82.0605 146.013 14 -4 4 4-259.275 209.429 3 4 -4 -3 1053.23 305.108 2 4 -4 -3 1662.94 348.223 14 4 -4 -2 4201.82 567.998 2 4 -4 -2 5724.25 611.940 14 4 -4 -2 5945.12 649.098 1 4 -4 -1 80146.9 2303.98 2 4 -4 -1 81537.7 2245.72 14 4 -4 -1 82354.3 2279.93 1 4 -4 -1 85535.9 1877.33 4 4 -4 0 34812.1 1469.68 14 4 -4 0 34373.7 1438.87 1 4 -4 0 35238.5 1488.59 2 4 -4 0 36133.2 1258.69 4 4 -4 1 3086.62 453.838 14 4 -4 1 2321.37 390.444 1 4 -4 1 2778.07 432.933 2 4 -4 1 2970.80 389.725 4 4 -4 2 7136.74 661.346 1 4 -4 2 7621.00 677.837 2 4 -4 2 7430.26 697.379 14 4 -4 2 7117.72 634.534 4 4 -4 2 7746.81 547.184 8 4 -4 3 3304.54 469.286 1 4 -4 3 2755.63 446.213 14 4 -4 3 3357.72 477.825 4 4 -4 4 809.127 273.757 14 4 -4 4 1255.48 330.214 1 -4 4 -4 1063.63 327.442 12 4 -4 4 745.492 251.359 4 4 -4 5 803.297 266.441 14 4 -4 5 681.745 277.206 1 -4 4 -5 540.033 281.567 12 4 -4 5 566.950 256.670 4 4 -4 6 2913.88 546.976 1 -4 4 -6 2344.48 526.309 12 4 -4 6 2973.57 547.520 4 -4 4 -7 13945.0 1336.46 12 4 -4 7 11804.2 1129.49 4 4 -4 8 3378.65 309.592 21 4 -4 9 6305.75 438.223 21 4 -4 10 1345.88 202.455 28 4 -4 10 1092.77 194.697 26 4 -4 11 88.4784 89.9509 28 4 -4 11 37.5918 101.708 26 4 -4 12 270.735 106.509 28 4 -4 12 276.320 120.292 26 4 -4 13 81.5745 63.8850 28 4 -4 13 75.0584 80.3463 26 4 -3 -13 35.1269 63.0505 23 4 -3 -12 1767.35 204.792 23 4 -3 -11 962.526 176.785 23 4 -3 -10 2364.07 271.888 23 4 -3 -9 17351.1 706.827 23 4 -3 -8 2690.77 282.247 23 4 -3 -8 2602.82 274.052 19 4 -3 -7-12.2580 206.277 2 -4 3 7-348.830 289.453 3 4 -3 -6 13.2271 143.156 2 -4 3 6 475.196 305.006 3 4 -3 -5 2245.53 461.374 2 4 -3 -5 2489.78 435.079 14 -4 3 5 1988.72 458.962 3 4 -3 -4-117.725 159.017 2 -4 3 4-209.192 202.625 3 4 -3 -4-381.736 204.540 14 4 -3 -3 177953. 3371.64 14 4 -3 -3 170566. 3501.25 2 4 -3 -2 94346.4 2375.73 14 4 -3 -2 93991.5 2397.55 1 4 -3 -2 92972.9 2070.92 4 4 -3 -2 96535.4 2462.85 2 4 -3 -1 687.041 220.548 2 4 -3 -1 550.144 209.421 14 4 -3 -1 605.367 183.253 4 4 -3 -1 727.977 230.544 1 4 -3 0 1621.27 333.959 1 4 -3 0 1753.20 332.655 14 4 -3 0 1562.87 303.894 2 4 -3 0 1451.41 286.399 4 4 -3 1 10486.0 736.291 2 4 -3 1 11873.7 815.786 1 4 -3 1 10983.2 799.523 14 4 -3 1 10494.9 734.220 4 4 -3 2 978.698 266.295 4 4 -3 2 941.735 270.502 14 4 -3 2 948.749 234.004 2 4 -3 2 892.437 263.425 1 4 -3 3 0.66450 156.607 4 4 -3 3 255.097 162.541 14 4 -3 3-79.6664 203.649 1 -4 3 -3 50.1689 150.417 12 4 -3 4 16.8579 140.434 4 4 -3 4 171.037 142.525 14 4 -3 4-78.7676 151.063 1 -4 3 -4 114.864 190.653 12 4 -3 5 1280.00 343.504 1 -4 3 -5 1016.27 361.852 12 4 -3 5 797.548 291.808 4 -4 3 -6 2347.90 543.388 12 4 -3 6 1893.33 452.753 1 4 -3 6 1112.56 367.377 4 4 -3 7-219.069 228.976 1 -4 3 -7-26.2059 295.189 12 4 -3 7-327.644 230.592 4 4 -3 8 11686.9 536.279 28 4 -3 8 12456.4 589.125 21 4 -3 9 1999.47 240.540 28 4 -3 9 1508.56 231.084 21 4 -3 10 9.04999 91.3684 28 4 -3 10-159.986 126.340 26 4 -3 11-11.9882 91.8787 28 4 -3 11 129.781 107.534 26 4 -3 12 933.520 151.554 26 4 -3 12 961.665 167.355 28 4 -3 13 156.266 85.7198 28 4 -2 -13 214.803 96.0811 23 4 -2 -12 20.8924 76.1564 23 4 -2 -11 889.602 176.618 23 -4 2 10 319.488 125.900 28 4 -2 -10 253.133 119.874 23 -4 2 9 1284.38 195.587 28 4 -2 -9 1356.73 210.852 23 4 -2 -8 2443.29 267.260 23 -4 2 7 11055.5 1119.26 3 4 -2 -7 8059.20 943.570 2 4 -2 -6 2224.82 491.296 2 -4 2 6 2645.22 547.384 3 4 -2 -5-431.120 245.790 2 -4 2 5-2.61829 175.489 3 4 -2 -4 5661.60 540.173 7 4 -2 -4 5015.23 639.583 2 4 -2 -3 59750.1 1654.17 7 4 -2 -3 58288.5 1878.72 1 4 -2 -3 59762.6 1974.17 2 4 -2 -2 128327. 2395.33 7 4 -2 -2 122426. 2634.20 1 4 -2 -2 122112. 2447.22 4 4 -2 -2 130445. 2706.42 2 4 -2 -1 18990.5 1018.06 1 4 -2 -1 19576.8 984.621 4 4 -2 -1 20710.6 1032.08 2 4 -2 0 12347.0 749.320 2 4 -2 0 11957.2 805.232 1 4 -2 0 12303.4 813.095 14 4 -2 0 12057.7 782.985 4 4 -2 1 537.351 211.282 4 4 -2 1 982.334 258.442 14 4 -2 1 1286.72 248.447 2 4 -2 1 971.480 288.848 1 4 -2 2 12032.9 661.713 2 4 -2 2 11965.4 793.138 14 4 -2 2 11327.8 811.802 4 4 -2 2 12163.1 876.519 1 4 -2 3 1745.59 349.955 4 4 -2 3 1783.75 369.908 1 4 -2 3 1772.42 328.192 14 -4 2 -3 2350.60 436.228 12 4 -2 4 1899.68 406.027 4 4 -2 4 1377.60 355.467 1 -4 2 -4 1232.75 380.932 12 4 -2 5-44.3132 131.697 1 -4 2 -5-275.774 243.716 12 4 -2 5 316.361 205.161 4 4 -2 6-54.1048 226.382 1 -4 2 -6 102.059 217.633 12 4 -2 6 57.5883 160.010 4 4 -2 7 854.606 330.015 1 -4 2 -7 479.010 317.587 12 4 -2 7 127.918 210.558 4 4 -2 8 164.018 98.3414 28 4 -2 8 499.117 165.422 21 4 -2 9 2424.85 271.095 28 4 -2 9 2375.82 281.898 21 4 -2 10 2527.56 263.690 26 4 -2 10 2234.23 266.320 28 4 -2 11 1836.34 223.252 28 4 -2 12 68.1138 93.0015 28 4 -1 -13 1950.79 205.543 23 4 -1 -12 2100.46 237.071 23 4 -1 -11 1704.52 229.410 23 4 -1 -11 1897.95 232.042 22 4 -1 -10 167.992 104.370 23 4 -1 -10 141.800 112.416 22 -4 1 9 1634.49 225.298 28 4 -1 -9 1729.93 244.147 23 4 -1 -9 1245.18 200.642 22 4 -1 -8-718.792 337.691 2 -4 1 8 1205.22 402.126 3 4 -1 -7 281.898 277.902 2 -4 1 7 496.710 292.531 3 4 -1 -6 598.968 274.803 7 4 -1 -6 927.621 338.905 2 -4 1 6 510.145 290.105 3 4 -1 -5 15047.3 983.822 7 -4 1 5 16177.1 1094.13 3 4 -1 -5 14114.3 1097.12 2 4 -1 -4 92682.4 2065.95 15 4 -1 -4 86885.4 2231.70 7 4 -1 -4 90021.2 2564.79 2 4 -1 -3 7588.99 648.853 7 4 -1 -3 7986.60 633.634 15 4 -1 -3 7540.62 657.324 1 4 -1 -3 8429.00 740.037 2 4 -1 -2 20341.9 1020.54 7 4 -1 -2 19698.3 1003.87 15 4 -1 -2 20435.7 1043.86 1 4 -1 -2 21078.1 1053.70 2 4 -1 -1 1239.84 282.377 1 4 -1 -1 1332.70 298.556 15 4 -1 -1 1068.74 242.021 2 4 -1 -1 1162.96 286.132 4 4 -1 0 18355.1 994.513 1 4 -1 0 17486.3 994.530 15 4 -1 0 17637.4 973.598 4 4 -1 0 18745.3 845.538 2 4 -1 1 3032.94 313.615 2 4 -1 1 2663.11 416.862 4 4 -1 1 2487.08 412.718 15 4 -1 1 2501.62 360.180 14 4 -1 1 2737.42 420.274 1 4 -1 2 1558.87 334.256 4 4 -1 2 1722.62 375.869 1 4 -1 2 1104.20 246.373 14 -4 1 -2 1348.62 337.700 12 -4 1 -3 21201.2 1242.89 12 4 -1 3 19630.1 1152.96 4 4 -1 3 19730.1 1206.79 1 -4 1 -4 35967.0 1750.19 12 4 -1 4 36936.9 1677.56 4 -4 1 -4 33975.7 1630.61 10 4 -1 4 35605.4 1736.57 1 -4 1 -5 1696.59 446.041 12 4 -1 5 2440.35 489.338 1 -4 1 -5 1580.06 393.663 10 4 -1 5 1961.64 430.652 4 -4 1 -6 8880.11 1044.53 12 4 -1 6 9158.43 959.143 4 4 -1 6 9742.51 1029.61 1 4 -1 7 5847.60 396.182 28 -4 1 -7 6657.15 410.059 18 4 -1 8 24.6119 95.0333 28 4 -1 8-51.7551 106.677 21 4 -1 9 480.419 159.751 28 4 -1 10 1729.51 227.681 28 4 -1 11 2092.91 229.819 28 4 -1 12 421.859 112.113 28 4 0 -14 632.128 111.377 23 4 0 -13 109.972 82.5505 23 4 0 -13-126.551 98.9201 22 4 0 -12 3532.52 308.691 23 4 0 -12 3264.98 290.694 22 4 0 -11 1074.23 189.213 23 4 0 -11 1394.19 219.666 22 4 0 -10 332.194 112.606 23 4 0 -10 317.641 131.081 22 4 0 -9 200.768 101.512 23 4 0 -9 202.588 114.777 22 4 0 -8 958.638 363.804 2 4 0 -8 712.158 241.205 7 4 0 -7 12423.0 1070.32 7 4 0 -7 11783.1 1146.94 2 4 0 -6 7716.92 792.709 7 -4 0 6 10297.8 893.641 3 4 0 -6 9449.00 980.838 2 4 0 -5 12390.2 949.134 7 4 0 -5 12391.1 880.831 15 4 0 -5 12434.5 1042.43 2 4 0 -4 10959.0 844.677 7 4 0 -4 10581.9 824.838 15 4 0 -4 10410.7 900.043 2 4 0 -4 11311.5 803.021 1 4 0 -3 138090. 2902.34 15 4 0 -3 141481. 2928.63 7 4 0 -3 141483. 2725.63 1 4 0 -3 146784. 