#------------------------------------------------------------------------------ #$Date: 2022-12-15 04:28:26 +0200 (Thu, 15 Dec 2022) $ #$Revision: 279898 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/81/1568128.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1568128 loop_ _publ_author_name 'Zhou, Jiazheng' 'Fan, Zhongxu' 'Zhang, Kewang' 'Yang, Zhihua' 'Pan, Shilie' 'Li, Junjie' _publ_section_title ; Rb2CdSi4S10: novel [Si4S10] T2-supertetrahedra-contained infrared nonlinear optical material with large band gap ; _journal_name_full 'Materials Horizons' _journal_paper_doi 10.1039/D2MH01200F _journal_year 2023 _chemical_formula_moiety 'Cd Rb2 S10 Si4' _chemical_formula_sum 'Cd Rb2 S10 Si4' _chemical_formula_weight 716.30 _space_group_crystal_system orthorhombic _space_group_IT_number 33 _space_group_name_Hall 'P 2c -2n' _space_group_name_H-M_alt 'P n a 21' _audit_creation_date 2021-08-04 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-10-19 deposited with the CCDC. 2022-11-25 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 18.6378(6) _cell_length_b 9.1309(3) _cell_length_c 10.6136(3) _cell_measurement_reflns_used 5068 _cell_measurement_temperature 303.0 _cell_measurement_theta_max 27.46 _cell_measurement_theta_min 2.48 _cell_volume 1806.22(10) _computing_cell_refinement 'SAINT V8.38A (?, 2016)' _computing_data_reduction 'SAINT V8.38A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 303.0 _diffrn_measured_fraction_theta_full 0.992 _diffrn_measured_fraction_theta_max 0.987 _diffrn_measurement_device_type 'PHOTON III C28 detector' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0407 _diffrn_reflns_av_unetI/netI 0.0629 _diffrn_reflns_Laue_measured_fraction_full 0.992 _diffrn_reflns_Laue_measured_fraction_max 0.987 _diffrn_reflns_limit_h_max 24 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 10977 _diffrn_reflns_point_group_measured_fraction_full 0.931 _diffrn_reflns_point_group_measured_fraction_max 0.919 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.547 _diffrn_reflns_theta_min 2.185 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 7.959 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.5892 _exptl_absorpt_correction_type numerical _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 2.634 _exptl_crystal_description block _exptl_crystal_F_000 1352 _exptl_crystal_size_max 0.166 _exptl_crystal_size_mid 0.093 _exptl_crystal_size_min 0.085 _refine_diff_density_max 0.486 _refine_diff_density_min -0.630 _refine_diff_density_rms 0.135 _refine_ls_abs_structure_details ; Flack x determined using 1369 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.016(7) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.900 _refine_ls_hydrogen_treatment undef _refine_ls_matrix_type full _refine_ls_number_parameters 154 _refine_ls_number_reflns 3825 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 0.900 _refine_ls_R_factor_all 0.0331 _refine_ls_R_factor_gt 0.0265 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0564 _refine_ls_wR_factor_ref 0.0638 _reflns_Friedel_coverage 0.766 _reflns_Friedel_fraction_full 0.863 _reflns_Friedel_fraction_max 0.842 _reflns_number_gt 3437 _reflns_number_total 3825 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d2mh01200f2.cif _cod_data_source_block 111111111 _cod_database_code 1568128 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.551 _shelx_estimated_absorpt_t_min 0.352 _olex2_refinement_description ; ; _shelx_res_file ; TITL 111111111_a.res in Pna2(1) 111111111.res created by SHELXL-2016/6 at 18:15:06 on 04-Aug-2021 REM Old TITL 111111111 in Pna2(1) REM SHELXT solution in Pna2(1): R1 0.056, Rweak 0.009, Alpha 0.001 REM 0.275 for 188 systematic absences, Orientation as input REM Flack x = 0.028 ( 0.007 ) from 1300 Parsons' quotients REM Formula found by SHELXT: Si4 S4 Rb2 Cd CELL 0.71073 18.6378 9.1309 10.6136 90 90 90 ZERR 4 0.0006 0.0003 0.0003 0 0 0 LATT -1 SYMM -X,-Y,0.5+Z SYMM 0.5+X,0.5-Y,+Z SYMM 0.5-X,0.5+Y,0.5+Z SFAC Cd Rb S Si UNIT 4 8 40 16 EQIV $1 1-X,-Y,0.5+Z EQIV $2 -0.5+X,0.5-Y,+Z EQIV $3 1.5-X,0.5+Y,-0.5+Z EQIV $4 1.5-X,-0.5+Y,-0.5+Z L.S. 4 0 0 PLAN 10 SIZE 0.166 0.085 0.093 TEMP 29.85 FREE Rb1 Si1 FREE Rb1 Si3_$4 FREE Rb2 Si2_$1 FREE Rb2 Si1_$2 FREE Si2 Rb1_$3 CONF list 4 MORE -1 fmap 2 53 acta OMIT 0 5 -11 OMIT 1 6 -9 OMIT 2 6 -9 REM REM REM WGHT 0.000000 FVAR 0.26098 CD1 1 0.914046 0.337762 0.255299 11.00000 0.02227 0.02317 = 0.02293 0.00012 -0.00075 -0.00095 RB1 2 0.827467 -0.145447 0.500906 11.00000 0.03933 0.02702 = 0.03921 0.00321 0.00572 0.00170 RB2 2 0.401807 0.142766 0.745933 11.00000 0.04588 0.04131 = 0.03743 0.00017 -0.00247 0.01153 S1 3 0.556589 0.144457 0.500717 11.00000 0.02056 0.02401 = 0.02308 0.00012 -0.00099 -0.00406 S2 3 0.760303 0.499616 0.501527 11.00000 0.02115 0.01893 = 0.03341 -0.00326 0.00365 -0.00192 S3 3 0.872441 0.209243 0.453197 11.00000 0.01754 0.02523 = 0.02306 0.00318 0.00175 0.00089 S4 3 0.706067 0.205055 0.309703 11.00000 0.01838 0.03049 = 0.02146 -0.00626 -0.00011 0.00040 S5 3 0.579952 0.108666 0.817294 11.00000 0.02698 0.02143 = 0.01980 0.00155 0.00436 -0.00222 S6 3 0.607720 0.441421 0.695735 11.00000 0.03441 0.01655 = 0.02145 -0.00275 0.00776 0.00099 S7 3 0.649388 0.777660 0.551030 11.00000 0.03064 0.01562 = 0.02632 0.00018 0.00801 -0.00045 S8 3 0.730481 0.156110 0.637191 11.00000 0.01893 0.02205 = 0.02422 0.00300 0.00149 0.00077 S9 3 0.585793 0.498641 0.373103 11.00000 0.03005 0.02176 = 0.02731 0.00110 -0.00700 -0.00024 SI1 4 0.766210 0.269846 0.471187 11.00000 0.01613 0.01800 = 0.01905 -0.00134 0.00025 -0.00016 SI2 4 0.596784 0.268309 0.345079 11.00000 0.01732 0.02276 = 0.01908 -0.00004 -0.00075 -0.00274 S10 3 0.542578 0.210310 0.183753 11.00000 0.02143 0.03947 = 0.01985 -0.00235 -0.00267 -0.00679 SI3 4 0.619185 0.211733 0.659099 11.00000 0.01813 0.01616 = 0.01971 0.00018 0.00195 -0.00154 SI4 4 0.649913 0.551695 0.534344 11.00000 0.02078 0.01613 = 0.02211 -0.00088 0.00208 0.00041 HKLF 4 REM 111111111_a.res in Pna2(1) REM R1 = 0.0265 for 3437 Fo > 4sig(Fo) and 0.0331 for all 3825 data REM 154 parameters refined using 1 restraints END WGHT 0.0000 0.0000 REM Highest difference peak 0.486, deepest hole -0.630, 1-sigma level 0.135 Q1 1 0.5043 0.0446 0.7717 11.00000 0.05 0.49 Q2 1 0.7379 0.0536 0.6219 11.00000 0.05 0.47 Q3 1 0.7221 0.5747 0.4983 11.00000 0.05 0.47 Q4 1 0.7624 0.2034 0.6006 11.00000 0.05 0.46 Q5 1 0.8599 0.3988 0.1652 11.00000 0.05 0.46 Q6 1 0.4864 0.2193 0.8549 11.00000 0.05 0.46 Q7 1 0.8753 0.4168 0.2564 11.00000 0.05 0.44 Q8 1 0.7656 0.1436 0.5750 11.00000 0.05 0.44 Q9 1 0.5014 -0.0159 0.4607 11.00000 0.05 0.44 Q10 1 0.9581 0.4003 0.2503 11.00000 0.05 0.44 ; _shelx_res_checksum 23464 _shelx_hkl_file ; 0 -1 0 0.10 0.70 0 1 0 0.30 0.80 0 -2 0 5731.43 382.36 0 3 0 0.40 2.30 0 -3 0 -1.50 2.20 0 -4 0 539.35 41.40 0 -4 0 549.15 41.50 0 -5 0 0.30 3.60 0 -5 0 0.10 3.60 0 -6 0 2652.53 186.68 0 -6 0 2426.06 175.18 0 -7 0 -16.60 6.60 0 -7 0 2.40 5.30 0 -8 0 218.68 25.10 0 -10 0 363.56 37.40 0 0 -1 1.20 0.80 0 0 1 0.20 0.50 0 0 -1 -0.20 0.30 0 1 1 1181.18 71.39 0 1 -1 954.70 70.09 0 -1 1 1111.89 70.29 0 -1 -1 953.10 70.99 0 -1 -1 1040.70 71.89 0 2 1 -0.40 1.70 0 -2 -1 0.70 1.60 0 -2 1 -0.20 1.40 0 2 -1 0.80 1.20 0 -3 -1 3754.72 248.18 0 -3 1 3502.55 246.98 0 -3 -1 3701.53 248.68 0 3 -1 3745.43 247.08 0 -4 1 -1.60 2.30 0 -4 -1 1.80 2.80 0 -4 -1 1.20 2.50 0 -5 1 145.09 15.10 0 -5 -1 126.19 15.30 0 -5 -1 131.79 15.90 0 -6 -1 0.10 3.50 0 -6 -1 -0.20 6.00 0 -6 1 -0.80 3.50 0 -6 1 -1.20 4.90 0 -7 -1 219.18 30.00 0 -7 1 238.98 24.40 0 -7 -1 242.48 24.90 0 -7 1 237.38 25.00 0 -8 -1 4.20 5.80 0 -8 1 4.50 5.80 0 -9 -1 98.19 18.70 0 -9 1 72.89 15.60 0 -10 -1 1.20 8.50 0 -10 1 -3.00 8.20 0 -11 1 37.10 14.60 0 -11 -1 13.20 11.40 0 0 -2 506.85 35.70 0 0 -2 530.25 37.10 0 0 2 541.75 37.30 0 -1 2 0.80 0.80 0 -1 -2 -1.40 1.20 0 -1 -2 1.50 1.80 0 -2 -2 486.05 36.60 0 2 -2 489.95 33.40 0 -2 2 457.75 33.20 0 -2 -2 476.85 35.30 0 -3 2 -1.50 1.40 0 -3 -2 1.20 2.60 0 -3 -2 0.50 2.70 0 -4 -2 1300.57 96.59 0 -4 2 1346.87 93.39 0 -4 -2 1373.76 95.39 0 -5 -2 2.90 3.70 0 -5 2 1.10 3.00 0 -5 -2 -4.30 4.50 0 -5 2 2.70 3.50 0 -6 2 192.18 18.60 0 -6 2 161.28 17.20 0 -6 -2 157.98 19.10 0 -6 -2 166.88 20.80 0 -7 2 1.80 5.50 0 -7 -2 -3.80 4.20 0 -7 2 -7.50 5.80 0 -8 2 458.25 41.50 0 -8 -2 517.05 43.90 0 -8 2 448.76 41.00 0 -9 -2 2.90 7.10 0 -9 2 -4.60 5.60 0 -10 -2 132.19 23.70 0 -10 2 170.38 25.80 0 -11 2 18.30 11.90 0 -11 -2 -4.50 11.10 0 0 -3 2.00 1.90 0 0 3 -0.70 1.60 0 0 -3 -0.70 0.90 0 -1 -3 1570.44 104.39 0 -1 -3 1554.64 102.19 0 -1 3 1383.66 101.29 0 -2 -3 1.60 2.40 0 -2 3 