#------------------------------------------------------------------------------ #$Date: 2016-04-02 20:33:16 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180760 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/81/2008110.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008110_Fobs loop_ _publ_author_name 'Plenio, H.' 'Diodone, R.' _publ_section_title ; A cylindrical macrocycle with two diaza-18-crown-6 macrocycles encapsulating two silver cations ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first IUC9800081 _journal_volume 55 _journal_year 1999 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.370 _cell_angle_gamma 90.000 _cell_length_a 11.1500 _cell_length_b 9.0280 _cell_length_c 25.6370 _exptl_crystal_F_000 1336.00 _reflns_d_resolution_high 0.8112 _cod_data_source_file qa0077sup2.hkl _cod_data_source_block rd24 #BEGIN Tags that were not found in dictionaries: _shelx_title ' rd24 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 286.36 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 972.97 1124.50 8.47 o 4 0 0 39193.16 37641.16 171.64 o 6 0 0 15738.42 15587.95 52.62 o 8 0 0 585.37 726.79 17.19 o 10 0 0 4765.32 4800.16 41.70 o 12 0 0 4.12 0.00 11.92 o 1 1 0 22462.83 23826.32 386.87 o 2 1 0 11747.25 11482.90 159.95 o 3 1 0 166.31 235.96 4.30 o 4 1 0 3916.71 4192.85 22.65 o 5 1 0 7813.39 7413.50 45.94 o 6 1 0 5163.70 4992.52 43.36 o 7 1 0 3155.00 3127.86 41.41 o 8 1 0 856.06 821.10 23.79 o 9 1 0 1381.14 1378.83 22.46 o 10 1 0 10.71 4.90 14.58 o 11 1 0 1505.95 1541.80 27.21 o 12 1 0 801.96 815.10 17.08 o 13 1 0 143.91 172.09 7.50 o 0 2 0 1395.54 1747.03 17.79 o 1 2 0 6412.22 7180.53 38.01 o 2 2 0 3765.77 4099.14 19.42 o 3 2 0 12587.47 13087.93 37.96 o 4 2 0 196.82 182.93 3.42 o 5 2 0 16.68 15.57 2.62 o 6 2 0 280.77 249.03 9.95 o 7 2 0 7287.84 7225.82 51.47 o 8 2 0 17.84 32.18 3.87 o 9 2 0 1827.93 1795.50 25.42 o 10 2 0 514.12 521.69 9.96 o 11 2 0 168.46 194.75 5.95 o 12 2 0 68.83 65.82 5.56 o 13 2 0 1071.63 1059.42 19.76 o 1 3 0 44077.93 45382.82 298.18 o 2 3 0 6596.70 6725.96 28.67 o 3 3 0 820.25 854.23 25.36 o 4 3 0 498.86 573.52 8.05 o 5 3 0 8519.88 8343.06 75.01 o 6 3 0 2603.20 2467.28 58.25 o 7 3 0 2449.60 2501.38 26.10 o 8 3 0 342.84 329.72 5.59 o 9 3 0 2020.80 1978.77 27.30 o 10 3 0 61.34 66.21 13.84 