#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2008130.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008130_Fobs loop_ _publ_author_name 'Manojlovic-Muir, L.' 'Muir, K. W.' 'Campbell, R. A.' 'McKendrick, J. E.' 'Robins, D. J.' _publ_section_title ; Pentaaqua(chelidonato-O^4^)copper(II) monohydrate ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 178 _journal_page_last 180 _journal_volume 55 _journal_year 1999 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 70.591 _cell_angle_beta 81.513 _cell_angle_gamma 71.158 _cell_length_a 7.3402 _cell_length_b 8.7066 _cell_length_c 11.1789 _exptl_crystal_F_000 362.00 _reflns_d_resolution_high 0.7114 _[local]_cod_data_source_file bm1282sup2.hkl _[local]_cod_data_source_block drcu #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Cu(OH2)5(C7H2O6)].H2O' _shelx_refln_list_code 4 _shelx_f_calc_maximum 120.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3607.89 2897.51 7.48 o 2 0 0 362.45 496.87 7.59 o 3 0 0 654.20 695.76 8.09 o 4 0 0 802.64 827.80 4.43 o 5 0 0 153.05 155.81 1.54 o 6 0 0 61.72 57.51 1.06 o 7 0 0 97.34 100.66 3.63 o 8 0 0 61.63 62.29 1.53 o 9 0 0 0.29 3.70 1.00 o -9 1 0 84.12 81.10 1.54 o -8 1 0 41.59 45.23 1.93 o -7 1 0 659.46 638.49 8.19 o -6 1 0 612.28 609.31 4.49 o -5 1 0 546.71 549.39 3.16 o -4 1 0 448.42 415.60 2.55 o -3 1 0 108.07 122.73 0.78 o -2 1 0 617.44 601.64 1.24 o -1 1 0 1903.46 2155.85 1.80 o 0 1 0 52.60 43.82 0.50 o 1 1 0 2812.89 2724.61 24.85 o 2 1 0 10904.39 9153.76 20.30 o 3 1 0 947.90 974.27 5.97 o 4 1 0 720.09 761.88 1.83 o 5 1 0 60.17 71.24 1.11 o 6 1 0 51.75 46.86 0.99 o 7 1 0 18.81 18.88 0.75 o 8 1 0 14.90 16.97 0.94 o 9 1 0 81.27 88.05 1.69 o -9 2 0 51.54 57.07 1.23 o -8 2 0 118.94 117.42 1.76 o -7 2 0 156.81 149.15 1.67 o -6 2 0 67.24 68.55 1.19 o -5 2 0 159.69 154.27 2.47 o -4 2 0 1733.97 1750.47 24.68 o -3 2 0 3634.43 4249.03 14.95 o -2 2 0 232.82 322.99 3.06 o -1 2 0 718.27 775.05 6.96 o 0 2 0 1220.85 1337.05 4.12 o 1 2 0 20.58 25.71 0.36 o 2 2 0 7173.56 6718.82 16.09 o 3 2 0 12.01 29.62 0.52 o 4 2 0 126.40 118.53 0.85 o 5 2 0 226.13 217.06 1.20 o 6 2 0 462.99 464.10 2.68 o 7 2 0 