#------------------------------------------------------------------------------ #$Date: 2022-12-14 01:15:54 +0200 (Wed, 14 Dec 2022) $ #$Revision: 279877 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/81/1568119.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1568119 loop_ _publ_author_name 'Cohen, Seth M.' 'Karges, Johannes' 'Giardini , Miriam' 'Blacque, Olivier' 'Woodworth, Brendon' 'Siqueira-Neto , Jair' _publ_section_title ; Enantioselective Inhibition of the SARS-CoV-2 Main Protease with Rhenium(I) Picolinic Acid Complexes ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D2SC05473F _journal_year 2022 _chemical_formula_moiety 'C9 H5 F N O6 Re, H2 O' _chemical_formula_sum 'C9 H7 F N O7 Re' _chemical_formula_weight 446.36 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-I 2ya' _space_group_name_H-M_alt 'I 1 2/a 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2021-03-04 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6272) ; _audit_update_record ; 2022-09-06 deposited with the CCDC. 2022-12-13 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 96.2130(10) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 9.04380(10) _cell_length_b 11.1598(2) _cell_length_c 23.9385(4) _cell_measurement_reflns_used 9862 _cell_measurement_temperature 160(1) _cell_measurement_theta_max 76.2270 _cell_measurement_theta_min 3.6530 _cell_volume 2401.85(6) _computing_cell_refinement 'CrysAlisPro 1.171.40.68a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.68a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.68a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015b)' _computing_structure_solution 'SHELXT (Sheldrick, 2015a)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 160(1) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.3801 _diffrn_detector_type Atlas _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -69.00 28.00 1.00 1.00 -- -42.24 57.00-150.00 97 2 \w -87.00 -6.00 1.00 1.00 -- -42.24 125.00 30.00 81 3 \w -21.00 74.00 1.00 1.00 -- 42.24 -77.00 -30.00 95 4 \w 27.00 97.00 1.00 1.00 -- 42.24-125.00 0.00 70 5 \w 36.00 109.00 1.00 1.00 -- 111.00-111.00-120.00 73 6 \w 30.00 107.00 1.00 1.00 -- 111.00 -94.00 -30.00 77 7 \w 36.00 135.00 1.00 1.00 -- 111.00 -30.00 0.00 99 8 \w 40.00 135.00 1.00 1.00 -- 111.00 -45.00 -30.00 95 9 \w 104.00 178.00 1.00 1.00 -- 111.00 111.00 30.00 74 10 \w 61.00 146.00 1.00 1.00 -- 111.00 178.00 -90.00 85 11 \w 104.00 178.00 1.00 1.00 -- 111.00 111.00 120.00 74 12 \w 83.00 178.00 1.00 1.00 -- 111.00 61.00 -90.00 95 13 \w 104.00 178.00 1.00 1.00 -- 111.00 111.00 0.00 74 14 \w 61.00 146.00 1.00 1.00 -- 111.00 178.00 -60.00 85 15 \w 36.00 109.00 1.00 1.00 -- 111.00-111.00 120.00 73 16 \w 87.00 178.00 1.00 1.00 -- 111.00 45.00-180.00 91 17 \w -112.00 -16.00 1.00 1.00 -- -42.24 -57.00 60.00 96 18 \w -112.00 -16.00 1.00 1.00 -- -42.24 -57.00 150.00 96 19 \w -112.00 -16.00 1.00 1.00 -- -42.24 -57.00-120.00 96 20 \w 87.00 141.00 1.00 1.00 -- 111.00 30.00 0.00 54 21 \w 87.00 178.00 1.00 1.00 -- 111.00 45.00 90.00 91 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, Atlas' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0978774000 _diffrn_orient_matrix_UB_12 -0.0268121000 _diffrn_orient_matrix_UB_13 0.0553261000 _diffrn_orient_matrix_UB_21 0.1022040000 _diffrn_orient_matrix_UB_22 -0.0785461000 _diffrn_orient_matrix_UB_23 -0.0322061000 _diffrn_orient_matrix_UB_31 0.0964747000 _diffrn_orient_matrix_UB_32 0.1104286000 _diffrn_orient_matrix_UB_33 -0.0095383000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0222 _diffrn_reflns_av_unetI/netI 0.0117 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_number 12376 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 74.479 _diffrn_reflns_theta_min 3.715 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 20.255 _exptl_absorpt_correction_T_max 0.354 _exptl_absorpt_correction_T_min 0.119 _exptl_absorpt_correction_type analytical _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.68a (Rigaku Oxford Diffraction, 2019) Analytical numeric absorption correction using a multifaceted crystal model based on expressions derived by R.C. Clark & J.S. Reid. (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 2.469 _exptl_crystal_description plate _exptl_crystal_F_000 1664 _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.11 _exptl_crystal_size_min 0.07 _refine_diff_density_max 0.808 _refine_diff_density_min -0.710 _refine_diff_density_rms 0.107 _refine_ls_extinction_coef 0.000132(9) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.154 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 191 _refine_ls_number_reflns 2446 _refine_ls_number_restraints 3 _refine_ls_restrained_S_all 1.153 _refine_ls_R_factor_all 0.0180 _refine_ls_R_factor_gt 0.0174 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0271P)^2^+3.7647P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0463 _refine_ls_wR_factor_ref 0.0467 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2384 _reflns_number_total 2446 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d2sc05473f2.cif _cod_data_source_block 32 _cod_database_code 1568119 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.331 _shelx_estimated_absorpt_t_min 0.121 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All O(H,H) groups 2. Restrained distances O7-H7B \\sim O7-H7C with sigma of 0.005 O7-H7C \\sim O7-H7B \\sim O7-H7A with sigma of 0.005 3. Others Fixed Sof: H7B(0.5) H7A(0.5) 4.a Aromatic/amide H refined with riding coordinates: C5(H5), C6(H6), C7(H7) ; _shelx_res_file ; TITL joha0503_a.res in I2/a joha0503.res created by SHELXL-2018/3 at 15:52:41 on 04-Mar-2021 CELL 1.54184 9.0438 11.1598 23.9385 90 96.213 90 ZERR 8 0.0001 0.0002 0.0004 0 0.001 0 LATT 2 SYMM 0.5-X,+Y,-Z SFAC C H F N O Re UNIT 72 56 8 8 56 8 SADI 0.005 O7 H7b O7 H7c SADI 0.005 O7 H7c O7 H7b O7 H7a L.S. 10 PLAN 20 SIZE 0.07 0.11 0.18 TEMP -113.1(10) CONF list 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.027100 3.764700 EXTI 0.000132 FVAR 1.07680 RE1 6 0.599816 0.826266 0.362858 11.00000 0.02836 0.02026 = 0.02557 -0.00160 0.00187 -0.00215 F1 3 0.451496 0.584496 0.297707 11.00000 0.03630 0.03303 = 0.03846 -0.00539 -0.00810 -0.00232 O1 5 0.583379 1.098864 0.375537 11.00000 0.05845 0.02131 = 0.05568 -0.00443 0.00541 -0.00107 O2 5 0.322377 0.850981 0.278674 11.00000 0.05882 0.04323 = 0.04790 0.00071 -0.02587 0.00125 O3 5 0.788115 0.875754 0.267252 11.00000 0.08322 0.04272 = 0.05275 -0.00754 0.03914 -0.01463 O4 5 0.467076 0.785723 0.431769 11.00000 0.03014 0.02431 = 0.02896 -0.00001 0.00226 0.00166 H4A 2 0.506399 0.755466 0.460390 11.00000 0.05663 H4B 2 0.425530 0.848299 0.440217 11.00000 0.04553 O5 5 0.917709 0.662032 0.478920 11.00000 0.02721 0.03409 = 0.03563 -0.00600 -0.00390 0.00276 O6 5 0.780760 0.795347 0.427015 11.00000 0.02736 0.02480 = 0.03449 -0.00427 -0.00251 -0.00033 N1 4 0.631611 0.628424 0.367029 11.00000 0.02517 0.02260 = 0.02800 -0.00260 0.00426 -0.00016 C1 1 0.589287 0.995993 0.371003 11.00000 0.03821 0.03297 = 0.02979 -0.00023 0.00433 -0.00150 C2 1 0.426786 0.840506 0.309767 11.00000 0.04748 0.02650 = 0.03297 -0.00047 0.00098 -0.00286 C3 1 0.717287 0.855053 0.303062 11.00000 0.04929 0.02351 = 0.04030 -0.00439 0.01096 -0.00499 C4 1 0.556091 0.545407 0.336880 11.00000 0.02627 0.03040 = 0.02809 -0.00510 0.00287 -0.00156 C5 1 0.577177 0.423503 0.344063 11.00000 0.03058 0.02849 = 0.04286 -0.00939 0.00646 -0.00554 AFIX 43 H5 2 0.519245 0.367420 0.321251 11.00000 -1.20000 AFIX 0 C6 1 0.684828 0.386144 0.385339 11.00000 0.03686 0.02377 = 0.04450 -0.00025 0.00729 0.00216 AFIX 43 H6 2 0.703317 0.303140 0.391513 11.00000 -1.20000 AFIX 0 C7 1 0.766504 0.471665 0.418015 11.00000 0.02937 0.02723 = 0.03972 -0.00159 0.00313 0.00246 AFIX 43 H7 2 0.841122 0.447983 0.446905 11.00000 -1.20000 AFIX 0 C8 1 0.736972 0.591079 0.407622 11.00000 0.02619 0.02597 = 0.02940 -0.00475 0.00522 -0.00114 C9 1 0.820639 0.688549 0.441180 11.00000 0.02624 0.02796 = 0.03006 -0.00494 0.00710 -0.00151 O7 5 0.866980 1.010370 0.470075 11.00000 0.03268 0.02761 = 0.03742 -0.00478 0.00343 -0.00759 H7C 2 0.852556 0.937810 0.455153 11.00000 -1.50000 PART -1 H7B 2 0.789582 1.022458 0.489336 10.50000 -1.50000 PART -2 H7A 2 0.946653 1.001223 0.494913 10.50000 0.06726 HKLF 4 REM joha0503_a.res in I2/a REM wR2 = 0.0467, GooF = S = 1.154, Restrained GooF = 1.153 for all data REM R1 = 0.0174 for 2384 Fo > 4sig(Fo) and 0.0180 for all 2446 data REM 191 parameters refined using 3 restraints END WGHT 0.0271 3.7486 REM Highest difference peak 0.808, deepest hole -0.710, 1-sigma level 0.107 Q1 1 0.6010 0.6889 0.3616 11.00000 0.05 0.81 Q2 1 0.6732 0.7803 0.3677 11.00000 0.05 0.58 Q3 1 0.4923 0.7946 0.3208 11.00000 0.05 0.54 Q4 1 0.5940 0.9633 0.3617 11.00000 0.05 0.52 Q5 1 0.7328 0.8029 0.4028 11.00000 0.05 0.51 Q6 1 0.6993 0.8174 0.4165 11.00000 0.05 0.47 Q7 1 0.4665 0.8531 0.3383 11.00000 0.05 0.47 Q8 1 0.6824 0.8834 0.3765 11.00000 0.05 0.46 Q9 1 0.4913 0.8829 0.3404 11.00000 0.05 0.45 Q10 1 0.7813 0.6363 0.4239 11.00000 0.05 0.39 Q11 1 0.5566 0.8224 0.4239 11.00000 0.05 0.39 Q12 1 0.5171 0.8939 0.3550 11.00000 0.05 0.38 Q13 1 0.8425 0.8335 0.2807 11.00000 0.05 0.37 Q14 1 0.5805 1.0316 0.3605 11.00000 0.05 0.34 Q15 1 0.7395 0.5469 0.4164 11.00000 0.05 0.31 Q16 1 0.7840 0.5283 0.4035 11.00000 0.05 0.31 Q17 1 0.8815 0.8543 0.4418 11.00000 0.05 0.30 Q18 1 0.3767 0.5324 0.2879 11.00000 0.05 0.28 Q19 1 0.7313 0.7416 0.4351 11.00000 0.05 0.27 Q20 1 0.6318 0.4081 0.3792 11.00000 0.05 0.27 ; _shelx_res_checksum 46819 _shelx_hkl_file ; 0 0 -2 5297.05 95.5744 1 0 0 2 5158.43 109.743 18 0 0 -4 307733. 