3028.76 2 4 0 -2 7098.51 656.094 7 4 0 -2 5859.14 615.521 15 4 0 -2 7084.30 611.987 1 4 0 -2 6234.08 575.943 2 4 0 -1 2150.80 315.093 2 4 0 -1 2242.65 379.735 4 4 0 -1 2558.11 400.160 7 4 0 -1 1687.11 341.827 15 4 0 -1 2866.65 396.360 1 4 0 0 7780.27 665.853 1 4 0 0 7240.07 694.516 15 4 0 0 8029.32 694.071 4 4 0 1-179.052 159.303 4 4 0 1 15.3939 147.179 15 4 0 1 147.195 161.704 1 -4 0 -1 389.602 188.849 12 4 0 2 1941.49 375.782 4 4 0 2 2266.67 423.003 1 4 0 2 1593.93 363.409 15 -4 0 -2 2419.09 425.928 12 -4 0 -3 9864.54 869.743 12 -4 0 -3 8938.65 882.548 10 4 0 3 9928.82 856.528 4 4 0 3 9161.39 870.886 1 -4 0 -4 11690.4 1031.87 12 4 0 4 8977.12 868.079 4 4 0 4 9874.68 981.254 1 -4 0 -4 11167.6 1004.82 10 4 0 5 599.418 289.634 1 -4 0 -5 1107.49 449.988 12 -4 0 -5 1042.71 373.452 10 4 0 5 1056.15 331.833 4 4 0 6 562.749 140.224 28 -4 0 -6 1116.47 417.880 12 4 0 7 6683.93 427.722 21 4 0 7 6604.88 431.874 28 -4 0 -7 5895.66 395.369 18 4 0 8 7644.43 466.172 28 -4 0 -8 7569.01 457.209 18 4 0 9 102.550 103.862 28 4 0 10 72.5433 85.7233 28 4 0 11 848.944 148.475 28 4 1 -14 153.087 68.8293 22 4 1 -13 921.699 144.503 23 4 1 -13 958.485 161.679 22 4 1 -12 42.9896 78.1692 23 4 1 -12-41.6764 91.9158 22 4 1 -11 2268.24 257.398 23 4 1 -11 2313.17 270.854 22 4 1 -10 547.922 140.667 23 4 1 -10 503.080 147.295 22 4 1 -9-318.091 114.227 23 4 1 -9 135.315 112.915 22 4 1 -8 1724.95 486.384 2 4 1 -8 1206.77 355.442 7 4 1 -7 1043.66 367.957 7 4 1 -6 24182.9 1455.29 7 4 1 -5 9084.67 859.334 7 4 1 -5 9299.91 869.695 15 4 1 -4 1092.58 329.016 7 4 1 -4 946.004 308.739 15 4 1 -3 853.372 296.413 15 4 1 -3 665.303 241.227 7 4 1 -3 737.335 209.652 1 4 1 -2 40497.9 1656.59 7 4 1 -2 40061.1 1721.55 15 4 1 -2 41244.3 1428.97 1 4 1 -2 41474.2 1487.96 2 4 1 -1 4692.11 515.137 1 4 1 -1 4039.94 567.880 15 4 1 -1 4956.48 578.637 4 4 1 0 12433.0 957.632 15 4 1 0 13172.1 934.012 4 4 1 0 12377.8 864.580 1 4 1 1 21288.2 1268.97 15 -4 -1 -1 21194.4 1327.12 10 4 1 1 20377.1 1155.20 4 4 1 1 20321.4 1188.99 1 4 1 2 220.987 178.700 4 4 1 2 426.707 237.433 15 4 1 2 158.357 165.751 1 -4 -1 -2 236.099 215.854 10 4 1 3 9.01503 110.902 4 4 1 3 24.6095 167.624 1 -4 -1 -3 223.687 194.254 10 4 1 4 2266.70 524.559 1 -4 -1 -4 1858.05 451.047 10 -4 -1 -5 13878.2 1232.26 10 4 1 6 53.2894 108.117 28 -4 -1 -6-47.2515 80.4509 18 4 1 7 269.601 137.195 28 -4 -1 -7 554.861 153.012 18 4 1 8 1249.42 202.047 28 -4 -1 -8 1228.43 198.349 18 4 1 9 1369.66 201.600 28 4 1 10 155.997 95.0720 28 4 1 11 45.9159 67.7654 28 -4 -1 -11 23.9217 55.7233 23 4 2 -14 67.0680 69.7417 22 4 2 -13 24.7569 78.6095 22 4 2 -12 136.193 112.776 22 -4 -2 11 365.086 135.333 26 4 2 -11 515.442 149.067 22 -4 -2 10 4884.02 381.607 26 4 2 -10 5064.53 369.149 23 4 2 -10 4546.81 371.581 22 -4 -2 9 5346.77 394.634 26 4 2 -9 6278.99 402.398 23 4 2 -9 5604.03 405.358 22 4 2 -8 561.932 152.077 22 4 2 -7 676.461 293.044 7 4 2 -6 687.842 307.425 7 4 2 -6 2395.74 546.082 15 4 2 -5 3854.66 600.259 7 4 2 -5 4234.75 690.530 15 4 2 -4-37.6215 211.013 7 4 2 -4 55.1871 243.773 15 4 2 -3 21329.5 1409.54 15 4 2 -3 20796.2 1281.67 7 4 2 -2 8212.04 820.694 7 4 2 -2 8755.17 894.834 15 4 2 -2 8929.34 802.567 4 4 2 -1 23378.6 1429.49 15 -4 -2 1 23542.1 1437.79 10 4 2 -1 23295.7 1283.19 4 4 2 0 1544.27 335.535 4 4 2 0 1047.06 329.704 15 -4 -2 0 1810.14 437.411 10 4 2 1 1334.39 337.960 4 4 2 1 1603.21 392.522 15 -4 -2 -1 1816.82 448.718 10 4 2 2 1961.51 425.391 1 4 2 2 1614.97 405.111 15 -4 -2 -2 844.791 316.081 10 4 2 3 1829.36 444.372 1 4 2 3 1773.24 432.924 15 -4 -2 -3 944.647 337.697 10 -4 -2 -4 335.816 123.881 18 4 2 4 58.3130 98.6833 28 -4 -2 -5 543.104 148.483 18 4 2 5 810.922 165.810 28 4 2 6 358.208 135.772 28 -4 -2 -6 361.773 135.906 18 4 2 7 2439.44 269.239 28 -4 -2 -7 2201.41 257.933 18 4 2 8 614.488 142.067 28 -4 -2 -8 576.196 144.600 18 4 2 9 573.635 127.236 28 4 2 10 9.63651 64.0450 28 -4 -2 -10-15.8700 55.7582 23 4 3 -14 101.352 78.4704 22 4 3 -13 213.580 109.629 22 -4 -3 12 67.6462 92.7019 26 4 3 -12-39.0348 97.5496 22 -4 -3 11-42.7001 107.582 26 4 3 -11 108.114 103.540 22 -4 -3 10-90.5995 113.747 26 4 3 -10-56.0152 97.7077 22 -4 -3 9 624.790 175.048 26 4 3 -9 303.318 130.022 22 -4 -3 8 3941.03 341.403 26 4 3 -8 3690.20 321.077 22 4 3 -7 714.888 401.663 15 4 3 -6 3529.27 625.787 7 4 3 -6 3216.55 660.576 15 4 3 -5 3798.26 622.609 7 4 3 -5 4445.02 754.355 15 -4 -3 5 3754.35 603.129 5 4 3 -4 1881.65 431.851 7 4 3 -4 2028.90 561.732 15 -4 -3 4 2030.94 474.331 5 4 3 -3 403.983 210.762 4 4 3 -3 76.2932 160.772 7 4 3 -3 172.129 254.671 15 -4 -3 3 426.152 270.175 10 4 3 -2 23661.9 1449.38 7 4 3 -2 21731.8 1530.75 15 -4 -3 2 27070.0 1617.80 10 4 3 -2 26007.6 1430.51 4 4 3 -1 32382.7 1842.95 15 -4 -3 1 32821.4 1823.47 10 4 3 0 8717.99 958.201 15 -4 -3 0 8148.26 944.853 10 4 3 1 172.891 194.884 15 -4 -3 -1-74.5380 173.260 10 4 3 2 350.883 222.765 15 -4 -3 -3-3.03380 83.1905 18 4 3 3 91.9771 93.8794 28 4 3 4 11272.4 547.073 28 -4 -3 -4 11445.2 561.000 18 -4 -3 -5 1368.51 209.807 18 4 3 5 1538.16 219.148 28 4 3 6 168.142 116.570 28 -4 -3 -6 122.098 90.1520 18 4 3 7 303.728 119.688 28 -4 -3 -7 413.019 137.770 18 4 3 8 768.780 145.086 28 -4 -3 -8 949.675 164.592 18 4 3 9-102.638 63.2821 28 4 4 -14 92.9657 65.4441 22 -4 -4 13-12.8340 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3034.80 301.707 20 5 -10 8 289.701 138.728 27 5 -10 8-95.4957 159.729 20 5 -10 9 1295.99 213.817 27 5 -10 9 748.449 166.772 20 5 -10 10-45.1832 109.192 20 5 -10 11 288.912 93.0373 26 5 -9 -7 143.557 85.6752 19 5 -9 -6-12.3103 77.1977 19 5 -9 -5 153.138 110.425 17 5 -9 -5-38.6022 90.9539 19 5 -9 -4 372.943 130.534 17 5 -9 -4 458.815 141.991 19 5 -9 -3 655.310 167.251 17 5 -9 -3 1065.94 200.193 25 5 -9 -3 841.840 178.717 19 5 -9 -2 316.927 148.031 17 5 -9 -2 187.497 146.596 25 5 -9 -2 177.566 110.302 19 5 -9 -1 5008.41 393.360 25 5 -9 -1 5153.51 386.733 19 5 -9 -1 4654.18 378.077 17 5 -9 0 236.413 122.748 17 5 -9 0 151.814 129.325 25 5 -9 1 664.964 176.252 17 5 -9 1 1020.51 184.029 27 5 -9 1 910.704 179.615 25 5 -9 2 21903.4 764.799 27 5 -9 2 22323.8 787.801 25 5 -9 2 21498.1 782.296 17 5 -9 2 21508.7 770.879 24 5 -9 3 297.260 132.845 17 5 -9 3 29.3621 100.399 27 5 -9 3 150.108 113.379 25 5 -9 3 162.960 111.197 24 5 -9 4 904.157 187.067 27 5 -9 4 859.310 182.776 24 5 -9 4 1017.97 188.930 16 5 -9 5 1144.50 196.373 24 5 -9 5 941.882 191.750 27 5 -9 6 19.2562 111.007 27 5 -9 7 47.7467 115.452 27 5 -9 8 1435.17 230.522 27 5 -9 9 617.649 168.920 27 5 -9 9 490.609 135.203 26 5 -9 10 96.5845 92.5632 26 5 -9 10-134.976 138.612 20 5 -9 11 385.102 124.310 26 5 -9 12 290.229 96.9963 26 5 -8 -8 451.284 116.427 19 5 -8 -7 811.633 163.170 19 5 -8 -6 257.714 124.295 19 5 -8 -5 1109.62 188.855 17 5 -8 -5 1241.96 209.881 19 5 -8 -4 364.009 151.270 17 5 -8 -4 61.2913 95.6443 19 5 -8 -3 39.1677 107.473 25 5 -8 -3 111.139 101.283 17 5 -8 -3 19.7490 93.0454 19 5 -8 -2 1772.17 236.194 17 5 -8 -2 1802.83 253.638 25 5 -8 -2 2074.61 259.934 19 5 -8 -1 13425.9 612.167 17 5 -8 -1 13912.5 630.764 25 5 -8 0 1355.50 204.617 17 5 -8 0 1108.22 194.324 25 5 -8 1 92.5614 121.404 17 5 -8 1-77.9847 133.471 27 5 -8 1 176.145 116.508 25 5 -8 2 11463.8 549.396 17 5 -8 2 11993.1 552.173 27 5 -8 2 12066.5 560.612 25 5 -8 2 10634.0 538.211 24 5 -8 3 680.897 156.141 27 5 -8 3 559.572 130.884 24 5 -8 3 640.018 162.491 17 5 -8 4 6242.61 417.929 27 5 -8 4 6324.68 409.379 24 5 -8 5 1421.77 218.453 27 5 -8 5 2109.62 259.757 24 5 -8 6 3047.76 309.586 27 5 -8 7 1362.26 224.029 27 5 -8 7 1076.50 182.271 26 5 -8 8 1372.94 213.833 27 5 -8 8 1690.07 227.360 26 5 -8 9 648.071 166.693 27 5 -8 9 547.439 142.422 26 5 -8 10 435.360 137.665 26 5 -8 11 168.539 107.562 26 5 -8 12 80.2790 89.2701 26 5 -7 -9 513.336 104.596 23 5 -7 -9 711.614 135.985 19 5 -7 -8-48.0403 71.3967 23 5 -7 -8 29.3977 88.0139 19 5 -7 -7 20.0835 84.7395 19 5 -7 -6 5799.63 424.877 19 5 -7 -5 2487.61 295.275 19 5 -7 -4 1687.61 233.470 17 5 -7 -4 2013.31 258.121 19 5 -7 -3 19275.4 724.336 17 5 -7 -3 18455.7 716.519 25 5 -7 -3 20571.7 764.304 19 5 -7 -2 5939.88 398.745 17 5 -7 -2 5654.39 401.435 25 5 -7 -2 6011.50 403.625 19 5 -7 -1 5130.25 747.906 14 -5 7 1 5821.59 803.550 3 5 -7 -1 5753.75 830.415 2 5 -7 0 3427.74 604.443 14 5 -7 0 3630.90 636.409 2 5 -7 1 1177.52 391.143 14 5 -7 2 16310.8 1301.26 14 5 -7 3 14491.8 