107.01 108.30 2.03 o 8 2 0 51.45 58.71 1.19 o 9 2 0 42.47 45.15 3.11 o 10 2 0 58.21 59.38 1.30 o -8 3 0 22.18 28.65 3.16 o -7 3 0 7.83 7.01 0.94 o -6 3 0 193.20 182.47 1.66 o -5 3 0 37.29 29.95 1.20 o -4 3 0 26.68 37.53 0.80 o -3 3 0 418.74 448.58 1.99 o -2 3 0 37.24 41.39 0.58 o -1 3 0 54.98 99.01 0.87 o 0 3 0 4336.46 4564.63 73.58 o 1 3 0 1085.14 1248.10 1.68 o 2 3 0 3054.04 3681.62 26.90 o 3 3 0 1369.16 1454.33 10.14 o 4 3 0 1364.66 1347.83 2.41 o 5 3 0 199.68 185.42 1.12 o 6 3 0 598.29 555.55 2.21 o 7 3 0 1059.81 1064.66 3.20 o 8 3 0 149.80 161.20 3.79 o 9 3 0 46.26 51.82 1.93 o 10 3 0 42.38 45.97 2.89 o -8 4 0 4.33 4.94 1.54 o -7 4 0 3.15 3.56 1.02 o -6 4 0 9.11 8.55 0.89 o -5 4 0 14.83 11.39 0.74 o -4 4 0 8.96 8.07 0.63 o -3 4 0 268.57 258.13 3.71 o -2 4 0 1457.32 1455.88 4.12 o -1 4 0 8041.61 8476.24 64.90 o 0 4 0 3800.73 3811.59 5.81 o 1 4 0 1302.84 1192.76 3.85 o 2 4 0 893.71 865.65 8.10 o 3 4 0 1942.68 2046.22 2.76 o 4 4 0 370.89 403.18 1.82 o 5 4 0 109.37 103.01 0.96 o 6 4 0 501.26 496.22 3.69 o 7 4 0 174.27 169.55 1.59 o 8 4 0 72.31 74.55 1.49 o 9 4 0 51.38 46.29 1.16 o 10 4 0 3.20 -0.20 1.39 o -7 5 0 43.59 37.33 1.17 o -6 5 0 148.13 145.58 1.86 o -5 5 0 132.42 131.23 2.08 o -4 5 0 678.43 684.70 2.98 o -3 5 0 59.38 75.52 1.09 o -2 5 0 93.42 79.87 1.11 o -1 5 0 881.81 826.18 6.55 o 0 5 0 4531.87 4499.57 14.64 o 1 5 0 1389.93 1311.40 9.30 o 2 5 0 271.74 261.89 1.41 o 3 5 0 486.71 454.75 2.52 o 4 5 0 591.58 581.75 1.73 o 5 5 0 0.58 6.88 0.55 o 6 5 0 107.58 107.95 4.75 o 7 5 0 7.25 9.06 1.18 o 8 5 0 3.75 3.22 1.34 o 9 5 0 19.05 21.36 1.11 o 10 5 0 4.15 6.85 1.02 o -6 6 0 134.72 131.02 3.08 o -5 6 0 249.26 242.09 4.91 o -4 6 0 588.70 601.74 3.46 o -3 6 0 1210.49 1134.82 3.21 o -2 6 0 187.85 207.21 2.58 o -1 6 0 299.55 307.22 3.56 o 0 6 0 161.22 153.65 2.38 o 1 6 0 105.75 119.55 1.70 o 2 6 0 296.33 306.86 1.28 o 3 6 0 1.07 5.76 0.90 o 4 6 0 293.47 285.27 2.08 o 5 6 0 58.89 61.95 1.09 o 6 6 0 3.74 10.80 0.73 o 7 6 0 96.55 98.01 1.54 o 8 6 0 15.08 15.69 1.03 o 9 6 0 5.62 6.42 1.05 o -5 7 0 38.78 43.61 1.86 o -4 7 0 30.18 28.43 1.98 o -3 7 0 124.38 128.28 1.63 o -2 7 0 4.79 5.41 0.82 o -1 7 