#------------------------------------------------------------------------------ #$Date: 2021-11-10 12:01:45 +0200 (Wed, 10 Nov 2021) $ #$Revision: 270564 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/51/1565161.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1565161 loop_ _publ_author_name 'Soldevila-Sanmart\'in, Joan' 'Guerrero, Miguel' 'Choquesillo-Lazarte, Duane' 'Giner Planas, Jos\'e' 'Pons, Josefina' _publ_section_title ; Dimeric metallacycles and coordination polymers: Zn(II), Cd(II) and Hg(II) complexes of two positional isomers of a flexible N,O-hybrid bispyrazole derived ligand ; _journal_name_full 'Inorganica Chimica Acta' _journal_page_first 119549 _journal_paper_doi 10.1016/j.ica.2020.119549 _journal_volume 506 _journal_year 2020 _chemical_formula_moiety 'C44 H60 Cd2 Cl4 N8 O4' _chemical_formula_sum 'C44 H60 Cd2 Cl4 N8 O4' _chemical_formula_weight 1131.60 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _cell_angle_alpha 90 _cell_angle_beta 97.179(2) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 9.5328(8) _cell_length_b 19.3000(16) _cell_length_c 13.5436(11) _cell_measurement_reflns_used 9486 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 34.01 _cell_measurement_theta_min 2.46 _cell_volume 2472.3(4) _computing_cell_refinement 'SAINT V8.38A (Bruker, 2016)' _computing_data_reduction 'SAINT V8.38A (Bruker, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'XS (Sheldrick, 2008)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.932 _diffrn_measured_fraction_theta_max 0.932 _diffrn_measurement_device_type synchrotron _diffrn_measurement_method '\f scans' _diffrn_radiation_detector 'Dectris PILATUS 6M' _diffrn_radiation_monochromator 'Si 111' _diffrn_radiation_probe x-ray _diffrn_radiation_type synchrotron _diffrn_radiation_wavelength 0.72929 _diffrn_reflns_av_R_equivalents 0.0646 _diffrn_reflns_av_unetI/netI 0.0565 _diffrn_reflns_Laue_measured_fraction_full 0.932 _diffrn_reflns_Laue_measured_fraction_max 0.932 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 19112 _diffrn_reflns_point_group_measured_fraction_full 0.932 _diffrn_reflns_point_group_measured_fraction_max 0.932 _diffrn_reflns_theta_full 25.812 _diffrn_reflns_theta_max 25.812 _diffrn_reflns_theta_min 2.461 _exptl_absorpt_coefficient_mu 1.196 _exptl_absorpt_correction_T_max 0.0922 _exptl_absorpt_correction_T_min 0.0385 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1636 before and 0.1036 after correction. The Ratio of minimum to maximum transmission is 0.4176. The \l/2 correction factor is 0.00400. ; _exptl_crystal_density_diffrn 1.520 _exptl_crystal_description block _exptl_crystal_F_000 1152 _refine_diff_density_max 1.108 _refine_diff_density_min -0.889 _refine_diff_density_rms 0.163 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.074 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 284 _refine_ls_number_reflns 4111 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.074 _refine_ls_R_factor_all 0.0688 _refine_ls_R_factor_gt 0.0672 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1387P)^2^+2.1593P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1866 _refine_ls_wR_factor_ref 0.1906 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 3963 _reflns_number_total 4111 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL js173_a.res in P2(1)/n js173.res created by SHELXL-2018/3 at 20:58:17 on 14-Sep-2019 CELL 0.72929 9.5328 19.3 13.5436 90 97.179 90 ZERR 2 0.0008 0.0016 0.0011 0 0.002 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Cd Cl N O DISP C 0.0037 0.0017 12.0603 DISP Cd -0.7547 1.2858 5507.1654 DISP Cl 0.1547 0.1686 724.1588 DISP H -0 0 0.625 DISP N 0.007 0.0034 20.6952 DISP O 0.0123 0.0065 34.4758 UNIT 88 120 4 8 16 8 L.S. 10 PLAN 20 TEMP -173(2) BOND $H LIST 4 fmap 2 acta OMIT 0 5 4 OMIT -4 0 6 OMIT -4 5 0 OMIT 1 7 3 OMIT -3 2 5 OMIT -4 2 4 OMIT -4 4 1 OMIT 3 6 3 OMIT 2 4 3 OMIT 0 4 1 OMIT 0 1 4 OMIT -2 1 -1 OMIT 0 1 6 OMIT 1 3 3 OMIT -3 0 3 OMIT -2 4 3 OMIT 1 1 4 OMIT 0 1 3 OMIT -2 4 0 OMIT -1 4 6 OMIT 2 1 5 OMIT -2 2 7 OMIT 3 4 3 OMIT -1 2 7 OMIT 0 0 6 OMIT -3 2 -2 OMIT -3 5 -2 OMIT 2 3 5 OMIT 3 0 3 OMIT -1 0 7 OMIT -4 2 -2 OMIT 2 6 4 OMIT 3 8 3 OMIT 3 3 4 OMIT -1 6 7 OMIT -4 10 1 OMIT -5 3 0 OMIT 2 4 7 OMIT -4 1 -1 OMIT -6 4 9 OMIT 0 7 6 OMIT -2 5 1 OMIT 1 4 6 OMIT 2 5 4 OMIT 0 8 4 OMIT 3 5 4 OMIT 2 0 6 OMIT 0 1 8 OMIT -2 7 1 OMIT -3 1 5 OMIT -3 1 5 OMIT -1 3 1 OMIT -1 8 3 OMIT -3 4 -1 OMIT -1 7 2 OMIT -2 3 3 OMIT 2 6 2 OMIT -2 4 4 OMIT -4 1 3 OMIT -2 8 -1 OMIT 2 3 4 OMIT 2 3 4 REM REM REM WGHT 0.138700 2.159300 FVAR 0.62337 CD1 3 0.782461 0.678520 0.383738 11.00000 0.05628 0.03706 = 0.03967 -0.00173 0.01070 -0.00357 CL1 4 0.702523 0.785152 0.299737 11.00000 0.07356 0.03701 = 0.05912 0.00392 0.00631 -0.00166 CL2 4 1.035235 0.665385 0.428591 11.00000 0.05324 0.05778 = 0.06407 -0.00412 0.02294 -0.00217 O1 6 0.616196 0.626761 0.018600 11.00000 0.07179 0.06271 = 0.04376 -0.00167 0.00832 -0.00810 O2 6 0.165805 0.442551 0.289406 11.00000 0.08087 0.05459 = 0.06067 0.00995 0.02478 -0.00263 N1 5 0.735841 0.584225 0.286438 11.00000 0.07201 0.03930 = 0.04393 -0.00187 -0.00082 -0.00205 N2 5 0.791462 0.580017 0.198397 11.00000 0.05801 0.05776 = 0.04913 -0.01291 0.00245 0.00573 N3 5 0.338415 0.327134 0.485438 11.00000 0.05094 0.04423 = 0.04874 -0.00023 0.01326 -0.00220 N4 5 0.288342 0.322292 0.387542 11.00000 0.06279 0.03409 = 0.04846 -0.00200 0.02086 -0.00445 C1 1 0.712007 0.518581 0.313114 11.00000 0.09270 0.04007 = 0.05654 0.00056 -0.02000 -0.00344 C2 1 0.652735 0.502417 0.406087 11.00000 0.16726 0.05247 = 0.05899 0.01156 -0.01270 -0.03675 AFIX 137 H2A 2 0.654750 0.544096 0.447571 11.00000 -1.50000 H2B 2 0.709217 0.465912 0.442260 11.00000 -1.50000 H2C 2 0.554895 0.486515 0.390140 11.00000 -1.50000 AFIX 0 C3 1 0.750857 0.473586 0.242247 