#------------------------------------------------------------------------------ #$Date: 2021-11-23 01:15:38 +0200 (Tue, 23 Nov 2021) $ #$Revision: 270814 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/53/1565346.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1565346 loop_ _publ_author_name 'Zhao, Yong-Ye' 'xiao, hongyan' 'Tung, Chen-Ho' 'Wu, Li-Zhu' 'Cong, Huan' _publ_section_title ; Adsorptive Separation of Cyclohexanol and Cyclohexanone by Nonporous Adaptive Crystals of RhombicArene ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC04728K _journal_year 2021 _chemical_formula_moiety '0.5(C74 H76 O12), 0.5(C74 H74 O12), C2 H3 N' _chemical_formula_sum 'C76 H78 N O12' _chemical_formula_weight 1197.39 _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2020-06-02 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-05-17 deposited with the CCDC. 2021-11-22 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 108.9620(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 20.06780(10) _cell_length_b 15.89110(10) _cell_length_c 25.6047(2) _cell_measurement_reflns_used 62384 _cell_measurement_temperature 170.00(13) _cell_measurement_theta_max 74.9900 _cell_measurement_theta_min 2.4310 _cell_volume 7722.23(10) _computing_cell_refinement 'CrysAlisPro 1.171.40.67a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.67a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.67a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 170.00(13) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.981 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -85.00 -8.00 0.50 0.20 -- -47.20 110.00 -85.00 154 2 \w -57.00 -31.00 0.50 2.00 -- -99.00 61.00 -60.00 52 3 \w -19.00 21.00 0.50 0.20 -- -47.20 19.00-150.00 80 4 \w -9.00 20.00 0.50 0.20 -- -47.20 19.00-180.00 58 5 \w -101.00 -75.00 0.50 0.20 -- -47.20-125.00 -30.00 52 6 \w -113.00 -75.00 0.50 0.20 -- -47.20-125.00 -90.00 76 7 \w -119.00 -83.00 0.50 0.20 -- -47.20-125.00 -60.00 72 8 \w -112.00 -86.00 0.50 2.00 -- -99.00 -61.00-150.00 52 9 \w -168.00 -97.00 0.50 2.00 -- -99.00 -45.00-180.00 142 10 \w -168.00-141.00 0.50 2.00 -- -99.00 -61.00-150.00 54 11 \w -102.00 -27.00 0.50 2.00 -- -99.00 77.00 -90.00 150 12 \w -102.00 -26.00 0.50 2.00 -- -99.00 110.00 -85.00 152 13 \w -68.00 -27.00 0.50 2.00 -- -99.00 61.00 60.00 82 14 \w -68.00 -42.00 0.50 2.00 -- -99.00 61.00 120.00 52 15 \w -68.00 -29.00 0.50 2.00 -- -99.00 61.00 90.00 78 16 \w -20.00 23.00 0.50 0.20 -- -47.20 38.00 90.00 86 17 \w 23.00 49.00 0.50 0.20 -- 47.20-110.00 179.00 52 18 \w 75.00 105.00 0.50 2.00 -- 103.25-110.00 179.00 60 19 \w 38.00 75.00 0.50 2.00 -- 103.25 -61.00 150.00 74 20 \w 90.00 156.00 0.50 2.00 -- 103.25 15.00 30.00 132 21 \w 93.00 169.00 0.50 2.00 -- 103.25 110.00 -85.00 152 22 \w 107.00 157.00 0.50 2.00 -- 103.25 61.00-120.00 100 23 \w 56.00 104.00 0.50 2.00 -- 103.25 -94.00-180.00 96 24 \w 36.00 71.00 0.50 2.00 -- 103.25 -61.00-150.00 70 25 \w 40.00 104.00 0.50 2.00 -- 103.25-125.00 -60.00 128 26 \w -139.00-114.00 0.50 2.00 -- -99.00-110.00 179.00 50 27 \w 104.00 129.00 0.50 2.00 -- 103.25 110.00 -85.00 50 28 \w -34.00 6.00 0.50 0.20 -- -47.20 38.00 -30.00 80 29 \w -61.00 24.00 0.50 0.20 -- -47.20 57.00-120.00 170 30 \w -120.00 -94.00 0.50 0.20 -- -47.20-125.00 60.00 52 31 \w -31.00 25.00 0.50 0.20 -- -47.20 38.00 150.00 112 32 \w -6.00 28.00 0.50 0.20 -- 47.20 -19.00 150.00 68 33 \w -89.00 -63.00 0.50 2.00 -- -99.00 77.00-180.00 52 34 \w -124.00 -98.00 0.50 2.00 -- -99.00 142.00 -69.27 52 35 \w -58.00 -26.00 0.50 2.00 -- -99.00 125.00-120.00 64 36 \w -59.00 -33.00 0.50 2.00 -- -99.00 143.00 16.09 52 37 \w -58.00 -32.00 0.50 2.00 -- -99.00 138.00 165.54 52 38 \w -56.00 -29.00 0.50 2.00 -- -99.00 61.00 -30.00 54 39 \w -143.00 -90.00 0.50 2.00 -- -99.00 -73.00-173.74 106 40 \w -151.00 -94.00 0.50 2.00 -- -99.00 -53.00 12.80 114 41 \w -167.00-132.00 0.50 2.00 -- -99.00 -53.00 25.79 70 42 \w -160.00-124.00 0.50 2.00 -- -99.00 -77.00-120.00 72 43 \w -121.00 -94.00 0.50 2.00 -- -99.00 -53.00 25.79 54 44 \w -153.00 -85.00 0.50 2.00 -- -99.00 -52.00 43.12 136 45 \w -118.00 -78.00 0.50 2.00 -- -99.00 138.00 165.54 80 46 \w -126.00-100.00 0.50 2.00 -- -99.00 144.00-171.50 52 47 \w -125.00-100.00 0.50 2.00 -- -99.00 143.00 16.09 50 48 \w -51.00 -26.00 0.50 2.00 -- -99.00 77.00-180.00 50 49 \w -112.00 -86.00 0.50 2.00 -- -99.00 125.00-120.00 52 50 \w 33.00 111.00 0.50 2.00 -- 103.25-125.00 0.00 156 51 \w 82.00 109.00 0.50 2.00 -- 103.25 -77.00 -30.00 54 52 \w 33.00 76.00 0.50 2.00 -- 103.25 -77.00 -30.00 86 53 \w 78.00 111.00 0.50 2.00 -- 103.25-125.00 120.00 66 54 \w 83.00 108.00 0.50 2.00 -- 103.25-110.00 179.00 50 55 \w 31.00 69.00 0.50 2.00 -- 103.25 -61.00-180.00 76 56 \w 40.00 109.00 0.50 2.00 -- 103.25-125.00-180.00 138 57 \w 61.00 106.00 0.50 2.00 -- 103.25 -94.00 -30.00 90 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy R, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0247797000 _diffrn_orient_matrix_UB_12 -0.0646384000 _diffrn_orient_matrix_UB_13 0.0472127000 _diffrn_orient_matrix_UB_21 -0.0426026000 _diffrn_orient_matrix_UB_22 -0.0692274000 _diffrn_orient_matrix_UB_23 -0.0387692000 _diffrn_orient_matrix_UB_31 0.0644536000 _diffrn_orient_matrix_UB_32 -0.0208053000 _diffrn_orient_matrix_UB_33 -0.0177735000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0425 _diffrn_reflns_av_unetI/netI 0.0349 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.981 _diffrn_reflns_limit_h_max 24 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -32 _diffrn_reflns_number 128124 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.961 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 75.437 _diffrn_reflns_theta_min 2.328 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'PhotonJet R (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.554 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.84403 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.67a (Rigaku Oxford Diffraction, 2019) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.030 _exptl_crystal_description plate _exptl_crystal_F_000 2548 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.05 _refine_diff_density_max 0.539 _refine_diff_density_min -0.308 _refine_diff_density_rms 0.054 _refine_ls_abs_structure_details ; Flack x determined using 11569 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.23(4) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.046 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 1665 _refine_ls_number_reflns 30735 _refine_ls_number_restraints 488 _refine_ls_restrained_S_all 1.089 _refine_ls_R_factor_all 0.0692 _refine_ls_R_factor_gt 0.0636 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1327P)^2^+1.3196P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1867 _refine_ls_wR_factor_ref 0.1945 _reflns_Friedel_coverage 0.889 _reflns_Friedel_fraction_full 0.993 _reflns_Friedel_fraction_max 0.940 _reflns_number_gt 27346 _reflns_number_total 30735 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1sc04728k2.cif _cod_data_source_block tx2347c_sq _cod_original_cell_volume 7722.22(10) _cod_database_code 1565346 _shelx_shelxl_version_number 2016/6 _chemical_oxdiff_usercomment 'C H O N Zn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _reflns_odcompleteness_completeness 99.99 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 68.13 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2. Restrained distances C98-C100 = C97-C103 = C110-C105 = C113-C106 = C150-C145 = C147-C146 = C44-C40 = C47-C41 = C50-C49 = C54-C53 = C7-C4 = C3-C10 = C17-C16 = C20-C15 1.51 with sigma of 0.01 C101-C100 = C102-C101 = C103-C102 = C111-C110 = C112-C111 = C113-C112 = C150- C149 = C149-C148 = C148-C147 = C138-C137 = C139-C138 = C140-C139 = C51-C50 = C52-C51 = C53-C52 = C45-C44 = C46-C45 = C47-C46 = C8-C7 = C9-C8 = C9-C10 = C18- C17 = C19-C18 = C20-C19 1.53 with sigma of 0.01 C44A-C40 = C44-C40 = C47A-C41 = C47-C41 1.51 with sigma of 0.01 C45-C44 = C45A-C44A = C46-C45 = C46A-C45A = C47A-C46A = C47-C46 = C47A-C41 = C47-C41 1.53 with sigma of 0.01 3. Uiso/Uaniso restraints and constraints C100 \\sim C101 \\sim C102 \\sim C103 \\sim C110 \\sim C111 \\sim C112 \\sim C113 \\sim C147 \\sim C148 \\sim C149 \\sim C150 \\sim C137 \\sim C138 \\sim C139 \\sim C140 \\sim C44 \\sim C45 \\sim C46 \\sim C47 \\sim C50 \\sim C51 \\sim C52 \\sim C53 \\sim C7 \\sim C8 \\sim C9 \\sim C10 \\sim C17 \\sim C18 \\sim C19 \\sim C20: within 1.7A with sigma of 0.02 and sigma for terminal atoms of 0.04 C44 \\sim C45 \\sim C46 \\sim C46A \\sim C45A \\sim C44A \\sim C47 \\sim C47A: within 1.7A with sigma of 0.02 and sigma for terminal atoms of 0.04 Uanis(C100) \\sim Ueq, Uanis(C101) \\sim Ueq, Uanis(C102) \\sim Ueq, Uanis(C103) \\sim Ueq, Uanis(C110) \\sim Ueq, Uanis(C111) \\sim Ueq, Uanis(C112) \\sim Ueq, Uanis(C113) \\sim Ueq, Uanis(C150) \\sim Ueq, Uanis(C149) \\sim Ueq, Uanis(C148) \\sim Ueq, Uanis(C147) \\sim Ueq, Uanis(C137) \\sim Ueq, Uanis(C138) \\sim Ueq, Uanis(C139) \\sim Ueq, Uanis(C140) \\sim Ueq, Uanis(C44) \\sim Ueq, Uanis(C45) \\sim Ueq, Uanis(C46) \\sim Ueq, Uanis(C47) \\sim Ueq, Uanis(C40) \\sim Ueq, Uanis(C50) \\sim Ueq, Uanis(C51) \\sim Ueq, Uanis(C52) \\sim Ueq, Uanis(C53) \\sim Ueq, Uanis(C7) \\sim Ueq, Uanis(C8) \\sim Ueq, Uanis(C9) \\sim Ueq, Uanis(C10) \\sim Ueq, Uanis(C17) \\sim Ueq, Uanis(C18) \\sim Ueq, Uanis(C19) \\sim Ueq, Uanis(C20) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C45) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 Uanis(C46) \\sim Ueq, Uanis(C47) \\sim Ueq, Uanis(C47A) \\sim Ueq, Uanis(C46A) \\sim Ueq, Uanis(C44) \\sim Ueq, Uanis(C45) \\sim Ueq, Uanis(C45A) \\sim Ueq, Uanis(C44A) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 4. Others Sof(C47A)=Sof(H47C)=Sof(H47D)=Sof(C46A)=Sof(H46C)=Sof(H46D)=Sof(C45A)= Sof(H45C)=Sof(H45D)=Sof(C44A)=Sof(H44C)=Sof(H44D)=1-FVAR(1) Sof(C44)=Sof(H44A)=Sof(H44B)=Sof(C45)=Sof(H45A)=Sof(H45B)=Sof(C46)=Sof(H46A)= Sof(H46B)=Sof(C47)=Sof(H47A)=Sof(H47B)=FVAR(1) Fixed Y: O24(0.17424) 5.a Secondary CH2 refined with riding coordinates: C7(H7A,H7B), C8(H8A,H8B), C9(H9A,H9B), C10(H10A,H10B), C17(H17A,H17B), C18(H18A,H18B), C19(H19A,H19B), C20(H20A,H20B), C29(H29A,H29B), C44(H44A,H44B), C45(H45A,H45B), C46(H46A,H46B), C47(H47A,H47B), C50(H50A,H50B), C51(H51A, H51B), C52(H52A,H52B), C53(H53A,H53B), C66(H66A,H66B), C85(H85A,H85B), C100(H10C,H10D), C101(H10E,H10F), C102(H10G,H10H), C103(H10I,H10J), C110(H11A, H11B), C111(H11C,H11D), C112(H11E,H11F), C113(H11G,H11H), C122(H12D,H12E), C137(H13D,H13E), C138(H13F,H13G), C139(H13H,H13I), C140(H14B,H14C), C147(H14D, H14E), C150(H15A,H15B), C47A(H47C,H47D), C46A(H46C,H46D), C45A(H45C,H45D), C44A(H44C,H44D) 5.b Aromatic/amide H refined with riding coordinates: C5(H5), C14(H14), C23(H23), C26(H26), C31(H31), C34(H34), C39(H39), C55(H55), C59(H59), C62(H62), C68(H68), C71(H71), C78(H78), C81(H81), C87(H87), C90(H90), C99(H99), C107(H107), C115(H115), C118(H118), C124(H124), C127(H127), C132(H132), C144(H144), C148(H148), C149(H149) 5.c Idealised Me refined as rotating group: C27(H27A,H27B,H27C), C28(H28A,H28B,H28C), C36(H36A,H36B,H36C), C37(H37A,H37B, H37C), C64(H64A,H64B,H64C), C65(H65A,H65B,H65C), C73(H73A,H73B,H73C), C74(H74A, H74B,H74C), C83(H83A,H83B,H83C), C84(H84A,H84B,H84C), C92(H92A,H92B,H92C), C93(H93A,H93B,H93C), C120(H12A,H12B,H12C), C129(H12F,H12G,H12H), C130(H13A, H13B,H13C), C155(H15C,H15D,H15E), C76(H76A,H76B,H76C), C154(H15F,H15G,H15H) 5.d Idealised tetrahedral OH refined as rotating group: O1(H1), O2(H2), O7(H7), O8(H8), O13(H13), O14(H14A), O19(H19), O20(H20) ; _shelx_res_file ; TITL tx2347c_a.res in P2(1) tx2347c_sq.res created by SHELXL-2016/6 at 15:07:56 on 02-Jun-2020 REM Old TITL tx2347c in P2(1)/m REM SHELXT solution in P2(1): R1 0.184, Rweak 0.021, Alpha 0.006 REM 0.653 for 10 systematic absences, Orientation as input REM Flack x = 0.209 ( 0.033 ) from 11983 Parsons' quotients REM Formula found by SHELXT: C149 N17 O21 CELL 1.54184 20.0678 15.8911 25.6047 90 108.962 90 ZERR 4 0.0001 0.0001 0.0002 0 0.001 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H N O UNIT 304 312 4 48 DFIX 1.51 0.01 C98 C100 C97 C103 C110 C105 C113 C106 C150 C145 C147 C146 = C44 C40 C47 C41 C50 C49 C54 C53 C7 C4 C3 C10 C17 C16 C20 C15 DFIX 1.53 0.01 C101 C100 C102 C101 C103 C102 C111 C110 C112 C111 C113 C112 = C150 C149 C149 C148 C148 C147 C138 C137 C139 C138 C140 C139 C51 C50 C52 C51 = C53 C52 C45 C44 C46 C45 C47 C46 C8 C7 C9 C8 C9 C10 C18 C17 C19 C18 C20 C19 DFIX 1.51 0.01 C44A C40 C44 C40 C47A C41 C47 C41 DFIX 1.53 0.01 C45 C44 C45A C44A C46 C45 C46A C45A C47A C46A C47 C46 C47A = C41 C47 C41 SIMU 0.02 0.04 1.7 C100 C101 C102 C103 C110 C111 C112 C113 C147 C148 C149 = C150 C137 C138 C139 C140 C44 C45 C46 C47 C50 C51 C52 C53 C7 C8 C9 C10 C17 = C18 C19 C20 SIMU 0.02 0.04 1.7 C44 C45 C46 C46A C45A C44A C47 C47A ISOR 0.01 0.02 C100 C101 C102 C103 C110 C111 C112 C113 C150 C149 C148 C147 = C137 C138 C139 C140 C44 C45 C46 C47 C40 C50 C51 C52 C53 C7 C8 C9 C10 C17 = C18 C19 C20 ISOR 0.001 0.002 C45 ISOR 0.01 0.02 C46 C47 C47A C46A C44 C45 C45A C44A L.S. 11 0 192 PLAN 30 BOND ABIN fmap 2 acta OMIT -10 0 12 OMIT -3 0 1 REM REM REM WGHT 0.132700 1.319600 FVAR 0.25721 0.63913 O1 4 0.272488 0.585555 1.110088 11.00000 0.06102 0.05851 = 0.05597 -0.00204 0.01711 0.01388 AFIX 147 H1 2 0.238216 0.597065 1.119505 11.00000 -1.50000 AFIX 0 O2 4 0.412113 0.513921 1.065072 11.00000 0.06199 0.04470 = 0.05256 -0.01100 0.03315 -0.01646 AFIX 147 H2 2 0.442521 0.499472 1.051907 11.00000 -1.50000 AFIX 0 O3 4 0.470804 0.435025 0.995491 11.00000 0.05654 0.05546 = 0.04798 0.00885 0.02915 0.00378 O4 4 0.260131 0.553419 0.811546 11.00000 0.06254 0.09056 = 0.05333 -0.00169 0.01100 -0.00867 O5 4 0.501490 0.674751 0.891900 11.00000 0.05443 0.04420 = 0.06437 -0.00593 0.02609 0.00443 O6 4 0.259290 0.846103 0.779327 11.00000 0.12722 0.12075 = 0.07043 -0.01387 -0.01040 0.07196 O7 4 0.261164 0.892362 0.894056 11.00000 0.11201 0.04691 = 0.08825 0.00309 0.06697 0.00079 AFIX 147 H7 2 0.267844 0.848053 0.880108 11.00000 -1.50000 AFIX 0 O8 4 0.319319 1.007710 1.014951 11.00000 0.05905 0.08513 = 0.04617 0.01477 0.02703 0.01778 AFIX 147 H8 2 0.326976 1.018303 1.047726 11.00000 -1.50000 AFIX 0 O9 4 0.311093 1.091051 1.106210 11.00000 0.06682 0.07280 = 0.05076 -0.00261 0.02933 -0.02532 O10 4 0.101635 0.880918 1.128369 11.00000 0.05989 0.06822 = 0.05621 -0.00331 0.03115 -0.01924 O11 4 0.361578 0.894432 1.260054 11.00000 0.05590 0.03736 = 0.06852 -0.01799 0.01673 -0.00655 O12 4 0.206001 0.605575 1.189194 11.00000 0.05116 0.04261 = 0.11723 -0.02158 0.03498 -0.01033 C1 1 0.324752 0.553225 1.154137 11.00000 0.04741 0.03284 = 0.05285 -0.00719 0.02641 -0.00421 C2 1 0.355322 0.477794 1.146237 11.00000 0.05091 0.02905 = 0.05143 -0.00282 0.03071 -0.00240 C3 1 0.410767 0.443702 1.188964 11.00000 0.05627 0.03632 = 0.05525 0.00164 0.03730 -0.00335 C4 1 0.437008 0.486395 1.239098 11.00000 0.03970 0.04113 = 0.05812 0.00836 0.02382 -0.00402 C5 1 0.404829 0.561482 1.246215 11.00000 0.04265 0.03851 = 0.05015 -0.00572 0.01642 -0.00756 AFIX 43 H5 2 0.422117 0.589746 1.279727 11.00000 -1.20000 AFIX 0 C6 1 0.348172 0.595171 1.205132 11.00000 0.04399 0.03086 = 0.05291 -0.01014 0.02354 -0.00464 C7 1 0.498106 0.452507 1.286046 11.00000 0.04819 0.06729 = 0.07642 0.02520 0.01921 0.00120 AFIX 23 H7A 2 0.481543 0.432811 1.315518 11.00000 -1.20000 H7B 2 0.532418 0.496747 1.300655 11.00000 -1.20000 AFIX 0 C8 1 0.534116 0.376045 1.263710 11.00000 0.04931 0.07011 = 0.11837 0.04005 0.01561 0.01138 AFIX 23 H8A 2 0.560973 0.398269 1.241418 11.00000 -1.20000 H8B 2 0.566362 0.346273 1.294779 11.00000 -1.20000 AFIX 0 C9 1 0.480271 0.317172 1.230383 11.00000 0.10013 0.07981 = 0.07849 0.01618 0.03488 0.02452 AFIX 23 H9A 2 0.502670 0.267299 1.221895 11.00000 -1.20000 H9B 2 0.449397 0.300074 1.250785 11.00000 -1.20000 AFIX 0 C10 1 0.439867 0.359509 1.179651 11.00000 0.08230 0.04808 = 0.07415 0.00899 0.05181 0.01421 AFIX 23 H10A 2 0.401051 0.323495 1.159383 11.00000 -1.20000 H10B 2 0.469777 0.367649 1.156967 11.00000 -1.20000 AFIX 0 C11 1 0.327115 0.435647 1.090482 11.00000 0.06024 0.03354 = 0.05497 -0.00771 0.03343 -0.00352 C12 1 0.357576 0.456319 1.050494 11.00000 0.05729 0.03164 = 0.05374 -0.00670 0.03383 -0.00770 C13 1 0.329826 0.425168 0.996599 11.00000 0.06248 0.03516 = 0.05343 -0.01033 0.03446 -0.01124 C14 1 0.273667 0.367944 0.985684 11.00000 0.07535 0.04849 = 0.06098 -0.02170 0.04181 -0.02450 AFIX 43 H14 2 0.255777 0.344958 0.950470 11.00000 -1.20000 AFIX 0 C15 1 0.243896 0.344379 1.025086 11.00000 0.08610 0.05233 = 0.06650 -0.02206 0.04832 -0.02912 C16 1 0.269713 0.379540 1.077492 11.00000 0.07059 0.04449 = 0.06014 -0.00874 0.04164 -0.01344 C17 1 0.237534 0.358275 1.122058 11.00000 0.09017 0.06292 = 0.06691 -0.01937 0.05491 -0.02899 AFIX 23 H17A 2 0.208800 0.405231 1.126243 11.00000 -1.20000 H17B 2 0.275096 0.350795 1.156891 11.00000 -1.20000 AFIX 0 C18 1 0.192151 0.278727 1.109415 11.00000 0.15114 0.12154 = 0.10997 -0.03765 0.08796 -0.08235 AFIX 23 H18A 2 0.222580 0.229705 1.118067 11.00000 -1.20000 H18B 2 0.162653 0.277408 1.132829 11.00000 -1.20000 AFIX 0 C19 1 0.148089 0.274565 1.052421 11.00000 0.14964 0.14611 = 0.10810 -0.07068 0.09104 -0.10673 AFIX 23 H19A 2 0.113838 0.319759 1.045676 11.00000 -1.20000 H19B 2 0.122242 0.221928 1.046798 11.00000 -1.20000 AFIX 0 C20 1 0.184884 0.280468 1.010231 11.00000 0.11502 0.09071 = 0.08551 -0.03762 0.06240 -0.06440 AFIX 23 H20A 2 0.150836 0.295556 0.974904 11.00000 -1.20000 H20B 2 0.203978 0.225693 1.006193 11.00000 -1.20000 AFIX 0 C21 1 0.349693 0.458891 0.949363 11.00000 0.06153 0.03170 = 0.04800 -0.00947 0.03088 -0.00822 C22 1 0.419325 0.465451 0.949999 11.00000 0.05820 0.03596 = 0.04514 -0.00407 0.02712 -0.00086 C23 1 0.433612 0.502417 0.905017 11.00000 0.05781 0.03294 = 0.04811 -0.00176 0.03026 -0.00496 AFIX 43 H23 2 0.480109 0.506664 0.905701 11.00000 -1.20000 AFIX 0 C24 1 0.380291 0.532797 0.859560 11.00000 0.06119 0.03435 = 0.04264 -0.00920 0.02222 -0.00408 C25 1 0.310606 0.522882 0.858279 11.00000 0.05970 0.04735 = 0.04604 -0.00857 0.01791 -0.00719 C26 1 0.295571 0.486747 0.902197 11.00000 0.05802 0.05063 = 0.04999 -0.01167 0.02259 -0.01134 AFIX 43 H26 2 0.248853 0.480700 0.900595 11.00000 -1.20000 AFIX 0 C27 1 0.187741 0.539702 0.807345 11.00000 0.05745 0.22271 = 0.07719 0.02338 0.00295 0.00450 AFIX 137 H27A 2 0.157557 0.562838 0.773219 11.00000 -1.50000 H27B 2 0.178240 0.566715 0.837713 11.00000 -1.50000 H27C 2 0.179100 0.480396 0.808297 11.00000 -1.50000 AFIX 0 C28 1 0.541549 0.437570 0.993941 11.00000 0.05787 0.09585 = 0.05342 0.02431 0.03116 0.01211 AFIX 137 H28A 2 0.543773 0.408441 0.961702 11.00000 -1.50000 H28B 2 0.572586 0.410920 1.026399 11.00000 -1.50000 H28C 2 0.555660 0.495054 0.992683 11.00000 -1.50000 AFIX 0 C29 1 0.397593 0.581106 0.815462 11.00000 0.07148 0.04093 = 0.03741 -0.00678 0.02551 0.00025 AFIX 23 H29A 2 0.365956 0.564707 0.779446 11.00000 -1.20000 H29B 2 0.445439 0.568677 0.816788 11.00000 -1.20000 AFIX 0 C30 1 0.390073 0.675098 0.824346 11.00000 0.07081 0.03822 = 0.03730 -0.00098 0.02684 0.00321 C31 1 0.329843 0.718074 0.795032 11.00000 0.07836 0.05499 = 0.04020 -0.00261 0.01346 0.00907 AFIX 43 H31 2 0.295832 0.690690 0.766499 11.00000 -1.20000 AFIX 0 C32 1 0.318481 0.801297 0.806921 11.00000 0.08084 0.05838 = 0.04667 0.00359 0.01423 0.02097 C33 1 0.368862 0.843666 0.849083 11.00000 0.07627 0.03807 = 0.04446 -0.00086 0.03374 0.00450 C34 1 0.430528 0.801559 0.877972 11.00000 0.06059 0.03642 = 0.04971 -0.00336 0.03423 -0.00180 AFIX 43 H34 2 0.464892 0.829353 0.906035 11.00000 -1.20000 AFIX 0 C35 1 0.441764 0.718668 0.865677 11.00000 0.05902 0.03292 = 0.04873 -0.00141 0.03187 0.00004 C36 1 0.550774 0.711671 0.938482 11.00000 0.06246 0.07266 = 0.07024 -0.02318 0.01798 0.00632 AFIX 137 H36A 2 0.566519 0.764239 0.928170 11.00000 -1.50000 H36B 2 0.590314 0.674608 0.952752 11.00000 -1.50000 H36C 2 0.529126 0.721364 0.966316 11.00000 -1.50000 AFIX 0 C37 1 0.219344 0.832192 0.733484 11.00000 0.08582 0.24195 = 0.13160 0.02636 -0.02019 0.01790 AFIX 137 H37A 2 0.245122 0.831339 0.707794 11.00000 -1.50000 H37B 2 0.184142 0.875518 0.723148 11.00000 -1.50000 H37C 2 0.197006 0.778659 0.733059 11.00000 -1.50000 AFIX 0 C38 1 0.358561 0.932066 0.864319 11.00000 0.08401 0.03695 = 0.04762 0.00670 0.03697 0.01378 C39 1 0.404594 0.995506 0.859940 11.00000 0.07477 0.04633 = 0.04636 0.00324 0.03508 0.00653 AFIX 43 H39 2 0.440566 0.982123 0.845878 11.00000 -1.20000 AFIX 0 C40 1 0.398438 1.078581 0.876002 11.00000 0.06965 0.03884 = 0.04724 0.00576 0.02922 0.00902 C41 1 0.345183 1.098405 0.898129 11.00000 0.07473 0.03872 = 0.04354 0.00266 0.02755 0.01098 C42 1 0.299773 1.034516 0.905040 11.00000 0.06651 0.04239 = 0.04545 0.00617 0.02925 0.01279 C43 1 0.306490 0.952497 0.887141 11.00000 0.07630 0.03870 = 0.05114 0.00566 0.03587 0.00630 PART 1 C44 1 0.447956 1.143731 0.867247 21.00000 0.07859 0.04354 = 0.06685 0.00606 0.04277 0.00586 AFIX 23 H44A 2 0.427516 1.170390 0.831515 21.00000 -1.20000 H44B 2 0.492131 1.117717 0.868380 21.00000 -1.20000 AFIX 0 C45 1 0.460651 1.208959 0.913241 21.00000 0.09698 0.09634 = 0.09822 -0.00177 0.03350 -0.00081 AFIX 23 H45A 2 0.482210 1.182099 0.948764 21.00000 -1.20000 H45B 2 0.492640 1.251939 0.908684 21.00000 -1.20000 AFIX 0 C46 1 0.392662 1.248417 0.911647 21.00000 0.07930 0.04165 = 0.08988 -0.01177 0.03548 -0.00076 AFIX 23 H46A 2 0.371859 1.275789 0.876202 21.00000 -1.20000 H46B 2 0.401837 1.291309 0.940066 21.00000 -1.20000 AFIX 0 C47 1 0.340928 1.185784 0.920284 21.00000 0.06163 0.05192 = 0.07153 -0.01363 0.03034 -0.00046 AFIX 23 H47A 2 0.293666 1.207313 0.902824 21.00000 -1.20000 H47B 2 0.348383 1.181555 0.959569 21.00000 -1.20000 AFIX 0 PART 0 C48 1 0.242498 1.052039 0.929130 11.00000 0.06455 0.03897 = 0.04067 0.00438 0.02443 0.01325 C49 1 0.176115 1.080119 0.895217 11.00000 0.06899 0.03924 = 0.04382 0.00078 0.02308 0.00541 C50 1 0.163577 1.093828 0.834220 11.00000 0.08246 0.05581 = 0.04693 0.01101 0.02859 0.01326 AFIX 23 H50A 2 0.205864 1.117520 0.829611 11.00000 -1.20000 H50B 2 0.155170 1.039760 0.815638 11.00000 -1.20000 AFIX 0 C51 1 0.102989 1.150579 0.807198 11.00000 0.09457 0.07881 = 0.05682 0.00773 0.02997 0.02547 AFIX 23 H51A 2 0.116962 1.208375 0.817177 11.00000 -1.20000 H51B 2 0.090730 1.145591 0.767429 11.00000 -1.20000 AFIX 0 C52 1 0.040081 1.130527 0.823488 11.00000 0.07287 0.12468 = 0.08704 0.05013 0.01564 0.00741 AFIX 23 H52A 2 0.022318 1.075928 0.808309 11.00000 -1.20000 H52B 2 0.003754 1.171668 0.806609 11.00000 -1.20000 AFIX 0 C53 1 0.051778 1.128944 0.885143 11.00000 0.06681 0.08145 = 0.06886 0.01494 0.02350 0.01961 AFIX 23 H53A 2 0.048266 1.185818 0.897755 11.00000 -1.20000 H53B 2 0.014961 1.095631 0.891984 11.00000 -1.20000 AFIX 0 C54 1 0.122530 1.092819 0.917819 11.00000 0.06384 0.04236 = 0.04823 0.00271 0.01817 0.00585 C55 1 0.134707 1.073526 0.973237 11.00000 0.06077 0.04491 = 0.05416 -0.00427 0.02778 -0.00116 AFIX 43 H55 2 0.098227 1.080690 0.987787 11.00000 -1.20000 AFIX 0 C56 1 0.199163 1.044032 1.007566 11.00000 0.05712 0.04917 = 0.04339 -0.00166 0.02433 0.00011 C57 1 0.254157 1.035990 0.985128 11.00000 0.06158 0.05187 = 0.04086 0.00288 0.02451 0.00541 C58 1 0.204995 1.017107 1.064551 11.00000 0.05285 0.05062 = 0.04343 -0.00302 0.02677 0.00113 C59 1 0.150825 0.964658 1.070007 11.00000 0.05177 0.05165 = 0.04510 -0.00308 0.02503 -0.00378 AFIX 43 H59 2 0.113471 0.950109 1.038789 11.00000 -1.20000 AFIX 0 C60 1 0.152563 0.934483 1.121379 11.00000 0.04886 0.04712 = 0.05007 -0.00767 0.02815 -0.00538 C61 1 0.207237 0.954355 1.168839 11.00000 0.05332 0.04091 = 0.04344 -0.00457 0.02819 0.00204 C62 1 0.259284 1.009274 1.163402 11.00000 0.05101 0.04395 = 0.04272 -0.00599 0.02225 -0.00311 AFIX 43 H62 2 0.294959 1.026633 1.194937 11.00000 -1.20000 AFIX 0 C63 1 0.258994 1.038535 1.112038 11.00000 0.05073 0.05162 = 0.04948 -0.00689 0.02677 -0.00895 C64 1 0.363837 1.119475 1.155307 11.00000 0.07939 0.11286 = 0.05903 -0.00987 0.02956 -0.04866 AFIX 137 H64A 2 0.392991 1.160748 1.145921 11.00000 -1.50000 H64B 2 0.392332 1.072670 1.173326 11.00000 -1.50000 H64C 2 0.341638 1.144110 1.179674 11.00000 -1.50000 AFIX 0 C65 1 0.047691 0.854369 1.080224 11.00000 0.08415 0.12173 = 0.06670 -0.01633 0.02547 -0.05754 AFIX 137 H65A 2 0.028517 0.902340 1.057526 11.00000 -1.50000 H65B 2 0.011117 0.827017 1.090470 11.00000 -1.50000 H65C 2 0.066842 0.815740 1.060013 11.00000 -1.50000 AFIX 0 C66 1 0.215313 0.913643 1.223533 11.00000 0.05604 0.03573 = 0.04604 -0.00247 0.02856 0.00436 AFIX 23 H66A 2 0.169415 0.905793 