0 58.69 54.12 1.12 o 0 7 0 56.10 53.39 1.03 o 1 7 0 9.38 8.93 0.59 o 2 7 0 11.50 12.43 1.67 o 3 7 0 100.86 98.37 1.36 o 4 7 0 171.30 169.47 1.42 o 5 7 0 161.02 151.14 1.73 o 6 7 0 828.06 854.98 7.67 o 7 7 0 210.54 231.50 2.05 o 8 7 0 83.20 85.37 3.47 o 9 7 0 36.72 35.17 1.13 o -4 8 0 22.06 25.45 1.21 o -3 8 0 46.64 44.34 1.20 o -2 8 0 88.04 91.00 1.62 o -1 8 0 780.28 767.09 8.01 o 0 8 0 484.98 474.65 2.29 o 1 8 0 316.04 326.21 3.56 o 2 8 0 200.22 208.89 3.64 o 3 8 0 126.45 124.29 1.43 o 4 8 0 115.30 124.81 1.50 o 5 8 0 43.50 49.83 1.07 o 6 8 0 297.46 307.76 2.24 o 7 8 0 198.88 204.52 2.11 o 8 8 0 52.62 51.08 1.20 o 9 8 0 32.57 26.03 1.04 o -3 9 0 173.45 174.29 2.18 o -2 9 0 169.18 172.13 2.13 o -1 9 0 310.88 330.92 3.70 o 0 9 0 281.66 287.71 2.22 o 1 9 0 258.50 261.77 2.08 o 2 9 0 371.02 393.00 2.69 o 3 9 0 476.15 523.06 6.76 o 4 9 0 42.55 48.39 1.11 o 5 9 0 54.76 57.66 1.18 o 6 9 0 108.45 113.12 2.46 o 7 9 0 19.97 23.17 1.14 o 8 9 0 0.80 0.45 2.00 o -2 10 0 110.77 101.69 1.99 o -1 10 0 130.72 132.67 3.96 o 0 10 0 182.38 180.08 2.63 o 1 10 0 3.74 1.65 1.30 o 2 10 0 16.31 17.12 1.20 o 3 10 0 12.51 13.25 1.18 o 4 10 0 0.86 1.40 1.55 o 5 10 0 32.91 29.21 1.22 o 6 10 0 0.10 -0.30 1.49 o 7 10 0 4.33 2.91 1.10 o 0 11 0 0.06 0.09 1.29 o 1 11 0 4.47 5.41 1.22 o 2 11 0 8.41 8.89 1.15 o 3 11 0 6.82 6.85 2.12 o 4 11 0 100.11 89.91 1.81 o 5 11 0 72.03 64.27 1.37 o -4 -11 1 65.42 56.33 1.75 o -3 -11 1 26.38 27.19 1.63 o -2 -11 1 63.12 60.29 1.79 o -1 -11 1 32.78 33.60 1.71 o -6 -10 1 148.82 141.18 2.73 o -5 -10 1 165.68 166.82 2.99 o -4 -10 1 64.71 64.92 1.98 o -3 -10 1 34.41 35.09 1.75 o -2 -10 1 361.81 375.37 3.77 o -1 -10 1 138.21 136.94 2.91 o 0 -10 1 19.32 16.74 1.76 o 1 -10 1 79.04 75.23 2.42 o -8 -9 1 38.12 31.43 1.50 o -7 -9 1 27.89 26.40 1.65 o -6 -9 1 117.37 126.90 2.69 o -5 -9 1 72.68 81.00 2.41 o -4 -9 1 48.22 54.33 1.66 o -3 -9 1 166.00 180.34 2.74 o -2 -9 1 3.69 1.00 1.44 o -1 -9 1 5.05 5.44 1.47 o 0 -9 1 18.93 17.37 1.58 o 1 -9 1 62.14 60.42 1.82 o 2 -9 1 34.91 34.45 1.78 o 3 -9 1 52.84 48.76 1.85 o -8 -8 1 36.94 36.47 1.62 o -7 -8 1 37.73 35.58 1.67 o -6 -8 1 10.55 14.15 1.48 o -5 -8 1 2.62 