1243.43 14 -5 7 -3 15106.9 1241.59 12 5 -7 4 265.380 213.013 14 -5 7 -4 301.400 236.106 12 5 -7 5 13618.8 600.875 27 5 -7 5 14409.2 613.277 24 -5 7 -5 13414.4 1275.14 12 5 -7 6 135.859 99.1936 27 5 -7 6 323.791 124.191 26 5 -7 7 6658.86 433.585 27 5 -7 7 7866.28 462.611 26 5 -7 8 5867.77 405.818 27 5 -7 8 6598.88 433.884 26 5 -7 9 176.723 113.038 26 5 -7 10 155.231 112.978 26 5 -7 11 47.8368 97.5770 26 5 -7 12 13.5071 82.8373 26 5 -7 13 378.548 101.403 26 5 -6 -10 568.406 119.169 23 5 -6 -10 578.470 114.635 19 5 -6 -9 374.921 113.619 23 5 -6 -9 362.823 118.533 19 5 -6 -8 1936.55 230.025 23 5 -6 -8 1632.86 224.810 19 5 -6 -7 154.420 92.0947 23 5 -6 -7 90.8291 89.7064 19 5 -6 -6 353.214 118.776 23 5 -6 -6 348.621 138.077 19 5 -6 -5 21129.0 790.475 19 5 -6 -4 2873.14 293.057 19 -5 6 3 142.571 206.585 3 5 -6 -3 141.463 223.330 2 5 -6 -2 2661.23 500.292 14 -5 6 2 1865.44 463.040 3 5 -6 -2 1722.09 442.581 2 5 -6 -1 14354.9 1210.26 2 5 -6 -1 18263.6 1302.70 14 5 -6 0 501.754 259.435 1 5 -6 0 452.931 269.088 14 5 -6 0 613.193 287.250 2 5 -6 1 23343.4 1485.30 2 5 -6 1 19961.8 1371.31 14 5 -6 1 22598.4 1372.38 1 5 -6 2 925.477 310.503 1 5 -6 2 845.368 313.838 14 5 -6 3 47153.1 2135.71 14 5 -6 3 53631.4 2131.23 1 5 -6 4 9061.86 913.385 1 5 -6 4 8345.47 915.485 14 -5 6 -4 9234.52 1005.98 12 5 -6 4 9423.56 905.938 4 5 -6 5 2217.29 509.772 14 -5 6 -5 1371.36 421.428 12 5 -6 5 2566.55 537.108 4 5 -6 6 834.042 342.751 14 5 -6 6 1437.97 414.277 4 5 -6 7 384.994 137.932 21 5 -6 8 1038.24 191.556 21 5 -6 9 1152.05 199.540 26 5 -6 9 1003.97 189.250 21 5 -6 10 27.5222 95.2140 26 5 -6 11 16.3297 86.7163 26 5 -6 12 30.4249 78.4070 26 5 -6 13 125.714 79.1923 26 5 -5 -11 364.677 95.4681 23 5 -5 -10 95.5991 85.5592 23 5 -5 -10 7.93088 79.2243 19 5 -5 -9 540.777 148.701 23 5 -5 -9 726.974 161.910 19 5 -5 -8 10387.0 538.323 23 5 -5 -8 10332.4 549.070 19 5 -5 -7 15362.1 649.934 23 5 -5 -7 13940.0 648.374 19 5 -5 -6 8752.67 481.482 23 5 -5 -6 12701.1 607.196 19 5 -5 -5 298.778 127.888 19 5 -5 -4 8341.75 963.943 2 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1243.63 14 5 -4 2 19261.1 1168.58 4 5 -4 3-72.2808 200.948 4 5 -4 3-165.747 154.720 14 5 -4 3 121.301 173.535 1 5 -4 4 5562.26 683.012 14 5 -4 4 4282.67 630.390 1 -5 4 -4 4638.13 694.703 12 5 -4 4 5374.87 697.875 4 5 -4 5 3798.88 631.529 1 -5 4 -5 3810.35 682.835 12 5 -4 5 3695.81 610.316 4 5 -4 6 171.389 157.643 1 -5 4 -6 367.763 295.660 12 5 -4 6 111.074 169.788 4 5 -4 7 2060.66 251.294 21 5 -4 8 6901.60 451.998 21 5 -4 9 88.5547 90.7370 28 5 -4 9 172.916 135.339 21 5 -4 10 31.6376 93.7185 28 5 -4 10 123.745 121.418 26 5 -4 11-6.10558 76.0479 28 5 -4 11 3.51222 80.4055 26 5 -4 12 304.118 93.5839 28 5 -4 12 347.711 104.488 26 5 -3 -12 1242.24 173.767 23 5 -3 -11 2901.00 281.273 23 5 -3 -10 470.613 147.922 23 5 -3 -9 567.687 152.655 23 5 -3 -9 476.548 139.662 19 5 -3 -8 3696.71 331.436 23 5 -3 -8 3628.26 339.785 19 5 -3 -7 2432.04 258.993 23 5 -3 -7 2295.99 258.181 19 5 -3 -6 2419.51 553.260 2 -5 3 6 2539.43 585.010 3 5 -3 -5 18.0980 143.199 2 5 -3 -5-85.2084 166.364 14 -5 3 5 119.905 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3 -7 15398.7 638.056 22 -5 -3 6 3841.28 335.945 26 5 3 -6 3590.60 304.645 22 -5 -3 5 13311.1 605.555 26 5 3 -5 13923.2 579.627 22 -5 -3 5 14783.3 603.346 18 5 3 -4 1355.57 387.198 4 -5 -3 4 801.299 163.218 26 -5 -3 4 1264.08 423.951 5 -5 -3 3 14475.4 1302.91 10 5 3 -3 15504.7 1252.22 4 -5 -3 2 3398.37 660.115 10 -5 -3 1 90.3586 85.9022 18 5 3 -1 198.448 101.735 28 5 3 0 12582.1 561.080 28 -5 -3 0 13418.1 588.190 18 -5 -3 -1 644.525 160.607 18 5 3 1 627.303 152.116 28 5 3 2 3110.77 297.113 28 -5 -3 -2 2852.11 283.306 18 -5 -3 -3 373.890 132.994 18 5 3 3 587.628 155.127 28 5 3 4 2053.18 249.061 28 -5 -3 -4 2275.11 257.346 18 5 3 5 396.969 135.315 28 -5 -3 -5 300.681 117.568 18 5 3 6 409.020 124.959 28 -5 -3 -6 451.416 133.882 18 5 3 7 960.365 148.395 28 -5 -3 -7 1172.23 169.289 18 5 3 8 361.063 87.8605 28 5 4 -13 91.3972 70.8269 22 -5 -4 12 132.545 97.3166 26 5 4 -12-47.6307 81.1503 22 -5 -4 11 308.936 125.417 26 5 4 -11 317.908 114.745 22 -5 -4 10 858.189 173.950 26 5 4 -10 1029.88 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10 6 -2 5 6616.52 423.442 28 6 -2 5 5933.40 417.183 21 6 -2 6 173.530 118.120 28 6 -2 6 188.175 129.969 21 6 -2 7 1641.09 235.748 28 6 -2 7 1630.09 239.328 21 6 -2 8 203.731 105.358 28 6 -2 8 85.5189 112.840 21 6 -2 9 501.506 126.090 28 6 -2 10 475.347 122.832 28 6 -2 11 318.010 89.6795 28 6 -1 -13 201.284 80.0303 23 6 -1 -12 303.842 111.193 23 6 -1 -12 191.376 84.4028 22 6 -1 -11 450.443 128.826 23 6 -1 -11 469.645 124.245 22 6 -1 -10 2076.00 252.444 23 6 -1 -10 2007.73 238.172 22 6 -1 -9 1745.53 234.570 23 6 -1 -9 1692.20 231.900 22 6 -1 -8 93.5860 91.9062 23 6 -1 -8 85.5677 112.154 22 6 -1 -7 8791.11 500.555 23 6 -1 -7 9872.60 511.541 22 6 -1 -7 8974.36 503.826 19 6 -1 -6 131.029 80.0580 23 6 -1 -6 223.576 96.2732 22 6 -1 -6 388.235 117.369 19 6 -1 -5 1107.27 394.296 7 6 -1 -5 1059.10 348.569 2 6 -1 -4 6546.90 788.027 7 6 -1 -4 7047.33 807.987 1 6 -1 -4 7337.20 853.811 4 6 -1 -4 7986.25 883.987 2 6 -1 -3 11460.2 1021.79 15 6 -1 -3 9447.96 919.707 1 6 -1 -3 10660.7 1008.57 4 6 -1 -3 11080.1 1000.57 2 6 -1 -2 8633.95 907.727 15 6 -1 -2 7761.00 853.654 1 6 -1 -2 7815.82 853.296 4 6 -1 -1 5591.04 739.151 15 6 -1 -1 5565.63 716.140 1 6 -1 -1 5593.46 725.862 4 6 -1 0 12072.6 1080.68 1 6 -1 0 12137.6 1055.65 14 6 -1 0 12838.7 1099.73 4 6 -1 1 3371.92 585.954 4 -6 1 -1 4581.15 662.403 12 6 -1 1 3835.40 635.335 1 6 -1 2 9322.05 1009.57 1 6 -1 2 10983.9 1055.68 4 6 -1 3 1817.91 445.314 4 6 -1 3 1913.02 497.440 1 -6 1 -3 1954.46 514.828 10 6 -1 4 6778.23 426.002 28 6 -1 4 6737.96 431.710 21 6 -1 5 951.144 187.000 28 6 -1 5 949.222 181.817 21 6 -1 6 553.470 169.081 28 6 -1 6 738.263 173.985 21 6 -1 7 66.9494 91.3709 28 6 -1 7 60.2621 103.570 21 6 -1 8 114.030 104.118 28 6 -1 9 318.949 119.413 28 6 -1 10 300.497 97.8633 28 6 0 -13 474.495 102.503 23 6 0 -13 564.960 109.146 22 6 0 -12 999.212 156.268 23 6 0 -12 944.803 157.028 22 6 0 -11 461.834 134.849 23 6 0 -11 453.410 134.896 22 6 0 -10 1276.66 211.777 23 6 0 -10 1138.38 195.049 22 6 0 -9 321.287 117.733 23 6 0 -9 475.270 153.160 22 6 0 -8 149.612 118.195 23 6 0 -8 83.1660 108.044 22 -6 0 7 2014.38 248.499 26 6 0 -7 2145.28 255.866 23 6 0 -7 1989.04 242.473 22 -6 0 6 1471.75 218.831 26 6 0 -6 1621.97 216.485 23 6 0 -6 2096.53 238.515 22 6 0 -5 4613.70 693.688 7 6 0 -5 8159.80 962.035 2 6 0 -4 464.373 234.139 4 6 0 -4-224.359 207.436 7 6 0 -4 382.005 349.083 15 6 0 -3 736.018 317.209 15 6 0 -3 290.826 226.616 4 6 0 -2 3993.12 645.517 4 6 0 -2 3209.49 560.127 15 6 0 -1 1077.53 352.142 4 6 0 -1 792.968 316.510 15 6 0 -1 923.550 317.431 1 6 0 0 1277.76 387.630 4 6 0 0 716.455 290.650 1 6 0 0 604.195 291.838 15 6 0 1 435.478 265.315 4 6 0 1-8.99441 182.971 1 6 0 2 2486.66 522.538 4 6 0 2 2263.77 254.839 28 6 0 2 1517.28 441.320 1 6 0 3 530.191 153.927 28 6 0 4 118.539 111.124 28 6 0 5 6717.32 445.517 28 6 0 5 7600.49 448.003 21 6 0 6 8432.73 488.586 28 6 0 6 8151.22 465.011 21 6 0 7 150.147 112.625 28 6 0 8 76.3478 91.9593 28 6 0 9 47.8112 85.7930 28 6 1 -13-23.0048 58.7940 23 6 1 -13 116.894 77.1990 22 6 1 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929.106 19 7 -3 -5 17359.0 676.111 23 7 -3 -5 16223.0 638.516 22 7 -3 -5 16763.9 699.693 19 7 -3 -4 10023.8 495.995 22 7 -3 -4 10724.2 553.345 19 7 -3 -3 339.283 223.507 4 7 -3 -3 137.465 161.605 2 7 -3 -3 304.279 142.536 19 7 -3 -2 2220.94 490.207 4 7 -3 -2 1485.60 420.242 1 7 -3 -2 1148.13 377.686 14 7 -3 -1-107.423 121.883 4 7 -3 -1-1.19367 191.836 1 7 -3 -1 33.7477 143.757 14 7 -3 0 2398.98 509.044 4 7 -3 0 855.794 300.602 14 7 -3 0 2365.43 525.973 1 7 -3 1-41.9299 187.250 4 