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#$Date: 2010-01-30 15:59:17 +0200 (Sat, 30 Jan 2010) $
#$Revision: 966 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/2000306.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2000306
loop_
_publ_author_name
'Gou, S.-H.'
'You, X.-Z.'
'Xu, Z.'
'Zhou, Z.-Y.'
'Yu, K.-B.'
'Yu, Y.-P.'
'Zhu, D.-L.'
_publ_section_title
;
 Structure of
 <i>catena</i>-poly{bis[4,4,4-trifluoro-1-(2-thienyl)-1,3-butanedionato-\k^2^<i>O</i>,<i>O</i>']copper-\m-(4,4'-bipyridine)-\k<i>N</i>:\k<i>N</i>'}--<i>N</i>,<i>N</i>-dimethylformamide
 (1/2)
;
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1303
_journal_page_last               1305
_journal_volume                  47
_journal_year                    1991
_chemical_formula_sum            'C32 H30 Cu F6 N4 O6 S2'
_[local]_cod_chemical_formula_sum_orig 'Cu1 C32 H30 F6 O6 S2 N4'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                73.400(10)
_cell_angle_beta                 65.410(10)
_cell_angle_gamma                69.290(10)
_cell_formula_units_Z            1
_cell_length_a                   9.637(2)
_cell_length_b                   9.820(2)
_cell_length_c                   11.505(2)
_cell_volume                     913.76(3)
_diffrn_radiation_type           mo
_diffrn_radiation_wavelength     0.71073
_exptl_absorpt_coefficient_mu    .782
_exptl_crystal_density_diffrn    1.469
_exptl_crystal_F_000             413
_[local]_cod_data_source_file    li0049.cif
_[local]_cod_data_source_block   li0049a
_[local]_cod_cif_authors_sg_H-M  P-1
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
Cu 0 0 0
S .3101(2) -.4964(2) .0163(3)
F1 -.4720(6) -.2560(6) .2650(8)
F2 -.5188(6) -.0577(7) .1431(7)
F3 -.4892(8) -.0626(10) .3138(7)
N1 -.0009(7) -.0095(6) .1937(6)
N2 .6861(13) .6250(10) .5519(9)
O1 .0853(5) -.2176(4) .0174(4)
O2 -.2316(5) -.0223(5) .0869(5)
O3 .7431(11) .4308(8) .4590(9)
C1 .3399(10) -.6808(8) .0729(9)
C2 .2070(10) -.7180(7) .1474(9)
C3 .0694(8) -.5978(7) .1641(8)
C4 .1090(7) -.4653(7) .0967(7)
C5 .0102(7) -.3132(7) .0860(6)
C6 -.1524(8) -.2842(7) .1488(7)
C7 -.2575(8) -.1443(7) .1430(7)
C8 -.4351(9) -.1328(8) .2185(9)
C9 .1093(8) -.1055(8) .2400(8)
C10 .1134(8) -.1064(8) .3594(8)
C11 -.0008(8) -.0022(7) .4372(7)
C12 -.1152(9) .0976(8) .3867(8)
C13 -.1118(9) .0906(8) .2667(8)
C14 .700(3) .5273(18) .4950(16)
C15 .789(2) .712(2) .5229(19)
C16 .535(2) .659(3) .6536(18)
H1 .4425 -.7506 .0528
H3 -.0364 -.6056 .2150
H6 -.1955 -.3658 .1995
H2 .1990 -.8134 .1714
H9 .2226 -.1784 .1663
H10 .2005 -.1763 .3968
H12 -.2156 .1632 .4492
H13 -.2264 .1547 .2283
_cod_database_code 2000306