0.09 1.76 o -4 -8 1 0.02 0.52 1.24 o -3 -8 1 48.21 50.59 1.54 o -2 -8 1 26.78 32.58 1.26 o -1 -8 1 73.13 77.08 1.95 o 0 -8 1 333.33 335.41 2.99 o 1 -8 1 1077.61 1109.66 5.02 o 2 -8 1 160.47 176.05 2.73 o 3 -8 1 6.60 6.68 1.57 o 4 -8 1 70.49 62.00 1.99 o -9 -7 1 0.05 -1.91 1.91 o -8 -7 1 2.38 2.68 1.50 o -7 -7 1 12.25 13.31 1.47 o -6 -7 1 18.87 19.26 1.35 o -5 -7 1 93.23 90.46 1.93 o -4 -7 1 74.36 84.51 1.72 o -3 -7 1 35.41 42.99 1.34 o -2 -7 1 330.69 335.57 2.46 o -1 -7 1 251.80 250.40 2.21 o 0 -7 1 309.71 305.46 2.45 o 1 -7 1 1373.59 1386.15 4.93 o 2 -7 1 966.40 967.67 4.48 o 3 -7 1 444.21 435.67 3.49 o 4 -7 1 143.26 144.78 2.67 o 5 -7 1 5.81 3.25 1.64 o -9 -6 1 27.28 27.81 1.63 o -8 -6 1 51.66 57.86 1.67 o -7 -6 1 26.20 35.59 1.43 o -6 -6 1 318.67 315.40 2.81 o -5 -6 1 314.07 310.77 2.51 o -4 -6 1 56.30 51.58 1.41 o -3 -6 1 1025.75 958.11 3.54 o -2 -6 1 1809.58 1727.48 4.13 o -1 -6 1 344.68 356.39 2.02 o 0 -6 1 238.72 228.85 1.92 o 1 -6 1 1161.48 1160.56 4.02 o 2 -6 1 480.39 500.76 2.97 o 3 -6 1 6.40 2.60 1.14 o 4 -6 1 170.70 158.34 2.48 o 5 -6 1 53.01 50.00 1.70 o 6 -6 1 3.86 5.33 1.55 o -9 -5 1 51.83 58.59 1.69 o -8 -5 1 186.70 202.61 2.81 o -7 -5 1 183.35 197.78 2.49 o -6 -5 1 120.66 120.42 1.92 o -5 -5 1 183.49 179.62 1.94 o -4 -5 1 76.56 61.44 1.17 o -3 -5 1 723.02 706.09 2.58 o -2 -5 1 719.78 669.20 2.40 o -1 -5 1 499.37 480.59 2.03 o 0 -5 1 790.22 746.56 2.53 o 1 -5 1 165.52 175.16 1.48 o 2 -5 1 39.99 38.37 1.15 o 3 -5 1 36.59 33.16 1.05 o 4 -5 1 0.14 0.38 1.44 o 5 -5 1 120.59 114.02 2.24 o 6 -5 1 81.68 85.82 2.40 o 7 -5 1 4.04 3.21 1.55 o -10 -4 1 45.26 44.93 1.63 o -9 -4 1 134.73 144.78 2.72 o -8 -4 1 50.86 62.58 1.81 o -7 -4 1 83.51 92.03 2.00 o -6 -4 1 260.49 261.31 2.35 o -5 -4 1 202.08 208.29 1.94 o -4 -4 1 0.56 2.91 0.64 o -3 -4 1 122.09 128.06 1.22 o -2 -4 1 46.09 42.26 0.84 o -1 -4 1 694.94 749.43 2.22 o 0 -4 1 258.79 256.87 1.40 o 1 -4 1 670.47 701.97 2.32 o 2 -4 1 172.23 185.78 1.47 o 3 -4 1 69.84 74.61 1.40 o 4 -4 1 497.86 478.32 2.90 o 5 -4 1 4.46 7.67 1.14 o 6 -4 1 82.32 90.78 2.22 o 7 -4 1 262.12 259.06 3.14 o 8 -4 1 217.34 206.16 3.19 o -10 -3 1 0.19 0.00 1.89 o -9 -3 1 13.79 16.29 1.50 o -8 -3 1 31.71 32.04 1.44 o -7 -3 1 11.90 12.98 1.10 o -6 -3 1 60.18 53.39 1.49 o -5 -3 1 92.55 94.07 1.34 o -4 -3 1 217.31 226.03 1.59 o -3 -3 1 34.87 38.94 0.84 o -2 -3 1 399.95 430.05 1.67 o -1 -3 1 1177.93 1198.94 2.51 o 0 -3 1 1695.86 1690.21 2.96 o 1 -3 1 7404.82 6211.32 23.18 o 2 -3 1 1720.63 1756.51 3.58 o 3 -3 1 170.35 169.28 1.45 o 4 -3 1 513.19 530.20 2.79 o 5 -3 1 892.35 869.42 3.87 o 6 -3 1 72.89 75.52 1.91 o 7 -3 1 101.72 105.65 2.34 o 8 -3 1 69.76 74.35 2.17 o -10 -2 1 0.65 2.44 1.43 o -9 -2 1 1.09 -1.26 1.91 o -8 -2 1 26.50 23.51 1.38 o -7 -2 1 140.71 152.30 2.17 o -6 -2 1 10.21 10.27 0.87 o -5 -2 1 182.76 173.67 1.60 o -4 -2 1 1420.95 1372.30 3.52 o -3 -2 1 3228.91 3318.91 4.95 o -2 -2 1 4315.51 4815.54 5.34 o -1 -2 1 119.39 116.25 0.82 o 0 -2 1 2690.98 3054.59 3.44 o 1 -2 1 4942.29 5763.35 5.27 o 2 -2 1 1064.51 1086.69 2.59 o 3 -2 1 69.32 46.61 0.96 o 4 -2 1 841.48 859.38 2.99 o 5 -2 1 104.72 102.37 1.67 o 6 -2 1 2.21 3.39 0.97 o 7 -2 1 401.70 380.88 3.24 o 8 -2 1 22.84 25.57 1.52 o 9 -2 1 7.94 5.23 1.55 o -9 -1 1 114.03 119.88 2.55 o -8 -1 1 50.96 54.85 1.58 o -7 -1 1 101.26 108.16 1.95 o -6 -1 1 277.10 277.09 2.33 o -5 -1 1 83.90 83.56 1.26 o -4 -1 1 79.78 62.93 1.04 o -3 -1 1 3341.89 3200.28 4.85 o -2 -1 1 14639.41 11185.26 32.69 o -1 -1 1 414.83 406.06 1.24 o 0 -1 1 6173.30 5835.32 15.20 o 1 -1 1 1494.92 1786.82 2.45 o 2 -1 1 100.40 107.73 0.88 o 3 -1 1 19.34 16.66 0.55 o 4 -1 1 413.75 430.02 2.07 o 5 -1 1 44.88 44.89 1.27 o 6 -1 1 30.03 35.03 1.08 o 7 -1 1 240.33 230.72 2.62 o 8 -1 1 9.76 13.51 1.38 o 9 -1 1 4.62 5.10 1.50 o -9 0 1 93.54 96.31 2.47 o -8 0 1 188.05 196.44 2.70 o -7 0 1 330.31 333.03 2.88 o -6 0 1 228.92 219.53 2.19 o -5 0 1 56.72 62.94 1.20 o -4 0 1 133.39 132.68 1.30 o -3 0 1 542.26 569.70 2.06 o -2 0 1 177.67 171.92 1.05 o -1 0 1 1430.61 1515.93 2.11 o 1 0 1 148.81 128.42 0.63 o 2 0 1 882.58 921.23 2.05 o 3 0 1 374.12 401.22 1.68 o 4 0 1 272.37 284.20 1.69 o 5 0 1 122.65 101.67 1.34 o 6 0 1 94.09 91.18 1.67 o 7 0 1 260.74 258.93 2.58 o 8 0 1 296.96 313.38 3.14 o 9 0 1 222.47 223.97 3.07 o -9 1 1 24.00 25.31 1.53 o -8 1 1 46.27 