#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/74/2007430.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2007430_Fobs loop_ _publ_author_name 'Uzelmeier, C. E.' 'Fourmigu\'e, M.' 'Dunbar, K. R.' _publ_section_title ; 3,4-Dimethyltetrathiafulvalene ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1047 _journal_page_last 1049 _journal_volume 54 _journal_year 1998 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.126 _cell_angle_gamma 90.000 _cell_length_a 7.4245 _cell_length_b 9.5676 _cell_length_c 14.0355 _exptl_crystal_F_000 480.00 _reflns_d_resolution_high 0.8884 _[local]_cod_data_source_file fr1086sup2.hkl _[local]_cod_data_source_block fr1086 #BEGIN Tags that were not found in dictionaries: _shelx_title ' SHELXL on TEXSAN' _shelx_refln_list_code 4 _shelx_f_calc_maximum 169.04 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 90.89 119.83 8.92 o 4 0 0 1661.02 1835.41 51.40 o 6 0 0 6417.12 6462.61 169.56 o 8 0 0 4.06 -1.06 18.50 o 1 1 0 1323.42 1478.68 38.56 o 2 1 0 316.12 336.05 13.43 o 3 1 0 326.60 277.77 13.45 o 4 1 0 6.56 -0.72 10.97 o 5 1 0 2709.47 2681.43 75.62 o 6 1 0 946.40 949.19 24.19 o 7 1 0 21.12 21.52 21.67 o 8 1 0 399.30 389.74 24.62 o 0 2 0 9.44 3.81 5.44 o 1 2 0 286.81 289.80 10.51 o 2 2 0 4709.93 4800.48 138.44 o 3 2 0 470.55 402.92 36.53 o 4 2 0 0.40 3.22 10.52 o 5 2 0 204.45 216.90 16.78 o 6 2 0 138.04 156.58 12.59 o 7 2 0 27.71 18.44 11.32 o 8 2 0 1469.78 1280.57 43.33 o 1 3 0 70.68 59.18 8.60 o 2 3 0 2270.60 2316.96 61.25 o 3 3 0 11641.14 13166.57 332.99 o 4 3 0 5.67 -3.21 8.23 o 5 3 0 3.30 20.09 9.95 o 6 3 0 957.83 943.91 40.92 o 7 3 0 35.46 6.37 21.71 o 0 4 0 382.92 377.25 13.66 o 1 4 0 91.61 104.79 8.14 o 2 4 0 102.49 115.77 9.47 o 3 4 0 1.99 3.19 7.14 o 4 4 0 70.67 77.44 11.74 o 5 4 0 238.10 214.06 25.03 o 6 4 0 268.08 248.21 15.60 o 7 4 0 21.07 21.14 11.90 o 1 5 0 90.47 47.67 11.17 o 2 5 0 484.72 446.89 14.63 o 3 5 0 494.04 529.29 14.94 o 4 5 0 755.18 782.40 20.05 o 5 5 0 1167.72 1163.74 93.90 o 6 5 0 517.98 476.84 17.43 o 7 5 0 52.13 49.46 12.67 o 0 6 0 3931.93 3746.41 98.12 o 1 6 0 81.87 93.71 10.45 o 2 6 0 268.56 254.83 21.59 o 3 6 0 640.83 614.54 17.30 o 4 6 0 709.13 661.99 20.91 o 5 6 0 9.72 -2.42 10.54 o 6 6 0 685.64 662.99 20.62 o 1 7 0 120.60 109.13 9.26 o 2 7 0 25.99 25.94 9.36 o 3 7 0 573.60 579.12 