0.60 0.90 0 -2 -3 -1.10 3.00 0 -3 -3 102.89 12.50 0 -3 -3 82.39 10.60 0 -3 3 91.79 8.50 0 -4 -3 0.90 3.30 0 -4 3 -1.40 1.70 0 -4 3 2.70 2.30 0 -4 -3 -1.90 4.80 0 -5 3 714.23 50.89 0 -5 3 659.03 48.70 0 -6 -3 4.30 7.70 0 -6 3 -1.20 3.30 0 -6 -3 -4.60 3.80 0 -6 3 -7.00 4.00 0 -7 -3 668.53 55.89 0 -7 3 682.03 52.39 0 -7 3 705.33 54.89 0 -8 3 1.20 5.80 0 -8 3 3.50 8.00 0 -9 -3 103.09 18.90 0 -9 3 74.39 15.60 0 -10 -3 -0.30 8.80 0 -10 3 -5.40 8.30 0 -11 3 222.08 31.00 0 -11 -3 226.38 33.40 0 0 -4 9540.55 643.84 0 0 -4 9848.81 646.34 0 1 -4 -0.20 0.80 0 -1 -4 2.30 2.10 0 -1 -4 -2.00 2.60 0 -1 4 0.50 1.90 0 -2 -4 530.25 39.00 0 -2 4 492.15 36.40 0 -2 -4 546.65 41.80 0 -3 4 0.60 1.30 0 -3 -4 0.50 2.70 0 -3 -4 1.10 4.30 0 -4 -4 2754.72 187.48 0 -4 -4 2563.24 189.48 0 -4 4 2810.92 183.08 0 -5 -4 -0.30 3.50 0 -5 -4 -2.20 7.30 0 -5 4 -1.60 2.30 0 -5 4 3.30 2.20 0 -6 4 1436.26 104.79 0 -6 4 1580.34 104.59 0 -6 -4 1477.35 108.89 0 -6 -4 1455.55 112.09 0 -7 4 -7.40 4.70 0 -7 4 1.50 3.80 0 -8 4 157.28 19.60 0 -8 4 160.68 21.00 0 -9 4 8.20 7.30 0 -9 -4 -4.60 7.20 0 -10 4 648.04 56.69 0 -10 -4 693.23 61.89 0 -11 4 15.30 12.10 0 -11 -4 2.70 12.70 0 0 -5 -0.90 2.80 0 0 -5 -0.10 1.50 0 1 -5 1509.05 104.49 0 -1 -5 1561.44 105.39 0 -1 -5 1525.55 108.29 0 -2 -5 2.40 2.60 0 -2 -5 1.30 4.00 0 -3 -5 262.57 23.00 0 -3 -5 238.58 25.40 0 -4 5 2.00 1.60 0 -4 -5 0.40 4.00 0 -4 -5 3.70 6.00 0 -5 5 313.17 22.30 0 -5 -5 234.18 29.40 0 -5 -5 249.08 26.00 0 -6 5 1.20 3.30 0 -6 -5 3.80 5.50 0 -7 5 295.17 25.90 0 -7 5 278.17 22.60 0 -8 5 -7.80 6.70 0 -8 5 3.30 5.30 0 -8 -5 4.30 6.60 0 -9 5 58.99 12.30 0 -9 -5 51.79 14.70 0 -10 -5 -16.60 9.40 0 -10 5 -7.10 7.00 0 -11 5 20.90 11.50 0 0 -6 976.70 66.39 0 0 -6 938.91 69.29 0 1 -6 3.20 2.90 0 -1 -6 3.50 2.60 0 -1 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0 -9 1.50 2.30 0 -1 -9 64.19 9.90 0 1 -9 68.69 9.70 0 -1 -9 75.09 15.10 0 -2 -9 -15.80 7.80 0 -2 -9 -1.10 4.00 0 -3 -9 160.48 26.20 0 -3 -9 140.29 17.90 0 -4 -9 -4.40 4.90 0 -4 -9 -10.30 17.20 0 -5 -9 189.48 23.10 0 -6 -9 -8.10 5.60 0 -7 -9 6.80 9.40 0 -8 -9 16.70 12.30 0 0 -10 360.06 26.90 0 -1 -10 -0.30 3.60 0 -1 -10 -8.00 8.60 0 1 -10 -0.40 4.10 0 -2 -10 653.43 49.70 0 -2 -10 618.64 55.99 0 -3 -10 6.50 6.10 0 -3 -10 -3.50 13.60 0 -4 -10 254.97 26.90 0 -6 -10 24.90 11.10 0 -7 -10 9.70 10.40 0 -8 -10 34.50 14.70 0 0 -11 2.70 3.30 0 0 -11 -7.30 8.60 0 -1 -11 344.77 28.50 0 -1 -11 362.06 36.70 0 -2 -11 -0.90 5.00 0 -3 -11 3.60 6.40 0 -4 -11 4.20 6.50 0 -5 -11 -15.30 6.40 0 -6 -11 -14.00 9.20 0 -7 -11 40.40 16.10 0 0 -12 391.86 36.60 0 1 -12 1.90 5.10 0 -1 -12 -8.40 4.10 0 1 -12 -0.80 5.10 0 -3 -12 4.30 7.80 0 -4 -12 580.44 58.69 0 -5 -12 -12.60 9.30 0 -1 -13 80.99 10.80 0 1 -13 85.69 10.60 0 -3 -13 -8.80 7.10 -1 0 0 -0.20 0.20 -1 -1 0 562.34 38.10 -1 -1 0 542.45 38.10 -1 -2 0 1128.69 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3 -3 381.96 34.70 10 3 -3 412.76 34.80 10 3 3 431.36 35.70 10 3 3 413.26 37.90 -10 -3 3 440.56 36.80 10 -4 3 88.09 12.90 10 4 -3 68.49 12.60 -10 -4 -3 100.79 16.40 -10 -4 -3 86.19 17.90 10 4 -3 93.09 15.10 -10 -4 3 143.69 20.30 10 4 3 149.88 23.20 10 4 3 102.99 15.20 10 -5 3 56.29 11.40 -10 -5 -3 24.00 8.90 10 5 -3 43.00 9.80 10 5 -3 36.20 9.40 -10 -5 3 63.59 14.10 10 5 3 44.10 12.90 10 5 3 46.60 11.60 10 6 -3 233.18 27.50 10 -6 3 342.17 29.40 10 6 -3 273.47 27.30 10 6 3 373.76 35.80 10 6 3 319.67 30.80 10 -7 3 63.99 13.20 10 7 -3 66.09 12.20 10 7 -3 49.60 12.20 10 7 3 63.09 15.40 10 7 3 63.89 15.50 -10 -8 -3 6.80 9.20 10 8 -3 20.90 9.30 10 -8 3 13.10 8.20 10 8 3 9.50 7.80 10 8 3 34.90 13.90 10 9 -3 23.90 10.00 -10 -9 -3 14.60 10.70 10 -9 3 10.70 10.40 10 -9 -3 11.00 16.40 10 9 3 5.00 8.70 10 10 -3 50.09 15.00 10 -10 3 46.50 14.80 -10 -10 -3 13.40 16.60 10 10 3 62.79 18.40 10 -10 -3 27.60 15.10 10 0 4 49.90 11.20 10 0 4 44.70 8.70 10 -1 4 185.18 18.80 10 1 -4 166.98 18.60 -10 -1 -4 139.99 18.40 10 1 4 178.78 21.80 -10 1 -4 157.18 17.60 10 1 4 158.18 17.20 10 -1 -4 139.79 18.50 10 2 -4 475.75 41.80 10 -2 4 573.24 43.10 -10 -2 -4 496.55 44.20 10 2 4 580.24 45.80 -10 -2 4 484.45 42.90 10 2 4 540.65 42.20 -10 2 -4 511.35 41.40 -10 -3 -4 134.09 21.00 10 3 -4 120.99 15.50 10 3 -4 103.69 14.90 10 -3 4 157.48 17.00 10 3 4 177.98 18.40 10 3 4 149.79 19.30 -10 -3 4 158.88 18.10 10 4 -4 1062.29 76.19 10 4 -4 1029.00 76.19 10 -4 4 1014.60 76.39 -10 -4 -4 1021.50 78.69 10 4 4 1037.30 78.09 -10 -5 -4 -3.70 5.20 10 5 -4 5.70 4.80 10 5 -4 -0.10 5.20 10 -5 4 3.50 5.10 10 5 4 0.90 5.80 10 5 4 4.00 5.80 10 -6 4 190.48 20.10 10 6 -4 177.58 18.50 10 6 -4 161.68 20.00 10 6 4 199.48 26.30 10 6 4 199.38 23.50 -10 -7 -4 95.99 19.80 10 7 -4 90.09 15.80 10 7 -4 97.09 12.10 10 -7 4 87.39 15.40 10 7 4 90.09 17.30 10 7 4 92.39 20.40 -10 -8 -4 81.19 18.70 10 8 -4 94.09 16.30 10 -8 4 96.39 17.10 10 -8 4 77.29 14.90 10 8 4 62.49 16.30 10 8 4 77.89 18.50 10 9 -4 38.30 12.30 -10 -9 -4 19.20 12.80 10 -9 4 22.80 11.20 10 -9 4 74.99 14.50 10 -9 -4 41.00 15.10 10 9 4 61.59 15.80 10 -10 4 124.29 22.40 10 10 -4 162.48 34.60 10 -10 4 154.98 20.90 -10 -10 -4 113.29 27.10 10 -10 -4 137.49 26.30 10 10 4 131.59 24.60 10 0 5 614.74 50.79 10 0 5 588.54 53.29 -10 0 -5 737.23 54.39 10 0 -5 784.42 55.79 10 -1 5 402.26 33.40 10 1 -5 442.66 36.90 -10 -1 -5 447.16 37.70 10 -1 5 402.86 36.30 10 1 5 413.06 34.40 -10 1 -5 425.36 35.40 10 1 5 390.66 37.30 10 -1 -5 410.16 37.40 10 2 -5 3.70 3.90 -10 -2 -5 2.50 6.40 10 -2 5 3.20 3.80 10 2 5 0.40 4.60 10 2 5 1.50 4.20 10 3 -5 13.60 5.30 10 -3 5 14.10 5.80 -10 -3 -5 15.10 11.60 10 3 -5 12.40 6.10 10 3 5 11.00 6.60 10 3 5 13.40 6.60 -10 -3 5 9.30 11.30 10 -4 5 348.57 31.50 -10 -4 -5 335.87 38.30 10 4 -5 384.86 31.10 10 4 -5 379.76 31.70 -10 -4 -5 377.16 34.50 -10 -4 5 344.97 36.30 10 4 5 382.76 37.90 10 4 5 338.77 33.50 10 5 -5 162.38 19.30 10 5 -5 169.58 17.50 -10 -5 -5 177.88 22.70 10 -5 5 184.08 19.50 10 5 5 189.18 25.00 10 5 5 183.28 22.50 10 6 -5 503.75 40.80 10 6 -5 526.85 37.40 10 -6 5 433.06 39.00 10 6 5 416.46 42.10 10 6 5 468.55 47.60 10 7 -5 146.89 18.30 -10 -7 -5 121.59 21.30 10 -7 5 116.99 16.50 10 7 5 139.19 22.30 10 7 5 97.39 21.20 10 -8 5 14.10 8.10 10 -8 5 9.40 7.20 10 8 -5 -2.40 6.60 10 8 5 16.00 12.20 10 -8 -5 7.70 9.20 10 8 5 -7.60 8.10 -10 -9 -5 21.90 14.30 10 9 -5 70.59 15.10 10 -9 5 80.49 18.90 10 -9 5 103.59 16.90 10 9 5 79.29 17.90 10 -9 -5 59.99 16.80 10 0 6 1059.79 75.89 10 0 -6 934.11 74.59 -10 0 -6 950.60 73.89 10 0 6 957.20 70.89 10 -1 6 572.64 46.10 10 -1 6 522.85 41.90 -10 -1 -6 538.45 46.40 10 1 -6 559.84 45.40 -10 1 -6 568.94 44.60 10 1 6 524.45 46.70 10 -1 -6 543.15 47.20 10 1 6 522.75 43.10 -10 -2 -6 68.09 14.70 10 2 -6 60.59 13.00 10 -2 6 105.69 11.70 10 -2 6 111.29 17.20 10 2 6 98.29 18.00 10 2 6 87.39 13.30 -10 2 -6 73.89 12.40 10 -3 6 206.18 20.90 10 3 -6 199.58 20.00 10 3 -6 181.98 19.40 -10 -3 -6 136.59 23.20 10 3 6 188.18 25.00 10 3 6 244.28 22.60 10 4 -6 513.25 42.10 10 4 -6 532.85 41.40 10 -4 6 561.34 43.60 -10 -4 -6 500.35 45.40 10 4 6 506.05 49.20 10 4 6 532.55 45.00 10 5 -6 734.83 56.09 10 -5 6 810.02 59.79 10 5 -6 730.63 59.09 10 5 6 834.02 69.89 10 5 6 802.62 63.19 10 -6 6 695.63 54.99 10 6 -6 761.12 56.19 10 6 6 692.63 59.49 10 6 6 671.03 63.99 -10 -7 -6 26.20 12.10 10 -7 6 56.49 11.30 10 7 -6 24.80 9.20 10 -7 6 49.90 10.80 10 7 6 47.50 18.10 10 7 6 48.60 13.80 10 -8 6 60.49 12.80 10 8 -6 85.49 15.10 -10 -8 -6 86.19 21.90 10 -8 6 68.79 13.40 10 8 6 76.89 17.70 10 -8 -6 93.09 19.70 10 9 -6 165.98 23.30 -10 -9 -6 147.29 28.20 10 -9 6 130.39 20.50 10 9 6 146.39 25.60 10 -9 -6 173.28 28.00 -10 0 -7 229.78 26.40 10 0 -7 268.57 28.20 10 0 7 292.47 29.40 10 0 7 297.27 25.30 10 -1 7 266.37 24.50 10 -1 7 297.57 29.20 10 1 -7 253.67 27.80 -10 -1 -7 325.27 31.00 -10 1 -7 314.47 28.10 10 -1 -7 308.57 31.10 10 1 7 283.87 26.20 10 1 7 268.57 30.10 10 -2 7 487.65 37.70 10 2 -7 462.95 40.40 10 -2 7 479.35 41.40 -10 2 -7 521.35 39.30 10 2 7 470.65 40.10 10 2 7 466.75 44.90 10 -3 7 23.70 8.60 10 -3 7 11.60 4.90 10 3 -7 31.50 7.40 10 3 -7 27.80 7.80 -10 -3 -7 9.90 14.40 10 3 7 12.10 8.60 10 3 7 16.00 7.50 10 -4 7 114.99 16.30 10 4 -7 142.49 16.20 10 4 -7 162.98 15.50 -10 -4 -7 133.39 20.40 10 4 7 147.19 19.20 10 4 7 114.99 22.40 10 5 -7 132.89 15.80 10 -5 7 97.99 14.90 10 5 7 133.79 25.30 10 5 7 125.09 19.60 -10 -6 -7 23.00 10.50 10 6 -7 34.20 8.80 10 -6 7 45.00 10.50 10 6 7 29.40 10.20 10 6 7 15.80 14.00 10 -7 7 59.09 11.80 -10 -7 -7 69.29 16.40 10 7 -7 65.29 12.50 10 7 7 78.59 16.70 10 -7 -7 73.29 17.70 10 7 7 95.69 23.40 -10 -8 -7 48.30 16.40 10 -8 7 58.69 12.70 10 8 -7 62.59 13.10 10 -8 -7 58.89 15.50 10 8 7 53.19 15.60 10 0 -8 335.17 31.20 10 0 8 267.37 25.00 -10 