data_2003122 _journal_name_full 'Acta Crystallographica, Section B' _journal_year 1998 _journal_volume B54 _journal_page_first 809 _journal_page_last 818 _chemical_formula_sum 'As F4 H2 K O2' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'C 2/c' _symmetry_space_group_name_Hall '-C 2yc' _cell_length_a 4.8180(10) _cell_length_b 16.001(4) _cell_length_c 6.374(2) _cell_angle_alpha 90 _cell_angle_beta 99.36(2) _cell_angle_gamma 90 _cell_volume 484.8(2) _cell_formula_units_Z 4 _diffrn_radiation_type 'Ag K\a' _diffrn_radiation_wavelength 0.5609 loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv As 0.000 0.63103(2) 0.25 ? K 0.5 0.59091(7) 0.75 ? F1 -0.0994(5) 0.62720(10) 0.4993(3) ? F2 0.2376(5) 0.55190(10) 0.3314(4) ? O3 0.2594(6) 0.7042(2) 0.3346(5) ?