o 11 3 0 1151.95 1198.11 20.67 o 12 3 0 324.97 344.01 7.39 o 13 3 0 0.25 0.00 14.61 o 0 4 0 39289.52 41778.40 116.71 o 1 4 0 1468.49 1510.05 16.03 o 2 4 0 2279.46 2203.81 19.42 o 3 4 0 961.14 932.03 14.01 o 4 4 0 3245.94 3308.11 25.92 o 5 4 0 775.88 709.84 10.26 o 6 4 0 9722.94 9892.16 49.65 o 7 4 0 321.75 342.77 6.42 o 8 4 0 9.69 11.86 9.29 o 9 4 0 73.17 69.13 5.01 o 10 4 0 4262.94 4180.61 68.36 o 11 4 0 400.29 409.67 10.31 o 12 4 0 40.70 33.48 6.41 o 1 5 0 146.88 159.70 4.88 o 2 5 0 2990.93 2820.85 26.88 o 3 5 0 4.99 0.00 7.38 o 4 5 0 1939.74 1768.96 51.99 o 5 5 0 11.42 19.07 3.69 o 6 5 0 486.99 457.70 8.29 o 7 5 0 801.87 817.24 13.25 o 8 5 0 655.43 620.67 19.46 o 9 5 0 42.59 44.74 7.54 o 10 5 0 87.03 79.24 21.46 o 11 5 0 142.61 137.33 10.13 o 12 5 0 820.32 777.87 25.16 o 0 6 0 840.66 1019.73 26.60 o 1 6 0 42.88 62.09 3.44 o 2 6 0 241.26 301.86 6.29 o 3 6 0 3315.37 3246.10 54.67 o 4 6 0 2179.16 2257.79 54.85 o 5 6 0 141.94 129.97 4.74 o 6 6 0 2398.21 2419.55 30.02 o 7 6 0 502.81 496.57 9.42 o 8 6 0 89.79 76.32 6.79 o 9 6 0 6.87 3.42 27.37 o 10 6 0 496.91 477.57 8.99 o 11 6 0 91.19 83.81 6.84 o 1 7 0 4899.45 4831.50 127.36 o 2 7 0 146.97 103.02 4.56 o 3 7 0 1379.25 1338.08 22.51 o 4 7 0 32.60 35.98 4.55 o 5 7 0 3737.47 3717.18 50.24 o 6 7 0 16.06 0.00 12.20 o 7 7 0 848.64 914.57 16.27 o 8 7 0 414.27 361.26 7.50 o 9 7 0 825.49 765.85 16.83 o 10 7 0 36.54 57.32 6.62 o 0 8 0 2688.61 2390.06 48.39 o 1 8 0 1642.93 1729.29 89.79 o 2 8 0 54.99 80.98 7.79 o 3 8 0 2124.19 2122.79 30.70 o 4 8 0 240.56 190.21 8.69 o 5 8 0 96.46 79.35 5.32 o 6 8 0 609.15 546.54 13.75 o 7 8 0 424.44 468.24 8.44 o 8 8 0 8.62 6.08 7.03 o 9 8 0 12.35 0.00 14.30 o 1 9 0 104.12 165.87 6.01 o 2 9 0 321.49 384.34 20.19 o 3 9 0 40.53 14.82 7.07 o 4 9 0 505.82 548.58 9.73 o 5 9 0 350.98 390.52 11.92 o 6 9 0 110.02 120.12 9.68 o 7 9 0 2.33 18.97 8.56 o 8 9 0 606.57 601.28 11.52 o 0 10 0 367.29 367.78 12.52 o 1 10 0 37.21 50.99 5.83 o 2 10 0 195.30 211.52 11.25 o 3 10 0 126.86 136.38 7.78 o 4 10 0 897.66 908.53 34.41 o 5 10 0 0.75 0.00 30.08 o 6 10 0 646.98 664.09 11.34 o 1 11 0 301.25 270.62 18.99 o 2 11 0 560.97 519.80 15.41 o -13 0 1 603.25 561.85 17.59 o -11 0 1 5969.16 5875.35 70.16 o -9 0 1 0.92 0.00 13.30 o -7 0 1 443.01 355.99 8.79 o -5 0 1 2651.38 3094.03 30.69 o -3 0 1 