0 -8 281.47 29.30 10 0 8 263.87 29.80 10 1 -8 396.46 34.70 -10 -1 -8 408.16 37.20 10 -1 8 372.86 35.10 10 -1 8 347.07 29.60 10 1 8 301.87 30.40 -10 1 -8 360.86 33.10 10 1 8 342.57 36.60 10 -1 -8 388.06 37.10 10 -2 8 164.78 20.40 10 2 -8 168.88 19.00 10 -2 8 160.38 15.40 -10 -2 -8 190.68 27.10 10 2 8 136.09 24.50 10 2 8 161.08 19.20 -10 2 -8 147.49 16.80 10 3 -8 103.29 14.40 10 -3 8 157.78 17.20 10 3 -8 105.09 13.90 10 -3 8 121.59 12.60 -10 -3 -8 73.29 22.50 10 3 8 133.39 25.30 -10 -4 -8 17.40 8.10 10 4 -8 14.10 5.30 10 -4 8 22.80 5.20 10 -4 8 28.60 8.50 10 4 -8 11.20 5.60 10 4 8 30.40 14.00 10 4 8 18.10 8.00 10 5 -8 85.49 12.60 10 -5 8 61.29 9.70 10 -5 8 82.59 14.40 10 5 8 84.89 16.40 10 5 8 74.19 22.00 -10 -6 -8 50.29 16.40 10 6 -8 81.89 13.40 10 -6 8 89.49 15.30 10 -6 8 68.99 11.30 10 6 8 126.99 27.80 10 6 8 82.39 16.60 10 -7 8 11.20 8.80 10 7 -8 15.90 8.50 10 -7 8 15.30 6.40 10 7 8 3.20 11.70 10 -7 -8 27.80 12.90 10 7 8 26.80 12.80 -10 -8 -8 4.70 13.40 10 8 -8 1.80 8.00 10 -8 -8 -2.60 12.80 10 8 8 1.20 10.10 10 0 -9 111.89 21.20 -10 0 -9 149.88 22.30 10 0 9 181.58 23.60 10 0 9 190.08 17.90 10 -1 9 90.29 12.30 10 1 -9 88.79 16.90 10 -1 9 101.69 19.50 -10 -1 -9 67.39 18.00 10 -1 -9 70.39 16.70 10 1 9 95.49 19.10 10 1 9 103.89 15.00 10 -2 9 140.99 14.90 10 -2 9 174.98 21.80 10 2 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-10 239.28 24.80 10 2 -10 172.98 18.80 10 -2 10 169.08 15.00 10 2 -10 165.98 19.20 10 -2 10 147.19 21.50 10 2 -10 164.88 21.10 10 2 10 149.49 19.30 10 2 10 152.58 27.90 10 3 -10 79.19 11.00 10 3 -10 64.19 11.10 10 -3 10 88.39 17.20 10 3 10 72.29 14.40 10 3 10 72.59 21.40 10 4 -10 117.39 14.70 10 -4 10 139.69 19.60 10 4 10 90.99 29.90 10 4 10 137.29 20.70 10 5 -10 453.95 36.80 10 -5 10 465.65 40.80 -10 -5 -10 483.15 46.10 10 -5 -10 453.15 45.30 10 5 10 462.85 43.50 10 5 10 458.15 52.49 -10 -6 -10 346.17 59.29 10 6 -10 265.37 23.10 10 -6 -10 191.28 31.50 10 6 10 209.68 35.30 10 0 -11 113.99 21.40 10 0 11 140.59 15.20 10 0 11 129.79 23.90 10 1 -11 20.30 9.30 10 -1 11 41.30 14.60 10 1 11 28.00 8.40 10 -1 -11 17.60 11.00 10 1 11 22.00 13.90 10 2 -11 2.00 5.50 10 2 -11 -1.20 5.40 10 -2 11 6.10 11.50 10 2 11 -6.00 7.40 10 2 11 -1.00 6.20 10 -2 -11 2.80 10.10 10 3 -11 28.90 7.50 10 -3 11 25.60 12.20 10 -3 -11 0.40 7.00 10 3 11 15.10 12.30 10 3 11 14.20 9.40 10 4 -11 8.50 5.90 10 -4 11 21.60 10.10 10 4 11 20.30 10.40 10 4 11 15.10 14.60 10 -4 -11 6.40 10.60 -10 -5 -11 24.00 13.70 10 5 -11 30.60 9.80 10 -5 -11 21.80 23.40 10 0 -12 101.09 19.70 10 0 12 101.69 22.90 10 1 -12 28.80 11.70 10 -1 12 27.40 13.10 10 -1 -12 27.90 13.20 10 -1 -12 38.30 11.40 10 1 12 30.40 15.00 10 2 -12 104.59 14.00 10 2 -12 87.59 12.70 10 -2 12 116.09 22.40 10 -2 -12 88.29 21.30 10 2 12 82.19 20.30 10 3 -12 97.79 12.70 10 -3 12 135.29 23.30 10 3 12 107.39 26.40 10 -3 -12 116.49 20.10 -11 0 0 5.40 5.40 11 0 0 7.50 5.50 11 -1 0 11.50 6.80 -11 -1 0 17.60 7.10 11 1 0 10.30 5.50 -11 -2 0 9.50 5.80 11 2 0 8.30 5.20 11 2 0 3.20 4.90 11 -2 0 9.10 5.90 11 -3 0 279.47 25.80 11 3 0 245.68 23.90 11 3 0 215.78 24.10 -11 -3 0 241.88 25.70 -11 -4 0 1460.85 109.69 11 -4 0 1342.17 107.29 11 4 0 1429.26 102.29 11 4 0 1390.56 103.49 11 5 0 338.87 32.80 11 5 0 265.17 28.90 11 6 0 272.47 28.50 11 6 0 279.27 29.60 11 7 0 28.50 10.90 11 7 0 30.60 10.50 -11 -7 0 29.60 10.80 11 8 0 118.39 20.90 11 8 0 100.49 18.50 -11 -8 0 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20.70 -13 -1 -3 108.09 21.60 13 -1 -3 183.78 21.20 -13 1 -3 161.38 19.50 13 1 3 138.19 17.70 13 1 3 150.18 19.80 13 2 -3 191.68 22.00 -13 -2 -3 177.88 24.10 13 -2 3 178.88 21.50 13 -2 -3 211.18 24.30 13 2 3 189.28 23.30 13 2 3 188.48 21.20 13 3 -3 196.68 21.70 13 3 -3 196.38 20.70 -13 -3 -3 198.28 25.60 13 -3 3 110.49 23.90 13 3 3 114.89 22.80 13 -3 -3 192.48 23.40 13 4 -3 23.60 8.80 13 -4 3 41.70 12.00 13 -4 -3 36.70 12.70 13 4 3 43.10 11.40 13 4 3 35.20 12.40 13 5 -3 12.20 7.80 13 5 -3 2.40 6.30 13 -5 3 27.40 10.00 13 5 3 24.30 11.70 13 5 3 22.60 9.00 13 6 -3 160.78 21.10 13 -6 3 192.18 23.40 13 6 -3 161.68 21.90 13 6 3 203.98 23.70 13 6 3 203.98 27.20 13 7 -3 12.60 8.00 13 7 -3 2.60 5.80 -13 -7 -3 1.90 9.50 13 7 3 1.80 9.50 13 7 3 9.10 8.10 13 -8 3 506.25 47.10 -13 -8 -3 488.65 51.99 13 8 -3 518.45 44.90 13 8 -3 491.55 46.90 13 8 3 539.05 49.40 13 8 3 546.25 53.79 -13 -9 -3 59.99 20.20 13 9 -3 32.70 13.30 13 -9 3 54.49 14.80 13 9 3 23.80 15.00 13 9 3 54.19 14.20 13 0 -4 1.20 5.20 13 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162.78 25.10 13 9 -4 173.98 25.60 -13 -9 -4 157.08 27.80 13 9 4 132.59 25.30 13 9 4 123.29 27.80 -13 0 -5 3.80 8.40 13 0 5 1.60 4.60 13 0 -5 -1.30 6.10 13 0 5 1.70 4.70 13 1 -5 28.30 10.90 13 -1 5 16.70 6.30 -13 -1 -5 44.50 16.00 13 -1 5 23.20 9.50 13 1 5 16.20 7.50 -13 1 -5 31.40 12.00 13 1 5 16.50 8.50 13 -1 -5 32.10 11.10 13 2 -5 513.75 44.10 -13 -2 -5 442.16 46.50 13 -2 5 530.55 50.29 13 2 5 513.15 46.50 13 -2 -5 497.55 46.20 13 2 5 486.95 42.50 -13 2 -5 521.35 43.20 13 -3 5 36.00 10.70 13 3 -5 8.70 7.90 13 3 -5 9.40 6.60 13 -3 -5 21.90 11.40 13 3 5 38.70 14.00 13 3 5 31.60 8.90 13 4 -5 490.55 41.80 13 -4 5 476.55 42.40 13 4 5 467.95 47.00 13 4 5 485.35 43.10 13 -5 5 53.59 12.60 13 5 -5 36.10 9.50 13 5 -5 28.80 9.80 13 5 5 29.30 11.10 13 5 5 48.10 17.10 13 -6 5 113.69 16.80 -13 -6 -5 117.79 21.70 13 6 -5 146.39 16.90 13 6 -5 117.89 18.30 13 6 5 132.49 22.10 13 6 5 74.69 19.40 -13 -7 -5 26.70 12.80 13 -7 5 57.99 13.80 13 7 -5 38.10 11.90 13 7 -5 47.10 10.50 13 7 5 49.40 18.40 13 7 5 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7.30 13 5 7 5.60 7.30 13 5 7 6.40 10.00 13 -6 7 54.09 13.10 13 6 -7 49.20 11.30 13 6 -7 42.10 8.30 13 6 7 32.10 12.90 13 6 7 50.69 17.20 13 7 -7 41.30 12.10 13 -7 7 14.70 8.20 -13 -7 -7 48.80 16.70 13 7 7 22.20 11.50 13 7 7 11.10 13.40 13 0 8 1.30 5.30 13 0 8 3.20 8.00 -13 0 -8 -6.10 12.20 13 0 -8 9.50 9.10 -13 -1 -8 19.70 16.60 13 -1 8 36.10 9.10 13 -1 8 27.10 11.30 13 1 -8 23.80 11.00 13 -1 -8 32.20 13.40 13 1 8 28.70 9.10 -13 1 -8 31.90 11.70 13 1 8 26.50 12.00 13 -2 8 570.44 48.50 13 -2 8 532.45 43.10 13 2 -8 516.25 46.90 13 2 8 558.34 46.20 -13 2 -8 529.75 46.00 13 -2 -8 541.45 52.29 13 2 8 530.55 52.09 13 3 -8 167.58 20.50 13 3 -8 155.08 23.90 13 -3 8 143.39 17.60 13 -3 8 175.68 21.80 13 3 8 168.38 30.50 13 3 8 171.28 22.20 13 -3 -8 172.58 31.40 13 -4 8 110.69 14.90 13 4 -8 139.79 16.60 13 4 -8 121.69 19.50 13 -4 8 139.09 19.80 13 4 8 157.28 36.00 13 4 8 116.09 19.60 13 -5 8 120.09 15.80 13 -5 8 139.89 19.50 13 5 -8 133.09 14.90 13 5 -8 138.39 19.30 13 5 8 110.49 26.00 13 5 8 143.69 22.80 13 -6 8 413.86 37.70 13 6 -8 367.36 35.80 13 6 8 380.26 40.00 13 6 8 420.76 49.10 13 7 -8 162.28 21.90 13 -7 8 138.89 18.90 -13 -7 -8 130.49 27.70 13 7 8 125.69 23.40 13 7 8 188.38 36.30 13 0 -9 0.70 7.70 13 0 9 8.40 9.70 13 0 9 -2.50 4.90 13 1 -9 18.20 11.70 13 -1 9 35.10 8.50 13 -1 9 29.30 11.80 13 1 9 26.50 15.50 13 1 9 47.50 14.20 13 -1 -9 29.70 11.70 13 -2 9 199.78 25.80 13 -2 9 174.78 20.10 13 2 -9 196.68 24.10 13 -2 -9 236.28 30.40 -13 2 -9 204.88 24.10 13 2 9 228.28 24.50 13 2 9 239.18 31.60 13 3 -9 55.39 13.00 13 -3 9 52.29 10.10 13 3 9 68.99 14.10 13 3 9 47.90 15.80 13 -3 -9 48.40 19.40 13 -4 9 137.19 19.40 13 4 -9 129.89 24.90 13 4 -9 126.69 15.90 13 -4 9 127.59 15.10 13 4 9 151.78 30.70 13 4 9 129.19 21.20 13 5 -9 18.40 8.30 13 -5 9 10.50 8.10 13 -5 9 11.40 6.00 13 5 9 -1.80 8.80 13 5 9 6.10 11.50 13 -6 9 19.30 9.40 13 -6 9 20.80 6.90 13 6 -9 35.30 11.00 13 6 9 25.20 12.60 13 6 9 21.50 18.60 13 0 -10 3.20 8.70 13 0 10 1.20 6.20 13 0 10 -5.90 7.70 13 1 -10 8.30 9.80 13 -1 10 9.70 8.90 13 -1 10 5.50 5.60 13 -1 -10 4.20 9.40 13 1 10 6.70 6.90 13 1 10 2.00 10.00 13 -2 10 13.40 10.20 13 2 -10 11.50 8.00 13 -2 10 4.60 6.00 13 2 -10 10.50 7.50 13 -2 -10 2.20 8.30 13 2 10 2.30 8.00 13 2 10 7.50 9.70 13 3 -10 330.27 30.00 13 -3 10 296.37 33.70 13 -3 10 294.37 26.20 13 -3 -10 347.97 40.80 13 3 10 325.57 41.40 13 3 10 310.97 32.20 13 -4 10 29.70 11.50 13 -4 10 31.70 6.70 13 4 -10 31.50 10.30 13 4 -10 26.80 9.30 13 4 -10 36.70 7.70 13 4 10 19.20 10.70 13 4 10 27.20 15.20 13 -5 10 67.69 15.70 13 5 10 77.59 23.20 13 5 10 64.09 16.40 13 0 11 -1.10 9.20 13 0 -11 3.40 7.30 13 0 11 -0.80 6.20 13 -1 11 -2.30 5.50 13 -1 11 -8.70 7.70 13 1 -11 9.80 9.30 13 1 11 6.80 8.20 13 1 11 10.90 11.60 13 -1 -11 -4.60 10.00 13 2 -11 257.27 26.80 13 2 -11 209.08 25.10 13 -2 11 252.97 21.70 13 -2 11 235.78 31.00 13 2 11 192.68 48.20 13 2 11 225.78 26.80 13 -2 -11 225.08 32.90 13 -3 11 59.49 15.80 13 -3 11 56.89 11.30 13 3 -11 77.39 14.80 13 3 -11 68.39 12.70 13 3 11 51.19 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725.93 