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#$Date: 2010-01-30 15:59:17 +0200 (Sat, 30 Jan 2010) $
#$Revision: 966 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/2001851.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2001851
loop_
_publ_author_name
'Hoang, N. N.'
'Valach, F.'
'Meln\'ik, M.'
_publ_section_title
;
 Structure of tetrakis(\m-acetato)-bis(4-pyridylmethanol)dicopper(II)
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              467
_journal_page_last               469
_journal_volume                  49
_journal_year                    1993
_chemical_formula_sum            'C20 H26 Cu2 N2 O10'
_chemical_formula_weight         581.53
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                91.4070(10)
_cell_angle_beta                 98.2470(10)
_cell_angle_gamma                114.242(3)
_cell_formula_units_Z            1
_cell_length_a                   7.301(4)
_cell_length_b                   8.216(4)
_cell_length_c                   10.709(5)
_cell_volume                     577.27
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.71069
_exptl_absorpt_coefficient_mu    1.90
_exptl_crystal_density_diffrn    1.67
_exptl_crystal_density_meas      1.63
_exptl_crystal_F_000             298
_[local]_cod_data_source_file    al0509.cif
_[local]_cod_data_source_block   al0509_structure_1_of_1
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
Cu .13287(8) .53911(7) .60644(5)
N .3673(6) .6161(5) .7722(3)
O(1) .0338(5) .7211(5) .6425(3)
O(2) .1872(5) .3413(4) .5375(3)
O(3) -.0928(5) .3609(5) .6817(3)
O(4) .3144(5) .7052(5) .4981(3)
O(5) 1.0173(6) .7600(6) 1.0782(4)
C(1) .3638(8) .7152(7) .8732(5)
C(2) .5211(9) .7787(7) .9740(4)
C(3) .6890(8) .7396(6) .9782(4)
C(4) .6885(7) .6322(7) .8764(4)
C(5) .5275(7) .5749(6) .7755(4)
C(6) .8603(9) .8114(8) 1.0885(5)
C(7) .2694(6) .7246(5) .3844(4)
C(8) .4350(7) .8569(7) .3214(5)
C(9) -.0998(6) .7456(6) .5689(4)
C(10) -.1602(8) .8906(6) .6091(5)
H(1) .2365 .7552 .8713
H(2) .5187 .8625 1.0528
H(3) .8166 .5936 .8789
H(4) .5314 .4893 .6994
H(5) .8025 .7720 1.1785
H(6) .9235 .9607 1.0969
H(7) 1.1381 .8151 1.1592
H(8) .5748 .9208 .3875
H(9) .3886 .9600 .2847
H(10) .4617 .7898 .2412
H(12) -.0285 1.0191 .6220
H(13) -.2180 .8641 .6973
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
Cu N 2.160(3)
Cu O(1) 1.962(4)
Cu O(2) 1.975(4)
Cu O(3) 1.992(3)
Cu O(4) 1.999(3)
C(7) O(3) 1.276(5)
C(7) O(4) 1.246(5)
C(7) C(8) 1.513(6)
C(9) O(1) 1.250(6)
C(9) O(2) 1.262(5)
C(9) C(10) 1.503(8)
N C(1) 1.347(7)
N C(5) 1.341(7)
C(1) C(2) 1.372(6)
C(2) C(3) 1.384(9)
C(3) C(4) 1.384(7)
C(3) C(6) 1.498(7)
C(4) C(5) 1.388(6)
C(6) O(5) 1.391(9)
_cod_database_code 2001851