1.227781 11.00000 -1.20000 H66B 2 0.243272 0.949346 1.253340 11.00000 -1.20000 AFIX 0 C67 1 0.251315 0.829362 1.225735 11.00000 0.05277 0.03459 = 0.04643 -0.00394 0.02796 0.00120 C68 1 0.211163 0.756713 1.208721 11.00000 0.04592 0.04838 = 0.05750 -0.00917 0.02796 -0.00041 AFIX 43 H68 2 0.162487 0.759421 1.200151 11.00000 -1.20000 AFIX 0 C69 1 0.242727 0.680111 1.204337 11.00000 0.04776 0.04044 = 0.06470 -0.01509 0.02996 -0.00791 C70 1 0.314675 0.674737 1.214765 11.00000 0.04636 0.03562 = 0.05023 -0.00979 0.02186 0.00107 C71 1 0.355192 0.745566 1.234850 11.00000 0.04582 0.03772 = 0.04731 -0.00959 0.01713 -0.00108 AFIX 43 H71 2 0.403975 0.741962 1.244670 11.00000 -1.20000 AFIX 0 C72 1 0.324256 0.822381 1.240667 11.00000 0.05209 0.03223 = 0.04410 -0.00908 0.01945 -0.00397 C73 1 0.435568 0.887702 1.278222 11.00000 0.05588 0.04853 = 0.11144 -0.02778 0.01586 -0.01298 AFIX 137 H73A 2 0.451151 0.875979 1.247270 11.00000 -1.50000 H73B 2 0.449999 0.842884 1.304649 11.00000 -1.50000 H73C 2 0.455987 0.939653 1.295129 11.00000 -1.50000 AFIX 0 C74 1 0.133653 0.606761 1.176282 11.00000 0.06026 0.06319 = 0.12627 0.00018 0.02134 -0.01419 AFIX 137 H74A 2 0.114009 0.648486 1.148408 11.00000 -1.50000 H74B 2 0.121778 0.620133 1.208746 11.00000 -1.50000 H74C 2 0.114860 0.552488 1.162714 11.00000 -1.50000 AFIX 0 O13 4 0.255825 0.388969 0.609715 11.00000 0.07386 0.03874 = 0.07233 0.00246 0.04355 0.00454 AFIX 147 H13 2 0.249584 0.343844 0.622955 11.00000 -1.50000 AFIX 0 O14 4 0.185831 0.487246 0.484987 11.00000 0.04314 0.09608 = 0.04209 -0.02113 0.01998 -0.02346 AFIX 147 H14A 2 0.168265 0.510008 0.454890 11.00000 -1.50000 AFIX 0 O15 4 0.181327 0.568611 0.389341 11.00000 0.05060 0.10150 = 0.04163 -0.00612 0.01585 0.02661 O16 4 0.399242 0.376467 0.364092 11.00000 0.05331 0.04896 = 0.05495 -0.00858 0.02729 0.00642 O17 4 0.137527 0.387355 0.229271 11.00000 0.05684 0.04113 = 0.06827 0.01963 0.01243 -0.00242 O18 4 0.292905 0.099982 0.306623 11.00000 0.03804 0.03851 = 0.08287 0.00245 0.01930 0.00119 O19 4 0.219556 0.070989 0.378086 11.00000 0.05795 0.06143 = 0.04888 0.00824 0.01313 -0.01017 AFIX 147 H19 2 0.253807 0.083492 0.368895 11.00000 -1.50000 AFIX 0 O20 4 0.079399 0.011350 0.423852 11.00000 0.05385 0.04583 = 0.04932 0.00953 0.03022 0.01717 AFIX 147 H20 2 0.053105 0.003164 0.442055 11.00000 -1.50000 AFIX 0 O21 4 0.021192 -0.064557 0.495318 11.00000 0.04420 0.05240 = 0.04175 -0.00981 0.02175 -0.00338 O22 4 0.243833 0.030454 0.676924 11.00000 0.05019 0.09813 = 0.05776 -0.00632 0.00080 0.01127 O23 4 0.266748 0.318198 0.713247 11.00000 0.06664 0.06223 = 0.06735 0.00283 0.00243 -0.02368 O24 4 0.005469 10.174240 0.613124 11.00000 0.04518 0.03714 = 0.05373 0.00261 0.01951 -0.00264 C77 1 0.347039 0.425873 0.371627 11.00000 0.04365 0.03628 = 0.04586 -0.00281 0.02341 -0.00462 C78 1 0.348535 0.456692 0.422707 11.00000 0.03905 0.03846 = 0.03911 -0.00238 0.01754 -0.00181 AFIX 43 H78 2 0.387429 0.445388 0.453562 11.00000 -1.20000 AFIX 0 C79 1 0.292944 0.504378 0.428940 11.00000 0.03972 0.04528 = 0.03582 0.00043 0.01831 -0.00102 C80 1 0.236672 0.522236 0.381754 11.00000 0.04211 0.05998 = 0.04001 -0.00118 0.01750 0.00656 C81 1 0.235920 0.493888 0.330418 11.00000 0.04288 0.05905 = 0.03482 0.00087 0.01525 0.00154 AFIX 43 H81 2 0.198157 0.507900 0.299350 11.00000 -1.20000 AFIX 0 C82 1 0.290053 0.445204 0.324288 11.00000 0.04700 0.04088 = 0.03827 -0.00222 0.02314 -0.00982 C83 1 0.457055 0.355829 0.411500 11.00000 0.08031 0.08986 = 0.06877 0.00312 0.02672 0.04951 AFIX 137 H83A 2 0.490509 0.322922 0.400687 11.00000 -1.50000 H83B 2 0.440591 0.324014 0.436751 11.00000 -1.50000 H83C 2 0.479195 0.406581 0.429149 11.00000 -1.50000 AFIX 0 C84 1 0.123885 0.588167 0.340718 11.00000 0.07909 0.21321 = 0.05215 -0.01106 0.00510 0.08136 AFIX 137 H84A 2 0.141315 0.616962 0.314835 11.00000 -1.50000 H84B 2 0.090866 0.623592 0.350292 11.00000 -1.50000 H84C 2 0.100890 0.537085 0.324368 11.00000 -1.50000 AFIX 0 C85 1 0.283424 0.406495 0.268807 11.00000 0.05492 0.03774 = 0.04340 -0.00531 0.02715 -0.01161 AFIX 23 H85A 2 0.329704 0.399510 0.265114 11.00000 -1.20000 H85B 2 0.255761 0.442851 0.239276 11.00000 -1.20000 AFIX 0 C86 1 0.247637 0.321765 0.265306 11.00000 0.04998 0.03844 = 0.03887 -0.00211 0.02211 -0.00962 C87 1 0.287467 0.248909 0.283823 11.00000 0.04502 0.04316 = 0.04465 -0.00952 0.02496 -0.01226 AFIX 43 H87 2 0.336271 0.251605 0.293462 11.00000 -1.20000 AFIX 0 C88 1 0.255719 0.172364 0.288168 11.00000 0.04291 0.03750 = 0.04623 0.00075 0.02013 -0.00255 C89 1 0.182902 0.167295 0.275062 11.00000 0.03806 0.03720 = 0.04249 0.00506 0.01490 -0.00572 C90 1 0.143127 0.238618 0.254450 11.00000 0.04036 0.03843 = 0.04319 0.00737 0.01279 -0.00679 AFIX 43 H90 2 0.094272 0.235520 0.244060 11.00000 -1.20000 AFIX 0 C91 1 0.174593 0.314613 0.248965 11.00000 0.04997 0.03824 = 0.04080 0.00745 0.01463 -0.00602 C92 1 0.063190 0.381560 0.212547 11.00000 0.06209 0.04943 = 0.12845 0.02553 0.01686 0.00313 AFIX 137 H92A 2 0.047385 0.338243 0.185160 11.00000 -1.50000 H92B 2 0.042844 0.434408 0.197240 11.00000 -1.50000 H92C 2 0.048906 0.368097 0.243892 11.00000 -1.50000 AFIX 0 C93 1 0.367365 0.102668 0.322921 11.00000 0.04156 0.06031 = 0.09770 -0.00468 0.01821 0.00410 AFIX 137 H93A 2 0.381559 0.121531 0.292507 11.00000 -1.50000 H93B 2 0.386057 0.047448 0.333945 11.00000 -1.50000 H93C 2 0.384978 0.140847 0.353365 11.00000 -1.50000 AFIX 0 C94 1 0.146842 0.088033 0.282741 11.00000 0.03777 0.03077 = 0.04810 0.00529 0.01739 -0.00111 C95 1 0.165730 0.043818 0.332558 11.00000 0.04229 0.03798 = 0.04775 0.00447 0.02037 -0.00031 C96 1 0.130020 -0.028259 0.338494 11.00000 0.05605 0.03082 = 0.05657 0.00514 0.03755 0.00654 C97 1 0.072072 -0.056761 0.294173 11.00000 0.05837 0.03592 = 0.07055 -0.01004 0.04634 -0.00746 C98 1 0.052258 -0.013008 0.244681 11.00000 0.04316 0.03864 = 0.06428 -0.00691 0.03013 -0.00337 C99 1 0.089500 0.059112 0.239750 11.00000 0.03926 0.03606 = 0.05277 0.00293 0.01759 -0.00255 AFIX 43 H99 2 0.075421 0.088682 0.206609 11.00000 -1.20000 AFIX 0 C100 1 -0.009074 -0.040513 0.195215 11.00000 0.05206 0.06168 = 0.07230 -0.01961 0.02800 -0.02014 AFIX 23 H10C 2 -0.048045 -0.002266 0.191397 11.00000 -1.20000 H10D 2 0.004691 -0.034535 0.162426 11.00000 -1.20000 AFIX 0 C101 1 -0.034846 -0.128096 0.196715 11.00000 0.09713 0.08040 = 0.09095 -0.01319 0.03102 -0.03451 AFIX 23 H10E 2 -0.080658 -0.135154 0.168835 11.00000 -1.20000 H10F 2 -0.002411 -0.167880 0.189242 11.00000 -1.20000 AFIX 0 C102 1 -0.039917 -0.143251 0.251555 11.00000 0.09409 0.08121 = 0.07793 -0.04073 0.04269 -0.04830 AFIX 23 H10G 2 -0.059025 -0.199124 0.252354 11.00000 -1.20000 H10H 2 -0.072658 -0.103071 0.258195 11.00000 -1.20000 AFIX 0 C103 1 0.032725 -0.135961 0.299519 11.00000 0.09502 0.04874 = 0.08105 -0.01341 0.06414 -0.02493 AFIX 23 H10I 2 0.024415 -0.135544 0.334781 11.00000 -1.20000 H10J 2 0.061463 -0.184714 0.298719 11.00000 -1.20000 AFIX 0 C104 1 0.154991 -0.074166 0.392196 11.00000 0.06698 0.03509 = 0.06416 0.01132 0.04429 0.00959 C105 1 0.207957 -0.135006 0.402099 11.00000 0.10344 0.04877 = 0.08955 0.03150 0.07815 0.03381 C106 1 0.233880 -0.173498 0.453982 11.00000 0.09750 0.05448 = 0.09139 0.03310 0.07044 0.03903 C107 1 0.210060 -0.145883 0.496176 11.00000 0.07025 0.04643 = 0.06835 0.02347 0.04719 0.02403 AFIX 43 H107 2 0.229106 -0.169693 0.531053 11.00000 -1.20000 AFIX 0 C108 1 0.158623 -0.083757 0.488276 11.00000 0.05010 0.03338 = 0.05495 0.00917 0.03080 0.00897 C109 1 0.129613 -0.050341 0.435058 11.00000 0.04815 0.03194 = 0.05169 0.00638 0.02988 0.00783 C110 1 0.236922 -0.159106 0.356324 11.00000 0.12960 0.06562 = 0.09351 0.03441 0.08995 0.04878 AFIX 23 H11A 2 0.266655 -0.113842 0.351236 11.00000 -1.20000 H11B 2 0.197983 -0.165270 0.322169 11.00000 -1.20000 AFIX 0 C111 1 0.279583 -0.240654 0.367693 11.00000 0.18576 0.10825 = 0.11368 0.05919 0.11716 0.09826 AFIX 23 H11C 2 0.247677 -0.288250 0.361388 11.00000 -1.20000 H11D 2 0.306185 -0.245138 0.342240 11.00000 -1.20000 AFIX 0 C112 1 0.329303 -0.243624 0.425848 11.00000 0.15052 0.11333 = 0.12979 0.07102 0.10904 0.09525 AFIX 23 H11E 2 0.361226 -0.196046 0.432147 11.00000 -1.20000 H11F 2 0.357204 -0.294675 0.431058 11.00000 -1.20000 AFIX 0 C113 1 0.289795 -0.241415 0.467717 11.00000 0.14091 0.07844 = 0.11995 0.05149 0.10002 0.07106 AFIX 23 H11G 2 0.267813 -0.295644 0.468200 11.00000 -1.20000 H11H 2 0.323006 -0.231255 0.504272 11.00000 -1.20000 AFIX 0 C114 1 0.143956 -0.049109 0.537671 11.00000 0.04525 0.03136 = 0.05097 0.00571 0.02451 0.00618 C115 1 0.200566 -0.027602 0.583753 11.00000 0.04301 0.04730 = 0.05856 0.00570 0.02107 0.00648 AFIX 43 H115 2 0.246168 -0.037303 0.583515 11.00000 -1.20000 AFIX 0 C116 1 0.190634 0.008026 0.630132 11.00000 0.04483 0.04845 = 0.05251 0.00406 0.00731 0.00484 C117 1 0.122413 0.024262 0.631580 11.00000 0.04979 0.03146 = 0.04099 0.00619 0.01630 0.00257 C118 1 0.066054 -0.000005 0.586764 11.00000 0.04356 0.03310 = 0.04417 0.00186 0.02110 0.00367 AFIX 43 H118 2 0.020529 0.009099 0.587361 11.00000 -1.20000 AFIX 0 C119 1 0.075635 -0.038031 0.540350 11.00000 0.04254 0.03403 = 0.03942 0.00514 0.01918 0.00421 C120 1 0.313757 0.005573 0.681232 11.00000 0.04570 0.17202 = 0.09425 -0.02645 -0.00051 0.02016 AFIX 137 H12A 2 0.329945 0.038625 0.656355 11.00000 -1.50000 H12B 2 0.313988 -0.052892 0.671853 11.00000 -1.50000 H12C 2 0.344371 0.014250 0.718385 11.00000 -1.50000 AFIX 0 C122 1 0.111634 0.071094 0.679088 11.00000 0.05841 0.03631 = 0.03397 0.00549 0.01591 -0.00221 AFIX 23 H12D 2 0.145093 0.051437 0.713517 11.00000 -1.20000 H12E 2 0.064481 0.060652 0.680180 11.00000 -1.20000 AFIX 0 C123 1 0.121775 0.164816 0.672575 11.00000 0.05197 0.03537 = 0.03359 0.00143 0.01720 -0.00151 C124 1 0.186463 0.203437 0.698890 11.00000 0.05500 0.04448 = 0.03965 0.00654 0.00970 -0.00505 AFIX 43 H124 2 0.222124 0.172487 0.723833 11.00000 -1.20000 AFIX 0 C125 1 0.198938 0.286269 0.688905 11.00000 0.05471 0.04695 = 0.04196 0.00166 0.01302 -0.00563 C126 1 0.145238 0.336308 0.653086 11.00000 0.05535 0.03429 = 0.03722 0.00053 0.02282 -0.00423 C127 1 0.079875 0.298196 0.627722 11.00000 0.04643 0.03477 = 0.03860 0.00093 0.02530 0.00278 AFIX 43 H127 2 0.043465 0.329576 0.603903 11.00000 -1.20000 AFIX 0 C128 1 0.068342 0.214395 0.637446 11.00000 0.04710 0.03507 = 0.03595 -0.00066 0.02231 -0.00122 C129 1 -0.047856 0.218135 0.572283 11.00000 0.04728 0.05577 = 0.05789 0.00691 0.01459 -0.00189 AFIX 137 H12F 2 -0.031021 0.233110 0.542458 11.00000 -1.50000 H12G 2 -0.060075 0.268232 0.588065 11.00000 -1.50000 H12H 2 -0.088687 0.182874 0.558587 11.00000 -1.50000 AFIX 0 C130 1 0.277565 0.371252 0.756801 11.00000 0.09573 0.10623 = 0.08444 -0.03171 0.00696 -0.01646 AFIX 137 H13A 2 0.241816 0.413991 0.747744 11.00000 -1.50000 H13B 2 0.323069 0.397088 0.765067 11.00000 -1.50000 H13C 2 0.275458 0.340182 0.788381 11.00000 -1.50000 AFIX 0 C131 1 0.156289 0.425055 0.638846 11.00000 0.05365 0.03448 = 0.03881 -0.00133 0.02125 -0.00429 C132 1 0.109288 0.487173 0.643232 11.00000 0.05713 0.04034 = 0.03783 -0.00279 0.02495 -0.00404 AFIX 43 H132 2 0.075065 0.473440 0.659075 11.00000 -1.20000 AFIX 0 C133 1 0.111928 0.569181 0.624643 11.00000 0.05118 0.03541 = 0.03702 -0.00554 0.02128 -0.00661 C134 1 0.162021 0.589477 0.599339 11.00000 0.05201 0.03512 = 0.03615 -0.00042 0.01856 -0.00790 C135 1 0.209525 0.528011 0.594332 11.00000 0.04725 0.03888 = 0.03456 -0.00345 0.01897 -0.00819 C136 1 0.207317 0.446854 0.615212 11.00000 0.05761 0.03368 = 0.04056 -0.00465 0.02511 -0.00381 C137 1 0.163872 0.675644 0.574519 11.00000 0.05311 0.04116 = 0.05738 0.01101 0.02263 -0.00111 AFIX 23 H13D 2 0.211420 0.697619 0.589276 11.00000 -1.20000 H13E 2 0.153131 0.669322 0.534954 11.00000 -1.20000 AFIX 0 C138 1 0.113754 0.739425 0.584802 11.00000 0.07535 0.04433 = 0.07615 0.01027 0.03467 0.00243 AFIX 23 H13F 2 0.103184 0.781828 0.556010 11.00000 -1.20000 H13G 2 0.136476 0.767255 0.619799 11.00000 -1.20000 AFIX 0 C139 1 0.045320 0.699748 0.585978 11.00000 0.07423 0.05285 = 0.08167 0.00478 0.03664 0.00834 AFIX 23 H13H 2 0.021550 0.673162 0.550727 11.00000 -1.20000 H13I 2 0.014520 0.742970 0.592076 11.00000 -1.20000 AFIX 0 C140 1 0.060561 0.634405 0.631952 11.00000 0.05470 0.04372 = 0.05367 -0.00627 0.02686 -0.00293 AFIX 23 H14B 2 0.080345 0.661872 0.667479 11.00000 -1.20000 H14C 2 0.017027 0.607102 0.631199 11.00000 -1.20000 AFIX 0 C141 1 0.263583 0.545216 0.567011 11.00000 0.04806 0.03325 = 0.03356 -0.00265 0.01878 -0.00662 C142 1 0.250057 0.523351 0.511861 11.00000 0.04028 0.04766 = 0.03444 -0.00497 0.01426 -0.00511 C143 1 0.301093 0.534565 0.485902 11.00000 0.04080 0.03394 = 0.03676 0.00041 0.01671 0.00000 C144 1 0.364663 0.571041 0.516572 11.00000 0.04027 0.03256 = 0.04188 0.00146 0.01691 -0.00041 AFIX 43 H144 2 0.398915 0.579422 0.499847 11.00000 -1.20000 AFIX 0 C145 1 0.379147 0.595526 0.571272 11.00000 0.04256 0.03596 = 0.04199 -0.00343 0.01204 -0.00485 C146 1 0.328788 0.580764 0.597199 11.00000 0.05018 0.03044 = 0.03425 -0.00141 0.01177 -0.00507 C147 1 0.343187 0.602831 0.657313 11.00000 0.06216 0.05541 = 0.03841 -0.01213 0.01735 -0.00895 AFIX 23 H14D 2 0.306420 0.640462 0.660075 11.00000 -1.20000 H14E 2 0.340447 0.551818 0.677319 11.00000 -1.20000 AFIX 0 C148 1 0.412290 0.643051 0.684403 11.00000 0.15255 0.17429 = 0.05267 -0.03302 0.03222 -0.11892 AFIX 43 H148 2 0.426891 0.651740 0.722371 11.00000 -1.20000 AFIX 0 C149 1 0.455701 0.668042 0.655304 11.00000 0.05792 0.16800 = 0.09004 -0.08340 0.03558 -0.04719 AFIX 43 H149 2 0.491572 0.706152 0.671712 11.00000 -1.20000 AFIX 0 C150 1 0.448124 0.637709 0.600204 11.00000 0.05013 0.06611 = 0.04999 -0.01642 0.01329 -0.01876 AFIX 23 H15A 2 0.485876 0.598212 0.602659 11.00000 -1.20000 H15B 2 0.453670 0.684887 0.577932 11.00000 -1.20000 AFIX 0 C155 1 -0.047464 -0.061742 0.500970 11.00000 0.03936 0.07978 = 0.04534 -0.01409 0.02164 -0.00855 AFIX 137 H15C 2 -0.080936 -0.087427 0.469293 11.00000 -1.50000 H15D 2 -0.060601 -0.004237 0.503725 11.00000 -1.50000 H15E 2 -0.046881 -0.091674 0.533683 11.00000 -1.50000 AFIX 0 N1 3 0.416489 0.901360 1.133507 11.00000 0.10691 0.22228 = 0.11835 0.05657 0.07126 0.03324 C75 1 0.366595 0.860789 1.114621 11.00000 0.09862 0.16358 = 0.08339 0.03743 0.06234 0.03853 C76 1 0.304751 0.816575 1.092703 11.00000 0.14629 0.10622 = 0.08973 0.01014 0.06607 0.04678 AFIX 137 H76A 2 0.277919 0.840786 1.057863 11.00000 -1.50000 H76B 2 0.277901 0.819185 1.117599 11.00000 -1.50000 H76C 2 0.315320 0.758930 1.087368 11.00000 -1.50000 AFIX 0 N3 3 0.085540 0.376751 0.370351 11.00000 0.13297 0.23059 = 0.13456 -0.05298 0.08421 -0.03815 C153 1 0.136553 0.339650 0.384783 11.00000 0.11577 0.15818 = 0.09154 -0.03198 0.06881 -0.04218 C154 1 0.200700 0.297323 0.401388 11.00000 0.15158 0.12634 = 0.08843 -0.01534 0.06024 -0.05369 AFIX 137 H15F 2 0.226743 0.311468 0.377100 11.00000 -1.50000 H15G 2 0.192397 0.237746 0.400087 11.00000 -1.50000 H15H 2 0.227236 0.313541 0.438437 11.00000 -1.50000 AFIX 0 PART 2 C47A 1 0.324791 1.187677 0.907973 -21.00000 0.07478 0.02824 = 0.05291 -0.00289 0.02949 0.01143 AFIX 23 H47C 2 0.275642 1.196638 0.886677 -21.00000 -1.20000 H47D 2 0.329561 1.193961 0.946704 -21.00000 -1.20000 AFIX 0 C46A 1 0.368478 1.253984 0.892620 -21.00000 0.09140 0.05412 = 0.10302 0.00324 0.03739 -0.00640 AFIX 23 H46C 2 0.335921 1.295799 0.870938 -21.00000 -1.20000 H46D 2 0.395872 1.281413 0.926672 -21.00000 -1.20000 AFIX 0 C45A 1 0.418382 1.233718 0.861936 -21.00000 0.08586 0.04503 = 0.10284 -0.00687 0.05461 0.00179 AFIX 23 H45C 2 0.456969 1.273708 0.872815 -21.00000 -1.20000 H45D 2 0.394004 1.241525 0.822785 -21.00000 -1.20000 AFIX 0 C44A 1 0.449042 1.145119 0.870851 -21.00000 0.08222 0.05956 = 0.07118 0.00643 0.03626 0.00043 AFIX 23 H44C 2 0.465206 1.130819 0.840142 -21.00000 -1.20000 H44D 2 0.489759 1.144811 0.904117 -21.00000 -1.20000 AFIX 0 HKLF 4 REM tx2347c_a.res in P2(1) REM R1 = 0.0636 for 27346 Fo > 4sig(Fo) and 0.0692 for all 30735 data REM 1665 parameters refined using 488 restraints END WGHT 0.1328 1.3195 REM Highest difference peak 0.539, deepest hole -0.308, 1-sigma level 0.054 Q1 1 0.5205 0.3688 1.2997 11.00000 0.05 0.54 Q2 1 0.0117 -0.1832 0.2639 11.00000 0.05 0.51 Q3 1 0.4353 0.6222 0.6866 11.00000 0.05 0.48 Q4 1 0.2309 0.3537 0.7213 11.00000 0.05 0.41 Q5 1 0.1794 0.6377 1.1554 11.00000 0.05 0.39 Q6 1 0.2252 0.8020 0.7825 11.00000 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7.50 0 10 -6 176.30 7.56 0 10 -6 169.63 8.18 0 10 -6 153.45 8.65 0 -10 -6 167.33 7.50 0 -10 7 3.19 1.68 0 -10 -7 4.06 1.67 0 -10 7 4.12 0.54 0 -10 -7 4.59 1.17 0 10 -7 3.68 0.49 0 -10 -7 3.01 0.67 0 10 -7 3.79 0.69 0 10 7 3.63 0.47 0 10 -7 5.99 1.30 0 10 -7 3.80 1.92 0 -10 -7 3.99 0.55 0 -10 -8 32.63 1.62 0 10 -8 32.27 1.69 0 10 -8 34.57 1.58 0 10 -8 34.09 2.36 0 10 -8 32.31 3.13 0 -10 8 30.25 2.68 0 -10 -8 32.00 2.73 0 -10 -8 27.47 2.70 0 -10 -8 29.19 2.19 0 -10 8 31.12 1.61 0 -10 -9 2.07 0.56 0 10 -9 0.67 0.69 0 10 -9 1.66 0.46 0 10 -9 1.17 1.13 0 10 -9 -0.75 1.93 0 -10 -9 1.91 1.65 0 -10 -9 2.43 1.03 0 -10 9 1.11 0.54 0 -10 -9 1.66 1.80 0 -10 9 2.43 1.67 0 -10 -10 31.89 1.59 0 10 -10 31.82 1.53 0 -10 -10 29.57 2.96 0 10 -10 33.46 3.24 0 -10 -10 26.72 2.60 0 -10 10 29.90 2.63 0 -10 -10 26.93 1.99 0 -10 -10 26.17 2.86 0 -10 -11 2.88 0.65 0 10 -11 2.80 0.52 0 -10 -11 2.38 1.96 0 10 -11 2.93 0.45 0 10 -11 2.14 2.12 0 -10 -11 -0.10 1.65 0 -10 11 3.06 1.64 0 -10 -11 1.27 1.90 0 -10 -12 20.93 1.24 0 10 -12 22.50 1.18 0 -10 -12 17.50 2.60 0 10 -12 22.69 1.12 0 10 -12 26.44 3.10 0 -10 -12 20.01 2.55 0 -10 12 20.57 1.23 0 -10 -12 19.22 2.22 0 -10 12 22.15 2.25 0 -10 -13 15.28 1.07 0 10 -13 19.05 1.04 0 -10 -13 12.06 2.42 0 10 -13 17.32 0.94 0 10 -13 18.29 2.86 0 -10 -13 9.61 1.96 0 -10 -13 11.96 2.45 0 10 -13 19.34 2.27 0 -10 13 16.48 1.04 0 -10 13 11.61 1.94 0 -10 -14 60.63 4.15 0 -10 14 78.62 3.40 0 10 -14 70.60 4.52 0 -10 -14 73.43 3.42 0 -10 -14 58.38 4.61 0 10 -14 68.30 3.47 0 -10 -14 61.42 3.35 0 10 -14 75.72 3.34 0 -10 14 69.28 3.36 0 10 -14 72.96 3.33 0 10 -14 63.39 5.01 0 -10 14 70.57 3.38 0 -10 -15 8.28 1.59 0 10 -15 8.06 2.00 0 -10 -15 7.82 0.85 0 10 -15 9.92 0.81 0 -10 -15 5.80 2.15 0 10 -15 7.14 0.99 0 -10 15 7.73 0.71 0 10 -15 8.88 0.69 0 -10 -15 6.15 0.70 0 10 -15 8.54 0.68 0 10 -15 7.99 2.50 0 -10 15 7.03 0.73 0 -10 -16 9.43 1.58 0 10 -16 9.58 1.99 0 -10 -16 8.15 0.77 0 10 -16 14.73 0.82 0 -10 -16 7.89 2.10 0 10 -16 10.38 1.08 0 -10 -16 10.57 0.78 0 -10 16 10.91 0.82 0 -10 16 10.95 0.73 0 10 -16 10.36 0.76 0 10 -16 10.24 2.49 0 -10 16 11.00 0.84 0 10 -17 2.30 1.62 0 -10 -17 0.90 0.53 0 10 -17 0.44 0.54 0 10 -17 1.61 0.85 0 -10 -17 4.30 1.78 0 -10 17 0.85 0.44 0 -10 17 1.19 0.59 0 10 -17 0.72 0.52 0 10 -17 1.74 2.19 0 -10 -17 0.64 0.51 0 -10 17 0.53 0.57 0 -10 18 16.77 0.98 0 -10 -18 13.77 0.90 0 10 -18 16.23 0.93 0 10 -18 16.71 1.21 0 10 -18 16.09 0.92 0 10 -19 7.83 0.67 0 10 -19 7.90 0.67 0 -10 19 8.22 0.72 0 -10 -19 7.49 0.61 0 10 -19 8.96 0.94 0 10 -19 8.60 0.62 0 10 -20 2.19 0.79 0 -10 -20 2.89 0.42 0 10 -20 3.24 0.48 0 -10 20 2.86 0.57 0 10 -20 2.94 0.49 0 -10 -20 1.52 0.70 0 10 -21 2.77 0.51 0 -10 21 2.74 0.56 0 10 -21 2.69 0.49 0 -10 -21 3.03 0.66 0 10 -21 1.06 0.68 0 10 -22 7.16 0.57 0 -10 22 9.15 0.64 0 10 -22 7.27 0.59 0 10 -22 6.88 0.75 0 -10 22 9.30 0.64 0 10 -22 5.92 0.45 0 -10 23 2.33 0.45 0 -10 23 2.29 0.47 0 10 -23 2.42 0.44 0 10 -23 2.92 0.41 0 10 -23 2.34 0.57 0 10 -24 6.02 0.47 0 -10 24 5.69 0.51 0 -10 24 6.45 0.50 0 -10 24 5.84 0.42 0 10 -25 0.91 0.31 0 -10 25 0.47 0.32 0 10 -25 0.43 0.31 0 -10 25 0.38 0.32 0 -11 0 0.93 1.59 0 -11 0 0.30 0.33 0 -11 0 0.78 1.60 0 11 0 1.42 1.36 0 -11 0 0.05 0.33 0 11 0 0.88 0.50 0 -11 0 -0.32 1.62 0 -11 1 2.58 0.42 0 -11 1 1.26 1.59 0 -11 -1 4.11 1.60 0 -11 -1 3.01 1.60 0 11 1 2.36 1.41 0 11 -1 5.84 1.41 0 -11 -1 2.44 0.40 0 -11 1 2.45 1.64 0 11 -1 2.75 0.58 0 11 1 2.16 0.52 0 -11 1 2.64 0.40 0 -11 -1 2.67 1.67 0 -11 2 14.95 0.88 0 -11 2 14.86 1.86 0 -11 -2 15.55 2.07 0 -11 -2 18.00 2.00 0 -11 2 15.65 0.83 0 11 2 17.53 0.94 0 -11 2 18.73 2.11 0 11 -2 16.78 1.01 0 -11 -2 18.13 2.21 0 11 -2 20.31 1.88 0 -11 -2 15.39 0.87 0 11 -3 11.82 0.74 0 -11 3 10.31 1.72 0 -11 -3 12.21 1.79 0 -11 3 9.21 1.93 0 -11 -3 13.15 2.08 0 -11 3 10.47 0.69 0 -11 -3 13.46 2.17 0 11 3 10.51 0.73 0 -11 3 9.35 0.61 0 11 -3 9.91 0.84 0 11 -3 8.44 2.05 0 11 -3 13.76 1.66 0 -11 -3 10.13 0.66 0 11 4 19.86 1.09 0 -11 -4 23.63 2.59 0 11 -4 19.72 1.18 0 -11 -4 20.69 1.06 0 -11 -4 15.76 1.97 0 -11 4 21.09 2.37 0 -11 4 22.10 1.97 0 -11 4 20.28 1.07 0 -11 -4 24.20 2.37 0 11 -4 18.71 1.88 0 11 -4 18.19 2.45 0 11 -4 20.54 1.09 0 -11 -5 4.30 0.52 0 -11 -5 3.17 1.43 0 -11 -5 1.74 1.83 0 -11 5 4.50 0.55 0 -11 5 5.70 1.95 0 -11 5 3.64 1.27 0 11 -5 4.30 0.56 0 -11 -5 4.23 0.64 0 11 5 4.79 0.53 0 11 -5 4.67 0.70 0 -11 -5 6.34 1.94 0 11 -5 4.45 1.92 0 11 -5 4.72 1.37 0 -11 -5 4.40 0.57 0 -11 -6 34.61 2.58 0 -11 6 35.69 1.75 0 -11 -6 31.69 2.89 0 -11 6 35.60 2.93 0 11 -6 36.99 1.73 0 -11 -6 38.55 1.80 0 11 -6 33.59 1.83 0 -11 -6 38.26 3.19 0 11 6 34.46 1.73 0 11 -6 35.52 3.16 0 11 -6 35.94 2.52 0 -11 -6 35.02 1.74 0 -11 -7 1.63 0.53 0 11 -7 1.51 0.69 0 11 -7 1.00 0.51 0 11 -7 1.56 1.24 0 11 -7 0.60 1.91 0 -11 -7 2.24 1.26 0 -11 -7 1.78 1.72 0 -11 7 0.42 1.70 0 -11 7 0.95 0.51 0 -11 -8 26.82 1.42 0 11 -8 27.89 1.54 0 11 -8 28.60 1.40 0 11 -8 23.51 2.90 0 -11 -8 28.55 2.68 0 -11 -8 25.28 2.07 0 -11 8 27.06 1.42 0 -11 8 29.56 2.69 0 -11 -9 6.79 0.71 0 11 -9 6.86 0.88 0 11 -9 7.13 0.63 0 11 -9 5.64 2.25 0 -11 9 7.08 0.68 0 -11 -9 6.29 1.97 0 -11 -9 6.53 1.81 0 -11 9 7.63 1.96 0 -11 -9 5.61 1.23 0 -11 -10 176.42 8.04 0 11 -10 183.21 8.01 0 -11 -10 162.71 9.26 0 11 -10 171.96 8.09 0 11 -10 171.28 9.54 0 -11 10 188.43 8.04 0 -11 -10 155.54 8.92 0 -11 10 170.68 8.98 0 -11 -11 1.42 0.66 0 11 -11 0.60 0.53 0 -11 -11 3.97 2.04 0 11 -11 1.17 0.47 0 11 -11 0.87 2.16 0 -11 -11 1.25 1.64 0 -11 11 0.64 1.56 0 -11 -12 50.33 2.37 0 11 -12 55.04 2.33 0 -11 -12 46.71 3.76 0 11 -12 44.94 2.27 0 -11 12 47.53 2.28 0 11 -12 44.16 3.94 0 -11 12 50.36 3.35 0 -11 -12 43.22 3.34 0 -11 -13 4.02 0.73 0 11 -13 4.64 0.68 0 -11 -13 3.77 2.05 0 -11 13 3.29 0.53 0 11 -13 3.89 0.55 0 -11 -13 3.51 0.63 0 11 -13 1.29 2.22 0 11 -13 2.23 1.75 0 -11 13 3.22 1.56 0 -11 -13 1.79 1.60 0 11 -14 17.15 2.26 0 -11 -14 10.24 1.76 0 -11 -14 14.60 1.00 0 11 -14 17.65 0.96 0 -11 -14 9.56 2.34 0 11 -14 12.09 0.83 0 -11 14 12.88 0.84 0 -11 -14 10.90 0.90 0 11 -14 6.36 2.38 0 -11 14 13.05 0.88 0 -11 -15 24.48 2.55 0 11 -15 39.98 3.08 0 -11 -15 37.29 1.93 0 11 -15 50.38 1.94 0 -11 -15 30.12 3.17 0 11 -15 36.31 2.02 0 -11 -15 34.10 1.84 0 11 -15 38.27 1.84 0 11 -15 39.05 1.82 0 -11 15 33.83 1.81 0 -11 15 36.02 1.83 0 11 -15 31.74 3.60 0 -11 15 38.33 1.87 0 -11 -16 32.60 1.72 0 11 -16 29.44 1.79 0 11 -16 32.80 1.60 0 -11 -16 29.10 1.61 0 -11 16 32.07 1.61 0 -11 16 31.08 1.60 0 -11 16 32.19 1.65 0 11 -17 13.59 0.80 0 11 -17 10.77 1.04 0 -11 17 10.17 0.74 0 -11 17 11.17 0.79 0 -11 -17 9.80 0.79 0 11 -17 12.94 0.78 0 -11 -17 12.03 0.98 0 -11 17 12.81 0.84 0 -11 18 26.63 1.36 0 -11 18 24.46 1.29 0 11 -18 26.83 1.34 0 -11 -18 23.63 1.32 0 11 -18 28.58 1.55 0 11 -18 28.59 1.35 0 -11 18 28.82 1.38 0 11 -19 0.17 0.71 0 -11 -19 0.65 0.41 0 -11 19 -0.53 0.51 0 11 -19 -0.21 0.44 0 11 -19 -0.02 0.46 0 -11 19 0.59 0.49 0 11 -19 0.26 0.47 0 11 -20 3.89 0.50 0 11 -20 3.41 0.47 0 -11 20 3.32 0.53 0 11 -20 3.35 0.71 0 -11 -20 3.28 0.41 0 11 -21 10.37 0.89 0 11 -21 12.11 0.71 0 -11 21 10.64 0.73 0 11 -21 11.32 0.70 0 11 -22 4.24 0.36 0 11 -22 5.56 0.48 0 11 -22 6.24 0.50 0 -11 22 5.53 0.50 0 11 -22 5.01 0.62 0 11 -23 4.50 0.43 0 11 -23 4.77 0.44 0 -11 23 4.65 0.45 0 11 -23 4.51 0.54 0 -11 23 5.02 0.42 0 11 -24 0.71 0.31 0 -11 24 0.46 0.31 0 11 -24 0.56 0.29 0 12 0 158.24 7.53 0 -12 0 155.61 7.63 0 -12 0 140.44 7.48 0 -12 0 142.86 6.54 0 -12 0 148.49 6.55 0 12 0 146.09 6.61 0 -12 0 160.18 7.81 0 -12 -1 19.42 0.98 0 12 1 17.70 2.09 0 12 -1 20.70 2.10 0 -12 1 15.97 2.05 0 -12 -1 18.86 2.28 0 -12 1 16.51 0.98 0 -12 -1 19.86 2.29 0 12 1 19.47 1.09 0 -12 1 19.74 2.43 0 -12 1 18.98 0.97 0 12 -1 17.46 1.12 0 -12 -1 20.73 2.43 0 -12 -2 167.36 7.60 0 -12 -2 170.62 8.81 0 12 2 176.88 7.64 0 12 -2 176.02 7.66 0 -12 2 167.89 7.58 0 12 2 163.95 8.53 0 12 -2 168.81 8.46 0 -12 2 169.31 8.45 0 -12 -2 172.22 8.59 0 -12 2 168.25 7.60 0 -12 -2 165.37 8.55 0 12 -3 -0.02 0.54 0 -12 -3 0.25 0.41 0 -12 -3 1.91 1.85 0 -12 3 0.08 0.33 0 12 3 0.77 0.50 0 12 -3 0.43 0.60 0 12 -3 0.37 1.30 0 -12 -3 0.19 1.54 0 -12 3 0.11 1.66 0 -12 3 0.07 0.44 0 -12 3 1.61 1.49 0 -12 -3 0.20 1.72 0 -12 4 21.53 1.15 0 -12 -4 21.67 2.48 0 -12 4 20.70 2.43 0 -12 -4 22.77 2.26 0 -12 4 23.55 2.07 0 12 -4 22.09 