11.00000 0.08375 0.04039 = 0.08535 -0.01549 -0.02559 0.01018 AFIX 43 H3 2 0.744640 0.424467 0.243106 11.00000 -1.20000 AFIX 0 C4 1 0.800412 0.513705 0.169997 11.00000 0.06082 0.06709 = 0.08141 -0.03612 -0.01152 0.00906 C5 1 0.861578 0.493553 0.078049 11.00000 0.07617 0.11687 = 0.10615 -0.06545 0.01688 -0.00432 AFIX 137 H5A 2 0.793451 0.503866 0.019555 11.00000 -1.50000 H5B 2 0.882648 0.443837 0.079979 11.00000 -1.50000 H5C 2 0.948834 0.519712 0.074183 11.00000 -1.50000 AFIX 0 C6 1 0.812531 0.642729 0.142755 11.00000 0.06502 0.07256 = 0.05156 -0.01161 0.01449 -0.01377 AFIX 23 H6A 2 0.873308 0.632067 0.090560 11.00000 -1.20000 H6B 2 0.862265 0.677473 0.188187 11.00000 -1.20000 AFIX 0 C7 1 0.674738 0.673081 0.094725 11.00000 0.07648 0.05088 = 0.04791 0.00299 0.00722 -0.01444 AFIX 23 H7A 2 0.608572 0.678989 0.144916 11.00000 -1.20000 H7B 2 0.691444 0.719016 0.065825 11.00000 -1.20000 AFIX 0 C8 1 0.468151 0.636060 -0.003696 11.00000 0.06807 0.05445 = 0.04795 0.00509 0.00245 -0.00605 AFIX 23 H8A 2 0.435194 0.612874 -0.067602 11.00000 -1.20000 H8B 2 0.447327 0.686136 -0.011824 11.00000 -1.20000 AFIX 0 C9 1 0.388001 0.607186 0.076440 11.00000 0.06229 0.04038 = 0.04505 0.00332 0.00069 -0.00237 C10 1 0.428129 0.543705 0.118760 11.00000 0.05956 0.04440 = 0.05395 0.00749 0.01104 0.00241 AFIX 43 H10 2 0.506609 0.519831 0.098113 11.00000 -1.20000 AFIX 0 C11 1 0.354837 0.514492 0.191163 11.00000 0.05809 0.04316 = 0.05694 0.01079 0.00528 0.00337 AFIX 43 H11 2 0.384485 0.471234 0.220070 11.00000 -1.20000 AFIX 0 C12 1 0.239653 0.547867 0.221173 11.00000 0.05736 0.04852 = 0.04395 -0.00128 0.00245 -0.00249 C13 1 0.200175 0.611543 0.179709 11.00000 0.05966 0.04471 = 0.06284 -0.00192 0.01029 0.00259 AFIX 43 H13 2 0.122082 0.635393 0.200962 11.00000 -1.20000 AFIX 0 C14 1 0.271804 0.640853 0.108445 11.00000 0.06915 0.03919 = 0.06308 0.00295 0.00106 0.00101 AFIX 43 H14 2 0.242213 0.684420 0.080574 11.00000 -1.20000 AFIX 0 C15 1 0.159566 0.515240 0.297549 11.00000 0.06192 0.05738 = 0.05789 0.00416 0.00897 0.00028 AFIX 23 H15A 2 0.201154 0.529766 0.365014 11.00000 -1.20000 H15B 2 0.059792 0.530705 0.287142 11.00000 -1.20000 AFIX 0 C16 1 0.094861 0.405570 0.358753 11.00000 0.05973 0.07212 = 0.05011 0.01650 0.00994 -0.00129 AFIX 23 H16A 2 -0.008769 0.409561 0.341062 11.00000 -1.20000 H16B 2 0.120309 0.424642 0.426480 11.00000 -1.20000 AFIX 0 C17 1 0.139316 0.331216 0.355625 11.00000 0.07416 0.06045 = 0.03590 0.00389 0.00527 -0.01468 AFIX 23 H17A 2 0.084724 0.303534 0.399132 11.00000 -1.20000 H17B 2 0.117015 0.313537 0.286836 11.00000 -1.20000 AFIX 0 C18 1 0.397496 0.316637 0.332845 11.00000 0.09037 0.03652 = 0.05469 -0.00240 0.03514 -0.00193 C19 1 0.375695 0.309897 0.223069 11.00000 0.11405 0.06629 = 0.06244 -0.01040 0.04077 -0.00482 AFIX 137 H19A 2 0.341477 0.263163 0.204909 11.00000 -1.50000 H19B 2 0.465404 0.317992 0.196637 11.00000 -1.50000 H19C 2 0.305780 0.344077 0.195021 11.00000 -1.50000 AFIX 0 C20 1 0.518218 0.316564 0.396858 11.00000 0.06690 0.04673 = 0.08517 0.00507 0.03834 0.00366 AFIX 43 H20 2 0.611650 0.312769 0.379904 11.00000 -1.20000 AFIX 0 C21 1 0.479951 0.323089 0.492258 11.00000 0.05691 0.04536 = 0.08059 0.00791 0.02401 0.00055 C22 1 0.568125 0.325564 0.589117 11.00000 0.05646 0.08986 = 0.09129 0.01324 0.00168 -0.01123 AFIX 137 H22A 2 0.547886 0.368187 0.624035 11.00000 -1.50000 H22B 2 0.668136 0.324813 0.579026 11.00000 -1.50000 H22C 2 0.547228 0.285343 0.628966 11.00000 -1.50000 AFIX 0 HKLF 4 REM js173_a.res in P2(1)/n REM wR2 = 0.190565, GooF = S = 1.07353, Restrained GooF = 1.07353 for all data REM R1 = 0.067166 for 3963 Fo > 4sig(Fo) and 0.068827 for all 4111 data REM 284 parameters refined using 0 restraints END WGHT 0.1387 2.1593 REM Highest difference peak 1.108, deepest hole -0.889, 1-sigma level 0.163 Q1 1 0.6968 0.6794 0.3776 11.00000 0.05 1.11 Q2 1 0.7782 0.6578 0.4150 11.00000 0.05 0.84 Q3 1 1.0602 0.3644 0.0906 11.00000 0.05 0.64 Q4 1 0.4386 0.2753 0.1967 11.00000 0.05 0.64 Q5 1 0.9793 0.6421 0.3860 11.00000 0.05 0.61 Q6 1 0.2922 0.3688 0.4919 11.00000 0.05 0.60 Q7 1 1.0200 0.6894 0.3825 11.00000 0.05 0.57 Q8 1 0.6130 0.7849 0.3242 11.00000 0.05 0.56 Q9 1 0.1612 0.2664 0.3334 11.00000 0.05 0.56 Q10 1 0.7871 0.7750 0.3220 11.00000 0.05 0.52 Q11 1 0.6988 0.4709 0.3328 11.00000 0.05 0.51 Q12 1 1.0208 0.7071 0.4853 11.00000 0.05 0.50 Q13 1 0.8242 0.7313 0.2663 11.00000 0.05 0.50 Q14 1 0.9240 0.4555 0.0760 11.00000 0.05 0.49 Q15 1 0.8437 0.5493 -0.0124 11.00000 0.05 0.48 Q16 1 0.2715 0.2903 0.4868 11.00000 0.05 0.48 Q17 1 0.1850 0.2809 0.1341 11.00000 0.05 0.48 Q18 1 0.3226 0.5509 0.2200 11.00000 0.05 0.47 Q19 1 0.4430 0.4588 0.2724 11.00000 0.05 0.47 Q20 1 0.8080 0.7494 0.2782 11.00000 0.05 0.46 REM The information below was added by Olex2. REM REM R1 = 0.067166 for 3963 Fo > 4sig(Fo) and 0.068827 for all 19675 data REM n/a parameters refined using n/a restraints REM Highest difference peak 1.11, deepest hole -0.89 REM Mean Shift 0, Max Shift 0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.068827 REM R1_gt = 0.067166 REM wR_ref = 0.190565 REM GOOF = 1.07353 REM Shift_max = 0.001 REM Shift_mean = 0 REM Reflections_all = 19675 REM Reflections_gt = 3963 REM Parameters = n/a REM Hole = -0.89 REM Peak = 1.11 REM Flack = n/a ; _cod_data_source_file ICA-2020-506-1195463.cif _cod_data_source_block js173 _cod_depositor_comments ; The following automatic conversions were performed: data item '_exptl_absorpt_correction_type' value 'MULTI-SCAN' was changed to 'multi-scan' in accordance with the built-in table derived from the CIF Core dictionary named 'cif_core.dic' version 2.4.5 last updated on 2014-11-21. Automatic conversion script Id: cif_fix_values 8738 2021-04-28 16:35:53Z antanas ; _cod_original_sg_symbol_H-M P2(1)/n _cod_database_code 1565161 