967.606 1 0 0 4 305283. 1085.94 18 0 0 -6 25258.6 326.649 1 0 0 6 24812.9 355.370 18 0 0 -8 114294. 463.439 2 0 0 8 112430. 821.453 18 0 0 -10 83205.7 726.564 1 0 0 -10 84440.8 330.805 2 0 0 10 84747.7 767.123 18 0 0 -12 102473. 852.651 1 0 0 12 106559. 924.305 18 0 0 -14 156606. 1121.63 1 0 0 14 164952. 1227.78 18 0 0 -16 19277.7 411.427 1 0 0 16 20671.4 469.769 3 0 0 16 20514.7 463.576 18 0 0 -18 109452. 1127.91 7 0 0 18 111317. 1114.15 3 0 0 -20 4959.20 229.498 20 0 0 -20 5087.87 245.964 7 0 0 20 5317.06 259.008 18 0 0 -20 5611.06 240.751 12 0 0 -20 5541.41 230.679 10 0 0 -22 37509.5 590.446 20 0 0 -22 37119.2 583.839 12 0 0 -22 38360.0 565.591 10 0 0 -24 3465.46 165.595 20 0 0 -24 3202.03 159.950 12 0 0 -24 3075.96 172.819 7 0 0 -26 22811.5 352.791 12 0 0 -26 23736.6 348.429 20 0 0 26 22743.8 437.250 16 0 0 28 2410.68 114.373 16 0 -1 1 18253.0 132.149 19 0 1 -1 17981.7 155.231 2 0 -1 3 21776.5 174.355 19 0 1 -3 21742.8 172.231 2 0 -1 -3 22387.3 162.942 1 0 1 -3 21776.2 253.414 1 0 -1 3 21635.3 210.791 18 0 -1 -5 1183.55 65.8122 1 0 1 -5 1058.09 80.3047 1 0 1 -5 1040.77 43.2612 2 0 1 5 1040.99 71.0794 18 0 -1 5 1149.61 76.3334 18 0 1 -7 37601.6 455.003 1 0 1 -7 39142.0 238.721 2 0 -1 7 38530.4 487.712 18 0 1 7 38470.1 474.387 18 0 -1 -9 7101.09 205.978 1 0 1 -9 7095.87 82.9609 2 0 1 -9 6888.60 214.779 1 0 -1 9 6926.67 231.289 18 0 1 9 6716.45 227.533 18 0 1 -11 87458.0 799.372 1 0 -1 -11 88559.6 750.860 1 0 1 11 87057.8 851.014 18 0 -1 11 87929.8 834.305 18 0 1 -13 53.7124 48.3041 1 0 -1 -13 48.6837 34.2554 1 0 -1 13 136.784 59.2409 18 0 1 13 81.3963 64.2369 18 0 1 -15 23527.7 464.257 1 0 -1 -15 23644.0 423.732 1 0 -1 15 23801.0 479.006 18 0 1 15 24763.8 511.830 18 0 -1 17 812.429 100.871 3 0 1 17 1014.23 123.478 3 0 1 -17 751.381 102.105 1 0 -1 17 732.093 101.173 18 0 1 17 953.386 116.927 18 0 1 -19 24984.3 513.876 1 0 1 19 24687.3 550.108 3 0 1 -19 25084.1 509.995 20 0 1 19 24339.8 495.916 21 0 -1 -19 24906.8 544.240 7 0 1 -19 25101.6 541.156 7 0 -1 19 25195.6 543.071 18 0 1 -19 24686.6 513.850 12 0 -1 -19 23264.6 479.447 12 0 1 -19 24976.6 494.041 10 0 1 21 6701.78 255.390 21 0 1 -21 7147.65 264.716 20 0 1 -21 7330.03 274.254 12 0 -1 -21 6709.74 253.291 12 0 1 -21 6694.17 249.823 10 0 -1 -21 6530.62 277.172 7 0 1 -21 6589.54 274.677 7 0 1 -23 3489.80 171.830 20 0 -1 -23 3494.32 179.000 20 0 1 23 3179.21 163.468 21 0 1 -23 3467.23 187.733 7 0 -1 -23 3570.39 194.374 7 0 1 -23 3546.81 179.863 12 0 -1 -23 3517.00 172.284 12 0 1 -23 3684.36 174.296 10 0 -1 -25 7405.94 224.422 20 0 -1 25 6820.03 267.433 16 0 -1 -25 7616.19 250.489 7 0 -1 -25 7132.31 212.664 12 0 1 -25 7250.53 222.967 12 0 1 -25 7108.02 207.819 10 0 1 27 9.67510 28.9350 16 0 -1 27 5.16652 43.8541 16 0 -1 -27 38.2168 21.7820 20 0 -1 29 4104.96 127.129 16 0 -1 29 4339.74 120.769 11 0 -2 0 59682.3 354.246 19 0 2 0 61825.6 315.336 4 0 2 0 60233.3 335.860 1 0 2 0 58119.8 268.818 3 0 2 2 193.340 15.9245 17 0 -2 2 295.052 27.7125 19 0 2 -2 116.976 18.5788 4 0 2 -2 339.508 16.9654 3 0 2 -2 112.228 33.5381 1 0 -2 4 43799.4 299.891 19 0 2 -4 43236.3 437.945 1 0 -2 6 388.889 39.8383 19 0 2 -6 415.785 67.2941 1 0 2 -6 563.448 44.4438 2 0 -2 6 474.129 56.5501 18 0 2 -8 13135.3 307.054 1 0 -2 -8 12526.7 219.396 1 0 -2 8 13438.5 289.919 18 0 2 8 13033.8 290.378 18 0 2 -10 33350.9 512.037 1 0 -2 10 32698.8 533.472 18 0 2 10 32905.0 537.634 18 0 -2 -12 10708.9 260.897 1 0 2 -12 11888.2 322.108 1 0 -2 12 11378.5 331.473 18 0 2 12 11857.1 352.097 18 0 2 -14 54897.1 733.623 1 0 2 14 58363.2 810.836 3 0 -2 14 56116.2 737.017 18 0 2 14 57820.5 807.488 18 0 2 16 17063.2 456.392 3 0 2 -16 16241.1 414.562 1 0 2 16 17327.1 466.199 18 0 -2 16 16621.0 417.816 18 0 2 18 19652.4 502.053 3 0 2 -18 20125.1 477.982 1 0 2 18 21839.5 541.995 18 0 -2 18 20768.5 481.051 18 0 2 18 19552.3 456.350 21 0 -2 -18 20925.7 498.425 7 0 2 -18 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274.810 61.2821 12 2 7 -21 170.742 53.1691 10 2 7 -19 193.140 56.9823 14 -2 7 19 199.658 84.8480 21 2 -7 -19 227.698 68.0021 12 2 7 -19 255.604 70.8826 10 2 7 -17 3942.48 206.278 14 -2 7 17 3978.12 221.315 21 2 -7 -17 3746.46 223.408 12 2 7 -17 3888.99 233.259 10 2 7 -15 31.5783 39.3406 5 -2 7 15 4.50684 83.7888 21 2 7 -15 4.17323 33.2424 15 2 7 -15 5.32566 59.5130 14 2 -7 -15-43.2278 62.9181 12 2 7 -13 875.503 114.769 5 -2 7 13 954.562 139.061 21 2 -7 -13 1059.79 134.217 19 -2 -7 13 1225.82 156.572 18 2 7 -13 1046.23 125.110 1 -2 7 13 676.518 105.142 3 2 7 -13 1175.67 138.746 14 2 7 -13 930.135 106.035 15 2 -7 -13 1046.89 129.656 12 2 7 -13 997.153 139.040 10 -2 7 13 1003.96 121.331 9 -2 7 11 1909.48 168.291 4 2 7 -11 1741.27 176.548 5 -2 7 11 1550.12 177.070 21 2 -7 -11 1707.13 181.665 19 -2 -7 11 1958.73 169.332 18 2 7 -11 2041.09 178.454 1 -2 7 11 1518.20 172.666 3 2 7 -11 1966.60 161.146 15 2 7 -11 1647.00 164.347 14 2 -7 -11 1800.95 161.040 12 2 7 -11 1783.86 181.284 10 -2 7 11 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10 -2 7 -17 603.283 89.9143 14 2 -7 17 424.435 109.883 16 2 7 17 651.061 106.813 21 2 7 17 512.530 106.244 6 -2 7 -17 472.041 83.6815 10 2 -7 19 523.327 106.652 16 -2 7 -19 781.793 86.7786 14 2 7 19 722.309 100.734 21 2 7 19 870.295 117.234 6 -2 7 -19 800.488 84.9073 5 -2 7 -19 754.845 91.9109 10 2 7 21 46.7988 48.6993 6 -2 7 -21-17.3349 31.9399 5 -2 7 -21 46.2197 30.5913 14 -2 7 -21 63.9495 41.4565 10 2 -7 23 613.075 68.9965 16 -2 -7 -23 808.094 63.6317 20 -2 7 -23 851.143 62.6056 10 2 7 23 712.885 65.0067 6 -2 8 24 9287.13 171.094 21 2 8 -24 9577.55 166.605 10 2 8 -22 436.337 42.3241 14 -2 8 22 512.734 67.2999 21 2 -8 -22 516.238 51.9893 12 2 8 -22 430.563 56.4131 10 2 8 -20 17737.1 320.632 14 -2 8 20 18702.3 369.173 21 2 -8 -20 17764.0 335.835 12 2 8 -18 2834.86 158.390 14 -2 8 18 3165.95 181.084 21 2 -8 -18 2873.45 168.520 12 2 8 -18 2859.29 183.383 10 2 8 -16 16804.4 389.619 5 2 8 -16 15526.9 408.477 14 2 8 -16 15155.0 348.911 15 -2 8 16 17464.2 435.789 21 2 -8 -16 16363.4 450.633 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44504.5 835.496 15 2 8 -6 45915.5 871.248 13 -2 8 6 44576.5 766.374 13 2 8 -6 44900.5 713.241 9 2 8 -6 45134.1 795.315 10 -2 8 6 44871.0 887.475 9 2 8 -4 1588.29 126.514 4 2 8 -4 915.748 128.248 5 2 -8 -4 901.499 131.422 19 -2 -8 4 929.786 109.844 18 2 8 -4 850.773 113.082 14 2 8 -4 935.412 131.351 15 2 8 -4 859.089 120.582 9 2 8 -4 748.919 116.582 10 2 8 -4 1434.92 180.407 13 -2 8 4 926.937 140.915 13 -2 8 4 942.411 155.360 9 2 8 -2 60148.0 753.818 4 2 8 -2 59380.7 878.578 5 2 -8 -2 59835.8 938.045 19 2 8 -2 60878.8 1038.37 13 -2 8 2 60273.9 995.390 13 -2 8 2 59638.9 1030.84 9 2 8 -2 60764.3 916.798 9 2 8 0 11258.3 378.932 5 2 8 0 11291.2 335.174 4 2 -8 0 11241.6 388.023 19 -2 -8 0 11135.7 382.602 19 2 8 0 10682.0 369.311 15 -2 8 0 11364.0 457.867 13 2 8 0 11314.0 438.048 13 2 8 0 10959.8 416.614 9 -2 8 0 11886.0 435.050 9 2 8 2 19404.4 457.993 4 2 8 2 18885.3 464.357 6 -2 8 -2 18835.6 511.481 5 2 8 2 18236.7 455.742 5 -2 8 -2 19356.0 573.574 1 -2 -8 -2 19408.5 537.858 19 2 -8 2 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833.047 13 2 9 9 52830.0 746.032 5 -2 9 -9 53073.3 950.904 5 2 9 9 54439.7 988.188 6 -2 9 -11 5269.17 272.695 14 2 9 11 5116.78 238.473 9 -2 9 -11 4899.86 240.210 13 2 9 11 5388.67 330.087 6 -2 9 -11 5017.01 278.315 5 -2 9 -13 22954.4 509.930 14 2 9 13 24089.8 522.031 21 -2 9 -13 23865.5 464.664 13 -2 9 -13 23739.2 530.859 5 -2 9 -15 16352.2 389.012 5 2 9 15 16970.1 477.973 6 -2 9 -15 16988.8 393.982 14 -2 9 -17 14444.9 314.342 5 2 9 17 14498.3 373.597 6 -2 9 -17 13417.1 307.106 14 -2 9 -17 13169.7 295.084 10 -2 9 -19 16198.8 270.874 5 -2 9 -19 16249.9 277.998 14 -2 9 -19 15637.1 262.833 10 2 9 21 1110.58 68.0383 6 -2 9 -21 1301.16 59.1444 14 -2 -9 -21 1130.01 58.3172 20 2 10 -20 100.377 24.4754 14 2 10 -20 76.0037 28.5519 10 -2 10 20 31.8160 24.0610 6 2 10 -18 191.613 31.3590 