17.66 o 4 7 0 65.68 74.97 10.94 o 5 7 0 30.06 57.57 11.55 o 6 7 0 97.09 104.71 13.73 o 0 8 0 515.58 465.81 21.03 o 1 8 0 1017.32 945.81 86.33 o 2 8 0 41.40 73.57 16.54 o 3 8 0 0.13 -1.87 10.36 o 4 8 0 66.83 75.37 16.28 o 5 8 0 217.34 208.48 14.43 o 1 9 0 440.27 365.63 19.39 o 2 9 0 665.42 690.29 25.78 o 3 9 0 0.01 2.71 23.31 o 4 9 0 24.41 13.03 26.49 o 0 10 0 320.66 330.56 20.06 o 1 10 0 28.05 26.87 13.78 o 2 10 0 205.10 220.57 27.66 o 3 10 0 18.50 11.57 15.80 o -7 0 1 0.17 4.42 15.42 o -5 0 1 1799.75 1960.89 56.15 o -3 0 1 2510.70 2836.90 74.70 o -1 0 1 978.38 1078.74 28.29 o 1 0 1 14974.23 15513.29 388.56 o 3 0 1 0.82 14.23 8.61 o 5 0 1 1362.13 1419.63 43.36 o 7 0 1 132.44 116.76 18.34 o -8 1 1 66.84 73.08 12.77 o -7 1 1 374.06 384.98 15.91 o -6 1 1 316.52 369.50 21.77 o -5 1 1 458.83 516.23 22.06 o -4 1 1 3669.67 4253.86 111.35 o -3 1 1 2448.90 2894.22 76.14 o -2 1 1 0.17 0.78 7.61 o -1 1 1 103.74 92.12 5.58 o 0 1 1 3787.34 3763.00 94.74 o 1 1 1 31.32 25.70 7.17 o 2 1 1 792.91 822.19 24.66 o 3 1 1 460.21 531.56 19.00 o 4 1 1 101.99 123.76 12.45 o 5 1 1 2176.78 2280.64 64.47 o 6 1 1 1688.74 1731.41 52.66 o 7 1 1 14.30 18.68 11.21 o 8 1 1 54.55 68.19 19.68 o -8 2 1 418.30 428.35 25.21 o -7 2 1 505.86 522.18 43.76 o -6 2 1 38.87 80.47 17.72 o -5 2 1 1.56 4.60 13.61 o -4 2 1 196.93 182.91 13.23 o -3 2 1 1707.07 1772.30 48.56 o -2 2 1 75.41 86.40 8.90 o -1 2 1 13468.48 13104.21 632.56 o 0 2 1 213.71 187.24 7.97 o 1 2 1 129.73 155.06 9.00 o 2 2 1 0.07 -5.75 5.75 o 3 2 1 8560.07 10205.17 258.99 o 4 2 1 171.11 171.73 10.09 o 5 2 1 1745.23 1791.92 52.80 o 6 2 1 144.87 137.32 23.09 o 7 2 1 39.59 43.88 16.26 o 8 2 1 15.92 9.87 16.12 o -8 3 1 225.71 185.04 19.42 o -7 3 1 142.49 144.77 13.18 o -6 3 1 335.43 384.83 39.18 o -5 3 1 204.04 201.42 12.12 o -4 3 1 1.48 -5.78 7.82 o -3 3 1 96.57 93.96 7.41 o -2 3 1 848.66 844.67 29.93 o -1 3 1 1978.95 1825.75 143.13 o 0 3 1 0.17 -6.78 6.78 o 1 3 1 10.20 -5.89 7.46 o 2 3 1 1534.83 1558.45 33.31 o 3 3 1 2948.89 3482.00 91.91 o 4 3 1 339.82 357.59 12.64 o 5 3 1 522.53 535.80 24.59 o 6 3 1 4.77 5.68 11.47 o 7 3 1 34.16 23.35 12.01 o -7 4 1 3.56 3.33 11.56 o -6 4 1 2734.80 2778.52 55.85 o -5 4 1 866.78 779.07 26.82 o -4 4 1 16.38 23.12 19.81 o -3 4 1 910.62 984.77 21.60 o -2 4 1 317.44 296.82 9.53 o -1 4 1 310.18 285.48 12.10 o 0 4 1 