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Secondary CH2 refined with riding coordinates: C6(H6A,H6B), C7(H7A,H7B), C8(H8A,H8B), C15(H15A,H15B), C16(H16A,H16B), C17(H17A,H17B) 2.b Aromatic/amide H refined with riding coordinates: C3(H3), C10(H10), C11(H11), C13(H13), C14(H14), C20(H20) 2.c Idealised Me refined as rotating group: C2(H2A,H2B,H2C), C5(H5A,H5B,H5C), C19(H19A,H19B,H19C), C22(H22A,H22B,H22C) ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cd1 Cd 0.78246(3) 0.67852(2) 0.38374(2) 0.0439(2) Uani 1 1 d . . . . . Cl1 Cl 0.70252(14) 0.78515(6) 0.29974(9) 0.0567(4) Uani 1 1 d . . . . . Cl2 Cl 1.03523(13) 0.66538(7) 0.42859(10) 0.0570(4) Uani 1 1 d . . . . . O1 O 0.6162(4) 0.62676(19) 0.0186(2) 0.0593(8) Uani 1 1 d . . . . . O2 O 0.1658(4) 0.44255(19) 0.2894(3) 0.0640(9) Uani 1 1 d . . . . . N1 N 0.7358(5) 0.5842(2) 0.2864(3) 0.0524(9) Uani 1 1 d . . . . . N2 N 0.7915(4) 0.5800(2) 0.1984(3) 0.0553(10) Uani 1 1 d . . . . . N3 N 0.3384(4) 0.32713(18) 0.4854(3) 0.0474(9) Uani 1 1 d . . . . . N4 N 0.2883(4) 0.32229(17) 0.3875(3) 0.0473(11) Uani 1 1 d . . . . . C1 C 0.7120(7) 0.5186(3) 0.3131(4) 0.0656(14) Uani 1 1 d . . . . . C2 C 0.6527(10) 0.5024(3) 0.4061(5) 0.095(3) Uani 1 1 d . . . . . H2A H 0.654750 0.544096 0.447571 0.143 Uiso 1 1 calc GR . . . . H2B H 0.709217 0.465912 0.442260 0.143 Uiso 1 1 calc GR . . . . H2C H 0.554895 0.486515 0.390140 0.143 Uiso 1 1 calc GR . . . . C3 C 0.7509(7) 0.4736(3) 0.2422(5) 0.0729(17) Uani 1 1 d . . . . . H3 H 0.744640 0.424467 0.243106 0.087 Uiso 1 1 calc R . . . . C4 C 0.8004(6) 0.5137(3) 0.1700(5) 0.0715(16) Uani 1 1 d . . . . . C5 C 0.8616(8) 0.4936(5) 0.0780(6) 0.099(3) Uani 1 1 d . . . . . H5A H 0.793451 0.503866 0.019555 0.149 Uiso 1 1 calc GR . . . . H5B H 0.882648 0.443837 0.079979 0.149 Uiso 1 1 calc GR . . . . H5C H 0.948834 0.519712 0.074183 0.149 Uiso 1 1 calc GR . . . . C6 C 0.8125(6) 0.6427(3) 0.1428(4) 0.0624(13) Uani 1 1 d . . . . . H6A H 0.873308 0.632067 0.090560 0.075 Uiso 1 1 calc R . . . . H6B H 0.862265 0.677473 0.188187 0.075 Uiso 1 1 calc R . . . . C7 C 0.6747(7) 0.6731(3) 0.0947(5) 0.0585(13) Uani 1 1 d . . . . . H7A H 0.608572 0.678989 0.144916 0.070 Uiso 1 1 calc R . . . . H7B H 0.691444 0.719016 0.065825 0.070 Uiso 1 1 calc R . . . . C8 C 0.4682(5) 0.6361(3) -0.0037(4) 0.0572(11) Uani 1 1 d . . . . . H8A H 0.435194 0.612874 -0.067602 0.069 Uiso 1 1 calc R . . . . H8B H 0.447327 0.686136 -0.011824 0.069 Uiso 1 1 calc R . . . . C9 C 0.3880(5) 0.6072(2) 0.0764(3) 0.0497(10) Uani 1 1 d . . . . . C10 C 0.4281(5) 0.5437(2) 0.1188(4) 0.0523(10) Uani 1 1 d . . . . . H10 H 0.506609 0.519831 0.098113 0.063 Uiso 1 1 calc R . . . . C11 C 0.3548(5) 0.5145(2) 0.1912(4) 0.0529(10) Uani 1 1 d . . . . . H11 H 0.384485 0.471234 0.220070 0.063 Uiso 1 1 calc R . . . . C12 C 0.2397(5) 0.5479(2) 0.2212(3) 0.0503(10) Uani 1 1 d . . . . . C13 C 0.2002(5) 0.6115(2) 0.1797(4) 0.0555(11) Uani 1 1 d . . . . . H13 H 0.122082 0.635393 0.200962 0.067 Uiso 1 1 calc R . . . . C14 C 0.2718(6) 0.6409(3) 0.1084(4) 0.0577(11) Uani 1 1 d . . . . . H14 H 0.242213 0.684420 0.080574 0.069 Uiso 1 1 calc R . . . . C15 C 0.1596(6) 0.5152(3) 0.2975(4) 0.0589(12) Uani 1 1 d . . . . . H15A H 0.201154 0.529766 0.365014 0.071 Uiso 1 1 calc R . . . . H15B H 0.059792 0.530705 0.287142 0.071 Uiso 1 1 calc R . . . . C16 C 0.0949(5) 0.4056(3) 0.3588(4) 0.0604(12) Uani 1 1 d . . . . . H16A H -0.008769 0.409561 0.341062 0.072 Uiso 1 1 calc R . . . . H16B H 0.120309 0.424642 0.426480 0.072 Uiso 1 1 calc R . . . . C17 C 0.1393(7) 0.3312(3) 0.3556(4) 0.0570(13) Uani 1 1 d . . . . . H17A H 0.084724 0.303534 0.399132 0.068 Uiso 1 1 calc R . . . . H17B H 0.117015 0.313537 0.286836 0.068 Uiso 1 1 calc R . . . . C18 C 0.3975(7) 0.3166(2) 0.3328(4) 0.0583(14) Uani 1 1 d . . . . . C19 C 0.3757(9) 0.3099(4) 0.2231(5) 0.0784(18) Uani 1 1 d . . . . . H19A H 0.341477 0.263163 0.204909 0.118 Uiso 1 1 calc GR . . . . H19B H 0.465404 0.317992 0.196637 0.118 Uiso 1 1 calc GR . . . . H19C H 0.305780 0.344077 0.195021 0.118 Uiso 1 1 calc GR . . . . C20 C 0.5182(7) 0.3166(2) 0.3969(5) 0.0638(15) Uani 1 1 d . . . . . H20 H 0.611650 0.312769 0.379904 0.077 Uiso 1 1 calc R . . . . C21 C 0.4800(6) 0.3231(2) 0.4923(5) 0.0596(14) Uani 1 1 d . . . . . C22 C 0.5681(7) 0.3256(4) 0.5891(6) 0.080(2) Uani 1 1 d . . . . . H22A H 0.547886 0.368187 0.624035 0.120 Uiso 1 1 calc GR . . . . H22B H 0.668136 0.324813 0.579026 0.120 Uiso 1 1 calc GR . . . . H22C H 0.547228 0.285343 0.628966 0.120 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cd1 0.0563(3) 0.0371(3) 0.0397(3) -0.00173(9) 0.01070(18) -0.00357(10) Cl1 0.0736(8) 0.0370(6) 0.0591(7) 0.0039(4) 0.0063(5) -0.0017(5) Cl2 0.0532(7) 0.0578(6) 0.0641(8) -0.0041(5) 0.0229(5) -0.0022(5) O1 0.072(2) 0.063(2) 0.0438(17) -0.0017(15) 0.0083(15) -0.0081(16) O2 0.081(2) 0.055(2) 0.061(2) 0.0100(16) 0.0248(17) -0.0026(17) N1 0.072(2) 0.0393(19) 0.044(2) -0.0019(15) -0.0008(17) -0.0020(17) N2 0.058(2) 0.058(2) 0.049(2) -0.0129(18) 0.0024(17) 0.0057(18) N3 0.051(2) 0.044(2) 0.049(2) -0.0002(14) 0.0133(17) -0.0022(14) N4 0.063(3) 0.034(2) 0.048(3) -0.0020(12) 0.021(2) -0.0044(13) C1 0.093(4) 0.040(2) 0.057(3) 0.001(2) -0.020(3) -0.003(2) C2 0.167(8) 0.052(3) 0.059(3) 0.012(3) -0.013(4) -0.037(4) C3 0.084(4) 0.040(2) 0.085(4) -0.015(3) -0.026(3) 0.010(2) C4 0.061(3) 0.067(3) 0.081(4) -0.036(3) -0.012(3) 0.009(2) C5 0.076(4) 0.117(6) 0.106(5) -0.065(5) 0.017(4) -0.004(4) C6 0.065(3) 0.073(4) 0.052(3) -0.012(2) 0.014(2) -0.014(2) C7 0.076(3) 0.051(3) 0.048(3) 0.0030(19) 0.007(3) -0.014(2) C8 0.068(3) 0.054(3) 0.048(2) 0.005(2) 0.002(2) -0.006(2) C9 0.062(3) 0.040(2) 0.045(2) 0.0033(17) 0.0007(18) -0.0024(18) C10 0.060(2) 0.044(2) 0.054(2) 0.0075(19) 0.011(2) 0.0024(19) C11 0.058(2) 0.043(2) 0.057(3) 0.0108(19) 0.005(2) 0.0034(19) C12 0.057(2) 0.049(2) 