1281.62 1314.09 15.71 o 3 0 1 1959.43 1671.43 17.90 o 5 0 1 11366.88 12039.58 59.34 o 7 0 1 15.70 15.55 4.11 o 9 0 1 1755.55 1735.55 34.48 o 11 0 1 48.45 49.04 7.25 o 13 0 1 428.26 441.27 12.48 o -13 1 1 338.28 347.01 12.21 o -12 1 1 76.27 3.25 18.61 o -11 1 1 405.03 432.51 12.34 o -10 1 1 698.85 706.06 18.65 o -9 1 1 4832.45 4894.76 55.24 o -8 1 1 263.50 259.04 7.33 o -7 1 1 165.07 189.71 5.97 o -6 1 1 1843.73 1725.12 26.22 o -5 1 1 15982.70 15356.04 68.03 o -4 1 1 224.78 215.56 5.76 o -3 1 1 9481.46 8539.68 39.61 o -2 1 1 6831.70 7656.57 31.96 o -1 1 1 9158.59 9842.12 29.91 o 0 1 1 13529.83 12881.10 33.15 o 1 1 1 48544.61 45398.14 17.61 o 2 1 1 104.44 74.62 2.56 o 3 1 1 208.51 169.24 4.70 o 4 1 1 18272.81 18229.67 66.10 o 5 1 1 5921.93 5936.02 42.95 o 6 1 1 9.12 24.28 4.15 o 7 1 1 5029.92 4989.94 47.76 o 8 1 1 7436.92 7184.04 61.72 o 9 1 1 1192.01 1156.61 29.31 o 10 1 1 372.47 400.79 9.94 o 11 1 1 1486.42 1533.35 39.35 o 12 1 1 559.61 576.87 14.41 o 13 1 1 295.69 285.55 11.95 o -13 2 1 12.08 0.00 21.48 o -12 2 1 18.03 0.00 16.58 o -11 2 1 0.20 0.00 16.43 o -10 2 1 1432.63 1367.77 34.63 o -9 2 1 45.91 34.07 6.10 o -8 2 1 4219.29 4300.96 49.15 o -7 2 1 15.17 0.43 11.47 o -6 2 1 141.41 96.46 4.53 o -5 2 1 4008.48 4233.90 37.94 o -4 2 1 25375.89 24640.89 81.49 o -3 2 1 10.11 1.49 6.54 o -2 2 1 7010.19 6813.28 35.18 o -1 2 1 15.43 20.54 2.30 o 0 2 1 14655.29 16044.88 51.53 o 1 2 1 14513.59 14766.83 47.76 o 2 2 1 14508.57 13787.92 50.02 o 3 2 1 2627.44 2761.89 25.62 o 4 2 1 1553.83 1471.81 21.46 o 5 2 1 140.72 141.81 4.64 o 6 2 1 21033.76 21002.37 90.85 o 7 2 1 1791.30 1792.22 30.52 o 8 2 1 950.10 997.81 26.33 o 9 2 1 941.73 875.44 19.15 o 10 2 1 361.52 363.30 11.05 o 11 2 1 61.81 61.28 7.20 o 12 2 1 736.88 756.50 23.01 o 13 2 1 75.04 49.62 9.67 o -13 3 1 263.41 237.50 11.95 o -12 3 1 956.48 967.60 25.06 o -11 3 1 319.87 337.37 9.73 o -10 3 1 1496.76 1476.39 37.32 o -9 3 1 140.01 135.45 6.87 o -8 3 1 167.82 177.95 6.38 o -7 3 1 432.91 452.26 13.36 o -6 3 1 6889.77 6636.44 54.36 o -5 3 1 987.33 912.19 20.39 o -4 3 1 961.89 915.64 18.91 o -3 3 1 89.65 100.61 3.68 o -2 3 1 19356.38 19804.93 68.95 o -1 3 1 175.23 178.71 4.12 o 0 3 1 13725.10 14058.29 59.30 o 1 3 1 13.81 17.32 3.01 o 2 3 1 4082.71 4145.75 32.45 o 3 3 1 581.82 538.06 14.48 o 4 3 1 13130.52 