5 -2 10 18 175.659 43.7933 6 2 10 -18 212.484 45.4887 14 -2 10 18 139.036 48.7645 21 2 -10 -18 234.295 42.1133 12 2 10 -18 179.819 46.0859 10 -2 10 16 642.946 82.4533 6 2 10 -16 772.520 72.4813 5 2 10 -16 712.179 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452.287 118.999 13 -2 10 4 450.879 105.603 13 2 10 -4 457.097 112.275 5 -2 10 2 431.826 111.525 9 2 10 -2 412.052 102.002 9 2 10 -2 188.492 73.0862 14 -2 10 2 429.690 117.780 13 2 10 -2 293.497 95.3573 13 2 10 -2 393.813 95.7588 5 -2 10 0 281.832 95.8877 9 2 10 0 291.321 104.843 13 -2 10 0 333.749 110.332 13 2 10 0 232.568 82.1080 5 -2 10 0 242.454 83.2717 5 2 10 0 364.874 116.147 9 -2 10 -2 715.848 114.805 9 2 10 2 922.413 157.043 9 2 10 2 954.342 144.928 13 -2 10 -2 779.217 146.730 13 2 10 2 938.834 120.861 5 -2 10 -2 782.295 121.452 5 -2 10 -4 314.257 91.7521 14 -2 10 -4 31.9848 51.1288 9 2 10 4 68.5842 93.2247 9 -2 10 -4 87.2646 70.3263 13 2 10 4 125.595 70.1335 13 2 10 4 245.666 78.2224 5 2 10 4 9.06203 50.3589 6 -2 10 -4 276.208 94.5261 5 -2 10 -6 306.601 104.042 14 2 10 6 277.586 101.261 9 2 10 6 292.897 85.2774 13 -2 10 -6 383.465 101.019 13 2 10 6 238.997 73.5553 6 2 10 6 260.736 71.1182 5 -2 10 -6 280.755 92.6624 5 -2 10 -8 582.707 117.260 14 2 10 8 713.340 118.006 9 -2 10 -8 713.803 113.050 13 -2 10 -8 754.802 129.827 5 2 10 8 662.666 118.951 6 2 10 8 603.462 89.4254 5 -2 10 -10 1445.30 146.130 14 2 10 10 1460.59 132.499 9 -2 10 -10 1462.80 132.908 13 2 10 10 1530.86 163.720 6 -2 10 -10 1568.95 163.514 5 -2 10 -12-12.8700 36.3711 13 -2 10 -12 58.1174 53.2715 14 -2 10 -12 69.5191 62.1935 5 2 10 12-21.8887 58.9492 6 -2 10 -14 47.3717 19.3696 13 -2 10 -14 20.4436 44.6838 5 2 10 14 34.2346 47.9255 6 -2 10 -14 50.8358 49.2831 14 -2 10 -16 114.001 39.4557 5 2 10 16 65.8443 50.5289 6 -2 10 -16 133.511 43.5555 14 -2 10 -18 384.663 43.8488 5 2 10 18 346.367 52.2986 6 -2 10 -18 350.903 44.5322 14 -2 -10 -18 343.140 39.2089 20 2 11 -17 13960.5 214.700 10 2 11 -17 16263.0 243.276 14 -2 11 15 21.9944 35.2494 9 2 11 -15 44.8381 41.2865 10 2 -11 -15 45.9328 32.4461 12 2 11 -15 66.3766 31.1913 5 2 11 -15 24.1817 36.5567 14 2 11 -13 29868.3 483.524 10 -2 11 13 29218.5 429.460 9 2 -11 -13 31195.9 483.425 12 2 11 -13 30348.7 457.021 5 2 11 -13 30819.3 489.522 14 -2 11 11 2327.60 148.157 9 2 11 -11 1995.22 142.902 10 2 -11 -11 2223.94 149.697 12 2 11 -11 2327.04 134.470 13 2 11 -11 2008.07 146.397 5 2 11 -11 2124.34 160.772 14 2 11 -9 23329.9 465.365 10 -2 11 9 23898.1 496.945 9 2 -11 -9 23701.2 488.949 12 2 11 -9 25182.3 489.628 13 2 11 -9 24624.9 563.852 5 2 11 -9 23566.9 558.744 14 -2 11 7 13186.4 403.370 9 2 11 -7 12062.4 316.026 9 2 11 -7 13378.4 402.131 13 -2 11 7 11221.1 333.171 13 2 11 -7 13364.7 426.233 5 2 11 -7 12473.5 407.568 14 2 11 -5 20779.3 457.111 9 -2 11 5 21513.8 555.434 9 2 11 -5 21259.9 560.664 13 2 11 -5 21372.4 538.667 5 2 11 -5 20249.1 509.515 14 2 11 -3 27834.1 567.385 9 -2 11 3 28385.4 647.520 9 -2 11 3 26282.3 599.087 13 2 11 -3 28206.2 682.664 13 2 11 -3 27862.6 613.009 5 2 11 -1 14452.2 442.043 9 -2 11 1 14956.6 450.898 9 2 11 -1 15244.0 441.029 5 2 11 -1 15235.8 493.436 13 -2 11 1 14859.2 473.813 13 2 11 1 45909.2 806.543 9 -2 11 -1 42921.9 720.887 9 2 11 1 45575.4 731.315 5 -2 11 -1 43919.4 676.962 5 -2 11 -1 45513.3 849.069 13 2 11 1 45091.6 819.189 13 2 11 3 1950.04 190.360 9 -2 11 -3 1795.58 148.391 9 -2 11 -3 1883.06 190.274 13 2 11 3 1891.56 171.798 13 2 11 3 1937.51 153.717 5 -2 11 -3 1943.94 159.356 5 2 11 5 38724.7 699.366 9 -2 11 -5 37559.1 722.174 13 2 11 5 36588.4 652.313 13 2 11 5 37443.4 599.858 5 -2 11 -5 37108.6 666.111 5 2 11 7 124.179 70.1472 9 -2 11 -7 77.4820 62.0757 13 -2 11 -7 11.9029 61.7640 5 2 11 7 176.648 64.2001 6 2 11 7 92.8667 51.3070 5 -2 11 -7 114.441 66.3349 14 2 11 9 32226.2 525.923 9 -2 11 -9 31968.2 545.094 13 -2 11 -9 31669.1 598.969 5 2 11 9 32741.3 558.623 6 2 11 11 2865.13 143.730 9 -2 11 -11 3016.68 151.070 13 2 11 11 3051.27 171.576 6 -2 11 -11 2812.19 165.457 5 -2 11 -11 2895.06 162.564 14 -2 11 -13 24769.9 340.461 13 -2 11 -13 25375.8 403.836 5 2 11 13 25717.2 433.779 6 -2 11 -13 24800.6 399.002 14 -2 11 -15 3621.39 127.953 5 2 11 15 3498.44 133.994 6 -2 11 -15 3742.84 133.578 14 2 12 -14 9159.90 165.544 5 2 12 -14 9265.97 182.979 14 -2 12 12 7618.33 186.629 9 2 -12 -12 8393.92 201.341 12 2 12 -12 8139.82 198.438 5 2 12 -12 7763.26 204.626 14 -2 12 10 11979.5 275.376 9 2 -12 -10 12670.0 286.039 12 2 12 -10 11896.4 286.918 5 -2 12 8 824.570 96.5169 9 2 -12 -8 860.937 93.5087 12 2 12 -8 850.031 90.6393 13 2 12 -8 931.341 105.184 5 2 12 -8 881.657 95.0584 14 -2 12 6 29775.4 534.844 9 -2 12 6 27079.3 445.895 13 2 12 -6 30000.4 537.480 13 2 -12 -6 28601.5 473.765 12 2 12 -6 30594.0 545.765 5 2 12 -6 27761.6 481.366 14 -2 12 4 78.1612 64.6821 9 2 12 -4 190.230 52.7472 9 2 12 -4 71.6110 65.2162 13 -2 12 4 124.618 67.9425 13 2 12 -4 263.038 76.2379 5 2 12 -4 134.192 47.2456 14 2 12 -2 28795.2 522.434 9 -2 12 2 29297.9 553.760 9 2 12 -2 28588.4 532.715 5 2 12 -2 29268.7 605.935 13 -2 12 2 27726.9 545.801 13 2 12 0 7106.16 274.629 9 -2 12 0 6628.00 253.999 9 2 12 0 6938.66 259.245 5 2 12 0 6916.02 291.187 13 -2 12 0 6866.43 289.195 13 2 12 2 18342.6 456.109 9 -2 12 -2 17735.7 376.756 9 -2 12 -2 16700.3 359.152 5 2 12 2 18419.1 395.498 5 2 12 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68.8570 43.3454 13 -2 13 -1 18.3976 27.7708 9 2 13 1 31.5827 35.9090 9 2 13 1 241.021 48.7167 5 -2 13 -1 210.777 55.2409 13 2 13 3-79.8416 43.1558 9 -2 13 -3 22.3369 48.2003 13 -2 13 -5 151.490 40.7230 13 -2 13 -5 90.0064 33.7138 5 -2 13 -7 50.5555 26.3960 13 -2 13 -7 19.9692 25.9762 5 -3 0 29-5.97717 35.0595 16 3 0 -29 104.949 25.7150 12 3 0 -27 28.7110 30.4568 12 3 0 -27-13.3649 37.3734 7 3 0 -25 65.1631 43.7100 12 3 0 -25 69.4785 50.5305 7 3 0 -23 40.0133 49.9932 12 3 0 -23-6.78466 58.0584 7 3 0 -21 98.0398 51.5910 12 3 0 -21 28.7242 59.9112 7 3 0 -19 173.858 56.0475 12 3 0 -19-60.5785 52.4596 8 3 0 -19 126.481 65.7130 7 -3 0 19 220.268 80.5397 18 -3 0 19-35.2914 64.9153 17 3 0 -17-73.0678 59.4676 7 3 0 -17-72.2786 65.9645 8 3 0 -17 3.46036 29.5346 12 -3 0 17 94.0266 66.3652 17 -3 0 17 212.816 74.4074 18 3 0 -17 259.552 76.1667 1 -3 0 15 189.115 73.1039 17 3 0 -15 54.6440 56.8807 1 -3 0 13-27.3734 51.8583 18 -3 0 13 24.6213 66.6748 17 3 0 -13 44.1529 60.9863 1 3 0 -13 27.3718 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166.808 2 3 1 2 4203.80 137.339 3 3 -1 2 3723.03 97.8011 18 3 -1 2 3905.84 163.050 19 -3 -1 -2 4027.04 114.148 17 -3 1 -2 3887.77 125.625 17 3 1 2 3802.42 112.116 4 3 1 4 203060. 908.301 2 3 -1 4 207530. 884.793 3 3 1 4 197513. 986.160 3 3 -1 4 209067. 1029.10 2 3 -1 4 202370. 902.859 18 -3 -1 -4 204364. 813.319 17 -3 1 -4 201346. 952.005 17 3 1 4 196349. 614.891 18 3 -1 4 206861. 1204.12 19 3 1 4 197001. 862.256 4 3 -1 4 198317. 531.538 4 3 -1 6 9563.94 173.667 2 3 1 6 8771.04 230.182 3 -3 -1 -6 8590.99 182.622 1 3 1 6 8610.57 173.770 2 3 -1 6 8420.53 195.391 3 3 -1 6 8317.09 230.112 18 3 1 6 7919.05 177.216 18 -3 1 -6 8026.70 209.456 17 -3 -1 -6 8326.28 182.841 17 3 1 6 8252.25 196.586 4 3 -1 6 7619.52 129.650 4 -3 -1 -8 204759. 1004.71 1 3 -1 8 197177. 1054.00 3 3 1 8 200466. 1217.28 3 -3 1 -8 202064. 1159.46 1 3 -1 8 202093. 1200.25 18 3 1 8 189869. 1112.25 18 3 1 8 195320. 1060.95 4 -3 1 -10 9913.99 288.893 1 3 1 10 9555.64 296.737 3 3 -1 10 9524.16 259.820 3 3 -1 10 8974.60 263.594 18 3 1 10 9433.50 275.336 18 -3 1 -12 59118.5 770.002 1 3 -1 12 59844.9 710.186 3 3 -1 12 58635.1 701.805 18 3 1 12 58032.7 717.707 18 -3 1 -14 33669.4 598.014 1 3 1 14 33713.8 625.388 3 3 -1 14 34049.2 562.141 18 3 1 14 35194.7 588.615 18 3 1 16 15861.4 484.928 16 3 1 16 15127.8 421.689 21 -3 1 -16 14983.2 439.631 20 -3 -1 -16 14848.2 433.696 20 3 1 16 14740.9 418.188 3 3 -1 16 14453.4 381.208 18 -3 1 -18 44520.6 732.751 20 -3 -1 -18 44663.8 719.885 20 3 1 18 46958.6 807.126 16 3 -1 18 46392.6 847.052 16 -3 1 -20 12577.7 367.767 20 -3 -1 -20 12058.0 359.668 20 3 -1 20 13245.1 428.080 16 -3 1 -22 28902.8 497.012 20 -3 -1 -22 29467.8 504.818 20 3 1 22 30747.3 565.360 11 3 -1 22 31827.2 590.685 16 -3 -1 -24 1101.55 90.1159 20 -3 1 -24 1066.34 89.7493 20 -3 1 -24 1281.44 90.6489 10 3 1 24 1089.47 100.715 11 -3 -1 -24 1148.87 81.8076 10 3 -1 24 1025.01 103.067 16 -3 -1 -26 21676.4 297.547 20 -3 1 -26 21554.2 289.168 20 3 1 26 21802.9 322.474 11 3 -1 26 21574.3 318.544 11 -3 1 -26 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707.026 1 3 -2 7 70681.6 688.626 18 -3 2 -7 69929.5 696.509 17 3 2 7 67141.0 555.442 18 3 2 7 72570.5 670.175 4 3 2 9 6546.54 249.633 3 -3 2 -9 6151.85 233.157 1 3 -2 9 6332.18 241.328 18 3 2 9 6092.40 207.558 18 3 2 9 6121.75 219.858 4 -3 2 -11 40294.9 639.468 1 3 2 11 41852.6 686.742 3 3 -2 