1.18 0 -12 -4 22.28 1.15 0 12 -4 23.02 1.26 0 12 4 21.27 1.17 0 -12 -4 19.21 2.54 0 12 -4 18.70 2.56 0 12 -4 21.28 1.99 0 -12 -4 19.66 1.12 0 -12 5 2.01 1.80 0 -12 5 0.36 0.50 0 -12 5 1.13 1.24 0 -12 -5 0.82 1.40 0 -12 -5 2.22 1.72 0 12 -5 -0.24 0.53 0 -12 -5 -0.22 0.51 0 12 -5 0.68 0.69 0 12 5 -0.08 0.50 0 -12 -5 -0.27 1.95 0 12 -5 -0.44 1.26 0 12 -5 1.33 1.84 0 -12 -5 -0.16 0.44 0 12 -6 120.56 5.19 0 -12 -6 112.98 5.20 0 12 -6 105.19 5.25 0 -12 -6 118.01 6.58 0 12 6 118.35 5.19 0 -12 -6 109.12 5.18 0 12 -6 95.99 6.50 0 -12 -6 103.84 5.93 0 -12 6 121.88 5.19 0 -12 6 126.02 6.40 0 -12 -6 107.31 6.27 0 -12 7 1.53 0.55 0 -12 -7 -0.08 1.18 0 -12 -7 0.11 1.73 0 -12 7 1.26 1.77 0 -12 -7 1.81 0.57 0 12 -7 1.51 0.53 0 -12 -7 3.50 2.09 0 12 -7 2.32 0.71 0 12 -7 3.67 2.04 0 -12 -7 1.24 0.52 0 -12 8 91.84 5.27 0 -12 -8 79.31 4.71 0 -12 8 93.22 4.09 0 -12 -8 90.23 4.09 0 12 -8 94.39 4.07 0 12 -8 90.25 4.16 0 -12 -8 85.67 4.07 0 12 -8 88.68 4.05 0 12 -8 82.51 5.58 0 -12 8 86.78 4.00 0 -12 -9 4.73 0.67 0 12 -9 4.34 0.62 0 12 -9 5.03 0.87 0 12 -9 4.49 0.58 0 12 -9 5.63 2.21 0 -12 -9 2.95 1.83 0 -12 9 4.54 0.66 0 -12 9 2.51 1.84 0 -12 -10 162.66 7.29 0 12 -10 176.45 7.27 0 12 -10 159.52 7.34 0 -12 10 150.14 7.22 0 12 -10 143.36 8.75 0 -12 -10 143.79 8.20 0 -12 10 171.88 7.29 0 -12 10 152.49 8.29 0 -12 -11 4.09 0.69 0 12 -11 4.31 0.61 0 -12 -11 3.25 1.97 0 12 -11 3.15 0.86 0 -12 -11 3.15 0.66 0 12 -11 3.33 0.52 0 -12 11 3.32 0.47 0 12 -11 0.90 2.14 0 -12 -11 3.22 1.74 0 -12 11 3.60 0.69 0 -12 11 2.33 1.66 0 -12 -12 9.03 0.87 0 12 -12 12.03 0.81 0 -12 -12 7.69 2.15 0 12 -12 10.10 0.72 0 -12 12 9.23 0.67 0 12 -12 8.57 2.46 0 -12 -12 6.88 1.73 0 -12 12 8.35 1.84 0 12 -12 11.83 1.95 0 -12 -13 4.90 1.57 0 12 -13 2.14 1.64 0 -12 -13 0.68 0.72 0 12 -13 1.56 0.65 0 -12 -13 1.17 1.86 0 12 -13 1.14 0.51 0 -12 13 0.47 0.44 0 12 -13 1.47 2.14 0 -12 13 0.26 0.55 0 12 -14 10.91 2.05 0 -12 -14 13.33 1.02 0 12 -14 21.21 1.11 0 -12 -14 9.53 2.25 0 12 -14 14.39 0.87 0 -12 -14 12.55 0.92 0 -12 14 14.76 0.86 0 12 -14 6.65 2.39 0 -12 14 14.50 0.93 0 -12 -15 7.15 0.69 0 -12 15 7.30 0.64 0 12 -15 7.55 0.66 0 -12 15 7.66 0.67 0 -12 -15 7.42 0.84 0 -12 15 7.97 0.70 0 12 -16 35.85 1.62 0 12 -16 31.67 1.77 0 12 -16 32.73 1.58 0 -12 -16 30.33 1.58 0 -12 16 32.78 1.58 0 -12 16 30.20 1.58 0 -12 -16 31.35 1.69 0 -12 16 32.50 1.60 0 -12 -17 2.48 0.69 0 12 -17 3.17 0.51 0 12 -17 1.10 0.78 0 -12 17 2.80 0.48 0 -12 17 2.21 0.45 0 12 -17 2.81 0.50 0 -12 -17 1.89 0.51 0 -12 17 2.78 0.55 0 12 -18 10.84 0.69 0 -12 18 9.69 0.64 0 -12 -18 9.73 0.67 0 -12 18 10.11 0.69 0 12 -18 11.43 0.69 0 -12 -18 10.04 0.81 0 -12 18 11.65 0.75 0 12 -18 9.76 0.93 0 12 -19 1.85 0.72 0 -12 -19 3.22 0.63 0 12 -19 3.57 0.48 0 -12 19 2.07 0.45 0 12 -19 3.17 0.45 0 12 -19 3.85 0.48 0 -12 -19 2.65 0.41 0 -12 19 2.87 0.51 0 -12 20 4.40 0.48 0 12 -20 3.65 0.46 0 -12 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0.69 0 -13 -3 5.03 0.61 0 13 -3 5.56 0.74 0 -13 -3 8.51 2.09 0 -13 3 5.64 0.45 0 13 3 5.21 0.65 0 13 3 5.16 1.70 0 -13 -3 5.91 0.51 0 -13 4 22.21 2.56 0 -13 -4 22.56 2.31 0 -13 4 19.53 2.03 0 -13 4 22.33 1.23 0 -13 -4 21.94 2.54 0 13 -4 23.36 1.28 0 -13 -4 25.07 1.25 0 13 4 23.23 1.27 0 13 -4 24.14 1.36 0 -13 -4 23.02 2.72 0 13 4 23.80 2.33 0 -13 -4 23.90 1.20 0 13 -5 16.64 0.98 0 -13 -5 16.26 0.96 0 13 -5 14.93 1.11 0 13 5 15.17 0.97 0 -13 -5 17.83 2.58 0 -13 -5 15.87 0.91 0 -13 -5 15.23 1.89 0 -13 5 15.97 2.34 0 -13 5 14.67 0.95 0 -13 -5 12.55 2.29 0 -13 6 130.46 5.83 0 -13 -6 115.13 6.61 0 -13 -6 116.34 6.87 0 -13 6 122.97 6.98 0 -13 -6 127.28 5.84 0 13 -6 135.26 5.84 0 -13 -6 135.12 7.27 0 13 -6 135.03 5.91 0 13 -6 117.81 7.22 0 -13 -6 125.62 5.81 0 -13 -7 3.95 1.29 0 -13 7 8.45 1.97 0 -13 7 4.06 0.63 0 -13 -7 6.07 1.99 0 -13 -7 4.40 0.63 0 13 -7 4.21 0.64 0 -13 -7 1.59 1.96 0 13 -7 5.29 0.84 0 13 -7 4.40 0.57 0 13 -7 3.76 2.04 0 -13 -7 4.40 0.58 0 -13 8 277.84 13.59 0 -13 -8 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767.95 32.97 -4 5 -2 711.28 32.45 4 5 2 761.84 32.61 4 -5 2 781.64 32.61 4 -5 2 813.49 32.61 4 -5 2 836.00 32.80 -4 -5 -3 21.09 1.70 -4 5 -3 20.14 1.12 4 5 3 20.94 1.95 4 5 3 19.80 1.39 4 -5 3 23.56 1.43 4 -5 3 20.92 1.68 -4 -5 -4 132.11 6.42 4 5 4 141.55 6.66 -4 5 -4 129.35 6.03 4 -5 4 142.23 6.38 4 5 5 25.47 2.16 -4 5 -5 22.23 1.26 -4 -5 -5 21.66 1.78 4 -5 5 21.56 1.73 4 5 6 606.38 26.90 -4 5 -6 561.07 26.36 -4 -5 -6 610.83 26.76 4 -5 6 647.47 26.62 4 5 7 69.35 3.75 -4 -5 -7 67.67 3.56 -4 5 -7 69.06 3.45 4 -5 7 68.33 3.33 4 5 8 237.98 12.13 -4 -5 -8 243.05 12.06 -4 5 -8 266.63 12.03 4 -5 8 274.77 11.85 4 -5 9 5.03 0.42 4 5 9 3.77 1.46 -4 -5 -9 5.21 1.42 -4 5 -9 5.40 1.32 4 -5 9 4.04 0.85 4 -5 9 3.97 0.42 -4 5 -9 4.69 0.36 4 -5 10 62.05 2.84 -4 5 -10 61.13 2.81 4 -5 10 61.88 2.82 4 -5 10 65.27 2.85 -4 5 -10 61.75 2.81 4 5 10 55.97 3.69 -4 -5 -10 62.69 3.67 -4 5 -10 62.87 3.55 4 -5 10 63.07 3.19 -4 5 -11 4.22 1.33 4 5 11 1.70 0.39 -4 5 -11 3.41 0.40 -4 -5 -11 2.86 0.50 4 -5 11 3.31 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114.63 5.57 4 -9 -12 124.97 5.64 4 9 -12 128.81 5.61 4 -9 -12 116.47 6.63 4 9 -12 121.69 5.50 4 9 -12 126.71 5.51 4 9 -12 126.54 6.57 4 -9 -12 123.69 5.56 4 -9 -11 3.70 1.55 4 -9 -11 3.31 0.79 4 9 -11 4.58 0.50 4 9 -11 3.33 0.59 4 -9 -11 5.51 1.74 4 9 -11 3.25 0.67 4 9 -11 4.25 0.44 4 9 -11 3.81 0.40 4 9 -11 5.06 1.65 4 -9 -11 2.99 0.52 4 9 -11 3.26 2.23 4 -9 -11 3.60 0.55 4 -9 -10 34.24 2.53 4 -9 -10 32.84 1.69 4 9 -10 34.01 1.54 4 -9 -10 31.96 2.78 4 9 -10 34.94 1.65 4 9 -10 27.89 1.58 4 9 -10 30.56 1.50 4 -9 -10 29.62 1.54 4 9 -10 32.16 1.48 4 9 -10 33.91 2.64 4 9 -10 29.00 3.21 4 -9 -10 32.08 1.55 4 -9 -9 9.95 0.91 4 9 -9 10.16 0.66 4 -9 -9 11.09 1.99 4 9 -9 10.55 0.81 4 9 -9 9.96 0.72 4 -9 -9 9.70 0.68 4 9 -9 10.44 0.62 4 9 -9 13.79 1.91 4 9 -9 9.13 2.34 4 -9 -9 11.18 0.68 4 -9 -8 33.69 1.67 4 -9 -8 28.51 1.63 4 9 -8 32.26 1.50 4 -9 -8 29.86 2.60 4 9 -8 32.16 1.59 4 9 -8 30.02 1.46 4 -9 -8 31.69 1.50 4 9 -8 30.45 3.07 4 9 -8 32.46 2.59 4 -9 -8 27.58 2.21 4 -9 -7 14.81 1.09 4 -9 -7 16.26 1.07 4 9 -7 17.49 0.90 4 9 -7 17.56 1.02 4 -9 -7 17.94 2.13 4 -9 -7 16.79 0.90 4 9 -7 20.02 2.07 4 9 -7 19.04 2.60 4 -9 -7 18.77 1.94 4 -9 -7 16.25 1.75 4 9 -6 40.19 1.95 4 -9 -6 40.19 3.00 -4 -9 6 44.90 2.66 4 9 -6 42.12 2.02 4 -9 -6 42.75 1.95 4 9 -6 45.65 3.44 4 9 -6 47.07 2.98 4 -9 -6 43.40 2.70 4 -9 -6 41.18 2.81 4 9 -5 26.99 1.31 4 -9 -5 26.80 1.34 -4 -9 5 25.64 2.07 4 9 -5 24.75 1.38 4 -9 -5 28.76 2.44 4 -9 -5 27.40 1.30 4 9 -5 31.71 2.44 4 9 -5 28.55 2.81 4 -9 -5 28.50 2.24 4 -9 -5 28.29 2.17 4 9 -4 20.21 1.12 -4 -9 4 24.64 1.99 4 -9 -4 25.32 2.25 4 -9 -4 22.01 1.15 4 9 -4 22.94 1.20 4 -9 -4 25.02 1.12 4 9 -4 26.78 2.25 4 9 -4 24.92 2.59 4 -9 -4 23.41 2.00 4 -9 -4 24.31 1.99 4 -9 -3 5.61 0.49 4 9 -3 4.54 0.44 -4 -9 3 5.45 1.42 4 -9 -3 4.82 0.42 4 9 -3 5.04 1.56 4 -9 -3 4.30 1.40 4 -9 -3 6.51 1.51 4 -9 -2 72.71 3.17 -4 -9 2 73.26 4.02 4 -9 -2 69.54 3.16 4 9 -2 66.16 3.15 4 9 -2 79.00 4.12 4 -9 -2 73.21 3.91 -4 -9 2 69.49 3.65 4 -9 -1 30.78 1.46 -4 9 1 29.49 1.91 4 9 -1 29.88 2.55 4 -9 -1 28.93 2.22 4 -9 -1 32.49 2.36 -4 -9 1 30.80 2.43 4 -9 -1 29.17 1.44 4 -9 0 56.73 2.67 4 9 0 57.65 2.70 4 -9 0 59.44 2.66 -4 -9 0 68.82 3.70 4 -9 0 61.61 3.52 4 -9 0 59.94 3.29 -4 9 0 55.93 3.40 -4 9 0 57.58 3.08 -4 -9 -1 4.66 1.56 4 9 1 4.73 0.51 4 -9 1 5.77 0.44 4 -9 1 3.61 1.54 4 -9 1 6.60 1.22 -4 9 -1 2.37 1.27 4 9 2 96.96 3.99 -4 -9 -2 90.99 4.96 4 -9 2 82.08 3.95 -4 9 -2 78.10 4.70 4 -9 2 87.07 3.95 4 -9 2 92.65 4.48 4 -9 2 97.11 4.81 4 9 3 4.05 0.50 4 -9 3 5.11 0.40 -4 9 -3 3.89 0.57 -4 -9 -3 5.02 1.69 -4 9 -3 4.73 0.46 -4 9 -3 4.52 1.47 4 -9 3 4.08 0.44 4 -9 3 4.96 1.02 4 -9 3 4.03 1.53 4 -9 4 4.61 0.36 4 -9 4 3.80 0.37 4 9 4 4.10 0.49 -4 -9 -4 6.64 1.74 -4 9 -4 3.50 0.58 -4 9 -4 4.04 0.45 -4 9 -4 7.14 1.63 4 -9 4 4.48 0.45 4 -9 4 3.74 0.91 4 -9 4 5.29 1.44 4 -9 5 44.17 2.22 4 -9 5 50.84 2.22 -4 9 -5 49.16 2.25 4 -9 5 49.37 2.22 -4 9 -5 50.09 2.33 -4 9 -5 44.07 3.32 -4 -9 -5 40.11 2.86 4 -9 5 52.98 3.22 4 -9 6 219.35 9.58 4 -9 6 207.65 9.58 -4 9 -6 218.80 9.60 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1.69 4 10 -8 6.46 2.32 4 -10 -8 7.12 0.59 4 -10 -7 11.82 1.72 4 -10 -7 14.20 1.94 4 -10 -7 13.45 1.04 4 -10 -7 11.73 0.99 4 10 -7 14.21 0.79 4 -10 -7 12.14 2.12 4 10 -7 13.26 0.94 4 -10 -7 11.69 0.84 4 -10 -7 13.16 0.79 4 10 -7 15.32 1.99 4 10 -7 13.18 2.52 4 -10 -7 13.85 0.76 4 -10 -6 138.03 6.13 4 -10 -6 122.49 6.11 4 10 -6 135.79 6.04 4 -10 -6 131.48 7.11 4 -10 -6 130.05 6.07 4 10 -6 138.35 6.11 4 -10 -6 142.52 6.04 4 10 -6 140.76 7.05 4 10 -6 136.45 7.49 4 -10 -6 129.42 6.83 4 -10 -6 125.94 6.77 4 -10 -5 21.40 1.35 4 10 -5 25.11 1.21 4 -10 -5 25.44 2.53 4 -10 -5 22.68 1.23 4 10 -5 24.78 1.30 -4 -10 5 24.32 2.10 4 -10 -5 23.82 1.19 4 10 -5 23.05 2.78 4 10 -5 24.54 2.35 4 -10 -5 23.43 2.23 4 -10 -5 24.60 2.14 4 -10 -4 169.42 8.32 4 -10 -4 171.94 8.32 4 -10 -4 163.68 7.59 4 10 -4 163.86 7.54 4 -10 -4 175.49 8.57 -4 -10 4 165.54 8.31 4 -10 -4 170.94 7.53 4 10 -4 172.41 8.49 4 -10 -4 175.75 7.56 4 -10 -3 3.13 1.34 4 -10 -3 0.41 1.39 4 -10 -3 1.15 0.65 4 10 -3 1.33 0.42 -4 -10 3 0.27 1.30 4 -10 -3 1.18 0.35 4 10 -3 1.55 1.51 4 -10 -3 1.25 0.43 4 -10 -2 32.33 2.38 4 -10 -2 31.21 1.68 4 10 -2 32.87 1.55 4 -10 -2 30.58 1.51 -4 10 2 32.31 2.12 4 10 -2 35.65 2.70 -4 10 2 32.35 1.57 4 -10 -2 32.63 1.55 -4 -10 2 35.62 2.62 4 -10 -2 33.31 1.56 4 -10 -1 2.60 1.25 -4 -10 1 2.72 1.17 4 -10 -1 1.89 0.40 -4 -10 1 2.23 1.41 4 10 -1 1.83 0.50 -4 10 1 1.47 0.47 4 -10 -1 1.71 0.65 4 -10 -1 2.02 0.34 4 10 -1 4.71 1.60 4 -10 -1 2.22 0.43 4 -10 0 92.18 4.81 4 -10 0 96.96 5.05 -4 -10 0 91.73 4.78 -4 10 0 84.32 4.14 4 10 0 98.59 4.16 4 -10 0 91.38 4.11 -4 -10 0 91.01 5.12 4 -10 0 88.19 4.18 -4 10 0 89.48 4.91 4 10 0 90.75 5.15 4 -10 0 92.42 4.13 4 -10 1 4.92 0.65 4 -10 1 4.64 0.45 4 10 1 4.97 0.57 -4 -10 -1 4.27 1.74 -4 10 -1 4.09 0.58 -4 10 -1 5.10 1.46 4 -10 1 5.86 1.25 4 -10 1 3.82 1.61 -4 -10 -1 4.44 1.44 -4 10 -2 74.69 3.43 4 -10 2 74.03 3.50 4 -10 2 73.90 3.42 4 10 2 80.90 3.47 -4 10 -2 73.18 3.48 -4 -10 -2 74.04 4.58 -4 10 -2 75.45 4.40 4 -10 2 84.55 4.42 4 -10 2 79.31 4.04 -4 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7.74 0.63 4 -12 -2 208.94 10.15 4 -12 -2 189.83 9.36 4 12 -2 207.35 9.32 -4 -12 2 214.89 10.39 4 12 -2 211.58 9.37 -4 12 2 199.32 9.34 4 -12 -2 216.82 9.33 4 -12 -2 207.52 9.29 4 12 -2 205.77 10.46 4 -12 -2 229.11 9.34 -4 12 1 13.35 0.89 4 12 -1 14.23 0.97 -4 -12 1 12.87 2.06 4 -12 -1 13.99 0.83 4 12 -1 13.71 0.87 4 12 -1 15.72 2.10 4 -12 -1 14.76 1.84 -4 -12 0 32.80 2.89 4 -12 0 33.04 1.64 4 12 0 37.60 1.73 -4 12 0 33.90 1.70 4 12 0 31.64 1.66 4 12 0 35.56 2.89 4 -12 0 35.41 2.46 -4 -12 0 30.09 2.77 4 -12 0 36.72 2.85 -4 -12 -1 24.79 2.67 4 12 1 28.32 1.43 -4 12 -1 24.57 1.42 4 -12 1 27.62 1.33 -4 12 -1 26.07 1.39 4 12 1 23.27 2.68 4 -12 1 25.13 2.15 -4 -12 -1 23.87 2.48 4 -12 1 23.00 2.48 4 12 2 86.31 3.87 4 -12 2 84.38 3.80 -4 -12 -2 81.75 5.12 -4 12 -2 79.83 3.87 -4 12 -2 84.12 3.84 4 12 2 79.36 5.09 4 -12 2 85.60 4.52 -4 -12 -2 82.67 4.79 4 -12 2 94.06 5.01 -4 -12 -3 8.60 2.15 4 12 3 9.39 0.78 4 -12 3 8.88 0.61 -4 12 -3 7.65 0.81 -4 12 -3 9.15 0.73 4 12 3 8.97 2.17 -4 -12 -3 6.67 1.64 4 -12 3 5.62 1.83 -4 -12 -3 9.24 1.81 -4 12 -4 33.22 1.75 4 -12 4 33.98 1.61 -4 -12 -4 33.70 3.08 -4 12 -4 34.21 1.68 4 -12 4 35.00 2.90 -4 -12 -4 32.58 2.58 -4 -12 -4 29.95 2.72 4 -12 5 1.73 0.40 -4 12 -5 1.83 0.52 -4 -12 -5 0.14 1.90 -4 12 -5 1.60 0.72 4 -12 5 2.05 0.39 -4 12 -5 -0.13 1.45 -4 -12 -5 1.11 1.31 4 -12 5 -0.54 1.76 -4 -12 -6 29.94 2.39 4 -12 6 34.45 2.79 -4 -12 -6 33.72 2.95 -4 -12 -6 34.59 1.78 -4 12 -6 34.26 1.71 4 -12 6 36.53 1.63 -4 12 -6 33.53 1.80 -4 -12 -6 35.72 3.22 4 -12 6 35.18 1.73 -4 12 -6 27.40 2.77 4 -12 6 36.07 1.64 4 -12 6 32.15 1.63 -4 -12 -7 13.49 2.34 4 -12 7 12.40 2.08 -4 -12 -7 10.10 2.20 -4 -12 -7 15.57 1.04 -4 12 -7 15.19 0.91 -4 12 -7 14.82 1.07 -4 -12 -7 16.73 2.47 -4 12 -7 15.05 0.92 4 -12 7 14.89 0.98 -4 12 -7 14.97 2.24 4 -12 7 15.32 0.80 4 -12 7 12.86 0.81 -4 -12 -8 106.76 6.94 4 -12 8 132.44 6.92 -4 -12 -8 106.60 6.96 -4 -12 -8 135.40 5.96 -4 12 -8 139.22 5.91 -4 12 -8 123.56 5.99 -4 -12 -8 120.57 7.32 4 -12 8 137.76 5.93 -4 12 -8 134.88 5.90 -4 12 -8 109.07 7.13 4 -12 8 124.35 5.87 4 -12 8 131.62 5.86 4 -12 9 2.23 0.46 4 -12 9 2.20 0.37 -4 12 -9 1.98 0.55 -4 -12 -9 1.50 1.94 -4 12 -9 1.91 0.81 -4 12 -9 2.40 0.55 4 -12 9 1.86 0.66 -4 12 -9 0.46 1.81 -4 -12 -9 1.62 1.83 -4 12 -9 3.90 1.69 4 -12 9 2.75 1.51 -4 -12 -9 -0.24 1.94 4 -12 10 45.64 2.18 4 -12 10 45.26 2.13 -4 12 -10 49.63 2.22 -4 12 -10 42.88 2.36 -4 -12 -10 44.59 3.74 -4 12 -10 48.87 2.20 4 -12 10 46.22 2.25 -4 12 -10 48.56 2.20 -4 12 -10 34.62 3.49 -4 12 -10 44.74 3.30 -4 -12 -10 38.64 3.31 4 -12 10 44.23 3.13 -4 -12 -10 39.61 3.52 4 -12 11 49.96 2.45 4 -12 11 51.67 2.50 -4 12 -11 65.47 2.58 -4 12 -11 46.30 2.69 -4 -12 -11 39.95 3.90 -4 12 -11 58.59 2.54 4 -12 11 54.84 2.58 -4 12 -11 60.92 2.54 -4 12 -11 28.75 3.68 -4 12 -11 51.75 3.69 -4 -12 -11 40.45 3.55 -4 -12 -11 41.48 3.75 -4 12 -12 219.23 9.98 4 -12 12 212.73 10.00 -4 12 -12 224.57 9.98 -4 12 -12 201.42 10.07 4 -12 12 218.66 9.98 -4 12 -13 0.84 0.51 -4 12 -13 0.05 0.85 4 -12 13 0.63 0.52 -4 12 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7.52 0.63 4 -13 -5 7.61 0.58 4 13 -5 7.86 1.91 4 -13 -5 9.03 0.70 4 -13 -4 130.63 6.79 -4 -13 4 122.36 7.01 4 -13 -4 136.93 6.93 4 -13 -4 125.63 5.92 4 13 -4 132.06 5.88 -4 13 4 124.29 5.86 4 -13 -4 131.12 5.88 4 13 -4 133.38 5.94 4 -13 -4 122.70 5.84 4 -13 -4 140.50 5.85 4 13 -4 125.53 7.03 4 -13 -4 133.89 5.89 4 -13 -3 18.61 2.14 4 -13 -3 20.49 2.27 -4 -13 3 15.11 2.40 4 -13 -3 17.44 1.21 4 13 -3 18.78 1.08 -4 13 3 17.97 1.06 -4 -13 3 17.60 2.15 4 13 -3 20.39 1.20 4 -13 -3 18.56 1.07 4 -13 -3 19.42 1.00 4 -13 -3 17.75 1.04 4 13 -3 20.57 2.42 4 -13 -3 22.39 1.10 4 -13 -2 30.55 1.69 4 13 -2 32.65 1.60 4 13 -2 31.94 1.67 -4 13 2 31.28 1.59 -4 -13 2 31.40 2.77 4 -13 -2 33.54 1.58 4 -13 -2 31.78 1.53 4 13 -2 31.30 2.88 4 -13 -2 33.54 2.53 -4 -13 2 32.35 2.86 4 -13 -2 28.75 2.70 4 -13 -1 3.47 0.72 4 13 -1 4.07 0.58 -4 13 1 2.90 0.64 4 13 -1 6.03 1.95 4 -13 -1 3.31 1.39 -4 -13 1 1.59 1.76 4 -13 -1 3.10 0.53 4 13 -1 4.71 0.69 -4 13 1 3.02 0.59 -4 -13 1 1.47 1.58 4 13 0 6.99 0.69 -4 13 0 6.64 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48.65 2.56 7 7 -16 2.70 0.58 7 7 -16 2.42 1.48 7 -7 -16 2.42 0.63 7 -7 -16 2.98 0.86 7 7 -16 3.60 0.50 7 -7 -16 2.60 0.51 7 -7 -16 1.25 1.14 7 7 -16 2.80 0.55 7 7 -16 2.80 0.39 7 7 -16 3.16 0.31 7 -7 -16 3.35 0.65 7 7 -16 2.78 2.11 7 7 -16 3.12 1.92 7 -7 -16 3.33 0.60 7 7 -15 114.82 4.91 7 7 -15 113.86 5.76 7 -7 -15 102.28 4.94 7 -7 -15 109.11 4.99 7 7 -15 120.09 4.88 7 -7 -15 98.49 5.57 7 7 -15 109.28 4.91 7 -7 -15 111.88 4.87 7 7 -15 104.69 4.84 7 7 -15 105.44 4.83 7 7 -15 116.51 6.09 7 -7 -15 100.96 4.92 7 7 -15 124.01 6.62 7 -7 -15 104.96 4.91 7 7 -14 11.11 0.83 7 7 -14 12.10 1.69 7 -7 -14 11.10 0.86 7 -7 -14 10.85 1.03 7 7 -14 17.79 0.84 7 -7 -14 10.09 1.52 7 7 -14 10.02 0.80 7 -7 -14 14.81 0.77 7 7 -14 12.01 0.67 7 7 -14 12.08 0.65 7 -7 -14 11.65 0.77 7 -7 -14 12.07 0.85 7 7 -14 10.61 1.69 7 7 -14 15.32 2.15 7 7 -14 12.20 2.47 7 -7 -14 12.59 0.82 7 7 -13 89.63 3.95 7 -7 -13 82.50 3.97 7 -7 -13 80.80 4.03 7 -7 -13 85.27 4.68 7 7 -13 86.16 3.96 7 7 -13 84.50 3.88 7 7 -13 83.94 3.88 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27.26 2.37 7 7 -8 23.79 1.25 7 -7 -8 28.33 1.22 7 -7 -7 429.25 17.92 7 -7 -7 391.75 17.95 7 7 -7 430.16 19.08 7 7 -7 413.33 18.73 7 7 -7 427.70 18.36 7 -7 -7 418.21 18.61 -7 -7 7 391.97 18.24 7 -7 -7 380.21 17.95 7 -7 -6 0.59 0.39 7 -7 -6 0.96 0.47 7 7 -6 -0.24 1.45 7 -7 -6 0.12 0.29 7 7 -6 -0.44 0.83 7 -7 -6 0.55 0.39 7 7 -6 1.89 1.65 7 7 -6 -0.50 0.43 -7 -7 6 0.36 0.73 7 -7 -6 -0.86 1.18 7 -7 -5 393.60 16.64 7 -7 -5 365.71 17.00 7 7 -5 367.66 17.03 -7 -7 5 384.45 17.08 7 -7 -5 355.68 16.64 7 7 -5 409.79 17.01 7 7 -4 36.35 2.33 7 -7 -4 38.62 2.29 -7 -7 4 43.68 2.51 7 7 -4 40.95 2.23 7 7 -3 545.25 25.39 7 -7 -3 534.60 25.36 -7 -7 3 584.53 25.58 7 7 -3 598.99 25.30 7 -7 -2 57.81 3.08 7 -7 -2 40.83 2.60 7 7 -2 45.97 2.69 7 7 -2 51.71 2.50 -7 -7 2 50.36 2.98 7 -7 -1 80.64 3.75 7 -7 -1 88.29 4.48 7 -7 -1 76.10 4.10 7 7 -1 77.42 4.15 7 -7 -1 87.81 3.75 7 -7 0 15.39 0.85 7 -7 0 12.51 1.29 7 7 0 14.33 1.36 7 -7 0 16.68 1.77 7 -7 0 17.13 0.87 -7 7 0 15.16 1.36 7 -7 0 18.29 0.84 7 -7 1 375.10 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31.50 1.61 8 -5 -14 30.85 1.61 8 5 -13 7.94 1.25 8 -5 -13 7.01 0.69 8 -5 -13 8.12 0.90 8 -5 -13 8.24 0.81 8 -5 -13 7.67 0.83 8 -5 -13 8.18 0.65 8 5 -13 9.47 0.54 8 -5 -13 8.65 0.53 8 -5 -13 6.31 1.05 8 5 -13 8.40 0.47 8 5 -13 8.25 0.48 8 -5 -13 7.94 0.65 8 5 -13 10.57 1.86 8 5 -13 7.35 1.86 8 5 -13 7.51 0.65 8 5 -12 47.68 2.89 8 -5 -12 47.44 2.49 8 -5 -12 55.05 2.47 8 -5 -12 46.94 2.45 8 -5 -12 52.74 2.38 8 5 -12 56.42 2.36 8 -5 -12 51.28 2.40 8 -5 -12 50.71 2.35 8 -5 -12 50.23 2.81 8 5 -12 50.49 2.32 8 -5 -12 48.09 2.38 8 5 -12 52.35 3.00 8 5 -12 59.69 3.58 8 5 -12 50.77 2.40 8 5 -12 52.88 2.38 8 -5 -12 51.65 2.38 8 -5 -11 29.12 1.50 8 -5 -11 31.75 1.53 8 -5 -11 29.09 1.47 8 -5 -11 32.33 2.01 8 5 -11 31.29 1.44 8 5 -11 36.12 2.17 8 -5 -11 34.28 1.53 8 5 -11 35.53 2.78 8 5 -11 31.86 1.54 8 -5 -10 286.89 12.23 8 -5 -10 265.22 12.21 8 -5 -10 275.57 12.23 8 -5 -10 268.67 12.64 8 5 -10 267.43 12.19 8 5 -10 295.29 12.72 8 -5 -10 289.25 12.24 8 5 -10 302.85 13.28 8 5 -10 277.50 12.24 8 5 -9 15.77 0.78 8 5 -9 20.14 1.54 8 5 -9 21.94 2.15 8 -5 -9 15.08 0.85 8 -5 -9 18.00 1.42 8 5 -8 1115.35 51.17 8 -5 -8 1104.60 51.12 8 5 -8 1159.83 50.97 8 5 -8 1229.35 51.52 8 5 -7 19.86 1.93 8 -5 -7 20.02 1.85 8 5 -7 23.84 1.59 8 5 -7 22.92 2.21 8 5 -7 21.23 2.06 8 5 -6 84.16 4.50 8 -5 -6 83.93 4.45 8 5 -6 87.57 4.18 8 5 -6 82.13 4.55 8 -5 -5 3.16 1.19 8 5 -5 4.42 1.29 -8 -5 5 4.02 0.81 8 5 -5 5.42 0.83 8 5 -5 5.69 1.36 8 -5 -4 205.19 9.44 8 5 -4 195.21 9.44 -8 -5 4 195.21 9.24 8 5 -4 206.83 9.20 8 5 -4 198.84 9.55 8 -5 -3 18.02 1.07 8 5 -3 22.89 1.95 8 -5 -3 18.74 1.67 8 5 -3 19.96 1.74 8 5 -2 328.23 15.60 8 -5 -2 334.46 15.48 8 5 -2 353.13 15.55 8 5 -1 21.98 2.00 8 -5 -1 20.55 1.73 8 5 -1 22.27 1.86 -8 5 0 273.47 12.68 8 -5 0 286.91 12.99 8 5 0 294.47 13.02 8 5 1 22.51 2.58 -8 5 -1 24.27 1.51 8 -5 1 25.85 1.86 8 5 1 24.74 1.94 8 -5 2 568.51 25.37 8 -5 2 571.23 25.35 8 5 2 576.15 26.30 -8 5 -2 596.42 25.65 8 -5 2 594.01 25.91 8 5 2 595.12 25.92 8 -5 3 37.26 1.75 8 -5 3 38.09 1.72 -8 -5 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2.63 8 6 -16 53.78 2.63 8 6 -15 0.39 1.22 8 -6 -15 0.22 0.92 8 -6 -15 0.87 0.77 8 -6 -15 1.06 0.61 8 6 -15 0.72 0.38 8 6 -15 1.04 0.49 8 -6 -15 0.78 0.49 8 6 -15 0.82 0.30 8 6 -15 1.00 0.33 8 6 -15 0.89 0.26 8 -6 -15 0.44 0.49 8 -6 -15 0.28 0.56 8 6 -15 0.29 1.87 8 6 -15 0.22 1.72 8 6 -15 0.24 0.57 8 6 -14 101.17 4.39 8 6 -14 90.68 5.02 8 -6 -14 94.25 4.44 8 -6 -14 96.42 4.50 8 -6 -14 90.17 4.40 8 6 -14 107.56 4.34 8 -6 -14 93.33 4.90 8 6 -14 94.93 4.30 8 6 -14 104.60 5.48 8 -6 -14 97.34 4.36 8 -6 -14 97.77 4.39 8 6 -14 101.41 5.77 8 6 -14 92.18 4.37 8 -6 -14 88.69 4.36 8 6 -13 0.20 0.51 8 6 -13 1.06 1.12 8 -6 -13 0.83 0.83 8 -6 -13 0.33 0.53 8 -6 -13 1.12 0.74 8 -6 -13 0.46 0.37 8 6 -13 1.20 0.37 8 -6 -13 1.29 0.93 8 6 -13 0.93 0.26 8 -6 -13 0.28 0.46 8 6 -13 0.61 1.15 8 6 -13 0.20 1.60 8 6 -13 0.13 1.69 8 -6 -13 0.67 0.40 8 6 -13 0.26 0.44 8 -6 -12 115.78 4.92 8 -6 -12 100.62 4.91 8 -6 -12 108.29 4.89 8 -6 -12 106.25 4.87 8 -6 -12 100.03 4.82 8 -6 -12 102.99 5.38 8 6 -12 102.20 4.80 8 -6 -12 102.87 4.85 8 6 -12 114.27 5.87 8 6 -12 116.71 5.49 8 6 -12 110.21 6.11 8 6 -12 103.46 4.87 8 -6 -11 9.70 0.84 8 -6 -11 9.09 0.74 8 6 -11 15.32 0.70 8 -6 -11 9.79 0.65 8 -6 -11 10.10 0.75 8 -6 -11 8.41 1.27 8 6 -11 11.43 0.84 8 6 -11 11.13 0.59 8 6 -11 9.96 1.85 8 -6 -11 11.49 0.74 8 6 -11 12.46 1.46 8 6 -11 11.83 2.21 8 6 -11 10.90 0.74 8 6 -10 10.82 0.58 8 -6 -10 9.31 0.64 8 -6 -10 8.91 0.64 8 -6 -10 8.71 0.57 8 -6 -10 9.62 1.26 8 6 -10 8.86 0.73 8 6 -10 8.59 0.51 8 -6 -10 9.68 0.65 8 6 -10 8.88 1.27 8 6 -10 9.05 1.85 8 6 -10 9.58 0.65 8 -6 -9 9.53 0.65 8 -6 -9 9.09 0.59 8 -6 -9 8.82 0.64 8 -6 -9 11.19 1.31 8 6 -9 9.78 0.53 8 6 -9 12.54 1.34 8 -6 -9 9.02 0.65 8 6 -9 9.34 1.97 8 6 -9 11.03 0.68 8 -6 -8 181.19 8.48 8 -6 -8 178.88 7.92 8 -6 -8 179.96 7.93 8 6 -8 197.90 8.38 8 6 -8 190.47 9.04 8 6 -8 172.47 7.92 8 -6 -8 175.00 7.90 8 -6 -7 2.86 0.40 8 -6 -7 2.59 0.37 8 6 -7 2.51 0.47 8 6 -7 1.37 1.22 8 -6 -7 2.44 1.15 8 6 -7 3.02 0.97 8 -6 -7 2.23 0.41 8 6 -7 2.39 1.57 8 -6 -6 697.25 30.52 8 -6 -6 670.36 30.52 8 6 -6 731.46 30.89 8 6 -6 710.55 31.07 8 -6 -6 689.10 31.03 8 6 -6 700.94 30.55 8 6 -5 2.94 0.81 8 6 -5 1.72 1.34 -8 -6 5 1.43 0.77 8 6 -5 1.76 1.13 8 -6 -5 1.84 1.07 8 6 -4 106.26 5.04 8 6 -4 104.03 5.50 -8 -6 4 109.04 5.19 8 6 -4 103.70 5.29 8 -6 -4 104.08 5.26 8 6 -3 17.84 1.80 -8 -6 3 16.41 1.50 8 -6 -3 16.05 1.56 8 6 -3 16.56 1.60 8 -6 -2 2.83 1.04 8 6 -2 1.24 1.01 8 6 -2 2.51 1.34 8 -6 -1 0.80 0.25 8 -6 -1 0.49 0.93 8 6 -1 2.74 1.08 8 6 -1 0.67 1.19 8 -6 0 112.70 5.11 8 6 0 123.00 5.92 8 -6 0 117.60 5.64 8 6 0 115.22 5.65 8 -6 1 43.91 2.10 8 -6 1 49.75 2.10 8 6 1 42.46 2.17 8 6 1 49.24 3.42 8 -6 1 42.18 2.70 8 6 1 43.26 2.73 8 -6 2 176.91 7.54 8 -6 2 169.06 7.53 8 6 2 161.75 7.58 8 -6 2 169.94 7.55 8 6 2 158.63 8.61 -8 6 -2 165.86 7.89 8 -6 2 167.50 8.08 8 6 2 154.01 8.07 8 -6 3 23.24 1.10 8 6 3 20.32 1.19 8 -6 3 22.50 1.14 8 -6 3 23.29 1.09 8 6 3 22.10 2.51 -8 6 -3 23.00 1.60 8 -6 3 23.19 1.82 8 6 3 20.98 1.86 8 6 4 35.62 1.93 8 -6 4 41.59 1.89 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8 8 -18 28.72 3.13 8 8 -18 24.79 1.37 8 8 -18 25.40 1.59 -8 -8 17 2.22 0.62 8 8 -17 2.27 1.39 8 -8 -17 2.43 0.67 8 -8 -17 2.89 0.95 8 8 -17 2.86 0.85 8 8 -17 1.85 0.55 8 8 -17 3.44 0.52 8 8 -17 2.54 0.39 8 8 -17 2.88 0.43 8 8 -17 2.51 0.32 8 8 -17 3.16 1.46 8 -8 -17 2.70 0.73 8 8 -17 4.82 2.23 8 8 -17 -0.26 1.83 8 8 -17 3.25 0.61 8 8 -16 141.32 6.94 8 -8 -16 141.33 6.10 8 -8 -16 124.83 6.02 8 8 -16 148.46 5.98 8 8 -16 130.89 6.00 8 8 -16 128.84 6.09 8 8 -16 133.18 5.93 8 8 -16 135.83 5.94 8 8 -16 127.49 5.93 8 8 -16 125.05 7.20 8 -8 -16 124.59 6.03 8 8 -16 135.12 7.69 8 8 -16 134.41 6.80 8 8 -16 132.86 6.00 8 8 -15 20.08 2.08 8 -8 -15 20.27 1.35 8 -8 -15 16.87 1.13 8 8 -15 24.81 1.06 8 8 -15 17.61 1.09 8 8 -15 18.24 1.25 8 8 -15 18.35 0.96 8 8 -15 22.64 2.01 8 -8 -15 18.10 1.17 8 8 -15 22.25 3.06 8 8 -15 17.25 2.38 8 8 -15 18.33 1.10 8 8 -14 223.89 11.38 8 -8 -14 264.01 10.74 8 -8 -14 231.59 10.63 8 8 -14 281.11 10.60 8 -8 -14 224.41 11.31 8 8 -14 231.08 10.61 8 8 -14 231.38 10.68 8 8 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57.36 3.47 8 8 -10 56.24 2.63 8 -8 -10 54.36 2.64 8 8 -10 58.07 2.70 8 8 -10 53.27 2.55 8 -8 -10 59.69 2.60 8 8 -10 60.09 3.27 8 8 -10 56.81 4.18 8 8 -10 57.97 3.78 8 8 -10 56.09 2.63 8 -8 -9 2.20 0.81 8 -8 -9 1.60 0.62 8 8 -9 2.50 0.36 8 8 -9 1.57 0.58 8 8 -9 3.01 0.48 8 -8 -9 3.21 1.26 8 -8 -9 2.64 0.41 8 8 -9 3.09 1.67 8 8 -9 2.02 1.06 8 -8 -9 2.53 0.54 8 8 -9 3.11 2.03 8 8 -9 1.43 0.48 8 -8 -9 1.69 0.53 8 -8 -8 40.73 2.06 8 -8 -8 40.01 2.07 8 8 -8 39.42 1.84 8 -8 -8 40.13 1.95 8 -8 -8 39.89 2.79 8 8 -8 38.06 1.91 8 -8 -8 39.93 1.89 8 8 -8 39.90 1.97 8 -8 -8 41.95 1.93 8 -8 -8 41.50 1.87 8 8 -8 40.63 2.44 8 8 -8 48.55 3.47 8 8 -8 38.26 2.95 8 8 -8 37.45 1.91 8 -8 -7 6.79 0.86 8 -8 -7 5.43 0.85 8 8 -7 7.56 0.48 8 8 -7 7.53 0.60 8 -8 -7 7.46 0.62 8 -8 -7 6.81 0.56 8 8 -7 7.20 0.69 8 -8 -7 7.96 0.48 8 8 -7 8.32 1.82 8 8 -7 8.83 1.16 8 8 -7 7.20 0.62 8 8 -6 9.05 0.70 8 -8 -6 9.35 0.89 8 -8 -6 9.34 0.89 8 8 -6 8.65 0.73 8 8 -6 9.47 0.53 8 -8 -6 8.35 0.59 8 8 -6 8.85 0.64 8 -8 -6 8.60 0.60 8 8 -6 8.26 0.72 8 -8 -6 9.64 0.54 8 8 -6 11.53 1.17 8 -8 -6 8.51 0.65 8 8 -6 8.91 0.66 8 8 -5 12.45 0.80 8 -8 -5 10.43 0.95 8 -8 -5 11.23 0.94 8 8 -5 12.09 0.81 8 8 -5 10.81 0.63 8 8 -5 11.84 0.74 -8 -8 5 9.65 1.26 8 8 -5 11.27 0.81 8 -8 -5 11.44 0.70 8 -8 -5 12.16 0.66 8 8 -5 12.88 1.17 8 8 -5 11.80 0.75 8 -8 -4 75.79 3.54 8 -8 -4 77.95 3.56 8 8 -4 74.55 3.49 -8 -8 4 72.17 4.04 8 8 -4 79.21 3.46 8 8 -4 72.42 3.50 8 8 -4 72.38 3.48 8 -8 -4 75.24 3.42 8 8 -4 72.73 3.77 8 8 -4 79.48 3.46 8 8 -3 7.66 0.58 -8 -8 3 6.53 1.31 8 8 -3 6.93 0.64 8 8 -3 6.67 0.63 8 -8 -3 7.00 0.53 8 8 -3 6.89 0.81 8 -8 -3 7.70 0.78 8 -8 -3 8.10 0.81 8 8 -3 6.69 0.62 8 -8 -2 126.65 5.80 8 8 -2 134.06 5.85 8 8 -2 137.86 5.83 -8 -8 2 127.39 6.53 8 -8 -2 128.58 5.89 8 8 -2 123.84 5.84 8 -8 -2 127.17 5.90 8 -8 -1 14.49 0.74 -8 -8 1 11.04 1.69 8 8 -1 13.14 0.79 8 8 -1 13.12 0.83 8 -8 -1 12.10 0.75 8 8 -1 10.17 1.96 8 -8 -1 12.04 0.91 8 8 -1 12.33 0.81 8 -8 -1 12.36 