13467.78 66.03 o 5 3 1 82.94 93.69 4.58 o 6 3 1 370.25 392.57 9.70 o 7 3 1 462.00 486.17 13.83 o 8 3 1 3628.53 3654.37 47.27 o 9 3 1 385.18 376.73 11.09 o 10 3 1 1893.77 1860.44 40.92 o 11 3 1 448.03 464.66 13.47 o 12 3 1 251.01 291.36 9.95 o 13 3 1 308.07 320.67 12.81 o -12 4 1 30.62 0.00 20.55 o -11 4 1 2367.19 2413.57 50.90 o -10 4 1 1449.78 1488.80 38.85 o -9 4 1 239.27 251.72 8.36 o -8 4 1 727.35 739.31 17.54 o -7 4 1 1604.10 1597.44 31.87 o -6 4 1 2340.56 2229.64 35.10 o -5 4 1 3679.56 3319.79 38.90 o -4 4 1 4347.17 4147.04 40.51 o -3 4 1 2734.02 2947.61 32.35 o -2 4 1 4037.72 4634.92 38.85 o -1 4 1 10143.74 10034.62 54.71 o 0 4 1 8735.37 9042.32 55.97 o 1 4 1 938.70 968.70 19.46 o 2 4 1 1326.73 1324.61 22.61 o 3 4 1 7796.72 7726.22 52.21 o 5 4 1 2372.96 2403.39 33.63 o 6 4 1 204.83 211.34 6.43 o 7 4 1 27.43 49.59 5.50 o 8 4 1 1014.73 961.74 20.12 o 9 4 1 1890.32 1899.44 40.19 o 10 4 1 203.67 193.88 9.10 o 11 4 1 14.50 10.68 18.75 o 12 4 1 222.58 234.07 11.27 o -12 5 1 55.56 58.51 9.86 o -11 5 1 161.72 150.28 8.91 o -10 5 1 10.58 0.00 19.03 o -9 5 1 2348.67 2410.29 45.84 o -8 5 1 57.59 75.48 6.30 o -7 5 1 3.07 11.83 5.53 o -6 5 1 783.21 775.25 17.18 o -5 5 1 5232.57 5583.57 53.87 o -4 5 1 0.48 0.00 10.65 o -3 5 1 6035.47 6134.78 51.50 o -2 5 1 946.22 887.39 20.99 o -1 5 1 372.66 429.11 11.14 o 0 5 1 8.89 20.12 4.73 o 1 5 1 25495.26 26277.98 100.83 o 2 5 1 1007.90 1023.62 22.58 o 3 5 1 4070.84 3954.58 42.18 o 4 5 1 271.36 230.46 6.22 o 5 5 1 6305.80 6560.37 58.81 o 6 5 1 310.79 291.94 8.12 o 7 5 1 2982.08 3010.48 45.65 o 8 5 1 95.17 90.20 6.91 o 9 5 1 20.60 3.56 17.10 o 10 5 1 69.78 45.84 8.28 o 11 5 1 1276.15 1327.00 29.27 o 12 5 1 44.03 40.00 10.05 o -11 6 1 167.66 185.39 10.71 o -10 6 1 670.42 615.05 17.37 o -9 6 1 178.08 216.10 8.71 o -8 6 1 664.01 687.49 20.41 o -7 6 1 1253.04 1185.95 32.70 o -6 6 1 78.03 106.61 6.74 o -5 6 1 2798.56 2790.12 42.45 o -4 6 1 4391.02 4204.04 49.23 o -3 6 1 16.47 19.18 4.85 o -2 6 1 8.74 25.59 4.77 o -1 6 1 2608.54 2480.81 35.57 o 0 6 1 405.40 372.95 9.43 o 1 6 1 0.63 0.00 11.04 o 2 6 1 3591.31 3546.72 43.32 o 3 6 1 3751.76 3727.71 45.30 o 4 6 1 47.07 45.43 5.78 o 5 6 1 1031.31 1026.00 28.28 o 6 6 1 3082.69 3217.87 48.08 o 7 6 1 1713.15 1785.85 39.89 o 8 6 1 88.77 72.81 7.89 o 9 6 1 1212.49 1277.33 27.12 