47.93 1.54 o -7 1 1 2.92 2.26 1.15 o -6 1 1 109.65 110.53 1.83 o -5 1 1 240.18 255.34 1.90 o -4 1 1 12.84 19.47 0.69 o -3 1 1 3.52 12.34 0.53 o -2 1 1 422.93 464.93 1.57 o -1 1 1 745.64 852.57 1.59 o 0 1 1 1424.36 1458.11 1.45 o 1 1 1 260.08 254.98 0.79 o 2 1 1 5740.30 6643.91 5.67 o 3 1 1 1452.92 1421.16 3.02 o 4 1 1 1244.10 1140.24 3.09 o 5 1 1 324.50 290.43 1.88 o 6 1 1 250.87 248.89 2.20 o 7 1 1 470.79 466.09 3.15 o 8 1 1 317.57 333.10 3.14 o 9 1 1 2.60 2.93 1.44 o 10 1 1 59.51 55.84 1.73 o -9 2 1 2.41 2.39 1.46 o -8 2 1 2.27 2.78 1.37 o -7 2 1 43.16 44.85 1.37 o -6 2 1 3.46 6.60 0.95 o -5 2 1 150.64 147.00 1.82 o -4 2 1 666.27 670.23 2.65 o -3 2 1 2232.60 2268.55 4.20 o -2 2 1 1904.07 1983.23 3.36 o -1 2 1 1173.18 1210.07 2.15 o 0 2 1 1758.03 1842.48 2.23 o 1 2 1 10328.83 8973.31 21.28 o 2 2 1 4345.56 5561.38 5.13 o 3 2 1 152.91 122.25 1.03 o 4 2 1 3992.37 3861.12 5.67 o 5 2 1 1853.41 1703.38 4.17 o 6 2 1 42.77 36.14 1.05 o 7 2 1 374.80 373.84 2.85 o 8 2 1 82.60 97.30 2.16 o 9 2 1 13.44 13.33 1.48 o 10 2 1 0.40 3.07 1.43 o -8 3 1 36.82 35.74 1.63 o -7 3 1 28.53 30.43 1.42 o -6 3 1 86.76 82.94 1.92 o -5 3 1 15.49 17.46 0.93 o -4 3 1 894.16 897.44 3.48 o -3 3 1 3275.04 3334.93 5.39 o -2 3 1 3313.04 3442.60 4.83 o -1 3 1 5417.75 5400.07 5.39 o 0 3 1 2296.58 2434.76 3.17 o 1 3 1 486.57 530.86 1.48 o 2 3 1 7.83 10.47 0.43 o 3 3 1 1474.65 1623.12 3.25 o 4 3 1 7.45 14.06 0.61 o 5 3 1 115.11 131.02 1.39 o 6 3 1 145.52 143.48 1.81 o 7 3 1 84.41 74.66 1.75 o 8 3 1 29.01 31.83 1.36 o 9 3 1 13.36 13.66 1.44 o 10 3 1 8.30 9.12 1.49 o -8 4 1 187.65 182.17 3.00 o -7 4 1 163.42 158.78 2.65 o -6 4 1 84.02 83.88 2.08 o -5 4 1 70.63 74.33 1.76 o -4 4 1 411.10 393.90 2.63 o -3 4 1 758.00 775.95 2.84 o -2 4 1 1332.57 1333.73 3.28 o -1 4 1 20.66 15.11 0.52 o 0 4 1 672.85 680.08 1.96 o 1 4 1 350.33 344.70 1.40 o 2 4 1 2.79 2.43 0.44 o 3 4 1 661.05 731.37 2.29 o 4 4 1 1269.13 1346.73 3.39 o 5 4 1 40.13 36.70 1.08 o 6 4 1 246.98 233.46 2.15 o 7 4 1 440.40 443.44 3.10 o 8 4 1 79.70 92.55 2.16 o 9 4 1 43.10 48.85 1.61 o 10 4 1 23.27 21.44 1.56 o -7 5 1 42.87 41.62 1.68 o -6 5 1 149.76 141.19 2.57 o -5 5 1 293.61 