data_2001849
_journal_name_full 'Acta Crystallographica, Section C'
_journal_year 1993
_journal_volume C49
_journal_page_first 460
_journal_page_last 464
loop_
_publ_author_name
'Bachechi, F.'
_chemical_formula_moiety 'C24 H63 P4 Pt2, C24 H20 B1'
_chemical_formula_sum 'C48 H83 B1 P4 Pt2'
_chemical_formula_weight 1185.1
_symmetry_cell_setting monoclinic
_symmetry_space_group_name_H-M 'C 2/n'
_symmetry_space_group_name_Hall '-C 2yac'
_cell_length_a 23.284(10)
_cell_length_b 20.923(7)
_cell_length_c 21.822(8)
_cell_angle_alpha  90
_cell_angle_beta 93.10(3)
_cell_angle_gamma  90
_cell_volume 10615(6)
_cell_formula_units_Z 8
_exptl_crystal_density_diffrn 1.483
_exptl_crystal_density_meas ?
_exptl_crystal_F_000 4736
_exptl_absorpt_coefficient_mu 5.47
_diffrn_radiation_type Mo
_diffrn_radiation_wavelength 0.71073
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
Pt(1) .05285(4) .15697(4) .21504(4) .0655(3)
Pt(2) .01627(5) .28094(5) .15292(4) .0732(3)
Pt(1') .0062(10) .1838(11) .1409(10) .089(3)
Pt(2') .0757(9) .0269(11) .2250(9) .073(2)
Pt(1") .0927(7) .2189(7) .1435(7) .083(3)
Pt(2") -.0108(7) .2263(7) .2184(8) .097(3)
P(1) .0761(3) .0857(4) .1427(3) .080(10)
P(2) .0399(3) .2057(3) .3067(3) .120(10)
P(3) -.0787(3) .2538(3) .1392(3) .100(10)
P(4) .1031(3) .3301(4) .1477(3) .080(10)
B -.2351(11) .0371(13) .4953(13) .100(10)
C(1) .150(3)   .067(3)   .138(3)   .110(10)
C(2) .185(2)   .059(2)   .188(2)   .140(10)
C(3) .085(4)   .105(5)   .063(4)   .13(2)
C(4) .052(3)   .124(3)   .037(3)   .120(10)
C(5) .033(2)   .013(3)   .137(3)   .110(10)
C(6) .006(3)   -.010(3)   .186(3)   .120(10)
C(7) .109(3)   .208(3)   .355(3)   .100(10)
C(8) .1563(14) .1785(15) .3476(15) .120(10)
C(9) -.001(3)   .167(3)   .356(3)   .110(10)
C(10) -.0477(14) .1256(16) .3426(14) .120(10)
C(11) .0115(16) .2878(18) .3108(17) .140(10)
C(12) .0154(12) .3181(14) .3734(13) .110(10)
C(13) -.130(2)   .291(2)   .187(2)   .150(10)
C(14) -.1230(13) .3504(16) .2108(14) .110(10)
C(15) -.113(4)   .173(4)   .141(4)   .140(10)
C(16) -.122(3)   .136(3)   .171(3)   .110(10)
C(17) -.109(2)   .277(3)   .063(3)   .110(10)
C(18) -.0772(13) .2698(15) .0092(14) .110(10)
C(19) .167(3)   .293(3)   .131(3)   .110(10)
C(20) .191(3)   .261(3)   .180(3)   .160(10)
C(21) .128(3)   .390(3)   .209(3)   .110(10)
C(22) .100(3)   .435(3)   .211(3)   .120(10)
C(23) .1051(16) .3851(19) .0813(18) .150(10)
C(24) .0943(16) .3500(18) .0231(17) .140(10)
C(31) -.2284(7) .0871(9) .4359(8) ?
C(32) -.2299(7) .1525(10) .4474(7) ?
C(33) -.2199(8) .1957(7) .4006(9) ?
C(34) -.2085(7) .1735(9) .3424(8) ?
C(35) -.2070(7) .1080(10) .3309(7) ?
C(36) -.2170(7) .0649(7) .3777(9) ?
C(37) -.1697(6) .028(2)   .5310(8) ?
C(38) -.1633(6) .005(2)   .5910(7) ?
C(39) -.1086(8) -.0014(9) .6194(6) ?
C(40) -.0603(6) .015(2)   .5878(8) ?
C(41) -.0667(6) .037(2)   .5278(7) ?
C(42) -.1214(8) .0438(8) .4995(6) ?
C(43) -.2808(7) .0725(12) .5433(10) ?
C(44) -.2616(6) .1012(16) .5982(7) ?
C(45) -.3003(7) .1331(8) .6338(6) ?
C(46) -.3582(7) .1363(12) .6146(6) ?
C(47) -.3774(6) .1076(16) .5597(7) ?
C(48) -.3387(7) .0757(8) .5241(6) ?
C(49) -.2604(8) -.0357(7) .4740(8) ?
C(50) -.3008(8) -.0416(7) .4249(8) ?
C(51) -.3243(7) -.1011(9) .4099(7) ?
C(52) -.3073(8) -.1548(7) .4439(8) ?
C(53) -.2670(8) -.1489(7) .4931(8) ?
C(54) -.2435(7) -.0894(9) .5081(7) ?