7 -3 1-73.3311 146.654 14 7 -3 2 473.552 144.656 21 7 -3 3 1343.83 215.562 21 7 -3 4 7553.25 473.298 21 7 -3 4 7322.22 434.795 28 7 -3 5 3231.39 304.288 28 7 -3 5 2811.47 304.701 21 7 -3 6 66.2942 105.437 28 7 -3 6-7.97221 114.677 21 7 -3 7 308.779 124.771 28 7 -3 7 418.085 147.190 21 7 -3 8 72.6103 104.293 28 7 -3 8 23.0042 94.6715 21 7 -3 9 24.8689 74.4358 28 7 -3 10 496.909 105.434 28 7 -3 10 423.177 108.212 26 7 -2 -12 334.394 99.2873 23 7 -2 -11-12.9990 73.5808 23 7 -2 -10 70.9921 88.7432 23 7 -2 -10 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309.193 129.397 28 7 -1 4 79.4155 105.660 21 7 -1 5 536.941 147.143 28 7 -1 5 618.434 164.000 21 7 -1 6 1524.22 217.822 28 7 -1 6 1767.86 231.491 21 7 -1 7 312.303 122.957 28 7 -1 7 308.131 125.624 21 7 -1 8 289.294 110.110 28 7 -1 9 148.463 84.2988 28 7 0 -12-100.002 76.7503 23 7 0 -12 6.97291 67.2176 22 7 0 -11 78.8660 80.5660 23 7 0 -11-39.4590 73.7809 22 7 0 -10 1439.18 208.303 23 7 0 -10 1894.49 230.691 22 7 0 -9 671.556 159.742 23 7 0 -9 490.651 147.738 22 7 0 -8 726.596 167.889 23 7 0 -8 1017.27 186.177 22 7 0 -7 93.3273 89.4904 23 7 0 -7-88.9958 103.622 22 7 0 -6 3257.34 318.474 23 7 0 -6 3768.99 330.302 22 7 0 -5 24419.4 783.979 28 7 0 -5 23892.5 811.517 23 7 0 -5 23538.7 794.537 22 7 0 -4 2681.32 270.208 28 7 0 -4 2750.86 281.666 23 7 0 -4 2329.60 259.241 22 7 0 -3 5242.18 370.280 28 7 0 -2 2453.75 269.505 28 7 0 -1 476.707 141.259 28 7 0 0 1666.58 231.447 28 7 0 1 79.2340 124.593 28 7 0 2 393.823 146.039 28 7 0 3 4631.14 374.745 28 7 0 4 3171.20 316.142 28 7 0 5 69.6237 88.7041 28 7 0 6 1446.35 207.193 28 7 0 7-2.83808 81.8510 28 7 0 8 558.935 116.432 28 7 1 -12 1022.19 147.770 22 7 1 -11 108.436 76.2617 23 7 1 -11 142.638 95.3383 22 7 1 -10-22.9521 73.6502 23 7 1 -10-9.14352 87.0561 22 7 1 -9-92.3903 91.2483 23 7 1 -9-28.3673 96.8824 22 7 1 -8 377.706 131.332 23 7 1 -8 396.950 128.594 22 7 1 -7 120.620 99.1582 23 7 1 -7-67.5765 104.128 22 7 1 -6 3357.43 306.664 28 7 1 -6 3469.01 321.885 23 7 1 -6 3334.51 311.840 22 7 1 -5 4880.50 364.936 28 7 1 -5 5215.77 384.240 22 7 1 -4 14614.7 615.662 28 7 1 -4 14125.6 617.912 22 7 1 -3 4787.00 364.267 28 7 1 -2 4707.90 363.304 28 7 1 -1 78.1358 119.460 28 7 1 0 276.400 124.338 28 7 1 1 1295.03 209.222 28 7 1 2 1549.83 225.019 28 7 1 3 152.160 116.393 28 7 1 4 287.522 125.986 28 7 1 5 176.711 110.589 28 7 1 6 86.6420 78.0607 28 7 1 7 189.220 89.6383 28 7 2 -12 426.751 98.3987 28 7 2 -12 143.101 76.6796 22 7 2 -11 850.531 139.822 28 7 2 -11 924.261 147.818 22 7 2 -10 2054.01 222.874 28 7 2 -10 1538.61 199.436 22 7 2 -9 3818.42 309.903 28 7 2 -9 4008.69 320.652 22 7 2 -8 2100.34 246.642 28 7 2 -8 2256.57 251.020 22 7 2 -7 2161.48 245.599 28 7 2 -7 2086.24 249.082 22 7 2 -6 5983.41 400.030 28 7 2 -6 6014.32 403.645 22 7 2 -5 5667.88 397.068 28 7 2 -5 5794.97 396.988 22 7 2 -4 2035.15 247.300 28 7 2 -3 19.9974 92.0025 28 7 2 -2 302.062 125.071 28 7 2 -1 60.0410 100.207 28 7 2 0 1753.14 229.189 28 7 2 1 34.8870 84.2303 28 7 2 2 154.040 113.305 28 7 2 3 149.448 101.435 28 7 2 4 1176.04 179.172 28 7 2 5 1349.18 174.583 28 7 2 6 115.669 71.6429 28 7 3 -11 169.606 79.3606 28 7 3 -11 75.3561 63.6625 22 7 3 -10 768.282 144.135 28 7 3 -10 685.254 136.468 22 7 3 -9 738.275 144.520 28 7 3 -9 661.558 140.792 22 7 3 -8 2244.30 239.922 28 7 3 -8 1915.11 224.152 22 7 3 -7 5316.57 368.549 28 7 3 -7 4777.65 350.018 22 7 3 -6 1068.88 184.109 28 7 3 -5 337.004 122.832 28 7 3 -4-32.6740 90.1686 28 7 3 -3 201.069 118.149 28 7 3 -2 211.529 104.852 28 7 3 -1 1787.77 229.234 28 7 3 0 179.862 102.248 28 7 3 1 105.828 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19 8 -6 -1 13657.9 601.845 24 8 -6 -1 14887.9 646.957 21 8 -6 0 2111.12 249.578 24 8 -6 0 2573.36 282.034 21 8 -6 1 8087.60 476.062 24 8 -6 1 8680.97 505.968 21 8 -6 2 3433.32 319.752 24 8 -6 2 4337.25 362.652 21 8 -6 3 289.347 139.509 21 8 -6 4 148.705 113.688 21 8 -6 5 14438.4 643.455 21 8 -6 6 19865.4 745.236 21 8 -6 7 1505.64 217.326 21 8 -6 8 526.101 143.551 21 8 -6 9 34.9456 77.3923 26 8 -6 9 14.4456 85.3803 21 8 -5 -10 153.800 71.9173 23 8 -5 -9 293.631 97.5400 23 8 -5 -8 82.8939 81.8440 23 8 -5 -8 79.4021 91.3241 19 8 -5 -7 3293.84 287.554 23 8 -5 -7 2502.05 278.467 19 8 -5 -6 1226.53 187.241 23 8 -5 -6 1273.07 213.261 19 8 -5 -5 430.312 127.842 23 8 -5 -5 579.633 163.523 19 8 -5 -4 6936.56 452.929 19 8 -5 -3 6168.27 420.436 19 8 -5 -2 1129.18 200.951 21 8 -5 -2 1267.00 209.863 19 8 -5 -1 5136.24 387.762 21 8 -5 0 112.783 104.148 21 8 -5 1 211.991 110.868 24 8 -5 1 87.0449 109.953 21 8 -5 2 342.318 142.300 21 8 -5 3 931.963 206.253 21 8 -5 4 43.1093 103.040 21 8 -5 5 209.659 130.862 21 8 -5 6 8337.55 492.389 21 8 -5 7 5732.79 399.949 21 8 -5 8 857.104 168.872 21 8 -5 9-7.56421 71.6466 26 8 -5 9-91.3278 94.9849 21 8 -4 -10 80.7414 71.2956 23 8 -4 -9 232.335 102.181 23 8 -4 -8 408.184 127.364 23 8 -4 -7 466.358 131.803 23 8 -4 -7 578.133 155.323 19 8 -4 -6 5593.40 389.134 23 8 -4 -6 6120.23 433.040 19 8 -4 -5 1027.45 182.004 23 8 -4 -5 854.537 190.879 19 8 -4 -4 17277.0 669.848 23 8 -4 -4 17236.8 709.238 19 8 -4 -3 733.621 150.530 23 8 -4 -2 3678.02 332.387 21 8 -4 -1 2427.52 277.806 21 8 -4 0 2328.72 270.199 21 8 -4 1 17745.6 716.252 21 8 -4 2 16146.4 691.758 21 8 -4 3 8090.82 499.824 21 8 -4 4 3458.80 337.910 21 8 -4 5 3134.00 315.577 21 8 -4 6 52.4923 113.973 21 8 -4 7 795.402 170.862 21 8 -4 8 20.3086 101.913 21 8 -4 9 219.130 90.7688 26 8 -3 -11 120.217 66.7721 23 8 -3 -10 163.219 94.3208 23 8 -3 -9 376.588 123.783 23 8 -3 -8 201.277 109.289 23 8 -3 -8 283.880 109.469 22 8 -3 -7 49.7879 87.5889 23 8 -3 -7-38.2118 86.3844 22 8 -3 -6 8352.18 480.020 23 8 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6969.55 435.672 22 8 -2 -5 936.938 174.208 28 8 -2 -5 989.570 191.772 23 8 -2 -5 1100.04 192.725 22 8 -2 -4 554.080 143.210 28 8 -2 -4 364.359 133.814 23 8 -2 -4 131.474 93.5193 21 8 -2 -3 7603.25 443.706 28 8 -2 -3 7036.44 447.366 21 8 -2 -2 13719.4 590.355 28 8 -2 -2 13312.4 602.770 21 8 -2 -1 8845.62 487.829 28 8 -2 -1 8340.69 485.888 21 8 -2 0 947.802 177.332 28 8 -2 0 1116.43 193.453 21 8 -2 1 394.357 128.634 28 8 -2 1 118.170 101.873 21 8 -2 2-6.86148 87.3383 28 8 -2 2 2.98598 99.7850 21 8 -2 3-75.0063 112.470 28 8 -2 3-43.2320 109.640 21 8 -2 4 571.874 148.194 28 8 -2 4 794.796 174.791 21 8 -2 5 380.794 126.753 28 8 -2 5 458.918 143.908 21 8 -2 6 167.185 107.952 28 8 -2 6 64.1484 80.4914 21 8 -2 7 585.034 130.826 28 8 -2 7 623.909 139.685 21 8 -2 8 50.4962 64.3231 28 8 -1 -11 140.228 78.3574 28 8 -1 -11 42.6022 69.9670 23 8 -1 -11-58.4666 76.6987 22 8 -1 -10 786.544 138.707 28 8 -1 -10 524.065 123.230 23 8 -1 -10 566.995 125.389 22 8 -1 -9 50.2186 84.4478 28 8 -1 -9-47.9994 80.2434 23 8 -1 -9-123.650 109.752 22 8 -1 -8 1793.71 218.525 28 8 -1 -8 1713.61 226.820 23 8 -1 -8 1815.57 226.989 22 8 -1 -7 1062.53 181.567 28 8 -1 -7 1072.21 193.653 23 8 -1 -7 850.719 173.327 22 8 -1 -6 972.554 182.474 28 8 -1 -6 1041.86 183.525 23 8 -1 -6 942.145 175.074 22 8 -1 -5 78.8472 95.8902 28 8 -1 -5-15.4225 84.3066 23 8 -1 -4 1601.48 215.828 28 8 -1 -4 1363.87 202.245 21 8 -1 -3 2519.10 270.102 28 8 -1 -3 2001.48 245.889 21 8 -1 -2 11417.0 551.200 28 8 -1 -2 10793.2 535.003 21 8 -1 -1 9937.68 518.816 28 8 -1 -1 9423.29 505.075 21 8 -1 0 4448.38 362.033 28 8 -1 0 4853.89 369.462 21 8 -1 1-99.5640 106.244 28 8 -1 1-19.2873 96.6129 21 8 -1 2 4608.65 363.821 28 8 -1 2 5051.08 373.663 21 8 -1 3 6080.92 415.104 28 8 -1 3 5741.77 389.124 21 8 -1 4 3430.46 309.098 28 8 -1 4 2993.05 280.274 21 8 -1 5 266.473 110.202 28 8 -1 5 300.852 113.232 21 8 -1 6 230.833 106.328 28 8 -1 6 177.321 91.8401 21 8 -1 7 49.1785 70.8621 28 8 0 -11 175.655 84.8992 28 8 0 -11 75.0195 71.2128 22 8 0 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115.736 