11 42290.7 627.605 18 3 2 11 40029.8 629.283 18 3 2 13 981.702 129.756 3 -3 2 -13 1233.25 133.237 1 3 -2 13 869.293 100.464 18 3 2 13 904.940 109.562 18 3 -2 15 48907.7 699.056 18 -3 2 -15 49322.4 773.887 1 3 2 15 49427.3 791.197 3 3 2 15 47992.9 756.467 21 3 -2 17 12068.9 453.927 16 3 -2 17 10791.0 333.273 18 3 2 17 11076.0 383.139 3 -3 2 -17 12106.1 394.296 20 -3 -2 -17 11573.4 369.737 20 3 2 17 11675.9 373.750 21 -3 2 -19 15435.7 420.027 20 -3 -2 -19 15268.5 412.979 20 3 2 19 16482.2 477.630 11 -3 2 -21 15973.4 389.411 20 -3 -2 -21 14698.4 370.255 20 3 2 21 15660.8 424.040 11 -3 2 -23 15509.0 332.592 20 -3 -2 -23 15422.3 335.433 20 -3 2 -23 15652.5 324.164 10 3 2 23 16180.8 376.763 11 -3 2 -25 9324.40 209.110 20 -3 -2 -25 9225.55 215.161 20 3 -2 25 9631.54 233.628 11 3 2 25 9464.52 234.220 11 -3 2 -25 9769.76 213.820 10 3 -2 25 8910.57 241.445 16 -3 -2 -27 3701.58 103.151 20 -3 2 -27 3806.59 97.9399 10 3 2 27 3589.21 103.015 11 3 -2 27 3645.00 107.332 11 3 -3 -28 108.586 27.6098 12 -3 -3 28 85.3584 42.3198 16 3 -3 -28 135.229 32.0032 7 3 -3 -26 645.491 68.1458 12 3 3 -26 746.123 73.1955 12 -3 3 26 634.664 64.2725 21 3 -3 -26 803.296 77.2344 7 3 3 -26 712.321 63.2948 7 -3 3 24-26.8280 68.4937 21 3 -3 -24 1.38239 43.1404 12 3 3 -24 17.2313 36.8404 12 3 3 -24-16.2859 25.2126 10 3 -3 -24 71.8364 44.8749 7 3 3 -24-59.7653 40.2688 7 -3 3 22 708.412 101.967 21 3 3 -22 816.923 103.881 12 3 -3 -22 843.615 99.5690 12 3 3 -22 847.223 93.3246 10 3 3 -22 865.073 96.4911 7 3 -3 -22 733.340 99.1936 7 -3 3 20 1007.85 123.028 21 3 3 -20 1141.41 117.753 7 3 -3 -20 1016.74 124.684 7 3 3 -20 1136.39 123.963 12 3 -3 -20 1036.24 118.881 12 3 3 -20 1213.54 115.702 10 -3 3 18 842.261 121.727 21 -3 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5332.91 240.115 2 3 3 -6 5849.16 200.475 1 3 -3 -6 5986.21 207.393 19 -3 -3 4 1777.52 103.616 17 -3 -3 4 1869.67 99.1770 18 3 3 -4 1739.29 98.7334 4 3 3 -4 1976.48 103.162 1 3 3 -4 1731.48 93.3089 3 3 3 -4 1609.26 129.330 2 3 -3 -4 2034.98 120.636 19 -3 -3 2 6436.02 163.399 17 -3 -3 2 6658.13 139.734 18 -3 3 2 6152.16 177.643 17 3 3 -2 6108.77 175.978 4 3 3 -2 5933.99 219.126 2 3 3 -2 6342.61 154.348 1 3 3 -2 5925.17 164.599 3 3 -3 -2 6179.12 201.502 19 -3 -3 0 13895.2 208.273 17 -3 3 0 14018.8 266.764 17 3 3 0 13856.9 261.896 4 3 3 0 13773.9 258.775 3 3 3 0 13644.6 314.186 2 3 -3 0 13391.6 290.078 19 -3 -3 -2 11177.5 164.371 17 -3 3 -2 10770.2 243.494 17 3 3 2 10404.2 230.882 4 3 3 2 10583.2 264.145 2 3 3 2 11233.3 248.631 3 3 -3 2 10799.4 269.126 19 -3 3 -4 16350.2 324.625 17 3 3 4 17007.0 317.232 4 3 3 4 16375.8 318.392 2 3 3 4 17280.0 335.602 3 3 -3 4 16753.6 351.720 19 -3 3 -6 299.467 68.9347 1 3 3 6 378.801 55.4619 2 3 -3 6 212.862 60.4567 19 3 -3 6 360.234 55.5577 18 -3 3 -6 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11642.5 275.725 20 -3 5 -22 11571.6 270.830 10 3 5 22 11908.0 283.778 11 -3 -5 -24 48.3950 30.6979 20 3 -5 24 41.7105 26.3975 11 3 5 24 2.47379 21.7061 11 -3 5 -24 6.15915 26.9554 10 3 -5 24-10.5776 40.3659 16 -3 6 25 3104.38 120.053 21 3 -6 -25 2978.95 106.107 12 3 6 -25 3024.28 105.051 10 -3 -6 25 2670.23 129.776 16 3 -6 -23-16.8026 48.1045 12 3 6 -23-4.90663 40.5864 10 -3 6 23-80.8672 75.6198 21 3 -6 -21 5889.33 209.066 7 -3 6 21 6311.13 239.779 21 3 -6 -21 5916.05 223.835 12 3 6 -21 6122.39 229.490 10 3 -6 -19 890.913 98.7955 7 -3 6 19 718.799 118.874 21 3 -6 -19 806.507 110.104 12 3 6 -19 776.687 103.161 10 3 6 -19 667.486 86.4463 14 -3 6 17 450.735 103.797 21 3 6 -17 371.412 63.7264 15 3 6 -17 486.645 84.3423 14 3 -6 -17 220.133 76.5168 12 3 6 -17 276.251 83.9143 10 3 6 -15 4589.26 261.191 1 -3 6 15 4512.79 278.045 3 -3 6 15 4539.15 253.590 21 3 -6 -15 4621.58 246.877 8 3 6 -15 4649.59 239.772 14 3 6 -15 4527.02 216.485 15 3 -6 -15 4140.49 257.598 12 3 6 -15 4289.68 270.016 10 3 6 -13 372.121 84.7153 1 -3 6 13 303.043 102.809 21 3 -6 -13 401.057 92.8922 19 -3 -6 13 305.078 83.2150 18 -3 6 13 69.1064 78.9096 9 3 -6 -13 169.473 72.6839 8 3 6 -13 220.814 64.5686 15 3 6 -13 187.474 67.5631 14 3 -6 -13 201.675 77.4172 12 3 6 -13 228.559 81.6883 10 3 6 -11 14149.7 430.636 5 -3 6 11 13564.1 445.420 21 3 -6 -11 14149.4 457.994 19 -3 -6 11 14041.7 422.635 18 3 6 -11 13540.2 439.653 1 3 6 -11 13736.5 450.057 14 3 6 -11 12726.9 397.556 15 3 -6 -11 14600.4 427.732 12 -3 6 11 14142.1 431.819 9 3 6 -11 14358.7 463.526 10 3 -6 -9 412.457 88.2614 19 -3 -6 9 409.699 85.7526 18 3 6 -9 539.928 94.0117 2 3 6 -9 418.126 87.0022 1 3 6 -7 16488.8 505.243 2 3 6 -7 16651.0 424.462 1 3 -6 -7 16210.1 459.871 19 -3 -6 7 16950.8 390.440 18 3 6 -7 16122.8 386.047 4 3 6 -5 3217.90 231.575 2 3 6 -5 2970.63 159.853 1 3 -6 -5 2856.04 188.885 19 -3 -6 5 3201.46 159.606 18 -3 6 5 2857.81 165.117 17 3 6 -5 2729.76 153.341 4 3 6 -3 11026.9 405.317 2 3 6 -3 10421.8 256.125 3 -3 -6 3 11207.9 272.481 18 -3 6 3 10698.4 312.405 17 3 6 -3 10125.4 287.273 4 3 -6 -1 272.855 68.6592 19 -3 6 1 337.988 64.6218 17 -3 -6 1 213.475 53.5787 19 3 6 -1 295.852 56.8390 4 3 6 -1 369.012 56.6398 3 3 6 1 2950.70 149.883 3 3 -6 1 3258.32 183.519 19 -3 6 -1 3141.39 185.139 17 3 6 1 3021.02 162.501 4 3 6 3 12324.5 327.611 3 -3 6 -3 11574.0 373.879 1 3 6 3 11488.9 326.997 4 3 -6 3 11747.3 349.100 19 3 6 5 3985.68 204.477 3 -3 6 -5 4284.47 240.244 1 3 -6 5 3913.25 207.585 19 3 6 5 3870.58 204.004 4 -3 6 -7 15681.8 474.404 1 3 6 7 17432.5 456.581 3 3 -6 7 16456.6 433.967 19 3 6 7 16268.3 446.916 4 3 -6 7 16435.9 400.442 18 3 6 9 17636.2 439.102 5 3 6 9 17543.8 539.296 6 3 6 9 16988.6 490.466 4 3 6 9 16257.3 466.242 21 3 -6 9 18699.1 467.097 19 3 -6 9 17627.6 445.974 18 -3 6 -9 17689.3 525.165 1 3 6 9 18080.5 509.165 3 -3 6 -9 17478.7 469.136 13 3 6 9 18401.4 490.214 11 3 6 11 9932.48 405.376 4 3 6 11 10885.1 455.218 6 3 6 11 9714.06 384.620 21 3 -6 11 10147.5 362.671 18 -3 6 -11 10683.4 427.213 1 3 6 11 10344.5 409.004 3 3 -6 11 10904.2 417.446 16 -3 6 -11 11110.3 390.177 14 -3 6 -11 10502.2 350.167 13 3 6 11 11066.6 401.790 11 -3 6 -11 10706.8 394.195 10 -3 6 -13 2147.21 194.046 20 3 6 13 1989.63 176.937 21 3 -6 13 1997.96 177.368 18 -3 6 -13 2096.59 172.238 14 3 -6 13 2316.84 215.627 16 3 6 13 2584.75 204.962 11 -3 6 -13 2371.42 184.537 10 3 6 13 2034.46 211.233 4 3 6 13 2046.30 217.158 6 -3 6 -13 2188.00 210.100 1 3 6 13 2121.05 203.571 3 3 -6 15 3506.43 267.065 16 -3 6 -15 3647.74 211.381 14 -3 6 -15 3731.68 229.960 20 3 6 15 3768.01 228.083 21 -3 6 -15 3762.75 214.267 10 3 6 15 4091.34 260.643 11 3 6 15 3712.06 257.020 6 3 6 17 36.1545 67.6971 6 3 -6 17 84.3855 78.1613 16 3 6 17 57.3432 74.7256 21 -3 6 -17 87.4362 54.3637 14 3 6 17 40.8312 60.6021 11 -3 6 -17 67.0266 53.9546 10 3 6 19 5030.64 233.133 6 -3 6 -19 4832.83 194.915 14 3 -6 19 4765.48 251.725 16 -3 6 -19 4826.83 203.739 10 3 6 19 5104.98 220.212 11 3 -6 21 818.602 102.668 16 -3 6 -21 867.220 74.1764 14 -3 -6 -21 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748.127 18 4 6 6 59794.0 857.446 11 4 6 6 59813.1 878.471 9 4 6 6 57636.1 799.674 5 4 6 6 57862.6 836.118 4 4 6 6 59207.0 892.713 6 -4 6 -6 59768.1 923.346 1 4 -6 8 20614.2 517.607 16 4 -6 8 20705.9 478.132 18 4 -6 8 19656.3 513.723 19 -4 6 -8 20963.4 565.280 1 4 6 8 21788.9 545.950 3 4 6 8 22111.0 550.595 11 4 6 8 22583.1 521.483 9 4 6 8 21167.7 537.054 4 4 6 8 21430.5 569.097 6 4 -6 10 63706.5 878.105 18 4 -6 10 68052.9 1031.32 16 4 6 10 68027.3 1003.59 11 4 6 10 66127.0 997.026 4 4 6 10 66959.3 1055.30 6 -4 6 -10 63895.0 1032.41 1 4 6 10 65715.2 1011.26 3 4 -6 12 238.579 98.2891 16 4 6 12 86.7462 77.4599 11 -4 6 -12 262.705 86.3831 10 -4 6 -12 3.52950 54.2834 13 -4 6 -12 386.485 90.8825 14 4 6 12 108.635 91.5982 6 4 6 14 53989.8 891.167 6 -4 6 -14 53081.7 767.396 10 4 -6 14 51660.8 923.069 16 -4 -6 -16 5878.97 246.595 20 4 6 16 6466.65 280.258 6 4 6 16 6183.88 285.857 11 -4 6 -16 5926.31 242.360 10 4 -6 16 6623.73 312.858 16 -4 6 -16 5911.92 245.164 14 -4 -6 -18 30178.6 489.679 20 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61.5715 14 4 7 -13 26.2852 56.2412 15 -4 7 13 55.5575 96.8509 21 4 -7 -13 32.5683 53.5576 12 4 7 -13-124.041 88.6063 10 4 7 -11 5337.46 259.130 5 4 7 -11 5560.18 279.455 15 4 7 -11 5560.29 295.092 14 4 -7 -11 5931.62 308.296 19 -4 7 11 5941.73 301.708 21 4 -7 -11 5240.97 275.892 12 -4 7 11 5687.01 285.203 9 4 7 -11 5292.73 294.542 10 4 7 -9 3731.98 231.416 5 4 -7 -9 4190.22 263.111 19 -4 7 9 3900.08 255.019 21 4 7 -9 4393.97 263.719 15 4 7 -9 4166.00 256.097 14 4 7 -9 4142.15 235.979 13 4 7 -9 3727.58 246.863 10 4 7 -7 169.830 58.2203 5 4 7 -7 157.827 68.5228 6 4 -7 -7 288.196 89.3247 19 4 7 -7 263.111 86.4138 14 4 7 -7 146.267 83.4351 15 4 7 -7 79.8203 63.5081 13 4 7 -7 236.199 78.7473 10 4 7 -5 3298.58 210.395 5 4 7 -5 3480.19 196.318 4 4 7 -5 3291.62 181.583 6 4 -7 -5 