#------------------------------------------------------------------------------
#$Date: 2009-11-14 15:09:05 +0200 (Sat, 14 Nov 2009) $
#$Revision: 846 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/2005896.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2005896
_journal_name_full               'Acta Crystallographica C'
_journal_volume                  53
_journal_year       1997
_journal_page_first    	92
_journal_page_last    	95
_publ_section_title
;
Methyl 4-Hydroxy-3-[4-methoxy-2-(methoxymethyleneoxy)phenyl]-
2-{[4-methoxy-2-(methoxymethyleneoxy)phenyl]methyl}-5-oxo-2,5-dihydrofuran-2-
carboxylate
;
_chemical_formula_sum    	'C25 H28 O11'
_chemical_formula_weight    	504.47
_symmetry_cell_setting    	Monoclinic
loop_
_symmetry_equiv_pos_as_xyz
    'x, y, z'
    '-x, y+1/2, -z+1/2'
    '-x, -y, -z'
    'x, -y-1/2, z-1/2'
_symmetry_space_group_name_H-M    	'P 21/c '
_cell_length_a    	14.6057(2)
_cell_length_b    	9.2370(1)
_cell_length_c    	18.6333(3)
_cell_angle_alpha    	90.00
_cell_angle_beta    	91.790(1)
_cell_angle_gamma    	90.00
_cell_volume    	2512.64(6)
_cell_formula_units_Z    	4
_exptl_crystal_density_diffrn    	1.334
_cell_measurement_temperature    	298(2)
loop_
_atom_site_label
_atom_site_occupancy
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
    O1 1 0.1981(2) 0.6965(3) 0.06868(12) 0.0615(7)
    O2 1 0.0916(2) 0.6013(3) -0.00656(14) 0.0780(8)
    O3 1 0.0198(2) 0.4621(3) 0.1215(2) 0.0777(9)
    H3 1 -0.0054(33) 0.4583(53) 0.0767(29) 0.104(16)
    O4 1 0.2809(2) 0.9251(3) 0.17939(15) 0.0734(8)
    O5 1 0.1289(2) 0.8928(3) 0.1673(2) 0.0788(9)
    O6 1 0.3880(2) 0.1315(3) -0.0131(2) 0.0923(10)
    O7 1 0.3062(2) 0.3545(3) 0.21339(13) 0.0700(8)
    O8 1 0.4390(2) 0.2702(4) 0.2721(2) 0.0933(10)
    O9 1 0.1447(3) 0.3961(4) 0.4663(2) 0.1260(15)
    O10 1 0.2184(2) 0.7532(3) 0.29535(13) 0.0741(8)
    O11 1 0.3245(2) 0.8063(4) 0.38881(15) 0.0888(9)
    C1 1 0.1237(2) 0.6137(4) 0.0542(2) 0.0640(10)
    C2 1 0.0940(2) 0.5494(4) 0.1208(2) 0.0610(9)
    C3 1 0.1482(2) 0.5910(4) 0.1772(2) 0.0549(9)
    C4 1 0.2213(2) 0.6887(4) 0.1459(2) 0.0557(9)
    C5 1 0.2151(3) 0.8491(4) 0.1679(2) 0.0613(9)
    C6 1 0.1136(3) 1.0452(5) 0.1831(4) 0.110(2)
    H6A 1 0.0491(3) 1.0650(5) 0.1811(4) 0.165
    H6B 1 0.1435(3) 1.1038(5) 0.1483(4) 0.165
    H6C 1 0.1382(3) 1.0671(5) 0.2302(4) 0.165
    C7 1 0.3200(2) 0.6325(4) 0.1540(2) 0.0609(9)
    H7A 1 0.3613(2) 0.7075(4) 0.1384(2) 0.073
    H7B 1 0.3337(2) 0.6142(4) 0.2045(2) 0.073
    C8 1 0.3382(2) 0.4964(4) 0.1123(2) 0.0599(9)
    C9 1 0.3325(2) 0.3593(4) 0.1423(2) 0.0602(9)
    C10 1 0.3483(2) 0.2348(4) 0.1026(2) 0.0639(10)
    H10 1 0.3433(2) 0.1439(4) 0.1236(2) 0.077
    C11 1 0.3715(3) 0.2478(4) 0.0318(2) 0.0716(11)
    C12 1 0.3796(3) 0.3832(5) -0.0001(2) 0.0782(12)
    H12 1 0.3962(3) 0.3917(5) -0.0477(2) 0.094
    C13 1 0.3625(3) 0.5042(4) 0.0403(2) 0.0724(10)
    H13 1 0.3674(3) 0.5948(4) 0.0189(2) 0.087
    C14 1 0.3744(4) -0.0099(5) 0.0142(3) 0.0955(14)
    H14A 1 0.3882(4) -0.0799(5) -0.0220(3) 0.143
    H14B 1 0.3118(4) -0.0207(5) 0.0275(3) 0.143
    H14C 1 0.4141(4) -0.0249(5) 0.0556(3) 0.143
    C15 1 0.3458(3) 0.2493(4) 0.2598(2) 0.0785(12)
    H15A 1 0.3154(3) 0.2522(4) 0.3053(2) 0.094
    H15B 1 0.3359(3) 0.1541(4) 0.2390(2) 0.094
    C16 1 0.4606(4) 0.3997(7) 0.3088(3) 0.115(2)
    H16A 1 0.5258(4) 0.4075(7) 0.3155(3) 0.173
    H16B 1 0.4325(4) 0.3993(7) 0.3547(3) 0.173
    H16C 1 0.4381(4) 0.4806(7) 0.2811(3) 0.173
    C17 1 0.1443(2) 0.5428(4) 0.2521(2) 0.0583(9)
    C18 1 0.1804(3) 0.6231(4) 0.3116(2) 0.0638(10)
    C19 1 0.1780(3) 0.5707(5) 0.3809(2) 0.0801(12)
    H19 1 0.2020(3) 0.6259(5) 0.4187(2) 0.096
    C20 1 0.1402(3) 0.4373(5) 0.3942(2) 0.0853(13)
    C21 1 0.1026(3) 0.3562(5) 0.3382(2) 0.0812(12)
    H21 1 0.0757(3) 0.2670(5) 0.3471(2) 0.097
    C22 1 0.1052(3) 0.4095(4) 0.2680(2) 0.0686(10)
    H22 1 0.0801(3) 0.3541(4) 0.2307(2) 0.082
    C23 1 0.1178(7) 0.2533(9) 0.4817(4) 0.186(4)
    H23A 1 0.1236(7) 0.2368(9) 0.5325(4) 0.279
    H23B 1 0.1563(7) 0.1865(9) 0.4572(4) 0.279
    H23C 1 0.0552(7) 0.2392(9) 0.4660(4) 0.279
    C24 1 0.2454(3) 0.8498(5) 0.3530(2) 0.0800(12)
    H24A 1 0.2545(3) 0.9460(5) 0.3335(2) 0.096
    H24B 1 0.1964(3) 0.8555(5) 0.3868(2) 0.096
    C25 1 0.4047(3) 0.8277(6) 0.3493(3) 0.101(2)
    H25A 1 0.4571(3) 0.7953(6) 0.3771(3) 0.152
    H25B 1 0.4112(3) 0.9288(6) 0.3385(3) 0.152
    H25C 1 0.4000(3) 0.7736(6) 0.3053(3) 0.152