59.19 -14 -2 -2 -23.20 14.30 14 -2 2 -5.70 3.70 14 2 -2 0.50 4.90 14 2 -2 -0.70 4.60 14 -2 -2 4.10 6.30 14 2 2 1.30 5.70 14 2 2 -4.00 5.60 14 3 -2 34.60 10.70 14 3 -2 27.00 9.30 14 -3 2 66.89 14.80 14 3 2 73.79 16.10 14 3 2 49.30 11.50 14 -3 -2 38.10 11.20 14 4 -2 51.59 12.50 14 4 -2 75.99 14.50 14 -4 2 81.69 16.60 14 4 2 66.49 16.10 14 4 2 93.09 16.30 14 -4 -2 42.80 13.00 14 5 -2 892.71 70.99 14 -5 2 943.91 72.39 14 5 -2 837.42 69.69 14 5 2 888.21 70.89 14 -5 -2 815.52 73.09 14 5 2 960.50 74.69 14 6 -2 243.18 27.20 14 -6 2 244.08 27.90 14 6 -2 237.78 27.60 14 -6 -2 224.88 30.20 14 6 2 229.28 29.60 14 6 2 256.07 27.90 14 7 -2 275.87 32.00 14 7 -2 313.17 32.90 14 -7 2 305.97 33.60 14 7 2 339.07 37.10 14 7 2 308.57 33.20 14 -8 2 42.90 13.40 14 8 -2 27.80 12.20 14 8 -2 40.90 12.80 14 8 2 17.90 13.30 14 8 2 31.80 12.60 14 9 -2 20.30 10.50 14 9 -2 6.90 9.80 14 -9 2 25.70 11.90 14 9 2 13.60 9.90 14 9 2 12.00 11.90 14 0 3 506.05 41.80 14 0 -3 474.75 44.60 14 0 3 537.45 45.40 -14 0 -3 480.55 48.80 14 1 -3 86.59 16.10 14 -1 3 142.99 18.50 -14 -1 -3 90.99 18.00 14 1 3 138.99 22.60 14 -1 -3 108.39 19.50 14 1 3 116.99 17.10 -14 1 -3 137.39 21.10 14 -2 3 46.60 13.30 14 2 -3 42.10 12.00 14 -2 -3 42.20 13.10 14 2 3 56.49 15.40 14 2 3 41.40 12.30 14 3 -3 215.58 23.80 14 -3 3 196.18 23.10 14 3 -3 189.38 22.10 14 3 3 180.48 24.50 14 -3 -3 195.58 25.30 14 3 3 183.78 22.10 14 4 -3 3.10 6.30 14 -4 3 2.90 4.80 14 4 -3 5.20 6.90 14 4 3 2.50 5.70 14 4 3 9.70 9.30 14 -4 -3 13.20 9.40 14 5 -3 245.38 27.20 14 5 -3 250.77 27.30 14 -5 3 253.47 27.90 14 -5 -3 257.77 31.60 14 5 3 279.47 28.70 14 5 3 255.17 30.80 14 6 -3 346.27 34.20 14 -6 3 383.66 36.00 14 6 -3 318.57 34.00 14 6 3 258.47 49.80 14 6 3 378.76 36.20 14 7 -3 28.50 10.50 14 -7 3 25.60 10.70 14 7 -3 30.30 10.10 14 7 3 21.10 9.50 14 7 3 36.20 16.30 14 8 -3 200.98 28.20 14 -8 3 285.17 30.80 14 8 -3 243.38 32.30 14 8 3 248.28 33.80 14 8 3 264.07 31.50 -14 -9 -3 64.99 21.90 14 -9 3 64.69 16.60 14 9 -3 83.69 17.60 14 9 3 63.39 16.40 14 9 3 92.89 23.10 14 0 4 640.64 57.59 14 0 -4 894.01 64.39 -14 0 -4 874.11 63.89 14 0 4 661.73 60.99 -14 -1 -4 911.21 75.99 14 1 -4 949.21 75.29 14 -1 4 996.70 75.69 -14 1 -4 955.40 74.49 14 1 4 988.40 76.69 14 -1 -4 896.41 75.99 14 1 4 985.10 73.09 14 -2 4 85.39 16.60 14 2 -4 86.39 17.10 14 2 4 82.79 17.60 14 -2 -4 81.99 18.20 14 2 4 92.09 15.40 14 -3 4 23.80 9.70 14 3 -4 17.70 8.80 14 3 -4 22.60 8.70 14 -3 -4 15.10 9.30 14 3 4 17.20 7.50 14 3 4 27.30 11.20 14 4 -4 126.59 19.70 14 -4 4 154.38 20.60 14 4 -4 131.59 21.60 14 4 4 170.28 24.10 14 4 4 156.78 20.60 14 -4 -4 133.49 26.20 14 5 -4 342.17 34.30 14 5 -4 346.37 34.40 14 5 4 421.46 41.60 14 5 4 372.66 36.40 14 6 -4 122.99 18.10 14 6 -4 135.29 20.30 14 6 4 155.28 29.10 14 6 4 115.69 20.50 14 -7 4 194.48 26.90 14 7 -4 110.79 20.40 14 7 -4 177.58 21.10 14 7 4 163.98 25.20 14 7 4 167.88 28.50 14 8 -4 111.19 21.20 14 -8 4 166.98 23.10 -14 -8 -4 146.19 28.80 14 8 -4 126.29 18.50 14 8 4 147.59 29.30 14 8 4 210.38 25.80 14 9 -4 125.79 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6.20 8.70 -14 -8 -5 72.29 19.80 14 8 -5 107.69 19.50 14 -8 5 115.19 20.40 14 8 -5 106.59 14.10 14 8 5 100.99 24.70 14 8 5 92.39 19.50 -14 0 -6 223.88 30.10 14 0 6 259.27 25.90 14 0 6 252.57 29.30 14 0 -6 282.77 30.50 14 1 -6 268.67 29.10 -14 -1 -6 281.47 33.20 14 -1 6 242.88 28.00 14 -1 6 243.88 24.80 14 -1 -6 233.68 29.10 14 1 6 243.68 29.00 -14 1 -6 262.47 29.00 14 1 6 239.08 29.30 14 -2 6 60.09 11.70 14 2 -6 60.59 14.60 -14 -2 -6 44.90 15.50 14 -2 6 86.79 17.60 14 2 6 62.29 17.50 14 -2 -6 41.90 13.20 14 2 6 54.09 12.80 -14 2 -6 78.09 15.60 14 3 -6 158.68 19.40 14 -3 6 134.89 22.60 14 3 -6 147.19 19.70 14 3 6 150.88 27.50 14 3 6 117.49 19.10 14 -3 -6 154.88 28.20 14 4 -6 97.39 16.90 14 -4 6 105.69 19.50 14 4 -6 135.39 17.80 14 4 6 133.09 26.50 14 4 6 96.19 17.20 14 -4 -6 96.09 20.70 14 5 -6 404.86 36.10 14 5 -6 430.06 37.70 14 -5 6 390.16 37.70 14 5 6 432.06 46.00 14 5 6 359.96 38.50 14 6 -6 45.80 10.60 14 6 -6 23.00 10.70 14 -6 6 38.40 11.40 14 6 6 41.80 16.70 14 6 6 26.30 14.20 14 7 -6 36.60 9.10 14 -7 6 27.80 11.60 14 7 -6 42.60 12.20 14 7 6 42.90 17.90 14 7 6 37.70 13.30 14 8 -6 10.10 8.80 14 -8 6 5.00 8.10 -14 -8 -6 -6.20 13.60 14 8 6 11.10 11.70 14 8 6 19.00 14.00 14 0 7 3.90 7.30 14 0 -7 2.50 8.40 14 0 7 8.70 5.40 -14 0 -7 -5.00 11.40 14 -1 7 30.80 10.40 14 -1 7 57.89 11.70 14 1 -7 43.50 13.10 -14 -1 -7 28.70 16.10 14 -1 -7 25.40 10.90 -14 1 -7 22.50 11.10 14 1 7 44.30 11.00 14 1 7 36.00 12.30 14 -2 7 68.09 16.70 14 -2 7 85.09 13.20 14 2 -7 79.49 16.60 -14 -2 -7 41.50 22.10 14 2 7 53.39 12.60 -14 2 -7 63.99 15.80 14 -2 -7 53.49 14.80 14 2 7 52.69 15.50 14 3 -7 120.69 17.80 14 -3 7 101.29 19.10 14 3 -7 146.69 19.40 14 -3 7 130.09 16.20 14 3 7 116.29 23.90 14 -3 -7 120.79 22.40 14 3 7 108.59 19.10 14 4 -7 67.29 13.80 14 -4 7 68.49 15.30 14 4 -7 42.80 11.80 14 -4 -7 52.49 18.80 14 4 7 61.89 13.80 14 4 7 53.29 17.70 14 -5 7 244.48 26.80 14 5 -7 202.58 23.10 14 5 -7 206.98 25.10 14 5 7 239.78 28.10 14 5 7 312.67 36.80 14 -6 7 131.39 21.80 14 6 -7 144.69 16.10 14 6 -7 103.79 19.20 14 6 7 127.79 28.70 14 6 7 134.79 23.20 14 -7 7 39.30 11.30 14 7 -7 30.20 10.90 14 7 7 11.40 16.40 14 7 7 28.20 12.40 14 0 8 152.38 19.40 14 0 8 174.78 28.30 14 -1 8 168.98 18.90 14 -1 8 172.08 22.80 14 1 -8 125.19 23.20 14 1 8 182.68 29.80 14 1 8 177.18 20.40 -14 1 -8 110.69 22.70 14 -1 -8 149.69 26.80 14 2 -8 15.00 8.80 14 -2 8 19.90 7.80 14 -2 8 4.30 6.90 14 2 8 5.40 6.60 -14 2 -8 9.60 12.60 14 2 8 12.80 9.60 14 -2 -8 8.10 9.20 14 -3 8 62.69 15.40 14 3 -8 76.89 15.30 14 -3 8 64.69 12.20 14 3 -8 59.69 13.10 14 3 8 59.79 18.30 14 -3 -8 52.59 16.20 14 3 8 78.89 16.30 14 -4 8 53.49 14.00 14 4 -8 28.80 10.00 14 -4 8 55.19 10.80 14 4 -8 23.40 9.40 14 4 8 53.59 12.50 14 -4 -8 18.20 14.60 14 4 8 36.40 14.90 14 -5 8 213.58 25.50 14 5 -8 189.28 23.60 14 -5 8 198.38 21.70 14 5 -8 208.58 21.00 14 5 8 206.98 26.30 14 5 8 207.58 36.10 14 6 -8 17.20 8.20 14 -6 8 23.50 9.90 14 6 8 7.20 14.30 14 6 8 24.30 12.30 14 0 9 306.87 33.60 14 0 -9 364.86 37.50 14 0 9 304.27 36.60 14 -1 9 136.29 17.30 14 -1 9 131.89 23.50 14 1 -9 165.98 23.40 14 -1 -9 128.09 23.50 14 1 9 139.29 25.60 14 1 9 155.48 19.40 14 2 -9 57.29 14.60 14 -2 9 54.59 10.70 14 -2 9 45.10 14.10 14 -2 -9 46.50 17.70 14 2 9 48.50 16.00 14 2 9 61.09 14.50 14 -3 9 12.40 6.10 14 3 -9 12.40 7.60 14 -3 9 7.60 8.30 14 3 -9 -6.00 6.20 14 3 9 20.40 9.00 14 3 9 4.40 15.10 14 -3 -9 14.80 12.70 14 4 -9 61.69 13.40 14 -4 9 68.69 16.60 14 4 -9 89.09 14.30 14 -4 9 51.29 16.80 14 4 9 63.99 14.60 14 -4 -9 92.09 23.60 14 4 9 73.69 21.70 14 5 -9 55.79 12.50 14 -5 9 41.50 9.60 14 -5 9 46.40 12.00 14 5 -9 59.89 9.70 14 5 9 67.69 16.30 14 5 9 32.70 16.90 14 0 10 83.29 20.20 14 0 -10 132.09 23.90 14 1 -10 138.49 25.50 14 -1 10 166.38 27.80 14 -1 10 212.08 20.90 14 -1 -10 177.18 30.10 14 1 10 142.29 27.80 14 1 10 193.58 22.50 14 -2 10 10.50 6.40 14 -2 10 24.20 11.30 14 2 -10 11.90 9.70 14 2 -10 -0.20 7.60 14 -2 -10 1.10 9.60 14 2 10 5.10 12.80 14 2 10 11.40 7.90 14 3 -10 69.79 13.40 14 -3 10 31.60 8.50 14 -3 10 50.49 14.50 14 3 -10 44.60 12.70 14 3 10 26.80 14.00 14 -3 -10 37.70 16.60 14 3 10 43.40 11.80 14 4 -10 -6.30 5.50 14 -4 10 -1.00 5.50 14 -4 10 -11.80 8.70 14 4 -10 5.50 8.10 14 -4 -10 -0.30 13.70 14 4 10 -7.80 10.30 14 4 10 -8.30 7.90 14 0 11 222.88 26.20 14 0 -11 216.38 29.90 14 0 11 246.58 32.60 14 -1 11 75.29 19.90 14 1 -11 124.89 21.20 14 -1 11 80.39 13.50 14 -1 -11 82.89 21.20 14 1 11 78.49 21.90 14 1 11 70.49 14.70 14 -2 11 25.10 11.80 14 2 -11 32.30 12.10 14 -2 11 12.50 7.00 14 2 11 31.20 15.90 14 2 11 24.30 9.90 14 -2 -11 15.90 12.10 15 0 0 7.10 6.40 -15 0 0 -5.50 7.90 15 1 0 9.70 8.10 -15 -1 0 8.00 11.60 15 -1 0 18.50 8.30 15 -2 0 175.38 22.00 15 2 0 134.09 18.40 15 3 0 27.10 10.40 15 3 0 46.90 11.50 15 -3 0 42.10 11.30 15 -4 0 1295.47 98.29 15 4 0 1300.07 98.09 15 4 0 1220.88 95.39 15 -5 0 95.69 19.00 15 5 0 80.99 15.70 15 5 0 64.39 15.40 15 6 0 83.39 16.30 15 6 0 50.19 14.10 15 -6 0 45.90 14.40 15 7 0 29.00 11.20 15 -7 0 26.50 11.80 15 7 0 42.70 14.20 15 8 0 8.20 8.40 15 8 0 7.30 10.40 15 -8 0 9.80 9.50 15 -9 0 1.70 11.60 15 9 0 4.00 10.10 15 9 0 -4.80 11.00 15 0 1 10.20 8.40 15 0 -1 -0.40 5.50 -15 0 -1 7.60 8.60 -15 -1 -1 556.04 50.29 15 -1 1 559.74 49.00 15 1 -1 576.44 49.10 15 1 1 478.45 47.40 15 1 1 564.04 46.40 15 -1 -1 590.04 49.60 15 2 -1 223.48 24.10 15 -2 1 174.98 24.20 15 2 -1 227.28 25.60 15 2 1 190.48 22.80 15 -2 -1 254.37 27.00 15 2 1 204.58 25.60 15 -3 1 285.87 30.90 15 3 -1 308.87 29.90 15 3 -1 295.57 31.30 15 3 1 261.17 28.90 15 3 1 278.27 31.30 15 -3 -1 