#------------------------------------------------------------------------------ #$Date: 2016-04-02 20:33:10 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180759 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/80/2008087.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008087_Fobs loop_ _publ_author_name 'Zachara, J.' 'Zimniak, A.' _publ_section_title ; A new polymorph of a carbonyliron complex from tetraphenylhexapentaene: bis(\m~3~,\h^2^,\s^2^-diphenylallenylidene)octacarbonyltriiron ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 58 _journal_page_last 60 _journal_volume 55 _journal_year 1999 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.313(13) _cell_angle_gamma 90.000 _cell_length_a 17.174(3) _cell_length_b 8.9483(16) _cell_length_c 22.132(4) _exptl_crystal_F_000 1560.00 _reflns_d_resolution_high 0.8392 _cod_data_source_file jz1302sup2.hkl _cod_data_source_block 4aza #BEGIN Tags that were not found in dictionaries: _shelx_title ' 4aza in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 301.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 32916.25 34333.07 57.46 o 3 0 0 90714.66 91919.05 124.43 o 4 0 0 23553.62 23498.81 60.93 o 6 0 0 1376.13 1511.66 19.58 o 7 0 0 10816.53 12324.89 57.17 o 8 0 0 1531.34 1409.31 24.95 o 9 0 0 3049.54 2610.67 32.23 o 10 0 0 1319.62 1307.75 27.25 o 11 0 0 10298.23 9936.01 68.45 o 12 0 0 15814.70 15070.19 89.65 o 13 0 0 123.22 130.09 17.27 o 14 0 0 7466.36 7290.25 70.46 o 15 0 0 364.87 347.48 19.06 o 16 0 0 629.71 671.84 22.19 o 17 0 0 1258.23 1355.03 31.13 o 18 0 0 2.62 6.32 15.47 o 19 0 0 0.34 0.69 16.19 o 20 0 0 536.03 557.65 25.96 o 1 1 0 61248.40 62562.94 92.76 o 2 1 0 8184.36 8991.23 25.64 o 3 1 0 45.27 54.51 3.49 o 4 1 0 9120.66 9795.88 40.71 o 5 1 0 4982.85 5045.98 32.02 o 6 1 0 338.34 414.11 9.32 o 7 1 0 1357.22 1348.64 21.97 o 8 1 0 5472.19 5456.09 42.78 o 9 1 0 20.54 17.00 6.64 o 10 1 0 5366.65 5048.55 47.16 o 11 1 0 9701.09 9477.09 67.72 o 12 1 0 891.85 875.11 20.52 o 13 1 0 8505.56 8448.96 71.84 o 14 1 0 6.02 23.48 12.23 o 15 1 0 2352.53 2324.34 46.96 o 16 1 0 332.20 330.14 18.80 o 17 1 0 185.46 210.96 15.99 o 18 1 0 455.37 406.14 20.10 o 20 1 0 77.04 40.62 18.22 o 0 2 0 1864.87 1752.00 17.81 o 1 2 0 39749.32 41004.67 91.76 o 2 2 0 6295.72 6442.67 34.11 o 3 2 0 2238.59 2440.65 22.45 o 4 2 0 1490.87 1540.41 19.51 o 5 2 0 8232.03 8830.69 46.98 o 6 2 0 448.49 528.23 13.00 o 7 2 0 558.59 571.53 12.46 o 8 2 0 1634.06 1780.33 27.87 o 9 2 0 76.75 62.24 8.02 o 10 2 0 1268.15 