0.044(2) -0.0013(18) 0.0024(18) -0.0025(19) C13 0.060(3) 0.045(2) 0.063(3) -0.002(2) 0.010(2) 0.0026(19) C14 0.069(3) 0.039(2) 0.063(3) 0.003(2) 0.001(2) 0.001(2) C15 0.062(3) 0.057(3) 0.058(3) 0.004(2) 0.009(2) 0.000(2) C16 0.060(3) 0.072(3) 0.050(2) 0.017(2) 0.010(2) -0.001(2) C17 0.074(3) 0.060(3) 0.036(2) 0.0039(19) 0.005(2) -0.015(2) C18 0.090(4) 0.037(2) 0.055(3) -0.0024(18) 0.035(3) -0.002(2) C19 0.114(5) 0.066(3) 0.062(4) -0.010(3) 0.041(4) -0.005(3) C20 0.067(3) 0.047(3) 0.085(4) 0.005(2) 0.038(3) 0.004(2) C21 0.057(3) 0.045(3) 0.081(4) 0.008(2) 0.024(3) 0.0006(18) C22 0.056(3) 0.090(5) 0.091(5) 0.013(3) 0.002(3) -0.011(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0037 0.0017 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cd Cd -0.7547 1.2858 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1547 0.1686 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0070 0.0034 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0123 0.0065 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 Cl2 Cd1 Cl1 116.75(4) . . N1 Cd1 Cl1 112.48(11) . . N1 Cd1 Cl2 100.31(11) . . N3 Cd1 Cl1 104.50(10) 3_666 . N3 Cd1 Cl2 113.04(12) 3_666 . N3 Cd1 N1 109.88(15) 3_666 . C8 O1 C7 111.4(4) . . C15 O2 C16 114.9(4) . . N2 N1 Cd1 119.2(3) . . C1 N1 Cd1 129.1(3) . . C1 N1 N2 106.0(4) . . N1 N2 C6 119.8(4) . . C4 N2 N1 110.6(5) . . C4 N2 C6 128.9(5) . . N4 N3 Cd1 128.3(3) . 3_666 C21 N3 Cd1 123.8(4) . 3_666 C21 N3 N4 106.9(4) . . N3 N4 C17 119.9(4) . . C18 N4 N3 109.9(5) . . C18 N4 C17 129.8(5) . . N1 C1 C2 121.6(5) . . N1 C1 C3 109.7(6) . . C3 C1 C2 128.7(5) . . C1 C2 H2A 109.5 . . C1 C2 H2B 109.5 . . C1 C2 H2C 109.5 . . H2A C2 H2B 109.5 . . H2A C2 H2C 109.5 . . H2B C2 H2C 109.5 . . C1 C3 H3 126.7 . . C4 C3 C1 106.6(5) . . C4 C3 H3 126.7 . . N2 C4 C3 107.0(5) . . N2 C4 C5 122.2(7) . . C3 C4 C5 130.7(6) . . C4 C5 H5A 109.5 . . C4 C5 H5B 109.5 . . C4 C5 H5C 109.5 . . H5A C5 H5B 109.5 . . H5A C5 H5C 109.5 . . H5B C5 H5C 109.5 . . N2 C6 H6A 109.2 . . N2 C6 H6B 109.2 . . N2 C6 C7 112.2(4) . . H6A C6 H6B 107.9 . . C7 C6 H6A 109.2 . . C7 C6 H6B 109.2 . . O1 C7 C6 108.0(5) . . O1 C7 H7A 110.1 . . O1 C7 H7B 110.1 . . C6 C7 H7A 110.1 . . C6 C7 H7B 110.1 . . H7A C7 H7B 108.4 . . O1 C8 H8A 109.1 . . O1 C8 H8B 109.1 . . O1 C8 C9 112.3(4) . . H8A C8 H8B 107.9 . . C9 C8 H8A 109.1 . . C9 C8 H8B 109.1 . . C10 C9 C8 119.0(4) . . C10 C9 C14 118.1(4) . . C14 C9 C8 122.9(4) . . C9 C10 H10 119.6 . . C9 C10 C11 120.8(5) . . C11 C10 H10 119.6 . . C10 C11 H11 119.8 . . C12 C11 C10 120.5(4) . . C12 C11 H11 119.8 . . C11 C12 C13 118.8(4) . . C11 C12 C15 120.0(4) . . C13 C12 C15 121.1(5) . . C12 C13 H13 119.4 . . C14 C13 C12 121.2(5) . . C14 C13 H13 119.4 . . C9 C14 H14 119.7 . . C13 C14 C9 120.6(4) . . C13 C14 H14 119.7 . . O2 C15 C12 109.5(4) . . O2 C15 H15A 109.8 . . O2 C15 H15B 109.8 . . C12 C15 H15A 109.8 . . C12 C15 H15B 109.8 . . H15A C15 H15B 108.2 . . O2 C16 H16A 110.2 . . O2 C16 H16B 110.2 . . O2 C16 C17 107.7(4) . . H16A C16 H16B 108.5 . . C17 C16 H16A 110.2 . . C17 C16 H16B 110.2 . . N4 C17 C16 112.2(4) . . N4 C17 H17A 109.2 . . N4 C17 H17B 109.2 . . C16 C17 H17A 109.2 . . C16 C17 H17B 109.2 . . H17A C17 H17B 107.9 . . N4 C18 C19 122.3(6) . . C20 C18 N4 107.5(5) . . C20 C18 C19 130.2(6) . . C18 C19 H19A 109.5 . . C18 C19 H19B 109.5 . . C18 C19 H19C 109.5 . . H19A C19 H19B 109.5 . . H19A C19 H19C 109.5 . . H19B C19 H19C 109.5 . . C18 C20 H20 126.4 . . C18 C20 C21 107.1(5) . . C21 C20 H20 126.4 . . N3 C21 C20 108.6(6) . . N3 C21 C22 121.2(6) . . C20 C21 C22 130.2(6) . . C21 C22 H22A 109.5 . . C21 C22 H22B 109.5 . . C21 C22 H22C 109.5 . . H22A C22 H22B 109.5 . . H22A C22 H22C 109.5 . . H22B C22 H22C 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Cd1 Cl1 2.4277(12) . Cd1 Cl2 2.4236(13) . Cd1 N1 2.258(4) . Cd1 N3 2.234(4) 3_666 O1 C7 1.425(7) . O1 C8 1.417(7) . O2 C15 1.409(7) . O2 C16 1.417(6) . N1 N2 1.367(6) . N1 C1 1.345(7) . N2 C4 1.342(7) . N2 C6 1.453(8) . N3 N4 1.355(6) . N3 C21 1.343(7) . N4 C17 1.443(8) . N4 C18 1.355(7) . C1 C2 1.476(10) . C1 C3 1.379(9) . C2 H2A 0.9800 . C2 H2B 0.9800 . C2 H2C 0.9800 . C3 H3 0.9500 . C3 C4 1.377(10) . C4 C5 1.491(9) . C5 H5A 0.9800 . C5 H5B 0.9800 . C5 H5C 0.9800 . C6 H6A 0.9900 . C6 H6B 0.9900 . C6 C7 1.509(9) . C7 H7A 0.9900 . C7 H7B 0.9900 . C8 H8A 0.9900 . C8 H8B 0.9900 . C8 C9 1.510(7) . C9 C10 1.386(6) . C9 C14 1.399(7) . C10 H10 0.9500 . C10 C11 1.392(7) . C11 H11 0.9500 . C11 C12 1.377(7) . C12 C13 1.384(7) . C12 C15 1.499(7) . C13 H13 0.9500 . C13 C14 1.372(8) . C14 H14 0.9500 . C15 H15A 0.9900 . C15 H15B 0.9900 . C16 H16A 0.9900 . C16 H16B 0.9900 . C16 C17 1.498(8) . C17 H17A 0.9900 . C17 H17B 0.9900 . C18 C19 1.481(9) . C18 C20 1.352(10) . C19 H19A 0.9800 . C19 H19B 0.9800 . C19 H19C 0.9800 . C20 H20 0.9500 . C20 C21 1.391(9) . C21 C22 1.468(11) . C22 H22A 0.9800 . C22 H22B 0.9800 . C22 H22C 0.9800 . loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_scale_group_code 1 0 0 0.36916 0.3275 2 -1 0 0 0.41234 0.249 2 3 0 0 0.35013 1.04016 2 5 0 0 0.57418 1.74078 2 -5 0 0 0.14363 0.30291 1 -6 0 0 22.1057 2.07521 1 6 0 0 22.9388 3.84122 2 7 0 0 -0.457 2.66285 2 -7 0 0 -0.0695 0.35487 1 8 0 0 76.2038 10.6058 2 8 0 0 86.5222 8.73395 2 9 0 0 -0.628 1.94758 2 -9 0 0 -0.2994 0.45391 1 -9 0 0 -0.198 0.54815 1 9 0 0 -2.7044 4.76653 2 10 0 0 72.352 9.54439 2 -10 0 0 94.6499 7.79278 1 -10 0 0 99.8814 8.02441 1 10 0 0 77.9112 13.7326 2 -11 0 0 -0.4298 0.50527 1 11 0 0 -1.1115 2.83631 2 -11 0 0 -0.4298 0.77768 1 11 0 0 -0.8589 7.49388 2 0 -1 0 0.82791 0.10092 1 0 1 0 1.24129 0.10633 1 -1 -1 0 34.8732 2.8247 1 -1 1 0 37.4904 3.15607 2 -1 1 0 30.6376 2.81216 1 1 1 0 28.7669 2.81958 1 -2 -1 0 21.2518 2.11284 1 2 1 0 27.2811 2.46819 2 4 1 0 909.409 77.9846 2 -6 -1 0 413.004 34.49 1 -6 1 0 396.883 34.5171 1 -7 -1 0 314.431 30.526 1 -7 1 0 324.302 30.5726 1 7 1 