2048.44 1796.52 47.96 o 1 4 1 76.84 59.20 8.49 o 2 4 1 1256.09 1269.36 36.36 o 3 4 1 77.66 64.42 20.32 o 4 4 1 287.68 315.57 12.59 o 5 4 1 411.65 449.23 34.42 o 6 4 1 3.04 1.19 11.42 o 7 4 1 59.80 61.23 12.77 o -7 5 1 0.78 2.82 12.20 o -6 5 1 259.97 237.91 14.10 o -5 5 1 854.44 828.24 21.76 o -4 5 1 1067.14 1033.95 24.42 o -3 5 1 1565.52 1579.49 32.82 o -2 5 1 123.08 160.80 25.68 o -1 5 1 314.01 308.60 9.39 o 0 5 1 4166.54 3583.75 65.91 o 1 5 1 1036.50 954.06 28.45 o 2 5 1 5253.28 5105.88 132.26 o 3 5 1 351.41 362.65 17.66 o 4 5 1 133.98 115.84 10.96 o 5 5 1 113.60 116.63 15.10 o 6 5 1 957.82 942.44 24.99 o 7 5 1 247.66 221.04 32.93 o -6 6 1 2.15 -6.46 11.47 o -5 6 1 245.54 227.39 50.20 o -4 6 1 2467.43 2430.78 48.70 o -3 6 1 388.51 380.79 13.60 o -2 6 1 38.90 26.69 10.80 o -1 6 1 4.36 7.91 6.87 o 0 6 1 538.50 502.89 18.51 o 1 6 1 95.86 97.13 10.80 o 2 6 1 3744.49 3661.91 97.30 o 3 6 1 10.18 1.92 9.62 o 4 6 1 75.42 85.39 20.89 o 5 6 1 322.41 292.07 14.57 o 6 6 1 34.48 28.01 12.61 o -6 7 1 298.06 305.86 30.90 o -5 7 1 10.06 26.95 11.24 o -4 7 1 32.58 24.53 13.07 o -3 7 1 3494.85 3513.63 67.60 o -2 7 1 680.51 657.48 60.14 o -1 7 1 270.09 261.86 11.03 o 0 7 1 6.77 12.30 7.82 o 1 7 1 37.07 59.54 11.58 o 2 7 1 308.16 318.77 18.31 o 3 7 1 398.87 374.98 18.26 o 4 7 1 194.13 180.98 15.84 o 5 7 1 975.09 964.22 33.05 o 6 7 1 0.02 -12.23 12.23 o -5 8 1 4.12 -12.23 12.23 o -4 8 1 24.53 7.12 25.25 o -3 8 1 1043.10 1072.03 47.46 o -2 8 1 239.39 217.18 11.73 o -1 8 1 2032.80 1830.43 106.42 o 0 8 1 892.51 805.84 28.23 o 1 8 1 1.41 11.39 11.88 o 2 8 1 352.21 346.30 14.14 o 3 8 1 1560.70 1568.85 34.56 o 4 8 1 456.52 433.59 16.73 o 5 8 1 1239.04 1232.28 31.06 o -4 9 1 9.44 4.60 17.83 o -3 9 1 39.22 43.11 11.00 o -2 9 1 0.84 -8.32 9.97 o -1 9 1 178.36 154.73 28.30 o 0 9 1 6.81 -11.42 11.42 o 1 9 1 39.77 40.60 12.60 o 2 9 1 0.22 1.17 14.08 o 3 9 1 371.11 397.21 38.52 o 4 9 1 0.24 -6.64 19.79 o -3 10 1 148.84 180.39 14.26 o -2 10 1 408.32 417.58 15.91 o -1 10 1 520.53 499.46 29.85 o 0 10 1 489.98 444.64 23.51 o 1 10 1 2.85 3.19 13.07 o 2 10 1 480.76 471.61 19.01 o -8 0 2 14.00 53.09 16.68 o -6 0 2 142.97 150.50 17.29 o -4 0 2 5468.64 6405.94 165.00 o -2 0 2 789.53 808.59 23.88 o 0 0 2 1803.94 1894.56 48.50 o 2 0 2 28573.94 28057.89 703.00 o 4 0 2 93.93 94.26 12.56 o 6 0 2 584.03 