1227.64 23.04 o 11 2 0 3.00 15.23 8.85 o 12 2 0 167.50 158.98 11.84 o 14 2 0 776.87 742.21 20.81 o 15 2 0 922.92 955.46 26.05 o 17 2 0 0.96 2.19 14.68 o 18 2 0 132.56 130.41 17.39 o 19 2 0 118.26 110.17 18.75 o 1 3 0 818.21 829.01 17.40 o 2 3 0 22556.41 23116.24 66.04 o 3 3 0 1097.89 1133.20 20.26 o 4 3 0 14073.86 14339.43 65.82 o 5 3 0 4241.17 4352.83 38.33 o 6 3 0 2513.12 2629.31 31.65 o 7 3 0 3251.34 3094.15 36.38 o 8 3 0 2361.13 2120.73 32.96 o 9 3 0 98.74 105.67 9.83 o 10 3 0 5040.75 4866.26 51.54 o 11 3 0 2201.54 2025.94 38.72 o 12 3 0 635.15 629.24 18.82 o 13 3 0 3465.99 3530.16 53.21 o 14 3 0 1012.59 1055.75 26.58 o 15 3 0 1077.68 1139.99 29.03 o 16 3 0 281.32 268.61 18.29 o 17 3 0 88.65 96.78 16.70 o 18 3 0 341.25 397.87 20.91 o 19 3 0 70.98 89.14 18.36 o 0 4 0 13395.91 12321.04 67.34 o 1 4 0 6941.02 6823.04 50.33 o 2 4 0 13938.68 14165.87 72.59 o 3 4 0 10498.70 10776.23 64.31 o 4 4 0 75.56 100.68 8.59 o 5 4 0 4766.14 4951.59 46.06 o 6 4 0 2076.92 1947.10 31.52 o 7 4 0 491.49 429.37 13.63 o 8 4 0 821.87 769.65 18.32 o 9 4 0 7083.13 6794.31 62.23 o 10 4 0 1110.08 1055.14 26.58 o 11 4 0 4041.64 3973.34 54.21 o 12 4 0 4760.33 4763.36 61.30 o 13 4 0 283.48 283.40 16.50 o 14 4 0 3384.25 3318.65 58.02 o 15 4 0 548.09 588.79 24.03 o 16 4 0 807.80 807.43 26.71 o 17 4 0 263.75 322.71 20.18 o 18 4 0 28.27 45.35 17.55 o 1 5 0 4899.55 4486.43 47.49 o 2 5 0 706.80 701.19 16.92 o 3 5 0 5556.40 5661.00 53.54 o 4 5 0 8050.17 7938.04 63.65 o 5 5 0 1192.54 1248.68 24.85 o 6 5 0 1009.72 1065.13 23.71 o 7 5 0 43.91 68.91 9.65 o 8 5 0 3816.30 3710.39 50.13 o 9 5 0 433.47 459.32 16.41 o 10 5 0 3829.13 3805.75 55.09 o 11 5 0 1474.01 1499.79 33.52 o 12 5 0 312.96 337.27 16.79 o 13 5 0 1347.45 1371.21 31.28 o 14 5 0 61.03 46.98 15.46 o 15 5 0 1768.16 1759.69 41.92 o 16 5 0 776.09 750.63 28.21 o 17 5 0 155.55 166.92 19.18 o 0 6 0 1574.45 1567.53 28.10 o 1 6 0 187.62 173.91 11.42 o 2 6 0 1712.19 1671.66 29.37 o 3 6 0 131.48 176.14 12.11 o 4 6 0 419.06 413.43 14.74 o 5 6 0 0.09 1.91 9.81 o 6 6 0 159.57 179.13 12.92 o 7 6 0 86.66 100.10 12.19 o 8 6 0 156.56 162.61 13.14 o 9 6 0 0.46 -4.79 11.78 o 10 6 0 209.35 210.41 15.44 o 11 6 0 19.50 21.10 13.30 o 12 6 0 19.49 38.95 14.26 o 13 6 0 7.91 1.30 14.76 o 14 6 0 252.20 287.21 19.61 o 15 6 0 27.79 40.39 16.51 o 16 6 0 66.66 69.93 18.26 o 1 7 0 1488.54 1469.37 31.80 o 2 7 0 296.93 290.24 14.19 o 3 7 0 152.24 135.95 12.98 o 4 7 0 518.80 533.36 19.95 o 5 7 0 548.36 606.96 19.09 o 6 7 0 130.68 155.42 14.87 o 7 7 0 774.39 844.54 