28 8 1 -1 3394.32 311.485 28 8 1 0 883.878 169.039 28 8 1 1-5.93785 89.6269 28 8 1 2 1708.24 219.010 28 8 1 3 969.006 170.013 28 8 1 4 701.715 137.650 28 8 1 5 507.648 116.065 28 8 2 -10 134.708 85.5475 28 8 2 -9 266.922 102.939 28 8 2 -8 1046.38 164.212 28 8 2 -7 479.422 127.348 28 8 2 -6 64.0609 87.7940 28 8 2 -5 542.820 137.050 28 8 2 -4 48.8685 83.5511 28 8 2 -3 34.1190 93.4372 28 8 2 -2 298.636 113.768 28 8 2 -1 43.7058 82.0763 28 8 2 0 1365.30 194.940 28 8 2 1 105.522 92.5366 28 8 2 2 119.045 85.7346 28 8 2 3 113.038 81.7828 28 8 2 4 48.8842 57.9530 28 8 3 -9 22.7120 73.4479 28 8 3 -8 262.590 99.9202 28 8 3 -7 26.1016 79.3099 28 8 3 -6 16.5177 77.8021 28 8 3 -5 531.826 134.179 28 8 3 -4 1047.19 167.076 28 8 3 -3 181.100 98.1123 28 8 3 -2-12.8766 79.6908 28 8 3 -1 643.598 135.388 28 8 3 0 696.922 132.690 28 8 3 1 10.5647 61.3806 28 8 3 2 215.673 78.4487 28 8 4 -7 547.276 103.177 28 8 4 -6 133.121 73.6002 28 8 4 -5 58.9058 65.3219 28 8 4 -4 958.894 141.379 28 8 4 -3 87.5974 74.7770 28 8 4 -2 3.50541 63.3016 28 8 4 -1 412.869 95.2094 28 9 -11 0 1747.98 177.914 24 9 -11 1 56.7940 71.6512 27 9 -11 1 55.0214 75.5068 24 9 -11 2 1606.81 181.111 27 9 -11 3 228.266 101.043 27 9 -11 3 15.9442 87.2554 20 9 -11 4 1182.00 160.273 27 9 -11 4 895.723 133.741 20 9 -11 5 1342.28 156.685 27 9 -11 5 1430.10 157.899 20 9 -10 -3 136.455 78.6416 24 9 -10 -2 210.422 88.9547 24 9 -10 -1 341.648 105.041 27 9 -10 -1 199.359 92.8440 24 9 -10 0 633.200 137.214 27 9 -10 0 509.255 130.259 24 9 -10 1 244.258 110.229 27 9 -10 1 279.705 106.229 24 9 -10 2 242.761 107.098 27 9 -10 2 298.735 112.699 24 9 -10 3 541.336 132.284 27 9 -10 4 1041.07 163.661 27 9 -10 5 15.0598 79.6941 27 9 -10 6 396.441 106.200 27 9 -9 -5 21.0155 59.5192 24 9 -9 -5 143.886 74.3112 19 9 -9 -4 110.053 74.4591 24 9 -9 -4 156.391 86.0874 19 9 -9 -3 656.492 129.416 24 9 -9 -3 538.232 119.758 19 9 -9 -2 1088.75 160.583 27 9 -9 -2 995.663 162.527 24 9 -9 -1 76.7622 94.6420 27 9 -9 -1 205.858 103.790 24 9 -9 0 58.9580 89.9077 24 9 -9 1-127.937 136.461 27 9 -9 1 49.1920 90.1791 24 9 -9 2-134.997 132.232 27 9 -9 2 30.6692 101.679 24 9 -9 3 284.302 120.400 27 9 -9 4 406.317 135.124 27 9 -9 5 1650.73 202.403 27 9 -9 6 27.6163 75.3530 27 9 -9 7 197.870 85.7008 27 9 -8 -6 64.7628 68.4731 19 9 -8 -5 6.59752 62.1147 24 9 -8 -5 111.408 92.5805 21 9 -8 -5 70.2638 77.8803 19 9 -8 -4 187.317 79.0831 24 9 -8 -4 131.566 84.6990 21 9 -8 -4 279.206 109.049 19 9 -8 -3-7.90379 82.4307 24 9 -8 -3 19.9457 85.4293 21 9 -8 -3 95.2102 90.1201 19 9 -8 -2 691.257 155.598 24 9 -8 -2 791.652 153.986 21 9 -8 -1 511.846 134.507 24 9 -8 -1 509.435 134.446 21 9 -8 0 1032.76 179.992 24 9 -8 0 1234.34 188.595 21 9 -8 1 48.2036 86.6123 24 9 -8 1 76.9931 98.6946 21 9 -8 2 1474.41 222.628 24 9 -8 2 1213.72 185.573 21 9 -8 3 1848.31 227.137 21 9 -8 4 30.2646 100.512 27 9 -8 4 241.983 114.322 21 9 -8 5 5244.44 349.521 27 9 -8 5 6070.19 366.166 21 9 -8 6 2148.58 211.176 27 9 -8 6 2889.08 248.085 21 9 -8 7 469.419 113.949 26 9 -8 7 428.821 114.649 21 9 -8 8 3466.43 220.827 26 9 -8 8 3134.01 209.729 21 9 -7 -7 11.1445 67.9106 21 9 -7 -6 29.4155 80.8677 21 9 -7 -6 163.685 97.0524 19 9 -7 -5 193.407 100.119 21 9 -7 -5 42.2895 89.9594 19 9 -7 -4 130.801 87.8023 21 9 -7 -4 282.633 114.322 19 9 -7 -3 284.212 117.862 21 9 -7 -3 49.0282 93.3139 19 9 -7 -2 73.6111 83.6443 24 9 -7 -2 130.381 104.344 21 9 -7 -1 826.869 164.018 24 9 -7 -1 756.834 158.291 21 9 -7 0 218.336 109.902 24 9 -7 0 125.482 112.971 21 9 -7 1 85.0599 91.0347 24 9 -7 1 20.3078 98.1194 21 9 -7 2 4687.72 374.649 21 9 -7 3 158.723 119.528 21 9 -7 4 657.979 170.983 21 9 -7 5 970.875 172.439 27 9 -7 5 983.185 181.218 21 9 -7 6 366.885 133.122 21 9 -7 7 81.9826 78.7847 26 9 -7 7-18.5003 85.3132 21 9 -7 8 1166.86 150.694 26 9 -7 8 1430.09 169.199 21 9 -6 -8 1150.61 151.912 21 9 -6 -7 23.1864 77.0730 21 9 -6 -6 1624.94 204.305 21 9 -6 -5 1147.55 185.581 21 9 -6 -5 978.779 179.923 19 9 -6 -4 219.382 123.912 21 9 -6 -3 48.6185 88.7448 21 9 -6 -2-84.7640 101.365 21 9 -6 -1 2092.21 256.757 21 9 -6 0 2418.46 272.396 21 9 -6 1 470.833 150.604 21 9 -6 2 3330.05 319.183 21 9 -6 3 2059.03 260.389 21 9 -6 4 129.222 127.187 21 9 -6 5 69.7061 98.7870 21 9 -6 6 2132.68 242.344 21 9 -6 7 1135.09 176.441 21 9 -6 8 81.7263 72.2592 26 9 -6 8 6.27136 78.5353 21 9 -5 -9 184.341 66.3891 23 9 -5 -9 215.932 89.1730 21 9 -5 -8 1902.04 187.539 23 9 -5 -7 4921.66 316.214 23 9 -5 -6 3240.41 270.273 23 9 -5 -6 3265.16 297.884 21 9 -5 -5 22.1806 67.9822 23 9 -5 -5 56.1997 98.5074 21 9 -5 -4 1409.91 212.938 21 9 -5 -3 2351.45 268.820 21 9 -5 -2 297.809 129.566 21 9 -5 -1 900.450 183.515 21 9 -5 0 1199.54 205.323 21 9 -5 1-11.1114 100.860 21 9 -5 2 45.8219 115.366 21 9 -5 3 638.692 156.697 21 9 -5 4 3118.78 309.169 21 9 -5 5 1130.70 199.267 21 9 -5 6 0.24604 92.7263 21 9 -5 7 113.854 98.5519 21 9 -5 8 39.5138 70.0984 26 9 -5 8 85.0227 84.4366 21 9 -4 -9 166.480 75.8480 23 9 -4 -8 1523.58 185.849 23 9 -4 -7 252.613 103.015 23 9 -4 -6 509.196 134.991 23 9 -4 -6 448.363 138.216 21 9 -4 -5 167.442 97.1256 23 9 -4 -5 175.726 115.299 21 9 -4 -4 270.806 123.724 21 9 -4 -3 845.956 182.874 21 9 -4 -2 69.5067 96.9310 21 9 -4 -1 336.019 130.190 21 9 -4 0 236.371 119.191 21 9 -4 1 230.263 117.918 21 9 -4 2 1209.21 208.229 21 9 -4 3-69.3175 110.758 21 9 -4 4 1244.79 203.147 21 9 -4 5 1106.21 187.600 21 9 -4 6 647.885 144.953 21 9 -4 7 122.220 90.3890 21 9 -3 -9 280.818 94.9605 23 9 -3 -9 594.288 129.707 21 9 -3 -8-206.584 94.4803 23 9 -3 -7 2819.00 264.249 23 9 -3 -7 2636.43 261.681 21 9 -3 -6 422.078 126.174 23 9 -3 -6 416.105 132.016 21 9 -3 -5 470.305 147.642 21 9 -3 -4 76.0316 98.2647 21 9 -3 -3 119.736 91.1077 21 9 -3 -2 121.896 101.794 21 9 -3 -1 2958.81 301.172 21 9 -3 0 1983.39 232.962 28 9 -3 0 1878.66 245.309 21 9 -3 1 2077.99 234.516 28 9 -3 1 1873.74 245.347 21 9 -3 2 4021.51 321.965 28 9 -3 2 3957.57 337.503 21 9 -3 3 458.249 131.316 28 9 -3 3 474.369 144.042 21 9 -3 4 1150.58 176.695 28 9 -3 4 1427.28 203.294 21 9 -3 5 768.304 137.550 28 9 -3 5 743.575 160.618 21 9 -3 6 319.715 99.6535 28 9 -3 6 208.420 101.331 21 9 -3 7 141.228 63.9799 28 9 -3 7 390.466 100.133 21 9 -2 -9 554.022 107.346 28 9 -2 -9 717.801 126.511 21 9 -2 -8 455.040 112.456 28 9 -2 -8 395.102 118.079 23 9 -2 -8 380.643 110.587 21 9 -2 -7 1462.45 184.597 28 9 -2 -7 1633.00 205.771 21 9 -2 -6 830.410 155.063 28 9 -2 -6 948.484 166.292 21 9 -2 -5 1069.37 175.162 28 9 -2 -5 1024.17 174.612 21 9 -2 -4 316.337 117.586 28 9 -2 -4 261.154 109.122 21 9 -2 -3 1799.25 223.220 28 9 -2 -3 1893.99 228.557 21 9 -2 -2 861.964 158.051 28 9 -2 -2 900.907 163.613 21 9 -2 -1 3750.30 315.878 28 9 -2 -1 4011.17 334.888 21 9 -2 0 55.8452 88.9898 28 9 -2 0 199.714 109.042 21 9 -2 1 2708.90 278.666 28 9 -2 1 2920.13 287.816 21 9 -2 2 3253.41 289.621 28 9 -2 2 3759.01 315.550 21 9 -2 3 4162.42 317.390 28 9 -2 3 3454.68 299.288 21 9 -2 4 464.141 125.570 28 9 -2 4 526.289 135.836 21 9 -2 5 110.012 90.9167 28 9 -2 5 91.1445 76.9805 21 9 -2 6 72.9804 66.0098 28 9 -2 6-62.8471 69.2132 21 9 -1 -9 101.278 84.7141 28 9 -1 -8 2.17904 72.3674 28 9 -1 -8 0.19738 69.4877 21 9 -1 -7 9.00581 71.8799 28 9 -1 -7-37.1703 89.0177 21 9 -1 -6-97.8826 88.3211 28 9 -1 -6-34.4229 86.7898 21 9 -1 -5-56.4860 98.8493 28 9 -1 -5 174.942 94.3363 21 9 -1 -4 185.915 92.0239 28 9 -1 -4 283.747 109.580 21 9 -1 -3 278.906 107.836 28 9 -1 -2 26.5170 86.7414 28 9 -1 -1 2215.98 248.817 28 9 -1 0 1606.01 221.144 28 9 -1 1 748.974 158.234 28 9 -1 2 12.6010 84.3180 28 9 -1 3 93.7548 92.9883 28 9 -1 4 623.523 134.194 28 9 -1 5 291.694 100.771 28 9 0 -9 302.488 94.3199 28 9 0 -8 207.991 92.4318 28 9 0 -7 488.087 121.643 28 9 0 -6 2296.75 234.955 28 9 0 -5 686.304 144.929 28 9 0 -4 49.6027 83.5978 28 9 0 -3 58.1402 91.4380 28 9 0 -2 112.458 