0.97 8 -8 0 53.90 2.80 8 -8 0 56.68 2.83 8 8 0 57.02 2.75 8 8 0 66.07 2.75 8 -8 0 60.42 2.71 -8 -8 0 57.79 3.62 8 8 0 58.68 2.77 8 -8 0 58.91 2.72 8 8 0 56.56 2.70 8 8 0 58.22 3.74 8 -8 0 61.91 2.70 8 8 1 11.77 0.81 8 -8 1 10.44 0.97 8 -8 1 12.84 0.79 8 8 1 12.91 2.04 8 -8 1 13.83 0.75 8 -8 1 14.53 0.73 8 -8 2 24.42 1.14 -8 8 -2 22.14 1.20 8 -8 2 23.41 1.12 8 8 2 21.94 1.20 8 -8 2 21.27 1.32 8 -8 3 4.27 0.76 8 -8 3 5.06 0.45 8 -8 3 4.94 0.55 8 8 3 5.54 0.51 8 -8 3 5.87 0.45 -8 8 -3 5.52 1.14 -8 8 -4 21.59 1.67 8 -8 4 21.30 1.24 8 -8 4 22.22 1.07 8 -8 4 18.47 1.00 8 -8 4 18.77 0.97 8 -8 4 20.17 0.99 8 8 4 18.77 1.03 8 -8 5 8.22 0.88 8 -8 5 9.58 0.69 8 8 5 7.85 0.72 8 -8 5 8.34 0.58 8 8 5 8.10 0.60 8 -8 5 10.26 0.57 8 -8 5 7.98 0.56 8 -8 6 30.81 1.50 8 -8 6 32.29 1.49 -8 8 -6 34.49 2.29 8 -8 6 32.66 1.71 8 -8 6 34.65 1.57 8 8 6 28.59 1.58 -8 8 -6 30.45 1.49 8 -8 6 31.22 1.52 8 8 6 28.33 3.10 8 8 6 30.75 1.52 -8 8 -7 20.93 1.87 8 -8 7 18.65 1.25 -8 8 -7 19.03 0.98 8 -8 7 20.47 1.09 8 8 7 15.28 1.09 8 -8 7 20.00 1.03 8 -8 7 21.10 0.99 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0.51 8 9 -17 0.96 0.81 8 9 -17 1.92 0.56 8 9 -17 1.58 0.35 8 9 -17 1.78 0.41 8 9 -17 1.77 0.33 8 9 -17 1.57 1.33 8 -9 -17 2.21 0.69 8 9 -17 4.10 2.28 8 9 -17 4.31 1.96 8 9 -17 2.12 0.55 -8 -9 16 2.47 0.69 8 9 -16 2.89 1.49 8 -9 -16 2.51 0.58 8 9 -16 3.34 0.54 8 9 -16 1.85 0.79 8 9 -16 2.18 0.58 8 9 -16 2.40 0.35 8 9 -16 2.52 1.44 8 -9 -16 3.09 0.73 8 9 -16 2.41 2.24 8 9 -16 1.86 1.87 8 9 -16 1.94 0.56 8 9 -15 7.77 1.67 8 -9 -15 5.36 0.65 8 9 -15 8.48 0.63 8 9 -15 4.58 0.87 8 9 -15 6.76 0.68 8 9 -15 5.92 0.46 8 9 -15 9.05 1.53 8 -9 -15 5.96 0.76 8 9 -15 4.01 2.29 8 9 -15 5.87 2.01 8 9 -15 6.59 0.65 8 -9 -14 4.22 0.55 8 9 -14 5.74 0.60 8 9 -14 3.38 0.78 8 9 -14 4.36 0.62 8 -9 -14 5.86 1.41 8 9 -14 3.96 0.41 8 9 -14 4.40 1.40 8 -9 -14 4.93 0.71 8 9 -14 3.70 1.88 8 9 -14 3.22 2.27 8 9 -14 2.99 0.58 8 9 -13 1.85 0.55 8 -9 -13 2.74 0.53 8 -9 -13 3.06 1.03 8 9 -13 3.25 0.64 8 9 -13 1.30 0.70 8 9 -13 2.78 0.56 8 -9 -13 2.10 1.36 8 9 -13 2.39 0.37 8 9 -13 3.32 1.30 8 9 -13 2.11 1.84 8 -9 -13 2.07 0.65 8 9 -13 1.22 2.19 8 -9 -13 2.04 0.49 8 -9 -12 106.84 5.10 8 -9 -12 105.86 5.05 8 -9 -12 97.83 4.94 8 -9 -12 106.34 5.78 8 9 -12 110.96 4.97 8 9 -12 96.51 5.00 8 9 -12 103.83 4.89 8 -9 -12 118.43 4.93 8 9 -12 107.03 6.13 8 9 -12 112.82 5.67 8 9 -12 113.97 6.71 8 9 -12 104.79 4.95 8 -9 -11 13.41 1.30 8 -9 -11 14.29 1.24 8 9 -11 19.95 0.94 8 -9 -11 16.12 1.03 8 9 -11 16.09 0.99 8 -9 -11 14.97 1.84 8 9 -11 13.41 1.08 8 9 -11 16.42 0.85 8 -9 -11 17.94 0.94 8 9 -11 18.69 1.81 8 9 -11 17.77 2.30 8 9 -11 13.18 2.75 8 9 -11 16.28 0.97 8 -9 -10 25.11 1.58 8 -9 -10 25.88 1.64 8 9 -10 30.20 1.34 8 -9 -10 24.51 2.29 8 9 -10 28.34 1.42 8 9 -10 27.43 1.48 8 9 -10 26.66 1.29 8 -9 -10 27.63 1.36 8 9 -10 29.26 2.15 8 9 -10 27.97 3.12 8 9 -10 25.18 2.64 8 9 -10 25.76 1.40 8 -9 -9 4.23 0.94 8 9 -9 6.82 0.51 8 -9 -9 4.91 0.71 8 9 -9 5.14 0.70 8 9 -9 5.34 0.63 8 -9 -9 6.13 1.63 8 -9 -9 5.59 0.59 8 -9 -9 7.61 0.55 8 9 -9 7.48 1.26 8 9 -9 6.70 1.90 8 9 -9 6.40 2.36 8 9 -9 5.62 0.61 8 -9 -8 191.22 8.96 8 9 -8 202.67 8.84 8 9 -8 194.34 8.88 8 -9 -8 200.17 8.86 8 9 -8 189.13 8.91 8 -9 -8 202.74 8.85 8 9 -8 201.70 9.41 8 9 -8 215.74 10.00 8 9 -8 198.87 8.87 8 -9 -7 1.14 0.84 8 9 -7 1.03 0.60 8 -9 -7 1.44 0.81 8 9 -7 1.64 0.36 8 9 -7 1.98 0.58 8 9 -7 1.74 0.49 8 -9 -7 1.14 0.45 8 -9 -7 1.97 0.35 8 9 -7 1.10 1.76 8 9 -7 1.64 1.00 8 9 -7 0.93 0.50 8 -9 -6 18.36 1.26 8 -9 -6 19.10 1.24 8 9 -6 18.18 1.10 8 9 -6 19.05 0.95 8 9 -6 21.01 1.06 8 9 -6 16.86 1.09 8 -9 -6 19.31 0.96 8 9 -6 21.03 2.29 8 9 -6 20.63 1.51 8 9 -6 17.81 1.03 8 9 -5 1.78 0.54 8 -9 -5 1.16 0.79 8 -9 -5 1.14 0.76 8 9 -5 0.86 0.54 8 9 -5 0.81 0.32 8 9 -5 1.54 0.48 8 9 -5 0.86 0.55 8 -9 -5 1.43 0.38 8 9 -5 0.90 0.83 8 9 -5 1.51 1.55 8 9 -5 0.99 0.46 8 9 -4 7.47 0.65 8 -9 -4 6.05 0.82 8 -9 -4 5.97 0.85 8 9 -4 5.51 0.62 8 9 -4 6.41 0.44 8 9 -4 5.96 0.58 -8 -9 4 7.23 1.27 8 9 -4 5.56 0.64 8 -9 -4 5.89 0.51 8 9 -4 6.97 0.88 8 9 -4 5.94 1.89 8 9 -4 6.08 0.59 8 -9 -3 5.75 0.79 8 9 -3 4.55 0.60 8 -9 -3 5.01 0.85 8 9 -3 5.50 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66.74 4.10 10 4 -5 6.07 0.53 10 -4 -5 5.83 0.43 10 -4 -5 6.15 1.47 10 4 -5 7.10 1.57 10 4 -5 8.58 1.34 10 -4 -4 23.16 1.95 10 4 -4 21.44 2.02 10 4 -4 24.21 1.90 10 4 -3 0.79 0.49 10 -4 -3 1.58 1.30 10 4 -3 1.19 1.34 10 4 -3 1.03 1.12 10 -4 -3 1.36 0.64 10 4 -2 90.03 3.94 10 -4 -2 84.65 3.87 10 4 -2 88.76 4.94 10 -4 -2 81.32 4.22 10 4 -2 85.06 4.50 10 -4 -2 82.75 4.57 10 4 -2 91.89 4.68 10 -4 -1 12.58 1.66 10 4 -1 14.86 1.76 10 -4 -1 12.79 0.67 10 4 -1 12.67 0.83 10 -4 -1 13.07 0.72 10 4 -1 14.07 2.06 10 4 -1 12.74 0.72 10 -4 -1 15.10 1.27 10 4 -1 13.05 1.50 10 -4 -1 12.30 0.66 10 4 0 246.49 11.05 10 -4 0 241.86 10.98 10 -4 0 254.05 11.00 10 4 0 247.64 11.01 10 -4 0 259.92 11.53 10 4 0 257.81 12.03 10 4 0 242.64 11.59 10 -4 0 251.32 11.72 10 4 0 264.95 11.75 10 -4 1 13.67 1.78 10 4 1 15.26 1.75 10 4 1 15.44 0.94 10 -4 1 17.13 0.85 10 -4 1 14.49 0.84 10 4 1 14.86 0.86 10 -4 1 15.81 0.86 10 4 1 16.78 0.87 10 4 1 13.93 1.58 10 4 1 17.03 2.20 10 4 1 14.36 0.86 10 -4 1 15.02 0.85 10 -4 1 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25.24 1.24 10 -5 -11 23.16 1.39 10 -5 -11 23.79 1.27 10 -5 -11 25.07 1.20 10 5 -11 24.86 1.16 10 -5 -11 21.97 1.18 10 -5 -11 26.77 1.24 10 5 -11 24.37 1.16 10 -5 -11 23.11 1.25 10 5 -11 25.47 1.97 10 5 -11 26.32 2.39 10 5 -11 26.06 2.50 10 5 -11 25.49 1.18 10 -5 -11 25.09 1.24 10 5 -11 22.61 1.24 10 -5 -11 20.55 1.35 10 -5 -10 25.39 1.37 10 -5 -10 26.99 1.41 10 -5 -10 25.30 1.27 10 -5 -10 25.97 1.21 10 -5 -10 24.96 1.25 10 -5 -10 25.58 1.35 10 -5 -10 22.30 1.17 10 -5 -10 24.82 1.20 10 -5 -10 22.66 1.16 10 5 -10 23.17 1.32 10 5 -10 23.17 1.13 10 5 -10 22.00 2.20 10 -5 -10 26.11 1.23 10 5 -10 24.64 1.79 10 5 -10 27.18 2.31 10 5 -10 23.32 1.25 10 5 -10 23.44 1.22 10 -5 -10 22.56 1.21 10 5 -9 5.22 1.65 10 -5 -9 3.93 1.54 10 -5 -9 4.52 0.78 10 -5 -9 4.74 0.72 10 -5 -9 5.23 0.49 10 -5 -9 5.49 0.55 10 -5 -9 4.79 0.69 10 -5 -9 5.88 0.46 10 -5 -9 6.08 0.49 10 5 -9 5.51 0.64 10 -5 -9 4.76 0.41 10 5 -9 5.95 0.38 10 5 -9 7.11 1.52 10 -5 -9 5.56 0.50 10 5 -9 5.44 0.57 10 5 -9 4.96 0.52 10 -5 -9 5.02 0.52 10 5 -8 116.65 6.08 10 -5 -8 123.88 6.09 10 -5 -8 116.56 5.31 10 -5 -8 113.92 5.26 10 -5 -8 118.88 5.24 10 5 -8 114.86 5.32 10 -5 -8 112.49 5.23 10 5 -8 121.05 5.22 10 -5 -8 114.50 5.26 10 5 -8 113.98 6.04 10 -5 -8 121.32 5.26 10 5 -8 114.07 5.26 10 5 -8 121.29 5.28 10 -5 -7 2.79 0.39 10 5 -7 2.15 0.49 10 -5 -7 2.81 0.40 10 -5 -7 3.23 0.45 10 -5 -7 2.31 0.36 10 -5 -7 2.44 0.32 10 5 -7 3.06 1.36 10 -5 -7 3.36 0.42 10 5 -7 2.69 0.53 10 5 -7 1.86 1.45 10 -5 -7 2.31 1.49 10 5 -6 116.77 5.21 10 -5 -6 111.64 5.18 10 -5 -6 118.83 5.18 10 -5 -6 116.18 5.16 10 5 -6 112.71 5.15 10 5 -6 121.19 5.98 10 5 -6 120.29 5.23 10 5 -6 113.72 5.96 10 -5 -6 122.08 5.94 10 5 -5 12.45 0.76 10 -5 -5 12.42 0.62 10 -5 -5 12.24 0.68 10 -5 -5 9.12 0.69 10 -5 -5 11.33 0.67 10 -5 -5 11.51 0.65 10 -5 -5 11.71 0.66 10 5 -5 13.20 0.62 10 5 -5 12.06 1.67 10 5 -5 12.75 0.78 10 -5 -5 12.79 1.61 10 5 -5 12.05 1.67 10 -5 -4 29.18 1.36 10 -5 -4 28.77 1.39 10 -5 -4 28.77 1.39 10 -5 -4 28.17 1.38 10 -5 -4 26.85 1.37 10 -5 -4 28.80 1.39 10 5 -4 32.07 1.35 10 5 -4 30.70 2.24 10 5 -4 29.89 1.46 10 -5 -4 28.78 2.25 10 5 -4 31.85 2.35 10 -5 -3 0.67 0.23 10 -5 -3 0.29 0.30 10 -5 -3 0.67 0.33 10 -5 -3 0.54 0.26 10 -5 -3 1.03 0.33 10 5 -3 0.46 0.22 10 5 -3 0.82 0.52 10 5 -3 0.95 0.34 10 5 -3 0.37 1.11 10 -5 -3 0.79 1.19 10 5 -3 0.68 1.28 10 5 -3 0.82 0.48 10 -5 -2 37.22 1.70 10 -5 -2 38.97 1.72 10 -5 -2 37.61 1.72 10 -5 -2 37.40 1.71 10 5 -2 33.40 1.80 10 -5 -2 37.89 1.73 10 5 -2 37.11 1.68 10 5 -2 34.37 1.73 10 5 -2 33.27 2.51 10 -5 -2 36.10 2.47 10 5 -2 36.37 2.61 10 -5 -1 4.43 1.33 10 5 -1 2.90 1.30 10 5 -1 3.55 1.83 10 -5 -1 3.00 0.36 10 -5 -1 3.77 0.34 10 5 -1 3.76 0.28 10 -5 -1 2.87 0.40 10 5 -1 4.14 0.60 10 -5 -1 3.58 0.79 10 5 -1 4.99 1.34 10 5 -1 3.22 0.40 10 -5 -1 3.19 0.37 10 -5 -1 4.07 0.33 10 -5 0 7.54 0.47 10 -5 0 8.00 0.55 10 5 0 7.16 0.54 10 -5 0 6.92 0.51 10 -5 0 8.48 1.43 10 5 0 7.67 1.43 10 5 0 7.14 0.63 10 -5 0 8.04 0.50 10 -5 0 8.92 0.49 10 5 0 7.64 0.42 10 5 0 6.79 0.68 10 5 0 7.72 0.55 10 5 0 6.40 1.40 10 -5 0 8.05 0.54 10 5 0 6.71 0.55 10 5 0 7.66 0.56 10 -5 1 3.57 0.39 10 -5 1 3.20 0.41 10 5 1 2.60 0.42 10 5 1 2.98 0.52 10 -5 1 2.66 0.41 10 5 1 3.08 0.45 10 5 1 2.48 0.41 10 5 1 2.86 0.57 10 -5 1 2.80 0.38 10 5 1 2.84 1.29 10 -5 1 3.02 1.30 10 5 1 2.54 1.30 10 -5 2 201.44 9.22 10 5 2 194.54 9.25 10 -5 2 182.29 8.47 10 5 2 183.63 8.45 10 5 2 192.56 8.46 10 -5 2 186.60 8.45 10 5 2 192.66 8.50 10 -5 2 192.62 8.45 10 -5 2 180.56 8.44 10 5 2 183.02 9.17 10 -5 2 200.16 8.45 10 -5 2 190.51 8.45 10 5 2 193.68 8.45 10 -5 3 6.50 0.64 10 5 3 8.12 0.59 10 -5 3 7.35 0.58 10 5 3 9.25 0.61 10 5 3 7.48 0.72 10 -5 3 7.77 0.59 10 -5 3 7.18 0.58 10 -5 3 8.30 0.51 10 -5 3 8.75 0.58 10 -5 3 8.46 0.59 10 5 3 7.29 0.59 10 -5 3 8.35 0.53 10 -5 3 8.12 1.49 10 5 3 7.81 1.63 10 -5 4 84.67 4.57 10 5 4 82.90 4.65 10 -5 4 85.22 3.79 10 -5 4 82.52 3.76 10 5 4 78.31 3.76 10 5 4 85.30 3.77 10 5 4 76.30 3.81 10 -5 4 89.05 3.76 10 -5 4 75.99 3.75 10 5 4 81.32 5.07 10 -5 4 85.01 3.76 10 -5 4 85.89 3.72 10 5 4 83.73 3.76 10 -5 4 85.25 3.76 10 -5 4 78.47 3.74 10 -5 5 15.25 1.92 10 5 5 13.16 1.88 10 -5 5 12.93 0.88 10 -5 5 13.06 0.82 10 5 5 12.22 0.84 10 5 5 13.83 0.83 10 5 5 12.45 0.94 10 -5 5 14.66 0.83 10 -5 5 14.86 0.83 10 5 5 15.38 2.46 10 -5 5 14.41 0.75 10 -5 5 13.28 0.84 10 -5 5 13.75 0.78 10 -5 6 109.47 5.52 10 5 6 103.30 5.57 10 -5 6 107.08 4.62 10 5 6 105.78 4.60 10 -5 6 106.98 4.59 10 5 6 97.94 4.59 10 5 6 103.67 4.64 10 -5 6 96.37 4.58 -10 5 -6 92.24 4.52 10 -5 6 104.04 4.59 10 5 6 96.23 5.99 10 -5 6 107.96 4.60 10 -5 6 102.19 4.55 10 -5 6 102.87 4.57 -10 5 -7 6.24 1.18 10 -5 7 8.49 1.61 10 5 7 5.62 1.74 10 -5 7 6.28 0.68 10 5 7 6.16 0.58 10 5 7 6.78 0.63 10 -5 7 6.37 0.60 -10 -5 -7 6.92 0.62 10 -5 7 6.24 0.58 10 5 7 5.72 0.74 10 -5 7 6.43 0.64 -10 5 -7 6.54 0.46 10 5 7 6.79 2.24 10 -5 7 6.58 0.59 10 -5 7 6.41 0.50 -10 5 -8 41.02 2.45 10 -5 8 32.23 2.75 10 5 8 36.60 2.84 10 -5 8 35.71 1.77 10 5 8 38.73 1.75 -10 -5 -8 33.54 1.71 10 -5 8 36.71 1.73 10 5 8 33.44 1.71 10 5 8 35.77 1.80 10 -5 8 33.93 1.74 -10 5 -8 34.08 1.63 10 5 8 33.29 3.32 10 -5 8 35.56 1.71 10 -5 9 28.63 2.58 10 5 9 26.52 2.69 10 -5 9 31.92 1.57 10 -5 9 30.10 1.53 -10 -5 -9 29.31 1.52 10 5 9 29.00 1.61 10 -5 9 29.44 1.56 -10 5 -9 28.28 1.42 10 5 9 29.24 3.18 10 -5 9 34.53 1.55 10 -5 9 30.92 1.53 10 5 10 26.76 2.53 10 -5 10 21.16 2.27 10 -5 10 25.10 1.25 -10 -5 -10 20.88 1.17 10 -5 10 23.85 1.21 10 5 10 19.47 1.29 10 -5 10 20.68 1.26 -10 5 -10 20.82 1.08 10 5 10 21.15 2.95 10 -5 10 23.84 1.23 10 -5 10 22.22 1.21 10 -5 11 9.23 0.80 10 -5 11 11.71 2.02 10 5 11 9.93 1.92 10 -5 11 9.77 0.82 10 -5 11 10.69 0.78 -10 -5 -11 8.49 0.73 10 5 11 10.06 0.89 10 -5 11 10.94 0.86 -10 5 -11 8.54 0.60 10 -5 11 9.76 0.85 10 -5 12 34.47 1.71 10 -5 12 29.59 2.85 10 5 12 31.60 2.82 10 -5 12 36.36 1.73 10 -5 12 34.60 1.70 10 5 12 31.64 1.73 10 -5 12 33.27 1.74 -10 5 -12 31.53 1.58 10 5 12 39.83 3.56 10 -5 12 33.61 1.72 10 -5 13 10.93 0.84 10 -5 13 7.89 1.88 10 5 13 11.39 2.05 10 -5 13 9.31 0.86 10 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12.80 0.76 10 -6 -23 11.93 0.82 10 6 -23 12.31 0.88 10 -6 -23 10.58 0.91 10 6 -23 13.75 1.16 10 6 -22 18.16 1.08 10 -6 -22 17.46 1.19 10 6 -22 17.36 1.27 10 6 -22 17.51 0.94 10 -6 -22 19.70 1.13 10 6 -22 15.73 1.04 10 -6 -22 16.02 1.03 10 6 -21 24.23 1.30 10 -6 -21 21.66 1.38 10 6 -21 22.03 1.51 -10 -6 21 18.68 1.15 10 6 -21 23.72 1.14 10 -6 -21 24.68 1.31 10 6 -21 27.67 2.85 10 -6 -21 19.99 1.24 10 6 -21 22.92 1.25 10 6 -20 60.87 2.71 10 -6 -20 56.44 2.75 10 6 -20 58.96 2.82 -10 -6 20 55.11 2.62 10 6 -20 56.07 2.58 10 -6 -20 57.03 2.70 10 6 -20 52.34 4.01 10 6 -20 52.51 4.00 10 -6 -20 56.28 2.66 10 6 -20 51.23 2.67 10 6 -19 6.68 0.76 10 -6 -19 5.39 0.83 10 6 -19 5.66 0.97 -10 -6 19 5.95 0.61 10 6 -19 4.97 0.50 10 6 -19 4.51 2.06 10 -6 -19 5.45 0.79 10 6 -19 3.53 1.89 10 -6 -19 5.44 0.65 10 6 -19 5.58 0.68 10 6 -18 87.60 3.73 10 -6 -18 90.16 3.79 10 -6 -18 77.82 3.77 10 -6 -18 73.45 3.62 10 6 -18 85.64 3.83 10 6 -18 82.39 4.41 10 6 -18 79.80 3.62 10 -6 -18 81.51 3.73 10 6 -18 80.73 5.05 10 6 -18 79.42 5.07 10 -6 -18 78.57 3.69 10 6 -18 79.03 3.71 10 6 -17 30.80 1.53 10 6 -17 31.61 2.26 10 -6 -17 27.72 1.60 10 -6 -17 27.40 1.56 10 -6 -17 24.51 1.34 10 6 -17 29.98 1.65 10 6 -17 29.01 1.34 10 -6 -17 28.53 1.48 10 6 -17 35.58 3.00 10 6 -17 30.51 2.91 10 -6 -17 25.98 1.45 10 6 -17 29.23 1.47 10 6 -16 55.21 2.59 10 6 -16 55.60 3.21 10 -6 -16 54.63 2.62 10 -6 -16 60.39 2.75 10 -6 -16 54.42 2.63 10 6 -16 54.50 2.48 10 -6 -16 51.88 2.48 10 6 -16 57.97 2.69 10 6 -16 52.04 2.45 10 6 -16 55.02 2.46 10 -6 -16 53.32 2.56 10 6 -16 60.72 3.40 10 6 -16 58.63 4.06 10 -6 -16 52.27 2.54 10 6 -16 52.91 2.55 10 6 -15 0.62 0.62 10 6 -15 1.91 1.11 10 -6 -15 0.62 0.96 10 -6 -15 1.52 0.78 10 -6 -15 1.37 0.63 10 -6 -15 1.22 0.46 10 6 -15 0.96 0.76 10 -6 -15 1.36 0.38 10 6 -15 1.01 0.35 10 6 -15 1.43 0.31 10 6 -15 0.91 0.31 10 -6 -15 0.83 0.60 10 6 -15 1.91 1.35 10 6 -15 -2.28 1.94 10 -6 -15 1.80 0.48 10 6 -15 0.89 0.51 10 6 -14 91.35 4.09 10 6 -14 91.08 4.66 10 -6 -14 93.34 4.16 10 -6 -14 88.50 4.10 10 -6 -14 86.15 4.14 10 -6 -14 95.94 4.20 10 -6 -14 90.94 4.09 10 6 -14 94.47 4.00 10 -6 -14 90.19 4.02 10 -6 -14 83.58 4.00 10 6 -14 87.42 4.14 10 6 -14 85.08 3.98 10 -6 -14 88.40 4.06 10 6 -14 93.13 4.77 10 -6 -14 91.88 4.08 10 6 -14 89.96 5.40 10 -6 -14 84.56 4.04 10 6 -14 88.14 4.05 10 6 -13 8.33 0.74 10 6 -13 8.18 1.21 10 -6 -13 5.90 0.86 10 -6 -13 6.95 1.00 10 -6 -13 7.31 0.71 10 -6 -13 7.67 0.69 10 -6 -13 6.32 0.73 10 -6 -13 7.80 0.89 10 -6 -13 6.36 0.57 10 6 -13 7.28 0.48 10 -6 -13 6.80 0.52 10 6 -13 7.33 0.82 10 6 -13 7.41 0.47 10 -6 -13 6.18 0.69 10 -6 -13 6.81 0.68 10 6 -13 7.84 1.39 10 6 -13 4.36 1.93 10 6 -13 5.65 0.57 10 6 -13 6.75 0.48 10 -6 -13 6.05 0.58 10 6 -12 29.03 1.55 10 6 -12 27.95 1.50 10 -6 -12 28.09 1.49 10 6 -12 28.26 2.05 10 -6 -12 30.89 1.72 10 -6 -12 30.45 1.55 10 -6 -12 33.14 1.66 10 6 -12 32.64 1.43 10 -6 -12 30.33 1.51 10 -6 -12 28.21 1.47 10 -6 -12 30.99 1.53 10 -6 -12 32.14 1.51 10 -6 -12 28.76 1.45 10 6 -12 31.50 1.63 10 6 -12 31.37 1.42 10 6 -12 34.76 2.22 10 -6 -12 29.33 1.53 10 6 -12 34.50 2.96 10 -6 -12 31.13 1.47 10 6 -12 28.04 1.48 10 6 -12 29.67 1.43 10 -6 -11 9.92 0.56 10 6 -11 10.96 0.80 10 6 -11 9.41 0.72 10 -6 -11 9.74 0.69 10 -6 -11 8.99 0.76 10 -6 -11 12.39 0.75 10 -6 -11 9.37 0.91 10 -6 -11 9.87 0.67 10 6 -11 11.73 0.61 10 -6 -11 11.52 0.76 10 -6 -11 10.97 0.72 10 -6 -11 10.14 0.64 10 6 -11 9.34 0.86 10 6 -11 11.05 0.59 10 6 -11 13.33 1.49 10 6 -11 12.86 1.99 10 -6 -11 10.45 0.75 10 6 -11 13.38 2.05 10 -6 -11 10.10 0.67 10 6 -11 10.48 0.67 10 6 -11 10.97 0.62 10 -6 -10 54.75 2.71 10 6 -10 63.68 2.82 10 6 -10 57.65 2.77 10 -6 -10 58.86 2.77 10 -6 -10 60.21 2.82 10 -6 -10 60.38 2.91 10 -6 -10 58.29 2.78 10 -6 -10 59.19 2.79 10 6 -10 70.85 2.74 10 -6 -10 61.88 2.87 10 -6 -10 58.38 2.76 10 -6 -10 57.97 2.75 10 -6 -10 58.81 2.78 10 6 -10 63.75 2.87 10 6 -10 61.09 2.73 10 6 -10 61.74 3.40 10 -6 -10 64.05 2.80 10 6 -10 60.96 3.83 10 6 -10 60.00 2.74 10 -6 -9 2.21 0.28 10 6 -9 2.60 0.53 10 -6 -9 2.68 0.45 10 6 -9 1.94 0.45 10 -6 -9 2.15 0.43 10 6 -9 3.13 0.61 10 -6 -9 2.00 0.72 10 -6 -9 2.06 0.48 10 -6 -9 2.25 0.42 10 -6 -9 2.35 0.65 10 -6 -9 2.70 0.50 10 6 -9 1.66 0.59 10 -6 -9 2.09 0.37 10 6 -9 2.53 0.32 10 6 -9 2.60 1.58 10 6 -9 1.26 1.00 10 -6 -9 2.69 0.48 10 6 -9 1.86 0.47 10 6 -8 238.73 10.45 10 6 -8 226.23 10.41 10 -6 -8 225.31 10.38 10 -6 -8 249.06 10.43 10 -6 -8 222.11 10.41 10 6 -8 237.42 11.18 10 -6 -8 240.79 11.16 10 6 -8 231.65 10.46 10 -6 -8 231.41 10.50 10 -6 -8 233.62 10.45 10 -6 -8 247.18 10.51 10 6 -8 243.87 10.48 10 -6 -8 221.52 10.47 10 -6 -8 224.71 10.42 10 -6 -8 232.82 10.41 10 6 -8 241.66 10.49 10 -6 -8 236.29 10.40 10 6 -8 244.70 10.39 10 -6 -8 244.93 10.44 10 6 -8 237.46 11.29 10 6 -8 233.73 10.45 10 6 -7 8.02 0.67 10 -6 -7 8.55 0.61 10 -6 -7 9.28 0.50 10 6 -7 9.27 1.67 10 -6 -7 5.98 1.50 10 6 -7 8.11 0.71 10 -6 -7 8.49 0.87 10 6 -7 8.55 0.74 10 -6 -7 8.82 0.85 10 -6 -7 8.73 0.75 10 -6 -7 8.48 0.61 10 -6 -7 9.29 0.61 10 -6 -7 7.94 0.58 10 -6 -7 8.55 0.55 10 6 -7 8.13 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1.00 10 -6 0 16.00 0.90 10 6 0 17.30 0.80 10 6 0 17.52 0.89 10 6 0 15.79 1.86 10 6 0 14.92 0.88 10 -6 1 6.35 0.48 10 6 1 5.37 0.51 10 -6 1 4.94 0.47 10 -6 1 5.38 0.76 10 6 1 5.13 0.62 10 -6 1 4.95 0.42 10 -6 1 5.61 0.58 10 6 1 5.82 0.51 10 -6 1 5.41 0.49 10 6 1 6.91 0.55 10 6 1 5.28 0.67 10 -6 1 5.75 0.47 10 6 1 5.90 0.37 10 6 1 5.74 0.52 10 6 1 7.02 1.45 10 -6 1 6.67 1.37 10 6 1 6.73 1.47 10 -6 2 82.37 4.52 10 6 2 80.65 4.55 10 -6 2 82.23 3.80 10 6 2 80.40 3.76 10 -6 2 80.83 3.76 10 6 2 81.84 3.78 10 6 2 80.14 3.70 10 6 2 83.87 3.83 10 -6 2 91.94 3.78 10 -6 2 80.03 3.75 10 6 2 90.88 5.21 10 6 2 78.97 4.63 10 -6 2 81.34 3.76 10 -6 2 90.42 3.77 10 -6 2 87.05 3.74 10 6 2 80.37 3.77 10 -6 3 14.76 0.92 10 -6 3 14.51 0.85 10 6 3 15.54 2.49 10 6 3 14.18 0.85 10 6 3 15.51 0.88 10 6 3 15.97 0.99 10 -6 3 15.99 0.88 10 -6 3 14.82 0.85 10 -6 3 17.27 0.88 10 -6 3 12.97 0.84 10 -6 3 17.37 0.81 10 -6 3 14.79 0.80 10 6 3 14.03 0.86 10 6 3 17.74 1.88 10 -6 3 11.84 1.70 10 -6 4 64.07 3.93 10 6 4 67.06 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0.54 10 6 7 4.60 2.32 10 -6 7 7.86 0.63 10 -6 7 8.40 0.57 10 -6 7 9.08 0.72 10 -6 8 14.59 1.81 10 6 8 14.90 1.94 10 -6 8 13.69 0.90 10 -6 8 12.66 0.84 10 6 8 11.94 0.85 -10 -6 -8 13.90 0.86 10 6 8 12.31 0.81 10 6 8 12.44 0.93 10 -6 8 13.71 0.85 10 -6 8 14.26 0.86 -10 6 -8 13.14 0.73 10 6 8 9.66 2.45 10 -6 8 13.07 0.76 10 -6 8 14.18 0.81 10 -6 9 14.09 1.97 10 6 9 13.14 2.03 10 -6 9 15.00 0.94 10 6 9 14.79 0.91 10 -6 9 14.19 0.90 -10 -6 -9 14.86 0.92 10 6 9 12.91 1.01 10 -6 9 13.51 0.90 10 -6 9 14.15 0.94 -10 6 -9 14.76 0.79 10 6 9 10.10 2.57 10 -6 9 15.48 0.89 10 -6 10 25.58 2.37 10 6 10 26.73 2.48 10 -6 10 27.96 1.42 10 -6 10 26.27 1.38 -10 -6 -10 24.00 1.37 10 6 10 26.71 1.39 10 6 10 25.77 1.43 10 -6 10 27.78 1.41 -10 6 -10 24.61 1.28 10 6 10 22.49 3.13 10 -6 10 29.90 1.43 10 -6 10 27.13 1.37 10 -6 11 14.15 2.00 10 6 11 10.96 1.89 10 -6 11 12.08 0.94 10 6 11 13.20 0.90 10 -6 11 12.03 0.88 -10 -6 -11 13.13 0.88 10 6 11 12.73 0.94 10 -6 11 13.81 0.95 -10 6 -11 12.48 0.76 10 6 11 13.35 2.63 10 -6 11 15.40 0.97 10 -6 11 14.61 0.89 10 -6 12 2.87 0.60 10 -6 12 3.37 1.60 10 6 12 3.59 1.59 10 -6 12 3.51 0.63 10 -6 12 2.58 0.58 10 6 12 3.41 0.62 -10 -6 -12 2.63 0.60 10 6 12 2.89 0.68 10 -6 12 3.86 0.66 -10 6 -12 2.25 0.43 10 6 12 1.53 2.06 10 -6 12 3.05 0.70 10 -6 13 2.45 0.63 10 -6 13 3.61 1.49 10 -6 13 2.59 0.62 10 -6 13 2.33 0.55 -10 -6 -13 1.88 0.56 10 6 13 2.37 0.60 -10 6 -13 2.30 0.43 10 6 13 2.46 0.61 10 -6 13 1.87 0.69 10 6 13 4.04 2.04 10 -6 13 2.68 0.64 -10 -6 -14 1.31 0.50 10 6 14 1.13 0.55 10 -6 14 0.40 0.54 -10 6 -14 1.77 0.40 10 6 14 0.58 0.54 10 -6 14 1.70 0.68 10 -6 14 1.35 0.59 10 -6 14 0.48 0.61 10 -6 14 0.95 0.63 10 -6 15 1.48 0.51 10 6 15 1.78 0.56 -10 6 -15 1.90 0.39 10 -6 15 1.47 0.64 10 -6 15 -0.04 0.56 10 -6 15 1.12 0.60 10 -6 15 1.16 0.59 10 6 16 1.18 0.50 10 -6 16 0.80 0.53 -10 6 -16 1.24 0.37 10 -6 16 1.14 0.61 10 -6 16 1.18 0.59 10 -6 16 -0.01 0.55 10 6 17 0.42 0.47 10 -6 17 0.54 0.48 -10 6 -17 0.54 0.34 10 -6 17 2.00 0.61 10 -6 17 1.08 0.58 10 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17.21 1.02 10 7 -19 16.04 1.02 10 7 -18 255.65 10.86 10 7 -18 247.22 11.58 10 -7 -18 272.31 10.91 10 -7 -18 244.29 10.89 10 -7 -18 229.21 10.79 10 7 -18 253.25 10.95 10 7 -18 243.81 10.77 10 7 -18 228.11 11.63 10 -7 -18 249.74 10.87 10 7 -18 250.35 12.14 10 7 -18 252.76 12.36 10 -7 -18 233.77 10.82 10 7 -18 230.33 10.83 10 7 -17 19.19 1.16 10 7 -17 14.87 1.82 10 -7 -17 18.58 1.32 10 -7 -17 18.34 1.16 10 7 -17 20.31 0.99 10 -7 -17 17.70 0.98 10 7 -17 19.86 1.34 10 7 -17 19.63 0.93 10 7 -17 18.53 0.95 10 -7 -17 18.54 1.10 10 7 -17 18.23 1.98 10 7 -17 20.23 2.63 10 7 -17 17.05 2.45 10 -7 -17 16.27 1.03 10 7 -17 16.71 1.04 10 7 -16 67.75 2.97 10 7 -16 62.16 3.64 10 -7 -16 61.13 2.98 10 -7 -16 61.52 3.04 10 -7 -16 71.01 3.15 10 7 -16 66.60 2.87 10 -7 -16 58.40 2.86 10 7 -16 68.13 3.07 10 7 -16 61.37 2.84 10 7 -16 61.79 2.84 10 -7 -16 65.32 2.91 10 7 -16 66.68 4.26 10 7 -16 61.22 3.71 10 7 -16 70.44 4.49 10 7 -16 59.95 2.90 10 -7 -16 59.09 2.89 10 7 -15 4.90 0.71 10 7 -15 4.54 1.22 10 -7 -15 4.12 0.91 10 -7 -15 4.25 1.06 10 -7 -15 4.97 0.68 10 7 -15 5.08 0.46 10 7 -15 5.11 0.87 10 -7 -15 4.32 0.50 10 7 -15 4.74 0.42 10 7 -15 4.64 0.40 10 -7 -15 4.47 0.64 10 7 -15 6.38 1.49 10 7 -15 2.64 1.98 10 7 -15 4.89 1.97 10 -7 -15 3.66 0.50 10 7 -14 165.69 7.56 10 7 -14 159.56 8.15 10 -7 -14 168.78 7.57 10 -7 -14 166.18 7.60 10 7 -14 179.70 7.49 10 -7 -14 158.62 7.50 10 7 -14 169.01 7.62 10 7 -14 166.91 7.47 10 -7 -14 170.43 7.53 10 7 -14 175.16 8.26 10 -7 -14 175.17 7.56 10 7 -14 171.75 9.03 10 -7 -14 159.26 7.51 10 7 -13 12.88 0.88 10 7 -13 12.77 1.53 10 -7 -13 11.20 1.07 10 -7 -13 10.45 0.83 10 -7 -13 12.49 1.02 10 7 -13 13.00 0.68 10 -7 -13 10.11 0.71 10 -7 -13 11.19 0.80 10 7 -13 10.80 0.95 10 7 -13 12.26 0.65 10 -7 -13 10.90 0.80 10 -7 -13 11.01 0.83 10 7 -13 13.82 1.66 10 7 -13 8.39 2.25 10 -7 -13 10.34 0.71 10 7 -13 9.95 0.65 10 -7 -12 7.59 0.48 10 7 -12 8.82 0.76 10 -7 -12 7.25 0.71 10 -7 -12 6.71 0.90 10 7 -12 9.52 0.54 10 -7 -12 6.81 0.67 10 -7 -12 7.41 0.59 10 7 -12 9.04 0.86 10 7 -12 9.59 0.54 10 -7 -12 9.14 0.74 10 7 -12 10.68 1.42 10 7 -12 8.27 2.09 10 7 -12 9.02 0.53 10 -7 -11 5.79 0.43 10 7 -11 7.38 0.69 10 -7 -11 6.45 0.64 10 -7 -11 5.68 1.01 10 -7 -11 6.21 0.82 10 -7 -11 6.32 0.65 10 -7 -11 5.59 0.78 10 7 -11 8.13 0.52 10 7 -11 6.04 0.79 10 -7 -11 6.81 0.63 10 -7 -11 6.41 0.55 10 7 -11 8.02 0.49 10 -7 -11 6.22 0.67 10 7 -11 9.36 1.37 10 7 -11 7.24 1.97 10 7 -11 7.66 0.49 10 -7 -10 84.35 4.18 10 7 -10 92.23 4.26 10 -7 -10 95.33 4.37 10 -7 -10 94.14 4.37 10 -7 -10 86.53 4.26 10 -7 -10 94.26 4.24 10 -7 -10 95.01 4.25 10 -7 -10 95.88 4.31 10 -7 -10 87.18 4.24 10 -7 -10 86.95 4.22 10 7 -10 94.34 4.32 10 7 -10 96.83 4.19 10 7 -10 95.86 4.82 10 -7 -10 92.35 4.26 10 7 -10 86.05 4.26 10 7 -10 99.93 4.20 10 -7 -9 12.30 0.84 10 7 -9 13.38 0.90 10 -7 -9 13.99 0.71 10 -7 -9 11.90 1.10 10 -7 -9 13.87 1.13 10 7 -9 11.84 0.94 10 -7 -9 12.01 0.85 10 -7 -9 12.70 0.83 10 -7 -9 13.15 0.98 10 7 -9 11.99 0.78 10 7 -9 13.85 0.98 10 -7 -9 14.17 0.78 10 7 -9 13.80 0.73 10 7 -9 13.04 2.04 10 7 -9 15.76 1.49 10 -7 -9 14.06 0.87 10 7 -9 12.77 0.85 10 -7 -8 115.99 4.89 10 -7 -8 104.92 4.82 10 7 -8 109.53 4.90 10 7 -8 113.22 4.93 10 -7 -8 104.03 4.89 10 7 -8 112.78 4.94 10 -7 -8 108.73 4.99 10 -7 -8 109.12 4.87 10 -7 -8 105.65 4.87 10 -7 -8 102.97 4.93 10 7 -8 111.00 4.86 10 7 -8 103.81 4.94 10 -7 -8 104.67 4.85 10 7 -8 107.68 4.83 10 7 -8 112.30 5.39 10 -7 -8 116.71 4.90 10 7 -8 104.18 5.87 10 7 -8 101.55 4.89 10 -7 -7 8.19 0.47 10 7 -7 7.57 0.65 10 -7 -7 7.46 0.60 10 7 -7 6.19 1.47 10 -7 -7 4.76 1.40 10 7 -7 6.58 0.71 10 -7 -7 5.65 0.89 10 -7 -7 5.97 0.57 10 7 -7 6.28 0.71 10 -7 -7 6.92 0.59 10 -7 -7 6.87 0.57 10 -7 -7 6.64 0.73 10 -7 -7 6.69 0.52 10 7 -7 7.67 0.52 10 7 -7 7.34 0.74 10 -7 -7 6.81 0.50 10 7 -7 8.01 1.83 10 7 -7 7.11 0.57 10 7 -6 134.98 6.92 10 -7 -6 140.79 6.88 10 7 -6 135.00 6.27 10 -7 -6 136.60 6.24 10 -7 -6 141.34 6.32 10 7 -6 135.58 6.28 10 -7 -6 135.48 6.22 10 -7 -6 139.10 6.27 10 -7 -6 135.50 6.21 10 -7 -6 136.41 6.21 10 7 -6 146.10 6.22 10 7 -6 137.25 6.29 10 -7 -6 138.81 6.20 10 7 -6 141.87 6.19 10 7 -6 139.96 7.21 10 -7 -6 148.79 6.24 10 -7 -6 138.37 6.19 10 7 -6 133.97 6.25 10 7 -5 21.72 1.20 10 7 -5 18.94 1.93 10 -7 -5 20.21 1.90 10 7 -5 20.53 1.19 10 -7 -5 19.58 1.31 10 -7 -5 20.70 1.10 10 -7 -5 17.90 1.07 10 -7 -5 18.57 1.18 10 -7 -5 20.91 1.07 10 7 -5 22.20 1.09 10 7 -5 21.32 1.22 10 -7 -5 22.43 1.07 10 7 -5 22.69 1.03 10 7 -5 23.25 2.25 10 -7 -5 22.68 1.04 10 -7 -5 21.67 1.11 10 7 -5 20.83 1.16 10 7 -4 55.98 2.66 10 7 -4 54.72 3.34 10 -7 -4 51.88 3.23 10 -7 -4 54.12 2.73 10 7 -4 57.69 2.67 10 -7 -4 52.28 2.72 10 -7 -4 48.51 2.58 10 -7 -4 52.37 2.59 10 -7 -4 51.80 2.65 10 -7 -4 61.68 2.59 10 7 -4 60.71 2.61 10 7 -4 59.09 2.69 10 -7 -4 58.85 2.59 10 7 -4 57.90 2.55 10 7 -4 53.93 2.58 10 7 -4 54.08 3.63 10 7 -4 58.93 2.64 10 -7 -4 56.56 2.61 10 -7 -4 59.81 2.57 10 7 -3 30.01 1.60 10 -7 -3 29.12 2.24 10 7 -3 28.70 2.32 10 -7 -3 30.25 1.69 10 -7 -3 29.93 1.70 10 7 -3 28.91 1.60 10 -7 -3 26.52 1.58 10 -7 -3 29.56 1.51 