0 400.091 32.8162 2 7 1 0 390.433 32.0279 2 -7 1 0 369.924 30.5482 1 8 -1 0 980.233 83.0561 2 -8 -1 0 974.785 81.617 1 -8 1 0 940.467 81.6659 1 -8 1 0 931.22 81.5838 1 8 1 0 977.727 82.9912 2 9 -1 0 49.9113 5.76489 2 9 -1 0 50.2835 10.0731 2 -9 -1 0 42.0243 4.0672 1 -9 1 0 45.3996 4.23567 1 9 1 0 41.1282 5.54573 2 9 1 0 53.7769 8.50645 2 -9 1 0 43.9441 4.06395 1 -10 -1 0 87.5463 7.38942 1 -10 -1 0 83.7745 7.55993 1 -10 1 0 80.0094 7.5519 1 11 -1 0 14.4585 9.57124 2 -11 -1 0 24.2282 2.4324 1 -11 -1 0 27.8187 2.73346 1 -11 1 0 23.7483 2.63189 1 -11 1 0 24.2296 2.37206 1 11 1 0 12.658 8.76348 2 -2 -2 0 15.8357 1.51171 1 -2 2 0 17.1732 1.51752 1 5 -2 0 377.226 31.7985 2 -5 -2 0 325.976 29.7207 1 -5 2 0 329.478 29.7318 1 5 2 0 367.902 30.8865 2 6 -2 0 7.57522 3.69904 2 -6 -2 0 7.53982 0.79712 1 -6 2 0 6.27746 0.73706 1 6 2 0 5.49103 2.19486 2 6 2 0 4.4875 2.17501 2 -7 -2 0 238.334 19.9329 1 7 -2 0 227.13 23.4295 2 -7 2 0 263.266 20.0252 1 7 2 0 216.157 21.8254 2 7 2 0 204.953 21.0372 2 -7 2 0 241.617 19.9135 1 8 -2 0 66.2507 10.4863 2 8 -2 0 65.3463 6.89172 2 -8 -2 0 55.1227 5.25043 1 -8 2 0 55.1848 5.21458 1 -8 2 0 54.1983 5.3376 1 8 2 0 66.5457 8.20462 2 8 2 0 64.1421 6.82727 2 -9 -2 0 122.473 11.161 1 9 -2 0 142.27 12.7188 2 9 -2 0 125.549 17.1599 2 -9 2 0 128.036 11.1654 1 9 2 0 133.022 12.9849 2 -9 2 0 123.02 11.3001 1 -10 -2 0 106.073 8.60691 1 10 -2 0 79.1455 14.8793 2 -10 2 0 102.499 8.77529 1 -10 2 0 103.64 8.55831 1 10 2 0 82.0839 10.6195 2 11 -2 0 17.4113 4.0598 2 11 -2 0 20.5396 10.3213 2 -11 -2 0 25.0085 2.34835 1 -11 -2 0 27.2287 2.55975 1 -11 2 0 21.194 2.20826 1 11 2 0 21.0672 4.79926 2 -11 2 0 23.7144 2.50586 1 11 2 0 14.8178 8.34875 2 0 3 0 1.38705 0.80796 2 -1 3 0 629.049 53.6758 2 -4 3 0 40.6647 4.06176 2 5 -3 0 5725.44 487.439 2 6 -3 0 3.10031 3.69225 2 -6 3 0 1.56955 0.50535 1 6 3 0 3.65604 1.94421 2 6 3 0 1.37633 1.81026 2 -6 3 0 2.32265 0.47564 1 -7 -3 0 1620.98 152.308 1 -7 3 0 1943.85 152.408 1 7 3 0 1831.38 154.105 2 7 3 0 1786.49 153.591 2 8 -3 0 3.43179 6.62353 2 -8 -3 0 4.95756 0.76926 1 8 3 0 3.09916 2.47581 2 -8 3 0 4.74023 0.74407 1 8 3 0 3.26551 3.14357 2 -8 3 0 5.84104 0.9371 1 -9 -3 0 363.842 28.9223 1 9 -3 0 309.174 30.0615 2 9 -3 0 327.408 35.3213 2 9 3 0 339.281 31.9544 2 9 3 0 311.781 30.6964 2 -9 3 0 353.08 29.0442 1 -9 3 0 356.057 28.8966 1 -10 -3 0 32.6825 2.7788 1 10 -3 0 15.4498 8.94832 2 -10 3 0 28.4822 2.90543 1 10 3 0 23.6554 6.2841 2 -10 3 0 27.7463 2.65862 1 -11 -3 0 208.668 16.291 1 11 3 0 171.181 21.598 2 -11 3 0 172.802 16.2174 1 -2 4 0 2343.03 199.446 2 4 4 0 302.469 24.5631 2 -4 4 0 267.944 23.9971 2 4 4 0 266.441 24.2123 2 -4 4 0 271.134 23.5818 1 5 -4 0 18.1969 4.51124 2 5 4 0 12.368 2.47231 2 -5 4 0 13.1447 1.26684 1 -5 4 0 11.8269 1.73994 2 5 4 0 8.84707 1.95913 2 -6 -4 0 87.1079 7.38347 1 6 -4 0 88.8937 10.7652 2 -6 4 0 90.7541 7.42348 1 6 4 0 72.3954 8.30899 2 -7 -4 0 363.578 31.0157 1 8 -4 0 -0.9502 6.48697 2 -8 -4 0 1.73468 0.77382 1 -8 4 0 2.9916 0.59749 1 -8 4 0 2.21008 0.7802 1 -9 -4 0 19.8215 2.04829 1 -9 4 0 20.2389 2.02416 1 -9 4 0 23.4728 2.26514 1 10 -4 0 8.21967 2.58411 2 -10 -4 0 9.73048 1.16025 1 10 -4 0 9.33313 8.36865 2 -10 4 0 9.42547 1.30703 1 -10 4 0 8.46667 1.01292 1 10 4 0 11.2083 4.46603 2 10 4 0 8.41364 3.42357 2 -11 -4 0 6.76155 1.02968 1 11 -4 0 5.13178 2.56862 2 11 -4 0 7.68005 8.6193 2 -11 4 0 5.57423 1.02505 1 11 4 0 5.95696 3.90994 2 -11 4 0 4.6922 0.75985 1 0 -5 0 1.13551 0.22856 1 0 5 0 2.25934 1.11804 2 0 5 0 0.84928 0.1612 1 -1 -5 0 119.558 10.2173 1 -2 -5 0 5.3139 0.70311 1 2 -5 0 3.38803 0.63227 1 2 -5 0 3.47835 1.12489 2 2 5 0 3.89643 0.72085 1 -2 5 0 6.15814 1.74401 2 2 5 0 1.63645 1.27271 2 -2 5 0 4.37761 0.62035 1 3 -5 0 1447.75 126.209 2 -3 5 0 1518.79 126.867 2 4 -5 0 -0.0046 0.05537 2 5 5 0 1781.19 157.757 2 5 5 0 1914.78 157.577 2 -6 -5 0 612.156 54.1542 1 6 5 0 618.663 55.3744 2 -6 5 0 707.279 54.2062 1 -6 5 0 609.506 54.4837 2 -7 -5 0 849.767 72.9126 1 7 5 0 827.703 74.4122 2 -7 5 0 891.721 72.9817 1 -7 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1 7 11 8 278.811 32.0902 2 -8 -12 8 60.7472 5.15239 1 8 12 -8 43.8305 8.53047 2 8 12 -8 55.507 5.02637 1 -7 -12 8 55.8903 4.99499 1 7 12 -8 52.8604 4.87932 1 -6 -12 8 32.3921 5.35586 2 -6 -12 8 45.8325 3.90002 1 6 12 -8 43.2912 3.76454 1 6 12 -8 40.4872 7.10249 2 -5 -12 8 328.187 28.483 1 -5 -12 8 322.057 30.256 2 5 12 -8 363.829 28.4408 1 5 12 -8 311.246 31.4629 2 -4 -12 8 373.814 38.0714 2 -4 -12 8 436.798 36.2325 1 4 -12 -8 441.552 36.1038 1 4 -12 -8 407.208 36.0176 1 4 12 -8 400.399 36.1583 1 -4 12 8 462.398 36.767 2 4 12 -8 488.739 39.7461 2 -4 12 8 383.631 37.971 2 -3 -12 8 654.31 56.703 2 3 -12 -8 642.692 54.5202 1 -3 -12 8 637.483 54.5497 1 3 -12 -8 679.541 54.4537 1 3 12 -8 696.002 54.5493 1 -3 12 8 570.578 58.3838 2 3 12 -8 588.095 57.3906 2 2 -12 -8 1459.38 138.064 1 -2 -12 8 1600.91 138.137 1 -2 -12 8 1726.08 140.646 2 2 -12 -8 1771.46 138.082 1 2 12 -8 1540.1 141.194 2 2 12 -8 1539.59 138.056 1 -2 12 8 1755.23 143.629 2 -1 -12 8 1213.9 98.28 1 -1 -12 8 1071.16 100.38 2 1 -12 -8 1250.87 98.2153 1 1 -12 -8 1154.7 98.2443 1 1 12 -8 1113.94 98.1918 1 1 12 -8 1097.94 101.517 2 -1 12 8 1179.93 103.61 2 0 -12 8 231.893 20.5174 1 0 -12 -8 236.439 20.5823 1 0 -12 8 269.857 23.1443 2 0 12 -8 224.814 24.2889 2 0 12 -8 227.751 20.4473 1 1 -12 8 494.296 39.0123 1 -1 -12 -8 474.996 38.9918 1 1 -12 8 433.53 41.2544 2 -1 12 -8 517.682 38.9279 1 1 12 8 391.519 43.3425 2 -1 12 -8 394.251 43.3496 2 2 -12 8 324.782 26.178 1 -2 -12 -8 290.868 26.1162 1 2 -12 8 295.267 28.3741 2 -2 12 -8 321.9 26.0632 1 -2 12 -8 274.511 31.5599 2 -3 -12 -8 23.4021 2.54522 1 3 -12 8 23.6718 5.00192 2 3 -12 8 25.0581 2.602 1 -3 -12 -8 23.0311 2.47864 1 -3 12 -8 21.992 8.58868 2 3 12 8 17.6831 7.39189 2 -3 12 -8 27.7952 2.49418 1 4 -12 8 1.46359 0.82759 