93.6719 28 9 0 -1 165.449 107.480 28 9 0 0 64.2291 93.2976 28 9 0 1 21.9505 81.2482 28 9 0 2 202.108 101.371 28 9 0 3 277.564 100.277 28 9 0 4 42.1928 70.7958 28 9 1 -8-46.1386 72.2598 28 9 1 -7 876.956 142.432 28 9 1 -6 616.933 136.827 28 9 1 -5 23.4249 87.8202 28 9 1 -4-43.8753 79.3036 28 9 1 -3 12.6572 75.6137 28 9 1 -2 409.251 121.973 28 9 1 -1 115.047 82.9808 28 9 1 0 275.135 103.640 28 9 1 1 129.988 91.8330 28 9 1 2 109.929 75.9656 28 9 2 -7 216.644 84.4371 28 9 2 -6 381.764 106.261 28 9 2 -5 122.833 82.1410 28 9 2 -4 61.5090 74.0989 28 9 2 -3-46.8957 86.5877 28 9 2 -2 113.173 89.8546 28 9 2 -1 321.519 97.6123 28 9 2 0-34.9107 66.0778 28 10 -10 0 270.092 89.1389 27 10 -10 1 1009.17 140.499 27 10 -10 2 1269.84 158.889 27 10 -10 3 1069.11 143.074 27 10 -9 -3 659.659 105.615 24 10 -9 -2 161.581 89.6523 27 10 -9 -2 157.032 78.8427 24 10 -9 -1 107.803 87.1487 27 10 -9 -1 294.718 106.526 24 10 -9 0-79.9464 113.793 27 10 -9 1-58.6230 88.3362 27 10 -9 2 61.5700 91.6247 27 10 -9 3-60.4335 82.3699 27 10 -9 4-120.960 91.2897 27 10 -9 5 1467.13 156.611 27 10 -8 -4 76.0297 73.3080 21 10 -8 -3 1297.88 163.121 21 10 -8 -2 56.6084 78.4335 21 10 -8 -1 422.548 117.895 24 10 -8 -1 244.839 102.724 21 10 -8 0 601.060 124.119 21 10 -8 1 768.186 150.392 21 10 -8 2 188.846 106.171 21 10 -8 3-157.101 118.863 27 10 -8 3-66.6453 91.1527 21 10 -8 4 1442.25 177.138 27 10 -8 4 1457.99 175.395 21 10 -8 5 616.519 108.432 27 10 -8 5 821.708 130.836 21 10 -8 6 183.912 86.1613 21 10 -7 -6 292.042 89.3662 21 10 -7 -5 920.620 142.000 21 10 -7 -4 202.740 100.483 21 10 -7 -3 73.7246 79.7667 21 10 -7 -2 603.796 141.962 21 10 -7 -1-70.2315 103.298 21 10 -7 0 41.1517 104.962 21 10 -7 1 30.3411 93.8161 21 10 -7 2 234.815 120.814 21 10 -7 3 352.889 128.675 21 10 -7 4 3489.81 259.274 27 10 -7 4 3431.07 278.840 21 10 -7 5 217.624 102.910 21 10 -7 6 233.282 80.9338 26 10 -7 6 168.456 86.3208 21 10 -6 -6 216.726 93.6370 21 10 -6 -5 950.558 162.876 21 10 -6 -4-12.2633 80.9092 21 10 -6 -3 722.606 152.904 21 10 -6 -2 97.3731 107.547 21 10 -6 -1-70.7134 101.093 21 10 -6 0 1148.83 192.756 21 10 -6 1 632.063 148.244 21 10 -6 2 145.355 114.636 21 10 -6 3 540.666 144.247 21 10 -6 4-43.6707 101.776 21 10 -6 5 581.413 135.864 21 10 -6 6 511.675 117.187 21 10 -5 -7 1314.50 162.200 21 10 -5 -6 2639.12 238.205 21 10 -5 -5 161.941 93.6361 21 10 -5 -4 130.439 96.3150 21 10 -5 -3 1140.11 187.188 21 10 -5 -2-22.6870 87.1579 21 10 -5 -1 954.631 176.164 21 10 -5 0 208.413 116.018 21 10 -5 1 148.313 110.915 21 10 -5 2 184.642 119.097 21 10 -5 3 391.745 135.968 21 10 -5 4 1539.54 195.109 21 10 -5 5 1199.16 166.462 21 10 -4 -7 869.930 136.762 21 10 -4 -6 53.5206 89.5995 21 10 -4 -5 204.512 108.765 21 10 -4 -4 752.100 158.704 21 10 -4 -3 121.011 99.8760 21 10 -4 -2 194.566 116.686 21 10 -4 -1-120.036 115.775 21 10 -4 0 45.2960 88.2419 21 10 -4 1-46.1605 89.0251 21 10 -4 2-71.3262 93.8283 21 10 -4 3 118.266 87.9309 21 10 -4 4 103.423 90.8498 21 10 -4 5 150.186 90.9164 21 10 -3 -8 823.644 124.003 21 10 -3 -7 25.5771 71.9896 21 10 -3 -6 547.127 126.083 21 10 -3 -5 16.3355 81.3031 21 10 -3 -4 167.491 95.5295 21 10 -3 -3 339.181 116.726 21 10 -3 -2-0.49298 98.6545 21 10 -3 -1-3.94479 97.6772 21 10 -3 0 5.81441 92.1307 21 10 -3 1 356.098 128.593 21 10 -3 2 1499.90 191.277 21 10 -3 3 1136.10 161.461 21 10 -3 4 88.4883 75.6036 21 10 -2 -7-123.559 80.0957 28 10 -2 -7-13.6708 57.5286 21 10 -2 -6 9.45649 66.8881 28 10 -2 -6 79.7500 88.0561 21 10 -2 -5-32.9795 72.4480 28 10 -2 -5 104.633 74.9201 21 10 -2 -4 199.918 90.0657 28 10 -2 -4 137.984 85.8463 21 10 -2 -3 60.0106 76.3436 28 10 -2 -3-27.8805 83.3799 21 10 -2 -2 424.878 119.901 28 10 -2 -2 250.588 88.2161 21 10 -2 -1 123.168 95.7526 28 10 -2 -1 62.2846 90.2910 21 10 -2 0 2324.05 224.181 28 10 -2 0 2441.68 226.649 21 10 -2 1 3027.05 243.362 28 10 -2 1 3179.93 250.022 21 10 -2 2 1234.10 157.533 28 10 -2 2 1375.29 160.146 21 10 -2 3 18.3015 67.1120 28 10 -1 -7-44.3958 67.3098 28 10 -1 -6 74.5054 75.6302 28 10 -1 -5 573.163 121.349 28 10 -1 -4 316.869 97.3346 28 10 -1 -3 132.662 89.2071 28 10 -1 -2 37.8239 72.8718 28 10 -1 -1 361.430 110.848 28 10 -1 0 245.773 98.2959 28 10 -1 1 395.856 108.190 28 10 -1 2 885.964 127.539 28 10 0 -6 1152.05 141.855 28 10 0 -5 10.5189 72.3155 28 10 0 -4 149.490 84.2923 28 10 0 -3 695.996 129.613 28 10 0 -2 1266.54 160.832 28 10 0 -1-3.93137 68.5748 28 10 0 0-79.4130 72.6891 28 11 -8 0 520.307 106.352 21 11 -8 1-181.055 85.8384 27 11 -8 1 14.6060 69.4408 21 11 -7 -3 37.0804 69.7151 21 11 -7 -2 166.986 86.2919 21 11 -7 -1 6.84248 73.0687 21 11 -7 0-78.0722 92.1482 21 11 -7 1 72.7452 77.1385 21 11 -7 2 536.706 104.046 27 11 -7 2 466.729 111.322 21 11 -6 -4 406.678 104.895 21 11 -6 -3 353.065 102.417 21 11 -6 -2 29.7709 88.7656 21 11 -6 -1 475.684 119.038 21 11 -6 0 477.653 114.166 21 11 -6 1-68.1645 86.6048 21 11 -6 2 258.699 100.406 21 11 -5 -4-28.2571 79.0247 21 11 -5 -3 50.5885 73.8862 21 11 -5 -2 1359.35 169.835 21 11 -5 -1 873.157 147.533 21 11 -5 0 89.0742 84.0394 21 11 -5 1 158.102 88.6223 21 11 -5 2 317.793 101.307 21 11 -4 -4 224.408 87.2474 21 11 -4 -3-94.4801 78.1004 21 11 -4 -2-11.1313 69.8970 21 11 -4 -1 304.015 95.6166 21 11 -4 0 195.742 98.1495 21 11 -4 1 4.69824 68.1941 21 11 -3 -4 47.8534 65.4015 21 11 -3 -3 691.316 115.717 21 11 -3 -2-72.5780 76.2560 21 11 -3 -1 508.074 103.659 21 11 -3 0 762.432 114.624 21 0 0 0 0.00 0.00 0 TITL zzy119 in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 9.521550 10.782304 12.633213 106.1775 93.8002 114.6144 ZERR 3.00 0.000264 0.000403 0.000527 0.0035 0.0028 0.0031 LATT 1 SFAC C H N O UNIT 42.00 45.00 6.00 12.00 TREF HKLF 4 END ; _shelx_hkl_checksum 63701 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.244 _oxdiff_exptl_absorpt_empirical_full_min 0.883 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.89738(19) 0.31207(18) 0.50692(17) 0.0676(5) Uani 1 1 d . . . . . O2 O 0.5901(4) -0.3333(3) 0.1411(2) 0.1162(10) Uani 1 1 d . . . . . O3 O 0.8335(4) -0.1799(3) 0.2243(2) 0.1010(9) Uani 1 1 d . . . . . N1 N 0.8373(2) 0.4069(2) 0.37849(19) 0.0578(5) Uani 1 1 d . . . . . H1 H 0.9039 0.4964 0.4120 0.069 Uiso 1 1 calc R . . . . N2 N 0.4428(2) -0.05588(19) 0.31626(17) 0.0556(5) Uani 1 1 d . . . . . N3 N 0.6913(4) -0.2119(3) 0.2005(2) 0.0836(8) Uani 1 1 d . . . . . N4 N 1.1080(7) 0.2046(7) 0.1508(5) 0.0908(17) Uani 0.763(5) 1 d D U P A 1 N4A N 1.057(3) 0.169(3) 0.108(2) 0.0908(17) Uani 0.237(5) 1 d . . P A 2 C1 C 0.8214(2) 0.2996(2) 0.4190(2) 0.0521(5) Uani 1 1 d . . . . . C2 C 0.6917(3) 0.1563(2) 0.33495(19) 0.0478(5) Uani 1 1 d . . . . . C3 C 0.6406(3) 0.2055(2) 0.24592(19) 0.0511(5) Uani 1 1 d . . . . . C4 C 0.7327(3) 0.3553(2) 0.2755(2) 0.0516(5) Uani 1 1 d . . . . . C5 C 0.7174(3) 0.4325(3) 0.2093(2) 0.0612(6) Uani 1 1 d . . . . . H5 H 0.7798 0.5322 0.2310 0.073 Uiso 1 1 calc R . . . . C6 C 0.6066(4) 0.3574(3) 0.1098(2) 0.0733(8) Uani 1 1 d . . . . . H6 H 0.5936 0.4068 0.0633 0.088 Uiso 1 1 calc R . . . . C7 C 0.5146(4) 0.2093(3) 0.0782(2) 0.0796(9) Uani 1 1 d . . . . . H7 H 0.4410 0.1605 0.0103 0.096 Uiso 1 1 calc R . . . . C8 C 0.5299(4) 0.1315(3) 0.1462(2) 0.0686(7) Uani 1 1 d . . . . . H8 H 0.4668 0.0320 0.1246 0.082 Uiso 1 1 calc R . . . . C9 C 0.5605(2) 0.0844(2) 0.39509(18) 0.0448(5) Uani 1 1 d . . . . . H9 H 0.6084 0.0673 0.4572 0.054 Uiso 1 1 calc R . . . . C10 C 0.2793(3) -0.0823(3) 0.3183(3) 0.0709(7) Uani 1 1 d . . . . . H10A H 0.2240 -0.1626 0.3446 0.085 Uiso 1 1 calc R . . . . H10B H 0.2219 -0.1017 0.2444 0.085 Uiso 1 1 calc R . . . . C11 C 0.3015(3) 0.0579(3) 0.4000(2) 0.0597(6) Uani 1 1 d . . . . . C12 C 0.4598(3) 0.1551(2) 0.43977(18) 0.0486(5) Uani 1 1 d . . . . . C13 C 0.5047(3) 0.2914(3) 0.5165(2) 0.0631(6) Uani 1 1 d . . . . . H13 H 0.6111 0.3575 0.5423 0.076 Uiso 1 1 calc R . . . . C14 C 0.3899(4) 0.3285(4) 0.5544(3) 0.0821(9) Uani 1 1 d . . . . . H14 H 0.4191 0.4203 0.6055 0.099 Uiso 1 1 calc R . . . . C15 C 0.2325(4) 0.2302(4) 0.5169(3) 0.0896(10) Uani 1 1 d . . . . . H15 H 0.1564 0.2556 0.5442 0.108 Uiso 1 1 calc R . . . . C16 C 0.1864(3) 0.0947(4) 0.4394(3) 0.0819(9) Uani 1 1 d . . . . . H16 H 0.0800 0.0290 0.4139 0.098 Uiso 1 1 calc R . . . . C17 C 0.4915(3) -0.1446(2) 0.2528(2) 0.0622(7) Uani 1 1 d . . . . . H17 H 0.4181 -0.2389 0.2102 0.075 Uiso 1 1 calc R . . . . C18 C 0.6453(4) -0.1006(3) 0.2489(2) 0.0630(7) Uani 1 1 d . . . . . C19 C 0.7694(3) 0.0521(3) 0.2952(3) 0.0633(7) Uani 1 1 d . . . . . H19 H 0.834(4) 0.069(3) 0.363(3) 0.076 Uiso 1 1 d R . . . . C20 C 0.8552(4) 0.0878(3) 0.1997(3) 0.0577(8) Uani 0.763(5) 1 d . . P A 1 H20 H 0.7981 0.0558 0.1267 0.069 Uiso 0.763(5) 1 calc R . P A 1 C20A C 0.9309(15) 0.1395(12) 0.2706(10) 0.0577(8) Uani 0.237(5) 1 d . . P A 2 H20A H 1.0168 0.2069 0.3288 0.069 Uiso 0.237(5) 1 calc R . P A 2 C21 C 1.0081(6) 0.1630(5) 0.2229(4) 0.0766(13) Uani 0.763(5) 1 d . . P A 1 H21 H 1.0570 0.1929 0.2979 0.092 Uiso 0.763(5) 1 calc R . P A 1 C21A C 0.9429(18) 0.1164(18) 0.1678(15) 0.0766(13) Uani 0.237(5) 1 d D . P A 2 H21A H 0.8485 0.0441 0.1197 0.092 Uiso 0.237(5) 1 calc R . P A 2 C22 C 1.0428(9) 0.1886(9) 0.0365(6) 0.097(2) Uani 0.763(5) 1 d . U P A 1 H22A H 0.9524 0.0939 0.0032 0.117 Uiso 0.763(5) 1 calc R . P A 1 H22B H 1.1218 0.1929 -0.0090 0.117 Uiso 0.763(5) 1 calc R . P A 1 C22A C 0.986(4) 0.170(3) 0.000(2) 0.097(2) Uani 0.237(5) 1 d . . P A 2 H22C H 1.0328 0.1392 -0.0615 0.117 Uiso 0.237(5) 1 calc R . P A 2 H22D H 0.8725 0.1129 -0.0195 0.117 Uiso 0.237(5) 1 calc R . P A 2 C23 C 0.9899(11) 0.3085(14) 0.0327(16) 0.106(2) Uani 0.763(5) 1 d . U P A 1 H23A H 0.9606 0.3011 -0.0447 0.127 Uiso 0.763(5) 1 calc R . P A 1 H23B H 0.8999 0.2971 0.0680 0.127 Uiso 0.763(5) 1 calc R . P A 1 C23A C 1.032(4) 0.315(5) 0.034(6) 0.106(2) Uani 0.237(5) 1 d D . P A 2 H23C H 0.9709 0.3284 0.0911 0.127 Uiso 0.237(5) 1 calc R . P A 2 H23D H 0.9849 0.3271 -0.0300 0.127 Uiso 0.237(5) 1 calc R . P A 2 C24 C 1.1295(9) 0.4523(9) 0.0960(7) 0.116(2) Uani 0.763(5) 1 d . U P A 1 H24A H 1.0977 0.5285 0.1038 0.139 Uiso 0.763(5) 1 calc R . P A 1 H24B H 1.2115 0.4686 0.0523 0.139 Uiso 0.763(5) 1 calc R . P A 1 C24A C 1.188(3) 0.451(3) 0.080(3) 0.116(2) Uani 0.237(5) 1 d D . P A 2 H24C H 1.2625 0.4472 0.0316 0.139 Uiso 0.237(5) 1 calc R . P A 2 H24D H 1.1741 0.5364 0.0867 0.139 Uiso 0.237(5) 1 calc R . P A 2 C25 C 1.1976(11) 0.4627(10) 0.2129(8) 0.120(2) Uani 0.763(5) 1 d . U P A 1 H25A H 1.2900 0.5558 0.2475 0.144 Uiso 0.763(5) 1 calc R . P A 1 H25B H 1.1199 0.4580 0.2596 0.144 Uiso 0.763(5) 1 calc R . P A 1 C25A C 1.242(4) 0.448(3) 0.193(3) 0.120(2) Uani 0.237(5) 1 d D . P A 2 H25C H 1.1724 0.4582 0.2439 0.144 Uiso 0.237(5) 1 calc R . P A 2 H25D H 1.3495 0.5213 0.2277 0.144 Uiso 0.237(5) 1 calc R . P A 2 C26 C 1.2431(9) 0.3436(8) 0.2091(6) 0.113(2) Uani 0.763(5) 1 d . U P A 1 H26A H 1.3296 0.3541 0.1700 0.135 Uiso 0.763(5) 1 calc R . P A 1 H26B H 1.2779 0.3496 0.2851 0.135 Uiso 0.763(5) 1 calc R . P A 1 C26A C 1.228(3) 0.297(3) 0.156(2) 0.113(2) Uani 0.237(5) 1 d D . P A 2 H26C H 1.2762 0.2836 0.2194 0.135 Uiso 0.237(5) 1 calc R . P A 2 H26D H 1.2898 0.2893 0.0980 0.135 Uiso 0.237(5) 1 calc R . P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0501(9) 0.0521(9) 0.0927(13) 0.0329(9) -0.0044(8) 0.0135(7) O2 0.199(3) 0.0638(13) 0.0939(17) 0.0084(12) 0.0197(18) 0.0796(17) O3 0.146(2) 0.0890(16) 0.130(2) 0.0617(15) 0.0795(18) 0.0870(17) N1 0.0503(10) 0.0399(9) 0.0821(14) 0.0262(9) 0.0117(9) 0.0165(8) N2 0.0565(11) 0.0406(9) 0.0594(11) 0.0147(8) 0.0053(9) 0.0149(8) N3 0.153(3) 0.0663(15) 0.0727(15) 0.0393(13) 0.0491(17) 0.0739(18) N4 0.096(4) 0.103(4) 0.122(5) 0.068(4) 0.062(3) 0.065(3) N4A 0.096(4) 0.103(4) 0.122(5) 0.068(4) 0.062(3) 0.065(3) C1 0.0406(11) 0.0445(11) 0.0755(15) 0.0268(10) 0.0134(10) 0.0189(9) C2 0.0529(12) 0.0396(10) 0.0573(12) 0.0214(9) 0.0178(9) 0.0227(9) C3 0.0687(14) 0.0422(11) 0.0536(12) 0.0203(9) 0.0234(10) 0.0313(10) C4 0.0581(13) 0.0459(11) 0.0631(13) 0.0236(10) 0.0251(10) 0.0297(10) C5 0.0784(16) 0.0472(12) 0.0775(16) 0.0327(12) 0.0324(13) 0.0365(12) C6 0.119(2) 0.0684(16) 0.0615(15) 0.0349(13) 0.0303(15) 0.0591(17) C7 0.130(3) 0.0646(16) 0.0488(13) 0.0179(12) 0.0097(15) 0.0510(17) C8 0.106(2) 0.0431(12) 0.0528(13) 0.0121(10) 0.0129(13) 0.0327(13) C9 0.0454(11) 0.0395(10) 0.0478(11) 0.0170(8) 0.0071(8) 0.0167(8) C10 0.0486(13) 0.0678(16) 0.0805(17) 0.0297(14) -0.0044(12) 0.0116(12) C11 0.0511(13) 0.0718(15) 0.0676(15) 0.0409(13) 0.0096(10) 0.0278(11) C12 0.0506(12) 0.0548(12) 0.0504(11) 0.0262(10) 0.0138(9) 0.0272(10) C13 0.0690(15) 0.0636(15) 0.0593(14) 0.0171(11) 0.0185(11) 0.0339(13) C14 0.104(2) 0.092(2) 0.0791(19) 0.0319(16) 0.0375(17) 0.066(2) C15 0.093(2) 0.121(3) 0.107(3) 0.062(2) 0.0476(19) 0.078(2) C16 0.0532(15) 0.111(2) 0.111(2) 0.066(2) 0.0239(15) 0.0455(16) C17 0.0898(19) 0.0369(11) 0.0540(13) 0.0154(9) 0.0068(12) 0.0245(12) C18 0.106(2) 0.0487(13) 0.0574(13) 0.0270(11) 0.0301(13) 0.0481(14) C19 0.0767(17) 0.0548(13) 0.0871(18) 0.0400(13) 0.0412(14) 0.0424(13) C20 0.073(2) 0.0516(17) 0.0600(19) 0.0216(15) 0.0250(16) 0.0351(16) C20A 0.073(2) 0.0516(17) 0.0600(19) 0.0216(15) 0.0250(16) 0.0351(16) C21 0.087(3) 0.092(3) 0.096(4) 0.060(3) 0.043(2) 0.059(3) C21A 0.087(3) 0.092(3) 0.096(4) 0.060(3) 0.043(2) 0.059(3) C22 0.119(6) 0.089(3) 0.101(5) 0.043(4) 0.058(4) 0.049(4) C22A 0.119(6) 0.089(3) 0.101(5) 0.043(4) 0.058(4) 0.049(4) C23 0.126(6) 0.100(3) 0.110(3) 0.049(2) 0.031(6) 0.059(4) C23A 0.126(6) 0.100(3) 0.110(3) 0.049(2) 0.031(6) 0.059(4) C24 0.138(6) 0.088(3) 0.131(4) 0.067(3) 0.041(4) 0.039(4) C24A 0.138(6) 0.088(3) 0.131(4) 0.067(3) 0.041(4) 0.039(4) C25 0.132(6) 0.106(3) 0.122(4) 0.062(3) 0.032(3) 0.038(3) C25A 0.132(6) 0.106(3) 0.122(4) 0.062(3) 0.032(3) 0.038(3) C26 0.096(3) 0.134(5) 0.129(5) 0.076(4) 0.050(4) 0.048(4) C26A 0.096(3) 0.134(5) 0.129(5) 0.076(4) 0.050(4) 0.048(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 N1 H1 124.0 . . ? C1 N1 C4 111.99(19) . . ? C4 N1 H1 124.0 . . ? C9 N2 C10 113.92(19) . . ? C17 N2 C9 118.9(2) . . ? C17 N2 C10 127.2(2) . . ? O2 N3 O3 123.3(3) . . ? O2 N3 C18 119.6(3) . . ? O3 N3 C18 117.1(3) . . ? C21 N4 C22 120.1(5) . . ? C21 N4 C26 110.8(5) . . ? C26 N4 C22 113.5(6) . . ? C21A N4A C22A 111(2) . . ? C21A N4A C26A 128(2) . . ? C22A N4A C26A 111(2) . . ? O1 C1 N1 126.6(2) . . ? O1 C1 C2 125.20(19) . . ? N1 C1 C2 108.2(2) . . ? C1 C2 C9 109.78(18) . . ? C1 C2 C19 107.18(19) . . ? C3 C2 C1 102.06(17) . . ? C3 C2 C9 114.53(18) . . ? C3 C2 C19 115.52(19) . . ? C9 C2 C19 107.37(17) . . ? C4 C3 C2 108.6(2) . . ? C8 C3 C2 132.4(2) . . ? C8 C3 C4 118.9(2) . . ? C3 C4 N1 109.1(2) . . ? C5 C4 N1 128.1(2) . . ? C5 C4 C3 122.8(2) . . ? C4 C5 H5 121.1 . . ? C4 C5 C6 117.7(2) . . ? C6 C5 H5 121.1 . . ? C5 C6 H6 119.6 . . ? C5 C6 C7 120.7(2) . . ? C7 C6 H6 119.6 . . ? C6 C7 H7 119.4 . . ? C6 C7 C8 121.3(3) . . ? C8 C7 H7 119.4 . . ? C3 C8 C7 118.5(2) . . ? C3 C8 H8 120.7 . . ? C7 C8 H8 120.7 . . ? N2 C9 C2 109.31(17) . . ? N2 C9 H9 108.1 . . ? N2 C9 C12 102.10(17) . . ? C2 C9 H9 108.1 . . ? C12 C9 C2 120.44(17) . . ? C12 C9 H9 108.1 . . ? N2 C10 H10A 111.4 . . ? N2 C10 H10B 111.4 . . ? N2 C10 C11 101.83(19) . . ? H10A C10 H10B 109.3 . . ? C11 C10 H10A 111.4 . . ? C11 C10 H10B 111.4 . . ? C12 C11 C10 111.6(2) . . ? C12 C11 C16 120.3(3) . . ? C16 C11 C10 128.1(3) . . ? C11 C12 C9 110.2(2) . . ? C13 C12 C9 129.3(2) . . ? C13 C12 C11 120.3(2) . . ? C12 C13 H13 120.4 . . ? C12 C13 C14 119.3(3) . . ? C14 C13 H13 120.4 . . ? C13 C14 H14 119.8 . . ? C15 C14 C13 120.3(3) . . ? C15 C14 H14 119.8 . . ? C14 C15 H15 119.6 . . ? C16 C15 C14 120.8(3) . . ? C16 C15 H15 119.6 . . ? C11 