10 -7 -3 33.01 1.50 -10 -7 3 28.04 2.14 10 -7 -3 30.13 1.51 10 7 -3 35.15 1.46 10 7 -3 29.46 1.50 10 7 -3 31.82 2.66 10 -7 -3 34.18 1.48 10 7 -2 33.10 1.67 10 -7 -2 31.34 2.27 10 7 -2 31.56 2.38 10 -7 -2 32.48 1.75 10 7 -2 32.24 1.65 10 -7 -2 29.14 1.63 10 -7 -2 32.77 1.57 10 -7 -2 32.33 1.56 -10 -7 2 28.12 2.23 10 -7 -2 34.38 1.59 10 7 -2 35.82 1.53 10 7 -2 32.22 1.57 10 7 -2 31.36 2.65 10 -7 -2 31.91 1.54 10 -7 -2 33.79 1.54 10 -7 -1 2.94 0.73 10 7 -1 2.36 0.54 10 -7 -1 2.25 0.40 10 -7 -1 2.85 0.54 10 -7 -1 2.48 1.17 10 7 -1 3.31 1.28 10 7 -1 2.36 0.60 10 -7 -1 2.56 0.45 10 7 -1 2.12 0.29 10 7 -1 2.25 0.41 10 7 -1 2.91 1.60 10 -7 -1 2.71 0.39 10 -7 -1 3.02 0.36 10 7 0 42.18 2.23 10 -7 0 48.23 2.33 10 -7 0 46.32 2.22 10 -7 0 43.53 2.16 10 -7 0 49.89 2.92 10 7 0 42.48 2.94 10 -7 0 44.57 2.18 10 7 0 50.36 2.12 10 7 0 45.98 2.18 10 7 0 45.28 3.25 10 -7 0 48.65 2.16 10 -7 1 1.24 0.40 10 7 1 1.05 0.53 10 -7 1 1.36 0.73 10 -7 1 0.60 0.48 10 -7 1 0.87 0.41 10 -7 1 1.41 1.17 10 7 1 0.79 1.20 10 7 1 1.00 0.25 10 7 1 0.84 0.61 10 7 1 0.84 0.42 10 7 1 1.39 1.55 10 7 1 0.76 0.44 10 -7 2 60.65 2.77 10 -7 2 64.58 2.74 10 -7 2 62.41 2.91 10 -7 2 57.99 2.80 10 -7 2 55.63 3.48 10 7 2 56.66 3.53 10 7 2 55.30 2.84 10 -7 2 55.74 2.75 10 7 2 61.49 2.71 10 7 2 57.10 3.79 10 7 2 61.62 2.79 10 -7 3 1.64 0.36 10 -7 3 1.66 0.37 10 -7 3 1.75 0.47 10 -7 3 1.25 0.77 10 -7 3 1.84 0.51 10 -7 3 1.18 1.18 10 7 3 2.76 1.34 10 -7 3 1.45 0.49 10 7 3 0.97 0.62 10 -7 3 1.34 0.41 10 7 3 2.70 1.58 10 7 3 2.19 2.09 10 7 3 1.99 0.47 10 -7 3 1.56 0.39 10 -7 4 -0.16 0.77 10 -7 4 0.28 0.51 10 -7 4 0.80 0.38 10 7 4 0.32 0.44 10 -7 4 0.04 0.49 10 7 4 1.20 0.63 10 -7 4 -0.15 0.42 10 -7 4 0.32 0.33 10 -7 4 -0.66 1.25 10 7 4 -0.52 1.18 10 -7 4 0.06 0.39 10 -7 4 0.02 0.45 10 -7 4 0.17 0.36 10 -7 5 6.93 0.66 10 7 5 6.61 2.40 10 -7 5 7.09 0.58 10 7 5 7.21 0.64 10 -7 5 7.59 0.66 10 7 5 6.55 0.77 10 -7 5 6.99 0.61 10 -7 5 8.01 1.49 10 7 5 9.34 1.55 10 -7 5 6.90 0.58 10 -7 5 9.00 0.55 10 -7 5 8.21 0.65 10 -7 5 7.48 0.55 10 -7 6 10.32 0.81 10 7 6 11.84 0.75 10 -7 6 11.36 0.72 10 7 6 11.18 2.47 10 7 6 12.35 0.76 10 7 6 10.32 0.89 10 -7 6 12.19 0.81 10 -7 6 10.75 0.77 10 -7 6 13.18 1.67 10 7 6 13.33 1.70 10 -7 6 10.95 0.80 10 -7 6 11.34 0.71 10 -7 6 12.80 0.69 10 -7 6 11.23 0.73 10 -7 7 0.75 0.51 10 7 7 0.69 0.45 10 7 7 1.46 2.22 -10 -7 -7 0.55 0.55 10 -7 7 0.56 0.42 10 7 7 0.68 0.47 10 -7 7 1.22 0.53 10 7 7 0.83 0.65 -10 7 -7 0.87 0.37 10 -7 7 0.61 0.48 10 7 7 0.48 0.46 10 -7 7 1.15 0.39 10 -7 7 0.38 0.43 10 -7 7 0.66 0.56 10 -7 7 0.92 0.41 10 -7 7 1.11 1.27 10 7 7 0.39 1.33 10 -7 8 49.05 3.50 10 -7 8 58.18 2.66 10 7 8 54.04 2.62 10 -7 8 56.74 2.63 -10 -7 -8 58.72 2.68 10 7 8 54.39 2.63 10 7 8 52.69 2.68 10 -7 8 55.88 2.65 10 -7 8 59.86 2.65 -10 7 -8 55.81 2.59 10 7 8 43.84 4.16 10 -7 8 62.34 2.67 10 -7 8 56.10 2.59 10 7 8 54.89 2.63 10 -7 8 56.92 2.63 10 -7 8 56.96 2.63 10 -7 9 6.53 0.63 10 7 9 7.67 0.65 -10 -7 -9 9.64 0.74 10 7 9 10.78 2.47 10 7 9 6.77 0.74 10 -7 9 9.35 0.72 10 -7 9 7.84 0.73 -10 7 -9 7.94 0.57 10 -7 9 5.23 0.70 10 -7 9 7.13 0.63 10 7 9 6.72 0.62 10 -7 9 7.34 0.65 10 -7 9 4.85 1.57 10 7 10 29.28 3.21 10 7 10 27.75 1.50 -10 -7 -10 29.66 1.54 10 -7 10 29.86 1.47 10 7 10 25.85 1.55 10 -7 10 29.88 1.50 10 -7 10 29.17 1.53 -10 7 -10 30.35 1.43 10 -7 10 26.47 1.53 10 -7 10 30.13 1.51 10 -7 10 32.89 1.50 10 7 10 29.89 1.50 10 -7 10 31.56 2.51 10 7 11 0.96 0.50 10 7 11 1.02 2.07 10 -7 11 0.54 0.49 -10 -7 -11 0.90 0.61 10 7 11 0.61 0.61 10 -7 11 0.96 0.63 -10 7 -11 0.87 0.41 10 -7 11 1.02 0.58 10 7 11 -0.08 0.48 10 -7 11 0.93 0.65 10 -7 11 -0.06 0.51 10 -7 11 0.89 0.55 10 7 12 9.21 0.70 10 -7 12 8.48 0.67 10 7 12 7.77 2.34 -10 -7 -12 8.64 0.76 10 7 12 7.20 0.73 10 -7 12 9.02 0.82 -10 7 -12 8.07 0.60 10 -7 12 7.80 0.72 10 -7 12 8.75 0.68 10 7 12 8.76 0.67 10 -7 12 9.25 0.81 10 -7 12 8.46 0.73 -10 -7 -13 7.40 0.71 10 7 13 6.50 0.68 10 -7 13 8.95 0.78 -10 7 -13 7.87 0.57 10 -7 13 6.25 0.68 10 -7 13 8.58 0.77 10 7 13 7.45 0.66 10 -7 13 8.51 0.73 10 7 14 11.57 0.78 -10 -7 -14 10.84 0.79 10 -7 14 9.94 0.79 10 -7 14 12.73 0.90 -10 7 -14 11.89 0.70 10 -7 14 13.48 0.87 10 7 14 9.93 0.76 10 -7 14 12.42 0.85 -10 7 -15 2.63 0.72 10 -7 15 2.83 0.61 -10 7 -15 2.96 0.41 10 -7 15 2.73 0.63 10 7 15 3.73 0.50 10 -7 15 4.55 0.64 -10 -7 -15 2.94 0.52 10 7 15 2.45 0.51 10 -7 16 12.39 0.96 -10 7 -16 10.28 0.86 10 -7 16 12.25 0.81 10 -7 16 12.48 0.81 -10 7 -16 9.77 0.64 10 -7 16 11.79 0.80 10 7 16 9.35 0.69 10 7 16 10.75 0.72 10 -7 17 3.62 0.70 -10 7 -17 1.91 0.57 -10 7 -17 1.75 0.34 10 -7 17 1.54 0.57 10 -7 17 2.32 0.52 10 -7 17 2.65 0.56 10 7 17 1.80 0.41 10 7 17 1.54 0.42 10 -7 18 3.05 0.63 10 -7 18 3.89 0.58 10 -7 18 4.61 0.53 10 -7 18 3.66 0.50 10 -7 19 -0.08 0.45 10 -7 19 -0.44 0.47 10 -7 19 -0.13 0.43 -10 7 -19 1.00 0.61 -10 7 -20 2.33 0.53 10 -7 20 2.79 0.42 10 7 20 2.55 0.41 -10 7 -21 0.51 0.42 10 -7 21 0.53 0.30 10 7 21 0.67 0.30 10 8 -29 6.59 0.48 10 8 -28 6.60 0.43 10 8 -28 7.10 0.55 -10 -8 28 6.46 0.44 10 8 -28 5.91 0.50 10 8 -28 5.10 0.46 10 8 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16.34 1.03 10 8 -18 16.53 1.81 10 -8 -18 17.73 1.28 10 -8 -18 15.77 1.07 10 8 -18 18.62 0.92 10 -8 -18 14.49 0.92 10 8 -18 16.82 1.26 10 8 -18 16.28 0.85 10 8 -18 16.85 0.88 10 8 -18 16.60 2.41 10 8 -18 17.69 1.86 10 -8 -18 16.29 1.13 10 8 -18 17.05 2.59 10 8 -18 17.71 1.06 10 8 -17 6.93 1.53 10 -8 -17 10.64 1.07 10 -8 -17 8.36 0.85 10 8 -17 12.37 0.69 10 -8 -17 9.99 0.67 10 8 -17 10.19 1.03 10 8 -17 9.66 0.61 10 8 -17 9.78 0.62 10 -8 -17 8.54 0.75 10 -8 -17 11.26 0.92 10 8 -17 11.59 1.69 10 8 -17 14.05 2.52 10 8 -17 13.27 2.34 10 8 -17 10.48 0.85 10 8 -16 30.53 2.34 10 -8 -16 31.06 1.60 10 -8 -16 32.15 1.79 10 8 -16 33.42 1.50 10 -8 -16 30.06 1.50 10 8 -16 29.46 1.74 10 8 -16 28.89 1.45 10 8 -16 29.55 1.44 10 -8 -16 31.75 1.54 10 8 -16 33.91 3.05 10 8 -16 33.04 2.42 10 8 -16 31.35 3.23 10 8 -16 30.87 1.59 10 8 -15 23.15 2.07 10 -8 -15 19.22 1.24 10 -8 -15 21.27 1.44 10 8 -15 24.54 1.13 10 -8 -15 20.14 1.14 10 8 -15 18.96 1.39 10 -8 -15 19.92 1.23 10 8 -15 23.48 1.08 10 8 -15 20.64 1.06 10 -8 -15 20.03 1.19 10 8 -15 24.33 2.74 10 8 -15 23.09 2.08 10 8 -15 28.35 2.96 10 8 -15 23.17 1.25 10 8 -14 170.28 8.65 10 -8 -14 171.94 7.97 10 -8 -14 171.61 8.03 10 8 -14 194.42 7.91 10 -8 -14 177.89 7.95 10 -8 -14 168.00 7.92 10 8 -14 184.51 8.04 10 8 -14 174.79 7.88 10 8 -14 179.21 9.19 10 -8 -14 172.59 7.93 10 8 -14 181.24 8.68 10 8 -14 183.89 9.57 10 8 -14 176.29 7.96 10 -8 -13 6.65 0.45 10 8 -13 7.00 0.71 10 -8 -13 5.52 0.66 10 -8 -13 5.25 0.99 10 -8 -13 6.79 1.14 10 8 -13 7.50 0.54 10 8 -13 6.71 0.87 10 -8 -13 6.35 0.70 10 -8 -13 5.80 0.56 10 8 -13 7.55 0.49 10 -8 -13 6.53 0.67 10 8 -13 5.98 1.47 10 8 -13 8.48 2.06 10 -8 -13 5.93 0.75 10 8 -13 8.18 2.21 10 8 -13 6.46 0.49 10 -8 -12 53.68 2.65 10 8 -12 56.98 2.76 10 -8 -12 59.61 2.75 10 -8 -12 56.91 2.83 10 -8 -12 58.28 2.94 10 -8 -12 56.74 2.87 10 8 -12 71.00 2.70 10 8 -12 58.45 2.70 10 -8 -12 57.67 2.70 10 8 -12 57.26 2.84 10 -8 -12 60.10 2.75 10 8 -12 57.06 2.66 10 8 -12 58.68 3.42 10 -8 -12 62.39 2.77 10 8 -12 56.00 2.75 10 8 -12 57.81 2.67 10 -8 -11 16.58 0.88 10 8 -11 18.02 1.09 10 -8 -11 16.37 1.18 10 -8 -11 15.80 1.00 10 -8 -11 14.51 1.33 10 8 -11 16.82 0.96 10 -8 -11 16.63 0.97 10 8 -11 16.26 1.17 10 -8 -11 16.65 1.04 10 8 -11 19.71 0.91 10 8 -11 16.27 1.73 10 -8 -11 17.11 1.07 10 8 -11 18.72 0.91 10 8 -11 15.59 1.01 10 -8 -10 51.18 2.37 10 8 -10 48.80 2.39 10 -8 -10 48.42 2.28 10 -8 -10 46.37 2.54 10 8 -10 49.03 2.45 10 -8 -10 45.05 2.36 10 -8 -10 51.85 2.45 10 8 -10 48.73 2.34 10 8 -10 48.40 2.45 10 -8 -10 47.68 2.33 10 8 -10 51.77 2.30 10 8 -10 50.30 2.95 10 8 -10 43.37 2.35 10 -8 -9 0.20 0.50 10 -8 -9 -0.06 0.31 10 8 -9 0.37 0.56 10 8 -9 0.35 0.66 10 -8 -9 0.51 0.43 10 -8 -9 0.72 0.90 10 -8 -9 0.78 0.69 10 8 -9 0.59 0.38 10 -8 -9 0.33 0.51 10 8 -9 0.36 0.64 10 -8 -9 -0.06 0.41 10 8 -9 0.54 0.40 10 8 -9 0.63 0.33 10 8 -9 0.50 1.01 10 8 -9 0.32 0.42 10 8 -8 8.74 0.80 10 -8 -8 8.70 0.62 10 -8 -8 8.66 1.00 10 -8 -8 8.40 0.82 10 -8 -8 8.79 0.65 10 8 -8 9.57 0.62 10 8 -8 9.61 0.82 10 -8 -8 9.02 0.62 10 -8 -8 7.92 0.54 10 8 -8 8.13 1.20 10 -8 -8 8.46 0.53 10 8 -8 8.35 0.73 10 -8 -8 8.82 0.68 10 8 -7 9.27 0.81 10 -8 -7 7.81 1.00 10 -8 -7 7.34 0.61 10 -8 -7 8.39 1.02 10 8 -7 8.28 0.79 10 -8 -7 9.16 0.96 10 -8 -7 6.78 0.78 10 -8 -7 7.98 0.62 10 -8 -7 9.86 0.65 10 8 -7 8.93 0.64 10 8 -7 9.39 0.82 10 -8 -7 8.92 0.56 10 8 -7 8.67 1.96 10 8 -7 9.78 0.75 10 -8 -7 9.37 0.57 10 -8 -7 10.54 0.70 10 8 -6 31.66 1.62 10 -8 -6 29.59 1.75 10 -8 -6 28.18 1.73 10 8 -6 32.07 1.62 10 -8 -6 32.73 1.62 10 -8 -6 29.54 1.49 10 -8 -6 31.08 1.60 10 -8 -6 29.62 1.51 10 8 -6 33.79 1.52 10 8 -6 33.09 1.64 10 -8 -6 29.56 1.49 10 8 -6 32.14 1.46 10 8 -6 29.51 2.76 10 8 -6 31.44 1.58 10 -8 -6 29.68 1.47 10 -8 -6 33.55 1.55 10 8 -5 6.66 0.72 10 -8 -5 6.13 0.86 10 8 -5 4.92 0.70 10 -8 -5 6.47 0.93 10 -8 -5 6.36 0.78 10 -8 -5 6.18 0.68 10 -8 -5 6.49 0.54 10 8 -5 7.47 0.56 10 8 -5 4.84 0.72 10 -8 -5 6.87 0.52 10 8 -5 6.62 0.46 10 8 -5 5.06 1.82 10 8 -5 6.54 0.66 10 -8 -5 7.20 0.62 10 -8 -5 6.82 0.49 10 8 -4 43.46 2.38 10 -8 -4 52.45 2.49 10 -8 -4 48.03 2.47 10 8 -4 47.21 2.39 10 -8 -4 45.82 2.37 10 -8 -4 50.89 2.36 10 -8 -4 50.16 2.31 10 8 -4 55.06 2.33 10 -8 -4 52.92 2.30 10 8 -4 50.16 2.27 10 8 -4 43.52 3.41 10 8 -4 49.58 2.36 10 -8 -4 47.70 2.28 10 8 -3 1.13 0.60 10 8 -3 1.42 0.59 10 -8 -3 1.99 0.79 10 -8 -3 1.12 0.80 10 -8 -3 2.16 0.69 10 -8 -3 0.96 0.55 10 -8 -3 2.22 0.42 10 -8 -3 1.87 0.43 10 8 -3 1.85 0.31 10 8 -3 1.61 1.67 10 -8 -3 2.45 0.37 10 8 -3 1.69 0.54 10 8 -2 157.27 6.77 10 -8 -2 153.37 6.81 10 -8 -2 143.34 6.83 10 8 -2 147.60 6.76 10 -8 -2 142.66 6.74 -10 -8 2 139.30 7.39 10 -8 -2 155.78 6.71 10 8 -2 156.58 6.67 10 8 -2 146.90 6.70 10 8 -2 159.78 7.81 10 -8 -2 151.95 6.69 10 -8 -2 141.79 6.68 10 8 -1 1.67 0.60 10 -8 -1 2.54 0.81 10 8 -1 2.17 0.59 10 -8 -1 1.30 0.76 10 -8 -1 1.78 0.55 -10 -8 1 1.91 1.22 10 -8 -1 2.90 0.49 10 8 -1 2.87 0.32 10 8 -1 2.33 0.42 10 8 -1 3.70 1.72 10 -8 -1 2.43 0.39 10 8 0 39.05 1.85 10 8 0 33.93 1.83 10 -8 0 36.16 1.96 10 -8 0 33.38 1.80 10 -8 0 39.58 1.78 10 8 0 37.78 1.70 10 8 0 37.42 1.76 10 8 0 36.58 2.96 10 -8 0 35.10 1.73 10 -8 1 44.33 1.94 10 -8 1 42.14 1.96 10 -8 1 46.36 1.96 10 8 1 41.32 1.91 10 -8 1 38.92 2.16 10 8 1 35.77 2.04 10 8 1 38.34 1.96 10 8 1 39.60 3.26 10 8 1 40.68 2.01 10 -8 2 152.53 6.81 10 -8 2 156.92 6.79 10 8 2 147.85 6.76 10 -8 2 150.71 6.93 10 8 2 157.35 6.82 10 8 2 143.81 7.90 10 8 2 149.89 6.83 10 -8 3 15.39 0.90 10 -8 3 17.09 0.84 10 -8 3 16.40 0.93 10 -8 3 13.80 0.83 10 8 3 14.81 0.76 10 8 3 17.16 2.33 10 8 3 15.74 0.90 10 -8 4 36.73 1.62 10 -8 4 33.17 1.56 -10 8 -4 30.48 1.54 10 -8 4 34.61 1.65 10 -8 4 30.24 1.58 10 -8 4 35.76 1.84 10 8 4 34.90 2.94 10 8 4 32.49 1.61 10 -8 5 12.92 1.11 10 -8 5 11.90 0.74 10 -8 5 14.55 0.85 10 -8 5 14.29 0.77 10 8 5 13.80 0.83 10 -8 5 14.55 0.90 10 8 5 12.45 0.96 -10 8 -5 12.98 0.73 10 -8 5 12.06 0.80 10 -8 6 46.32 2.40 10 -8 6 49.14 2.25 10 -8 6 45.22 2.18 10 -8 6 50.14 2.18 10 8 6 43.30 2.20 -10 8 -6 44.78 2.16 10 8 6 44.20 2.27 10 -8 6 51.03 2.25 10 -8 6 48.28 2.21 10 -8 7 16.89 1.31 10 -8 7 20.87 1.11 10 -8 7 19.52 0.99 10 -8 7 18.10 1.00 10 8 7 19.44 2.92 -10 -8 -7 19.70 1.13 10 8 7 16.25 1.02 10 8 7 15.32 1.12 10 -8 7 18.56 1.10 -10 8 -7 20.01 0.99 10 -8 7 18.27 1.04 10 -8 8 15.41 1.17 10 8 8 12.45 0.94 10 -8 8 15.25 0.93 -10 8 -8 14.26 0.82 10 -8 8 13.08 0.88 10 -8 8 14.67 0.85 10 -8 8 16.87 0.96 10 -8 8 15.07 0.81 -10 -8 -8 15.41 1.00 10 8 8 12.83 0.83 10 -8 9 4.05 0.51 10 -8 9 3.53 0.61 10 8 9 3.01 0.66 -10 8 -9 3.90 0.48 10 -8 9 3.21 0.60 10 -8 9 3.19 0.90 10 8 9 5.11 2.31 -10 -8 -9 3.34 0.70 10 -8 9 4.03 0.45 10 -8 9 3.40 0.65 10 -8 10 27.40 1.41 10 8 10 23.06 1.44 10 -8 10 28.59 1.43 10 -8 10 27.40 1.44 -10 8 -10 28.48 1.36 10 -8 10 30.63 1.64 10 8 10 28.40 3.26 -10 -8 -10 27.71 1.47 10 -8 11 5.09 0.92 -10 8 -11 5.91 0.53 10 -8 11 4.75 0.68 10 -8 11 5.90 0.63 10 8 11 7.56 2.33 -10 -8 -11 6.37 0.74 10 -8 12 10.91 1.03 10 -8 12 12.27 0.85 -10 8 -12 10.21 0.70 10 -8 12 11.68 0.81 10 -8 12 11.97 0.87 -10 -8 -12 10.99 0.83 10 -8 13 26.35 1.65 10 -8 13 27.66 1.50 -10 8 -13 27.25 1.38 10 -8 13 29.63 1.47 10 -8 13 31.92 1.54 -10 -8 -13 27.52 1.48 10 -8 14 45.35 2.26 10 -8 14 46.05 2.14 -10 8 -14 38.43 2.04 10 -8 14 49.21 2.14 10 -8 14 52.21 2.17 -10 -8 -14 41.37 2.11 10 -8 15 10.43 0.96 10 -8 15 10.91 0.81 -10 8 -15 11.64 0.69 10 -8 15 12.47 0.78 10 -8 15 12.78 0.86 -10 -8 -15 11.19 0.78 10 -8 16 12.52 0.94 10 -8 16 12.90 0.81 10 -8 16 13.00 0.85 -10 8 -16 12.02 0.71 -10 -8 -16 11.71 0.76 -10 8 -17 5.03 0.70 10 -8 17 3.29 0.62 -10 8 -17 3.54 0.38 10 -8 17 5.42 0.55 10 -8 17 4.40 0.56 10 -8 17 4.39 0.52 10 -8 18 13.57 0.74 -10 8 -18 11.06 0.88 10 -8 18 8.96 0.75 10 -8 18 11.46 0.75 10 8 18 13.43 0.74 10 -8 18 11.60 0.74 10 8 19 1.88 0.41 -10 8 -19 2.60 0.54 10 -8 19 2.72 0.42 -10 8 -20 -0.58 0.44 10 -8 20 0.71 0.32 10 9 -28 5.11 0.42 10 9 -28 5.81 0.43 10 9 -27 0.62 0.31 10 9 -27 0.82 0.43 -10 -9 27 1.40 0.32 10 9 -27 1.01 0.42 10 9 -27 0.94 0.28 10 9 -26 0.87 0.48 10 9 -26 0.07 0.34 10 9 -26 -0.48 0.49 -10 -9 26 0.36 0.39 -10 -9 26 0.27 0.28 10 9 -26 -0.36 0.37 10 9 -25 0.32 0.35 10 9 -25 0.04 0.58 10 9 -25 0.40 0.60 10 -9 -25 0.06 0.38 -10 -9 25 0.13 0.32 10 9 -25 -0.20 0.43 10 -9 -24 0.85 0.36 10 -9 -24 1.09 0.43 -10 -9 24 0.58 0.37 10 -9 -23 0.35 0.49 10 -9 -23 0.90 0.48 -10 -9 23 0.73 0.41 10 9 -23 0.75 0.69 10 -9 -22 4.58 0.58 -10 -9 22 4.87 0.51 10 -9 -22 5.09 0.59 10 9 -22 4.39 0.82 10 -9 -21 0.77 0.55 -10 -9 21 1.26 0.49 10 -9 -21 1.35 0.56 10 9 -21 1.23 0.50 10 9 -21 1.50 0.78 10 -9 -20 1.56 0.58 -10 -9 20 1.61 0.53 10 9 -20 1.37 0.51 10 -9 -20 1.42 0.58 10 9 -20 1.68 0.82 10 -9 -19 1.47 0.59 10 -9 -19 1.07 0.43 10 9 -19 2.16 0.84 10 9 -19 1.71 0.56 10 -9 -19 1.84 0.62 -10 -9 19 1.71 0.60 -10 -9 18 54.44 2.52 10 -9 -18 49.29 2.52 10 -9 -18 56.55 2.67 10 9 -18 56.66 2.45 10 9 -18 51.36 2.40 10 9 -18 52.64 2.51 10 9 -18 53.34 3.34 10 9 -18 57.63 3.94 10 9 -18 47.30 4.01 10 -9 -18 51.35 2.52 10 -9 -18 50.91 2.45 10 9 -18 55.26 2.64 10 9 -17 3.94 1.32 10 9 -17 2.07 0.83 10 -9 -17 2.53 0.49 10 -9 -17 1.80 0.97 10 -9 -17 2.10 0.59 10 9 -17 2.69 0.47 10 9 -17 2.17 0.37 10 9 -17 2.50 0.37 10 9 -17 3.54 1.34 10 -9 -17 3.21 0.71 10 9 -17 4.02 2.06 10 9 -17 1.94 1.80 10 -9 -17 2.48 0.68 10 9 -17 3.08 0.64 10 9 -16 3.67 1.32 10 -9 -16 3.01 1.00 10 -9 -16 1.83 0.57 10 9 -16 3.47 0.86 10 -9 -16 2.01 0.48 10 9 -16 2.21 0.47 10 9 -16 2.20 0.35 10 9 -16 2.20 0.38 10 9 -16 2.50 1.32 10 9 -16 0.70 1.97 10 9 -16 1.93 1.84 10 -9 -16 2.35 0.63 10 9 -16 1.66 0.62 10 9 -15 7.94 1.54 10 -9 -15 8.20 1.10 10 -9 -15 8.50 0.75 10 9 -15 10.93 0.65 10 9 -15 7.72 0.97 10 9 -15 8.01 0.66 10 -9 -15 7.50 0.80 10 -9 -15 8.07 0.68 10 9 -15 9.21 0.57 10 -9 -15 7.19 0.67 10 9 -15 8.79 1.58 10 9 -15 9.30 2.43 10 9 -15 9.53 2.22 10 9 -15 9.52 0.80 10 -9 -14 8.64 0.56 10 9 -14 9.08 0.81 10 9 -14 10.86 1.59 10 -9 -14 9.50 0.77 10 -9 -14 11.20 1.26 10 9 -14 10.57 0.68 10 9 -14 8.68 0.95 10 9 -14 9.55 0.69 10 -9 -14 10.66 0.72 10 -9 -14 10.99 0.82 10 9 -14 10.07 0.62 10 -9 -14 9.47 0.73 10 9 -14 9.43 1.57 10 9 -14 5.63 2.12 10 9 -14 8.71 2.32 10 9 -14 9.06 0.76 10 -9 -13 35.60 1.73 10 9 -13 37.06 1.87 10 -9 -13 31.19 2.09 10 -9 -13 32.99 1.83 10 9 -13 47.74 1.81 10 9 -13 35.23 1.80 10 -9 -13 35.20 1.88 10 -9 -13 36.78 1.81 10 9 -13 33.92 1.96 10 9 -13 42.49 1.76 10 -9 -13 34.88 1.81 10 9 -13 36.08 3.32 10 9 -13 42.60 2.68 10 9 -13 36.92 1.76 10 9 -13 36.07 1.85 10 -9 -12 27.14 1.41 10 9 -12 30.77 1.56 10 -9 -12 29.88 1.82 10 -9 -12 26.54 1.50 10 -9 -12 30.49 1.56 10 9 -12 29.21 1.49 10 -9 -12 28.23 1.48 10 9 -12 29.80 1.66 10 9 -12 29.82 1.43 10 9 -12 29.86 2.92 10 -9 -12 28.87 1.51 10 9 -12 30.43 2.27 10 9 -12 31.37 1.44 10 -9 -11 11.35 0.66 10 9 -11 10.59 0.88 10 -9 -11 13.25 0.86 10 -9 -11 10.81 1.24 10 9 -11 11.47 1.00 10 -9 -11 9.27 0.74 10 9 -11 11.18 0.78 10 9 -11 10.65 0.95 10 -9 -11 11.76 0.77 10 9 -11 12.20 0.69 10 9 -11 9.03 2.10 10 9 -11 11.85 1.47 10 9 -11 11.95 0.70 10 -9 -10 106.95 5.31 10 9 -10 110.50 5.34 10 -9 -10 113.46 5.41 10 9 -10 114.55 5.26 10 9 -10 111.97 5.34 10 -9 -10 113.23 5.25 10 9 -10 118.25 5.22 10 9 -10 111.53 5.87 10 -9 -10 108.43 5.21 10 9 -10 112.87 5.29 10 -9 -10 123.33 5.29 10 -9 -9 9.60 1.16 10 9 -9 9.60 0.92 10 -9 -9 10.33 0.95 10 9 -9 13.14 0.69 10 9 -9 10.94 0.77 10 9 -9 11.78 0.95 10 -9 -9 12.10 0.76 10 9 -9 11.04 0.68 10 9 -9 11.75 1.44 10 -9 -9 10.74 0.81 10 -9 -9 11.77 0.66 10 9 -9 10.64 0.84 10 -9 -8 111.99 4.87 10 -9 -8 99.06 4.84 10 9 -8 101.17 4.77 10 -9 -8 101.78 4.73 10 9 -8 116.83 4.67 10 9 -8 104.63 4.70 10 9 -8 100.55 4.77 10 -9 -8 100.07 4.69 10 -9 -8 96.33 4.65 10 9 -8 98.77 5.20 10 -9 -8 110.68 4.72 10 -9 -8 100.73 4.65 10 9 -8 103.93 4.73 10 -9 -7 5.11 0.72 10 -9 -7 6.45 0.58 10 9 -7 6.76 0.61 10 9 -7 5.81 0.76 10 -9 -7 5.60 0.49 10 9 -7 5.57 0.74 10 -9 -7 4.95 0.98 10 -9 -7 5.54 0.98 10 -9 -7 6.47 0.49 10 9 -7 6.40 0.67 10 -9 -7 7.15 0.65 10 -9 -6 14.48 1.21 10 -9 -6 13.85 1.19 10 9 -6 13.88 0.99 10 -9 -6 12.87 0.97 10 -9 -6 14.85 0.85 10 9 -6 16.38 0.89 10 9 -6 13.20 1.00 10 -9 -6 13.30 0.81 10 9 -6 15.39 0.79 10 -9 -6 14.06 0.90 10 9 -6 14.84 0.94 10 -9 -6 14.74 0.79 10 9 -6 15.32 0.99 10 9 -5 4.68 0.70 10 9 -5 3.41 0.68 10 -9 -5 4.14 0.90 10 -9 -5 4.45 0.96 10 -9 -5 4.47 0.64 10 -9 -5 4.51 0.52 10 9 -5 5.69 0.57 10 9 -5 4.63 0.71 10 -9 -5 4.92 0.48 10 9 -5 4.89 0.43 10 9 -5 1.90 1.81 10 -9 -5 5.89 0.59 10 -9 -5 5.21 0.46 10 9 -5 4.10 0.63 10 -9 -4 12.41 1.11 10 -9 -4 9.74 1.07 10 9 -4 12.85 0.89 10 9 -4 13.03 0.78 10 -9 -4 10.58 0.74 10 9 -4 12.58 0.68 10 9 -4 11.01 0.90 10 9 -4 12.55 0.84 10 -9 -4 11.33 0.70 10 -9 -3 1.04 0.83 10 9 -3 -0.03 0.58 10 -9 -3 0.62 0.87 10 -9 -3 -0.13 0.45 10 9 -3 0.01 0.32 10 9 -3 0.68 0.62 10 9 -3 0.59 1.77 10 9 -3 0.24 0.56 10 -9 -3 0.47 0.38 10 -9 -2 17.67 1.23 10 9 -2 16.31 1.01 10 -9 -2 15.47 1.16 10 9 -2 16.64 1.04 10 -9 -2 16.73 0.92 10 9 -2 15.75 0.83 10 9 -2 16.98 2.28 10 -9 -2 15.63 0.87 10 -9 -1 6.35 0.95 10 -9 -1 5.90 0.88 10 9 -1 5.79 0.70 -10 -9 1 5.97 1.55 10 -9 -1 7.64 0.57 10 9 -1 6.31 0.75 10 -9 -1 8.15 0.64 10 9 -1 7.77 0.48 10 9 -1 6.02 1.96 10 -9 -1 6.25 0.52 10 -9 0 34.22 1.84 10 9 0 32.40 1.74 10 -9 0 35.03 1.88 10 -9 0 35.61 1.66 -10 -9 0 28.41 2.63 10 9 0 33.95 1.76 10 -9 0 34.66 1.70 10 9 0 35.73 1.60 10 9 0 32.09 1.64 10 9 0 33.43 2.92 10 -9 0 35.08 1.64 10 -9 1 28.32 1.39 10 -9 1 30.24 1.38 10 -9 1 23.86 1.59 10 -9 1 25.66 1.65 10 -9 1 29.51 1.39 -10 -9 -1 26.69 2.48 10 9 1 25.98 1.51 10 -9 1 29.23 1.44 10 9 1 29.10 1.32 10 9 1 24.89 1.38 10 9 1 23.33 2.65 10 9 1 27.25 1.44 10 -9 2 155.86 6.73 10 -9 2 151.46 6.74 10 -9 2 143.97 6.84 10 -9 2 149.52 6.88 -10 -9 -2 130.91 7.75 10 9 2 151.37 6.80 10 9 2 145.39 6.70 10 9 2 156.55 6.75 10 9 2 147.40 7.92 10 9 2 152.36 6.76 10 -9 3 5.05 0.50 10 -9 3 4.27 0.57 10 -9 3 4.53 0.84 10 -9 3 4.75 0.91 -10 9 -3 4.77 0.62 10 9 3 5.11 0.70 10 9 3 4.99 0.38 10 9 3 4.96 0.56 10 9 3 5.91 1.98 10 9 3 4.75 0.56 10 -9 4 98.03 4.21 10 -9 4 98.91 4.17 -10 9 -4 85.54 4.22 10 -9 4 93.87 4.35 -10 9 -4 83.06 4.15 10 -9 4 99.02 4.22 10 9 4 86.87 5.44 10 9 4 92.67 4.21 10 -9 5 14.05 0.76 10 -9 5 11.62 0.81 -10 9 -5 9.71 0.87 10 -9 5 11.05 1.11 -10 9 -5 11.67 0.71 10 -9 5 13.92 0.86 10 -9 5 10.56 0.72 10 9 5 12.66 2.17 10 9 5 11.83 0.78 10 -9 6 11.67 0.80 10 -9 6 11.05 0.68 10 -9 6 11.02 0.71 -10 9 -6 9.56 0.89 10 -9 6 10.54 1.08 -10 9 -6 10.83 0.66 10 -9 6 11.90 0.85 10 -9 6 10.91 0.72 10 9 6 12.13 2.06 -10 -9 -6 11.51 0.89 10 9 6 10.43 0.73 10 -9 7 10.34 1.13 -10 9 -7 12.37 0.72 10 -9 7 12.08 0.90 -10 9 -7 12.51 0.77 10 -9 7 11.37 0.78 -10 9 -7 10.70 0.97 10 -9 7 13.44 0.88 10 -9 7 14.35 0.76 10 -9 7 12.43 0.76 -10 -9 -7 12.69 0.97 10 -9 8 11.85 1.14 -10 9 -8 12.95 0.73 10 -9 8 11.91 0.90 -10 9 -8 13.25 0.77 10 -9 8 12.48 0.81 -10 9 -8 10.88 1.00 10 -9 8 13.45 0.77 10 -9 8 13.02 0.78 10 -9 8 12.10 0.89 -10 -9 -8 13.49 0.97 10 -9 9 11.03 1.12 10 -9 9 11.84 0.77 10 -9 9 13.63 0.90 10 -9 9 12.30 0.75 -10 -9 -9 12.73 0.96 -10 9 -9 11.40 0.71 10 -9 9 13.19 0.88 -10 9 -9 12.28 0.75 10 -9 9 11.03 0.82 10 -9 10 28.03 1.65 10 -9 10 26.24 1.44 -10 9 -10 28.97 1.37 10 -9 10 26.51 1.43 10 -9 10 26.87 1.40 10 -9 10 29.57 1.49 -10 -9 -10 28.51 1.51 -10 9 -11 4.07 0.83 10 -9 11 4.11 0.56 -10 9 -11 4.48 0.48 10 -9 11 3.79 0.57 10 -9 11 5.23 0.89 -10 -9 -11 4.21 0.71 -10 9 -12 28.72 1.59 10 -9 12 28.04 1.41 10 -9 12 26.10 1.44 -10 9 -12 28.58 1.37 10 -9 12 28.63 1.62 -10 -9 -12 28.95 1.48 -10 9 -13 3.01 0.76 10 -9 13 1.96 0.52 10 -9 13 2.22 0.55 -10 9 -13 2.10 0.42 10 -9 13 2.87 0.76 -10 -9 -13 3.33 0.62 10 -9 14 0.94 0.70 -10 9 -14 1.22 0.70 10 -9 14 0.68 0.46 -10 9 -14 0.97 0.38 10 -9 14 0.82 0.49 10 -9 14 0.86 0.56 -10 -9 -14 1.05 0.54 10 -9 15 1.69 0.64 -10 9 -15 0.64 0.69 10 -9 15 2.09 0.46 -10 9 -15 0.75 0.36 10 -9 15 1.20 0.48 -10 -9 -15 1.56 0.48 10 -9 15 1.67 0.55 10 -9 16 14.91 0.81 10 -9 16 11.00 0.84 -10 9 -16 11.30 0.92 -10 -9 -16 10.29 0.73 10 -9 16 12.22 0.77 -10 9 -16 10.50 0.67 10 9 16 13.91 0.81 10 -9 16 15.23 0.77 10 9 17 3.25 0.51 10 -9 17 4.26 0.51 10 -9 17 3.62 0.47 -10 9 -17 2.65 0.33 -10 9 -18 4.27 0.58 10 -9 18 3.61 0.44 10 9 18 4.28 0.46 10 9 19 0.25 0.32 -10 9 -19 0.50 0.45 -10 9 -20 0.56 0.32 -10 -10 27 0.95 0.27 10 10 -27 0.74 0.29 10 10 -27 0.32 0.24 10 10 -27 0.51 0.33 10 10 -26 0.69 0.31 10 10 -26 0.92 0.40 -10 -10 26 1.05 0.33 -10 -10 26 0.58 0.23 10 10 -26 0.22 0.42 10 10 -25 3.15 0.53 -10 -10 25 3.34 0.37 10 -10 -25 3.46 0.39 10 10 -25 3.71 0.39 10 -10 -24 18.63 1.01 10 -10 -24 21.99 1.05 -10 -10 24 23.04 1.03 10 10 -24 21.36 1.15 10 10 -24 17.84 1.02 -10 -10 23 1.88 0.43 10 -10 -23 1.71 0.47 10 10 -23 1.48 0.63 10 10 -23 1.35 0.40 10 -10 -22 17.73 1.02 10 10 -22 19.35 1.15 -10 -10 22 19.77 0.98 10 10 -22 16.38 0.99 10 -10 -21 7.72 0.66 10 10 -21 8.40 0.85 -10 -10 21 8.07 0.63 10 10 -21 6.31 0.61 10 10 -20 0.52 0.73 10 -10 -20 0.27 0.55 10 10 -20 0.35 0.44 -10 -10 20 0.19 0.49 10 10 -20 0.45 0.47 10 -10 -19 7.73 0.72 10 10 -19 7.15 0.89 10 -10 -19 7.92 0.58 10 10 -19 6.56 0.64 10 10 -19 6.73 0.61 -10 -10 19 8.66 0.73 10 -10 -18 1.15 0.44 10 10 -18 1.71 0.74 10 10 -18 1.34 0.50 10 10 -18 1.70 0.44 10 10 -18 1.57 0.31 10 10 -18 1.61 0.50 10 -10 -18 1.55 0.61 -10 -10 18 1.68 0.60 -10 -10 17 3.23 0.67 10 -10 -17 2.94 0.53 10 -10 -17 2.17 0.49 10 10 -17 3.00 0.78 10 10 -17 2.52 0.44 10 10 -17 2.56 0.37 10 10 -17 2.81 0.53 10 10 -17 3.15 0.54 10 -10 -17 2.26 0.66 10 10 -16 24.14 2.08 10 -10 -16 19.90 1.18 10 10 -16 23.96 1.15 10 10 -16 21.26 1.15 10 -10 -16 23.12 1.27 10 -10 -16 21.50 1.16 10 10 -16 23.73 1.38 10 10 -16 21.46 1.09 10 10 -16 24.70 2.04 10 10 -16 20.68 2.46 10 10 -16 22.51 1.19 10 10 -15 15.47 1.82 10 -10 -15 10.92 0.84 10 10 -15 16.26 0.85 10 -10 -15 14.07 1.00 10 10 -15 13.30 0.84 10 -10 -15 13.86 0.88 10 10 -15 12.95 1.10 10 10 -15 15.26 0.79 10 10 -15 13.06 1.69 10 10 -15 12.84 2.23 10 10 -15 14.40 0.91 10 10 -14 36.40 2.67 10 -10 -14 32.20 1.73 10 10 -14 42.83 1.73 10 -10 -14 35.47 1.81 10 10 -14 36.60 1.74 10 -10 -14 35.55 1.74 10 10 -14 36.96 1.91 10 10 -14 36.49 1.68 10 10 -14 42.26 3.21 10 10 -14 34.15 2.52 10 -10 -14 31.87 1.65 10 10 -14 35.73 1.77 10 10 -13 5.18 0.90 10 -10 -13 3.50 1.19 10 10 -13 6.80 0.56 10 10 -13 4.91 0.84 10 -10 -13 3.87 0.59 10 10 -13 4.74 0.57 10 10 -13 5.75 0.47 10 -10 -13 3.76 0.57 10 10 -13 4.08 1.32 10 10 -13 6.01 1.99 10 -10 -13 5.33 0.70 10 -10 -13 4.37 0.42 10 10 -13 4.92 0.67 10 -10 -12 59.24 2.80 10 -10 -12 54.48 2.68 10 10 -12 59.91 2.78 10 -10 -12 57.00 3.00 10 -10 -12 55.65 2.95 10 10 -12 60.43 2.88 10 10 -12 55.94 2.75 10 10 -12 58.82 2.86 10 -10 -12 58.39 2.75 10 10 -12 59.20 2.70 10 10 -12 53.22 4.03 10 -10 -12 53.96 2.74 10 10 -12 56.08 3.44 10 10 -12 59.98 2.70 10 -10 -11 5.22 0.48 10 10 -11 5.44 0.68 10 -10 -11 5.55 0.70 10 10 -11 4.68 0.81 10 -10 -11 5.17 1.10 10 -10 -11 4.59 1.03 10 10 -11 8.30 0.66 10 10 -11 5.28 0.83 10 -10 -11 3.92 0.60 10 10 -11 5.76 0.62 10 10 -11 6.19 0.50 10 10 -11 4.82 1.92 10 10 -11 5.75 1.28 10 10 -11 5.43 0.48 10 10 -10 98.03 4.50 10 -10 -10 95.46 4.59 10 -10 -10 89.66 4.53 10 10 -10 98.04 4.42 10 10 -10 87.65 4.50 10 -10 -10 100.21 4.41 10 10 -10 96.72 4.37 10 10 -10 92.28 5.00 10 10 -10 92.51 5.70 10 -10 -10 97.31 4.44 10 -10 -10 89.58 4.36 10 10 -10 90.17 4.43 10 -10 -9 6.33 1.09 10 10 -9 4.75 0.80 10 -10 -9 4.16 0.71 10 10 -9 5.67 0.50 10 -10 -9 4.92 0.60 10 10 -9 5.27 0.62 10 10 -9 4.91 0.76 10 10 -9 5.47 0.49 10 10 -9 5.00 1.92 10 10 -9 5.77 1.22 10 -10 -9 5.52 0.49 10 10 -9 4.84 0.64 10 -10 -9 5.53 0.68 10 10 -8 129.11 5.17 10 -10 -8 112.92 5.19 10 