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Information card for entry 1574993
Preview
| Coordinates | 1574993.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C25 H51 N3 P2 |
|---|---|
| Calculated formula | C25 H51 N3 P2 |
| Title of publication | Diastereoselective Arylation of Bis-Lactim Ethers Catalyzed by N-coordinating Ylide-Functionalized Phosphine (NYPhos) |
| Authors of publication | Sowa Prendes, Daniel; Löffler, Julian; Martins Barreto, Ivan; Sankaran, Nagesh; Remm, Henning; Oliveira, Ronaldo; Gessner, Viktoria H.; Goossen, Lukas J. |
| Journal of publication | Chemical Science |
| Year of publication | 2025 |
| a | 17.505 ± 0.0001 Å |
| b | 18.2908 ± 0.0002 Å |
| c | 20.1417 ± 0.0002 Å |
| α | 66.305 ± 0.001° |
| β | 68.119 ± 0.001° |
| γ | 72.629 ± 0.001° |
| Cell volume | 5395.23 ± 0.1 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0595 |
| Residual factor for significantly intense reflections | 0.054 |
| Weighted residual factors for significantly intense reflections | 0.1498 |
| Weighted residual factors for all reflections included in the refinement | 0.1562 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.041 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 300270 (current) | 2025-07-01 | cif/ Adding structures of 1574991, 1574992, 1574993 via cif-deposit CGI script. |
1574993.cif |
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Users of the data should acknowledge the original authors of the
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