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Information card for entry 1574598
Preview
| Coordinates | 1574598.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C22 H34 B2 O4 |
|---|---|
| Calculated formula | C22 H34 B2 O4 |
| Title of publication | Synthesis of gem-Di(boryl)cyclopropanes from Non-Activated Olefins via Mn-Photocatalyzed Atom Transfer Radical Addition |
| Authors of publication | Hu, Jiefeng; Zhang, Kun; Wang, Jing; Huang, Mingming; Chen, Shuangru; Shi, Zhuangzhi; Marder, Todd B. |
| Journal of publication | Chemical Science |
| Year of publication | 2025 |
| a | 13.1753 ± 0.0017 Å |
| b | 15.5076 ± 0.0019 Å |
| c | 12.1845 ± 0.0015 Å |
| α | 90° |
| β | 115.425 ± 0.003° |
| γ | 90° |
| Cell volume | 2248.4 ± 0.5 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296.15 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.2089 |
| Residual factor for significantly intense reflections | 0.0988 |
| Weighted residual factors for significantly intense reflections | 0.2314 |
| Weighted residual factors for all reflections included in the refinement | 0.2878 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.019 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 299618 (current) | 2025-05-13 | cif/ Adding structures of 1574598 via cif-deposit CGI script. |
1574598.cif |
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Users of the data should acknowledge the original authors of the
structural data.