#------------------------------------------------------------------------------
#$Date: 2008-01-26 15:05:32 +0200 (Sat, 26 Jan 2008) $
#$Revision: 19 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/2001843.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2001843
_journal_name_full 'Acta Crystallographica, Section C'
_journal_year 1993
_journal_volume C49
_journal_page_first 435
_journal_page_last 437
loop_
_publ_author_name
'Elmokhtar, O.S.M.M.'
'Rzaigui, M.'
'Jouini, A.'
_chemical_formula_moiety 'H16 Li2 N4 O18 P6,4(H2 O1)'
_chemical_formula_sum 'H24 Li2 N4 O22 P6'
_chemical_formula_weight 631.93
_symmetry_cell_setting monoclinic
_symmetry_space_group_name_H-M 'P 1 21/c 1'
_symmetry_space_group_name_Hall '-P 2ybc'
_cell_length_a 9.429(2)
_cell_length_b 15.824(3)
_cell_length_c 7.9310(10)
_cell_angle_alpha  90
_cell_angle_beta 106.260(10)
_cell_angle_gamma  90
_cell_volume 1136
_cell_formula_units_Z 2
_exptl_crystal_density_diffrn 1.85
_exptl_crystal_density_meas ?
_exptl_crystal_F_000 648
_exptl_absorpt_coefficient_mu 0.562
_diffrn_radiation_type Mo
_diffrn_radiation_wavelength 0.7107
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
P(1) .50460(8) .11912(4) .12998(9)
P(2) .21096(8) .40084(5) .39760(10)
P(3) .76155(8) .03347(5) .35240(10)
O(E11) .5735(2) .14560(10)
 -.0089(3)
O(E12) .4772(3) .18520(10)
 .2492(3)
O(L12) .3554(2) .43240(10)
 .5462(3)
O(L23) .1696(2) .01500(10)
 .7844(3)
O(E21) .2532(2) .33150(10)
 .2962(3)
O(E22) .0912(2) .3873(2) .4813(3)
O(E31) .2380(3) .02220(10)
 .4974(3)
O(E32) .8321(2) .11710(10)
 .3812(3)
O(L13) .5913(2) .45800(10)
 .7419(3)
O(W1) .4841(3) .1319(2) .5816(3)
O(W2) .8195(3) .2621(2) .1205(4)
N(1) .0992(3) .3278(2) .8179(4)
N(2) .7905(3) .4116(2) .3103(4)
Li .4482(6) .3030(4) .2694(7)
H1(W1) .403(6) .092(4) .555(8)
H2(W1) .489(5) .348(3) -.001(7)
H1(W2) .817(5) .206(3) .539(7)
H2(W2) .765(6) .226(4) .105(8)
H1(N1) .116(6) .347(3) .729(7)
H2(N1) .864(5) .776(3) .682(7)
H3(N1) .861(5) .632(3) .091(7)
H4(N1) .979(6) .830(4) .673(8)
H1(N2) .113(5) .587(3) .623(6)
H2(N2) .205(5) .864(3) .247(6)
H3(N2) .787(6) .048(4) .726(8)
H4(N2) .267(6) .591(4) .615(8)