311.37 32.30 15 4 -1 130.29 20.20 15 -4 1 139.99 20.10 15 4 -1 127.49 21.60 15 4 1 141.09 18.50 15 -4 -1 92.69 19.80 15 4 1 148.99 21.20 15 5 -1 21.90 10.60 15 5 -1 7.50 7.70 15 -5 1 18.30 9.50 15 5 1 11.40 7.80 15 -5 -1 6.80 7.90 15 5 1 11.70 7.80 15 6 -1 61.19 14.90 15 -6 1 58.89 14.40 15 6 -1 34.10 12.40 15 6 1 75.49 15.50 15 -6 -1 45.20 14.20 15 7 -1 145.29 22.60 15 7 -1 169.78 23.30 15 -7 1 128.49 23.50 15 -7 -1 168.58 29.10 15 7 1 109.79 21.40 15 7 1 112.99 22.50 15 8 -1 24.20 12.20 15 -8 1 23.60 12.80 15 8 -1 24.10 11.00 15 -8 -1 32.20 15.70 15 8 1 35.20 16.00 15 8 1 23.70 11.00 15 -9 1 36.90 14.00 15 9 -1 64.59 17.20 15 9 -1 48.30 15.70 15 -9 -1 42.50 18.40 15 9 1 54.99 16.50 15 9 1 47.40 16.20 15 0 -2 -0.50 5.30 -15 0 -2 4.60 8.50 15 0 2 2.60 4.60 -15 -1 -2 82.39 22.70 15 1 -2 64.19 14.30 15 -1 2 69.99 16.60 15 1 2 34.70 11.40 -15 1 -2 96.29 17.80 15 -1 -2 82.69 16.40 15 1 2 60.19 12.40 15 -2 2 301.67 31.60 15 2 -2 324.47 30.70 15 2 -2 296.97 32.00 15 -2 -2 370.76 35.30 15 2 2 313.57 30.40 15 2 2 277.77 32.10 15 -3 2 614.44 56.59 15 3 -2 708.63 55.99 15 3 -2 755.82 58.79 15 -3 -2 721.93 59.79 15 3 2 632.64 54.89 15 3 2 659.03 58.29 15 4 -2 317.27 31.60 15 4 -2 303.17 29.70 15 -4 2 260.67 30.10 15 4 2 246.38 28.60 15 -4 -2 291.37 32.40 15 4 2 268.37 31.30 15 -5 2 189.38 24.80 15 5 -2 206.28 24.80 15 5 -2 183.68 24.60 15 5 2 225.48 28.50 15 5 2 211.18 25.30 15 -5 -2 212.28 28.10 15 6 -2 11.70 8.30 15 -6 2 1.80 7.80 15 6 -2 5.00 6.00 15 6 2 10.40 8.70 15 -6 -2 5.00 8.90 15 6 2 18.60 9.40 15 7 -2 643.54 52.19 15 7 -2 516.35 49.80 15 -7 2 544.15 51.19 15 -7 -2 573.74 55.79 15 7 2 489.35 52.59 15 7 2 614.34 57.99 15 8 -2 429.56 44.10 15 8 -2 426.06 43.40 15 -8 2 436.06 45.50 15 8 2 540.95 51.09 15 8 2 472.45 45.60 15 9 -2 144.89 24.30 15 -9 2 156.78 26.80 15 9 -2 142.99 24.20 15 9 2 141.99 25.80 15 9 2 164.88 29.90 -15 0 -3 0.70 7.50 15 0 -3 -1.10 4.90 15 0 3 -3.00 4.80 -15 -1 -3 118.19 20.50 15 -1 3 83.29 16.10 15 1 -3 94.29 18.80 -15 1 -3 129.69 20.70 15 -1 -3 79.69 17.10 15 1 3 106.59 16.20 15 1 3 106.09 19.40 15 -2 3 105.09 18.50 15 2 -3 108.89 19.20 15 2 3 125.09 19.00 15 -2 -3 100.59 20.70 15 2 3 120.89 21.90 15 3 -3 257.77 28.10 15 -3 3 274.67 29.50 15 3 -3 275.97 29.60 15 3 3 249.18 30.80 15 3 3 290.97 28.90 15 -3 -3 292.97 32.30 15 4 -3 132.89 22.70 15 -4 3 104.79 19.10 15 4 -3 156.18 19.70 15 4 3 132.49 20.80 15 4 3 158.78 26.10 15 -4 -3 114.49 23.70 15 5 -3 35.10 11.10 15 -5 3 33.90 12.30 15 5 -3 42.70 11.60 15 5 3 28.20 12.20 15 -5 -3 21.30 11.30 15 5 3 28.50 10.50 15 6 -3 326.37 31.50 15 -6 3 233.58 29.70 15 6 -3 258.87 29.50 15 -6 -3 314.97 36.40 15 6 3 248.98 29.80 15 6 3 276.87 34.60 15 -7 3 41.50 14.00 15 7 -3 23.50 12.80 15 7 -3 22.90 9.20 15 7 3 35.30 13.40 15 7 3 42.60 15.40 15 8 -3 124.59 20.70 15 -8 3 118.69 22.90 15 8 -3 169.98 25.00 15 8 3 126.79 27.50 15 8 3 101.29 21.90 15 0 4 -1.60 6.50 15 0 4 5.40 7.50 15 0 -4 -0.60 5.70 -15 0 -4 -23.50 10.10 15 -1 4 40.20 12.90 15 1 -4 46.70 13.60 -15 -1 -4 45.50 14.10 -15 1 -4 32.60 12.70 15 -1 -4 14.70 8.60 15 1 4 21.30 9.50 15 1 4 52.09 12.00 15 2 -4 255.37 28.30 15 -2 4 252.27 28.30 15 -2 -4 249.58 29.70 15 2 4 276.87 30.70 15 2 4 232.38 26.20 15 3 -4 231.78 26.00 15 3 -4 257.47 28.00 15 -3 4 262.37 27.90 15 -3 -4 284.07 31.50 15 3 4 232.18 29.50 15 3 4 194.58 24.90 15 4 -4 307.37 29.80 15 4 -4 260.07 29.30 15 -4 4 258.87 29.50 15 4 4 241.58 29.00 15 4 4 297.87 33.50 15 -4 -4 278.57 33.30 15 5 -4 228.58 26.50 15 -5 4 228.78 27.20 15 5 -4 230.38 26.40 15 5 4 238.78 27.80 15 -5 -4 255.67 32.70 15 6 -4 50.99 13.00 15 -6 4 87.49 17.20 15 6 -4 73.99 15.10 15 6 4 62.69 19.00 15 6 4 82.49 16.00 15 7 -4 77.49 15.40 15 7 -4 47.10 13.20 15 -7 4 44.70 12.80 15 7 4 64.99 20.20 15 7 4 61.19 15.30 15 -8 4 184.18 25.10 15 8 -4 183.58 27.10 15 8 -4 166.98 22.00 15 8 4 186.58 33.40 15 8 4 172.18 26.70 15 0 5 4.20 6.40 15 0 5 -1.60 6.70 15 0 -5 11.90 9.10 -15 0 -5 5.20 11.10 15 -1 5 19.80 9.10 15 -1 5 18.00 8.50 15 1 -5 9.80 8.60 -15 -1 -5 -1.40 12.90 15 1 5 7.40 6.20 15 1 5 10.40 8.20 -15 1 -5 7.30 9.70 15 -1 -5 14.00 9.10 15 2 -5 12.40 8.60 15 -2 5 0.00 5.60 15 -2 -5 14.00 8.20 15 2 5 -0.90 6.90 15 2 5 7.30 5.50 15 -3 5 773.92 65.59 15 3 -5 835.22 65.89 15 3 -5 784.22 63.79 15 3 5 777.92 68.89 15 -3 -5 866.21 70.39 15 3 5 781.72 64.39 15 -4 5 87.29 18.00 15 4 -5 109.69 18.20 15 4 -5 105.79 17.40 15 4 5 79.09 16.50 15 4 5 56.69 16.80 15 -4 -5 74.39 16.90 15 -5 5 186.18 25.00 15 5 -5 202.68 24.20 15 5 -5 227.88 25.00 15 5 5 245.68 32.40 15 5 5 241.28 27.20 15 6 -5 165.88 22.40 15 6 -5 202.88 23.10 15 -6 5 196.08 24.00 15 6 5 144.69 26.30 15 6 5 119.09 33.50 15 7 -5 56.19 13.10 15 7 -5 43.30 12.60 15 -7 5 51.69 14.80 15 7 5 42.30 14.80 15 7 5 59.49 21.30 15 -8 5 26.70 11.40 15 8 -5 17.60 11.00 15 8 -5 19.50 8.70 15 8 5 31.60 14.30 15 8 5 29.40 19.00 -15 0 -6 -6.30 11.70 15 0 -6 -2.50 5.90 15 0 6 3.10 5.00 15 0 6 3.10 7.10 15 -1 6 222.88 26.30 15 -1 6 198.38 31.50 15 1 -6 194.28 24.90 -15 -1 -6 198.28 31.20 15 -1 -6 181.48 26.50 15 1 6 228.18 23.50 15 1 6 216.78 27.60 -15 1 -6 182.98 25.80 15 2 -6 337.97 35.10 15 -2 6 341.07 35.40 15 -2 6 345.27 31.80 15 2 6 322.87 37.20 15 -2 -6 321.47 37.00 15 2 6 374.46 33.90 -15 2 -6 352.76 35.80 15 -3 6 540.75 48.80 15 3 -6 510.15 47.60 15 3 -6 515.65 46.40 15 -3 -6 731.13 72.39 15 3 6 550.94 47.80 15 3 6 557.74 53.19 15 4 -6 122.19 19.30 15 4 -6 105.99 17.70 15 -4 6 87.69 17.70 15 -4 -6 140.09 28.00 15 4 6 85.19 16.90 15 4 6 100.29 24.70 15 -5 6 15.30 9.60 15 5 -6 30.90 10.10 15 5 -6 38.40 10.20 15 -5 -6 37.50 16.50 15 5 6 26.50 10.80 15 5 6 21.70 11.60 15 6 -6 59.19 13.30 15 6 -6 62.19 13.80 15 6 6 62.09 15.70 15 6 6 51.09 17.20 15 7 -6 52.89 11.10 15 -7 6 34.30 10.60 15 7 -6 42.40 14.20 15 7 6 44.20 18.80 15 7 6 43.40 14.50 15 0 7 1.20 5.40 15 0 -7 2.00 5.70 15 0 7 -4.10 6.60 15 -1 7 78.69 17.20 15 1 -7 120.59 21.40 15 1 7 125.99 23.80 -15 1 -7 88.49 19.70 15 1 7 101.39 16.50 15 -1 -7 96.19 23.50 15 -2 7 102.29 20.70 15 -2 7 105.29 15.70 15 2 -7 86.39 18.20 15 2 7 89.99 20.60 15 -2 -7 71.09 17.90 15 2 7 96.39 16.60 -15 2 -7 135.49 21.50 15 3 -7 32.90 12.00 15 -3 7 55.19 14.50 15 3 -7 46.20 11.30 15 -3 7 41.00 10.20 15 3 7 26.70 12.90 15 -3 -7 29.60 13.40 15 3 7 46.40 12.00 15 4 -7 11.70 7.60 15 -4 7 5.00 8.00 15 4 -7 6.60 6.00 15 -4 -7 12.00 9.60 15 4 7 7.20 8.70 15 4 7 2.70 9.00 15 -5 7 53.89 17.10 15 5 -7 58.39 14.10 15 5 -7 58.39 13.20 15 -5 -7 46.80 17.10 15 5 7 49.00 15.90 15 5 7 42.30 16.50 15 6 -7 10.40 6.40 15 6 -7 3.50 7.20 15 -6 7 3.80 8.50 15 6 7 6.20 12.30 15 6 7 -2.40 8.20 15 7 -7 66.09 16.20 15 -7 7 141.99 22.80 15 7 7 120.59 23.20 15 7 7 87.89 25.20 15 0 8 4.70 6.10 15 0 -8 -2.10 7.40 15 0 8 1.50 8.10 15 -1 8 61.09 15.30 15 1 -8 59.09 15.70 15 -1 8 91.29 23.00 15 1 8 72.19 13.90 15 1 8 77.79 19.00 15 -1 -8 58.89 17.50 15 -2 8 198.88 22.40 15 -2 8 173.38 24.60 15 2 -8 205.78 25.50 15 2 8 195.98 24.20 15 2 8 207.68 30.20 15 -2 -8 222.78 30.20 15 3 -8 15.50 7.50 15 -3 8 0.20 7.20 15 -3 8 -1.70 4.70 15 3 8 3.50 7.90 15 -3 -8 3.50 10.50 15 4 -8 46.50 11.90 15 -4 8 35.70 10.00 15 4 -8 43.40 11.60 15 -4 8 55.69 14.00 15 -4 -8 38.00 15.80 15 4 8 43.30 12.20 15 4 8 48.00 18.30 15 5 -8 4.30 6.30 15 -5 8 -1.90 5.90 15 5 -8 11.20 9.60 15 5 8 1.90 8.70 15 5 8 0.80 8.90 15 -5 -8 -6.60 11.20 15 6 -8 34.90 7.60 15 6 -8 29.20 10.90 15 -6 8 33.60 13.40 15 6 8 26.00 12.00 15 6 8 40.70 18.00 15 0 9 -0.30 9.60 15 0 9 4.80 6.20 15 0 -9 -3.30 7.10 15 1 -9 4.50 9.60 15 -1 9 20.60 11.60 15 -1 -9 12.00 11.20 15 1 9 11.90 10.80 15 1 9 -1.10 7.00 15 -2 9 84.19 18.70 15 -2 9 92.09 14.40 15 2 -9 85.89 16.20 15 2 -9 92.19 18.80 15 2 9 70.89 19.40 15 -2 -9 76.19 20.70 15 2 9 102.69 17.40 15 -3 9 163.88 18.70 15 3 -9 160.28 22.00 15 3 -9 180.98 22.20 15 -3 9 157.88 22.80 15 3 9 181.68 23.00 15 -3 -9 173.28 29.80 15 3 9 102.79 24.20 15 4 -9 20.20 9.40 15 -4 9 16.20 9.40 15 -4 9 17.60 7.60 15 4 9 10.30 14.90 15 -4 -9 31.70 16.10 15 4 9 17.00 10.60 15 5 -9 70.09 15.70 15 5 -9 95.79 13.00 15 -5 9 79.89 13.50 15 5 9 75.79 23.00 15 5 9 63.69 16.40 15 -5 -9 91.69 25.10 15 0 10 9.40 10.50 15 0 -10 -3.40 7.80 15 0 10 3.70 7.60 15 -1 10 110.99 19.10 15 1 -10 124.29 21.90 15 -1 10 67.39 18.70 15 1 10 74.99 15.20 15 -1 -10 80.19 19.60 15 1 10 82.79 20.00 15 -2 10 233.78 25.80 15 2 -10 257.97 29.10 15 -2 10 329.27 34.80 15 2 -10 264.07 30.30 15 -2 -10 317.17 37.10 15 2 10 280.47 37.70 15 2 10 265.07 29.90 15 -3 10 302.37 29.60 15 3 -10 305.97 32.50 15 -3 10 395.26 38.90 15 3 -10 338.37 33.30 15 -3 -10 321.77 41.70 15 3 10 377.16 44.60 15 3 10 384.16 36.40 16 0 0 868.41 70.89 16 -1 0 780.52 65.19 16 -2 0 27.50 12.30 16 2 0 42.70 