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#$Date: 2008-01-26 15:05:32 +0200 (Sat, 26 Jan 2008) $
#$Revision: 19 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/2000782.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2000782
_journal_name_full  'Acta Cryst.'
_journal_year  1992
_journal_volume  C48
_journal_page_first  1309
_journal_page_last  1310
loop_
_publ_author_name
 'Belanger-Gariepy, F.'
 'Leger, R.'
 'Hanessian, S.'
_chemical_formula_sum  'C18 H32 O4 Sn1'
_chemical_formula_weight  431.14
_symmetry_cell_setting  triclinic
_symmetry_space_group_name_H-M  'P -1'
_symmetry_space_group_name_Hall  '-P 1'
_cell_length_a  7.674(2)
_cell_length_b  11.113(3)
_cell_length_c  13.346(4)
_cell_angle_alpha  71.64(2)
_cell_angle_beta  79.49(2)
_cell_angle_gamma  86.62(2)
_cell_volume  1062.1(5)
_cell_formula_units_Z  2
_exptl_crystal_density_diffrn  1.348
_exptl_crystal_density_meas  ?
_exptl_crystal_F_000  444
_exptl_absorpt_coefficient_mu  1.22
_diffrn_radiation_type  Mo
_diffrn_radiation_wavelength  0.71069
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
 Sn .28289(8) 1.25178(4) .11247(4) .075
 O(1) .1279(6) .7673(5) .4702(4) .082
 O(2) .3397(6) .6215(4) .4611(4) .076
 O(3) .6628(5) .7854(5) .2555(4) .084
 O(4) .5600(5) .8671(5) .3851(4) .078
 C(1') .2352(9) 1.0817(6) .0800(5) .066
 C(1) .3464(7) .8003(5) .3104(4) .046
 C(2) .2648(7) .9312(5) .2654(5) .049
 C(3) .3259(8) .9646(6) .1452(5) .052
 C(4) .1237(10) .8165(8) .1004(7) .085
 C(5) .0947(11) .6774(8) .1518(8) .099
 C(6) .1562(11) .6518(7) .2565(7) .088
 C(7) .3233(8) .7330(6) .2286(5) .058
 C(8) .3044(8) .8395(6) .1236(5) .058
 C(9) .2577(8) .7320(6) .4224(5) .058
 C(10) .2693(12) .5441(8) .5700(6) .099
 C(11) .3533(16) .5786(10) .6453(7) .131
 C(12) .5417(8) .8149(6) .3118(5) .058
 C(131) .7502(13) .8955(12) .3833(10) .072
 C(132) .722(3)   .860(3)   .428(2)   .112
 C(141) .7398(18) .9398(18) .4795(14) .116
 C(142) .763(3)   .991(3)   .418(3)   .135
 C(15) .3022(13) 1.4094(8) -.0308(7) .101
 C(16) .5260(13) 1.2356(9) .1694(8) .110
 C(17) .0760(18) 1.2840(11) .2281(10) .147
 H(1'A) .1110 1.0670 .0957 ?
 H(1'B) .2772 1.0934 .0061 ?
 H(2A) .1391 .9276 .2828 ?
 H(2B) .3072 .9913 .2925 ?
 H(3) .4492 .9822 .1312 ?
 H(4A) .1254 .8394 .0254 ?
 H(4B) .0339 .8633 .1311 ?
 H(5B) .1629 .6308 .1096 ?
 H(6A) .0687 .6767 .3065 ?
 H(6B) .1832 .5645 .2853 ?
 H(7) .4253 .6832 .2167 ?
 H(8) .3951 .8316 .0672 ?
 H(10A) .2919 .4572 .5766 ?
 H(10B) .1451 .5576 .5847 ?
 H(11A) .3165 .6613 .6466 ?
 H(11B) .3206 .5198 .7148 ?
 H(11C) .4784 .5774 .6244 ?
 H(131A) .8216 .8216 .3897 ?
 H(131B) .7963 .9600 .3194 ?
 H(132A) .7046 .8091 .5006 ?
 H(132B) .8147 .8259 .3873 ?
 H(141A) .8551 .9604 .4854 ?
 H(141B) .6661 1.0128 .4720 ?
 H(141C) .6914 .8744 .5423 ?
 H(142A) .7358 1.0027 .4868 ?
 H(142B) .8855 1.0066 .3905 ?
 H(142C) .6948 1.0480 .3711 ?
 H(15A) .3348 1.3803 -.0914 ?
 H(15B) .1909 1.4515 -.0339 ?
 H(15C) .3893 1.4668 -.0311 ?
 H(16A) .5349 1.3020 .1989 ?
 H(16B) .5308 1.1562 .2231 ?
 H(16C) .6217 1.2415 .1118 ?
 H(17A) .1077 1.3511 .2512 ?
 H(17B) -.0287 1.3064 .1979 ?
 H(17C) .0553 1.2092 .2878 ?