3160.66 221.081 19 4 7 -5 3318.42 220.869 14 4 7 -5 3791.01 245.758 15 -4 7 5 3678.21 232.412 13 4 7 -5 3452.16 248.411 13 4 7 -5 3645.27 222.240 10 4 7 -5 3630.02 217.508 9 4 7 -3 752.632 91.2959 4 4 7 -3 1046.44 129.447 5 4 7 -3 835.457 102.589 6 4 -7 -3 550.758 103.665 19 -4 7 3 750.105 113.322 17 4 7 -3 624.767 73.8232 3 4 7 -3 623.378 102.359 14 4 7 -3 666.236 110.288 15 -4 7 3 667.139 121.002 13 4 7 -3 718.881 97.6217 11 4 7 -3 734.703 135.396 13 4 7 -3 546.822 107.034 9 4 7 -3 587.796 101.052 10 4 7 -1 9535.05 345.094 5 4 7 -1 9673.38 320.524 6 4 7 -1 9874.40 324.959 4 4 -7 -1 9921.64 370.814 19 -4 7 1 10042.5 368.681 17 4 7 -1 9820.94 304.778 3 4 7 -1 9389.14 339.578 15 4 7 -1 9263.15 336.062 14 4 7 -1 9515.80 327.530 11 -4 7 1 9657.98 403.797 13 4 7 -1 9745.41 402.989 13 4 7 -1 9122.51 374.986 9 4 7 -1 9739.43 335.867 10 4 7 1 193.240 96.8692 9 4 7 1 254.069 62.4936 11 4 7 1 79.3300 57.7859 10 4 -7 1 159.359 70.6412 19 -4 -7 -1 111.354 59.6762 19 4 7 1 65.1863 53.9348 15 4 7 1 185.891 61.2220 14 -4 7 -1 210.918 103.713 13 4 7 1 167.860 87.7180 13 -4 7 -1 261.213 79.9863 1 4 7 1 174.558 49.9896 3 4 7 1 101.210 59.8711 5 4 7 1 162.545 57.3230 4 4 7 1 232.781 63.2529 6 4 7 3 2339.58 176.150 4 4 7 3 2323.72 173.531 5 4 7 3 2233.22 171.797 6 4 -7 3 2177.62 177.765 19 4 7 3 2116.70 155.843 3 -4 7 -3 2248.91 194.553 1 -4 7 -3 2009.05 207.869 13 4 7 3 2149.54 158.880 11 4 7 3 2225.33 200.343 9 -4 7 -3 1842.64 155.022 9 4 7 5 65.0731 79.7534 9 4 7 5 52.8494 40.0859 11 4 -7 5 77.8979 64.8367 19 4 -7 5 113.012 48.8904 18 -4 7 -5 20.0398 56.0870 1 4 7 5 48.8699 34.8839 3 -4 7 -5 80.4952 65.4716 13 4 7 5 80.2972 65.7617 5 4 7 5 44.0440 54.0406 4 4 7 5-38.5230 64.3314 6 4 7 7 1495.60 153.011 9 4 -7 7 1373.71 146.384 19 4 -7 7 1705.92 151.705 18 -4 7 -7 1563.21 175.008 1 4 7 7 1440.54 150.350 3 -4 7 -7 1571.68 166.317 14 4 7 7 1608.64 149.811 11 -4 7 -7 1702.72 160.768 13 4 7 7 1613.27 147.367 5 4 7 7 1328.40 149.644 4 4 7 7 1740.38 167.423 6 4 -7 9 14874.9 456.299 16 4 -7 9 13550.7 409.653 18 4 7 9 15035.4 463.131 11 4 7 9 14957.1 423.280 9 -4 7 -9 14152.6 430.850 13 4 7 9 14043.4 483.078 6 -4 7 -9 14477.0 463.660 14 4 7 11 416.485 100.011 11 4 -7 11 371.504 100.343 16 -4 7 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19740.7 499.612 4 -4 8 0 19165.4 574.367 1 4 -8 0 19443.5 553.499 19 4 8 0 19280.8 484.204 14 4 8 0 19270.4 494.831 15 4 8 0 19393.2 487.825 11 -4 8 0 19650.2 592.957 13 4 8 0 19705.1 581.372 13 -4 8 0 19444.4 544.936 9 4 8 0 20285.9 493.716 10 4 8 0 19616.4 562.106 9 4 8 2 32073.7 637.849 5 4 8 2 31257.6 623.732 6 4 8 2 33555.8 667.482 4 4 -8 2 31816.2 691.824 19 -4 8 -2 32554.6 755.847 1 4 8 2 30509.5 585.220 14 4 8 2 31738.5 599.201 15 -4 8 -2 31443.9 728.293 14 -4 8 -2 33389.0 793.283 13 4 8 2 32239.7 623.709 11 4 8 2 33349.6 752.115 9 -4 8 -2 30659.2 633.349 9 4 8 4 15016.4 431.877 5 4 8 4 14322.6 441.721 6 4 8 4 15851.0 480.122 4 4 -8 4 14781.5 466.572 19 4 -8 4 14082.6 410.825 18 -4 8 -4 14238.2 517.666 14 -4 8 -4 14246.1 505.110 1 4 8 4 14968.1 433.604 3 -4 8 -4 14381.4 505.337 13 4 8 4 14556.4 429.301 11 4 8 4 14967.0 482.242 9 -4 8 -4 13884.9 395.081 9 4 8 6 32834.1 669.763 9 4 8 6 33183.9 651.649 11 -4 8 -6 31842.9 702.698 13 4 8 6 32361.8 631.763 5 4 8 6 32640.3 688.773 6 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293.220 86.3121 5 4 9 5 363.964 90.7117 6 -4 9 -7 26525.3 624.656 14 4 9 7 27590.9 570.364 9 -4 9 -7 28234.4 610.983 13 4 9 7 28755.3 581.977 11 4 9 7 27806.8 616.256 6 -4 9 -7 26212.8 612.268 5 4 9 9 13904.6 400.648 11 -4 9 -9 13607.2 392.156 13 -4 9 -9 13054.7 406.746 14 4 9 9 14140.9 444.477 6 -4 9 -11 19940.1 423.620 13 -4 9 -11 19573.8 451.388 14 4 9 11 20750.7 534.435 6 -4 9 -11 19594.4 469.917 5 -4 9 -13 22398.0 433.416 14 4 9 13 22676.5 481.393 6 -4 9 -13 21224.8 431.445 5 -4 9 -15 5743.80 193.726 14 4 9 15 5981.84 213.629 6 -4 9 -15 5515.20 190.791 5 -4 9 -17 14114.2 248.860 14 4 9 17 14518.8 269.455 6 -4 9 -17 14462.3 250.707 5 4 -10 -18 612.128 52.8268 12 4 10 -18 655.088 51.5946 14 4 10 -18 637.109 56.9819 10 4 10 -16 70.5646 37.3728 14 -4 10 16-4.06702 43.9279 21 4 -10 -16 108.021 41.5703 12 -4 10 16 180.473 42.5694 9 4 10 -16 135.649 46.4220 10 4 10 -14 1439.58 126.989 10 -4 10 14 1444.77 106.629 9 4 10 -14 1491.75 110.500 14 4 -10 -14 1581.39 119.968 12 4 10 -14 1547.00 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681.203 2 6 1 -3 25960.6 638.791 2 -6 -1 3 25837.5 477.607 17 -6 1 3 27284.1 501.893 17 6 -1 -1 76.9114 73.7409 2 6 1 -1 14.6917 60.5730 2 6 1 -1 87.2685 49.8731 3 -6 -1 1 68.7172 43.3481 17 -6 1 1 153.745 52.5536 17 6 -1 1 15882.9 458.413 2 6 1 1 15567.4 436.409 2 6 1 1 16086.1 383.552 3 -6 -1 -1 15782.3 347.330 17 -6 1 -1 15708.6 372.595 17 6 -1 3 5722.83 250.931 2 6 1 3 5410.48 238.264 2 6 -1 3 5945.55 239.608 3 6 1 3 5635.10 235.295 3 -6 -1 -3 5563.16 207.586 17 -6 1 -3 5703.64 229.000 17 6 -1 5 28304.3 523.267 3 6 1 5 27586.4 525.271 3 -6 -1 -5 27081.0 465.762 17 -6 1 -5 28669.8 522.155 17 -6 1 -7 6059.27 281.616 20 6 1 7 6707.03 272.101 3 -6 1 -7 6558.10 270.810 1 6 1 7 5468.72 256.939 11 -6 1 -7 6455.81 262.790 17 6 1 7 5788.87 262.134 16 6 -1 7 6291.58 281.118 16 -6 1 -9 8734.78 352.468 20 -6 -1 -9 8319.81 330.416 20 6 1 9 8595.96 323.445 3 6 -1 9 8515.69 339.043 16 6 1 9 8480.27 330.961 16 6 1 9 8323.17 328.179 11 6 1 11 26212.2 595.685 16 6 -1 11 26255.5 613.286 16 6 1 11 25655.1 598.858 11 6 -1 11 26027.7 575.968 11 -6 1 -11 27481.2 636.358 20 -6 -1 -11 26317.5 604.867 20 6 1 13 4199.32 246.727 16 6 -1 13 4215.15 265.590 16 6 1 13 3689.12 240.377 11 6 -1 13 3520.59 227.626 11 -6 1 -13 4152.88 250.169 20 -6 -1 -13 3964.91 237.216 20 6 1 15 17928.5 449.068 16 6 -1 15 17451.8 473.198 16 -6 1 -15 16818.7 452.344 20 -6 -1 -15 17135.7 444.112 20 6 1 15 15899.9 452.404 11 -6 1 -17 467.912 85.3432 20 -6 -1 -17 447.887 84.2723 20 6 1 17 445.057 87.5505 11 6 -1 17 372.833 80.5417 11 6 -1 17 469.726 89.5457 16 6 1 17 369.394 73.9011 16 6 -1 19 4583.88 190.308 16 6 1 19 4288.94 185.268 11 6 -1 19 3972.15 174.456 11 -6 1 -19 4525.77 188.007 20 -6 -1 -19 4199.28 178.578 20 6 -1 21 542.162 61.3336 16 -6 1 -21 564.069 60.0547 20 -6 -1 -21 503.578 55.5797 20 6 1 21 573.833 62.8675 11 6 -1 21 406.525 53.0093 11 -6 1 -23 4114.29 107.543 20 -6 -1 -23 3934.63 104.849 20 6 1 23 4025.86 107.074 11 -6 1 -23 4009.77 103.377 10 -6 -1 -23 3932.28 99.5424 10 6 -2 -26 328.952 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157.287 11 7 -4 11 47561.7 758.144 16 7 4 11 48511.0 644.295 6 7 4 13 4941.33 236.932 11 7 -4 13 5324.88 245.186 16 7 4 15 21625.1 419.292 11 7 -4 15 23701.9 439.519 16 -7 4 -17 11531.8 228.452 14 7 -4 17 11559.9 261.118 16 7 4 17 10959.5 245.827 11 7 -4 19 3106.13 107.608 16 7 4 19 2984.23 102.356 11 -7 4 -19 2814.55 85.5613 10 -7 5 22 10496.5 183.663 21 7 -5 -22 10573.9 183.506 7 7 -5 -20 2356.46 96.4859 15 7 5 -20 2232.40 97.6017 15 -7 5 20 2124.42 111.848 21 7 -5 -20 2262.28 97.5032 12 7 -5 -20 2167.69 111.865 7 7 -5 -18 13877.7 328.240 8 7 -5 -18 14122.1 325.967 7 -7 5 18 14670.8 323.839 21 7 5 -18 13614.8 290.083 15 7 -5 -18 13364.8 274.012 12 7 5 -18 13920.8 273.812 10 7 -5 -16 4954.99 226.812 7 7 -5 -16 4988.83 228.447 8 -7 5 16 4565.48 216.185 21 7 5 -16 4454.09 195.571 15 7 -5 -16 4756.68 185.611 12 7 5 -16 5081.09 201.986 10 7 -5 -14 4811.72 239.731 7 7 -5 -14 5032.58 251.705 8 -7 5 14 5266.73 253.911 21 7 5 -14 4810.47 226.356 15 7 -5 -14 5056.84 211.355 12 7 5 -14 4777.86 227.579 10 7 -5 -12 12938.0 395.387 7 7 -5 -12 13219.7 417.108 8 -7 5 12 13752.4 415.649 21 7 5 -12 12347.4 387.360 15 7 -5 -12 13508.9 360.517 12 7 5 -12 13147.6 391.110 10 7 5 -10 7493.39 332.918 15 7 -5 -10 7142.68 310.292 8 7 -5 -10 7289.87 299.282 7 -7 5 10 7072.21 308.972 21 7 5 -10 7679.25 307.762 10 -7 5 8 31702.7 645.838 21 7 -5 -8 29984.9 620.593 8 7 -5 -8 30430.6 616.286 7 7 5 -8 31035.3 622.520 10 7 5 -8 31087.3 615.223 6 7 5 -6 2203.65 197.609 15 7 -5 -6 2117.30 172.887 7 7 -5 -6 2130.90 172.254 8 7 -5 -6 2187.37 165.423 16 7 5 -6 2150.12 169.998 6 7 -5 -4 38698.8 651.795 16 7 5 -4 37570.0 728.503 15 7 -5 -4 37920.8 661.374 7 7 -5 -4 36147.4 670.578 8 7 5 -4 35972.8 656.991 11 7 5 -4 36280.4 657.607 6 7 -5 -2 546.581 98.0411 8 7 5 -2 484.159 97.0423 15 7 -5 -2 594.412 102.761 16 7 5 -2 506.165 105.345 11 7 5 -2 472.746 101.439 6 7 -5 0 34130.8 620.946 16 7 5 0 32725.0 626.067 11 7 5 0 33086.2 637.803 6 7 -5 2 6368.79 275.468 16 7 5 2 6350.03 286.230 11 7 5 2 6950.48 296.600 6 7 5 2 6830.85 274.048 8 7 -5 4 15806.2 429.932 16 7 5 4 14883.3 430.668 11 7 5 4 16295.7 451.193 6 7 5 4 16588.9 429.378 8 7 -5 6 14118.7 408.948 16 7 5 6 12910.1 401.890 11 7 5 6 13761.7 409.790 6 7 5 6 14277.2 407.717 8 7 -5 8 11947.6 378.008 16 7 5 8 11280.7 376.195 11 7 5 8 