11.50 16 2 0 49.80 14.70 16 3 0 25.60 10.70 16 3 0 17.10 8.50 16 -3 0 18.80 11.40 16 -4 0 51.69 13.70 16 4 0 46.60 12.70 16 4 0 33.50 10.80 16 -5 0 235.08 29.10 16 5 0 253.87 29.90 16 5 0 198.98 25.50 16 6 0 29.50 12.50 16 -6 0 33.50 13.50 16 6 0 41.70 10.80 16 -7 0 405.16 43.60 16 7 0 379.46 40.10 16 7 0 428.56 43.30 16 8 0 2.10 9.00 16 -8 0 -9.10 8.10 16 8 0 5.60 10.30 16 0 1 514.45 47.60 16 0 -1 533.75 48.10 -16 0 -1 530.75 48.80 16 -1 1 296.67 32.50 16 1 -1 291.97 32.50 16 1 1 330.17 31.10 16 1 1 336.97 34.00 16 2 -1 70.59 13.90 16 -2 1 64.09 14.40 16 2 -1 53.99 15.00 16 2 1 59.29 13.60 16 -2 -1 38.70 12.50 16 2 1 78.79 14.00 16 -3 1 144.69 21.20 16 3 -1 142.19 21.50 16 3 -1 168.38 22.40 16 -3 -1 94.99 19.10 16 3 1 148.09 19.40 16 3 1 177.78 23.20 16 -4 1 396.06 37.20 16 4 -1 300.87 32.50 16 4 -1 298.07 34.50 16 4 1 345.57 33.30 16 4 1 400.26 37.90 16 -4 -1 270.67 34.10 16 -5 1 21.90 10.80 16 5 -1 35.40 12.00 16 5 -1 28.40 11.60 16 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183.18 30.00 18 -3 2 143.49 24.70 18 3 -2 118.89 19.80 18 3 2 86.09 19.50 18 3 2 90.69 17.10 18 -3 -2 71.39 17.70 18 4 -2 418.46 43.20 18 4 -2 450.15 42.10 18 -4 2 475.15 44.70 18 -4 -2 418.46 45.20 18 4 2 421.66 41.30 18 4 2 389.26 44.00 18 -5 2 114.09 23.10 18 5 -2 96.69 17.30 18 5 -2 77.59 19.00 18 -5 -2 72.39 19.30 18 5 2 95.79 21.10 18 5 2 101.59 23.80 18 6 -2 308.47 33.50 18 -6 2 333.17 37.00 18 6 -2 342.17 36.70 18 6 2 311.47 38.10 18 -6 -2 250.87 36.60 18 6 2 291.37 34.20 18 -7 2 -3.30 8.80 18 7 -2 13.10 9.80 18 7 -2 2.60 8.50 18 7 2 3.90 11.70 18 -7 -2 -1.10 9.50 18 7 2 -2.10 8.80 18 0 3 484.65 44.40 18 0 3 493.85 48.10 18 0 -3 512.95 48.30 18 -1 3 102.19 19.10 18 1 -3 157.68 26.40 -18 1 -3 117.69 27.30 18 1 3 175.88 24.30 18 1 3 147.19 21.20 18 -1 -3 89.29 20.10 18 2 -3 54.59 18.80 18 2 -3 40.80 12.40 18 -2 3 49.90 16.10 18 2 3 36.40 13.80 18 -2 -3 46.30 16.20 18 2 3 47.10 12.30 18 -3 3 42.30 12.70 18 3 -3 51.69 16.40 18 3 -3 51.69 13.90 18 -3 -3 62.69 19.10 18 3 3 39.70 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8 82.19 19.80 19 2 -8 92.39 18.00 19 2 8 126.89 28.40 19 -2 -8 80.69 24.50 19 2 8 84.29 17.80 20 0 0 5.90 11.30 20 1 0 449.86 43.70 20 1 0 475.15 48.00 20 -1 0 474.75 50.19 20 -2 0 5.30 9.80 20 2 0 -3.50 8.50 20 2 0 0.60 7.80 20 3 0 -1.50 7.60 20 -3 0 -1.90 8.90 20 4 0 65.89 16.60 20 -4 0 84.49 27.10 20 4 0 87.39 21.80 20 -5 0 81.99 23.60 20 5 0 73.59 18.40 20 5 0 78.89 19.90 20 6 0 51.19 18.30 20 6 0 34.40 13.60 20 -6 0 38.70 16.50 20 0 1 268.17 36.20 20 0 -1 195.98 29.40 20 1 -1 39.70 14.60 20 -1 1 39.10 15.50 20 1 1 79.89 20.40 20 -1 -1 66.29 18.80 20 1 1 32.10 11.80 20 -2 1 65.29 16.30 20 2 -1 83.99 20.60 20 2 -1 50.79 13.50 20 -2 -1 62.79 19.60 20 2 1 89.99 20.70 20 2 1 82.69 16.00 20 3 -1 141.99 26.10 20 -3 1 113.79 22.80 20 3 1 164.58 29.20 20 -3 -1 91.59 21.70 20 3 1 159.08 28.60 20 4 -1 256.37 33.00 20 4 -1 229.88 28.90 20 -4 1 239.48 32.70 20 -4 -1 271.67 35.20 20 4 1 289.87 34.90 20 4 1 215.98 28.10 20 5 -1 173.58 26.90 20 -5 1 182.08 32.70 20 5 -1 228.18 30.70 20 5 1 227.18 35.90 20 5 1 176.28 27.20 20 -5 -1 166.18 28.90 20 6 -1 76.69 20.50 20 6 -1 76.59 17.80 20 6 1 104.79 24.90 20 6 1 71.69 18.00 20 -6 -1 87.49 20.90 20 0 2 69.99 16.40 20 0 2 66.09 19.00 20 0 -2 92.79 22.50 20 1 -2 20.20 12.70 20 -1 2 38.20 14.90 20 -1 -2 21.20 13.50 20 1 2 19.00 14.00 20 1 2 37.90 12.40 20 2 -2 101.19 21.50 20 2 -2 96.39 18.70 20 -2 2 129.69 24.40 20 2 2 91.19 20.40 20 2 2 100.69 18.20 20 -2 -2 108.99 25.00 20 3 -2 27.10 13.10 20 3 -2 20.90 13.10 20 -3 2 22.10 11.10 20 3 2 41.60 15.90 20 -3 -2 35.80 13.00 20 3 2 26.90 11.70 20 -4 2 1.30 10.30 20 4 -2 16.90 12.00 20 4 -2 17.10 10.00 20 -4 -2 30.90 15.50 20 4 2 1.30 11.90 20 4 2 14.80 9.10 20 5 -2 73.49 16.30 20 5 -2 73.19 19.80 20 -5 2 77.39 20.10 20 5 2 72.39 19.90 20 5 2 64.19 18.10 20 -5 -2 69.89 22.10 20 -6 2 16.00 11.10 20 6 -2 -2.90 10.00 20 6 -2 11.50 11.40 20 -6 -2 4.50 13.70 20 6 2 12.60 10.10 20 6 2 24.90 14.90 20 0 -3 73.89 19.60 20 0 3 92.29 21.30 20 0 3 81.59 17.00 20 1 -3 53.29 16.70 20 -1 3 35.50 14.90 20 1 3 27.50 11.20 20 -1 -3 60.79 18.80 20 1 3 27.00 12.80 20 -2 3 40.30 14.80 20 2 -3 59.39 18.20 20 2 -3 26.30 12.00 20 -2 -3 58.59 20.60 20 2 3 38.20 12.50 20 2 3 28.50 14.20 20 3 -3 40.00 12.70 20 3 -3 51.59 18.50 20 -3 3 55.49 17.20 20 3 3 40.60 15.70 20 -3 -3 83.79 23.10 20 3 3 44.80 14.20 20 4 -3 40.80 15.70 20 -4 3 38.50 16.00 20 4 -3 47.00 13.60 20 4 3 60.79 19.40 20 4 3 32.00 13.00 20 -4 -3 44.60 17.90 20 -5 3 361.36 39.30 20 5 -3 309.77 37.60 20 5 -3 277.97 34.30 20 5 3 402.36 43.40 20 -5 -3 297.67 40.60 20 5 3 317.97 36.70 20 -6 3 84.39 21.20 20 6 -3 162.18 27.70 20 6 -3 143.19 24.10 20 6 3 117.89 25.80 20 -6 -3 131.49 26.70 20 6 3 125.99 23.40 20 0 4 119.69 19.50 20 0 -4 126.89 26.30 20 0 4 88.19 19.60 20 1 -4 492.25 49.70 20 -1 4 472.45 44.90 20 -1 4 478.85 49.50 20 -1 -4 517.95 51.29 20 1 4 465.75 49.50 20 1 4 478.45 44.90 20 2 -4 170.08 29.80 20 2 -4 151.38 36.10 20 -2 4 174.48 29.40 20 2 4 181.28 40.20 20 2 4 198.08 33.10 20 -2 -4 180.28 32.00 20 3 -4 10.60 9.20 20 3 -4 10.10 10.10 20 -3 4 -0.20 8.10 20 3 4 -8.20 8.20 20 3 4 13.60 10.10 20 -3 -4 -3.10 8.60 20 4 -4 129.59 25.20 20 4 -4 81.29 18.60 20 -4 4 120.19 23.50 20 -4 -4 185.28 33.20 20 4 4 136.69 22.90 20 4 4 113.49 24.40 20 -5 4 225.38 30.60 20 5 -4 192.98 31.30 20 5 -4 226.08 28.00 20 5 4 189.08 28.20 20 -5 -4 175.48 32.60 20 5 4 192.08 32.50 20 0 -5 771.22 70.99 20 0 5 801.92 65.79 20 1 -5 434.06 45.20 20 -1 5 419.46 40.10 20 -1 5 402.16 44.00 20 1 5 415.46 40.50 20 1 5 399.46 44.70 20 -1 -5 368.26 44.70 20 -2 5 80.09 18.80 20 2 -5 85.29 21.60 20 2 -5 76.59 17.50 20 -2 5 78.39 15.90 20 2 5 90.69 22.40 20 2 5 76.89 16.70 20 -2 -5 65.69 19.40 20 3 -5 98.49 21.40 20 3 -5 72.89 15.50 20 -3 5 60.69 17.40 20 3 5 67.89 21.30 20 -3 -5 64.89 19.50 20 3 5 50.69 14.50 20 4 -5 31.70 15.30 20 -4 5 19.10 12.20 20 4 -5 41.50 12.40 20 4 5 27.50 13.30 20 4 5 31.40 11.60 20 -4 -5 44.50 17.30 20 5 -5 171.58 27.70 20 -5 5 134.19 25.80 20 5 -5 108.69 20.70 20 5 5 156.08 25.90 20 5 5 128.39 26.80 20 -5 -5 190.58 36.10 20 0 6 220.68 31.90 20 0 6 217.58 27.70 20 1 -6 109.09 23.80 20 -1 6 101.69 18.30 20 -1 6 90.79 21.60 20 1 6 75.89 19.50 20 -1 -6 69.39 19.00 20 -2 6 40.50 12.90 20 2 -6 36.40 12.60 20 -2 6 42.40 13.90 20 2 -6 26.00 13.70 20 2 6 33.90 16.00 20 -2 -6 36.00 15.00 20 2 6 44.60 14.70 20 -3 6 90.09 21.80 20 3 -6 94.99 21.40 20 3 -6 76.59 16.90 20 -3 6 112.99 19.70 20 -3 -6 107.29 27.00 20 3 6 102.49 25.00 20 3 6 110.69 21.40 20 -4 6 90.39 19.90 20 4 -6 82.69 18.00 20 4 -6 106.39 21.70 20 4 6 60.99 21.30 20 4 6 88.49 19.40 20 -4 -6 64.39 21.90 20 0 7 54.29 16.90 20 0 -7 78.39 19.60 20 0 7 65.39 17.90 20 -1 7 85.19 28.30 20 -1 7 144.29 22.20 20 1 -7 146.59 28.80 20 -1 -7 115.79 25.90 20 1 7 106.69 25.00 20 1 7 129.19 22.20 20 2 -7 1.40 11.50 20 -2 7 21.40 11.70 20 2 -7 12.80 11.80 20 -2 7 14.90 9.30 20 2 7 10.70 12.50 20 -2 -7 19.60 13.40 20 2 7 14.60 11.80 21 0 0 2.00 9.60 21 1 0 118.99 21.10 21 -1 0 157.38 29.30 21 1 0 110.49 22.50 21 -2 0 63.59 16.80 21 2 0 95.69 24.00 21 2 0 61.89 14.80 21 -3 0 178.08 32.20 21 3 0 174.48 27.60 21 3 0 204.48 33.90 21 4 0 77.89 17.60 21 -4 0 82.19 22.20 21 4 0 87.69 21.90 21 5 0 22.30 14.00 21 5 0 16.10 11.00 21 -5 0 23.90 15.10 21 0 1 1.20 10.10 21 0 -1 2.20 8.30 21 1 -1 263.57 35.50 21 -1 1 363.56 39.10 21 1 -1 265.67 33.20 21 -1 -1 318.17 38.00 21 1 1 286.87 36.60 21 1 1 315.47 34.20 21 -2 1 -5.40 8.20 21 2 -1 -6.60 7.80 21 2 -1 -1.00 8.00 21 2 1 -5.60 7.90 21 -2 -1 -5.10 9.10 21 2 1 10.70 7.80 21 3 -1 181.28 31.30 21 -3 1 130.79 27.10 21 3 -1 133.19 23.20 21 3 1 168.08 26.60 21 -3 -1 109.59 22.80 21 3 1 193.58 32.20 21 4 -1 8.80 10.10 21 4 -1 20.30 13.10 21 -4 1 27.80 15.10 21 -4 -1 16.90 14.00 21 4 1 30.60 11.20 21 4 1 17.80 12.70 21 5 -1 12.10 10.70 21 5 -1 -3.70 8.20 21 -5 1 -6.60 8.20 21 5 1 12.30 10.30 21 5 1 0.10 9.70 21 -5 -1 4.40 9.70 21 0 2 -2.20 8.60 21 0 2 -18.70 11.40 21 0 -2 11.10 9.60 21 -1 2 14.10 11.50 21 1 -2 10.40 11.10 21 1 2 9.80 9.80 21 1 2 -1.90 7.40 21 -1 -2 15.00 9.40 21 2 -2 27.10 9.70 21 2 -2 20.20 12.70 21 -2 2 30.40 15.40 21 2 2 10.30 10.20 21 2 2 25.40 11.40 21 -2 -2 22.10 12.30 21 3 -2 10.20 9.50 21 3 -2 18.40 13.00 21 3 2 15.40 9.80 21 3 2 5.20 11.40 21 -3 -2 7.50 12.00 21 4 -2 195.88 30.80 21 4 -2 254.07 33.40 21 -4 2 166.38 37.00 21 -4 -2 263.27 35.10 21 4 2 242.98 38.30 21 4 2 220.98 28.40 21 -5 2 49.70 18.40 21 5 -2 43.40 12.70 21 5 -2 56.29 16.90 21 5 2 42.60 15.00 21 -5 -2 25.70 14.10 21 5 2 54.89 20.10 21 0 3 -0.80 9.70 21 0 3 -10.10 8.40 21 0 -3 2.00 9.60 21 -1 3 83.19 22.30 21 