1 4 -12 8 1.31846 3.03001 2 -4 -12 -8 0.87165 0.81015 1 -4 12 -8 0.35111 0.57687 1 4 12 8 0.47998 5.86713 2 -4 12 -8 2.57442 7.37652 2 -5 -12 -8 0.24155 0.6274 1 5 -12 8 1.00892 3.26601 2 -5 -12 -8 0.35399 0.76688 1 5 -12 8 0.13908 0.72854 1 -5 12 -8 -1.0506 6.55942 2 5 12 8 0.62755 6.0144 2 -5 12 -8 0.61717 0.63557 1 6 -12 8 12.2296 1.6403 1 6 -12 8 19.8849 5.11094 2 -6 -12 -8 11.8526 1.67643 1 -6 -12 -8 12.8908 1.46816 1 6 12 8 14.4884 8.26246 2 -6 12 -8 14.0261 7.90777 2 -6 12 -8 11.8797 1.55032 1 -7 -12 -8 1.22278 0.76875 1 -7 -12 -8 1.48034 0.73249 1 7 -12 8 1.1421 0.79316 1 7 12 8 1.63032 7.33163 2 -7 12 -8 1.48967 5.34188 2 -8 -13 8 56.2477 8.0019 2 -8 -13 8 72.9802 6.14762 1 8 13 -8 71.2966 6.05999 1 8 13 -8 62.4927 9.90491 2 7 13 -8 72.5574 6.45948 1 -6 -13 8 115.26 10.7506 1 -6 -13 8 137.637 12.8672 2 6 13 -8 120.431 14.1779 2 6 13 -8 121.136 10.6612 1 5 13 -8 44.339 7.12926 2 5 13 -8 35.003 3.39368 1 4 -13 -8 4.01065 0.48392 1 4 -13 -8 2.79105 0.59477 1 -4 -13 8 4.12577 0.77652 1 -4 -13 8 4.50866 3.32707 2 -4 13 8 4.52966 3.79364 2 4 13 -8 5.65527 4.17112 2 4 13 -8 3.47552 0.72733 1 -4 13 8 5.08209 1.65909 2 -3 -13 8 37.9593 5.90422 2 3 -13 -8 42.9488 3.42622 1 3 -13 -8 35.3261 3.54981 1 3 13 -8 44.1529 3.54933 1 3 13 -8 29.1752 6.38652 2 -3 13 8 26.9437 8.07059 2 -3 13 8 33.0444 4.52518 2 -2 -13 8 11.9275 3.37766 2 2 -13 -8 7.5604 1.18873 1 -2 -13 8 5.83099 0.96116 1 2 -13 -8 8.31313 1.01515 1 -2 13 8 20.5683 8.07671 2 2 13 -8 6.67422 1.04953 1 2 13 -8 12.2974 3.86004 2 -1 -13 8 16.4231 3.94268 2 1 -13 -8 19.7142 1.86082 1 1 -13 -8 16.9712 1.96976 1 -1 -13 8 15.1891 1.82733 1 -1 13 8 19.9024 7.67199 2 1 13 -8 15.6432 4.73891 2 0 -13 8 530.508 46.3969 2 0 -13 8 515.8 43.8385 1 0 13 -8 485.52 47.7996 2 0 13 -8 516.94 43.7822 1 -1 -13 -8 160.601 14.2445 1 1 -13 8 150.9 16.4701 2 1 -13 8 167.654 14.2531 1 -1 -13 -8 171.873 14.1625 1 -1 13 -8 146.801 18.8904 2 -1 13 -8 172.607 14.1601 1 1 13 8 159.037 19.1247 2 -2 -13 -8 236.009 21.3047 1 -2 -13 -8 264.598 21.2508 1 2 13 8 263.015 26.4125 2 -2 13 -8 227.895 21.2113 1 -3 -13 -8 12.4874 1.59086 1 3 -13 8 15.833 1.76043 1 -3 -13 -8 14.0036 1.53019 1 3 -13 8 13.9257 4.07286 2 -3 13 -8 12.7796 1.54736 1 3 13 8 6.1854 5.83687 2 -3 13 -8 12.522 7.91524 2 -4 -13 -8 170.96 14.7064 1 4 -13 8 176.317 17.5084 2 4 -13 8 162.412 14.7251 1 -4 -13 -8 167.317 14.568 1 -4 13 -8 147.289 14.5563 1 -4 13 -8 207.836 22.7455 2 -5 -13 -8 124.645 11.1076 1 -5 -13 -8 137.821 11.3066 1 5 -13 8 116.931 11.2491 1 5 -13 8 118.614 14.0394 2 -5 13 -8 134.705 11.18 1 6 -13 8 182.314 16.4135 1 -6 -13 -8 177.419 16.2525 1 -6 -13 -8 200.696 16.1374 1 6 -13 8 220.407 20.2979 2 -6 13 -8 183.097 16.1975 1 -6 13 -8 146.048 21.8254 2 -7 -14 8 95.2126 8.07477 1 7 14 -8 85.7984 7.97025 1 -6 -14 8 295.983 28.3008 2 -6 -14 8 335.547 26.6094 1 6 14 -8 268.491 29.6937 2 6 14 -8 329.349 26.4905 1 -5 -14 8 3.417 0.76464 1 -5 -14 8 3.96339 3.00556 2 5 14 -8 1.82303 0.61475 1 5 14 -8 6.27535 4.25136 2 -4 -14 8 1531.33 118.32 1 4 -14 -8 1315.18 118.047 1 -4 -14 8 1356.13 120.223 2 4 -14 -8 1486.1 118.152 1 -4 14 8 1289.58 118.97 2 4 14 -8 1554.17 118.253 1 4 14 -8 1204.22 121.176 2 3 -14 -8 14.8071 1.6246 1 -3 -14 8 16.0367 1.62469 1 -3 -14 8 7.76472 3.92548 2 3 -14 -8 14.2438 1.39586 1 -3 14 8 3.15738 6.25222 2 -2 -14 8 2013.16 170.228 1 2 -14 -8 1971.38 170.145 1 -2 -14 8 1898.01 172.347 2 2 14 -8 1903.56 173.375 2 -2 14 8 2168.52 171.705 2 2 14 -8 2123.56 170.171 1 -2 14 8 1947.49 175.679 2 1 -14 -8 72.3217 6.99578 1 1 -14 -8 86.1939 6.87851 1 -1 -14 8 77.0779 9.21026 2 -1 -14 8 86.8629 6.99665 1 -1 14 8 85.1499 12.6792 2 1 14 -8 65.835 6.81781 1 1 14 -8 70.1261 9.96713 2 0 -14 8 1452.69 113.429 1 0 -14 -8 1424.12 113.407 1 0 -14 8 1260.26 115.737 2 0 14 -8 1196.15 113.289 1 -1 -14 -8 65.5485 6.22886 1 1 -14 8 66.0797 6.34546 1 -1 -14 -8 70.5102 6.37899 1 -1 14 -8 76.319 6.28082 1 2 -14 8 565.344 50.8145 2 -2 -14 -8 564.052 48.3106 1 -2 -14 -8 620.839 48.2346 1 2 -14 8 587.061 48.3604 1 -2 14 -8 521.294 48.2016 1 2 14 8 525.459 52.5303 2 3 -14 8 191.993 20.3986 2 -3 -14 -8 218.436 18.1417 1 3 -14 8 212.355 18.0991 1 -3 14 -8 217.422 17.9744 1 -3 14 -8 186.214 24.1887 2 4 -14 8 2.55853 0.96624 1 -4 -14 -8 2.81487 0.80445 1 -4 -14 -8 3.22464 0.88371 1 4 -14 8 1.14143 3.02208 2 -4 14 -8 0.77141 7.44328 2 -4 14 -8 3.1851 0.78569 1 4 14 8 0.69546 4.82974 2 -5 -14 -8 0.31906 0.58082 1 5 -14 8 -0.1923 3.17615 2 -5 -14 -8 0.21837 0.60587 1 5 -14 8 0.14727 0.78296 1 5 14 8 -0.3087 4.01256 2 -5 14 -8 0.33413 0.63843 1 -5 14 -8 0.42633 7.26644 2 -6 -14 -8 35.7303 3.10392 1 6 -14 8 27.0756 3.24885 1 -7 -15 8 15.8658 3.40502 2 -7 -15 8 13.7261 1.6964 1 7 15 -8 19.3285 6.89117 2 -6 -15 8 49.3158 4.41479 1 -6 -15 8 44.3953 6.06225 2 6 15 -8 50.9703 4.3228 1 6 15 -8 37.589 7.52942 2 -5 -15 8 41.5053 3.53565 1 -5 -15 8 32.3464 5.05381 2 5 15 -8 37.2148 3.39455 1 5 15 -8 30.9912 6.55265 2 -4 -15 8 49.077 7.0051 2 4 -15 -8 57.6936 5.23171 1 4 -15 -8 61.078 5.3586 1 4 15 -8 70.1497 5.44157 1 4 15 -8 70.5142 9.2143 2 -4 15 8 55.8824 6.38145 2 3 -15 -8 67.2475 6.22254 1 3 -15 -8 71.6724 6.02335 1 -3 -15 8 71.2787 8.58062 2 3 15 -8 76.8381 6.17145 1 -3 15 8 64.4576 11.6193 2 3 15 -8 58.0823 9.22148 2 -3 15 8 64.5664 7.29137 2 2 -15 -8 5.56546 0.80825 1 2 -15 -8 4.87708 1.05297 1 -2 15 8 5.46727 2.36475 2 -2 15 8 3.23916 6.93564 2 1 -15 -8 28.537 3.14433 1 1 -15 -8 28.2658 2.90164 1 -1 -15 8 32.1197 3.07062 1 -1 -15 8 33.9266 5.33476 2 -1 15 8 35.6242 4.84439 2 -1 15 8 36.0201 9.23947 2 1 15 -8 29.1219 2.92927 1 1 15 -8 33.4142 6.78671 2 0 -15 8 4.09671 0.88154 1 0 -15 -8 2.51201 0.77411 1 0 -15 -8 1.94116 0.93094 1 0 -15 8 0.81782 3.22174 2 0 15 -8 0.38684 3.87175 2 0 15 -8 2.93453 0.7367 1 0 15 8 -1.4466 5.92881 2 1 -15 8 37.1261 5.90873 2 -1 -15 -8 31.7549 3.35969 1 -1 -15 -8 35.5443 