569.13 25.77 o 8 0 2 2494.64 2353.59 72.47 o -8 1 2 153.93 147.62 19.95 o -7 1 2 38.58 32.57 15.76 o -6 1 2 2352.21 2402.21 64.83 o -5 1 2 6.28 22.83 12.44 o -4 1 2 2184.90 2446.09 66.37 o -3 1 2 11230.69 12963.48 327.06 o -2 1 2 10.17 13.48 7.14 o -1 1 2 6228.75 5793.70 146.00 o 0 1 2 157.12 183.26 7.74 o 1 1 2 123.64 151.97 8.28 o 2 1 2 1422.84 1478.04 40.77 o 3 1 2 34.18 12.20 9.49 o 4 1 2 4.81 13.07 11.17 o 5 1 2 518.92 508.80 22.73 o 6 1 2 628.81 585.86 25.99 o 7 1 2 1086.27 1112.06 39.63 o 8 1 2 74.56 79.39 18.98 o -8 2 2 57.48 73.48 37.32 o -7 2 2 1131.44 1118.72 39.57 o -6 2 2 2855.36 2885.56 106.07 o -5 2 2 100.79 102.50 17.29 o -4 2 2 17.65 22.04 7.29 o -3 2 2 1023.02 1054.29 22.03 o -2 2 2 552.23 628.31 35.83 o -1 2 2 22605.23 20864.20 369.57 o 0 2 2 12130.41 12324.27 309.32 o 1 2 2 43.74 41.97 8.38 o 2 2 2 160.20 154.63 10.75 o 3 2 2 676.16 780.01 25.43 o 4 2 2 1915.41 1745.44 35.43 o 5 2 2 5.57 40.72 14.66 o 6 2 2 325.89 317.56 27.35 o 7 2 2 11.44 -16.69 16.69 o -8 3 2 5.03 1.45 13.17 o -7 3 2 36.00 24.27 12.06 o -6 3 2 146.09 169.51 19.65 o -5 3 2 571.43 636.51 20.84 o -4 3 2 724.93 726.02 32.62 o -3 3 2 9.65 15.18 6.57 o -2 3 2 19.08 25.38 6.64 o -1 3 2 15945.87 15754.36 909.22 o 0 3 2 648.98 561.42 17.64 o 1 3 2 485.37 501.82 16.90 o 2 3 2 36.42 26.64 9.57 o 3 3 2 767.41 814.22 27.22 o 4 3 2 1.34 -12.72 12.72 o 5 3 2 6955.98 6648.12 425.44 o 6 3 2 12.86 5.77 16.45 o 7 3 2 16.47 49.12 15.80 o -7 4 2 175.27 164.66 13.83 o -6 4 2 187.73 215.44 13.74 o -5 4 2 10.52 6.08 36.39 o -4 4 2 195.06 211.73 10.76 o -3 4 2 306.89 261.45 13.79 o -2 4 2 157.21 187.17 12.83 o -1 4 2 1822.80 1758.00 33.41 o 0 4 2 22.85 28.61 6.86 o 1 4 2 879.37 928.75 27.69 o 2 4 2 2104.27 2165.68 59.15 o 3 4 2 293.27 324.15 15.82 o 4 4 2 347.53 372.38 19.76 o 5 4 2 854.97 934.71 33.81 o 6 4 2 152.28 137.99 13.06 o 7 4 2 30.37 38.40 12.78 o -7 5 2 4.63 -8.38 12.41 o -6 5 2 69.07 86.64 25.90 o -5 5 2 240.26 231.42 12.73 o -4 5 2 346.71 405.37 23.10 o -3 5 2 1235.73 1179.65 25.65 o -2 5 2 43.58 35.49 7.06 o -1 5 2 35.96 42.79 15.15 o 0 5 2 873.26 798.01 24.59 o 1 5 2 911.74 886.30 19.42 o 2 5 2 3.63 -10.52 10.52 o 3 5 2 582.82 638.72 24.45 o 4 5 2 43.08 45.55 10.40 o 5 5 2 172.43 196.27 35.36 o 6 5 2 115.51 112.98 15.61 o 7 5 2 1189.65 1139.90 31.23 o -6 6 2 85.80 104.27 12.39 o -5 6 