24.15 o 8 7 0 528.69 537.78 20.82 o 9 7 0 339.27 347.71 18.43 o 10 7 0 2160.81 2133.73 43.58 o 11 7 0 1033.93 955.77 28.10 o 12 7 0 37.79 37.25 16.08 o 13 7 0 172.48 160.12 18.65 o 14 7 0 14.53 22.08 17.04 o 15 7 0 185.57 163.33 20.46 o 0 8 0 2969.85 2817.33 55.27 o 1 8 0 127.48 145.16 15.26 o 2 8 0 2196.63 2174.88 42.02 o 3 8 0 1834.77 1854.65 40.21 o 4 8 0 315.59 332.29 18.37 o 5 8 0 1095.23 1120.87 32.00 o 6 8 0 132.69 165.74 17.65 o 7 8 0 15.01 26.77 16.06 o 8 8 0 222.88 256.20 20.42 o 9 8 0 845.88 881.59 29.23 o 10 8 0 694.87 700.46 26.97 o 11 8 0 431.99 432.90 23.68 o 12 8 0 823.20 871.63 31.77 o 13 8 0 136.76 114.95 21.69 o 1 9 0 911.38 908.01 27.22 o 2 9 0 70.39 91.11 15.86 o 3 9 0 541.99 511.84 21.35 o 4 9 0 302.31 281.29 19.26 o 5 9 0 273.61 264.11 18.80 o 6 9 0 2.62 -8.00 16.37 o 7 9 0 13.30 20.71 17.26 o 8 9 0 143.83 176.44 18.57 o 9 9 0 215.62 213.24 20.82 o 10 9 0 140.43 112.17 21.41 o 0 10 0 542.35 489.64 23.24 o 1 10 0 11.21 33.33 17.44 o 2 10 0 42.23 42.20 17.67 o 3 10 0 5.25 5.36 17.67 o 4 10 0 286.18 277.98 20.91 o 5 10 0 59.09 43.46 18.69 o 6 10 0 48.99 72.08 19.54 o 7 10 0 2.80 -3.05 19.74 o -20 1 1 284.77 308.41 21.76 o -19 1 1 112.18 69.51 17.45 o -18 1 1 378.78 357.95 19.57 o -17 1 1 2.10 4.59 14.30 o -16 1 1 242.56 286.51 16.62 o -15 1 1 594.16 497.03 20.70 o -14 1 1 1501.90 1347.20 31.94 o -12 1 1 170.52 173.98 11.50 o -11 1 1 255.95 270.31 11.97 o -10 1 1 1261.56 1221.75 26.74 o -9 1 1 0.77 1.36 6.40 o -8 1 1 5891.75 6334.07 45.44 o -7 1 1 2311.18 2605.61 28.18 o -6 1 1 1151.46 1164.89 18.53 o -5 1 1 25027.30 25921.13 74.06 o -4 1 1 11.14 7.98 3.51 o -3 1 1 9217.77 9843.71 37.45 o -2 1 1 1416.73 1618.58 13.92 o -1 1 1 11167.95 11376.65 34.45 o 0 1 1 8608.76 8834.91 245.40 o 1 1 1 2432.20 2649.00 15.33 o 2 1 1 1462.21 1715.93 13.93 o 3 1 1 13315.16 12654.97 34.85 o 4 1 1 4716.05 4587.29 28.13 o 5 1 1 8549.41 8879.15 42.62 o 6 1 1 7.82 11.86 4.47 o 7 1 1 5045.28 4980.31 38.13 o 8 1 1 54.60 69.37 6.85 o 9 1 1 3831.67 3876.32 39.47 o 10 1 1 593.09 572.49 15.59 o 11 1 1 197.07 208.66 12.37 o 12 1 1 545.34 518.72 16.49 o 13 1 1 365.71 371.17 15.71 o 14 1 1 366.30 372.43 16.69 o 15 1 1 6.96 10.84 12.35 o 16 1 1 11.62 29.43 13.28 o 17 1 1 112.84 128.70 15.44 o 18 1 1 0.27 -6.66 15.35 o 19 1 1 103.86 123.25 18.08 o -19 2 1 404.44 472.64 22.17 o -18 2 1 183.76 204.15 17.84 o -17 2 1 698.86 607.26 23.88 o -16 2 1 33.64 39.24 13.55 o -15 2 1 623.83 695.98 21.43 o -14 2 1 30.09 41.57 11.88 o -13 2 1 1761.99 1711.83 31.64 o -12 2 1 