o 10 6 1 270.58 256.25 10.14 o 11 6 1 4.00 9.57 19.66 o -10 7 1 221.09 220.68 10.99 o -9 7 1 93.42 106.96 8.43 o -8 7 1 567.13 576.22 16.60 o -7 7 1 34.74 41.55 7.55 o -6 7 1 2351.04 2471.39 46.17 o -5 7 1 212.56 246.68 8.42 o -4 7 1 8.41 0.00 14.10 o -3 7 1 49.28 62.50 6.24 o -2 7 1 3162.25 3249.47 45.30 o -1 7 1 63.83 82.51 6.22 o 0 7 1 281.95 292.20 8.17 o 1 7 1 35.81 11.77 5.78 o 2 7 1 577.77 658.31 16.77 o 3 7 1 0.24 0.00 6.29 o 4 7 1 2930.98 2924.01 45.80 o 5 7 1 6.93 22.76 6.72 o 6 7 1 844.59 839.45 21.82 o 7 7 1 259.49 299.69 9.86 o 8 7 1 1358.25 1524.84 41.77 o 9 7 1 275.29 245.18 10.13 o 10 7 1 419.55 406.09 13.32 o -9 8 1 18.39 25.89 9.02 o -8 8 1 395.69 339.74 12.34 o -7 8 1 668.44 692.89 18.42 o -6 8 1 1444.44 1459.68 28.41 o -5 8 1 39.01 59.75 7.03 o -4 8 1 699.92 670.98 19.69 o -3 8 1 22.11 32.74 6.94 o -2 8 1 241.83 208.34 8.10 o -1 8 1 1308.80 1541.41 36.17 o 0 8 1 4696.82 4742.34 62.50 o 1 8 1 34.41 30.09 7.30 o 2 8 1 3107.32 3138.23 50.18 o 3 8 1 923.35 1095.91 23.31 o 4 8 1 375.31 397.74 10.76 o 5 8 1 188.61 234.73 8.91 o 6 8 1 262.36 272.85 9.67 o 7 8 1 41.02 37.69 8.09 o 8 8 1 82.56 79.00 9.87 o 9 8 1 145.19 182.10 11.28 o -8 9 1 0.23 0.00 21.33 o -7 9 1 247.39 267.75 11.49 o -6 9 1 151.49 143.82 10.39 o -5 9 1 415.17 376.11 10.80 o -4 9 1 262.60 272.55 9.83 o -3 9 1 950.54 850.43 22.89 o -2 9 1 231.94 203.57 8.74 o -1 9 1 153.44 111.68 7.97 o 0 9 1 44.91 54.52 7.94 o 1 9 1 1174.16 1047.65 24.53 o 2 9 1 59.04 75.06 7.52 o 3 9 1 256.85 261.56 9.51 o 4 9 1 249.37 190.22 9.38 o 5 9 1 699.57 686.80 18.43 o 6 9 1 5.87 0.00 9.23 o 7 9 1 838.49 818.90 21.48 o 8 9 1 22.78 0.00 22.80 o -6 10 1 9.90 11.35 22.31 o -5 10 1 683.53 650.53 17.38 o -4 10 1 26.99 12.28 21.24 o -3 10 1 401.85 384.92 12.71 o -2 10 1 6.63 0.00 19.40 o -1 10 1 503.54 522.65 12.04 o 0 10 1 297.13 236.14 10.10 o 1 10 1 40.00 13.34 20.26 o 2 10 1 24.31 0.00 19.70 o 3 10 1 833.18 860.09 21.07 o 4 10 1 0.01 0.00 22.05 o 5 10 1 589.87 547.77 14.94 o -1 11 1 108.35 135.51 11.48 o 0 11 1 156.35 166.44 11.58 o 1 11 1 327.06 367.67 13.81 o -12 0 2 220.54 257.21 9.16 o -10 0 2 402.63 403.63 11.03 o -8 0 2 6828.12 7111.08 60.78 o -6 0 2 509.63 547.50 11.50 o -4 0 2 38196.05 36478.55 91.50 o -2 0 2 14373.89 13450.44 40.33 o 2 0 2 73147.92 67425.50 24.80 o 4 0 2 20831.53 