2 5.46 -10.46 10.46 o -4 6 2 527.81 504.22 33.69 o -3 6 2 1192.40 1207.68 27.01 o -2 6 2 1137.54 1091.96 102.12 o -1 6 2 390.74 349.35 11.00 o 0 6 2 96.93 107.46 7.74 o 1 6 2 6.39 12.98 10.28 o 2 6 2 1311.31 1372.43 40.87 o 3 6 2 401.55 418.79 20.46 o 4 6 2 230.76 238.68 13.06 o 5 6 2 92.06 100.07 11.92 o 6 6 2 357.00 328.82 16.04 o -6 7 2 428.22 441.38 18.32 o -5 7 2 2.99 22.80 10.66 o -4 7 2 7.73 22.08 17.37 o -3 7 2 23.90 40.58 10.20 o -2 7 2 38.42 40.06 9.42 o -1 7 2 179.71 174.02 9.92 o 0 7 2 24.65 34.05 8.07 o 1 7 2 740.64 715.49 53.12 o 2 7 2 117.70 119.99 15.26 o 3 7 2 714.92 725.91 28.54 o 4 7 2 101.07 105.16 15.09 o 5 7 2 529.33 507.25 25.73 o 6 7 2 15.89 43.42 12.15 o -5 8 2 37.67 50.65 21.13 o -4 8 2 336.97 313.04 15.17 o -3 8 2 447.16 442.75 15.93 o -2 8 2 101.06 97.32 12.52 o -1 8 2 0.16 -0.64 8.64 o 0 8 2 357.62 340.23 12.90 o 1 8 2 489.97 505.38 22.51 o 2 8 2 702.33 692.56 27.24 o 3 8 2 1058.31 1059.88 26.14 o 4 8 2 13.32 37.68 10.93 o 5 8 2 182.06 205.41 14.33 o -4 9 2 786.49 834.95 25.06 o -3 9 2 25.34 14.59 11.08 o -2 9 2 84.06 72.07 10.42 o -1 9 2 0.03 8.86 9.52 o 0 9 2 211.74 210.35 11.81 o 1 9 2 583.52 620.64 26.13 o 2 9 2 27.30 15.21 15.11 o 3 9 2 236.76 260.58 19.92 o 4 9 2 82.86 84.43 12.29 o -3 10 2 0.11 10.26 15.35 o -2 10 2 176.55 167.22 12.56 o -1 10 2 364.49 342.85 16.29 o 0 10 2 1320.39 1251.36 45.40 o 1 10 2 15.15 35.55 10.19 o 2 10 2 302.07 286.31 20.57 o -7 0 3 1741.57 1851.39 57.06 o -5 0 3 90.19 97.05 13.99 o -3 0 3 3657.35 4290.64 110.84 o -1 0 3 3733.47 3621.99 92.00 o 1 0 3 1407.60 1333.40 36.01 o 3 0 3 604.21 656.99 22.16 o 5 0 3 261.28 257.82 18.33 o 7 0 3 1767.37 1812.07 56.90 o -8 1 3 24.49 25.70 12.49 o -7 1 3 1024.69 1008.94 51.94 o -6 1 3 628.45 655.41 27.07 o -5 1 3 109.77 147.64 14.71 o -4 1 3 166.17 190.53 12.77 o -3 1 3 2021.37 2287.24 60.75 o -2 1 3 1820.68 1769.34 185.06 o -1 1 3 2664.71 2534.64 65.07 o 0 1 3 3468.57 3548.65 90.52 o 1 1 3 0.63 0.11 7.80 o 2 1 3 1081.20 953.38 28.20 o 3 1 3 103.05 130.11 11.86 o 4 1 3 2021.94 2097.41 58.87 o 5 1 3 41.20 28.18 15.30 o 6 1 3 64.59 45.68 11.55 o 7 1 3 1.65 20.18 16.44 o -8 2 3 1.56 5.63 11.52 o -7 2 3 136.45 123.39 12.94 o -6 2 3 1132.18 1170.28 27.81 o -5 2 3 244.85 255.54 26.60 o -4 2 3 0.60 4.61 7.63 o -3 2 3 5.49 7.24 6.29 o -2 2 3 725.81 752.71 96.03 o -1 2 3 