3.23167 1 -1 15 -8 30.5217 3.22353 1 -1 15 -8 42.5073 8.76846 2 1 15 8 35.1241 8.11431 2 2 -15 8 7.70504 3.10635 2 -2 -15 -8 9.05657 1.29155 1 2 -15 8 7.91254 1.26312 1 -2 -15 -8 9.19807 1.14289 1 2 15 8 0.76743 3.9565 2 -2 15 -8 7.73957 7.75259 2 -2 15 -8 7.61559 1.12136 1 3 -15 8 206.216 18.7326 1 3 -15 8 206.712 21.2632 2 -3 -15 -8 220.874 18.5593 1 -3 -15 -8 212.658 18.6847 1 -3 15 -8 226.689 18.6229 1 4 -15 8 59.0311 5.62174 1 -4 -15 -8 64.1689 5.41858 1 -4 -15 -8 66.5746 5.61463 1 4 -15 8 58.4845 8.43012 2 -4 15 -8 51.2303 12.2048 2 -4 15 -8 53.4654 5.424 1 4 15 8 55.7737 10.0194 2 -5 -15 -8 7.43615 1.3314 1 -5 -15 -8 9.59258 1.2097 1 5 15 8 9.4589 6.59883 2 -6 -16 8 138.21 15.6297 2 6 16 -8 184.424 14.1248 1 -5 -16 8 327.68 30.6726 2 -5 -16 8 344.271 28.7443 1 5 16 -8 361.58 28.6311 1 5 16 -8 298.667 31.8411 2 -4 -16 8 483.122 42.7522 2 4 -16 -8 478.021 40.4623 1 -4 -16 8 558.58 40.6683 1 4 -16 -8 443.814 40.373 1 4 16 -8 477.05 44.0093 2 -4 16 8 411.004 41.513 2 3 -16 -8 258.339 26.1385 1 -3 -16 8 340.668 26.3844 1 -3 -16 8 336.692 28.7285 2 3 -16 -8 282.194 26.32 1 3 16 -8 335.108 26.2952 1 -3 16 8 311.804 27.667 2 3 16 -8 278.856 29.4764 2 -3 16 8 311.934 31.9925 2 2 -16 -8 150.96 11.9496 1 -2 -16 8 125.871 13.9903 2 -2 -16 8 150.473 11.8408 1 2 -16 -8 119.97 11.6241 1 -2 16 8 131.206 18.0748 2 -2 16 8 115.233 13.0584 2 2 16 -8 145.913 11.744 1 1 -16 -8 707.566 62.4505 1 -1 -16 8 798.656 62.2957 1 1 -16 -8 700.719 62.115 1 -1 -16 8 756.322 64.593 2 1 16 -8 627.257 65.4098 2 1 16 -8 780.97 62.1841 1 0 -16 -8 619.579 49.4973 1 0 -16 -8 619.302 49.67 1 0 16 8 485.485 54.1751 2 -1 -16 -8 356.374 29.6528 1 -1 -16 -8 371.753 29.4911 1 1 16 8 300.07 31.34 2 -2 -16 -8 222.758 19.1107 1 -2 -16 -8 232.833 18.9874 1 -2 16 -8 215.979 19.0877 1 2 16 8 201.713 23.3559 2 -3 -16 -8 148.878 12.8594 1 -3 -16 -8 155.581 12.714 1 3 16 8 123.948 16.9105 2 -4 -16 -8 41.1872 3.58674 1 4 -16 8 30.4064 6.27977 2 -4 -16 -8 47.2828 3.87889 1 4 -16 8 40.132 3.84627 1 -4 16 -8 20.1952 9.97808 2 4 16 8 29.2954 7.92619 2 -4 16 -8 32.982 3.9568 1 -5 -16 -8 48.9408 4.324 1 5 -16 8 52.2346 4.61968 1 5 -16 8 47.4788 8.04611 2 -5 16 -8 29.5169 11.7803 2 5 16 8 32.7354 8.39186 2 -5 -17 8 125.094 13.844 2 5 17 -8 149.468 12.0384 1 -4 -17 8 45.7118 5.93263 2 4 17 -8 27.4612 5.91333 2 -4 17 8 35.7927 5.50468 2 -3 -17 8 49.5921 6.61067 2 3 -17 -8 45.3884 4.63296 1 3 -17 -8 44.1665 4.42817 1 -3 -17 8 59.3258 4.69436 1 -3 17 8 48.7706 6.26447 2 3 17 -8 50.6543 8.10019 2 -3 17 8 41.7056 9.81288 2 3 17 -8 55.8097 4.58945 1 -2 -17 8 50.97 3.92659 1 2 -17 -8 44.2948 3.99618 1 2 -17 -8 40.0905 3.68623 1 -2 -17 8 39.5588 6.15552 2 2 17 -8 30.9073 6.73908 2 -2 17 8 28.4559 9.08618 2 -2 17 8 33.6211 5.32688 2 1 -17 -8 60.6895 5.28526 1 -1 -17 8 56.4661 5.13188 1 1 -17 -8 57.9408 4.98614 1 -1 -17 8 52.8822 7.37582 2 1 17 -8 42.5127 8.31054 2 1 17 -8 59.6409 5.03591 1 -1 17 8 49.841 10.4863 2 -1 17 8 48.4415 6.73854 2 0 -17 8 0.13315 2.64626 2 0 -17 -8 3.42878 0.98388 1 0 -17 -8 3.13668 0.78347 1 0 17 -8 0.50754 5.00981 2 0 17 8 1.58548 5.64056 2 0 17 8 1.27982 2.2832 2 -1 -17 -8 103.45 9.1223 1 1 -17 8 91.7501 9.04345 1 1 -17 8 100.129 11.6108 2 -1 -17 -8 103.447 8.95803 1 -1 17 -8 107.591 8.98098 1 2 -17 8 1.04841 0.7607 1 -2 -17 -8 0.69468 0.8072 1 -2 -17 -8 0.81042 0.64742 1 2 -17 8 2.5428 3.39056 2 2 17 8 2.60489 3.02259 2 -2 17 -8 0.68177 0.60648 1 -2 17 -8 2.19414 7.15765 2 2 17 8 0.00768 4.5319 2 3 -17 8 233.637 22.9982 2 -3 -17 -8 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5 -11 809.044 70.6069 2 -2 5 11 756.477 64.5719 1 -1 -5 11 9.75732 1.36248 1 -1 -5 11 6.56724 3.03668 2 1 5 -11 8.74726 7.46474 2 1 5 -11 7.65659 1.11412 1 0 -5 -11 46.8868 7.41994 2 0 -5 -11 53.4192 4.99615 1 0 -5 11 52.864 4.96541 1 0 -5 11 46.2054 6.95377 2 0 5 -11 57.282 4.88239 1 0 5 -11 53.9867 11.1642 2 -1 -5 -11 5.76232 3.64911 2 1 -5 11 6.32678 1.24411 1 1 -5 11 7.51498 4.38409 2 -1 -5 -11 7.7155 1.3263 1 -1 5 -11 7.52192 7.97114 2 1 5 11 7.8963 7.62309 2 -1 5 -11 5.92081 1.10838 1 -2 -5 -11 116.101 9.98995 1 2 -5 11 124.282 13.3567 2 -2 -5 -11 97.1852 11.7954 2 2 -5 11 107.201 9.83337 1 2 5 11 100.795 16.0395 2 -2 5 -11 128.122 17.2297 2 -2 5 -11 105.381 9.82858 1 -3 -5 -11 318.624 28.3189 2 3 -5 11 332.384 29.9733 2 3 -5 11 291.074 25.8042 1 -3 -5 -11 271.07 25.9223 1 -3 5 -11 248.493 30.9278 2 -3 5 -11 327.462 25.9322 1 -4 -5 -11 200.299 17.0092 1 -4 -5 -11 182.8 18.7086 2 5 -5 11 217.931 22.6549 2 5 -5 11 213.39 17.3112 1 -5 5 -11 172.452 21.1713 2 -5 5 -11 189.237 17.3984 1 6 -5 11 193.363 24.6922 2 -6 -5 -11 227.727 22.1294 2 -6 5 -11 263.582 24.3355 2 6 5 11 225.202 29.591 2 -6 5 -11 244.012 20.3483 1 8 -6 -11 0.9646 1.35204 2 8 -6 -11 0.72098 0.23363 1 -8 -6 11 0.66082 2.70763 2 -7 -6 11 19.9735 4.17437 2 -7 -6 11 19.4729 2.19429 1 7 6 -11 21.7756 2.04324 1 7 6 -11 13.5135 6.38216 2 6 -6 -11 49.5189 8.27519 2 -6 -6 11 47.3444 6.93349 2 -6 -6 11 48.6343 4.92783 1 6 -6 -11 57.6405 4.73347 1 -6 6 11 56.0709 4.81163 1 6 6 -11 57.9406 4.81786 1 -6 6 11 47.3903 6.57548 2 -5 -6 11 342.491 31.2346 1 -5 -6 11 342.093 33.3664 2 5 -6 -11 383.007 35.007 2 5 -6 -11 366.205 31.0642 1 -5 6 11 348.356 32.883 2 5 6 -11 383.208 31.1371 1 -5 6 11 382.097 31.1676 1 4 -6 -11 2.72661 0.60535 1 4 -6 -11 9.19277 5.09132 2 4 6 -11 1.46523 0.56686 1 -4 6 11 5.18811 2.76871 2 4 6 -11 3.35641 4.57921 2 -4 6 11 3.38069 0.81602 1 3 -6 -11 89.9189 8.49711 1 -3 -6 11 111.988 11.4247 2 3 -6 -11 116.4 12.3903 2 -3 -6 11 93.593 8.62616 1 3 6 -11 104.346 13.9679 2 3 6 -11 83.7167 8.4711 1 2 -6 -11 12.1627 1.51331 1 -2 -6 11 10.4991 1.50108 1 -2 -6 11 12.23 3.40924 2 2 -6 -11 20.819 5.16221 2 2 6 -11 21.6443 7.50336 2 -2 6 11 22.604 6.33261 2 -1 -6 11 262.837 24.2072 1 -1 -6 11 318.554 26.9196 2 1 6 -11 290.112 30.0061 2 1 6 -11 258.963 24.0708 