66.79 85.82 10.48 o -11 2 1 259.14 255.08 12.26 o -10 2 1 1358.34 1290.52 23.21 o -9 2 1 4684.82 4925.71 45.84 o -8 2 1 2986.41 2996.44 34.69 o -7 2 1 6429.54 6689.10 46.80 o -6 2 1 74.91 56.62 5.83 o -5 2 1 4851.99 4928.38 35.68 o -4 2 1 5932.03 6239.87 37.69 o -3 2 1 5894.18 6378.50 36.24 o -2 2 1 883.67 911.05 14.39 o -1 2 1 16745.90 17382.40 46.41 o 0 2 1 8882.55 9468.27 99.75 o 1 2 1 190.81 256.79 6.35 o 2 2 1 795.52 908.68 14.04 o 3 2 1 18417.07 19070.27 50.75 o 4 2 1 3175.56 3372.10 27.78 o 5 2 1 50.53 38.62 4.96 o 6 2 1 3568.92 3561.43 32.65 o 7 2 1 7.89 4.35 5.75 o 8 2 1 4904.12 4846.22 42.99 o 9 2 1 7165.45 7303.63 55.31 o 10 2 1 4489.54 4368.61 46.79 o 11 2 1 3889.15 3846.97 46.43 o 12 2 1 208.69 187.69 12.35 o 13 2 1 179.39 179.48 13.15 o 14 2 1 1240.50 1203.65 26.17 o 15 2 1 216.77 214.92 14.77 o 16 2 1 233.73 236.85 16.66 o 17 2 1 2.45 -14.97 14.97 o 18 2 1 1479.68 1511.41 35.66 o 19 2 1 46.75 50.98 19.27 o -19 3 1 6.21 -16.75 17.63 o -18 3 1 966.02 949.77 28.93 o -17 3 1 39.30 51.20 15.44 o -16 3 1 1006.51 1051.66 29.39 o -15 3 1 383.98 399.26 19.49 o -14 3 1 735.55 759.12 22.01 o -13 3 1 8.56 8.75 11.62 o -12 3 1 14.58 10.22 10.70 o -11 3 1 1677.44 1624.07 35.36 o -10 3 1 8.47 30.71 8.87 o -9 3 1 2787.32 2739.92 37.84 o -8 3 1 1105.98 1064.93 20.71 o -7 3 1 6457.04 6262.16 49.87 o -6 3 1 4150.47 4095.01 38.91 o -5 3 1 3098.46 3201.99 33.35 o -4 3 1 3208.92 3110.37 32.09 o -3 3 1 682.09 770.97 14.69 o -2 3 1 18884.21 19680.02 74.75 o -1 3 1 39359.38 38867.00 108.53 o 0 3 1 533.73 633.81 8.94 o 1 3 1 204.71 192.56 6.83 o 2 3 1 521.60 589.67 12.75 o 3 3 1 14866.25 15526.13 66.19 o 4 3 1 204.35 262.59 9.01 o 5 3 1 8981.25 9366.18 54.58 o 6 3 1 7.18 4.81 6.21 o 7 3 1 1681.38 1578.43 28.22 o 8 3 1 3274.96 3154.29 38.54 o 9 3 1 158.69 183.74 10.50 o 10 3 1 2002.75 2026.07 36.40 o 11 3 1 468.00 461.54 16.35 o 12 3 1 1146.39 1125.09 27.50 o 13 3 1 16.37 18.79 11.86 o 14 3 1 57.59 63.33 13.71 o 15 3 1 524.81 555.59 22.57 o 16 3 1 490.47 428.00 20.67 o 17 3 1 1235.53 1237.72 32.71 o 18 3 1 51.85 38.91 16.90 o 19 3 1 1060.70 1019.98 32.07 o -18 4 1 0.46 27.54 17.14 o -17 4 1 73.03 76.35 18.24 o -16 4 1 103.34 97.80 17.27 o -15 4 1 0.31 -2.96 15.19 o -14 4 1 442.75 464.39 20.65 o -13 4 1 1154.38 1209.98 28.32 o -12 4 1 338.39 351.29 16.93 o -11 4 1 101.88 107.17 12.49 o -10 4 1 527.08 511.08 17.43 o -9 4 1 390.68 414.87 15.41 o -8 4 1 865.21 962.02 22.79 o -7 4 1 1081.73 939.41 21.46 o -6 4 1 878.23 952.02 20.84 o -5 4 1 3500.02 3498.88 39.81 o -4 4 1 125.04 96.73 8.45 o -3 4 1 2074.41 2094.43 30.74 o -2 4 1 1267.80 1355.46 25.58 o -1 4 1 461.16 522.64 13.31 o 0 4 1 282.83 279.15 7.06 o 1 4 1 352.52 372.94 11.88 o 2 4 1 407.41 385.56 12.53 o 3 4 1 2796.22 2924.84 35.10 o 4 4 1 6284.54 6387.61 50.40 o 5 4 1 1583.29 1541.03 28.68 o 6 4 1 3719.42 3727.70 42.02 o 7 4 1 1862.20 1686.08 31.57 o 8 4 1 167.97 182.44 10.93 o 9 4 1 2380.83 2415.48 40.38 o 10 4 1 511.94 470.60 17.75 o 11 4 1 650.14 689.36 22.52 o 12 4 1 0.29 -2.40 12.31 o 13 4 1 3.21 -6.64 13.18 o 14 4 1 162.31 157.42 16.17 o 15 4 1 950.51 945.72 26.29 o 16 4 1 115.70 139.14 17.02 o 17 4 1 109.75 69.33 17.57 o 18 4 1 334.10 322.42 21.97 o -17 5 1 66.77 49.35 17.67 o -16 5 1 72.71 63.04 17.89 o -15 5 1 190.97 200.17 19.44 o -14 5 1 724.39 672.18 24.89 o -13 5 1 100.96 103.45 15.38 o -12 5 1 110.51 106.40 14.04 o -11 5 1 129.14 119.12 13.51 o -10 5 1 311.58 295.28 14.84 o -9 5 1 6.25 3.19 10.44 o -8 5 1 201.06 243.44 12.54 o -7 5 1 76.01 88.34 10.20 o -6 5 1 512.14 496.75 15.50 o -5 5 1 4135.73 4143.62 48.53 o -4 5 1 801.60 791.23 18.57 o -3 5 1 4638.05 4653.77 49.59 o -2 5 1 24.72 28.66 8.73 o -1 5 1 49.68 34.55 8.29 o 0 5 1 541.28 497.75 20.58 o 1 5 1 63.45 83.44 8.37 o 2 5 1 680.52 648.23 16.61 o 3 5 1 297.20 281.93 11.77 o 4 5 1 311.38 325.03 12.30 o 5 5 1 678.35 684.61 17.89 o 6 5 1 907.93 934.31 19.96 o 7 5 1 1313.65 1226.91 26.38 o 8 5 1 132.17 130.87 11.66 o 9 5 1 2547.32 2604.83 44.93 o 10 5 1 91.98 86.96 13.32 o 11 5 1 924.70 955.24 26.54 o 12 5 1 325.21 310.78 16.95 o 13 5 1 30.30 33.12 14.16 o 14 5 1 283.35 282.16 18.35 o 15 5 1 21.19 30.12 15.62 o 16 5 1 6.75 -3.84 16.21 o 17 5 1 2.34 2.78 16.84 o -16 6 1 19.22 56.40 17.59 o -15 6 1 60.31 99.56 17.22 o -14 6 1 47.47 96.65 16.31 o -13 6 1 7.35 21.22 15.27 o -12 6 1 205.37 210.97 16.50 o -11 6 1 308.81 340.33 17.05 o -10 6 1 4.15 -4.08 12.49 o -9 6 1 263.12 246.53 14.98 o -8 6 1 208.80 246.24 14.53 o -7 6 1 659.89 607.92 18.88 o -6 6 1 518.64 556.98 17.96 o -5 6 1 544.85 534.19 17.53 o -4 6 1 1534.28 1537.48 29.92 o -3 6 1 3257.87 3193.51 47.17 o -1 6 1 628.39 546.84 16.11 o 0 6 1 14.81 19.93 6.30 o 1 6 1 2180.84 2226.28 39.53 o 2 6 1 17.27 22.06 9.32 o 3 6 1 634.52 644.25 17.29 o 4 6 1 413.92 346.29 14.39 o 5 6 1 69.85 91.48 10.93 o 6 6 1 1961.70 1872.01 32.62 o 7 6 1 108.59 140.37 12.37 o 8 6 1 1709.58 1699.24 33.77 o 9 6 1 383.70 388.23 16.02 o 10 6 1 573.03 583.72 19.22 o 11 6 1 15.99 38.08 13.53 o 12 6 1 71.33 54.05 15.17 o 13 6 1 53.22 59.93 15.27 o 14 6 1 5.24 3.72 15.50 