10 -8 119.93 5.21 10 10 -8 113.75 5.27 10 -10 -8 104.58 5.15 10 -10 -8 113.60 5.33 10 10 -8 110.32 5.27 10 -10 -8 111.33 5.16 10 10 -8 113.95 5.21 10 -10 -8 122.27 5.23 10 10 -7 0.46 0.34 10 -10 -7 0.67 0.49 10 10 -7 1.02 0.52 10 10 -7 -0.08 0.67 10 10 -7 0.24 0.66 10 -10 -7 -0.60 0.98 10 -10 -7 0.60 0.91 10 -10 -7 0.13 0.37 10 10 -7 -0.07 0.58 10 -10 -7 0.27 0.56 10 -10 -7 0.49 0.38 10 -10 -6 29.53 1.50 10 10 -6 31.72 1.54 10 -10 -6 29.33 1.74 10 -10 -6 30.72 1.78 10 10 -6 30.73 1.61 10 10 -6 30.52 1.55 10 -10 -6 29.19 1.46 10 -10 -6 29.03 1.47 10 10 -6 31.58 1.45 10 10 -5 1.99 0.53 10 -10 -5 2.67 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1.92 11 2 -6 9.00 1.84 11 2 -6 10.92 0.68 11 2 -6 10.56 0.69 11 -2 -6 10.89 0.68 11 -2 -5 334.01 14.05 11 2 -5 311.61 14.05 11 2 -5 314.99 14.08 11 2 -5 314.34 14.08 11 -2 -5 310.35 14.08 11 2 -5 310.96 14.07 11 2 -5 317.65 14.52 11 -2 -5 332.62 14.90 11 2 -5 323.62 14.90 11 2 -4 11.64 0.65 11 2 -4 11.19 0.74 11 -2 -4 11.37 0.73 11 2 -4 14.35 0.80 11 2 -4 10.78 0.69 11 -2 -4 11.26 1.23 11 2 -4 11.64 1.27 11 -2 -4 11.87 1.79 11 2 -3 275.83 12.90 11 2 -3 324.48 12.96 11 2 -3 283.46 12.93 11 -2 -3 281.09 12.93 11 2 -3 303.62 12.92 11 -2 -3 290.73 12.92 11 2 -3 294.50 13.74 11 2 -3 293.86 13.34 11 -2 -3 286.81 13.39 11 -2 -3 299.42 13.72 11 2 -3 309.25 13.75 11 -2 -2 5.84 1.55 11 2 -2 3.98 1.53 11 2 -2 5.94 0.59 11 2 -2 5.81 0.98 11 2 -2 4.97 0.46 11 -2 -2 4.30 0.46 11 -2 -2 5.20 1.13 11 -2 -2 5.34 0.49 11 2 -2 4.93 0.50 11 2 -2 5.35 1.58 11 -2 -2 5.18 0.49 11 2 -2 5.56 0.49 11 -2 -1 118.20 5.75 11 2 -1 116.03 5.79 11 2 -1 123.62 5.86 11 2 -1 113.59 4.86 11 -2 -1 104.81 4.85 11 -2 -1 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33.09 1.64 11 3 -5 33.49 2.26 11 -3 -5 33.33 2.58 11 3 -5 37.08 2.64 11 3 -5 34.43 1.67 11 -3 -4 14.33 0.82 11 3 -4 17.21 0.90 11 -3 -4 16.45 0.89 11 3 -4 17.49 0.97 11 3 -4 16.19 0.79 11 3 -4 16.26 0.87 11 -3 -4 14.89 1.25 11 3 -4 19.34 1.61 11 -3 -4 17.73 2.02 11 3 -4 18.91 2.08 11 -3 -3 60.56 2.81 11 -3 -3 64.40 2.85 11 3 -3 67.07 2.86 11 -3 -3 57.03 2.79 11 3 -3 63.55 2.79 11 3 -3 65.10 2.85 11 3 -3 62.51 3.39 11 -3 -3 60.35 3.26 11 -3 -3 67.78 3.74 11 3 -3 62.33 3.77 11 -3 -2 7.02 1.57 11 3 -2 5.99 1.66 11 3 -2 6.33 1.78 11 -3 -2 7.05 0.54 11 3 -2 5.59 0.54 11 3 -2 6.67 0.52 11 -3 -2 6.38 1.08 11 3 -2 7.46 1.17 11 -3 -2 7.25 0.43 11 -3 -2 7.80 0.56 11 3 -2 6.92 0.56 11 -3 -2 6.16 0.49 11 -3 -2 6.83 0.45 11 -3 -1 85.39 4.49 11 3 -1 91.76 4.58 11 3 -1 79.80 3.63 11 -3 -1 82.97 3.63 11 3 -1 85.86 3.63 11 -3 -1 73.99 3.61 11 3 -1 83.61 4.77 11 -3 -1 77.96 4.17 11 3 -1 84.50 4.18 11 -3 -1 80.92 3.58 11 -3 -1 71.67 3.60 11 -3 -1 80.63 3.63 11 3 -1 83.25 3.63 11 -3 0 42.49 2.86 11 3 0 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2.91 0.52 12 -2 -1 3.74 0.35 12 -2 -1 3.63 0.37 12 -2 -1 4.32 0.52 12 2 -1 4.25 0.40 12 2 -1 3.53 0.52 12 -2 -1 3.97 0.48 12 2 -1 3.62 0.50 12 2 -1 4.18 0.60 12 2 -1 2.97 0.85 12 2 -1 4.15 0.48 12 2 -1 3.34 1.65 12 -2 -1 4.26 0.47 12 -2 -1 4.48 1.21 12 -2 -1 3.87 0.42 12 -2 -1 5.61 1.67 12 2 -1 4.02 1.65 12 -2 0 7.54 0.55 12 -2 0 6.85 1.74 12 2 0 8.65 1.78 12 -2 0 7.59 0.62 12 2 0 8.05 0.64 12 2 0 8.05 0.64 12 -2 0 7.51 0.63 12 2 0 8.19 0.52 12 2 0 8.04 1.01 12 2 0 8.16 0.59 12 -2 0 7.66 0.59 12 -2 0 8.42 1.43 12 2 0 5.92 1.73 12 2 0 7.64 0.62 12 -2 0 8.17 0.63 12 -2 0 7.04 0.58 12 -2 0 8.53 0.68 12 2 0 9.40 0.66 12 -2 0 8.12 0.48 12 -2 0 7.73 0.49 12 -2 1 3.25 0.45 12 -2 1 2.82 1.58 12 2 1 2.19 1.62 12 -2 1 2.55 0.34 12 -2 1 2.60 0.56 12 2 1 3.17 0.53 12 -2 1 2.90 0.31 12 2 1 3.32 0.47 12 2 1 3.28 0.53 12 -2 1 3.28 0.53 12 2 1 3.66 0.37 12 2 1 3.65 0.52 12 2 1 1.84 0.81 12 -2 1 1.65 1.27 12 -2 1 3.07 0.45 12 2 1 1.23 1.63 12 2 1 3.25 0.52 12 -2 1 3.28 0.52 12 -2 1 3.20 0.47 12 -2 2 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37.77 1.71 12 -7 -14 34.40 1.73 12 -7 -14 33.91 1.79 12 7 -14 36.22 1.98 12 7 -14 36.68 1.72 12 -7 -14 36.25 1.84 12 7 -14 37.52 3.13 12 -7 -14 35.75 1.85 12 7 -14 35.68 1.75 12 7 -14 35.08 1.87 12 7 -13 12.59 0.94 12 -7 -13 11.17 0.80 12 -7 -13 8.87 1.09 12 -7 -13 10.92 0.89 12 -7 -13 9.65 1.05 12 7 -13 11.59 0.64 12 -7 -13 12.32 1.13 12 -7 -13 10.59 0.92 12 -7 -13 11.58 0.69 12 -7 -13 9.85 0.76 12 7 -13 11.49 1.01 12 7 -13 12.78 0.68 12 -7 -13 11.77 0.90 12 -7 -13 11.45 0.89 12 7 -13 13.11 2.07 12 7 -13 11.43 0.73 12 7 -13 11.24 0.89 12 -7 -12 396.09 18.95 12 7 -12 457.54 19.05 12 7 -12 423.83 19.01 12 -7 -12 426.26 19.00 12 -7 -12 450.81 19.02 12 -7 -12 422.33 19.06 12 -7 -12 441.66 19.08 12 -7 -12 436.66 19.02 12 -7 -12 428.01 19.02 12 -7 -12 434.01 18.99 12 -7 -12 401.60 19.01 12 7 -12 436.95 19.11 12 7 -12 441.04 18.97 12 7 -12 426.94 20.14 12 -7 -12 450.65 19.04 12 7 -12 433.06 19.06 12 7 -12 435.54 18.99 12 -7 -11 11.41 0.77 12 -7 -11 11.64 0.62 12 7 -11 11.28 0.91 12 7 -11 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0.34 1.55 12 7 -9 0.89 0.39 12 7 -9 0.36 0.51 12 -7 -8 10.80 0.69 12 7 -8 8.07 0.82 12 -7 -8 10.06 0.57 12 -7 -8 8.96 0.67 12 7 -8 8.60 1.75 12 -7 -8 10.59 1.77 12 7 -8 8.64 0.86 12 -7 -8 10.25 1.10 12 -7 -8 9.97 0.73 12 -7 -8 11.58 1.06 12 -7 -8 9.78 0.65 12 7 -8 9.22 0.86 12 -7 -8 8.58 0.92 12 -7 -8 10.84 0.75 12 -7 -8 8.19 0.73 12 -7 -8 10.25 0.65 12 -7 -8 9.93 0.64 12 7 -8 9.34 0.89 12 7 -8 10.22 1.83 12 7 -8 10.74 0.75 12 7 -8 11.20 0.65 12 7 -7 7.69 0.76 12 -7 -7 7.46 0.61 12 -7 -7 7.83 0.48 12 -7 -7 5.05 0.56 12 -7 -7 5.15 1.57 12 7 -7 6.83 0.79 12 7 -7 5.68 1.63 12 -7 -7 6.97 0.65 12 -7 -7 5.86 0.54 12 -7 -7 6.30 0.98 12 -7 -7 5.63 0.95 12 7 -7 7.40 0.79 12 -7 -7 5.62 0.80 12 -7 -7 6.10 0.66 12 -7 -7 5.29 0.59 12 -7 -7 5.71 0.54 12 -7 -7 7.33 0.53 12 7 -7 7.45 0.81 12 7 -7 7.98 0.49 12 7 -7 4.01 1.59 12 7 -7 6.14 0.61 12 7 -6 50.11 2.47 12 -7 -6 54.42 2.35 12 -7 -6 49.17 2.38 12 7 -6 52.48 2.50 12 7 -6 46.94 3.34 12 -7 -6 49.18 3.26 12 -7 -6 54.95 2.43 12 -7 -6 53.93 2.60 12 -7 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-3 -0.18 1.38 12 7 -3 -0.47 1.48 12 7 -3 0.66 0.66 12 -7 -3 1.30 0.82 12 7 -3 0.45 0.64 12 -7 -3 -0.01 0.63 12 -7 -3 1.12 0.42 12 -7 -3 0.56 0.47 12 -7 -3 0.60 0.38 12 -7 -3 0.49 0.47 12 7 -3 0.63 0.30 12 7 -3 1.04 0.48 12 7 -3 0.11 1.57 12 7 -3 0.53 0.43 12 -7 -2 21.77 1.07 12 -7 -2 20.55 1.09 12 -7 -2 20.16 1.10 12 7 -2 22.02 1.27 12 -7 -2 17.90 1.97 12 7 -2 20.20 2.10 12 -7 -2 19.67 1.09 12 7 -2 23.48 1.25 12 -7 -2 19.66 1.24 12 -7 -2 20.47 1.10 12 -7 -2 22.99 1.09 12 7 -2 22.34 1.04 12 -7 -2 21.53 1.14 12 7 -2 21.49 1.14 12 7 -2 21.81 2.29 12 7 -2 22.55 1.14 12 7 -2 21.27 1.18 12 -7 -1 8.65 0.57 12 -7 -1 7.99 0.60 12 -7 -1 6.98 0.60 12 7 -1 8.86 0.81 12 -7 -1 6.59 1.00 12 -7 -1 7.65 0.78 12 -7 -1 7.33 0.61 12 -7 -1 9.26 1.63 12 7 -1 7.47 1.70 12 7 -1 6.54 0.79 12 7 -1 8.71 0.51 12 -7 -1 7.89 0.67 12 7 -1 7.64 0.64 12 7 -1 7.77 1.75 12 7 -1 6.87 0.61 12 7 -1 8.12 0.70 12 -7 0 283.50 12.47 12 -7 0 262.73 12.47 12 -7 0 296.06 12.60 12 -7 0 275.57 12.46 12 -7 0 279.04 12.52 12 -7 0 255.45 13.25 12 7 0 244.03 13.25 12 7 0 282.72 12.43 12 -7 0 298.00 12.49 12 7 0 286.03 12.49 12 7 0 271.55 13.44 12 7 0 282.09 12.51 12 -7 1 10.87 0.71 12 -7 1 8.83 0.69 12 -7 1 9.10 1.06 12 -7 1 9.25 0.84 12 -7 1 9.40 1.66 12 7 1 11.46 1.75 12 7 1 9.62 0.92 12 7 1 10.21 0.56 12 7 1 9.75 0.75 12 7 1 6.69 1.78 12 7 1 11.34 0.77 12 -7 2 65.33 2.96 12 -7 2 70.50 3.00 12 -7 2 60.40 2.98 12 7 2 60.36 2.99 12 -7 2 68.34 3.19 12 -7 2 64.06 3.06 12 -7 2 55.40 3.82 12 7 2 60.05 3.95 12 7 2 65.90 3.10 12 -7 2 72.59 3.02 12 7 2 61.83 2.91 12 7 2 67.82 3.02 12 7 2 60.22 4.04 12 7 2 66.89 3.02 12 -7 3 13.82 0.83 12 7 3 9.95 0.81 12 -7 3 14.14 0.76 12 -7 3 11.55 0.79 12 -7 3 13.27 1.19 12 -7 3 11.22 0.93 12 -7 3 10.70 1.77 12 7 3 6.79 1.72 12 7 3 12.01 1.02 12 -7 3 14.88 0.87 12 7 3 13.27 0.86 12 7 3 10.54 1.93 12 7 3 10.96 0.80 12 7 3 12.97 0.85 12 -7 4 93.38 3.86 12 -7 4 90.61 3.91 12 -7 4 83.64 3.88 12 7 4 83.31 3.89 12 -7 4 92.31 4.07 12 -7 4 84.82 3.94 12 7 4 81.89 3.89 12 -7 4 81.00 3.85 12 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1.58 12 -7 12 22.37 1.32 12 7 12 24.32 1.32 12 -7 12 27.42 1.31 12 7 12 19.81 1.30 12 -7 12 24.04 1.34 12 7 12 29.49 1.39 12 7 12 24.63 1.28 12 7 13 3.19 0.49 12 -7 13 3.00 0.61 12 -7 13 3.81 0.88 12 7 13 3.10 0.59 12 -7 13 3.01 0.56 12 -7 13 2.92 0.55 12 -7 13 3.45 0.62 12 7 13 3.26 0.64 12 7 13 3.31 0.52 12 7 14 8.13 0.65 12 -7 14 10.96 0.76 12 -7 14 9.60 0.97 12 -7 14 10.30 0.71 12 -7 14 10.75 0.73 12 7 14 12.36 0.79 12 7 14 8.94 0.66 12 -7 15 1.79 0.54 12 -7 15 1.02 0.49 12 -7 15 0.82 0.68 12 7 15 0.87 0.55 12 7 15 0.93 0.40 -12 7 -15 0.73 0.55 12 -7 16 8.06 0.61 12 -7 16 8.21 0.79 -12 7 -17 2.25 0.55 12 -7 17 2.07 0.44 12 -7 17 1.91 0.57 12 -7 18 3.38 0.50 -12 7 -18 4.29 0.52 12 7 19 5.30 0.39 -12 7 -19 3.60 0.44 12 8 -28 1.63 0.28 12 8 -28 2.14 0.40 -12 -8 28 1.18 0.27 12 8 -27 2.05 0.51 12 8 -27 1.24 0.41 12 8 -27 1.22 0.36 -12 -8 27 1.47 0.36 12 8 -26 5.49 0.66 12 -8 -26 5.57 0.51 12 8 -26 5.20 0.57 12 8 -26 5.20 0.52 12 -8 -25 3.46 0.52 12 -8 -25 3.34 0.38 12 8 -25 3.77 0.61 12 8 -25 3.78 0.70 12 8 -25 3.90 0.44 -12 -8 25 3.30 0.35 12 8 -25 3.14 0.53 12 8 -24 2.95 0.67 12 -8 -24 3.50 0.55 12 -8 -24 2.89 0.42 12 8 -24 2.88 0.71 12 8 -24 3.56 0.46 -12 -8 24 3.07 0.39 12 8 -24 3.31 0.57 12 8 -23 1.43 0.42 12 8 -23 0.50 0.77 12 8 -23 0.85 0.66 12 -8 -23 0.75 0.55 12 -8 -23 0.73 0.45 12 8 -23 1.03 0.56 12 8 -22 11.01 0.77 12 -8 -22 10.74 0.82 12 -8 -22 11.21 0.75 12 8 -22 11.13 0.92 12 8 -22 11.68 0.69 -12 -8 22 10.25 0.67 12 8 -22 11.05 1.01 12 -8 -22 10.55 0.71 12 -8 -22 10.28 0.85 12 8 -22 10.08 0.83 12 -8 -21 3.38 0.52 12 8 -21 2.86 0.61 12 8 -21 2.41 0.79 12 -8 -21 3.20 0.64 12 8 -21 4.51 0.50 -12 -8 21 3.52 0.49 12 8 -21 3.57 0.87 12 -8 -21 3.90 0.72 12 8 -21 2.98 0.66 12 -8 -20 69.44 3.19 12 8 -20 70.17 3.25 12 8 -20 70.97 3.10 -12 -8 20 61.94 3.12 12 8 -20 65.82 3.18 12 8 -20 69.00 3.16 12 -8 -20 66.31 3.13 12 8 -20 70.10 3.29 12 8 -19 3.53 0.88 12 -8 -19 2.45 0.86 12 -8 -19 1.67 0.66 -12 -8 19 2.78 0.57 12 8 -19 2.50 0.68 12 -8 -19 3.17 0.58 12 8 -19 2.24 0.65 12 -8 -18 3.60 0.58 12 8 -18 3.86 0.71 12 -8 -18 5.37 0.94 12 -8 -18 4.78 0.71 12 -8 -18 3.54 0.63 12 8 -18 3.96 0.71 12 8 -18 4.35 0.88 12 8 -17 5.48 0.77 12 -8 -17 4.85 0.47 12 8 -17 6.24 0.95 12 -8 -17 5.34 0.54 12 -8 -17 6.08 0.65 12 -8 -17 4.94 0.95 12 -8 -17 6.03 0.71 12 -8 -17 6.26 0.69 12 -8 -17 7.06 0.81 12 8 -17 5.81 0.73 12 -8 -16 40.68 1.97 12 8 -16 41.96 2.03 12 -8 -16 38.60 1.89 12 -8 -16 36.50 1.92 12 8 -16 42.30 2.14 12 -8 -16 41.02 2.01 12 -8 -16 40.09 2.15 12 8 -16 40.07 1.88 12 -8 -16 42.66 1.98 12 -8 -16 41.20 2.03 12 8 -16 42.08 2.02 12 -8 -15 3.16 0.59 12 8 -15 1.60 0.72 12 -8 -15 2.65 0.65 12 -8 -15 3.19 0.96 12 8 -15 2.56 0.87 12 -8 -15 2.14 0.41 12 8 -15 2.46 0.39 12 8 -15 3.34 0.41 12 -8 -15 1.61 0.66 12 -8 -15 2.92 0.72 12 8 -15 2.05 0.45 12 8 -15 2.65 0.67 12 -8 -14 21.12 1.20 12 8 -14 21.51 1.25 12 -8 -14 19.46 1.22 12 -8 -14 20.64 1.45 12 8 -14 19.91 1.37 12 8 -14 21.76 1.06 12 -8 -14 21.78 1.10 12 8 -14 21.72 1.37 12 8 -14 21.69 1.08 12 -8 -14 21.39 1.23 12 -8 -14 23.30 1.26 12 8 -14 23.42 2.54 12 8 -14 21.97 1.10 12 8 -14 19.64 1.23 12 -8 -13 3.10 0.60 12 -8 -13 2.99 0.31 12 8 -13 2.28 0.73 12 8 -13 2.90 0.83 12 -8 -13 3.27 0.99 12 -8 -13 3.55 0.63 12 -8 -13 2.38 0.91 12 8 -13 3.30 0.37 12 8 -13 3.15 0.42 12 8 -13 2.61 0.44 12 8 -13 3.43 0.64 12 -8 -13 3.25 0.70 12 -8 -13 3.12 0.67 12 8 -13 4.70 1.98 12 8 -13 4.24 0.87 12 -8 -13 3.24 0.46 12 -8 -12 141.65 6.61 12 8 -12 153.23 6.72 12 -8 -12 149.62 6.68 12 -8 -12 152.89 6.76 12 -8 -12 145.26 6.70 12 -8 -12 151.36 6.84 12 8 -12 156.79 6.77 12 -8 -12 153.04 6.65 12 8 -12 149.20 6.78 12 8 -12 151.72 6.63 12 8 -12 141.50 7.88 12 8 -12 146.57 6.71 12 8 -12 144.23 6.64 12 -8 -11 28.82 1.55 12 -8 -11 31.38 1.44 12 8 -11 30.25 1.61 12 -8 -11 28.65 1.85 12 -8 -11 25.92 1.56 12 8 -11 27.96 1.69 12 -8 -11 26.86 1.69 12 -8 -11 30.44 1.49 12 8 -11 28.86 1.71 12 8 -11 33.98 1.47 12 8 -11 28.17 2.85 12 8 -11 26.82 1.56 12 8 -11 34.29 1.49 12 -8 -10 34.02 1.73 12 -8 -10 34.61 1.63 12 8 -10 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2.27 0.50 12 -8 -3 2.56 0.41 12 8 -3 2.30 0.66 12 -8 -2 171.27 7.30 12 -8 -2 152.29 7.30 12 8 -2 164.25 7.39 12 -8 -2 169.74 7.47 12 -8 -2 165.83 7.45 12 8 -2 163.50 7.40 12 -8 -2 157.35 7.37 12 -8 -2 166.90 7.31 12 8 -2 170.15 7.28 12 -8 -2 163.92 7.33 12 8 -2 155.60 7.33 12 8 -2 149.89 8.40 12 8 -2 162.99 7.36 12 -8 -1 2.39 0.44 12 -8 -1 1.89 0.43 12 8 -1 1.44 0.72 12 8 -1 2.97 0.69 12 -8 -1 2.08 0.86 12 -8 -1 1.99 0.92 12 -8 -1 1.54 0.64 12 -8 -1 2.21 0.46 12 -8 -1 2.62 0.55 12 8 -1 2.76 0.35 12 8 -1 2.76 0.50 12 8 -1 3.86 1.78 12 8 -1 3.06 0.61 12 -8 0 193.64 8.78 12 -8 0 193.92 8.92 12 -8 0 187.85 8.82 12 8 0 195.92 8.86 12 8 0 197.62 8.73 12 -8 0 201.11 8.80 12 8 0 198.93 8.80 12 8 0 188.20 9.85 12 8 0 202.83 8.82 12 -8 1 37.29 1.68 12 -8 1 33.86 1.95 12 -8 1 28.00 1.75 12 8 1 34.58 1.81 12 8 1 33.70 1.59 12 8 1 33.98 1.70 12 8 1 30.72 2.94 12 8 1 38.23 1.74 12 -8 2 30.10 1.42 12 -8 2 31.83 1.47 12 -8 2 25.69 1.53 12 -8 2 28.86 1.74 12 8 2 27.30 1.34 12 8 2 30.51 1.48 12 8 2 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4.52 0.51 14 6 -14 4.66 0.77 14 -6 -14 4.90 0.62 14 -6 -14 4.16 0.73 14 -6 -14 5.29 1.05 14 -6 -14 4.40 0.79 14 6 -14 4.07 0.43 14 6 -14 3.76 0.83 14 -6 -14 5.34 1.11 14 -6 -14 4.07 0.92 14 -6 -14 4.01 0.72 14 6 -14 3.18 0.60 14 -6 -14 5.19 0.62 14 -6 -14 4.37 0.81 14 -6 -14 4.17 0.65 14 6 -14 4.20 1.86 14 6 -14 3.07 0.58 14 6 -14 3.66 0.76 14 -6 -13 21.51 1.13 14 6 -13 23.45 1.32 14 6 -13 20.11 1.24 14 -6 -13 21.90 1.21 14 -6 -13 22.49 1.24 14 -6 -13 22.15 1.28 14 -6 -13 19.83 1.47 14 6 -13 22.21 1.07 14 -6 -13 23.11 1.18 14 6 -13 19.16 1.18 14 -6 -13 22.30 1.57 14 -6 -13 20.62 1.29 14 6 -13 20.15 1.36 14 6 -13 18.22 1.19 14 -6 -13 20.89 1.19 14 -6 -13 21.13 1.05 14 -6 -13 21.72 1.31 14 -6 -13 21.44 1.22 14 6 -13 20.82 2.52 14 6 -13 20.57 1.28 14 6 -13 22.35 1.17 14 -6 -12 438.88 18.71 14 6 -12 429.75 18.76 14 6 -12 420.76 18.73 14 -6 -12 419.41 18.72 14 -6 -12 427.07 18.81 14 -6 -12 430.04 18.74 14 6 -12 419.76 18.67 14 -6 -12 427.94 18.71 14 -6 -12 426.19 18.73 14 -6 -12 424.49 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14 -6 -5 10.12 0.72 14 -6 -5 9.42 0.95 14 -6 -5 9.13 0.71 14 -6 -5 7.77 1.94 14 6 -5 8.02 2.01 14 6 -5 8.75 0.59 14 6 -5 10.51 0.77 14 6 -5 8.52 1.68 14 6 -5 10.47 0.78 14 -6 -5 9.69 0.95 14 6 -5 11.14 0.70 14 6 -4 249.52 11.20 14 -6 -4 253.21 11.12 14 6 -4 236.83 11.17 14 -6 -4 233.61 11.16 14 -6 -4 246.37 11.23 14 -6 -4 245.86 11.15 14 -6 -4 256.46 11.15 14 -6 -4 253.32 11.12 14 -6 -4 259.14 11.28 14 -6 -4 244.41 11.16 14 6 -4 260.28 11.24 14 -6 -4 225.14 12.09 14 6 -4 234.95 12.21 14 6 -4 237.36 11.18 14 6 -4 226.00 12.00 14 6 -4 258.71 11.19 14 -6 -4 248.38 11.21 14 6 -4 272.41 11.16 14 6 -4 264.93 11.20 14 6 -3 2.30 0.71 14 -6 -3 3.33 0.41 14 6 -3 3.24 0.60 14 -6 -3 2.31 0.56 14 -6 -3 2.50 0.40 14 -6 -3 2.40 0.75 14 -6 -3 3.37 0.54 14 -6 -3 2.76 0.47 14 -6 -3 4.26 0.96 14 6 -3 3.46 0.75 14 -6 -3 3.09 1.64 14 6 -3 2.34 1.63 14 6 -3 2.59 0.76 14 6 -3 4.38 1.49 14 6 -3 2.28 0.60 14 6 -3 4.40 0.65 14 6 -3 2.68 0.59 14 -6 -3 3.60 0.77 14 6 -3 3.95 0.51 14 -6 -2 92.77 4.13 14 6 -2 89.18 4.19 14 -6 -2 88.07 4.18 14 -6 -2 94.48 4.15 14 -6 -2 90.20 4.26 14 -6 -2 93.60 4.33 14 -6 -2 87.77 4.15 14 6 -2 89.24 4.26 14 -6 -2 87.17 5.20 14 6 -2 84.91 5.31 14 6 -2 91.31 4.20 14 6 -2 88.33 5.09 14 6 -2 89.71 4.20 14 -6 -2 85.87 4.22 14 6 -2 102.79 4.17 14 6 -2 94.04 4.21 14 -6 -1 30.10 1.33 14 6 -1 22.94 1.41 14 -6 -1 24.07 1.40 14 -6 -1 24.19 1.65 14 -6 -1 24.63 1.53 14 -6 -1 24.92 1.34 14 -6 -1 22.87 2.54 14 6 -1 21.36 2.56 14 6 -1 28.62 1.55 14 6 -1 25.82 1.42 14 6 -1 26.51 2.38 14 6 -1 25.01 1.42 14 6 -1 31.48 1.38 14 6 -1 28.62 1.45 14 6 0 228.42 9.31 14 6 0 208.71 9.35 14 -6 0 201.25 9.29 14 6 0 194.69 9.33 14 -6 0 212.63 9.38 14 -6 0 180.66 10.28 14 6 0 185.61 10.35 14 6 0 218.22 9.39 14 6 0 205.42 9.40 14 6 0 209.93 9.34 14 6 0 188.70 10.12 14 -6 0 220.35 9.29 14 -6 0 211.95 9.32 14 -6 0 198.59 9.33 14 6 0 200.08 9.34 14 6 1 11.68 0.71 14 6 1 8.58 0.80 14 6 1 7.41 0.76 14 -6 1 7.55 0.92 14 -6 1 6.31 1.81 14 6 1 6.57 1.96 14 6 1 9.64 1.02 14 6 1 8.76 1.64 14 6 1 9.59 0.80 14 -6 1 10.56 0.67 14 -6 1 7.67 0.76 14 -6 1 9.13 0.75 14 6 1 9.04 0.77 14 6 2 216.87 8.75 14 6 2 197.19 8.79 14 -6 2 195.94 8.81 14 6 2 177.10 8.77 14 -6 2 182.32 9.80 14 6 2 184.41 9.86 14 6 2 193.51 8.85 14 6 2 208.60 8.79 14 -6 2 197.30 8.76 14 -6 2 191.41 8.76 14 6 2 184.73 8.76 14 6 3 0.39 0.62 14 6 3 0.45 0.46 14 -6 3 0.32 0.72 14 6 3 0.71 0.61 14 -6 3 4.13 1.70 14 6 3 1.61 1.73 14 6 3 0.46 0.88 14 6 3 0.30 0.65 14 -6 3 1.20 0.57 14 6 3 0.61 0.62 14 -6 3 0.36 0.59 14 -6 4 155.60 6.85 14 -6 4 155.97 6.88 14 6 4 148.39 6.86 14 -6 4 155.21 7.01 14 -6 4 142.33 6.91 14 6 4 149.65 6.87 14 -6 4 137.51 6.82 14 -6 4 147.18 7.93 14 6 4 131.03 7.93 14 6 4 150.69 6.94 14 6 4 169.80 6.89 14 6 4 141.99 6.86 14 6 4 168.48 6.83 14 6 4 160.09 6.88 14 -6 5 2.93 0.62 14 6 5 2.54 0.65 14 -6 5 2.73 0.68 14 -6 5 1.81 1.01 14 -6 5 3.07 0.78 14 6 5 2.14 0.61 14 -6 5 0.12 1.65 14 6 5 3.14 1.80 14 -6 5 2.28 0.49 14 6 5 2.08 0.85 14 6 5 2.67 0.72 14 6 5 1.56 0.62 14 6 5 2.72 0.47 14 6 5 1.84 0.61 14 -6 6 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-9 7.69 0.49 24 4 -9 6.89 0.52 24 4 -9 8.70 0.62 24 -4 -8 0.16 0.52 24 4 -8 0.70 0.30 24 4 -8 0.96 0.35 24 4 -8 0.28 0.42 24 -4 -7 0.79 0.51 24 4 -7 0.40 0.29 24 4 -7 0.67 0.35 24 4 -7 1.07 0.41 24 -4 -6 1.79 0.45 24 4 -6 1.41 0.34 24 4 -6 2.27 0.40 24 -4 -5 -0.01 0.43 24 -4 -4 0.84 0.38 24 -4 -3 -0.17 0.37 24 5 -14 1.65 0.38 24 5 -13 0.95 0.41 24 5 -11 0.95 0.28 24 5 -11 2.30 0.45 24 -5 -10 0.88 0.48 24 5 -10 -0.13 0.40 24 -5 -9 -0.21 0.42 24 5 -9 -0.31 0.40 24 -5 -8 2.22 0.43 24 5 -8 3.01 0.43 24 -5 -7 0.30 0.44 24 5 -7 0.26 0.37 24 -5 -6 0.96 0.41 24 -5 -5 -0.01 0.34 24 6 -10 0.56 0.33 24 6 -9 0.77 0.35 0 0 0 0.00 0.00 TITL tx2347c in P2(1)/m REM P2(1)/m (#11 in standard setting) CELL 1.54184 20.067776 15.891072 25.604748 90.0000 108.9622 90.0000 ZERR 34.00 0.000122 0.000084 0.000169 0.0000 0.0007 0.0000 LATT 1 SYMM -x, y+1/2,-z SFAC C H N O UNIT 374.00 340.00 34.00 34.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 61809 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3 3 29 0.52 0.17 4 3 29 -0.18 0.22 -18 4 29 0.12 0.01 -17 4 29 0.76 0.59 1 4 29 -0.19 0.26 2 4 29 0.51 -0.05 3 4 29 -0.33 -0.88 4 4 29 0.19 -0.17 -18 5 29 0.41 -0.10 -17 5 29 0.09 0.37 -16 5 29 0.27 0.15 1 5 29 0.20 -0.31 2 5 29 -0.26 0.25 3 5 29 -0.83 0.16 -17 6 29 0.38 0.16 -16 6 29 -0.61 0.12 -15 6 29 0.94 0.27 0 6 29 0.16 -0.21 1 6 29 0.02 0.14 2 6 29 -0.50 0.26 -16 7 29 0.21 -0.12 -15 7 29 -0.13 -0.38 -14 7 29 -0.55 0.23 -13 7 29 0.30 0.09 -2 7 29 0.03 0.09 -1 7 29 -0.37 -0.19 0 7 29 -0.09 -0.34 1 7 29 -0.13 0.01 -15 8 29 -0.35 0.19 -14 8 29 -0.82 0.05 -13 8 29 0.67 -0.86 -12 8 29 -0.61 0.49 -6 8 29 -0.28 -0.40 -5 8 29 0.93 0.80 -4 8 29 0.03 -0.65 -3 8 29 0.15 -0.07 -2 8 29 0.21 0.34 -1 8 29 0.10 -0.18 0 8 29 0.36 0.53 -13 9 29 0.12 0.17 -12 9 29 -0.15 0.24 -11 9 29 -0.28 -0.79 -10 9 29 -0.71 -0.04 -9 9 29 0.04 -1.03 -8 9 29 -0.21 0.01 -7 9 29 0.34 -0.19 -6 9 29 0.10 0.11 -5 9 29 0.21 -0.77 -4 9 29 -0.11 -0.06 -3 9 29 -0.11 -0.24 -2 9 29 -0.30 -0.04 -10 10 29 0.33 0.45 -9 10 29 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7 30 -0.08 0.17 -7 7 30 0.07 -0.24 -6 7 30 0.35 0.77 -5 7 30 0.33 -0.43 -4 7 30 0.15 0.44 -3 7 30 0.19 0.03 -2 7 30 0.06 0.05 -1 7 30 0.03 -0.08 -13 8 30 -0.10 -0.02 -12 8 30 0.06 -0.73 -11 8 30 -0.92 0.11 -10 8 30 0.59 -0.44 -9 8 30 -0.41 0.04 -8 8 30 0.63 -0.27 -7 8 30 0.27 0.41 -6 8 30 -0.22 -0.09 -5 8 30 -0.30 -0.54 -4 8 30 0.51 -0.11 -3 8 30 -0.08 -0.22 -9 9 30 -0.20 -0.10 -8 9 30 -0.09 -0.68 -7 9 30 0.48 0.10 -6 9 30 -0.49 -0.25 -17 0 31 0.26 -0.08 -16 0 31 0.45 -0.25 -15 0 31 -0.09 0.03 -13 0 31 -0.50 0.09 -1 0 31 0.67 -0.01 0 0 31 0.26 -0.01 1 0 31 -0.24 0.04 -17 1 31 0.51 0.05 -16 1 31 -0.36 -0.45 -15 1 31 1.43 -0.08 -14 1 31 -0.09 -0.21 -1 1 31 0.20 -0.61 0 1 31 0.46 -0.36 1 1 31 0.29 -0.27 -16 2 31 -0.07 0.07 -15 2 31 0.19 -0.76 -14 2 31 0.04 0.23 -2 2 31 -0.25 0.17 -1 2 31 0.18 0.45 0 2 31 -0.01 0.20 1 2 31 -0.10 -0.02 -16 3 31 -0.08 0.23 -15 3 31 -0.13 0.38 -14 3 31 0.05 -0.56 -2 3 31 -0.53 0.16 -1 3 31 0.21 0.37 0 3 31 -0.20 -0.04 -15 4 31 0.12 0.27 -14 4 31 -0.15 -0.29 -13 4 31 0.30 0.16 -3 4 31 -0.37 0.55 -2 4 31 -0.23 0.18 -1 4 31 -0.45 0.18 0 4 31 0.00 -0.09 -15 5 31 0.18 -0.04 -14 5 31 -0.22 0.62 -13 5 31 -0.54 -0.30 -12 5 31 0.13 -0.23 -11 5 31 -0.42 0.01 -10 5 31 -0.02 -0.24 -5 5 31 -0.08 -0.60 -4 5 31 0.29 -0.73 -3 5 31 -0.34 0.60 -2 5 31 0.35 -0.68 -1 5 31 -0.45 0.17 -13 6 31 -0.24 -0.25 -12 6 31 -0.46 0.02 -11 6 31 -0.02 -0.19 -10 6 31 -0.14 0.58 -9 6 31 0.17 -0.39 -8 6 31 -0.27 0.40 -7 6 31 -0.18 0.60 -6 6 31 -0.24 0.17 -5 6 31 -0.23 -0.13 -4 6 31 0.15 0.10 -3 6 31 -0.66 -0.37 -2 6 31 0.23 -0.79 -12 7 31 -0.81 -0.07 -11 7 31 0.35 0.01 -10 7 31 -0.19 -0.12 -9 7 31 0.30 -0.08 -8 7 31 0.50 0.60 -7 7 31 -0.01 -0.35 -6 7 31 0.07 -0.15 -5 7 31 0.37 0.26 -4 7 31 -0.02 -0.03 -15 0 32 0.25 -0.27 -14 0 32 -0.18 -0.01 -13 0 32 0.48 -0.02 -12 0 32 -0.26 -0.04 -11 0 32 1.04 -0.02 -5 0 32 0.18 -0.10 -4 0 32 0.05 -0.24 -3 0 32 0.79 -0.12 -2 0 32 0.74 -0.06 -1 0 32 0.21 -0.08 -15 1 32 -0.14 -0.35 -14 1 32 0.85 0.24 -13 1 32 0.32 0.26 -12 1 32 0.22 -0.24 -11 1 32 0.57 0.00 -10 1 32 -0.23 -0.25 -6 1 32 0.10 -0.08 -5 1 32 0.08 0.19 -4 1 32 0.21 -0.65 -3 1 32 -0.09 0.33 -2 1 32 -0.59 -0.26 -1 1 32 0.13 -0.13 -15 2 32 0.09 0.05 -14 2 32 0.50 -1.01 -13 2 32 -0.49 0.27 -12 2 32 0.06 -0.10 -11 2 32 -0.26 0.44 -10 2 32 0.14 0.19 -9 2 32 -0.08 -0.45 -8 2 32 -0.23 0.91 -7 2 32 -0.42 0.38 -6 2 32 -0.07 0.76 -5 2 32 -0.49 0.25 -4 2 32 0.17 0.19 -3 2 32 -0.40 0.47 -2 2 32 -0.16 0.34 -14 3 32 -0.15 -0.01 -13 3 32 -0.28 -0.17 -12 3 32 0.25 -0.46 -11 3 32 -0.27 -0.03 -10 3 32 -0.62 -0.18 -9 3 32 0.12 -0.28 -8 3 32 -0.57 0.49 -7 3 32 -0.15 -0.32 -6 3 32 -0.17 -0.22 -5 3 32 -0.07 0.06 -4 3 32 -0.25 0.55 -3 3 32 0.15 0.10 -2 3 32 0.15 -0.27 -13 4 32 0.10 -0.26 -12 4 32 0.21 0.06 -11 4 32 0.00 -0.13 -10 4 32 -0.13 0.31 -9 4 32 0.39 -0.05 -8 4 32 0.09 0.57 -7 4 32 0.61 -0.42 -6 4 32 -0.30 0.07 -5 4 32 0.02 -0.30 -4 4 32 -0.50 -0.02 -3 4 32 -0.13 -0.36 -12 5 32 -0.47 -0.16 -11 5 32 0.01 0.08 -10 5 32 -0.02 -0.04 -9 5 32 -0.34 0.01 -8 5 32 -0.46 -0.17 -7 5 32 -0.27 -0.29 -6 5 32 0.19 -0.08 -5 5 32 -0.03 -0.17 -9 6 32 0.42 0.85 -8 6 32 -0.10 -0.42 -7 6 32 -0.11 0.39 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 280317) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 -0.028 0.000 1078 164 ' ' 2 0.500 -0.017 0.500 1170 175 ' ' 3 0.482 0.038 0.224 7 0 ' ' 4 0.908 0.223 0.746 11 0 ' ' 5 0.196 0.309 0.856 28 1 ' ' 6 0.518 0.538 0.776 7 0 ' ' 7 0.092 0.723 0.254 11 0 ' ' 8 0.804 0.808 0.144 29 1 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 0 0 1 1.824 3 0 1 7.793 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL tx2347c_a.res in P2(1) CELL 20.0678 15.8911 25.6047 90.00 108.96 90.00 SPGR P21 # Solvent Accessible Volume = 2333 # Electrons Found in S.A.V. = 342 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.532 0.892 0.431 ! 4.62 eA-3 C102 0.837 0.693 0.468 ! 3.75 eA-3 C103 0.347 0.688 0.971 ! 3.68 eA-3 C104 0.597 0.863 0.424 ! 3.46 eA-3 C105 0.488 0.918 0.439 ! 3.45 eA-3 C106 0.042 0.877 0.929 ! 3.27 eA-3 C107 0.116 0.500 0.938 ! 2.96 eA-3 C108 0.235 0.184 0.561 ! 2.95 eA-3 C109 0.114 0.858 0.922 ! 2.63 eA-3 C110 0.652 0.520 0.507 ! 2.61 eA-3 C111 0.376 0.971 0.546 ! 2.57 eA-3 C112 0.479 0.623 0.409 ! 2.46 eA-3 C113 0.428 0.202 0.719 ! 2.41 eA-3 C114 0.572 0.704 0.330 ! 2.27 eA-3 C115 0.145 0.532 0.995 ! 1.94 eA-3 C116 0.914 0.041 0.967 ! 1.93 eA-3 C117 0.368 0.113 0.471 ! 1.84 eA-3 C118 0.937 0.201 0.222 ! 1.82 eA-3 C119 0.886 0.127 0.966 ! 1.77 eA-3 C120 0.981 0.641 0.907 ! 1.77 eA-3 C121 0.330 0.666-0.003 ! 1.67 eA-3 C122 0.065 0.718 0.812 ! 1.60 eA-3 C123 0.365 0.169 0.462 ! 1.53 eA-3 C124 0.524 0.611 0.389 ! 1.48 eA-3 C125 0.108 0.822 0.843 ! 1.33 eA-3 C126 0.510 0.655 0.451 ! 1.26 eA-3 C127 0.543 0.667 0.503 ! 1.24 eA-3 C128 0.403 0.999 0.459 ! 1.20 eA-3 C129 0.394 0.084 0.458 ! 1.00 eA-3 C130 0.978 0.120 0.108 ! 0.99 eA-3 C131 1.004 0.700 0.952 ! 0.90 eA-3 C132 0.760 0.142 0.016 ! 0.72 eA-3 C133 0.789 0.185 0.024 ! 0.71 eA-3 C134 0.073 0.874 0.732 ! 0.70 eA-3 C135 0.605 0.824 0.351 ! 0.65 eA-3 Q136 0.528 0.374 0.303 ! 0.60 eA-3 Q137 0.991 0.310 0.737 ! 0.58 eA-3 C138 0.093 0.874 0.763 ! 0.57 eA-3 C139 0.667 0.726 0.507 ! 0.56 eA-3 C140 0.071 0.612 0.927 ! 0.56 eA-3 C141 0.385 0.307 0.671 ! 