9117.54 8749.93 169.00 o 0 2 3 10983.00 11223.28 431.35 o 1 2 3 2174.01 2205.89 44.04 o 2 2 3 202.46 234.28 12.40 o 3 2 3 263.91 283.08 14.81 o 4 2 3 33.55 43.57 12.44 o 5 2 3 5559.69 5686.79 149.76 o 6 2 3 94.49 87.38 11.46 o 7 2 3 181.43 211.60 20.05 o -7 3 3 114.82 125.60 12.82 o -6 3 3 26.56 32.45 10.97 o -5 3 3 205.83 187.08 11.78 o -4 3 3 2274.64 2414.85 108.65 o -3 3 3 799.85 842.70 18.93 o -2 3 3 137.70 167.03 30.74 o -1 3 3 163.95 153.24 6.20 o 0 3 3 1136.33 1016.39 96.22 o 1 3 3 4722.73 4986.00 127.77 o 2 3 3 147.08 156.79 11.30 o 3 3 3 42.46 7.55 11.78 o 4 3 3 1508.80 1503.47 96.99 o 5 3 3 379.00 387.27 28.93 o 6 3 3 17.75 54.25 16.10 o 7 3 3 350.12 369.91 22.50 o -7 4 3 62.63 86.93 22.18 o -6 4 3 42.37 64.72 12.55 o -5 4 3 1057.81 996.35 24.55 o -4 4 3 6485.58 6371.93 116.90 o -3 4 3 644.01 594.47 27.30 o -2 4 3 420.86 449.87 28.83 o -1 4 3 15.35 28.51 5.42 o 0 4 3 195.05 197.93 15.91 o 1 4 3 2281.42 2320.99 62.23 o 2 4 3 5247.71 5368.47 138.77 o 3 4 3 211.68 243.86 16.35 o 4 4 3 1.47 10.54 10.16 o 5 4 3 536.81 575.42 26.15 o 6 4 3 116.03 114.73 29.59 o 7 4 3 93.52 86.58 19.35 o -7 5 3 446.19 419.62 18.27 o -6 5 3 46.84 39.26 10.87 o -5 5 3 80.09 91.60 11.40 o -4 5 3 4.55 -7.64 9.82 o -3 5 3 562.46 548.37 15.46 o -2 5 3 647.40 635.58 47.39 o -1 5 3 1059.45 930.70 19.84 o 0 5 3 213.51 254.16 14.75 o 1 5 3 511.31 479.00 24.36 o 2 5 3 6388.61 6722.10 122.61 o 3 5 3 560.85 559.30 23.46 o 4 5 3 1505.91 1575.05 121.32 o 5 5 3 23.47 15.80 11.48 o 6 5 3 48.45 57.46 11.63 o -6 6 3 1322.20 1305.65 37.94 o -5 6 3 38.14 22.77 13.50 o -4 6 3 61.78 75.28 10.47 o -3 6 3 189.58 197.79 15.44 o -2 6 3 2227.11 2204.52 177.74 o -1 6 3 663.51 583.02 14.95 o 0 6 3 24.09 17.94 7.35 o 1 6 3 1.04 11.83 13.22 o 2 6 3 203.57 203.57 16.40 o 3 6 3 28.68 36.66 14.13 o 4 6 3 2976.89 3157.57 87.81 o 5 6 3 58.96 37.64 11.99 o 6 6 3 0.68 -10.15 12.18 o -6 7 3 190.52 192.26 14.60 o -5 7 3 4.30 11.40 10.91 o -4 7 3 66.99 56.36 10.85 o -3 7 3 137.93 158.41 15.45 o -2 7 3 230.34 218.86 11.47 o -1 7 3 3467.59 3112.33 74.34 o 0 7 3 383.03 353.92 23.58 o 1 7 3 191.99 234.15 15.91 o 2 7 3 338.57 373.75 13.94 o 3 7 3 166.27 160.14 17.29 o 4 7 3 1.23 -10.24 10.60 o 5 7 3 121.64 137.63 13.03 o -5 8 3 16.35 19.81 11.94 o -4 8 3 986.01 1064.40 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