data_2000300
_journal_name_full 'Acta Cryst. C'
_journal_year   1991
_journal_volume  47
_journal_page_first  1164
_journal_page_last  1167
_chemical_formula_  'C10 H12 Ni1 S8'
_symmetry_cell_setting  orthorhombic
_symmetry_space_group_name_h-m  Iba2
_symmetry_space_group_name_hall  ?
_cell_length_a  13.027(3)
_cell_length_b  16.042(6)
_cell_length_c  7.486(2)
_cell_angle_alpha  90
_cell_angle_beta  90
_cell_angle_gamma  90
_cell_volume  1564.5(8)
_cell_formula_units_z  4
_exptl_crystal_density_diffrn  1.857
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  912
_diffrn_radiation_type  mo
_diffrn_radiation_wavelength  0.71069
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Ni .0000 .0000 .0000 .01620(10)
 S1 .05121(5) -.12566(4) .0051(2) .0178(2)
 S2 .15455(5) .04403(5) .0249(2) .0178(2)
 S3 .23525(6) -.22181(5) .04578(15) .0173(2)
 S4 .35823(6) -.02140(5) .0968(2) .0182(2)
 C1 .1811(2) -.1216(2) .0358(5) .0149(8)
 C2 .2286(2) -.0436(2) .0514(5) .0155(8)
 C3 .3666(3) -.2063(2) -.0279(5) .0179(9)
 C4 .4391(3) -.1835(2) .1252(5) .0189(9)
 C5 .4000(2) -.1090(2) .2342(5) .0165(8)
 H3A .3677 -.1622 -.1138 .0380
 H3B .3904 -.2561 -.0833 .0380
 H4A .5047 -.1702 .0781 .0380
 H4B .4453 -.2305 .2028 .0380
 H5A .3433 -.1272 .3048 .0380
 H5B .4535 -.0907 .3108 .0380