1 0 -6 11 43.2961 4.09831 1 0 -6 11 43.8201 6.60904 2 0 -6 -11 47.4148 6.533 2 0 6 11 44.4175 9.64791 2 0 6 -11 58.0843 11.2471 2 0 6 -11 34.7956 3.89544 1 1 -6 11 438.217 38.7507 1 1 -6 11 474.399 41.558 2 -1 -6 -11 443.252 40.8856 2 -1 6 -11 508.307 46.1845 2 -1 6 -11 412.622 38.6494 1 2 -6 11 63.5875 5.88646 1 -2 -6 -11 65.9313 8.20282 2 -2 -6 -11 60.8194 5.94363 1 2 -6 11 55.9264 8.3185 2 -2 6 -11 58.0616 12.2467 2 -2 6 -11 68.2121 5.85116 1 3 -6 11 188.81 16.5373 1 3 -6 11 207.515 20.2333 2 -3 -6 -11 161.58 16.611 1 -3 -6 -11 213.012 18.9095 2 3 6 11 174.058 23.3634 2 -3 6 -11 192.478 16.6003 1 4 -6 11 145.278 11.8451 1 4 -6 11 110.884 18.7047 2 -4 -6 -11 155.004 12.1003 1 -4 -6 -11 123.724 13.6557 2 -4 6 -11 108.971 16.9387 2 5 -6 11 128.832 12.2083 1 -5 -6 -11 145.032 14.4264 2 5 -6 11 160.644 17.3082 2 5 6 11 120.517 20.5521 2 -6 -6 -11 38.4628 3.59717 1 6 -6 11 27.3374 8.00855 2 -6 -6 -11 24.9745 4.87583 2 -6 6 -11 26.0874 6.77906 2 -6 6 -11 33.8889 3.38043 1 -8 -7 11 6.66649 3.25898 2 -8 -7 11 9.65002 1.41773 1 8 7 -11 4.55995 5.46393 2 8 7 -11 10.9267 1.14454 1 -7 -7 11 233.427 22.2514 2 -6 -7 11 2.17785 0.82875 1 -6 -7 11 1.16689 2.86816 2 6 -7 -11 1.44463 2.57722 2 6 -7 -11 0.31184 0.35543 1 -6 7 11 0.29348 2.16225 2 6 7 -11 0.36991 0.51636 1 6 7 -11 1.15877 5.19285 2 5 -7 -11 1116.26 97.9336 1 -5 -7 11 1057.92 100.175 2 5 -7 -11 1190.69 100.531 2 -5 -7 11 1219.02 98.1464 1 -5 7 11 1152.7 99.8111 2 5 7 -11 1181.8 98.0228 1 -4 -7 11 118.242 9.28492 1 -4 -7 11 93.9974 11.3722 2 -4 7 11 95.8784 10.9724 2 -3 -7 11 945.47 93.1955 2 3 -7 -11 1036.43 93.4096 2 3 -7 -11 1069.12 90.975 1 -3 -7 11 1163.15 91.1291 1 3 7 -11 962.183 95.5699 2 3 7 -11 1073.61 90.9906 1 -3 7 11 1235.55 94.5851 2 -2 -7 11 97.6774 11.8245 2 2 -7 -11 120.49 9.64192 1 -2 -7 11 103.46 9.63215 1 2 7 -11 80.354 14.0434 2 -2 7 11 106.838 14.021 2 2 7 -11 123.976 9.57949 1 -1 -7 11 50.3161 7.58425 2 1 -7 -11 49.7039 7.3145 2 -1 -7 11 62.8606 5.27706 1 0 -7 -11 9.92831 3.47205 2 0 -7 -11 10.2389 1.52455 1 0 -7 11 12.7085 1.60378 1 0 -7 11 7.51415 3.3233 2 0 7 -11 10.0899 8.37331 2 0 7 11 9.59338 7.81521 2 0 7 -11 9.56517 1.258 1 1 -7 11 31.9709 3.02643 1 -1 -7 -11 31.5196 3.0991 1 1 -7 11 24.9526 4.92006 2 -1 -7 -11 23.1271 4.81797 2 -1 7 -11 16.5575 9.4954 2 2 -7 11 1.71001 2.81738 2 -2 -7 -11 1.18226 2.15042 2 2 -7 11 1.06746 0.90584 1 -2 -7 -11 0.72119 0.78105 1 -2 7 -11 3.73814 7.64725 2 -2 7 -11 0.63739 0.63581 1 2 7 11 0.75287 5.76552 2 3 -7 11 233.105 21.3752 2 3 -7 11 177.038 17.657 1 -3 -7 -11 236.125 19.981 2 -3 -7 -11 193.29 17.8327 1 -3 7 -11 187.678 17.6742 1 -3 7 -11 206.408 24.6312 2 4 -7 11 27.1147 6.42803 2 4 -7 11 27.7736 3.15473 1 -4 -7 -11 33.888 3.42399 1 -4 7 -11 37.0152 3.3302 1 4 7 11 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5.34651 2 0 -5 15 1.11065 0.79389 1 0 -5 15 2.0068 3.86427 2 0 -5 -15 1.80544 0.85146 1 0 -5 -15 2.60732 3.92409 2 0 5 -15 1.53194 0.88349 1 0 5 -15 3.04213 6.34607 2 0 5 15 4.10025 6.45403 2 -1 -5 -15 25.0837 5.60273 2 -1 -5 -15 23.2901 2.80983 1 1 5 15 31.116 9.35348 2 2 -5 15 69.1349 9.94399 2 -2 5 -15 74.7765 6.83064 1 -4 -6 15 3.58821 3.76379 2 4 -6 -15 8.73765 1.17549 1 4 -6 -15 2.94947 4.8962 2 -4 -6 15 7.89518 1.47276 1 4 6 -15 9.67199 1.18886 1 -4 6 15 4.6044 3.76206 2 4 6 -15 5.2916 8.9711 2 3 -6 -15 239.662 25.4522 2 -3 -6 15 265.135 21.6322 1 -3 -6 15 211.933 24.0346 2 3 -6 -15 267.935 21.4315 1 -3 6 15 246.44 24.8116 2 3 6 -15 218.961 28.5966 2 3 6 -15 262.455 21.442 1 2 -6 -15 15.8982 5.08016 2 -2 -6 15 16.8098 2.15491 1 -2 -6 15 13.28 4.56004 2 2 -6 -15 18.5333 2.03307 1 2 6 -15 11.5908 9.38128 2 -2 6 15 15.3327 5.4582 2 2 6 -15 15.9025 1.84123 1 -1 -6 15 207.037 16.4261 1 1 -6 -15 179.325 19.319 2 -1 -6 15 155.936 18.5702 2 1 -6 -15 173.439 16.2367 1 1 6 -15 169.322 23.4659 2 -1 6 15 202.954 21.9051 2 1 6 -15 205.066 16.2516 1 0 -6 -15 143.146 11.4816 1 0 -6 15 106.689 13.8241 2 0 6 15 128.517 17.4277 2 1 -6 15 357.149 31.4418 2 1 6 15 284.458 34.0195 2 3 -7 -15 191.956 15.2457 1 -3 -7 15 150.74 18.0167 2 3 -7 -15 170.625 18.7094 2 -3 -7 15 178.904 15.4359 1 -3 7 15 172.252 19.0104 2 -2 -7 15 16.6678 2.09738 1 -2 -7 15 11.9374 3.92787 2 2 -7 -15 19.4806 2.06346 1 2 -7 -15 14.7665 4.82896 2 -2 7 15 14.3199 5.89938 2 2 7 -15 20.8114 2.00297 1 2 7 -15 6.99964 7.20534 2 -1 -7 15 0.77148 2.9239 2 1 -7 -15 0.83482 0.91353 1 1 -7 -15 1.40752 3.64143 2 1 7 -15 0.19536 0.61613 1 -1 7 15 2.54691 6.45463 2 0 -7 15 24.8051 2.65272 1 0 -7 -15 18.1887 5.05516 2 0 7 -15 12.3127 9.71973 2 0 7 15 22.4713 8.86014 2 -1 7 -15 1.43521 8.5909 2 -1 7 -15 0.85895 0.98584 1 2 -8 -15 153.352 16.5775 2 -2 -8 15 130.464 13.1426 1 2 -8 -15 155.486 13.1242 1 -2 8 15 161.164 18.6707 2 1 -8 -15 490.238 41.328 1 -1 -8 15 418.197 41.2749 1 -1 8 15 500.671 48.0357 2 1 8 -15 518.047 41.2468 1 0 8 -15 69.9908 6.45681 1 -2 0 16 383.168 41.3607 2 -2 0 16 478.62 38.8769 1 2 0 -16 486.774 38.7357 1 -1 0 16 0.13155 0.89067 1 1 0 -16 0.40322 6.61965 2 -1 0 16 -0.0245 2.80964 2 1 0 -16 0.19555 0.75241 1 0 0 -16 110.273 9.94124 1 2 -1 -16 40.909 10.1368 2 -2 -1 16 43.2479 4.31713 1 -2 -1 16 38.1727 6.84076 2 2 -1 -16 44.6395 4.16467 1 2 1 -16 37.6367 10.6497 2 -2 1 16 41.1828 7.26895 2 -2 1 16 48.919 4.37608 1 2 1 -16 43.2918 4.12168 1 1 -1 -16 110.916 9.42549 1 1 -1 -16 79.6844 14.3469 2 -1 -1 16 96.2541 12.4301 2 -1 -1 16 117.499 9.55652 1 -1 1 16 96.8613 12.6161 2 -1 1 16 107.672 9.46988 1 1 1 -16 79.7444 14.988 2 1 1 -16 120.105 9.45493 1 -2 -2 16 128.089 15.7566 2 -2 -2 16 154.152 13.3254 1 2 -2 -16 157.607 13.1821 1 -2 2 16 140.04 16.2978 2 -2 2 16 146.887 13.2567 1 2 2 -16 165.347 13.198 1 -1 -2 16 33.501 3.75 1 1 -2 -16 38.9704 3.74028 1 -1 -2 16 36.5827 6.79023 2 1 2 -16 38.3161 3.66721 1 -1 2 16 38.4524 7.41056 2 1 2 -16 26.1521 9.30983 2 -1 2 16 43.32 3.84375 1