0.54 eA-3 ) ; _shelx_fab_checksum 9918 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.611 _oxdiff_exptl_absorpt_empirical_full_min 0.507 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.27249(16) 0.5856(2) 1.11009(12) 0.0590(7) Uani 1 1 d . . . . . H1 H 0.238216 0.597065 1.119505 0.088 Uiso 1 1 calc GR . . . . O2 O 0.41211(14) 0.51392(19) 1.06507(11) 0.0496(6) Uani 1 1 d . . . . . H2 H 0.442521 0.499472 1.051907 0.074 Uiso 1 1 calc GR . . . . O3 O 0.47080(14) 0.4350(2) 0.99549(11) 0.0504(6) Uani 1 1 d . . . . . O4 O 0.26013(17) 0.5534(3) 0.81155(13) 0.0707(8) Uani 1 1 d . . . . . O5 O 0.50149(14) 0.67475(18) 0.89190(12) 0.0527(6) Uani 1 1 d . . . . . O6 O 0.2593(3) 0.8461(3) 0.77933(17) 0.1164(19) Uani 1 1 d . . . . . O7 O 0.2612(2) 0.8924(2) 0.89406(16) 0.0741(9) Uani 1 1 d . . . . . H7 H 0.267844 0.848053 0.880108 0.111 Uiso 1 1 calc GR . . . . O8 O 0.31932(15) 1.0077(3) 1.01495(11) 0.0610(8) Uani 1 1 d . . . . . H8 H 0.326976 1.018303 1.047726 0.092 Uiso 1 1 calc GR . . . . O9 O 0.31109(16) 1.0911(2) 1.10621(12) 0.0610(7) Uani 1 1 d . . . . . O10 O 0.10163(15) 0.8809(2) 1.12837(12) 0.0585(7) Uani 1 1 d . . . . . O11 O 0.36158(15) 0.8944(2) 1.26005(13) 0.0548(6) Uani 1 1 d . . . . . O12 O 0.20600(15) 0.6056(2) 1.18919(17) 0.0685(9) Uani 1 1 d . . . . . C1 C 0.32475(18) 0.5532(2) 1.15414(15) 0.0419(7) Uani 1 1 d . . . . . C2 C 0.35532(18) 0.4778(2) 1.14624(14) 0.0404(7) Uani 1 1 d . . . . . C3 C 0.41077(19) 0.4437(2) 1.18896(15) 0.0446(7) Uani 1 1 d D . . . . C4 C 0.43701(17) 0.4864(2) 1.23910(15) 0.0444(7) Uani 1 1 d D . . . . C5 C 0.40483(18) 0.5615(2) 1.24622(15) 0.0434(7) Uani 1 1 d . . . . . H5 H 0.422117 0.589746 1.279727 0.052 Uiso 1 1 calc R . . . . C6 C 0.34817(17) 0.5952(2) 1.20513(15) 0.0407(7) Uani 1 1 d . . . . . C7 C 0.4981(2) 0.4525(3) 1.2860(2) 0.0642(11) Uani 1 1 d D U . . . H7A H 0.481543 0.432811 1.315518 0.077 Uiso 1 1 calc R . . . . H7B H 0.532418 0.496747 1.300655 0.077 Uiso 1 1 calc R . . . . C8 C 0.5341(2) 0.3760(3) 1.2637(3) 0.0821(16) Uani 1 1 d D U . . . H8A H 0.560973 0.398269 1.241418 0.098 Uiso 1 1 calc R . . . . H8B H 0.566362 0.346273 1.294779 0.098 Uiso 1 1 calc R . . . . C9 C 0.4803(3) 0.3172(4) 1.2304(2) 0.0847(15) Uani 1 1 d D U . . . H9A H 0.502670 0.267299 1.221895 0.102 Uiso 1 1 calc R . . . . H9B H 0.449397 0.300074 1.250785 0.102 Uiso 1 1 calc R . . . . C10 C 0.4399(3) 0.3595(3) 1.17965(19) 0.0618(11) Uani 1 1 d D U . . . H10A H 0.401051 0.323495 1.159383 0.074 Uiso 1 1 calc R . . . . H10B H 0.469777 0.367649 1.156967 0.074 Uiso 1 1 calc R . . . . C11 C 0.3271(2) 0.4356(2) 1.09048(16) 0.0460(8) Uani 1 1 d . . . . . C12 C 0.35758(19) 0.4563(2) 1.05049(15) 0.0437(7) Uani 1 1 d . . . . . C13 C 0.3298(2) 0.4252(2) 0.99660(15) 0.0466(8) Uani 1 1 d . . . . . C14 C 0.2737(2) 0.3679(3) 0.98568(18) 0.0568(10) Uani 1 1 d . . . . . H14 H 0.255777 0.344958 0.950470 0.068 Uiso 1 1 calc R . . . . C15 C 0.2439(3) 0.3444(3) 1.02509(19) 0.0626(11) Uani 1 1 d D . . . . C16 C 0.2697(2) 0.3795(3) 1.07749(17) 0.0535(9) Uani 1 1 d D . . . . C17 C 0.2375(3) 0.3583(3) 1.12206(19) 0.0662(12) Uani 1 1 d D U . . . H17A H 0.208800 0.405231 1.126243 0.079 Uiso 1 1 calc R . . . . H17B H 0.275096 0.350795 1.156891 0.079 Uiso 1 1 calc R . . . . C18 C 0.1922(4) 0.2787(5) 1.1094(3) 0.117(3) Uani 1 1 d D U . . . H18A H 0.222580 0.229705 1.118067 0.140 Uiso 1 1 calc R . . . . H18B H 0.162653 0.277408 1.132829 0.140 Uiso 1 1 calc R . . . . C19 C 0.1481(4) 0.2746(5) 1.0524(3) 0.123(3) Uani 1 1 d D U . . . H19A H 0.113838 0.319759 1.045676 0.147 Uiso 1 1 calc R . . . . H19B H 0.122242 0.221928 1.046798 0.147 Uiso 1 1 calc R . . . . C20 C 0.1849(3) 0.2805(4) 1.0102(2) 0.0899(18) Uani 1 1 d D U . . . H20A H 0.150836 0.295556 0.974904 0.108 Uiso 1 1 calc R . . . . H20B H 0.203978 0.225693 1.006193 0.108 Uiso 1 1 calc R . . . . C21 C 0.3497(2) 0.4589(2) 0.94936(15) 0.0439(7) Uani 1 1 d . . . . . C22 C 0.41933(19) 0.4655(2) 0.95000(14) 0.0439(7) Uani 1 1 d . . . . . C23 C 0.4336(2) 0.5024(2) 0.90502(14) 0.0431(7) Uani 1 1 d . . . . . H23 H 0.480109 0.506664 0.905701 0.052 Uiso 1 1 calc R . . . . C24 C 0.3803(2) 0.5328(2) 0.85956(14) 0.0448(7) Uani 1 1 d . . . . . C25 C 0.3106(2) 0.5229(3) 0.85828(16) 0.0509(8) Uani 1 1 d . . . . . C26 C 0.2956(2) 0.4867(3) 0.90220(16) 0.0517(8) Uani 1 1 d . . . . . H26 H 0.248853 0.480700 0.900595 0.062 Uiso 1 1 calc R . . . . C27 C 0.1877(3) 0.5397(7) 0.8073(3) 0.124(3) Uani 1 1 d . . . . . H27A H 0.157557 0.562838 0.773219 0.186 Uiso 1 1 calc GR . . . . H27B H 0.178240 0.566715 0.837713 0.186 Uiso 1 1 calc GR . . . . H27C H 0.179100 0.480396 0.808297 0.186 Uiso 1 1 calc GR . . . . C28 C 0.5415(2) 0.4376(4) 0.99394(18) 0.0659(12) Uani 1 1 d . . . . . H28A H 0.543773 0.408441 0.961702 0.099 Uiso 1 1 calc GR . . . . H28B H 0.572586 0.410920 1.026399 0.099 Uiso 1 1 calc GR . . . . H28C H 0.555660 0.495054 0.992683 0.099 Uiso 1 1 calc GR . . . . C29 C 0.3976(2) 0.5811(2) 0.81546(14) 0.0480(8) Uani 1 1 d . . . . . H29A H 0.365956 0.564707 0.779446 0.058 Uiso 1 1 calc R . . . . H29B H 0.445439 0.568677 0.816788 0.058 Uiso 1 1 calc R . . . . C30 C 0.3901(2) 0.6751(2) 0.82435(14) 0.0465(8) Uani 1 1 d . . . . . C31 C 0.3298(2) 0.7181(3) 0.79503(16) 0.0593(10) Uani 1 1 d . . . . . H31 H 0.295832 0.690690 0.766499 0.071 Uiso 1 1 calc R . . . . C32 C 0.3185(3) 0.8013(3) 0.80692(17) 0.0635(11) Uani 1 1 d . . . . . C33 C 0.3689(2) 0.8437(3) 0.84908(15) 0.0495(8) Uani 1 1 d . . . . . C34 C 0.4305(2) 0.8016(2) 0.87797(15) 0.0450(7) Uani 1 1 d . . . . . H34 H 0.464892 0.829353 0.906035 0.054 Uiso 1 1 calc R . . . . C35 C 0.4418(2) 0.7187(2) 0.86568(15) 0.0434(7) Uani 1 1 d . . . . . C36 C 0.5508(3) 0.7117(4) 0.9385(2) 0.0693(12) Uani 1 1 d . . . . . H36A H 0.566519 0.764239 0.928170 0.104 Uiso 1 1 calc GR . . . . H36B H 0.590314 0.674608 0.952752 0.104 Uiso 1 1 calc GR . . . . H36C H 0.529126 0.721364 0.966316 0.104 Uiso 1 1 calc GR . . . . C37 C 0.2193(4) 0.8322(9) 0.7335(4) 0.167(5) Uani 1 1 d . . . . . H37A H 0.245122 0.831339 0.707794 0.250 Uiso 1 1 calc GR . . . . H37B H 0.184142 0.875518 0.723148 0.250 Uiso 1 1 calc GR . . . . H37C H 0.197006 0.778659 0.733059 0.250 Uiso 1 1 calc GR . . . . C38 C 0.3586(2) 0.9321(3) 0.86432(15) 0.0524(9) Uani 1 1 d . . . . . C39 C 0.4046(2) 0.9955(3) 0.85994(16) 0.0521(9) Uani 1 1 d . . . . . H39 H 0.440566 0.982123 0.845878 0.063 Uiso 1 1 calc R . . . . C40 C 0.3984(2) 1.0786(2) 0.87600(15) 0.0494(8) Uani 1 1 d D U . . . C41 C 0.3452(2) 1.0984(2) 0.89813(15) 0.0503(8) Uani 1 1 d D . . . . C42 C 0.2998(2) 1.0345(3) 0.90504(15) 0.0488(8) Uani 1 1 d . . . . . C43 C 0.3065(2) 0.9525(3) 0.88714(16) 0.0517(8) Uani 1 1 d . . . . . C44 C 0.4480(6) 1.1437(5) 0.8672(7) 0.058(4) Uani 0.639(11) 1 d D U P A 1 H44A H 0.427516 1.170390 0.831515 0.070 Uiso 0.639(11) 1 calc R . P A 1 H44B H 0.492131 1.117717 0.868380 0.070 Uiso 0.639(11) 1 calc R . P A 1 C45 C 0.4607(5) 1.2090(7) 0.9132(5) 0.097(3) Uani 0.639(11) 1 d D U P A 1 H45A H 0.482210 1.182099 0.948764 0.116 Uiso 0.639(11) 1 calc R . P A 1 H45B H 0.492640 1.251939 0.908684 0.116 Uiso 0.639(11) 1 calc R . P A 1 C46 C 0.3927(5) 1.2484(6) 0.9116(5) 0.068(2) Uani 0.639(11) 1 d D U P A 1 H46A H 0.371859 1.275789 0.876202 0.082 Uiso 0.639(11) 1 calc R . P A 1 H46B H 0.401837 1.291309 0.940066 0.082 Uiso 0.639(11) 1 calc R . P A 1 C47 C 0.3409(7) 1.1858(5) 0.9203(6) 0.060(3) Uani 0.639(11) 1 d D U P A 1 H47A H 0.293666 1.207313 0.902824 0.071 Uiso 0.639(11) 1 calc R . P A 1 H47B H 0.348383 1.181555 0.959569 0.071 Uiso 0.639(11) 1 calc R . P A 1 C48 C 0.2425(2) 1.0520(2) 0.92913(14) 0.0463(8) Uani 1 1 d . . . . . C49 C 0.1761(2) 1.0801(3) 0.89522(15) 0.0495(8) Uani 1 1 d D . . . . C50 C 0.1636(3) 1.0938(3) 0.83422(16) 0.0599(10) Uani 1 1 d D U . . . H50A H 0.205864 1.117520 0.829611 0.072 Uiso 1 1 calc R . . . . H50B H 0.155170 1.039760 0.815638 0.072 Uiso 1 1 calc R . . . . C51 C 0.1030(3) 1.1506(4) 0.8072(2) 0.0754(13) Uani 1 1 d D U . . . H51A H 0.116962 1.208375 0.817177 0.091 Uiso 1 1 calc R . . . . H51B H 0.090730 1.145591 0.767429 0.091 Uiso 1 1 calc R . . . . C52 C 0.0401(3) 1.1305(5) 0.8235(2) 0.097(2) Uani 1 1 d D U . . . H52A H 0.022318 1.075928 0.808309 0.117 Uiso 1 1 calc R . . . . H52B H 0.003754 1.171668 0.806609 0.117 Uiso 1 1 calc R . . . . C53 C 0.0518(3) 1.1289(4) 0.8851(2) 0.0720(12) Uani 1 1 d D U . . . H53A H 0.048266 1.185818 0.897755 0.086 Uiso 1 1 calc R . . . . H53B H 0.014961 1.095631 0.891984 0.086 Uiso 1 1 calc R . . . . C54 C 0.1225(2) 1.0928(3) 0.91782(16) 0.0515(8) Uani 1 1 d D . . . . C55 C 0.1347(2) 1.0735(3) 0.97324(16) 0.0511(8) Uani 1 1 d . . . . . H55 H 0.098227 1.080690 0.987787 0.061 Uiso 1 1 calc R . . . . C56 C 0.1992(2) 1.0440(3) 1.00757(15) 0.0480(8) Uani 1 1 d . . . . . C57 C 0.2542(2) 1.0360(3) 0.98513(15) 0.0495(8) Uani 1 1 d . . . . . C58 C 0.20499(19) 1.0171(3) 1.06455(14) 0.0463(8) Uani 1 1 d . . . . . C59 C 0.1508(2) 0.9647(3) 1.07001(15) 0.0473(8) Uani 1 1 d . . . . . H59 H 0.113471 0.950109 1.038789 0.057 Uiso 1 1 calc R . . . . C60 C 0.15256(19) 0.9345(3) 1.12138(15) 0.0458(7) Uani 1 1 d . . . . . C61 C 0.20724(19) 0.9544(2) 1.16884(14) 0.0429(7) Uani 1 1 d . . . . . C62 C 0.25928(19) 1.0093(2) 1.16340(14) 0.0442(7) Uani 1 1 d . . . . . H62 H 0.294959 1.026633 1.194937 0.053 Uiso 1 1 calc R . . . . C63 C 0.25899(19) 1.0385(3) 1.11204(15) 0.0481(8) Uani 1 1 d . . . . . C64 C 0.3638(3) 1.1195(4) 1.1553(2) 0.0820(16) Uani 1 1 d . . . . . H64A H 0.392991 1.160748 1.145921 0.123 Uiso 1 1 calc GR . . . . H64B H 0.392332 1.072670 1.173326 0.123 Uiso 1 1 calc GR . . . . H64C H 0.341638 1.144110 1.179674 0.123 Uiso 1 1 calc GR . . . . C65 C 0.0477(3) 0.8544(5) 1.0802(2) 0.0906(19) Uani 1 1 d . . . . . H65A H 0.028517 0.902340 1.057526 0.136 Uiso 1 1 calc GR . . . . H65B H 0.011117 0.827017 1.090470 0.136 Uiso 1 1 calc GR . . . . H65C H 0.066842 0.815740 1.060013 0.136 Uiso 1 1 calc GR . . . . C66 C 0.21531(19) 0.9136(2) 1.22353(14) 0.0430(7) Uani 1 1 d . . . . . H66A H 0.169415 0.905793 1.227781 0.052 Uiso 1 1 calc R . . . . H66B H 0.243272 0.949346 1.253340 0.052 Uiso 1 1 calc R . . . . C67 C 0.25132(18) 0.8294(2) 1.22574(14) 0.0417(7) Uani 1 1 d . . . . . C68 C 0.21116(19) 0.7567(3) 1.20872(16) 0.0479(8) Uani 1 1 d . . . . . H68 H 0.162487 0.759421 1.200151 0.057 Uiso 1 1 calc R . . . . C69 C 0.24273(19) 0.6801(3) 1.20434(17) 0.0481(8) Uani 1 1 d . . . . . C70 C 0.31468(18) 0.6747(2) 1.21477(15) 0.0426(7) Uani 1 1 d . . . . . C71 C 0.35519(19) 0.7456(2) 1.23485(15) 0.0431(7) Uani 1 1 d . . . . . H71 H 0.403975 0.741962 1.244670 0.052 Uiso 1 1 calc R . . . . C72 C 0.32426(19) 0.8224(2) 1.24067(14) 0.0419(7) Uani 1 1 d . . . . . C73 C 0.4356(2) 0.8877(3) 1.2782(3) 0.0747(14) Uani 1 1 d . . . . . H73A H 0.451151 0.875979 1.247270 0.112 Uiso 1 1 calc GR . . . . H73B H 0.449999 0.842884 1.304649 0.112 Uiso 1 1 calc GR . . . . H73C H 0.455987 0.939653 1.295129 0.112 Uiso 1 1 calc GR . . . . C74 C 0.1337(3) 0.6068(4) 1.1763(3) 0.0854(16) Uani 1 1 d . . . . . H74A H 0.114009 0.648486 1.148408 0.128 Uiso 1 1 calc GR . . . . H74B H 0.121778 0.620133 1.208746 0.128 Uiso 1 1 calc GR . . . . H74C H 0.114860 0.552488 1.162714 0.128 Uiso 1 1 calc GR . . . . O13 O 0.25583(16) 0.3890(2) 0.60972(13) 0.0568(7) Uani 1 1 d . . . . . H13 H 0.249584 0.343844 0.622955 0.085 Uiso 1 1 calc GR . . . . O14 O 0.18583(14) 0.4872(3) 0.48499(11) 0.0589(8) Uani 1 1 d . . . . . H14A H 0.168265 0.510008 0.454890 0.088 Uiso 1 1 calc GR . . . . O15 O 0.18133(15) 0.5686(3) 0.38934(11) 0.0644(8) Uani 1 1 d . . . . . O16 O 0.39924(14) 0.3765(2) 0.36409(11) 0.0501(6) Uani 1 1 d . . . . . O17 O 0.13753(15) 0.3874(2) 0.22927(13) 0.0573(7) Uani 1 1 d . . . . . O18 O 0.29290(13) 0.09998(19) 0.30662(13) 0.0532(6) Uani 1 1 d . . . . . O19 O 0.21956(15) 0.0710(2) 0.37809(11) 0.0571(7) Uani 1 1 d . . . . . H19 H 0.253807 0.083492 0.368895 0.086 Uiso 1 1 calc GR . . . . O20 O 0.07940(13) 0.01135(19) 0.42385(10) 0.0464(5) Uani 1 1 d . . . . . H20 H 0.053105 0.003164 0.442055 0.070 Uiso 1 1 calc GR . . . . O21 O 0.02119(12) -0.0646(2) 0.49532(9) 0.0442(5) Uani 1 1 d . . . . . O22 O 0.24383(16) 0.0305(3) 0.67692(13) 0.0728(9) Uani 1 1 d . . . . . O23 O 0.26675(17) 0.3182(2) 0.71325(14) 0.0701(9) Uani 1 1 d . . . . . O24 O 0.00547(13) 0.174240 0.61312(11) 0.0445(5) Uani 1 1 d . . . . . C77 C 0.34704(17) 0.4259(2) 0.37163(14) 0.0398(6) Uani 1 1 d . . . . . C78 C 0.34853(16) 0.4567(2) 0.42271(13) 0.0377(6) Uani 1 1 d . . . . . H78 H 0.387429 0.445388 0.453562 0.045 Uiso 1 1 calc R . . . . C79 C 0.29294(16) 0.5044(2) 0.42894(13) 0.0388(6) Uani 1 1 d . . . . . C80 C 0.23667(18) 0.5222(3) 0.38175(14) 0.0464(8) Uani 1 1 d . . . . . C81 C 0.23592(18) 0.4939(3) 0.33042(14) 0.0449(7) Uani 1 1 d . . . . . H81 H 0.198157 0.507900 0.299350 0.054 Uiso 1 1 calc R . . . . C82 C 0.29005(17) 0.4452(2) 0.32429(13) 0.0398(7) Uani 1 1 d . . . . . C83 C 0.4571(3) 0.3558(4) 0.4115(2) 0.0790(15) Uani 1 1 d . . . . . H83A H 0.490509 0.322922 0.400687 0.119 Uiso 1 1 calc GR . . . . H83B H 0.440591 0.324014 0.436751 0.119 Uiso 1 1 calc GR . . . . H83C H 0.479195 0.406581 0.429149 0.119 Uiso 1 1 calc GR . . . . C84 C 0.1239(3) 0.5882(6) 0.3407(2) 0.119(3) Uani 1 1 d . . . . . H84A H 0.141315 0.616962 0.314835 0.178 Uiso 1 1 calc GR . . . . H84B H 0.090866 0.623592 0.350292 0.178 Uiso 1 1 calc GR . . . . H84C H 0.100890 0.537085 0.324368 0.178 Uiso 1 1 calc GR . . . . C85 C 0.28342(19) 0.4065(2) 0.26881(14) 0.0426(7) Uani 1 1 d . . . . . H85A H 0.329704 0.399510 0.265114 0.051 Uiso 1 1 calc R . . . . H85B H 0.255761 0.442851 0.239276 0.051 Uiso 1 1 calc R . . . . C86 C 0.24764(18) 0.3218(2) 0.26531(13) 0.0406(7) Uani 1 1 d . . . . . C87 C 0.28747(18) 0.2489(2) 0.28382(14) 0.0418(7) Uani 1 1 d . . . . . H87 H 0.336271 0.251605 0.293462 0.050 Uiso 1 1 calc R . . . . C88 C 0.25572(18) 0.1724(2) 0.28817(15) 0.0408(7) Uani 1 1 d . . . . . C89 C 0.18290(17) 0.1673(2) 0.27506(14) 0.0388(6) Uani 1 1 d . . . . . C90 C 0.14313(17) 0.2386(2) 0.25445(14) 0.0408(7) Uani 1 1 d . . . . . H90 H 0.094272 0.235520 0.244060 0.049 Uiso 1 1 calc R . . . . C91 C 0.17459(19) 0.3146(2) 0.24896(14) 0.0430(7) Uani 1 1 d . . . . . C92 C 0.0632(3) 0.3816(3) 0.2125(3) 0.0834(17) Uani 1 1 d . . . . . H92A H 0.047385 0.338243 0.185160 0.125 Uiso 1 1 calc GR . . . . H92B H 0.042844 0.434408 0.197240 0.125 Uiso 1 1 calc GR . . . . H92C H 0.048906 0.368097 0.243892 0.125 Uiso 1 1 calc GR . . . . C93 C 0.3674(2) 0.1027(3) 0.3229(2) 0.0676(12) Uani 1 1 d . . . . . H93A H 0.381559 0.121531 0.292507 0.101 Uiso 1 1 calc GR . . . . H93B H 0.386057 0.047448 0.333945 0.101 Uiso 1 1 calc GR . . . . H93C H 0.384978 0.140847 0.353365 0.101 Uiso 1 1 calc GR . . . . C94 C 0.14684(16) 0.0880(2) 0.28274(14) 0.0380(6) Uani 1 1 d . . . . . C95 C 0.16573(17) 0.0438(2) 0.33256(14) 0.0413(7) Uani 1 1 d . . . . . C96 C 0.13002(19) -0.0283(2) 0.33849(15) 0.0432(7) Uani 1 1 d . . . . . C97 C 0.0721(2) -0.0568(2) 0.29417(17) 0.0488(8) Uani 1 1 d D . . . . C98 C 0.05226(17) -0.0130(2) 0.24468(16) 0.0456(8) Uani 1 1 d D . . . . C99 C 0.08950(17) 0.0591(2) 0.23975(15) 0.0421(7) Uani 1 1 d . . . . . H99 H 0.075421 0.088682 0.206609 0.050 Uiso 1 1 calc R . . . . C100 C -0.0091(2) -0.0405(3) 0.19522(19) 0.0601(10) Uani 1 1 d D U . . . H10C H -0.048045 -0.002266 0.191397 0.072 Uiso 1 1 calc R . . . . H10D H 0.004691 -0.034535 0.162426 0.072 Uiso 1 1 calc R . . . . C101 C -0.0348(3) -0.1281(4) 0.1967(2) 0.0894(16) Uani 1 1 d D U . . . H10E H -0.080658 -0.135154 0.168835 0.107 Uiso 1 1 calc R . . . . H10F H -0.002411 -0.167880 0.189242 0.107 Uiso 1 1 calc R . . . . C102 C -0.0399(3) -0.1433(4) 0.2516(2) 0.0808(15) Uani 1 1 d D U . . . H10G H -0.059025 -0.199124 0.252354 0.097 Uiso 1 1 calc R . . . . H10H H -0.072658 -0.103071 0.258195 0.097 Uiso 1 1 calc R . . . . C103 C 0.0327(3) -0.1360(3) 0.29952(19) 0.0663(12) Uani 1 1 d D U . . . H10I H 0.024415 -0.135544 0.334781 0.080 Uiso 1 1 calc R . . . . H10J H 0.061463 -0.184714 0.298719 0.080 Uiso 1 1 calc R . . . . C104 C 0.1550(2) -0.0742(2) 0.39220(17) 0.0498(8) Uani 1 1 d . . . . . C105 C 0.2080(3) -0.1350(3) 0.4021(2) 0.0693(14) Uani 1 1 d D . . . . C106 C 0.2339(3) -0.1735(3) 0.4540(2) 0.0715(14) Uani 1 1 d D . . . . C107 C 0.2101(2) -0.1459(3) 0.49618(18) 0.0557(10) Uani 1 1 d . . . . . H107 H 0.229106 -0.169693 0.531053 0.067 Uiso 1 1 calc R . . . . C108 C 0.15862(19) -0.0838(2) 0.48828(15) 0.0428(7) Uani 1 1 d . . . . . C109 C 0.12961(18) -0.0503(2) 0.43506(14) 0.0406(7) Uani 1 1 d . . . . . C110 C 0.2369(3) -0.1591(3) 0.3563(2) 0.0832(17) Uani 1 1 d D U . . . H11A H 0.266655 -0.113842 0.351236 0.100 Uiso 1 1 calc R . . . . H11B H 0.197983 -0.165270 0.322169 0.100 Uiso 1 1 calc R . . . . C111 C 0.2796(4) -0.2407(4) 0.3677(3) 0.119(3) Uani 1 1 d D U . . . H11C H 0.247677 -0.288250 0.361388 0.143 Uiso 1 1 calc R . . . . H11D H 0.306185 -0.245138 0.342240 0.143 Uiso 1 1 calc R . . . . C112 C 0.3293(4) -0.2436(5) 0.4258(3) 0.116(3) Uani 1 1 d D U . . . H11E H 0.361226 -0.196046 0.432147 0.139 Uiso 1 1 calc R . . . . H11F H 0.357204 -0.294675 0.431058 0.139 Uiso 1 1 calc R . . . . C113 C 0.2898(4) -0.2414(4) 0.4677(3) 0.099(2) Uani 1 1 d D U . . . H11G H 0.267813 -0.295644 0.468200 0.119 Uiso 1 1 calc R . . . . H11H H 0.323006 -0.231255 0.504272 0.119 Uiso 1 1 calc R . . . . C114 C 0.14396(17) -0.0491(2) 0.53767(14) 0.0404(7) Uani 1 1 d . . . . . C115 C 0.20057(19) -0.0276(3) 0.58375(16) 0.0485(8) Uani 1 1 d . . . . . H115 H 0.246168 -0.037303 0.583515 0.058 Uiso 1 1 calc R . . . . C116 C 0.19063(19) 0.0080(3) 0.63013(16) 0.0507(8) Uani 1 1 d . . . . . C117 C 0.12241(18) 0.0243(2) 0.63158(14) 0.0404(7) Uani 1 1 d . . . . . C118 C 0.06605(17) 0.0000(2) 0.58676(14) 0.0386(6) Uani 1 1 d . . . . . H118 H 0.020529 0.009099 0.587361 0.046 Uiso 1 1 calc R . . . . C119 C 0.07563(17) -0.0380(2) 0.54035(13) 0.0372(6) Uani 1 1 d . . . . . C120 C 0.3138(3) 0.0056(6) 0.6812(3) 0.110(3) Uani 1 1 d . . . . . H12A H 0.329945 0.038625 0.656355 0.164 Uiso 1 1 calc GR . . . . H12B H 0.313988 -0.052892 0.671853 0.164 Uiso 1 1 calc GR . . . . H12C H 0.344371 0.014250 0.718385 0.164 Uiso 1 1 calc GR . . . . C122 C 0.1116(2) 0.0711(2) 0.67909(13) 0.0427(7) Uani 1 1 d . . . . . H12D H 0.145093 0.051437 0.713517 0.051 Uiso 1 1 calc R . . . . H12E H 0.064481 0.060652 0.680180 0.051 Uiso 1 1 calc R . . . . C123 C 0.12178(18) 0.1648(2) 0.67258(13) 0.0395(7) Uani 1 1 d . . . . . C124 C 0.1865(2) 0.2034(3) 0.69889(14) 0.0478(8) Uani 1 1 d . . . . . H124 H 0.222124 0.172487 0.723833 0.057 Uiso 1 1 calc R . . . . C125 C 0.1989(2) 0.2863(3) 0.68890(15) 0.0485(8) Uani 1 1 d . . . . . C126 C 0.14524(19) 0.3363(2) 0.65309(13) 0.0404(7) Uani 1 1 d . . . . . C127 C 0.07987(17) 0.2982(2) 0.62772(13) 0.0372(6) Uani 1 1 d . . . . . H127 H 0.043465 0.329576 0.603903 0.045 Uiso 1 1 calc R . . . . C128 C 0.06834(17) 0.2144(2) 0.63745(13) 0.0372(6) Uani 1 1 d . . . . . C129 C -0.0479(2) 0.2181(3) 0.57228(17) 0.0543(9) Uani 1 1 d . . . . . H12F H -0.031021 0.233110 0.542458 0.081 Uiso 1 1 calc GR . . . . H12G H -0.060075 0.268232 0.588065 0.081 Uiso 1 1 calc GR . . . . H12H H -0.088687 0.182874 0.558587 0.081 Uiso 1 1 calc GR . . . . C130 C 0.2776(4) 0.3713(5) 0.7568(3) 0.101(2) Uani 1 1 d . . . . . H13A H 0.241816 0.413991 0.747744 0.151 Uiso 1 1 calc GR . . . . H13B H 0.323069 0.397088 0.765067 0.151 Uiso 1 1 calc GR . . . . H13C H 0.275458 0.340182 0.788381 0.151 Uiso 1 1 calc GR . . . . C131 C 0.15629(19) 0.4251(2) 0.63885(13) 0.0408(7) Uani 1 1 d . . . . . C132 C 0.10929(19) 0.4872(2) 0.64323(14) 0.0428(7) Uani 1 1 d . . . . . H132 H 0.075065 0.473440 0.659075 0.051 Uiso 1 1 calc R . . . . C133 C 0.11193(18) 0.5692(2) 0.62464(13) 0.0395(7) Uani 1 1 d . . . . . C134 C 0.16202(18) 0.5895(2) 0.59934(13) 0.0401(7) Uani 1 1 d . . . . . C135 C 0.20953(18) 0.5280(2) 0.59433(13) 0.0389(6) Uani 1 1 d . . . . . C136 C 0.20732(19) 0.4469(2) 0.61521(13) 0.0417(7) Uani 1 1 d . . . . . C137 C 0.1639(2) 0.6756(2) 0.57452(17) 0.0494(8) Uani 1 1 d D U . . . H13D H 0.211420 0.697619 0.589276 0.059 Uiso 1 1 calc R . . . . H13E H 0.153131 0.669322 0.534954 0.059 Uiso 1 1 calc R . . . . C138 C 0.1138(2) 0.7394(3) 0.5848(2) 0.0628(10) Uani 1 1 d D U . . . H13F H 0.103184 0.781828 0.556010 0.075 Uiso 1 1 calc R . . . . H13G H 0.136476 0.767255 0.619799 0.075 Uiso 1 1 calc R . . . . C139 C 0.0453(3) 0.6997(3) 0.5860(2) 0.0668(11) Uani 1 1 d D U . . . H13H H 0.021550 0.673162 0.550727 0.080 Uiso 1 1 calc R . . . . H13I H 0.014520 0.742970 0.592076 0.080 Uiso 1 1 calc R . . . . C140 C 0.0606(2) 0.6344(3) 0.63195(16) 0.0485(8) Uani 1 1 d D U . . . H14B H 0.080345 0.661872 0.667479 0.058 Uiso 1 1 calc R . . . . H14C H 0.017027 0.607102 0.631199 0.058 Uiso 1 1 calc R . . . . C141 C 0.26358(17) 0.5452(2) 0.56701(13) 0.0370(6) Uani 1 1 d . . . . . C142 C 0.25006(17) 0.5234(2) 0.51186(13) 0.0403(7) Uani 1 1 d . . . . . C143 C 0.30109(16) 0.5346(2) 0.48590(13) 0.0362(6) Uani 1 1 d . . . . . C144 C 0.36466(16) 0.5710(2) 0.51657(13) 0.0374(6) Uani 1 1 d . . . . . H144 H 0.398915 0.579422 0.499847 0.045 Uiso 1 1 calc R . . . . C145 C 0.37915(17) 0.5955(2) 0.57127(14) 0.0406(7) Uani 1 1 d D . . . . C146 C 0.32879(18) 0.5808(2) 0.59720(13) 0.0388(6) Uani 1 1 d D . . . . C147 C 0.3432(2) 0.6028(3) 0.65731(14) 0.0517(8) Uani 1 1 d D U . . . H14D H 0.306420 0.640462 0.660075 0.062 Uiso 1 1 calc R . . . . H14E H 0.340447 0.551818 0.677319 0.062 Uiso 1 1 calc R . . . . C148 C 0.4123(4) 0.6431(6) 0.6844(2) 0.127(3) Uani 1 1 d D U . . . H148 H 0.426891 0.651740 0.722371 0.152 Uiso 1 1 calc R . . . . C149 C 0.4557(3) 0.6680(5) 0.6553(2) 0.103(2) Uani 1 1 d D U . . . H149 H 0.491572 0.706152 0.671712 0.123 Uiso 1 1 calc R . . . . C150 C 0.4481(2) 0.6377(3) 0.60020(16) 0.0561(9) Uani 1 1 d D U . . . H15A H 0.485876 0.598212 0.602659 0.067 Uiso 1 1 calc R . . . . H15B H 0.453670 0.684887 0.577932 0.067 Uiso 1 1 calc R . . . . C155 C -0.04746(18) -0.0617(3) 0.50097(15) 0.0529(9) Uani 1 1 d . . . . . H15C H -0.080936 -0.087427 0.469293 0.079 Uiso 1 1 calc GR . . . . H15D H -0.060601 -0.004237 0.503725 0.079 Uiso 1 1 calc GR . . . . H15E H -0.046881 -0.091674 0.533683 0.079 Uiso 1 1 calc GR . . . . N1 N 0.4165(4) 0.9014(7) 1.1335(3) 0.141(3) Uani 1 1 d . . . . . C75 C 0.3666(5) 0.8608(7) 1.1146(3) 0.107(3) Uani 1 1 d . . . . . C76 C 0.3048(5) 0.8166(5) 1.0927(3) 0.107(2) Uani 1 1 d . . . . . H76A H 0.277919 0.840786 1.057863 0.161 Uiso 1 1 calc GR . . . . H76B H 0.277901 0.819185 1.117599 0.161 Uiso 1 1 calc GR . . . . H76C H 0.315320 0.758930 1.087368 0.161 Uiso 1 1 calc GR . . . . N3 N 0.0855(5) 0.3768(8) 0.3704(4) 0.156(4) Uani 1 1 d . . . . . C153 C 0.1366(5) 0.3396(7) 0.3848(3) 0.113(3) Uani 1 1 d . . . . . C154 C 0.2007(5) 0.2973(6) 0.4014(3) 0.117(3) Uani 1 1 d . . . . . H15F H 0.226743 0.311468 0.377100 0.175 Uiso 1 1 calc GR . . . . H15G H 0.192397 0.237746 0.400087 0.175 Uiso 1 1 calc GR . . . . H15H H 0.227236 0.313541 0.438437 0.175 Uiso 1 1 calc GR . . . . C47A C 0.3248(12) 1.1877(7) 0.9080(10) 0.050(4) Uani 0.361(11) 1 d D U P A 2 H47C H 0.275642 1.196638 0.886677 0.060 Uiso 0.361(11) 1 calc R . P A 2 H47D H 0.329561 1.193961 0.946704 0.060 Uiso 0.361(11) 1 calc R . P A 2 C46A C 0.3685(11) 1.2540(13) 0.8926(9) 0.081(5) Uani 0.361(11) 1 d D U P A 2 H46C H 0.335921 1.295799 0.870938 0.098 Uiso 0.361(11) 1 calc R . P A 2 H46D H 0.395872 1.281413 0.926672 0.098 Uiso 0.361(11) 1 calc R . P A 2 C45A C 0.4184(8) 1.2337(7) 0.8619(7) 0.072(3) Uani 0.361(11) 1 d D U P A 2 H45C H 0.456969 1.273708 0.872815 0.087 Uiso 0.361(11) 1 calc R . P A 2 H45D H 0.394004 1.241525 0.822785 0.087 Uiso 0.361(11) 1 calc R . P A 2 C44A C 0.4490(12) 1.1451(9) 0.8709(15) 0.068(7) Uani 0.361(11) 1 d D U P A 2 H44C H 0.465206 1.130819 0.840142 0.082 Uiso 0.361(11) 1 calc R . P A 2 H44D H 0.489759 1.144811 0.904117 0.082 Uiso 0.361(11) 1 calc R . P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0610(16) 0.0585(16) 0.0560(15) -0.0020(13) 0.0171(12) 0.0139(13) O2 0.0620(15) 0.0447(13) 0.0526(14) -0.0110(11) 0.0331(12) -0.0165(11) O3 0.0565(14) 0.0555(14) 0.0480(13) 0.0089(11) 0.0291(11) 0.0038(12) O4 0.0625(17) 0.091(2) 0.0533(16) -0.0017(15) 0.0110(13) -0.0087(16) O5 0.0544(14) 0.0442(13) 0.0644(16) -0.0059(11) 0.0261(12) 0.0044(11) O6 0.127(4) 0.121(4) 0.070(2) -0.014(2) -0.010(2) 0.072(3) O7 0.112(3) 0.0469(15) 0.088(2) 0.0031(15) 0.067(2) 0.0008(16) O8 0.0591(15) 0.085(2) 0.0462(14) 0.0148(14) 0.0270(12) 0.0178(14) O9 0.0668(16) 0.0728(19) 0.0508(14) -0.0026(13) 0.0293(13) -0.0253(14) O10 0.0599(15) 0.0682(17) 0.0562(15) -0.0033(13) 0.0311(13) -0.0192(14) O11 0.0559(14) 