12622.7 381.876 6 7 5 8 13131.2 391.602 8 7 -5 10 14203.1 409.659 16 7 5 10 14432.3 375.315 6 7 5 10 13574.0 400.018 11 7 -5 12 1543.00 145.195 16 7 5 12 1603.46 145.479 11 7 5 12 1600.79 117.979 6 -7 5 -14 19384.3 367.796 14 7 5 14 18975.7 392.072 11 -7 5 -14 18681.2 310.097 13 7 -5 14 19850.8 405.569 16 7 5 16 81.0668 38.6552 8 7 -5 16 177.620 49.0100 16 -7 5 -16 195.725 41.5594 14 7 5 16 170.376 46.6403 11 -7 5 -18 7568.28 143.541 14 7 5 18 7825.02 163.782 11 -7 6 21 19.0320 29.5440 21 7 6 -19 1334.55 78.1521 15 -7 6 19 1301.16 90.2462 21 7 -6 -19 1410.92 76.5838 12 7 -6 -19 1302.77 82.3039 7 7 -6 -17 197.437 49.3816 8 -7 6 17 268.150 56.8729 9 7 -6 -17 246.409 55.0800 7 -7 6 17 284.507 68.3252 21 7 6 -17 266.504 52.3972 15 7 -6 -17 278.815 46.7753 12 7 6 -17 337.191 53.4746 10 7 -6 -15 2464.92 154.694 7 7 -6 -15 2671.00 155.056 8 -7 6 15 2497.13 159.819 21 7 6 -15 2704.27 151.647 15 7 -6 -15 2514.21 135.894 12 -7 6 15 2704.68 150.294 9 7 6 -15 2731.96 156.273 10 7 -6 -13 128.741 59.8530 7 7 -6 -13 112.498 57.2592 8 -7 6 13 155.674 91.1038 21 7 6 -13 180.296 64.2212 15 7 -6 -13 210.163 54.3388 12 7 6 -13 185.650 57.7660 10 7 -6 -11 2021.72 157.589 7 7 -6 -11 1998.33 161.408 8 -7 6 11 2158.65 180.111 21 7 6 -11 2004.93 165.476 15 7 -6 -11 2140.51 152.819 12 7 6 -11 1934.68 159.298 10 -7 6 9 509.853 112.175 21 7 6 -9 425.621 102.299 15 7 -6 -9 408.360 88.7047 8 7 -6 -9 484.589 98.1054 7 7 6 -9 525.152 100.303 6 7 6 -9 438.909 93.0748 10 7 -6 -7 1100.60 122.938 7 7 6 -7 868.833 129.483 15 -7 6 7 749.709 128.571 21 7 6 -7 811.368 111.323 6 7 -6 -5 4188.99 217.319 16 7 -6 -5 4078.23 220.224 7 7 6 -5 4335.04 251.915 15 -7 6 5 4011.86 243.194 21 7 6 -5 4114.47 226.226 6 -7 6 3 5953.28 287.995 21 7 -6 -3 6026.57 255.312 16 7 -6 -3 5923.35 259.890 7 7 6 -3 5992.71 276.916 11 7 6 -3 6221.47 272.382 6 7 6 -3 6416.67 287.220 15 7 -6 -1 5647.28 247.551 16 7 6 -1 5141.60 258.770 11 7 6 -1 5248.11 256.875 6 7 6 -1 5414.09 246.557 15 7 -6 1 7849.84 293.203 16 7 6 1 8030.97 312.814 6 7 6 1 7853.50 314.103 11 7 -6 3 1305.84 127.644 16 7 6 3 1139.37 132.528 6 7 6 3 1334.58 139.776 11 7 -6 5 1579.87 141.585 16 7 6 5 1522.08 149.892 11 7 6 5 1545.39 149.346 6 7 -6 7 3082.00 192.461 16 7 6 7 3008.77 198.114 11 7 6 7 3295.16 200.033 6 7 6 7 3582.16 193.329 8 7 -6 9 607.004 95.9946 16 7 6 9 641.189 87.7276 8 7 6 9 602.484 103.442 11 7 6 9 737.334 105.668 6 7 -6 11 2553.95 169.072 16 7 6 11 2492.57 149.829 8 7 6 11 2518.59 168.995 11 -7 6 -11 2725.74 145.113 13 7 6 11 2609.33 148.930 6 -7 6 -11 2496.94 153.709 14 7 6 13 329.249 54.3375 8 -7 6 -13 435.561 64.0996 14 7 -6 13 301.133 70.6986 16 7 6 13 396.713 69.9587 11 -7 6 -13 425.541 56.1180 13 7 6 13 266.146 58.0015 6 -7 6 -15 3515.43 131.656 14 7 6 15 3321.26 135.997 11 7 -6 15 3306.01 140.598 16 -7 6 -17 22.6824 17.7601 14 7 6 17 12.9918 19.5626 11 7 -6 17 27.8857 29.5120 16 7 -7 -18 13264.4 211.841 12 -7 7 18 13948.1 242.592 21 7 7 -18 13730.0 228.782 15 -7 7 16 7579.27 213.870 21 7 7 -16 7315.61 205.258 15 7 -7 -16 7223.90 186.343 12 -7 7 16 6864.30 183.935 9 7 7 -16 7112.10 205.505 10 7 -7 -14 11171.7 274.384 7 -7 7 14 11648.6 299.211 21 7 7 -14 11296.6 292.860 15 7 -7 -14 10524.9 259.721 12 -7 7 14 11015.3 278.874 9 7 7 -14 11543.1 309.697 10 7 -7 -12 27173.6 487.321 7 -7 7 12 25910.5 490.344 21 7 7 -12 27624.4 510.604 15 7 -7 -12 27267.6 455.922 12 -7 7 12 27991.3 498.145 9 7 7 -12 27460.9 526.101 10 7 -7 -10 6426.15 245.990 7 -7 7 10 6180.26 267.922 21 7 7 -10 7046.55 291.461 15 7 -7 -10 6684.49 248.869 12 7 7 -10 6435.53 270.265 10 -7 7 8 38392.3 663.522 21 7 -7 -8 38048.2 609.172 7 7 -7 -8 38038.0 616.232 12 7 7 -8 36768.4 604.995 6 7 7 -6 457.507 95.2154 15 7 -7 -6 368.251 84.9649 7 -7 7 6 718.879 121.434 21 7 7 -6 511.964 89.6201 6 -7 7 4 46356.6 744.715 21 7 -7 -4 44397.0 672.324 7 -7 7 4 44271.5 725.829 13 7 7 -4 43374.1 684.440 6 7 7 -4 46023.9 739.156 15 7 -7 -2 2131.74 154.150 7 7 7 -2 2488.27 168.237 15 7 7 -2 2318.87 176.783 11 -7 7 2 2434.80 193.045 13 7 7 -2 2407.77 171.095 6 7 -7 0 27467.1 505.809 16 7 7 0 28382.3 588.120 11 -7 7 0 29022.4 648.603 13 7 7 0 28126.4 554.815 6 7 -7 0 28175.2 524.075 7 7 7 2 11818.8 366.653 6 7 -7 2 11516.7 332.028 16 7 7 2 12089.4 384.437 11 7 7 4 17591.4 440.784 6 7 -7 4 16518.1 399.676 16 -7 7 -4 18050.2 478.203 13 7 7 4 16635.1 445.509 11 7 7 6 28157.4 543.663 6 7 7 6 26940.0 554.418 11 -7 7 -6 28771.5 553.348 13 7 -7 6 27066.8 502.502 16 -7 7 -8 15123.1 378.445 14 7 7 8 15410.2 388.854 6 7 7 8 14109.4 390.403 11 -7 7 -8 14388.5 355.726 13 7 -7 8 14631.3 362.780 16 -7 7 -10 24085.8 430.015 14 7 7 10 23488.9 423.850 6 7 7 10 23126.5 472.876 11 -7 7 -10 22951.3 396.634 13 7 -7 10 22775.9 432.675 16 -7 7 -12 2030.53 116.333 14 7 7 12 2152.40 112.958 6 7 7 12 2197.47 132.718 11 -7 7 -12 2101.11 106.482 13 7 -7 12 2017.25 124.144 16 -7 7 -14 22260.5 310.133 14 7 7 14 22844.2 329.783 11 7 -7 14 22760.1 325.580 16 7 -8 -17 2.80816 14.7311 12 -7 8 17 74.8488 29.6483 21 7 8 -15 6984.01 186.894 15 -7 8 15 7112.10 182.506 21 7 -8 -15 6878.08 164.816 12 -7 8 15 6990.53 173.520 9 7 8 -13 1131.06 93.6832 15 -7 8 13 947.045 90.0047 21 7 -8 -13 1004.21 78.5561 12 -7 8 13 908.990 88.5540 9 7 8 -11 6326.01 236.134 15 -7 8 11 5827.65 210.036 21 7 -8 -11 5485.22 193.776 12 -7 8 11 5808.60 219.699 9 7 8 -9 3262.98 194.830 15 -7 8 9 2990.51 164.102 21 7 -8 -9 3023.50 160.200 12 -7 8 9 2945.09 180.157 9 7 8 -7 8549.76 276.295 6 7 8 -7 9072.50 322.017 15 -7 8 7 8602.22 282.870 21 7 -8 -7 8824.27 275.973 12 -7 8 7 9015.58 315.667 9 -7 8 5 6317.50 282.117 9 -7 8 5 5884.63 236.678 13 7 8 -5 6026.61 237.850 6 7 8 -5 6779.21 270.234 15 -7 8 3 9395.64 334.137 9 -7 8 3 8842.36 310.561 13 7 8 -3 9174.19 296.790 6 7 8 -3 9317.85 301.907 15 -7 8 1 17056.5 415.302 9 -7 8 1 17805.5 458.975 13 7 8 -1 17911.9 416.634 6 7 8 1 544.610 95.4171 11 -7 8 -1 555.759 81.1197 9 -7 8 -1 480.669 102.355 13 7 8 1 593.536 95.8377 6 7 8 3 22261.6 485.806 11 -7 8 -3 21924.0 506.325 13 7 8 3 22183.5 459.702 6 -7 8 -3 20890.3 474.874 14 7 8 5 124.212 57.6312 11 -7 8 -5 24.3468 63.5716 13 -7 8 -5 93.0386 60.9505 14 7 8 5 154.497 63.3564 6 7 8 7 11005.8 324.072 11 -7 8 -7 10986.1 295.623 13 7 8 7 10742.0 303.061 6 -7 8 -7 10552.3 297.207 14 7 8 9 46.1458 47.2730 11 7 -8 9 157.492 37.4591 16 -7 8 -9 21.8623 40.2067 13 -7 8 -9 118.281 46.1208 14 7 8 9 69.8864 45.3024 6 -7 8 -11 11191.9 239.927 14 7 8 11 10696.0 231.394 6 -7 8 -11 11072.5 223.048 13 7 8 11 11465.3 265.263 11 7 -8 11 10980.6 231.367 16 7 8 13 3217.89 112.102 11 -7 8 -13 3160.96 109.294 14 7 8 13 2859.33 95.8231 6 -7 8 -13 2962.04 100.501 5 7 -9 -14 1662.87 69.3870 12 -7 9 14 1605.62 77.0614 9 7 9 -14 1696.10 85.3737 15 -7 9 12 688.030 58.3456 21 7 9 -12 654.029 67.1808 15 7 -9 -12 645.666 55.9071 12 -7 9 12 687.371 70.3160 9 7 9 -10 209.760 57.2385 15 7 -9 -10 103.319 29.0237 12 -7 9 10 137.510 53.1218 9 7 -9 -8 2127.58 116.944 12 -7 9 8 2126.67 136.819 9 7 9 -6 96.1418 52.3653 15 7 -9 -6 60.0535 31.3964 12 -7 9 6 39.6751 54.5125 9 -7 9 4 4101.03 198.630 9 7 9 -4 4545.01 195.362 15 -7 9 4 4060.63 177.560 13 7 9 -4 4292.98 185.365 6 7 9 -2 79.2612 40.5736 15 -7 9 2 153.682 58.5206 13 -7 9 2 111.063 52.2233 9 7 9 -2 50.5092 41.8216 6 -7 9 0 5267.66 228.165 13 7 9 0 5328.99 207.275 6 -7 9 -2 122.606 58.2191 13 7 9 2 100.572 49.5888 6 -7 9 -4 3802.66 182.005 13 7 9 4 3626.12 167.623 6 7 9 6 816.049 88.9019 11 -7 9 -6 711.470 74.2433 13 7 9 6 756.312 81.0970 6 -7 9 -6 703.466 79.2994 14 7 9 8 856.514 79.0216 11 -7 9 -8 754.863 68.6161 13 7 9 8 727.300 74.5607 6 -7 9 -8 695.253 71.2573 14 -7 9 -10 2925.75 102.789 13 7 9 10 2694.47 107.263 6 -7 9 -10 2807.97 104.824 14 -7 10 11 23471.6 279.952 9 -7 10 9 4076.31 140.264 9 -7 10 7 24265.7 364.380 9 -7 10 5 8643.53 233.996 9 7 10 -3 10228.8 236.109 6 -7 10 3 10246.0 243.783 9 -7 10 1 17251.0 326.910 13 -7 10 1 17351.3 287.998 9 7 10 1 2577.47 121.434 6 -7 10 -1 2347.97 130.988 13 7 10 3 23963.9 354.176 6 -7 10 -3 24214.7 386.445 13 7 10 5 756.881 65.3202 6 -7 10 -5 693.904 69.3712 13 7 10 7 21372.0 282.318 6 -7 10 -7 21094.9 274.230 13 8 0 -22 6531.94 154.303 7 8 0 -20 19996.2 346.179 8 8 0 -20 20043.4 338.516 7 8 0 -20 20670.3 311.162 15 8 0 -18 4411.50 189.850 7 8 0 -18 4372.96 197.309 8 8 0 -18 4646.26 182.775 15 8 0 -16 27686.3 535.531 7 8 0 -16 27652.6 545.261 8 -8 0 16 28775.4 482.276 21 8 0 -14 6171.16 266.661 15 8 0 -14 5992.32 262.741 7 8 0 -14 6146.86 271.252 8 -8 0 14 6158.06 253.430 21 8 0 -12 32538.8 648.871 15 8 0 -12 33480.3 621.088 7 8 0 -12 32642.6 624.568 8 -8 0 12 34857.4 608.634 21 8 0 -10 11611.4 373.748 8 8 0 -10 11319.3 365.982 7 8 0 -8 35091.7 648.789 8 8 0 -8 34127.3 629.943 7 8 0 -6 36139.0 637.361 7 8 0 -6 33922.6 630.894 8 8 0 -4 23104.6 511.226 7 8 0 -4 22252.9 508.323 8 8 