C16 H16 120.5 . . ? C15 C16 C11 119.0(3) . . ? C15 C16 H16 120.5 . . ? N2 C17 H17 119.4 . . ? N2 C17 C18 121.3(2) . . ? C18 C17 H17 119.4 . . ? N3 C18 C19 118.5(3) . . ? C17 C18 N3 116.7(3) . . ? C17 C18 C19 124.7(2) . . ? C2 C19 H19 102.6(19) . . ? C18 C19 C2 110.0(2) . . ? C18 C19 H19 111.0(19) . . ? C18 C19 C20 107.6(2) . . ? C18 C19 C20A 135.3(5) . . ? C20 C19 C2 109.2(2) . . ? C20 C19 H19 116.4(19) . . ? C20A C19 C2 108.3(4) . . ? C20A C19 H19 81.8(19) . . ? C19 C20 H20 120.4 . . ? C21 C20 C19 119.1(4) . . ? C21 C20 H20 120.4 . . ? C19 C20A H20A 121.1 . . ? C21A C20A C19 117.7(12) . . ? C21A C20A H20A 121.1 . . ? N4 C21 H21 115.7 . . ? C20 C21 N4 128.7(5) . . ? C20 C21 H21 115.7 . . ? N4A C21A H21A 111.1 . . ? C20A C21A N4A 137.7(18) . . ? C20A C21A H21A 111.1 . . ? N4 C22 H22A 108.9 . . ? N4 C22 H22B 108.9 . . ? N4 C22 C23 113.5(9) . . ? H22A C22 H22B 107.7 . . ? C23 C22 H22A 108.9 . . ? C23 C22 H22B 108.9 . . ? N4A C22A H22C 112.4 . . ? N4A C22A H22D 112.4 . . ? H22C C22A H22D 110.0 . . ? C23A C22A N4A 97(4) . . ? C23A C22A H22C 112.4 . . ? C23A C22A H22D 112.4 . . ? C22 C23 H23A 110.5 . . ? C22 C23 H23B 110.5 . . ? H23A C23 H23B 108.7 . . ? C24 C23 C22 106.3(9) . . ? C24 C23 H23A 110.5 . . ? C24 C23 H23B 110.5 . . ? C22A C23A H23C 103.3 . . ? C22A C23A H23D 103.3 . . ? C22A C23A C24A 135(4) . . ? H23C C23A H23D 105.2 . . ? C24A C23A H23C 103.3 . . ? C24A C23A H23D 103.3 . . ? C23 C24 H24A 108.9 . . ? C23 C24 H24B 108.9 . . ? C23 C24 C25 113.3(10) . . ? H24A C24 H24B 107.7 . . ? C25 C24 H24A 108.9 . . ? C25 C24 H24B 108.9 . . ? C23A C24A H24C 111.2 . . ? C23A C24A H24D 111.2 . . ? H24C C24A H24D 109.1 . . ? C25A C24A C23A 103(4) . . ? C25A C24A H24C 111.2 . . ? C25A C24A H24D 111.2 . . ? C24 C25 H25A 109.1 . . ? C24 C25 H25B 109.1 . . ? H25A C25 H25B 107.8 . . ? C26 C25 C24 112.5(7) . . ? C26 C25 H25A 109.1 . . ? C26 C25 H25B 109.1 . . ? C24A C25A H25C 112.1 . . ? C24A C25A H25D 112.1 . . ? C24A C25A C26A 98(2) . . ? H25C C25A H25D 109.7 . . ? C26A C25A H25C 112.1 . . ? C26A C25A H25D 112.1 . . ? N4 C26 C25 109.2(7) . . ? N4 C26 H26A 109.8 . . ? N4 C26 H26B 109.8 . . ? C25 C26 H26A 109.8 . . ? C25 C26 H26B 109.8 . . ? H26A C26 H26B 108.3 . . ? N4A C26A H26C 108.2 . . ? N4A C26A H26D 108.2 . . ? C25A C26A N4A 116(3) . . ? C25A C26A H26C 108.2 . . ? C25A C26A H26D 108.2 . . ? H26C C26A H26D 107.4 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C1 1.227(3) . ? O2 N3 1.229(4) . ? O3 N3 1.242(4) . ? N1 H1 0.8600 . ? N1 C1 1.348(3) . ? N1 C4 1.399(3) . ? N2 C9 1.461(3) . ? N2 C10 1.464(3) . ? N2 C17 1.328(3) . ? N3 C18 1.439(3) . ? N4 C21 1.386(8) . ? N4 C22 1.468(8) . ? N4 C26 1.448(9) . ? N4A C21A 1.38(3) . ? N4A C22A 1.49(3) . ? N4A C26A 1.57(4) . ? C1 C2 1.537(3) . ? C2 C3 1.502(3) . ? C2 C9 1.545(3) . ? C2 C19 1.578(3) . ? C3 C4 1.400(3) . ? C3 C8 1.378(4) . ? C4 C5 1.373(3) . ? C5 H5 0.9300 . ? C5 C6 1.376(4) . ? C6 H6 0.9300 . ? C6 C7 1.382(4) . ? C7 H7 0.9300 . ? C7 C8 1.396(4) . ? C8 H8 0.9300 . ? C9 H9 0.9800 . ? C9 C12 1.504(3) . ? C10 H10A 0.9700 . ? C10 H10B 0.9700 . ? C10 C11 1.493(4) . ? C11 C12 1.383(3) . ? C11 C16 1.390(4) . ? C12 C13 1.382(3) . ? C13 H13 0.9300 . ? C13 C14 1.383(4) . ? C14 H14 0.9300 . ? C14 C15 1.377(5) . ? C15 H15 0.9300 . ? C15 C16 1.377(5) . ? C16 H16 0.9300 . ? C17 H17 0.9300 . ? C17 C18 1.347(4) . ? C18 C19 1.483(4) . ? C19 H19 0.94(3) . ? C19 C20 1.550(4) . ? C19 C20A 1.540(12) . ? C20 H20 0.9300 . ? C20 C21 1.300(6) . ? C20A H20A 0.9300 . ? C20A C21A 1.27(2) . ? C21 H21 0.9300 . ? C21A H21A 0.9300 . ? C22 H22A 0.9700 . ? C22 H22B 0.9700 . ? C22 C23 1.581(18) . ? C22A H22C 0.9700 . ? C22A H22D 0.9700 . ? C22A C23A 1.36(6) . ? C23 H23A 0.9700 . ? C23 H23B 0.9700 . ? C23 C24 1.505(10) . ? C23A H23C 0.9700 . ? C23A H23D 0.9700 . ? C23A C24A 1.51(2) . ? C24 H24A 0.9700 . ? C24 H24B 0.9700 . ? C24 C25 1.528(9) . ? C24A H24C 0.9700 . ? C24A H24D 0.9700 . ? C24A C25A 1.50(2) . ? C25 H25A 0.9700 . ? C25 H25B 0.9700 . ? C25 C26 1.508(10) . ? C25A H25C 0.9700 . ? C25A H25D 0.9700 . ? C25A C26A 1.513(19) . ? C26 H26A 0.9700 . ? C26 H26B 0.9700 . ? C26A H26C 0.9700 . ? C26A H26D 0.9700 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A N1 H1 O1 0.86 2.05 2.890(2) 165.2 2_766 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C1 C2 C3 179.7(2) . . . . ? O1 C1 C2 C9 57.8(3) . . . . ? O1 C1 C2 C19 -58.5(3) . . . . ? O2 N3 C18 C17 18.0(4) . . . . ? O2 N3 C18 C19 -164.8(3) . . . . ? O3 N3 C18 C17 -160.2(2) . . . . ? O3 N3 C18 C19 17.1(4) . . . . ? N1 C1 C2 C3 -1.0(2) . . . . ? N1 C1 C2 C9 -122.9(2) . . . . ? N1 C1 C2 C19 120.8(2) . . . . ? N1 C4 C5 C6 179.1(2) . . . . ? N2 C9 C12 C11 6.4(2) . . . . ? N2 C9 C12 C13 -178.7(2) . . . . ? N2 C10 C11 C12 0.7(3) . . . . ? N2 C10 C11 C16 -177.2(3) . . . . ? N2 C17 C18 N3 165.4(2) . . . . ? N2 C17 C18 C19 -11.6(4) . . . . ? N3 C18 C19 C2 175.6(2) . . . . ? N3 C18 C19 C20 56.7(3) . . . . ? N3 C18 C19 C20A 28.1(8) . . . . ? N4 C22 C23 C24 52.7(12) . . . . ? N4A C22A C23A C24A 58(8) . . . . ? C1 N1 C4 C3 0.6(3) . . . . ? C1 N1 C4 C5 -178.9(2) . . . . ? C1 C2 C3 C4 1.3(2) . . . . ? C1 C2 C3 C8 179.1(3) . . . . ? C1 C2 C9 N2 -176.54(16) . . . . ? C1 C2 C9 C12 65.8(2) . . . . ? C1 C2 C19 C18 159.5(2) . . . . ? C1 C2 C19 C20 -82.6(3) . . . . ? C1 C2 C19 C20A -44.0(6) . . . . ? C2 C3 C4 N1 -1.3(2) . . . . ? C2 C3 C4 C5 178.3(2) . . . . ? C2 C3 C8 C7 -177.3(3) . . . . ? C2 C9 C12 C11 127.6(2) . . . . ? C2 C9 C12 C13 -57.5(3) . . . . ? C2 C19 C20 C21 102.3(4) . . . . ? C2 C19 C20A C21A -106.4(11) . . . . ? C3 C2 C9 N2 69.4(2) . . . . ? C3 C2 C9 C12 -48.3(3) . . . . ? C3 C2 C19 C18 -87.6(2) . . . . ? C3 C2 C19 C20 30.3(3) . . . . ? C3 C2 C19 C20A 68.9(6) . . . . ? C3 C4 C5 C6 -0.3(4) . . . . ? C4 N1 C1 O1 179.6(2) . . . . ? C4 N1 C1 C2 0.3(3) . . . . ? C4 C3 C8 C7 0.3(4) . . . . ? C4 C5 C6 C7 -0.1(4) . . . . ? C5 C6 C7 C8 0.5(5) . . . . ? C6 C7 C8 C3 -0.6(5) . . . . ? C8 C3 C4 N1 -179.4(2) . . . . ? C8 C3 C4 C5 0.1(4) . . . . ? C9 N2 C10 C11 3.7(3) . . . . ? C9 N2 C17 C18 -8.8(3) . . . . ? C9 C2 C3 C4 119.9(2) . . . . ? C9 C2 C3 C8 -62.4(3) . . . . ? C9 C2 C19 C18 41.6(3) . . . . ? C9 C2 C19 C20 159.5(2) . . . . ? C9 C2 C19 C20A -161.9(5) . . . . ? C9 C12 C13 C14 -173.3(2) . . . . ? C10 N2 C9 C2 -134.8(2) . . . . ? C10 N2 C9 C12 -6.2(2) . . . . ? C10 N2 C17 C18 171.8(2) . . . . ? C10 C11 C12 C9 -4.6(3) . . . . ? C10 C11 C12 C13 180.0(2) . . . . ? C10 C11 C16 C15 178.8(3) . . . . ? C11 C12 C13 C14 1.1(4) . . . . ? C12 C11 C16 C15 1.2(4) . . . . ? C12 C13 C14 C15 0.6(4) . . . . ? C13 C14 C15 C16 -1.4(5) . . . . ? C14 C15 C16 C11 0.5(5) . . . . ? C16 C11 C12 C9 173.4(2) . . . . ? C16 C11 C12 C13 -2.0(4) . . . . ? C17 N2 C9 C2 45.7(3) . . . . ? C17 N2 C9 C12 174.38(19) . . . . ? C17 N2 C10 C11 -176.9(2) . . . . ? C17 C18 C19 C2 -7.4(4) . . . . ? C17 C18 C19 C20 -126.3(3) . . . . ? C17 C18 C19 C20A -154.9(7) . . . . ? C18 C19 C20 C21 -138.3(3) . . . . ? C18 C19 C20A C21A 41.4(14) . . . . ? C19 C2 C3 C4 -114.6(2) . . . . ? C19 C2 C3 C8 63.2(3) . . . . ? C19 C2 C9 N2 -60.3(2) . . . . ? C19 C2 C9 C12 -178.0(2) . . . . ? C19 C20 C21 N4 178.7(5) . . . . ? C19 C20A C21A N4A 178(2) . . . . ? C21 N4 C22 C23 76.5(9) . . . . ? C21 N4 C26 C25 -81.8(6) . . . . ? C21A N4A C22A C23A 103(3) . . . . ? C21A N4A C26A C25A -75(3) . . . . ? C22 N4 C21 C20 12.0(9) . . . . ? C22 N4 C26 C25 56.8(8) . . . . ? C22 C23 C24 C25 -51.5(12) . . . . ? C22A N4A C21A C20A -145(2) . . . . ? C22A N4A C26A C25A 67(3) . . . . ? C22A C23A C24A C25A -68(8) . . . . ? C23 C24 C25 C26 55.9(10) . . . . ? C23A C24A C25A C26A 53(3) . . . . ? C24 C25 C26 N4 -55.1(7) . . . . ? C24A C25A C26A N4A -67(3) . . . . ? C26 N4 C21 C20 147.5(5) . . . . ? C26 N4 C22 C23 -57.9(8) . . . . ? C26A N4A C21A C20A -4(4) . . . . ? C26A N4A C22A C23A -45(3) . . . . ?