20160.75 68.79 o 6 0 2 6428.87 6340.25 48.74 o 8 0 2 8161.81 8129.82 65.40 o 10 0 2 425.70 419.84 10.15 o 12 0 2 2710.33 2686.52 53.71 o -13 1 2 642.80 664.62 18.99 o -12 1 2 56.99 53.99 7.17 o -11 1 2 198.54 212.68 8.49 o -10 1 2 2675.01 2621.33 44.91 o -9 1 2 2188.96 2251.14 38.88 o -8 1 2 809.93 736.44 15.96 o -7 1 2 11292.42 11544.09 71.61 o -6 1 2 93.44 152.22 4.59 o -5 1 2 2941.61 3041.68 31.45 o -4 1 2 14120.69 14617.25 59.47 o -3 1 2 17736.13 17149.88 56.69 o -2 1 2 1170.06 1109.07 13.53 o -1 1 2 5982.26 5932.19 24.91 o 0 1 2 16815.52 16522.73 40.34 o 1 1 2 14174.17 15425.95 40.70 o 2 1 2 1485.59 1939.94 17.59 o 3 1 2 2170.57 2098.74 20.86 o 4 1 2 10310.80 10612.88 51.30 o 5 1 2 509.59 637.51 16.25 o 6 1 2 4783.52 4725.06 42.74 o 7 1 2 4334.01 4364.89 44.85 o 8 1 2 764.76 685.84 16.17 o 9 1 2 1827.16 1864.76 36.27 o 10 1 2 1513.07 1467.12 35.72 o 11 1 2 249.68 220.18 8.84 o 12 1 2 32.88 34.26 7.77 o 13 1 2 269.93 309.50 11.68 o -13 2 2 94.03 114.83 9.73 o -12 2 2 177.12 178.08 8.64 o -11 2 2 2880.33 3007.63 51.94 o -10 2 2 102.72 106.90 6.99 o -9 2 2 2508.43 2495.30 41.21 o -8 2 2 1239.84 1183.68 27.94 o -7 2 2 2248.01 2217.95 33.58 o -6 2 2 146.08 149.84 5.16 o -5 2 2 17457.63 17361.02 75.67 o -4 2 2 6111.36 6115.03 41.45 o -3 2 2 3.11 4.99 6.48 o -2 2 2 474.64 397.95 10.32 o -1 2 2 5810.70 5656.58 30.55 o 0 2 2 6073.15 6824.63 34.92 o 1 2 2 13755.16 15798.82 51.46 o 2 2 2 1026.18 1252.20 16.44 o 3 2 2 3204.85 3251.23 27.96 o 4 2 2 631.69 629.51 15.16 o 5 2 2 8616.21 8620.00 54.12 o 6 2 2 670.02 708.38 13.84 o 7 2 2 312.44 325.73 8.25 o 8 2 2 896.88 872.63 18.38 o 9 2 2 1046.66 1015.53 20.21 o 10 2 2 9.41 8.43 6.98 o 11 2 2 901.34 855.27 22.20 o 12 2 2 0.18 5.05 18.32 o 13 2 2 3.45 13.83 8.97 o -13 3 2 1058.26 1091.27 28.41 o -12 3 2 0.60 0.00 19.22 o -11 3 2 0.84 12.34 7.00 o -10 3 2 298.03 312.45 9.26 o -9 3 2 2170.95 2127.20 39.02 o -8 3 2 9.95 9.51 12.88 o -7 3 2 2189.49 2368.60 35.96 o -6 3 2 315.11 283.02 6.72 o -5 3 2 2068.98 2076.95 29.11 o -4 3 2 1979.74 1929.01 26.40 o -3 3 2 14578.23 13816.39 62.13 o -2 3 2 2192.40 2267.67 24.50 o -1 3 2 8373.22 8777.10 45.19 o 0 3 2 707.33 707.46 15.83 o 1 3 2 7965.45 8171.23 44.51 o 2 3 2 2813.63 2956.00 28.11 o 3 3 2 11519.56 11029.15 56.16 o 4 3 2 1406.33 1349.89 23.01 o 5 3 2 215.64 