0 -4 22640.4 524.886 16 8 0 -2 69756.9 1012.73 15 8 0 -2 67544.4 886.801 8 8 0 -2 68313.3 902.152 16 8 0 0 989.881 121.587 8 8 0 0 924.527 119.963 16 8 0 2 47102.9 744.522 8 8 0 2 45553.3 736.455 16 8 0 4 163.819 68.6644 16 8 0 4 100.839 69.1403 8 8 0 6 36691.8 677.441 8 8 0 6 37349.0 661.989 16 8 0 8 1589.55 149.989 8 8 0 8 1556.90 146.778 16 8 0 10 33493.0 634.760 8 8 0 10 33859.7 597.607 16 8 0 12 15126.0 398.393 8 8 0 12 15065.9 363.377 16 8 0 14 16534.8 366.149 8 8 0 14 17739.2 334.719 16 8 0 16 13353.4 271.572 8 8 0 16 14004.8 235.851 16 8 0 18 3923.12 114.046 8 8 -1 -23 641.436 45.1796 7 8 -1 -21 2981.31 125.111 8 8 1 -21 3084.88 112.720 7 8 -1 -21 3262.39 126.783 7 8 1 -21 3160.44 107.073 15 8 -1 -21 3243.59 107.591 15 8 1 -19 1021.20 84.0920 15 8 -1 -19 1087.02 84.9858 15 8 1 -19 1042.89 88.6517 8 8 -1 -19 1113.12 97.3444 8 8 1 -19 967.097 83.9088 7 8 -1 -19 1030.17 91.7674 7 -8 1 19 952.591 80.2162 21 8 1 -17 4072.74 187.647 15 8 -1 -17 4474.66 192.745 15 8 1 -17 4358.23 195.776 7 8 -1 -17 4122.26 202.729 7 8 1 -17 4255.64 203.423 8 8 -1 -17 4017.88 205.695 8 -8 1 17 4361.13 187.514 21 8 1 -15 1051.45 115.065 15 8 -1 -15 1163.33 122.027 15 8 1 -15 935.016 111.564 7 8 -1 -15 925.852 111.803 7 8 1 -15 1087.07 117.956 8 8 -1 -15 980.134 117.789 8 -8 1 15 1101.48 125.718 21 8 1 -13 8234.90 323.756 15 8 1 -13 8713.37 318.738 7 8 -1 -13 8772.60 320.808 7 8 1 -13 8637.28 313.986 8 8 -1 -13 8205.53 317.887 8 -8 -1 13 8807.16 292.035 21 -8 1 13 8223.66 305.796 21 8 1 -11 528.284 106.705 15 8 -1 -11 449.765 86.9680 7 8 -1 -11 457.896 95.0341 8 8 1 -11 352.750 74.1272 8 8 1 -11 452.291 89.2005 7 -8 1 11 382.251 109.453 21 8 -1 -9 9451.59 345.033 8 8 1 -9 9773.86 336.626 8 8 1 -9 10000.9 342.393 7 8 -1 -9 9572.14 340.007 7 8 1 -9 9537.24 392.809 15 8 1 -7 478.153 84.7427 7 8 -1 -7 258.175 77.9952 8 8 1 -7 333.736 77.4120 8 8 -1 -7 234.662 71.7253 7 8 1 -7 325.973 109.091 15 8 -1 -5 6912.37 287.560 16 8 1 -5 6846.97 276.435 7 8 -1 -5 7158.42 288.992 7 8 -1 -5 7024.88 293.804 8 8 1 -5 6663.70 276.429 8 8 1 -5 6694.04 350.697 15 8 1 -3 3263.27 234.085 15 8 1 -3 3590.86 201.512 7 8 -1 -3 3617.63 213.550 8 8 1 -3 3418.39 201.908 8 8 1 -3 3471.12 213.935 16 8 -1 -3 3577.23 214.932 16 8 1 -3 3451.27 220.021 6 8 -1 -1 13692.9 402.677 8 8 1 -1 13055.8 388.872 8 8 1 -1 12802.9 393.603 16 8 -1 -1 13022.4 394.334 16 8 1 -1 13871.5 427.392 6 8 1 1 2642.92 183.698 16 8 -1 1 2316.15 176.268 16 8 -1 1 2440.29 176.058 8 8 1 1 2673.15 181.053 8 8 -1 3 8217.11 317.712 16 8 1 3 8575.68 321.667 16 8 -1 3 8249.21 319.592 8 8 1 3 8760.22 324.621 8 8 1 5 11704.3 370.598 16 8 -1 5 12034.4 380.796 16 8 -1 5 12143.8 387.997 8 8 1 5 11871.2 384.618 8 8 1 7 3923.25 200.722 11 8 1 7 3809.58 210.847 16 8 -1 7 4103.19 225.856 16 8 -1 7 4125.12 229.221 8 8 1 7 4162.22 232.499 8 8 1 9 14829.1 372.811 11 8 1 9 14834.7 398.760 16 8 -1 9 15089.3 413.889 16 8 1 9 15522.6 436.053 8 8 -1 9 16018.7 437.639 8 8 1 11 875.232 100.212 16 8 -1 11 1065.68 118.566 16 8 1 11 772.639 98.8933 11 8 1 11 1109.87 127.277 8 8 -1 11 1012.46 121.025 8 8 1 13 4182.33 178.071 11 8 1 13 4405.87 207.984 8 8 -1 13 4535.82 203.333 8 8 -1 15 386.881 61.6876 16 8 1 15 325.280 52.2045 11 8 -1 15 298.698 55.0025 8 8 1 15 283.282 59.7290 8 8 1 17 4835.73 149.769 8 8 1 17 5162.09 125.742 11 8 -2 -22 1015.41 63.8564 7 8 2 -20 4283.00 138.139 15 8 -2 -20 4573.34 142.181 15 8 -2 -20 4242.69 159.434 8 8 -2 -20 4113.70 154.158 7 8 2 -18 46.5213 38.9696 15 8 -2 -18 22.4710 33.5349 15 8 2 -18-5.65297 34.9225 8 8 -2 -18 42.8459 43.9564 8 8 2 -18 93.6064 32.7726 7 8 -2 -18-34.6587 42.9664 7 -8 2 18 33.3103 47.6080 21 8 2 -16 9203.20 286.019 15 8 -2 -16 8946.92 287.092 15 8 2 -16 9276.97 276.505 7 8 -2 -16 8908.29 312.795 8 8 -2 -16 9136.76 307.805 7 8 2 -16 9249.13 298.375 8 -8 2 16 9413.95 296.138 21 8 2 -14 166.449 70.5410 15 8 -2 -14 122.938 69.0857 8 8 2 -14 207.320 63.8446 8 8 -2 -14 138.055 67.2005 7 8 2 -14 198.121 62.3805 7 -8 2 14 219.237 85.3188 21 8 2 -12 13477.5 410.214 15 8 2 -12 13744.1 390.877 7 8 -2 -12 13489.8 395.820 7 8 -2 -12 13277.1 405.727 8 8 2 -12 13976.2 392.938 8 -8 2 12 13172.7 393.254 21 8 2 -10 1067.56 119.300 7 8 -2 -10 980.426 122.291 8 8 2 -10 1032.25 114.049 8 8 -2 -10 830.171 111.010 7 8 2 -10 920.678 128.382 15 8 -2 -8 9514.66 345.924 8 8 2 -8 9281.08 327.037 8 8 2 -8 10108.5 340.203 7 8 -2 -8 9764.31 339.042 7 8 2 -8 9762.16 408.386 15 8 -2 -6 4558.87 240.466 16 8 -2 -6 4785.15 238.466 7 8 -2 -6 4605.14 245.830 8 8 2 -6 4453.30 228.077 8 8 2 -6 4547.56 229.331 7 8 2 -6 4635.92 292.118 15 8 2 -4 8708.49 372.591 15 8 2 -4 8550.15 307.188 7 8 -2 -4 8942.72 322.050 7 8 -2 -4 8097.49 317.004 8 8 2 -4 8301.85 305.734 8 8 -2 -4 8548.37 321.553 16 8 2 -4 8065.63 330.678 6 8 2 -2 5369.85 272.687 15 8 2 -2 5672.64 267.423 16 8 -2 -2 5009.72 245.849 16 8 2 -2 5524.80 274.080 6 8 2 -2 5733.91 252.369 7 8 -2 -2 5869.45 269.418 8 8 2 -2 5738.94 257.490 8 8 2 0 868.648 112.254 16 8 -2 0 844.757 115.071 16 8 2 0 838.206 106.047 11 8 2 0 827.572 113.290 6 8 -2 0 686.271 104.856 8 8 2 0 784.364 106.046 8 8 -2 2 20529.3 492.082 16 8 2 2 19786.5 488.768 16 8 -2 2 20362.2 493.284 8 8 2 2 22162.2 505.528 8 8 2 2 20109.3 449.684 11 8 2 2 22251.8 516.635 6 8 2 4 680.374 104.004 16 8 -2 4 768.230 108.257 16 8 2 4 585.125 90.9410 11 8 -2 4 714.696 103.110 8 8 2 4 725.861 105.777 8 8 -2 6 18053.4 464.900 8 8 2 6 19019.5 481.140 8 8 -2 6 18590.3 466.275 16 8 -2 8 264.173 88.1277 16 8 2 8 269.836 72.7412 11 8 -2 8 303.055 78.6005 8 8 2 8 408.965 92.1137 8 8 2 10 6789.31 285.702 8 8 -2 10 6559.92 266.883 8 8 -2 10 6812.58 277.270 16 8 2 12 4868.36 227.177 8 8 -2 12 4587.19 205.339 8 8 -2 12 4738.21 212.577 16 8 2 12 4505.80 201.917 11 8 2 14 4633.64 194.560 8 8 -2 14 4164.04 166.899 8 8 2 14 4226.70 168.149 11 -8 2 -16 2845.53 105.483 14 8 2 16 2740.90 109.634 11 8 -2 16 3062.36 121.828 16 8 2 16 2532.40 121.474 8 -8 2 -18 603.150 40.9657 10 8 2 18 570.756 47.5282 8 8 3 -21 1976.74 76.1823 15 8 -3 -21 1958.90 92.0412 7 -8 3 21 1909.13 79.6115 21 8 3 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229.465 16 8 -3 -3 4337.97 236.545 8 8 3 -3 4119.75 213.675 8 8 3 -3 4100.99 242.283 15 8 3 -3 3894.12 210.062 11 8 3 -3 4634.77 250.239 6 8 -3 -1 37857.4 659.062 16 8 3 -1 38421.5 633.028 11 8 3 -1 39365.7 694.935 6 8 -3 -1 38559.4 672.253 8 8 3 -1 38290.3 642.261 8 8 -3 1 12516.6 384.197 16 8 3 1 12181.5 359.912 11 8 3 1 12920.6 395.529 6 8 -3 1 12925.5 388.843 8 8 3 1 12813.6 377.339 8 8 -3 3 14847.3 416.234 16 8 3 3 15654.4 407.140 11 8 3 3 16527.2 437.847 6 8 -3 3 16128.0 435.545 8 8 3 3 16300.4 428.939 8 8 -3 5 18557.0 464.573 16 8 3 5 18029.9 435.337 11 8 3 5 19513.4 460.616 6 8 -3 5 18019.2 459.153 8 8 3 5 19089.8 470.653 8 8 -3 7 8192.39 304.463 8 8 3 7 8207.09 310.418 8 8 -3 7 7701.67 299.114 16 8 3 7 7355.68 278.949 11 8 3 9 35091.2 628.359 8 8 -3 9 33918.4 598.061 8 8 -3 9 31767.3 586.189 16 8 3 9 31729.1 557.089 11 8 3 11 2053.36 154.276 8 8 -3 11 2115.92 146.007 8 8 -3 11 2149.74 153.278 16 8 3 11 1977.28 141.675 11 8 3 13 24651.5 450.539 8 8 -3 13 23728.6 385.881 8 8 3 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257.503 8 10 3 -1 9483.97 249.164 8 10 -3 1 6874.50 220.840 16 10 -3 1 6821.04 218.477 7 10 -3 1 7214.88 221.269 8 10 3 1 7146.81 213.627 8 10 -3 3 22880.7 384.327 16 10 -3 3 21656.7 368.017 7 10 -3 3 22720.4 367.021 8 10 3 3 22544.6 365.323 8 10 -3 5 3457.97 145.227 16 10 -3 5 3199.24 136.970 7 10 -3 5 3479.68 137.492 8 10 3 5 3494.95 139.718 8 10 -3 7 16708.1 285.084 16 10 -3 7 14918.6 267.295 7 10 -3 7 14996.2 226.228 8 10 3 7 16200.5 272.333 8 10 3 9 219.781 32.4575 8 10 -3 9 215.200 34.2860 7 10 -3 9 239.985 36.3787 16 10 -4 -12 742.107 58.9517 15 10 4 -12 803.314 59.0035 15 -10 4 12 671.725 65.7749 21 10 -4 -12 808.583 67.8856 7 10 -4 -12 731.658 63.5610 8 10 -4 -10 921.588 73.9399 15 10 4 -10 942.551 71.9890 15 -10 4 10 934.679 80.9045 21 10 -4 -10 977.660 79.4708 7 10 -4 -10 1019.83 82.0135 8 10 -4 -8 1283.37 90.0812 15 10 4 -8 1335.78 85.5241 15 -10 4 8 1243.58 100.566 21 10 -4 -8 1328.49 95.4203 7 10 -4 -8 1354.84 98.3606 8 10 4 -6 123.847 30.3042 15 10 -4 -6 39.5197 34.0264 15 -10 4 6 44.0586 55.6628 21 10 -4 -6-43.4220 39.5004 7 10 -4 -6 90.2973 43.3149 8 -10 4 4 2777.32 149.830 21 10 -4 -4 2730.25 135.480 8 10 4 -4 2871.17 120.412 8 10 -4 -4 2497.36 131.213 7 -10 4 2 192.570 64.3004 21 10 -4 -2 355.635 59.6096 7 10 -4 -2 397.599 62.4295 8 10 4 -2 404.583 51.9297 8 10 -4 0 3032.44 137.786 7 10 -4 0 3441.30 145.155 8 10 4 0 3239.56 129.837 8 10 -4 2 275.194 52.5705 16 10 -4 2 344.169 53.9388 8 10 4 2 253.084 43.8947 8 10 -4 2 212.036 48.7011 7 10 -4 4 886.540 74.6050 7 10 4 4 938.258 67.5877 8 10 -4 4 944.304 77.8312 16 10 -4 6 1675.77 90.4548 7 10 4 6 1711.97 