1 -3 96.99 23.00 21 1 3 78.49 20.90 21 1 3 81.09 18.30 21 -1 -3 51.59 16.80 21 2 -3 3.00 9.20 21 2 -3 -4.80 7.80 21 -2 -3 0.60 11.70 21 2 3 5.70 11.90 21 2 3 -0.20 7.50 21 3 -3 313.27 34.00 21 -3 3 246.48 35.70 21 3 -3 295.77 36.30 21 3 3 251.87 35.50 21 3 3 238.48 31.20 21 -3 -3 304.77 38.80 21 4 -3 47.00 17.20 21 -4 3 53.29 19.20 21 4 -3 35.40 12.60 21 4 3 29.80 16.30 21 -4 -3 22.00 12.90 21 4 3 33.40 13.20 21 5 -3 46.70 14.80 21 5 -3 66.89 19.60 21 -5 -3 31.80 18.60 21 5 3 36.10 14.40 21 5 3 21.90 11.20 21 0 4 -1.60 10.10 21 0 -4 1.30 9.30 21 0 4 -3.80 8.20 21 -1 4 134.09 24.70 21 -1 4 172.98 36.60 21 1 -4 146.99 28.40 21 -1 -4 138.69 25.90 21 1 4 151.38 23.10 21 1 4 143.89 26.80 21 2 -4 391.66 43.50 21 2 -4 355.06 39.10 21 -2 -4 373.26 44.70 21 2 4 405.76 39.70 21 2 4 387.16 44.20 21 3 -4 109.09 20.30 21 3 -4 139.19 28.20 21 -3 4 78.89 20.60 21 3 4 119.19 21.30 21 3 4 129.29 27.90 21 -3 -4 130.79 28.50 21 -4 4 125.59 24.90 21 4 -4 166.18 28.10 21 4 -4 141.69 24.10 21 -4 -4 107.89 25.50 21 4 4 173.48 31.90 21 4 4 135.79 24.20 21 0 -5 -0.10 10.20 21 0 5 -7.80 9.30 21 0 5 7.20 8.30 21 1 -5 4.90 9.80 21 -1 5 11.40 10.10 21 -1 5 16.10 8.90 21 -1 -5 16.80 13.00 21 1 5 4.50 7.40 21 1 5 3.40 10.10 21 -2 5 20.10 10.40 21 2 -5 10.60 11.00 21 2 -5 -6.00 9.70 21 2 5 -6.00 8.40 21 -2 -5 4.50 10.40 21 2 5 -4.90 7.90 21 3 -5 118.19 25.50 21 3 -5 109.19 21.60 21 -3 5 131.79 25.30 21 -3 -5 131.59 30.80 21 3 5 141.89 23.10 21 3 5 153.58 30.10 21 4 -5 46.10 16.00 21 4 -5 67.29 18.60 21 -4 5 45.50 17.20 21 -4 -5 43.60 18.20 21 4 5 43.10 16.20 21 4 5 86.89 23.40 21 0 -6 -1.20 11.80 21 0 6 -0.10 8.60 21 0 6 -4.30 8.80 21 -1 6 -6.60 7.90 21 1 -6 -3.80 8.30 21 -1 6 7.60 10.30 21 -1 -6 9.70 12.90 21 1 6 10.80 9.50 21 1 6 1.30 9.80 21 2 -6 8.70 12.20 21 2 -6 7.60 11.70 21 -2 6 23.40 11.60 21 -2 6 0.00 10.00 21 -2 -6 6.30 11.00 21 2 6 3.50 10.80 21 2 6 8.70 9.80 22 0 0 380.26 43.90 22 1 0 -1.60 8.30 22 1 0 13.50 9.40 22 -1 0 0.50 11.70 22 2 0 69.59 19.60 22 2 0 86.79 19.80 22 -2 0 109.99 23.70 22 -3 0 12.60 11.60 22 3 0 13.70 13.40 22 3 0 13.10 9.80 22 4 0 40.90 13.90 22 4 0 67.79 19.30 22 -4 0 59.19 19.40 22 0 -1 323.97 40.10 22 0 1 355.86 37.60 22 0 1 325.17 40.30 22 1 -1 75.09 16.80 22 -1 1 41.30 15.70 22 1 -1 83.19 21.40 22 1 1 54.39 17.30 22 1 1 57.29 15.50 22 -1 -1 100.59 24.30 22 2 -1 148.79 29.20 22 -2 1 96.09 22.00 22 2 -1 134.89 23.50 22 2 1 148.69 24.40 22 -2 -1 131.19 28.30 22 2 1 159.38 31.00 22 3 -1 6.60 11.20 22 3 -1 18.30 11.70 22 -3 1 -2.50 9.80 22 3 1 26.30 11.50 22 -3 -1 5.10 9.30 22 3 1 12.40 11.50 22 -4 1 159.38 29.00 22 4 -1 188.28 29.80 22 4 -1 221.28 35.50 22 -4 -1 168.08 33.80 22 4 1 222.48 27.80 22 4 1 156.68 30.10 22 0 2 46.80 18.40 22 0 2 36.00 13.30 22 0 -2 64.09 21.00 22 -1 2 36.50 14.90 22 1 -2 60.59 15.50 22 1 -2 59.59 19.90 22 1 2 76.79 21.60 22 1 2 59.29 15.50 22 -1 -2 59.09 19.40 22 -2 2 4.20 9.60 22 2 -2 6.90 10.30 22 2 -2 17.20 10.70 22 -2 -2 7.00 10.00 22 2 2 6.70 10.30 22 2 2 11.80 10.90 22 3 -2 84.09 22.10 22 3 -2 67.09 16.90 22 3 2 50.89 16.30 22 -3 -2 77.79 23.60 22 3 2 45.20 16.20 22 4 -2 64.29 17.70 22 -4 2 44.40 17.60 22 4 -2 84.69 22.30 22 4 2 97.99 20.70 22 4 2 74.49 20.80 22 -4 -2 55.59 17.00 22 0 3 236.88 27.90 22 0 3 185.58 32.90 22 0 -3 166.98 30.30 22 1 -3 40.90 15.60 22 -1 3 45.70 16.40 22 -1 3 48.00 14.40 22 1 3 20.70 12.10 22 1 3 56.59 20.20 22 -1 -3 53.09 18.60 22 2 -3 18.40 11.00 22 2 -3 16.00 12.80 22 -2 3 6.70 10.60 22 -2 -3 32.40 16.50 22 2 3 19.30 11.40 22 2 3 8.60 12.90 22 3 -3 64.99 20.10 22 3 -3 51.19 16.60 22 -3 3 30.10 13.70 22 3 3 41.50 13.70 22 -3 -3 34.30 14.90 22 3 3 37.50 16.60 22 4 -3 64.39 17.90 22 4 -3 57.19 17.70 22 -4 3 101.59 24.40 22 4 3 52.49 15.80 22 4 3 57.19 18.60 22 -4 -3 71.09 23.60 22 0 4 73.79 17.80 22 0 4 102.89 24.90 22 0 -4 133.79 26.50 22 -1 4 17.10 10.30 22 -1 4 5.00 12.30 22 1 -4 3.00 11.30 22 1 4 17.50 11.80 22 1 4 22.40 11.90 22 -1 -4 8.70 13.40 22 -2 4 139.29 23.60 22 2 -4 120.09 21.90 22 -2 4 101.09 24.60 22 2 -4 126.89 27.10 22 -2 -4 130.79 28.70 22 2 4 94.69 20.40 22 2 4 104.99 25.20 22 3 -4 31.70 15.60 22 -3 4 30.20 14.40 22 3 -4 34.90 14.60 22 3 4 31.40 12.50 22 3 4 42.30 19.20 22 -3 -4 26.90 13.40 22 0 5 131.89 27.80 22 0 5 127.69 21.70 22 0 -5 141.19 29.10 22 1 -5 63.69 18.00 22 -1 5 33.50 12.80 22 -1 5 70.79 19.70 22 1 5 46.20 18.40 22 -1 -5 43.80 19.30 22 1 5 55.49 15.40 22 2 -5 -7.10 10.50 22 2 -5 -0.30 8.90 22 -2 5 5.40 9.00 22 -2 5 -2.00 12.00 22 2 5 6.10 10.30 22 2 5 -1.90 9.30 22 -2 -5 2.30 10.40 23 0 0 -2.00 8.60 23 1 0 -8.50 9.10 23 -1 0 -1.00 10.30 23 1 0 5.20 9.80 23 -2 0 17.80 14.80 23 2 0 21.00 12.10 23 2 0 0.00 10.40 23 -3 0 26.30 16.20 23 3 0 26.90 12.80 23 3 0 32.00 16.70 23 0 1 3.40 10.40 23 0 -1 -3.10 9.60 23 0 1 1.60 9.60 23 1 -1 21.80 14.00 23 -1 1 22.60 15.30 23 1 -1 15.20 10.40 23 -1 -1 20.30 15.60 23 1 1 10.90 10.90 23 1 1 8.80 13.80 23 -2 1 43.90 16.50 23 2 -1 109.59 26.60 23 2 -1 79.39 16.80 23 -2 -1 82.79 23.00 23 2 1 72.49 16.80 23 2 1 37.30 18.00 23 3 -1 -9.40 8.80 23 -3 1 5.00 9.90 23 3 -1 4.90 12.00 23 -3 -1 -10.20 8.80 23 3 1 -0.30 10.60 23 3 1 13.40 13.90 23 0 -2 9.60 11.20 23 0 2 1.80 9.60 23 0 2 -2.20 10.10 23 1 -2 184.88 30.10 23 1 -2 258.17 35.00 23 -1 2 217.28 37.00 23 1 2 181.78 32.80 23 -1 -2 247.08 35.40 23 1 2 240.48 29.90 23 2 -2 99.59 21.50 23 2 -2 75.49 18.70 23 -2 2 102.69 23.30 23 -2 -2 63.19 22.80 23 2 2 94.99 24.50 23 2 2 95.09 20.10 23 -3 2 307.37 39.90 23 3 -2 317.77 36.90 23 3 -2 312.87 40.10 23 -3 -2 354.96 42.90 23 3 2 316.87 37.10 23 3 2 289.37 39.90 23 0 -3 -2.60 9.20 23 0 3 -2.40 10.40 23 0 3 -7.60 9.30 23 -1 3 28.70 12.00 23 1 -3 -9.10 9.90 23 1 -3 25.40 17.10 23 -1 3 16.70 12.20 23 1 3 34.10 15.50 23 1 3 7.50 10.60 23 -1 -3 13.90 12.30 23 -2 3 97.99 24.70 23 2 -3 80.49 20.00 23 2 -3 91.29 22.00 23 2 3 146.49 29.20 23 -2 -3 85.59 22.90 23 2 3 118.09 21.70 23 0 4 -4.50 8.80 23 0 4 -7.60 9.30 23 0 -4 -2.80 9.10 23 1 -4 9.00 10.80 23 -1 4 7.10 12.30 23 -1 4 7.70 10.90 23 -1 -4 21.60 15.70 23 1 4 0.50 12.40 23 1 4 2.80 10.60 24 0 0 176.98 31.50 24 0 0 97.69 21.00 24 -1 0 4.50 11.40 24 1 0 5.80 10.00 24 1 0 -15.40 10.70 24 0 1 44.30 17.40 24 0 1 11.30 12.60 24 0 -1 47.40 16.50 24 1 -1 191.98 29.50 24 1 -1 152.48 29.90 24 -1 1 193.38 33.80 24 -1 -1 172.38 34.40 24 1 1 240.98 29.50 24 1 1 174.78 33.70 24 0 2 269.87 38.50 24 0 -2 285.27 39.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 84138 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cd1 Cd 0.91405(3) 0.33776(6) 0.25530(5) 0.02279(13) Uani 1 1 d . . . . . Rb1 Rb 0.82747(4) -0.14545(8) 0.50091(9) 0.03519(19) Uani 1 1 d . . . . . Rb2 Rb 0.40181(5) 0.14277(9) 0.74593(9) 0.0415(2) Uani 1 1 d . . . . . S1 S 0.55659(9) 0.14446(19) 0.5007(2) 0.0226(3) Uani 1 1 d . . . . . S2 S 0.76030(9) 0.49962(19) 0.50153(19) 0.0245(4) Uani 1 1 d . . . . . S3 S 0.87244(9) 0.2092(2) 0.45320(17) 0.0219(4) Uani 1 1 d . . . . . S4 S 0.70607(9) 0.2051(2) 0.30970(17) 0.0234(4) Uani 1 1 d . . . . . S5 S 0.57995(10) 0.1087(2) 0.81729(17) 0.0227(4) Uani 1 1 d . . . . . S6 S 0.60772(10) 0.4414(2) 0.69574(17) 0.0241(4) Uani 1 1 d . . . . . S7 S 0.64939(11) 0.7777(2) 0.55103(18) 0.0242(4) Uani 1 1 d . . . . . S8 S 0.73048(10) 0.1561(2) 0.63719(17) 0.0217(4) Uani 1 1 d . . . . . S9 S 0.58579(10) 0.4986(2) 0.37310(18) 0.0264(4) Uani 1 1 d . . . . . Si1 Si 0.76621(10) 0.2698(2) 0.47119(17) 0.0177(4) Uani 1 1 d . . . . . Si2 Si 0.59678(10) 0.2683(2) 0.34508(18) 0.0197(4) Uani 1 1 d . . . . . S10 S 0.54258(10) 0.2103(2) 0.18375(17) 0.0269(4) Uani 1 1 d . . . . . Si3 Si 0.61919(10) 0.2117(2) 0.65910(18) 0.0180(4) Uani 1 1 d . . . . . Si4 Si 0.64991(11) 0.5517(2) 0.53434(17) 0.0197(4) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cd1 0.0223(3) 0.0232(3) 0.0229(3) 0.0001(2) -0.0007(2) -0.0010(2) Rb1 0.0393(5) 0.0270(4) 0.0392(4) 0.0032(4) 0.0057(4) 0.0017(3) Rb2 0.0459(5) 0.0413(5) 0.0374(5) 0.0002(4) -0.0025(4) 0.0115(4) S1 0.0206(9) 0.0240(9) 0.0231(8) 0.0001(8) -0.0010(7) -0.0041(7) S2 0.0211(9) 0.0189(8) 0.0334(9) -0.0033(9) 0.0036(8) -0.0019(7) S3 0.0175(9) 0.0252(10) 0.0231(8) 0.0032(7) 0.0017(6) 0.0009(7) S4 0.0184(8) 0.0305(10) 0.0215(8) -0.0063(8) -0.0001(6) 0.0004(7) S5 0.0270(10) 0.0214(9) 0.0198(9) 0.0015(8) 0.0044(7) -0.0022(7) S6 0.0344(10) 0.0166(9) 0.0214(8) -0.0027(8) 0.0078(7) 0.0010(7) S7 0.0306(10) 0.0156(9) 0.0263(9) 0.0002(8) 0.0080(7) -0.0004(7) S8 0.0189(9) 0.0220(9) 0.0242(9) 0.0030(7) 0.0015(7) 0.0008(7) S9 0.0301(10) 0.0218(10) 0.0273(10) 0.0011(8) -0.0070(8) -0.0002(8) Si1 0.0161(9) 0.0180(10) 0.0190(10) -0.0013(8) 0.0002(6) -0.0002(7) Si2 0.0173(10) 0.0228(11) 0.0191(10) 0.0000(8) -0.0008(7) -0.0027(8) S10 0.0214(9) 0.0395(11) 0.0198(9) -0.0023(8) -0.0027(7) -0.0068(8) Si3 0.0181(10) 0.0162(10) 0.0197(10) 0.0002(8) 0.0020(7) -0.0015(7) Si4 0.0208(10) 0.0161(10) 0.0221(10) -0.0009(8) 0.0021(7) 0.0004(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Cd Cd -0.8075 1.2024 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag S3 Cd1 Rb2 123.32(5) . 