278.78 6.86 o 6 3 2 1644.81 1601.70 28.37 o 7 3 2 5977.06 5828.30 55.46 o 8 3 2 1425.03 1393.93 31.10 o 9 3 2 2503.97 2303.43 42.36 o 10 3 2 272.70 296.74 8.99 o 11 3 2 382.93 335.10 10.18 o 12 3 2 2.72 11.38 18.13 o 13 3 2 526.51 539.10 14.50 o -12 4 2 423.20 429.19 12.64 o -11 4 2 73.16 50.97 8.10 o -10 4 2 460.52 433.35 13.01 o -9 4 2 1451.85 1438.11 36.05 o -8 4 2 785.34 817.79 18.12 o -7 4 2 725.63 738.37 16.55 o -6 4 2 999.01 1078.39 25.49 o -5 4 2 1350.47 1355.39 25.80 o -4 4 2 2631.00 2617.35 32.82 o -3 4 2 625.11 543.55 11.47 o -2 4 2 2536.86 2447.00 29.02 o -1 4 2 1155.89 1168.95 20.72 o 0 4 2 69.75 80.29 4.77 o 1 4 2 11175.98 11488.04 60.93 o 2 4 2 36439.41 37408.90 110.10 o 3 4 2 2167.81 2195.76 29.16 o 4 4 2 1806.81 1620.87 26.94 o 5 4 2 5985.44 6031.76 52.47 o 6 4 2 1283.63 1332.70 28.15 o 7 4 2 84.44 102.85 5.99 o 8 4 2 4241.64 4211.10 53.53 o 9 4 2 1012.83 1087.60 22.63 o 10 4 2 94.00 78.77 7.78 o 11 4 2 68.84 76.51 8.10 o 12 4 2 1212.96 1235.45 29.07 o -12 5 2 18.61 22.45 8.71 o -11 5 2 2.18 0.00 19.17 o -10 5 2 3364.73 3331.06 57.66 o -9 5 2 166.37 156.72 8.22 o -8 5 2 82.99 86.74 6.73 o -7 5 2 1078.98 1064.83 29.29 o -6 5 2 3701.67 3564.06 46.37 o -5 5 2 30.41 27.59 5.23 o -4 5 2 4741.16 4610.10 46.98 o -3 5 2 259.39 299.71 8.80 o -2 5 2 2887.81 2812.86 34.67 o -1 5 2 228.52 192.93 5.40 o 0 5 2 5229.56 4941.52 48.03 o 1 5 2 2803.57 2919.06 36.14 o 2 5 2 223.69 237.72 6.29 o 3 5 2 404.44 534.28 13.25 o 4 5 2 3313.26 3097.46 39.36 o 5 5 2 76.16 79.76 5.93 o 6 5 2 894.00 925.90 18.37 o 7 5 2 31.42 19.37 6.33 o 8 5 2 346.50 385.23 11.15 o 9 5 2 78.93 84.62 7.86 o 10 5 2 1581.90 1675.00 42.48 o 11 5 2 8.10 0.00 20.35 o 12 5 2 77.51 63.22 9.70 o -11 6 2 381.78 370.93 12.67 o -10 6 2 86.75 96.46 8.35 o -9 6 2 104.86 106.19 7.87 o -8 6 2 2492.23 2536.64 47.79 o -7 6 2 162.49 161.45 7.68 o -6 6 2 129.95 133.09 7.27 o -5 6 2 1893.00 1825.88 35.38 o -4 6 2 1945.27 2060.14 35.88 o -3 6 2 8.44 8.55 12.02 o -2 6 2 5555.97 5923.74 54.95 o -1 6 2 64.22 62.72 5.10 o 0 6 2 181.54 220.71 6.95 o 1 6 2 28.21 18.61 4.86 o 2 6 2 748.97 875.24 23.71 o 3 6 2 1.03 0.00 12.30 o 4 6 2 570.96 589.53 15.37 o 5 6 2 1661.35 1515.54 33.23 o 6 6 2 500.48 533.77 13.84 o 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10.43 o 0 2 31 361.07 332.91 14.24 o