81.0693 8 10 -4 6 1750.04 94.4948 16 -10 4 -8 875.729 60.0155 14 10 -4 8 803.372 57.0532 7 -10 4 -8 973.867 56.8675 13 10 -4 8 1047.97 62.8797 16 10 -5 -11 7914.14 163.728 15 10 5 -11 8213.95 157.724 15 10 -5 -11 8275.38 178.716 7 -10 5 11 8607.60 179.537 21 -10 5 11 8826.53 176.997 9 10 5 -9 45.4155 25.0903 15 10 -5 -9 69.4031 28.4337 15 10 -5 -9 65.7113 33.4387 7 -10 5 9 87.6647 44.0649 21 10 -5 -7 13731.7 261.763 7 10 -5 -7 13033.0 243.932 8 -10 5 7 13610.7 270.083 21 10 -5 -5 659.865 56.3262 15 -10 5 5 694.062 77.8529 21 10 -5 -5 646.114 67.8562 7 10 -5 -3 3921.93 149.433 7 -10 5 3 4159.03 158.873 21 -10 5 3 4304.58 144.614 13 10 -5 -1 3248.13 132.982 7 -10 5 1 3295.21 136.206 21 -10 5 1 3367.37 139.086 13 10 -5 1 2317.12 109.283 7 -10 5 -1 2324.88 105.823 21 -10 5 -1 2335.00 120.452 13 -10 5 -3 8379.92 200.171 13 10 -5 3 7986.29 187.145 7 -10 5 -5 3736.32 120.493 13 10 -5 5 3529.65 116.646 7 -10 6 8 8140.21 167.180 9 -10 6 6 1922.73 90.7300 9 10 -6 -6 1918.75 87.0515 7 -10 6 4 11992.9 213.534 9 10 -6 -4 11993.6 212.658 7 10 -6 -2 747.070 58.6848 7 10 -6 0 20233.4 266.230 7 -10 6 0 19816.1 273.840 13 -10 6 -2 491.452 50.0140 13 11 0 -9 30.0461 23.8464 8 11 0 -7 21.7805 25.0519 8 11 0 -5 16.8344 22.9434 8 11 0 -5 27.4740 21.5385 7 -11 0 5 34.9608 36.8883 21 11 0 -3 23.7584 24.4353 8 11 0 -3-29.0931 22.5755 7 11 0 -1 7.29048 27.8863 8 11 0 -1 35.8307 20.4934 7 11 0 1 17.4288 27.9626 8 11 0 3 3.14987 21.9009 8 11 -1 -8 9493.60 184.787 7 11 -1 -8 9534.57 199.651 8 11 1 -8 9285.30 189.274 8 -11 1 8 9121.39 181.463 21 11 -1 -6 2591.83 103.341 7 11 -1 -6 2559.94 110.557 8 11 1 -6 2553.94 106.031 8 -11 -1 6 2479.44 100.244 21 -11 1 6 2304.66 103.718 21 11 -1 -4 9632.76 198.859 7 11 -1 -4 9750.97 212.049 8 11 1 -4 9866.59 208.367 8 -11 -1 4 9595.26 207.865 21 11 -1 -2 2485.61 109.705 8 11 1 -2 2701.75 110.419 8 11 -1 -2 2670.04 106.206 7 11 -1 0 4360.12 138.748 8 11 1 0 4395.89 136.947 8 11 -1 0 4228.63 128.414 7 11 -1 2 8124.99 175.863 8 11 1 2 8094.43 175.052 8 11 -1 2 7839.00 161.434 7 11 -2 -7 746.373 57.7702 7 11 -2 -7 795.800 62.7990 8 -11 2 7 758.241 60.5423 21 11 -2 -5 9203.23 192.198 7 11 -2 -5 9284.52 200.246 8 11 2 -5 9203.99 184.485 8 11 -2 -3 138.484 36.0663 8 11 2 -3 84.0520 30.2198 8 11 -2 -3 62.7989 30.5521 7 11 -2 -1 17483.5 263.195 8 11 2 -1 17687.0 255.827 8 11 -2 -1 17451.3 260.694 7 11 -2 1 1896.05 84.7813 8 11 2 1 1817.65 81.0465 8 11 -2 1 1822.37 83.9932 7 11 -3 -4 389.481 41.2156 7 -11 3 4 323.342 46.1639 21 11 -3 -2 1251.05 68.6201 7 -11 3 2 1192.63 72.6622 21 0 0 0 0.00 0.00 0 TITL joha0503 in I2/a REM I2/a (#15 in standard setting) CELL 1.54184 9.043794 11.159848 23.938486 90.0000 96.2133 90.0000 ZERR 7.00 0.000135 0.000171 0.000381 0.0000 0.0014 0.0000 LATT 2 SYMM -x+1/2, y,-z SFAC C H N O F Re UNIT 63.00 49.00 7.00 49.00 7.00 7.00 TREF HKLF 4 END ; _shelx_hkl_checksum 90682 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Re1 Re 0.59982(2) 0.82627(2) 0.36286(2) 0.02481(7) Uani 1 1 d . . . . . F1 F 0.4515(2) 0.58450(17) 0.29771(8) 0.0368(4) Uani 1 1 d . . . . . O1 O 0.5834(3) 1.0989(2) 0.37554(12) 0.0452(6) Uani 1 1 d . . . . . O2 O 0.3224(3) 0.8510(2) 0.27867(12) 0.0523(7) Uani 1 1 d . . . . . O3 O 0.7881(4) 0.8758(2) 0.26725(12) 0.0572(8) Uani 1 1 d . . . . . O4 O 0.4671(2) 0.7857(2) 0.43177(9) 0.0279(4) Uani 1 1 d . . . . . H4A H 0.506(5) 0.755(4) 0.460(2) 0.057(13) Uiso 1 1 d . . . . . H4B H 0.426(5) 0.848(4) 0.4402(19) 0.046(12) Uiso 1 1 d . . . . . O5 O 0.9177(2) 0.66203(19) 0.47892(10) 0.0328(5) Uani 1 1 d . . . . . O6 O 0.7808(2) 0.7953(2) 0.42702(9) 0.0293(4) Uani 1 1 d . . . . . N1 N 0.6316(3) 0.6284(2) 0.36703(9) 0.0252(5) Uani 1 1 d . . . . . C1 C 0.5893(3) 0.9960(3) 0.37100(13) 0.0336(7) Uani 1 1 d . . . . . C2 C 0.4268(4) 0.8405(3) 0.30977(14) 0.0359(7) Uani 1 1 d . . . . . C3 C 0.7173(4) 0.8551(3) 0.30306(14) 0.0373(7) Uani 1 1 d . . . . . C4 C 0.5561(3) 0.5454(3) 0.33688(12) 0.0283(6) Uani 1 1 d . . . . . C5 C 0.5772(3) 0.4235(3) 0.34406(14) 0.0338(6) Uani 1 1 d . . . . . H5 H 0.519245 0.367420 0.321251 0.041 Uiso 1 1 calc R U . . . C6 C 0.6848(4) 0.3861(3) 0.38534(14) 0.0348(6) Uani 1 1 d . . . . . H6 H 0.703317 0.303140 0.391513 0.042 Uiso 1 1 calc R U . . . C7 C 0.7665(3) 0.4717(3) 0.41802(13) 0.0322(6) Uani 1 1 d . . . . . H7 H 0.841122 0.447983 0.446905 0.039 Uiso 1 1 calc R U . . . C8 C 0.7370(3) 0.5911(3) 0.40762(12) 0.0270(6) Uani 1 1 d . . . . . C9 C 0.8206(3) 0.6885(3) 0.44118(13) 0.0278(6) Uani 1 1 d . . . . . O7 O 0.8670(2) 1.01037(19) 0.47007(9) 0.0326(4) Uani 1 1 d D . . . . H7C H 0.853(5) 0.938(3) 0.4552(17) 0.049 Uiso 1 1 d D U . . . H7B H 0.790(7) 1.022(7) 0.489(3) 0.049 Uiso 0.5 1 d D U P A -1 H7A H 0.947(7) 1.001(10) 0.495(3) 0.07(3) Uiso 0.5 1 d D . P B -2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Re1 0.02836(9) 0.02026(9) 0.02557(9) -0.00160(4) 0.00187(6) -0.00215(4) F1 0.0363(9) 0.0330(10) 0.0385(9) -0.0054(7) -0.0081(7) -0.0023(7) O1 0.0584(15) 0.0213(12) 0.0557(14) -0.0044(10) 0.0054(12) -0.0011(10) O2 0.0588(17) 0.0432(14) 0.0479(15) 0.0007(11) -0.0259(13) 0.0012(12) O3 0.083(2) 0.0427(15) 0.0527(16) -0.0075(12) 0.0391(15) -0.0146(14) O4 0.0301(10) 0.0243(10) 0.0290(10) 0.0000(8) 0.0023(8) 0.0017(8) O5 0.0272(10) 0.0341(12) 0.0356(11) -0.0060(8) -0.0039(9) 0.0028(8) O6 0.0274(10) 0.0248(10) 0.0345(10) -0.0043(8) -0.0025(8) -0.0003(8) N1 0.0252(10) 0.0226(12) 0.0280(11) -0.0026(9) 0.0043(8) -0.0002(10) C1 0.0382(16) 0.0330(18) 0.0298(14) -0.0002(12) 0.0043(12) -0.0015(12) C2 0.0475(19) 0.0265(16) 0.0330(16) -0.0005(11) 0.0010(14) -0.0029(13) C3 0.0493(19) 0.0235(14) 0.0403(17) -0.0044(13) 0.0110(14) -0.0050(13) C4 0.0263(13) 0.0304(15) 0.0281(13) -0.0051(11) 0.0029(10) -0.0016(11) C5 0.0306(14) 0.0285(16) 0.0429(16) -0.0094(13) 0.0065(12) -0.0055(12) C6 0.0369(16) 0.0238(15) 0.0445(17) -0.0003(12) 0.0073(13) 0.0022(12) C7 0.0294(14) 0.0272(15) 0.0397(16) -0.0016(12) 0.0031(12) 0.0025(12) C8 0.0262(13) 0.0260(14) 0.0294(13) -0.0047(11) 0.0052(11) -0.0011(11) C9 0.0262(13) 0.0280(14) 0.0301(14) -0.0049(11) 0.0071(11) -0.0015(11) O7 0.0327(10) 0.0276(10) 0.0374(11) -0.0048(9) 0.0034(8) -0.0076(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Re Re -5.2083 5.8923 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0 0 -1 0.0392 0 0 1 0.0292 1 -1 0 0.0575 -1 1 0 0.0575 5 4 -3 0.0773 -4 -5 3 0.0854 3 5 0 0.0839 -1 0 5 0.0490 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O4 Re1 N1 80.80(8) . . ? O6 Re1 O4 82.27(8) . . ? O6 Re1 N1 73.98(8) . . ? C1 Re1 O4 95.20(11) . . ? C1 Re1 O6 97.41(11) . . ? C1 Re1 N1 170.86(11) . . ? C1 Re1 C2 86.51(13) . . ? C2 Re1 O4 92.40(12) . . ? C2 Re1 O6 173.63(11) . . ? C2 Re1 N1 101.80(11) . . ? C3 Re1 O4 177.76(11) . . ? C3 Re1 O6 96.95(13) . . ? C3 Re1 N1 96.97(11) . . ? C3 Re1 C1 86.98(13) . . ? C3 Re1 C2 88.24(15) . . ? Re1 O4 H4A 120(3) . . ? Re1 O4 H4B 108(3) . . ? H4A O4 H4B 108(4) . . ? C9 O6 Re1 120.66(19) . . ? C4 N1 Re1 128.0(2) . . ? C4 N1 C8 117.4(3) . . ? C8 N1 Re1 114.56(19) . . ? O1 C1 Re1 179.5(3) . . ? O2 C2 Re1 178.6(3) . . ? O3 C3 Re1 178.1(3) . . ? F1 C4 C5 119.2(3) . . ? N1 C4 F1 116.2(3) . . ? N1 C4 C5 124.6(3) . . ? C4 C5 H5 121.1 . . ? C6 C5 C4 117.7(3) . . ? C6 C5 H5 121.1 . . ? C5 C6 H6 120.4 . . ? C5 C6 C7 119.1(3) . . ? C7 C6 H6 120.4 . . ? C6 C7 H7 120.6 . . ? C8 C7 C6 118.7(3) . . ? C8 C7 H7 120.6 . . ? N1 C8 C7 122.4(3) . . ? N1 C8 C9 115.8(3) . . ? C7 C8 C9 121.8(3) . . ? O5 C9 O6 125.4(3) . . ? O5 C9 C8 119.8(3) . . ? O6 C9 C8 114.8(3) . . ? H7C O7 H7B 105(6) . . ? H7C O7 H7A 104(8) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Re1 O4 2.190(2) . ? Re1 O6 2.147(2) . ? Re1 N1 2.227(3) . ? Re1 C1 1.908(3) . ? Re1 C2 1.913(4) . ? Re1 C3 1.900(3) . ? F1 C4 1.331(3) . ? O1 C1 1.155(4) . ? O2 C2 1.143(4) . ? O3 C3 1.148(4) . ? O4 H4A 0.81(5) . ? O4 H4B 0.83(5) . ? O5 C9 1.226(4) . ? O6 C9 1.280(4) . ? N1 C4 1.319(4) . ? N1 C8 1.351(4) . ? C4 C5 1.382(4) . ? C5 H5 0.9500 . ? C5 C6 1.375(5) . ? C6 H6 0.9500 . ? C6 C7 1.394(4) . ? C7 H7 0.9500 . ? C7 C8 1.377(4) . ? C8 C9 1.506(4) . ? O7 H7C 0.89(3) . ? O7 H7B 0.89(3) . ? O7 H7A 0.89(3) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Re1 O6 C9 O5 -176.5(2) . . . . ? Re1 O6 C9 C8 3.0(3) . . . . ? Re1 N1 C4 F1 2.7(4) . . . . ? Re1 N1 C4 C5 -176.3(2) . . . . ? Re1 N1 C8 C7 176.8(2) . . . . ? Re1 N1 C8 C9 -3.0(3) . . . . ? F1 C4 C5 C6 -179.2(3) . . . . ? N1 C4 C5 C6 -0.3(5) . . . . ? N1 C8 C9 O5 179.8(3) . . . . ? N1 C8 C9 O6 0.2(4) . . . . ? C4 N1 C8 C7 -0.1(4) . . . . ? C4 N1 C8 C9 -179.9(2) . . . . ? C4 C5 C6 C7 0.4(5) . . . . ? C5 C6 C7 C8 -0.3(5) . . . . ? C6 C7 C8 N1 0.1(4) . . . . ? C6 C7 C8 C9 -180.0(3) . . . . ? C7 C8 C9 O5 -0.1(4) . . . . ? C7 C8 C9 O6 -179.7(3) . . . . ? C8 N1 C4 F1 179.1(2) . . . . ? C8 N1 C4 C5 0.1(4) . . . . ?