4_654 ? S3 Cd1 S5 104.37(6) . 4_654 ? S3 Cd1 S7 117.91(6) . 4_644 ? S3 Cd1 S10 117.10(6) . 3 ? S5 Cd1 Rb2 50.48(4) 4_654 4_654 ? S7 Cd1 Rb2 118.70(5) 4_644 4_654 ? S7 Cd1 S5 116.74(6) 4_644 4_654 ? S7 Cd1 S10 98.42(6) 4_644 3 ? S10 Cd1 Rb2 51.15(5) 3 4_654 ? S10 Cd1 S5 101.63(6) 3 4_654 ? Rb2 Rb1 Rb2 118.51(2) 2_654 3_545 ? Rb2 Rb1 Rb2 117.75(2) 2_654 3 ? Rb2 Rb1 Rb2 114.32(2) 3_545 3 ? S2 Rb1 Rb2 72.61(4) 1_545 2_654 ? S2 Rb1 Rb2 46.27(3) 1_545 3_545 ? S2 Rb1 Rb2 151.12(4) 1_545 3 ? S2 Rb1 S4 65.33(5) 1_545 4_645 ? S2 Rb1 S6 109.46(5) 1_545 4_644 ? S2 Rb1 S8 122.15(5) 1_545 . ? S2 Rb1 Si2 86.66(5) 1_545 4_645 ? S3 Rb1 Rb2 144.24(4) . 3_545 ? S3 Rb1 Rb2 97.16(4) . 2_654 ? S3 Rb1 Rb2 37.15(3) . 3 ? S3 Rb1 S2 169.25(6) . 1_545 ? S3 Rb1 S4 122.78(5) . 4_645 ? S3 Rb1 S5 114.58(5) . 4_644 ? S3 Rb1 S6 64.21(4) . 4_644 ? S3 Rb1 S7 117.28(5) . 1_545 ? S3 Rb1 S8 56.77(4) . . ? S3 Rb1 Si2 103.77(5) . 4_645 ? S4 Rb1 Rb2 85.94(3) 4_645 3 ? S4 Rb1 Rb2 109.99(4) 4_645 2_654 ? S4 Rb1 Rb2 44.76(3) 4_645 3_545 ? S4 Rb1 Si2 32.35(4) 4_645 4_645 ? S5 Rb1 Rb2 97.12(4) 4_644 2_654 ? S5 Rb1 Rb2 133.82(4) 4_644 3 ? S5 Rb1 Rb2 66.17(3) 4_644 3_545 ? S5 Rb1 S2 64.70(5) 4_644 1_545 ? S5 Rb1 S4 110.80(5) 4_644 4_645 ? S5 Rb1 S6 57.14(4) 4_644 4_644 ? S5 Rb1 S8 168.55(5) 4_644 . ? S5 Rb1 Si2 102.25(4) 4_644 4_645 ? S6 Rb1 Rb2 99.25(3) 4_644 3 ? S6 Rb1 Rb2 122.63(4) 4_644 3_545 ? S6 Rb1 Rb2 78.35(4) 4_644 2_654 ? S6 Rb1 S4 166.90(5) 4_644 4_645 ? S6 Rb1 S8 111.54(5) 4_644 . ? S6 Rb1 Si2 139.36(5) 4_644 4_645 ? S7 Rb1 Rb2 42.89(4) 1_545 2_654 ? S7 Rb1 Rb2 110.10(4) 1_545 3 ? S7 Rb1 Rb2 90.08(4) 1_545 3_545 ? S7 Rb1 S2 57.37(4) 1_545 1_545 ? S7 Rb1 S4 67.30(5) 1_545 4_645 ? S7 Rb1 S5 116.07(5) 1_545 4_644 ? S7 Rb1 S6 121.09(5) 1_545 4_644 ? S7 Rb1 S8 66.96(4) 1_545 . ? S7 Rb1 Si2 99.18(5) 1_545 4_645 ? S8 Rb1 Rb2 77.70(3) . 2_654 ? S8 Rb1 Rb2 125.28(4) . 3_545 ? S8 Rb1 Rb2 44.91(3) . 3 ? S8 Rb1 S4 80.63(5) . 4_645 ? S8 Rb1 Si2 87.75(5) . 4_645 ? Si2 Rb1 Rb2 68.91(3) 4_645 3 ? Si2 Rb1 Rb2 142.07(4) 4_645 2_654 ? Si2 Rb1 Rb2 45.96(3) 4_645 3_545 ? S10 Rb1 Rb2 156.46(4) 4_645 2_654 ? S10 Rb1 Rb2 82.63(4) 4_645 3 ? S10 Rb1 Rb2 37.99(4) 4_645 3_545 ? S10 Rb1 S2 83.88(5) 4_645 1_545 ? S10 Rb1 S3 106.38(5) 4_645 . ? S10 Rb1 S4 56.86(4) 4_645 4_645 ? S10 Rb1 S5 73.18(5) 4_645 4_644 ? S10 Rb1 S6 111.61(5) 4_645 4_644 ? S10 Rb1 S7 121.69(5) 4_645 1_545 ? S10 Rb1 S8 115.37(5) 4_645 . ? S10 Rb1 Si2 30.99(4) 4_645 4_645 ? Cd1 Rb2 Rb1 130.31(2) 4_645 2_655 ? S1 Rb2 Cd1 56.02(3) . 4_645 ? S1 Rb2 Cd1 52.99(3) 2_655 4_645 ? S1 Rb2 Rb1 78.31(3) 2_655 2_655 ? S1 Rb2 Rb1 170.28(4) . 2_655 ? S1 Rb2 S1 108.90(2) 2_655 . ? S1 Rb2 S2 93.30(4) . 3_455 ? S1 Rb2 S2 112.00(4) 2_655 3_455 ? S1 Rb2 S8 134.54(5) 2_655 3_455 ? S2 Rb2 Cd1 109.16(3) 3_455 4_645 ? S2 Rb2 Rb1 77.72(3) 3_455 2_655 ? S3 Rb2 Cd1 113.09(4) 3_455 4_645 ? S3 Rb2 Rb1 110.35(4) 3_455 2_655 ? S3 Rb2 S1 159.58(5) 3_455 2_655 ? S3 Rb2 S1 60.69(4) 3_455 . ? S3 Rb2 S2 54.86(4) 3_455 3_455 ? S3 Rb2 S4 113.82(5) 3_455 2_655 ? S3 Rb2 S7 136.22(5) 3_455 2_665 ? S3 Rb2 S8 53.85(4) 3_455 3_455 ? S3 Rb2 S9 89.51(5) 3_455 2_665 ? S3 Rb2 S10 104.04(5) 3_455 2_655 ? S4 Rb2 Cd1 83.16(3) 2_655 4_645 ? S4 Rb2 Rb1 57.62(3) 2_655 2_655 ? S4 Rb2 S1 54.16(4) 2_655 2_655 ? S4 Rb2 S1 120.85(4) 2_655 . ? S4 Rb2 S2 59.17(4) 2_655 3_455 ? S4 Rb2 S8 90.75(4) 2_655 3_455 ? S5 Rb2 Cd1 35.31(3) . 4_645 ? S5 Rb2 Rb1 134.60(4) . 2_655 ? S5 Rb2 S1 65.57(4) . 2_655 ? S5 Rb2 S1 55.10(4) . . ? S5 Rb2 S2 140.30(5) . 3_455 ? S5 Rb2 S3 113.03(5) . 3_455 ? S5 Rb2 S4 113.34(5) . 2_655 ? S5 Rb2 S7 94.57(5) . 2_665 ? S5 Rb2 S8 155.88(5) . 3_455 ? S5 Rb2 S9 86.36(5) . 2_665 ? S5 Rb2 S10 70.46(5) . 2_655 ? S7 Rb2 Cd1 109.02(4) 2_665 4_645 ? S7 Rb2 Rb1 42.59(3) 2_665 2_655 ? S7 Rb2 S1 62.60(4) 2_665 2_655 ? S7 Rb2 S1 146.35(5) 2_665 . ? S7 Rb2 S2 120.28(5) 2_665 3_455 ? S7 Rb2 S4 82.14(5) 2_665 2_655 ? S7 Rb2 S8 87.23(5) 2_665 3_455 ? S7 Rb2 S9 57.81(5) 2_665 2_665 ? S8 Rb2 Cd1 161.55(4) 3_455 4_645 ? S8 Rb2 Rb1 57.24(3) 3_455 2_655 ? S8 Rb2 S1 114.33(5) 3_455 . ? S8 Rb2 S2 53.38(4) 3_455 3_455 ? S9 Rb2 Cd1 121.47(4) 2_665 4_645 ? S9 Rb2 Rb1 81.20(3) 2_665 2_655 ? S9 Rb2 S1 101.70(4) 2_665 . ? S9 Rb2 S1 110.40(5) 2_665 2_655 ? S9 Rb2 S2 126.96(5) 2_665 3_455 ? S9 Rb2 S4 137.23(5) 2_665 2_655 ? S9 Rb2 S8 74.26(4) 2_665 3_455 ? S10 Rb2 Cd1 35.16(3) 2_655 4_645 ? S10 Rb2 Rb1 111.14(4) 2_655 2_655 ? S10 Rb2 S1 55.72(4) 2_655 2_655 ? S10 Rb2 S1 69.67(4) 2_655 . ? S10 Rb2 S2 76.45(4) 2_655 3_455 ? S10 Rb2 S4 54.20(4) 2_655 2_655 ? S10 Rb2 S7 117.32(5) 2_655 2_665 ? S10 Rb2 S8 129.49(5) 2_655 3_455 ? S10 Rb2 S9 156.24(5) 2_655 2_665 ? Rb2 S1 Rb2 128.17(5) 2_654 . ? Si2 S1 Rb2 141.26(9) . . ? Si2 S1 Rb2 75.33(8) . 2_654 ? Si3 S1 Rb2 129.73(9) . 2_654 ? Si3 S1 Rb2 83.08(8) . . ? Si3 S1 Si2 105.34(10) . . ? Rb1 S2 Rb2 93.91(4) 1_565 3 ? Si1 S2 Rb1 154.40(9) . 1_565 ? Si1 S2 Rb2 74.82(7) . 3 ? Si1 S2 Si4 107.08(10) . . ? Si4 S2 Rb1 98.01(8) . 1_565 ? Si4 S2 Rb2 127.78(9) . 3 ? Cd1 S3 Rb1 130.14(7) . . ? Cd1 S3 Rb2 121.37(7) . 3 ? Rb1 S3 Rb2 106.31(5) . 3 ? Si1 S3 Cd1 104.28(9) . . ? Si1 S3 Rb1 90.29(8) . . ? Si1 S3 Rb2 87.92(8) . 3 ? Rb1 S4 Rb2 93.58(4) 4_654 2_654 ? Si1 S4 Rb1 135.81(9) . 4_654 ? Si1 S4 Rb2 130.55(9) . 2_654 ? Si1 S4 Si2 106.45(10) . . ? Si2 S4 Rb1 83.85(7) . 4_654 ? Si2 S4 Rb2 75.86(7) . 2_654 ? Cd1 S5 Rb1 138.96(7) 4_645 4_655 ? Cd1 S5 Rb2 94.21(6) 4_645 . ? Rb2 S5 Rb1 123.60(6) . 4_655 ? Si3 S5 Cd1 102.49(9) . 4_645 ? Si3 S5 Rb1 89.17(8) . 4_655 ? Si3 S5 Rb2 97.04(8) . . ? Si3 S6 Rb1 85.00(8) . 4_655 ? Si4 S6 Rb1 135.40(10) . 4_655 ? Si4 S6 Si3 106.20(10) . . ? Cd1 S7 Rb1 122.69(7) 4_655 1_565 ? Cd1 S7 Rb2 128.97(7) 4_655 2_664 ? Rb1 S7 Rb2 94.52(5) 1_565 2_664 ? Si4 S7 Cd1 106.96(9) . 4_655 ? Si4 S7 Rb1 100.71(9) . 1_565 ? Si4 S7 Rb2 97.51(8) . 2_664 ? Rb1 S8 Rb2 93.94(4) . 3 ? Si1 S8 Rb1 83.37(7) . . ? Si1 S8 Rb2 76.06(7) . 3 ? Si3 S8 Rb1 135.21(9) . . ? Si3 S8 Rb2 130.84(9) . 3 ? Si3 S8 Si1 105.87(10) . . ? Si2 S9 Rb2 148.21(10) . 2_664 ? Si2 S9 Si4 106.30(11) . . ? Si4 S9 Rb2 93.37(8) . 2_664 ? S2 Si1 Rb2 73.81(7) . 3 ? S2 Si1 S4 111.62(11) . . ? S2 Si1 S8 109.66(10) . . ? S3 Si1 Rb2 60.51(7) . 3 ? S3 Si1 S2 109.16(11) . . ? S3 Si1 S4 110.83(11) . . ? S3 Si1 S8 104.08(10) . . ? S4 Si1 Rb2 171.29(9) . 3 ? S4 Si1 S8 111.21(11) . . ? S8 Si1 Rb2 71.95(7) . 3 ? S1 Si2 Rb2 72.64(8) . 2_654 ? S1 Si2 S4 108.96(11) . . ? S4 Si2 Rb2 71.81(8) . 2_654 ? S9 Si2 Rb2 170.84(9) . 2_654 ? S9 Si2 S1 112.34(11) . . ? S9 Si2 S4 112.33(11) . . ? S10 Si2 Rb2 62.02(8) . 2_654 ? S10 Si2 S1 109.56(11) . . ? S10 Si2 S4 104.52(11) . . ? S10 Si2 S9 108.82(12) . . ? Cd1 S10 Rb1 155.94(8) 3_455 4_654 ? Cd1 S10 Rb2 93.69(6) 3_455 2_654 ? Rb1 S10 Rb2 105.03(6) 4_654 2_654 ? Si2 S10 Cd1 104.93(9) . 3_455 ? Si2 S10 Rb1 91.47(8) . 4_654 ? Si2 S10 Rb2 86.20(9) . 2_654 ? S1 Si3 Rb1 161.36(9) . 4_655 ? S1 Si3 S6 111.69(11) . . ? S1 Si3 S8 111.97(11) . . ? S5 Si3 Rb1 59.69(7) . 4_655 ? S5 Si3 S1 108.44(11) . . ? S5 Si3 S6 105.30(11) . . ? S5 Si3 S8 108.85(11) . . ? S6 Si3 Rb1 62.56(7) . 4_655 ? S6 Si3 S8 110.32(11) . . ? S8 Si3 Rb1 86.27(8) . 4_655 ? S2 Si4 S9 110.85(11) . . ? S6 Si4 S2 112.30(11) . . ? S6 Si4 S9 109.17(11) . . ? S7 Si4 S2 103.88(11) . . ? S7 Si4 S6 113.53(11) . . ? S7 Si4 S9 106.91(11) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cd1 Rb2 4.4210(9) 4_654 ? Cd1 S3 2.5279(19) . ? Cd1 S5 2.5621(19) 4_654 ? Cd1 S7 2.5297(19) 4_644 ? Cd1 S10 2.5511(19) 3 ? Rb1 Rb2 5.4132(12) 3_545 ? Rb1 Rb2 5.4544(12) 3 ? Rb1 Rb2 5.0581(13) 2_654 ? Rb1 S2 3.4743(18) 1_545 ? Rb1 S3 3.383(2) . ? Rb1 S4 3.605(2) 4_645 ? Rb1 S5 3.437(2) 4_644 ? Rb1 S6 3.547(2) 4_644 ? Rb1 S7 3.434(2) 1_545 ? Rb1 S8 3.597(2) . ? Rb1 Si2 3.995(2) 4_645 ? Rb1 S10 3.372(2) 4_645 ? Rb2 S1 3.885(2) . ? Rb2 S1 3.846(2) 2_655 ? Rb2 S2 3.921(2) 3_455 ? Rb2 S3 3.432(2) 3_455 ? Rb2 S4 3.819(2) 2_655 ? Rb2 S5 3.420(2) . ? Rb2 S7 3.453(2) 2_665 ? Rb2 S8 3.860(2) 3_455 ? Rb2 S9 3.549(2) 2_665 ? Rb2 S10 3.450(2) 2_655 ? S1 Si2 2.137(3) . ? S1 Si3 2.136(3) . ? S2 Si1 2.125(3) . ? S2 Si4 2.140(3) . ? S3 Si1 2.065(3) . ? S4 Si1 2.132(3) . ? S4 Si2 2.150(3) . ? S5 Si3 2.059(3) . ? S6 Si3 2.144(3) . ? S6 Si4 2.137(3) . ? S7 Si4 2.071(3) . ? S8 Si1 2.151(3) . ? S8 Si3 2.148(3) . ? S9 Si2 2.134(3) . ? S9 Si4 2.143(3) . ? Si2 S10 2.057(3) . ?