0.0374(12) 0.0685(17) -0.0180(12) 0.0167(13) -0.0065(11) O12 0.0512(15) 0.0426(14) 0.117(3) -0.0216(16) 0.0350(16) -0.0103(12) C1 0.0474(17) 0.0328(15) 0.0529(18) -0.0072(13) 0.0264(15) -0.0042(13) C2 0.0509(17) 0.0290(14) 0.0514(18) -0.0028(13) 0.0307(15) -0.0024(12) C3 0.0563(19) 0.0363(16) 0.0553(19) 0.0016(14) 0.0373(16) -0.0033(14) C4 0.0397(15) 0.0411(16) 0.058(2) 0.0084(15) 0.0238(14) -0.0040(13) C5 0.0427(16) 0.0385(16) 0.0502(18) -0.0057(14) 0.0164(14) -0.0076(13) C6 0.0440(16) 0.0309(14) 0.0529(18) -0.0101(13) 0.0235(14) -0.0046(12) C7 0.048(2) 0.067(3) 0.076(3) 0.025(2) 0.0192(19) 0.0012(18) C8 0.049(2) 0.070(3) 0.118(4) 0.040(3) 0.016(2) 0.011(2) C9 0.100(4) 0.080(3) 0.078(3) 0.016(3) 0.035(3) 0.025(3) C10 0.082(3) 0.048(2) 0.074(3) 0.0090(18) 0.052(2) 0.0142(19) C11 0.060(2) 0.0335(15) 0.0550(19) -0.0077(14) 0.0334(16) -0.0035(14) C12 0.0573(19) 0.0316(14) 0.0537(18) -0.0067(13) 0.0338(16) -0.0077(14) C13 0.062(2) 0.0352(15) 0.0534(19) -0.0103(14) 0.0345(17) -0.0112(15) C14 0.075(2) 0.048(2) 0.061(2) -0.0217(17) 0.042(2) -0.0245(18) C15 0.086(3) 0.052(2) 0.066(2) -0.0221(19) 0.048(2) -0.029(2) C16 0.071(2) 0.0445(18) 0.060(2) -0.0087(16) 0.042(2) -0.0134(17) C17 0.090(3) 0.063(2) 0.067(2) -0.019(2) 0.055(2) -0.029(2) C18 0.151(5) 0.122(5) 0.110(4) -0.038(4) 0.088(4) -0.082(4) C19 0.150(5) 0.146(5) 0.108(4) -0.071(4) 0.091(4) -0.107(5) C20 0.115(4) 0.091(4) 0.086(3) -0.038(3) 0.062(3) -0.064(3) C21 0.062(2) 0.0317(15) 0.0480(17) -0.0095(13) 0.0309(15) -0.0082(14) C22 0.0582(19) 0.0360(15) 0.0451(17) -0.0041(13) 0.0271(15) -0.0009(14) C23 0.0578(19) 0.0329(14) 0.0481(17) -0.0018(13) 0.0303(15) -0.0050(13) C24 0.061(2) 0.0344(15) 0.0426(17) -0.0092(13) 0.0222(15) -0.0041(14) C25 0.060(2) 0.0474(19) 0.0460(18) -0.0086(15) 0.0179(16) -0.0072(16) C26 0.058(2) 0.0506(19) 0.0500(19) -0.0117(16) 0.0226(16) -0.0113(16) C27 0.057(3) 0.223(10) 0.077(4) 0.023(5) 0.003(3) 0.004(4) C28 0.058(2) 0.096(3) 0.053(2) 0.024(2) 0.0312(18) 0.012(2) C29 0.071(2) 0.0409(17) 0.0374(16) -0.0068(13) 0.0255(16) 0.0002(16) C30 0.071(2) 0.0382(16) 0.0373(16) -0.0010(13) 0.0268(16) 0.0032(15) C31 0.078(3) 0.055(2) 0.0402(18) -0.0026(16) 0.0135(18) 0.0091(19) C32 0.081(3) 0.058(2) 0.047(2) 0.0036(17) 0.0142(19) 0.021(2) C33 0.076(2) 0.0381(17) 0.0445(17) -0.0009(14) 0.0337(17) 0.0045(16) C34 0.061(2) 0.0364(16) 0.0497(18) -0.0034(14) 0.0342(16) -0.0018(14) C35 0.0590(19) 0.0329(15) 0.0487(18) -0.0014(13) 0.0319(16) 0.0000(14) C36 0.062(2) 0.073(3) 0.070(3) -0.023(2) 0.018(2) 0.006(2) C37 0.086(5) 0.242(15) 0.132(7) 0.026(8) -0.020(5) 0.018(7) C38 0.084(3) 0.0369(17) 0.0476(18) 0.0067(14) 0.0370(18) 0.0138(17) C39 0.075(2) 0.0463(19) 0.0464(18) 0.0032(15) 0.0351(18) 0.0065(17) C40 0.070(2) 0.0388(17) 0.0472(18) 0.0058(14) 0.0292(17) 0.0090(16) C41 0.075(2) 0.0387(17) 0.0435(17) 0.0027(14) 0.0276(17) 0.0110(16) C42 0.067(2) 0.0424(18) 0.0455(17) 0.0062(14) 0.0292(16) 0.0128(16) C43 0.076(2) 0.0387(17) 0.0511(19) 0.0057(14) 0.0359(18) 0.0063(16) C44 0.079(6) 0.044(5) 0.067(6) 0.006(4) 0.043(5) 0.006(5) C45 0.097(3) 0.096(3) 0.098(3) -0.0018(14) 0.0335(16) -0.0008(14) C46 0.079(5) 0.042(4) 0.090(6) -0.012(4) 0.035(4) -0.001(4) C47 0.062(5) 0.052(5) 0.072(7) -0.014(4) 0.030(5) 0.000(3) C48 0.065(2) 0.0390(16) 0.0407(16) 0.0044(13) 0.0244(15) 0.0133(15) C49 0.069(2) 0.0392(16) 0.0438(18) 0.0008(14) 0.0231(16) 0.0054(16) C50 0.082(3) 0.056(2) 0.0469(19) 0.0110(17) 0.0286(19) 0.013(2) C51 0.095(3) 0.079(3) 0.057(2) 0.008(2) 0.030(2) 0.025(3) C52 0.073(3) 0.125(5) 0.087(4) 0.050(4) 0.016(3) 0.007(3) C53 0.067(3) 0.081(3) 0.069(3) 0.015(2) 0.023(2) 0.020(2) C54 0.064(2) 0.0424(18) 0.0482(19) 0.0027(15) 0.0182(16) 0.0059(16) C55 0.061(2) 0.0449(18) 0.054(2) -0.0043(16) 0.0278(17) -0.0012(16) C56 0.057(2) 0.0492(19) 0.0434(17) -0.0017(14) 0.0243(15) 0.0001(15) C57 0.062(2) 0.052(2) 0.0409(17) 0.0029(15) 0.0245(15) 0.0054(16) C58 0.0529(19) 0.0506(19) 0.0434(17) -0.0030(14) 0.0268(15) 0.0011(15) C59 0.0518(18) 0.0516(19) 0.0451(18) -0.0031(15) 0.0250(15) -0.0038(15) C60 0.0489(18) 0.0471(18) 0.0501(18) -0.0077(15) 0.0282(15) -0.0054(14) C61 0.0533(18) 0.0409(16) 0.0434(16) -0.0046(13) 0.0282(14) 0.0020(14) C62 0.0510(17) 0.0440(17) 0.0427(16) -0.0060(14) 0.0222(14) -0.0031(14) C63 0.0507(18) 0.0516(19) 0.0495(18) -0.0069(15) 0.0268(15) -0.0090(15) C64 0.079(3) 0.113(4) 0.059(2) -0.010(3) 0.030(2) -0.049(3) C65 0.084(3) 0.122(5) 0.067(3) -0.016(3) 0.025(3) -0.058(4) C66 0.0560(19) 0.0357(16) 0.0460(17) -0.0025(13) 0.0286(15) 0.0044(14) C67 0.0528(18) 0.0346(15) 0.0464(17) -0.0039(13) 0.0280(15) 0.0012(13) C68 0.0459(18) 0.0484(19) 0.057(2) -0.0092(16) 0.0280(16) -0.0004(15) C69 0.0478(18) 0.0404(17) 0.065(2) -0.0151(15) 0.0300(17) -0.0079(14) C70 0.0464(17) 0.0356(16) 0.0502(18) -0.0098(13) 0.0219(14) 0.0011(13) C71 0.0458(17) 0.0377(16) 0.0473(18) -0.0096(13) 0.0171(14) -0.0011(13) C72 0.0521(18) 0.0322(15) 0.0441(16) -0.0091(12) 0.0194(14) -0.0040(13) C73 0.056(2) 0.049(2) 0.111(4) -0.028(2) 0.016(2) -0.0130(19) C74 0.060(3) 0.063(3) 0.126(5) 0.000(3) 0.021(3) -0.014(2) O13 0.0739(17) 0.0387(12) 0.0723(18) 0.0025(12) 0.0436(15) 0.0045(12) O14 0.0431(12) 0.096(2) 0.0421(13) -0.0211(13) 0.0200(10) -0.0235(14) O15 0.0506(14) 0.102(2) 0.0416(13) -0.0061(14) 0.0159(11) 0.0266(15) O16 0.0533(14) 0.0490(14) 0.0549(14) -0.0086(11) 0.0273(11) 0.0064(11) O17 0.0568(15) 0.0411(13) 0.0683(17) 0.0196(12) 0.0124(13) -0.0024(11) O18 0.0380(12) 0.0385(12) 0.0829(19) 0.0025(12) 0.0193(12) 0.0012(10) O19 0.0579(15) 0.0614(16) 0.0489(14) 0.0082(12) 0.0131(12) -0.0102(13) O20 0.0538(13) 0.0458(13) 0.0493(13) 0.0095(10) 0.0302(11) 0.0172(11) O21 0.0442(12) 0.0524(13) 0.0418(11) -0.0098(10) 0.0218(10) -0.0034(10) O22 0.0502(15) 0.098(2) 0.0578(17) -0.0063(17) 0.0008(13) 0.0113(16) O23 0.0666(18) 0.0622(18) 0.0674(18) 0.0028(14) 0.0024(14) -0.0237(14) O24 0.0452(12) 0.0371(11) 0.0537(13) 0.0026(10) 0.0195(10) -0.0026(9) C77 0.0436(16) 0.0363(15) 0.0459(16) -0.0028(13) 0.0234(13) -0.0046(13) C78 0.0391(15) 0.0385(15) 0.0391(15) -0.0024(12) 0.0175(12) -0.0018(12) C79 0.0397(15) 0.0453(17) 0.0358(15) 0.0004(13) 0.0183(12) -0.0010(13) C80 0.0421(16) 0.060(2) 0.0400(16) -0.0012(15) 0.0175(13) 0.0066(15) C81 0.0429(16) 0.059(2) 0.0348(15) 0.0009(14) 0.0152(13) 0.0015(15) C82 0.0470(16) 0.0409(16) 0.0383(15) -0.0022(13) 0.0231(13) -0.0098(13) C83 0.080(3) 0.090(4) 0.069(3) 0.003(3) 0.027(2) 0.050(3) C84 0.079(3) 0.213(9) 0.052(3) -0.011(4) 0.005(2) 0.081(5) C85 0.0549(19) 0.0377(16) 0.0434(17) -0.0053(13) 0.0271(15) -0.0116(14) C86 0.0500(17) 0.0384(16) 0.0389(15) -0.0021(12) 0.0221(14) -0.0096(13) C87 0.0450(16) 0.0432(17) 0.0447(17) -0.0095(13) 0.0250(14) -0.0123(13) C88 0.0429(16) 0.0375(16) 0.0462(17) 0.0007(13) 0.0201(13) -0.0025(13) C89 0.0381(15) 0.0372(15) 0.0425(16) 0.0051(12) 0.0149(13) -0.0057(12) C90 0.0404(16) 0.0384(16) 0.0432(16) 0.0074(13) 0.0128(13) -0.0068(13) C91 0.0500(18) 0.0382(16) 0.0408(16) 0.0075(13) 0.0146(14) -0.0060(14) C92 0.062(3) 0.049(2) 0.128(5) 0.026(3) 0.017(3) 0.003(2) C93 0.0416(19) 0.060(2) 0.098(3) -0.005(2) 0.018(2) 0.0041(17) C94 0.0378(15) 0.0308(14) 0.0481(17) 0.0053(12) 0.0174(13) -0.0011(12) C95 0.0423(16) 0.0380(15) 0.0477(17) 0.0045(13) 0.0204(13) -0.0003(13) C96 0.0561(18) 0.0308(14) 0.0566(19) 0.0051(13) 0.0376(16) 0.0065(13) C97 0.058(2) 0.0359(16) 0.071(2) -0.0100(16) 0.0463(18) -0.0075(14) C98 0.0432(16) 0.0386(16) 0.064(2) -0.0069(15) 0.0301(16) -0.0034(13) C99 0.0393(15) 0.0361(15) 0.0528(18) 0.0029(13) 0.0176(14) -0.0026(12) C100 0.052(2) 0.062(2) 0.072(3) -0.020(2) 0.0280(19) -0.0201(18) C101 0.097(4) 0.080(3) 0.091(4) -0.013(3) 0.031(3) -0.035(3) C102 0.094(3) 0.081(3) 0.078(3) -0.041(3) 0.043(3) -0.048(3) C103 0.095(3) 0.049(2) 0.081(3) -0.013(2) 0.064(3) -0.025(2) C104 0.067(2) 0.0351(16) 0.064(2) 0.0113(15) 0.0443(19) 0.0096(15) C105 0.103(3) 0.049(2) 0.090(3) 0.031(2) 0.078(3) 0.034(2) C106 0.097(3) 0.054(2) 0.091(3) 0.033(2) 0.070(3) 0.039(2) C107 0.070(2) 0.0464(18) 0.068(2) 0.0235(18) 0.047(2) 0.0240(18) C108 0.0501(17) 0.0334(15) 0.0550(19) 0.0092(14) 0.0308(15) 0.0090(13) C109 0.0481(17) 0.0319(14) 0.0517(17) 0.0064(13) 0.0299(14) 0.0078(13) C110 0.130(4) 0.066(3) 0.094(3) 0.034(2) 0.090(3) 0.049(3) C111 0.186(6) 0.108(4) 0.114(4) 0.059(3) 0.117(4) 0.098(4) C112 0.151(5) 0.113(4) 0.130(5) 0.071(4) 0.109(4) 0.095(4) C113 0.141(5) 0.078(3) 0.120(4) 0.051(3) 0.100(4) 0.071(3) C114 0.0453(16) 0.0314(14) 0.0510(17) 0.0057(13) 0.0245(14) 0.0062(12) C115 0.0430(17) 0.0473(18) 0.059(2) 0.0057(16) 0.0211(15) 0.0065(14) C116 0.0448(17) 0.0485(19) 0.0525(19) 0.0041(16) 0.0073(15) 0.0048(14) C117 0.0498(17) 0.0315(14) 0.0410(15) 0.0062(12) 0.0163(13) 0.0026(12) C118 0.0436(15) 0.0331(14) 0.0442(16) 0.0019(12) 0.0211(13) 0.0037(12) C119 0.0425(16) 0.0340(14) 0.0394(15) 0.0051(12) 0.0192(12) 0.0042(12) C120 0.046(2) 0.172(8) 0.094(4) -0.026(5) -0.001(2) 0.020(3) C122 0.0584(19) 0.0363(15) 0.0340(15) 0.0055(12) 0.0159(13) -0.0022(14) C123 0.0520(17) 0.0354(15) 0.0336(14) 0.0014(12) 0.0172(13) -0.0015(13) C124 0.0550(19) 0.0445(18) 0.0397(16) 0.0065(14) 0.0097(14) -0.0050(15) C125 0.0547(19) 0.0469(18) 0.0420(17) 0.0017(14) 0.0130(15) -0.0056(15) C126 0.0554(18) 0.0343(15) 0.0372(15) 0.0005(12) 0.0228(14) -0.0042(13) C127 0.0464(16) 0.0348(15) 0.0386(15) 0.0009(12) 0.0253(13) 0.0028(12) C128 0.0471(16) 0.0351(15) 0.0360(14) -0.0007(12) 0.0223(13) -0.0012(12) C129 0.0473(19) 0.056(2) 0.058(2) 0.0069(17) 0.0146(16) -0.0019(16) C130 0.096(4) 0.106(5) 0.084(4) -0.032(4) 0.007(3) -0.016(4) C131 0.0537(18) 0.0345(15) 0.0388(15) -0.0013(12) 0.0213(14) -0.0043(13) C132 0.0571(18) 0.0403(17) 0.0378(15) -0.0028(12) 0.0249(14) -0.0040(14) C133 0.0512(17) 0.0354(15) 0.0370(15) -0.0055(12) 0.0213(13) -0.0066(13) C134 0.0520(17) 0.0351(15) 0.0362(14) -0.0004(12) 0.0186(13) -0.0079(13) C135 0.0473(16) 0.0389(16) 0.0346(14) -0.0034(12) 0.0190(12) -0.0082(13) C136 0.0576(19) 0.0337(15) 0.0406(15) -0.0047(12) 0.0251(14) -0.0038(13) C137 0.0531(19) 0.0412(17) 0.057(2) 0.0110(15) 0.0226(16) -0.0011(15) C138 0.075(3) 0.0443(19) 0.076(3) 0.0103(19) 0.035(2) 0.0024(18) C139 0.074(3) 0.053(2) 0.082(3) 0.005(2) 0.037(2) 0.008(2) C140 0.0547(19) 0.0437(17) 0.0537(19) -0.0063(15) 0.0269(16) -0.0029(15) C141 0.0481(16) 0.0333(14) 0.0336(14) -0.0027(11) 0.0188(12) -0.0066(12) C142 0.0403(15) 0.0477(17) 0.0344(14) -0.0050(13) 0.0143(12) -0.0051(13) C143 0.0408(15) 0.0339(14) 0.0368(15) 0.0004(12) 0.0167(12) 0.0000(12) C144 0.0403(15) 0.0326(14) 0.0419(15) 0.0015(12) 0.0169(12) -0.0004(12) C145 0.0426(16) 0.0360(15) 0.0420(16) -0.0034(13) 0.0120(13) -0.0049(12) C146 0.0502(17) 0.0304(14) 0.0343(14) -0.0014(11) 0.0118(13) -0.0051(12) C147 0.062(2) 0.055(2) 0.0384(17) -0.0121(15) 0.0173(15) -0.0089(17) C148 0.153(5) 0.174(6) 0.053(3) -0.033(3) 0.032(3) -0.119(5) C149 0.058(2) 0.168(6) 0.090(4) -0.083(4) 0.036(2) -0.047(3) C150 0.0501(19) 0.066(2) 0.050(2) -0.0164(18) 0.0133(16) -0.0188(18) C155 0.0394(17) 0.080(3) 0.0453(18) -0.0141(18) 0.0216(14) -0.0085(17) N1 0.107(5) 0.222(10) 0.118(5) 0.057(6) 0.071(5) 0.033(6) C75 0.099(5) 0.164(8) 0.083(4) 0.037(5) 0.062(4) 0.039(5) C76 0.146(7) 0.106(5) 0.090(4) 0.010(4) 0.066(5) 0.047(5) N3 0.133(6) 0.231(11) 0.135(6) -0.053(7) 0.084(6) -0.038(7) C153 0.116(6) 0.158(8) 0.092(5) -0.032(5) 0.069(5) -0.042(6) C154 0.152(7) 0.126(6) 0.088(4) -0.015(4) 0.060(5) -0.054(6) C47A 0.075(9) 0.028(5) 0.053(7) -0.003(4) 0.029(7) 0.011(5) C46A 0.091(9) 0.054(7) 0.103(9) 0.003(7) 0.037(7) -0.006(7) C45A 0.086(7) 0.045(5) 0.103(7) -0.007(5) 0.055(6) 0.002(5) C44A 0.082(10) 0.060(11) 0.071(10) 0.006(9) 0.036(8) 0.000(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C22 O3 C28 116.5(3) . . ? C25 O4 C27 116.8(4) . . ? C35 O5 C36 117.9(3) . . ? C37 O6 C32 126.7(7) . . ? C63 O9 C64 117.8(3) . . ? C60 O10 C65 117.3(3) . . ? C72 O11 C73 116.7(3) . . ? C74 O12 C69 118.6(4) . . ? O1 C1 C2 117.4(3) . . ? O1 C1 C6 121.6(3) . . ? C2 C1 C6 120.9(3) . . ? C1 C2 C3 119.9(3) . . ? C1 C2 C11 118.2(3) . . ? C3 C2 C11 121.9(3) . . ? C2 C3 C4 120.0(3) . . ? C2 C3 C10 118.2(3) . . ? C4 C3 C10 121.8(4) . . ? C3 C4 C5 118.9(3) . . ? C3 C4 C7 121.7(3) . . ? C5 C4 C7 119.4(4) . . ? C6 C5 C4 122.2(3) . . ? C1 C6 C70 121.6(3) . . ? C5 C6 C1 117.9(3) . . ? C5 C6 C70 120.5(3) . . ? C4 C7 C8 109.2(4) . . ? C9 C8 C7 110.8(4) . . ? C10 C9 C8 108.3(5) . . ? C9 C10 C3 113.7(4) . . ? C12 C11 C2 118.1(3) . . ? C12 C11 C16 119.8(3) . . ? C16 C11 C2 122.0(3) . . ? O2 C12 C11 117.1(3) . . ? O2 C12 C13 121.8(3) . . ? C11 C12 C13 120.8(3) . . ? C12 C13 C14 117.5(3) . . ? C12 C13 C21 123.2(3) . . ? C14 C13 C21 118.7(3) . . ? C15 C14 C13 122.7(4) . . ? C14 C15 C16 118.9(3) . . ? C14 C15 C20 119.2(4) . . ? C16 C15 C20 121.9(4) . . ? C11 C16 C17 118.5(3) . . ? C15 C16 C11 120.2(3) . . ? C15 C16 C17 121.3(3) . . ? C16 C17 C18 113.2(4) . . ? C19 C18 C17 112.3(6) . . ? C18 C19 C20 116.3(6) . . ? C19 C20 C15 113.0(4) . . ? C22 C21 C13 123.2(3) . . ? C22 C21 C26 118.5(3) . . ? C26 C21 C13 118.3(3) . . ? O3 C22 C21 117.3(3) . . ? O3 C22 C23 123.2(3) . . ? C21 C22 C23 119.5(3) . . ? C24 C23 C22 121.8(3) . . ? C23 C24 C25 118.3(3) . . ? C23 C24 C29 120.5(3) . . ? C25 C24 C29 121.1(3) . . ? O4 C25 C24 115.3(3) . . ? O4 C25 C26 124.0(4) . . ? C26 C25 C24 120.7(4) . . ? C25 C26 C21 121.2(4) . . ? C24 C29 C30 109.3(3) . . ? C31 C30 C29 121.0(4) . . ? C31 C30 C35 118.0(3) . . ? C35 C30 C29 120.8(3) . . ? C30 C31 C32 121.9(4) . . ? O6 C32 C31 123.9(4) . . ? O6 C32 C33 116.1(4) . . ? C33 C32 C31 120.0(4) . . ? C32 C33 C34 118.5(3) . . ? C32 C33 C38 122.2(4) . . ? C34 C33 C38 119.3(4) . . ? C35 C34 C33 121.2(4) . . ? O5 C35 C30 115.9(3) . . ? O5 C35 C34 123.8(3) . . ? C34 C35 C30 120.3(3) . . ? C39 C38 C33 120.5(3) . . ? C43 C38 C33 121.1(4) . . ? C43 C38 C39 118.2(3) . . ? C38 C39 C40 122.2(3) . . ? C39 C40 C44 118.7(5) . . ? C39 C40 C44A 120.8(10) . . ? C41 C40 C39 118.9(3) . . ? C41 C40 C44 122.4(5) . . ? C41 C40 C44A 120.3(10) . . ? C40 C41 C42 119.8(3) . . ? C40 C41 C47 120.2(6) . . ? C40 C41 C47A 124.0(9) . . ? C42 C41 C47 119.7(5) . . ? C42 C41 C47A 115.5(9) . . ? C41 C42 C48 122.1(3) . . ? C43 C42 C41 119.5(3) . . ? C43 C42 C48 118.4(3) . . ? O7 C43 C38 120.8(3) . . ? O7 C43 C42 117.9(3) . . ? C38 C43 C42 121.3(4) . . ? C40 C44 C45 107.8(9) . . ? C46 C45 C44 110.0(8) . . ? C45 C46 C47 112.8(9) . . ? C46 C47 C41 115.2(8) . . ? C49 C48 C42 120.3(3) . . ? C57 C48 C42 119.6(3) . . ? C57 C48 C49 120.0(3) . . ? C48 C49 C50 119.3(3) . . ? C54 C49 C48 119.6(3) . . ? C54 C49 C50 121.1(4) . . ? C51 C50 C49 113.7(4) . . ? C52 C51 C50 112.3(4) . . ? C51 C52 C53 115.9(5) . . ? C54 C53 C52 112.5(4) . . ? C49 C54 C53 122.7(4) . . ? C49 C54 C55 119.2(4) . . ? C55 C54 C53 118.1(4) . . ? C56 C55 C54 122.6(3) . . ? C55 C56 C57 117.8(3) . . ? C55 C56 C58 118.6(3) . . ? C57 C56 C58 123.5(3) . . ? O8 C57 C48 116.5(3) . . ? O8 C57 C56 122.7(3) . . ? C48 C57 C56 120.7(4) . . ? C59 C58 C56 116.7(3) . . ? C63 C58 C56 125.5(3) . . ? C63 C58 C59 117.8(3) . . ? C60 C59 C58 120.9(3) . . ? O10 C60 C59 122.8(3) . . ? C61 C60 O10 115.8(3) . . ? C61 C60 C59 121.4(3) . . ? C60 C61 C62 117.3(3) . . ? C60 C61 C66 122.3(3) . . ? C62 C61 C66 120.1(3) . . ? C63 C62 C61 121.8(3) . . ? O9 C63 C62 122.1(3) . . ? C58 C63 O9 117.2(3) . . ? C58 C63 C62 120.6(3) . . ? C61 C66 C67 108.7(3) . . ? C68 C67 C66 120.0(3) . . ? C72 C67 C66 121.8(3) . . ? C72 C67 C68 118.0(3) . . ? C69 C68 C67 121.1(3) . . ? O12 C69 C68 123.8(3) . . ? O12 C69 C70 115.4(3) . . ? C70 C69 C68 120.8(3) . . ? C69 C70 C6 121.3(3) . . ? C69 C70 C71 118.1(3) . . ? C71 C70 C6 120.6(3) . . ? C70 C71 C72 121.4(3) . . ? O11 C72 C67 115.8(3) . . ? O11 C72 C71 124.0(3) . . ? C67 C72 C71 120.2(3) . . ? C80 O15 C84 116.5(3) . . ? C77 O16 C83 117.5(3) . . ? C91 O17 C92 116.5(3) . . ? C88 O18 C93 118.8(3) . . ? C119 O21 C155 115.8(2) . . ? C116 O22 C120 117.6(4) . . ? C130 O23 C125 117.7(5) . . ? C128 O24 C129 118.1(3) . . ? O16 C77 C78 123.4(3) . . ? O16 C77 C82 116.7(3) . . ? C78 C77 C82 119.9(3) . . ? C77 C78 C79 121.6(3) . . ? C78 C79 C143 116.5(3) . . ? C80 C79 C78 117.7(3) . . ? C80 C79 C143 125.7(3) . . ? C79 C80 O15 116.4(3) . . ? C81 C80 O15 122.6(3) . . ? C81 C80 C79 120.9(3) . . ? C82 C81 C80 121.5(3) . . ? C77 C82 C85 121.3(3) . . ? C81 C82 C77 118.3(3) . . ? C81 C82 C85 120.1(3) . . ? C82 C85 C86 108.2(3) . . ? C87 C86 C85 120.5(3) . . ? C91 C86 C85 121.5(3) . . ? C91 C86 C87 117.6(3) . . ? C88 C87 C86 121.6(3) . . ? O18 C88 C87 123.3(3) . . ? O18 C88 C89 116.5(3) . . ? C89 C88 C87 120.2(3) . . ? C88 C89 C94 122.1(3) . . ? C90 C89 C88 118.3(3) . . ? C90 C89 C94 119.6(3) . . ? C89 C90 C91 121.6(3) . . ? O17 C91 C86 115.6(3) . . ? O17 C91 C90 123.8(3) . . ? C90 C91 C86 120.6(3) . . ? C95 C94 C89 123.0(3) . . ? C99 C94 C89 119.1(3) . . ? C99 C94 C95 117.8(3) . . ? O19 C95 C94 121.4(3) . . ? O19 C95 C96 117.3(3) . . ? C96 C95 C94 121.3(3) . . ? C95 C96 C97 119.9(3) . . ? C95 C96 C104 118.3(3) . . ? C97 C96 C104 121.8(3) . . ? C96 C97 C103 120.8(4) . . ? C98 C97 C96 119.4(3) . . ? C98 C97 C103 119.8(4) . . ? C97 C98 C99 119.4(3) . . ? C97 C98 C100 122.2(3) . . ? C99 C98 C100 118.3(3) . . ? C94 C99 C98 122.0(3) . . ? C101 C100 C98 116.3(4) . . ? C102 C101 C100 108.2(4) . . ? C101 C102 C103 113.7(4) . . ? C97 C103 C102 111.6(4) . . ? C105 C104 C96 120.9(3) . . ? C105 C104 C109 119.5(3) . . ? C109 C104 C96 119.3(3) . . ? C104 C105 C106 120.0(3) . . ? C104 C105 C110 119.6(4) . . ? C106 C105 C110 120.4(4) . . ? C105 C106 C113 123.4(4) . . ? C107 C106 C105 119.0(3) . . ? C107 C106 C113 117.5(4) . . ? C106 C107 C108 122.5(4) . . ? C107 C108 C109 117.6(3) . . ? C107 C108 C114 118.6(3) . . ? C109 C108 C114 123.4(3) . . ? O20 C109 C104 117.3(3) . . ? O20 C109 C108 121.4(3) . . ? C108 C109 C104 121.1(3) . . ? C105 C110 C111 113.5(4) . . ? C112 C111 C110 111.5(5) . . ? C111 C112 C113 111.5(5) . . ? C106 C113 C112 111.6(4) . . ? C115 C114 C108 118.6(3) . . ? C115 C114 C119 118.0(3) . . ? C119 C114 C108 123.4(3) . . ? C116 C115 C114 121.5(3) . . ? O22 C116 C115 124.6(3) . . ? O22 C116 C117 114.8(3) . . ? C115 C116 C117 120.6(3) . . ? C116 C117 C122 120.7(3) . . ? C118 C117 C116 118.0(3) . . ? C118 C117 C122 121.2(3) . . ? C117 C118 C119 121.7(3) . . ? O21 C119 C114 116.3(3) . . ? O21 C119 C118 123.7(3) . . ? C118 C119 C114 120.0(3) . . ? C117 C122 C123 109.7(3) . . ? C124 C123 C122 121.0(3) . . ? C124 C123 C128 117.5(3) . . ? C128 C123 C122 121.4(3) . . ? C125 C124 C123 121.8(3) . . ? O23 C125 C126 120.9(3) . . ? C124 C125 O23 118.3(3) . . ? C124 C125 C126 120.8(3) . . ? C125 C126 C131 123.3(3) . . ? C127 C126 C125 117.4(3) . . ? C127 C126 C131 119.2(3) . . ? C128 C127 C126 121.2(3) . . ? O24 C128 C123 115.5(3) . . ? O24 C128 C127 123.2(3) . . ? C127 C128 C123 121.2(3) . . ? C132 C131 C126 119.4(3) . . ? C136 C131 C126 122.0(3) . . ? C136 C131 C132 118.1(3) . . ? C133 C132 C131 122.2(3) . . ? C132 C133 C134 119.1(3) . . ? C132 C133 C140 119.6(3) . . ? C134 C133 C140 121.3(3) . . ? C133 C134 C135 119.7(3) . . ? C133 C134 C137 121.5(3) . . ? C135 C134 C137 118.8(3) . . ? C134 C135 C136 120.0(3) . . ? C134 C135 C141 122.3(3) . . ? C136 C135 C141 117.7(3) . . ? O13 C136 C131 121.4(3) . . ? O13 C136 C135 117.6(3) . . ? C131 C136 C135 120.9(3) . . ? C138 C137 C134 115.1(3) . . ? C137 C138 C139 112.5(4) . . ? C138 C139 C140 110.0(4) . . ? C133 C140 C139 110.1(3) . . ? C142 C141 C135 119.8(3) . . ? C142 C141 C146 119.9(3) . . ? C146 C141 C135 120.3(3) . . ? O14 C142 C141 117.0(3) . . ? O14 C142 C143 121.8(3) . . ? C141 C142 C143 121.2(3) . . ? C142 C143 C79 123.9(3) . . ? C144 C143 C79 118.4(3) . . ? C144 C143 C142 117.6(3) . . ? C143 C144 C145 122.6(3) . . ? C144 C145 C146 119.0(3) . . ? C144 C145 C150 118.7(3) . . ? C146 C145 C150 122.3(3) . . ? C141 C146 C147 119.3(3) . . ? C145 C146 C141 119.6(3) . . ? C145 C146 C147 121.1(3) . . ? C148 C147 C146 114.7(4) . . ? C149 C148 C147 122.2(4) . . ? C148 C149 C150 123.1(4) . . ? C149 C150 C145 114.7(3) . . ? N1 C75 C76 176.4(10) . . ? N3 C153 C154 177.1(11) . . ? C46A C47A C41 113.6(15) . . ? C45A C46A C47A 122.3(17) . . ? C46A C45A C44A 115.3(15) . . ? C40 C44A C45A 114.3(13) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C1 1.366(5) . ? O2 C12 1.382(4) . ? O3 C22 1.370(5) . ? O3 C28 1.434(5) . ? O4 C25 1.380(5) . ? O4 C27 1.438(7) . ? O5 C35 1.361(5) . ? O5 C36 1.407(5) . ? O6 C32 1.368(6) . ? O6 C37 1.207(10) . ? O7 C43 1.370(5) . ? O8 C57 1.359(5) . ? O9 C63 1.383(4) . ? O9 C64 1.428(6) . ? O10 C60 1.386(4) . ? O10 C65 1.415(6) . ? O11 C72 1.370(4) . ? O11 C73 1.408(5) . ? O12 C69 1.382(4) . ? O12 C74 1.380(6) . ? C1 C2 1.391(4) . ? C1 C6 1.404(5) . ? C2 C3 1.392(5) . ? C2 C11 1.511(5) . ? C3 C4 1.395(5) . ? C3 C10 1.509(5) . ? C4 C5 1.397(5) . ? C4 C7 1.510(5) . ? C5 C6 1.382(5) . ? C6 C70 1.490(4) . ? C7 C8 1.611(7) . ? C8 C9 1.474(7) . ? C9 C10 1.454(6) . ? C11 C12 1.392(5) . ? C11 C16 1.408(5) . ? C12 C13 1.400(5) . ? C13 C14 1.404(5) . ? C13 C21 1.491(5) . ? C14 C15 1.381(5) . ? C15 C16 1.389(6) . ? C15 C20 1.512(5) . ? C16 C17 1.521(5) . ? C17 C18 1.530(6) . ? C18 C19 1.441(8) . ? C19 C20 1.496(6) . ? C21 C22 1.396(5) . ? C21 C26 1.408(6) . ? C22 C23 1.403(5) . ? C23 C24 1.387(5) . ? C24 C25 1.397(5) . ? C24 C29 1.497(5) . ? C25 C26 1.381(6) . ? C29 C30 1.526(5) . ? C30 C31 1.379(6) . ? C30 C35 1.401(5) . ? C31 C32 1.392(6) . ? C32 C33 1.390(6) . ? C33 C34 1.390(6) . ? C33 C38 1.490(5) . ? C34 C35 1.390(5) . ? C38 C39 1.396(6) . ? C38 C43 1.391(5) . ? C39 C40 1.400(5) . ? C40 C41 1.399(5) . ? C40 C44 1.501(8) . ? C40 C44A 1.501(13) . ? C41 C42 1.413(6) . ? C41 C47 1.513(7) . ? C41 C47A 1.520(9) . ? C42 C43 1.403(5) . ? C42 C48 1.497(5) . ? C44 C45 1.527(10) . ? C45 C46 1.490(8) . ? C46 C47 1.506(8) . ? C48 C49 1.406(5) . ? C48 C57 1.399(5) . ? C49 C50 1.515(5) . ? C49 C54 1.392(5) . ? C50 C51 1.491(6) . ? C51 C52 1.487(7) . ? C52 C53 1.519(7) . ? C53 C54 1.508(6) . ? C54 C55 1.394(5) . ? C55 C56 1.388(6) . ? C56 C57 1.406(5) . ? C56 C58 1.488(5) . ? C58 C59 1.412(5) . ? C58 C63 1.383(5) . ? C59 C60 1.390(5) . ? C60 C61 1.383(5) . ? C61 C62 1.402(5) . ? C61 C66 1.503(5) . ? C62 C63 1.393(5) . ? C66 C67 1.514(4) . ? C67 C68 1.394(5) . ? C67 C72 1.392(5) . ? C68 C69 1.393(5) . ? C69 C70 1.383(5) . ? C70 C71 1.386(5) . ? C71 C72 1.399(5) . ? O13 C136 1.379(4) . ? O14 C142 1.374(4) . ? O15 C80 1.398(4) . ? O15 C84 1.429(6) . ? O16 C77 1.372(4) . ? O16 C83 1.418(6) . ? O17 C91 1.378(4) . ? O17 C92 1.415(6) . ? O18 C88 1.369(4) . ? O18 C93 1.415(5) . ? O19 C95 1.376(4) . ? O20 C109 1.368(4) . ? O21 C119 1.372(4) . ? O21 C155 1.432(4) . ? O22 C116 1.368(5) . ? O22 C120 1.427(6) . ? O23 C125 1.395(5) . ? O23 C130 1.358(7) . ? O24 C128 1.370(4) . ? O24 C129 1.413(5) . ? C77 C78 1.388(4) . ? C77 C82 1.404(5) . ? C78 C79 1.400(4) . ? C79 C80 1.389(5) . ? C79 C143 1.493(4) . ? C80 C81 1.385(5) . ? C81 C82 1.383(5) . ? C82 C85 1.514(4) . ? C85 C86 1.515(4) . ? C86 C87 1.399(5) . ? C86 C91 1.392(5) . ? C87 C88 1.394(5) . ? C88 C89 1.391(5) . ? C89 C90 1.388(5) . ? C89 C94 1.497(4) . ? C90 C91 1.391(4) . ? C94 C95 1.396(5) . ? C94 C99 1.387(5) . ? C95 C96 1.385(5) . ? C96 C97 1.410(6) . ? C96 C104 1.492(5) . ? C97 C98 1.386(6) . ? C97 C103 1.515(4) . ? C98 C99 1.396(5) . ? C98 C100 1.516(5) . ? C100 C101 1.490(6) . ? C101 C102 1.460(7) . ? C102 C103 1.576(7) . ? C104 C105 1.398(5) . ? C104 C109 1.404(5) . ? C105 C106 1.400(6) . ? C105 C110 1.517(5) . ? C106 C107 1.387(6) . ? C106 C113 1.514(5) . ? C107 C108 1.395(5) . ? C108 C109 1.401(5) . ? C108 C114 1.494(5) . ? C110 C111 1.528(6) . ? C111 C112 1.500(9) . ? C112 C113 1.527(6) . ? C114 C115 1.389(5) . ? C114 C119 1.406(4) . ? C115 C116 1.387(6) . ? C116 C117 1.405(5) . ? C117 C118 1.379(5) . ? C117 C122 1.500(5) . ? C118 C119 1.401(4) . ? C122 C123 1.520(4) . ? C123 C124 1.395(5) . ? C123 C128 1.397(5) . ? C124 C125 1.379(5) . ? C125 C126 1.412(5) . ? C126 C127 1.398(5) . ? C126 C131 1.491(4) . ? C127 C128 1.388(4) . ? C131 C132 1.395(5) . ? C131 C136 1.392(5) . ? C132 C133 1.394(5) . ? C133 C134 1.399(4) . ? C133 C140 1.516(5) . ? C134 C135 1.400(5) . ? C134 C137 1.515(4) . ? C135 C136 1.402(5) . ? C135 C141 1.495(4) . ? C137 C138 1.510(5) . ? C138 C139 1.520(6) . ? C139 C140 1.524(6) . ? C141 C142 1.393(4) . ? C141 C146 1.404(5) . ? C142 C143 1.402(4) . ? C143 C144 1.389(5) . ? C144 C145 1.390(5) . ? C145 C146 1.398(5) . ? C145 C150 1.499(4) . ? C146 C147 1.512(4) . ? C147 C148 1.479(6) . ? C148 C149 1.376(7) . ? C149 C150 1.451(6) . ? N1 C75 1.156(14) . ? C75 C76 1.377(14) . ? N3 C153 1.134(14) . ? C153 C154 1.391(15) . ? C47A C46A 1.502(13) . ? C46A C45A 1.495(13) . ? C45A C44A 1.524(14) . ?