267.74 2.77 o -4 5 1 42.85 35.11 1.08 o -3 5 1 104.40 93.64 1.57 o -2 5 1 113.71 114.97 1.34 o -1 5 1 29.73 29.08 0.83 o 0 5 1 16.30 12.67 0.55 o 1 5 1 1832.71 1838.14 3.50 o 2 5 1 738.11 696.29 2.24 o 3 5 1 35.01 22.47 0.67 o 4 5 1 1229.88 1220.25 3.35 o 5 5 1 786.70 749.14 3.21 o 6 5 1 15.31 13.44 0.91 o 7 5 1 172.11 171.66 2.26 o 8 5 1 322.64 343.46 3.22 o 9 5 1 34.35 35.31 1.57 o 10 5 1 20.32 20.06 1.51 o -6 6 1 4.08 6.71 1.55 o -5 6 1 0.12 0.56 1.84 o -4 6 1 95.67 100.35 2.17 o -3 6 1 285.13 274.30 2.47 o -2 6 1 527.64 496.95 2.80 o -1 6 1 406.65 405.44 2.36 o 0 6 1 316.35 306.04 1.79 o 1 6 1 117.00 132.59 1.29 o 2 6 1 325.27 302.37 1.73 o 3 6 1 1575.65 1472.04 3.67 o 4 6 1 2098.59 2000.65 4.96 o 5 6 1 43.44 37.17 1.00 o 6 6 1 991.43 952.16 4.14 o 7 6 1 355.16 359.00 3.08 o 8 6 1 25.73 26.60 1.46 o 9 6 1 0.47 -1.96 1.96 o 10 6 1 18.72 17.13 1.45 o -6 7 1 20.44 21.51 1.75 o -5 7 1 66.48 66.78 2.22 o -4 7 1 377.98 382.29 3.48 o -3 7 1 783.81 766.92 4.18 o -2 7 1 392.55 384.63 2.88 o -1 7 1 1781.13 1699.45 5.10 o 0 7 1 830.39 806.25 3.40 o 1 7 1 319.77 318.91 2.22 o 2 7 1 35.49 33.56 1.04 o 3 7 1 8.15 9.08 0.81 o 4 7 1 407.91 400.96 2.63 o 5 7 1 502.84 506.55 3.09 o 6 7 1 20.30 19.21 1.24 o 7 7 1 34.88 33.94 1.44 o 8 7 1 8.24 6.19 1.49 o 9 7 1 1.31 -2.01 2.01 o -5 8 1 183.06 177.65 3.15 o -4 8 1 105.67 99.21 2.65 o -3 8 1 247.73 247.06 3.13 o -2 8 1 402.19 373.06 3.26 o -1 8 1 135.96 140.74 2.24 o 0 8 1 235.09 235.06 2.43 o 1 8 1 300.16 288.10 2.49 o 2 8 1 4.29 4.72 0.93 o 3 8 1 255.07 264.52 2.42 o 4 8 1 4.86 3.97 1.03 o 5 8 1 21.47 22.71 1.27 o 6 8 1 7.97 8.75 1.34 o 7 8 1 14.60 10.38 1.52 o 8 8 1 153.11 149.87 2.79 o 9 8 1 14.22 13.69 1.45 o -3 9 1 30.44 28.01 1.83 o -2 9 1 88.61 86.91 2.55 o -1 9 1 0.15 0.89 1.95 o 0 9 1 8.67 8.59 1.39 o 1 9 1 135.96 133.35 2.38 o 2 9 1 28.51 26.68 1.35 o 3 9 1 77.89 84.87 2.14 o 4 9 1 99.15 106.95 2.30 o 5 9 1 27.10 33.16 1.53 o 6 9 1 31.71 33.67 1.62 o 7 9 1 177.68 181.18 2.96 o 8 9 1 10.20 10.05 1.50 o -2 10 1 4.04 7.61 1.69 o -1 10 1 36.44 39.48 1.81 o 0 10 1 42.99 38.51 1.77 o 1 10 1 7.81 9.27 1.64 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