o 15 6 1 0.24 8.47 16.29 o 16 6 1 243.64 226.23 20.36 o -15 7 1 194.29 172.49 20.29 o -14 7 1 18.17 6.86 17.73 o -13 7 1 256.66 273.15 19.53 o -11 7 1 245.15 250.64 19.32 o -10 7 1 604.37 594.16 22.57 o -9 7 1 761.24 825.19 24.90 o -8 7 1 558.04 625.03 22.53 o -7 7 1 817.98 854.98 24.07 o -6 7 1 2134.63 2126.47 39.01 o -5 7 1 155.53 163.95 14.02 o -4 7 1 2099.17 1987.15 36.91 o -3 7 1 211.29 186.02 14.35 o -2 7 1 10.27 21.24 11.21 o -1 7 1 3.16 4.35 10.82 o 0 7 1 5.71 19.71 7.71 o 1 7 1 234.46 296.43 14.14 o 2 7 1 98.43 106.14 12.53 o 3 7 1 2333.80 2260.22 45.96 o 4 7 1 542.32 551.74 19.97 o 5 7 1 3154.02 3152.72 54.60 o 6 7 1 1615.65 1678.26 36.51 o 7 7 1 649.25 630.90 22.96 o 8 7 1 1882.45 1917.42 39.85 o 9 7 1 40.07 21.33 14.42 o 10 7 1 524.68 535.85 22.53 o 11 7 1 5.66 -4.10 15.80 o 12 7 1 54.80 44.64 17.83 o 13 7 1 114.90 134.91 18.42 o 14 7 1 18.55 22.91 17.79 o 15 7 1 197.44 238.80 21.29 o -13 8 1 111.26 118.99 20.58 o -12 8 1 23.32 47.46 19.13 o -11 8 1 83.97 85.55 19.01 o -10 8 1 674.35 687.93 26.48 o -9 8 1 605.27 607.22 24.91 o -8 8 1 1645.95 1688.98 42.49 o -7 8 1 1265.68 1287.63 33.21 o -6 8 1 124.09 172.56 17.49 o -5 8 1 2400.69 2394.92 45.73 o -4 8 1 45.02 39.56 15.70 o -3 8 1 62.27 76.08 15.21 o -2 8 1 721.85 691.85 24.10 o -1 8 1 727.14 744.39 23.66 o 0 8 1 8.60 28.23 12.29 o 1 8 1 890.14 834.99 24.79 o 2 8 1 393.01 392.90 19.86 o 3 8 1 31.05 39.20 15.19 o 4 8 1 1875.52 1886.22 41.83 o 5 8 1 673.00 800.80 25.95 o 6 8 1 1059.15 1032.30 31.28 o 7 8 1 1787.42 1722.58 42.30 o 8 8 1 65.19 72.26 17.02 o 9 8 1 897.43 899.80 29.56 o 10 8 1 61.94 72.53 19.58 o 11 8 1 5.69 18.32 18.42 o 12 8 1 95.42 78.50 20.53 o 13 8 1 328.84 348.02 24.71 o -10 9 1 27.67 23.86 19.37 o -9 9 1 400.66 393.98 23.88 o -8 9 1 194.77 194.42 19.81 o -7 9 1 86.60 89.29 17.39 o -6 9 1 605.12 533.05 24.62 o -5 9 1 283.67 304.65 19.02 o -4 9 1 310.69 255.78 20.36 o -3 9 1 162.40 150.04 17.75 o -2 9 1 56.80 42.59 15.62 o -1 9 1 73.59 107.32 15.29 o 0 9 1 144.36 125.52 11.55 o 1 9 1 128.92 135.73 16.01 o 2 9 1 171.33 168.55 17.51 o 3 9 1 37.51 45.45 16.09 o 4 9 1 31.37 22.48 16.55 o 5 9 1 991.02 1007.40 29.46 o 6 9 1 31.25 27.28 16.59 o 7 9 1 42.74 46.20 17.10 o 8 9 1 152.14 155.36 19.72 o 9 9 1 83.33 83.70 19.07 o 10 9 1 0.50 -1.69 19.09 o -7 10 1 81.28 97.55 19.88 o -6 10 1 217.53 203.38 21.31 o -5 10 1 84.47 111.22 18.75 o -4 10 1 15.05 18.44 17.91 o -3 10 1 281.73 265.38 20.46 o -2 10 1 0.74 2.32 17.16 o -1 10 1 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