#------------------------------------------------------------------------------ #$Date: 2016-04-02 20:33:27 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180762 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/83/2008350.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008350_Fobs loop_ _publ_author_name 'Batey, R. A.' 'Yoshina-Ishii, C.' 'Lough, A. J.' _publ_section_title ; 3-Methyl-1-(1,2,3,4-tetrahydroisoquinolin-2-ylcarbonyl)imidazolium iodide ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 615 _journal_page_last 618 _journal_volume 55 _journal_year 1999 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.2974 _cell_length_b 7.9474 _cell_length_c 27.3988 _exptl_crystal_F_000 1456.00 _reflns_d_resolution_high 0.8004 _cod_data_source_file fg1529sup2.hkl _cod_data_source_block k9893a #BEGIN Tags that were not found in dictionaries: _shelx_title ' k9893a in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 355.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 34915.14 33631.17 1832.23 o 6 0 0 87318.37 91553.20 6763.69 o 8 0 0 28031.91 27656.36 1712.99 o 10 0 0 21451.10 23229.15 1072.44 o 12 0 0 4577.67 4106.28 799.13 o 14 0 0 5006.51 4770.98 819.09 o 16 0 0 370.71 379.69 288.00 o 4 1 0 37269.64 37957.69 1800.15 o 6 1 0 1016.08 1051.38 95.26 o 8 1 0 59.20 152.81 98.74 o 10 1 0 863.19 931.19 139.91 o 12 1 0 338.24 -35.27 246.86 o 14 1 0 1102.17 1355.62 190.47 o 16 1 0 137.63 244.49 152.81 o 0 2 0 52651.02 54431.63 4427.97 o 2 2 0 126130.64 129828.19 5548.92 o 4 2 0 38446.30 37185.07 1374.95 o 6 2 0 41382.50 41339.64 1524.00 o 8 2 0 31069.79 32399.67 1356.77 o 10 2 0 4114.43 4187.54 201.26 o 12 2 0 4869.78 4904.42 336.61 o 14 2 0 389.66 213.95 142.24 o 16 2 0 401.97 811.11 208.07 o 2 3 0 263.82 162.23 77.59 o 4 3 0 4627.13 4743.23 170.83 o 6 3 0 10383.64 10765.99 583.16 o 8 3 0 5310.78 5325.05 214.32 o 10 3 0 7708.76 7774.37 434.72 o 12 3 0 2003.34 1985.14 159.94 o 14 3 0 2218.09 2200.34 216.39 o 0 4 0 6231.12 6551.42 363.12 o 2 4 0 5068.83 4924.77 243.88 o 4 4 0 7.27 216.28 104.61 o 6 4 0 425.33 660.69 112.86 o 8 4 0 1743.86 1920.52 198.76 o 10 4 0 297.43 440.82 136.36 o 12 4 0 122.69 56.42 143.41 o 14 4 0 163.92 169.27 212.76 o 2 5 0 471.48 493.76 129.32 o 4 5 0 1738.38 1604.25 118.79 o 6 5 0 7603.14 8041.80 386.48 o 8 5 0 6845.20 6764.94 373.34 o 10 5 0 741.75 618.39 112.86 o 12 5 0 2808.21 2785.23 256.41 o 14 5 0 1333.88 1121.67 236.33 o 0 6 0 4367.92 4210.50 411.99 o 2 6 0 9530.85 8365.22 659.08 o 4 6 0 9885.45 10006.04 491.64 o 6 6 0 575.26 465.54 122.26 o 8 6 0 657.11 500.81 132.85 o 10 6 0 2164.40 2339.13 286.95 o 12 6 0 546.07 1021.56 229.23 o 2 7 0 369.00 366.77 134.01 o 4 7 0 6.77 -135.17 135.17 o 6 7 0 1888.31 1719.30 156.41 o 8 7 0 846.38 953.46 149.31 o 10 7 0 528.85 625.40 327.98 o 0 8 0 3443.82 4097.56 318.82 o 2 8 0 8875.23 9267.67 414.67 o 4 8 0 5346.78 5345.74 306.01 o 6 8 0 3624.71 3841.01 364.69 o 8 8 0 2816.13 2678.11 239.94 o 2 9 0 224.74 358.52 209.23 o 4 9 0 32.08 212.75 178.66 o 6 9 0 6.34 62.30 206.87 o 3 1 1 97304.59 101314.32 4544.04 o 4 1 1 14870.92 15037.61 456.26 o 5 1 1 22522.86 21492.43 567.10 o 6 1 1 2380.41 2313.71 77.67 o 7 1 1 5846.46 5302.08 219.20 o 8 1 1 11107.72 11438.87 315.22 o 9 1 1 8818.28 8731.39 266.48 o 10 1 1 5894.23 6065.00 201.38 o 11 1 1 3871.79 3915.14 155.33 o 12 1 1 5357.84 5406.70 241.32 o 13 1 1 1199.32 1288.66 110.52 o 14 1 1 2326.09 2283.95 145.83 o 15 1 1 356.33 304.46 145.76 o 16 1 1 1222.49 1341.51 177.54 o 0 2 1 7927.18 8598.38 386.04 o 1 2 1 5348.05 5701.17 165.35 o 2 2 1 74286.59 77223.13 2045.94 o 3 2 1 996.90 975.11 55.28 o 4 2 1 36511.49 35536.62 1027.24 o 5 2 1 122.58 109.32 48.20 o 6 2 1 9603.20 9210.71 266.84 o 7 2 1 2071.74 1922.29 88.23 o 8 2 1 6444.64 6553.51 212.09 o 9 2 1 503.06 719.48 84.64 o 10 2 1 4899.22 5105.62 221.32 o 11 2 1 1351.90 1275.83 123.47 o 12 2 1 1537.69 1513.39 143.46 o 13 2 1 618.00 559.59 106.98 o 14 2 1 592.47 552.52 108.15 o 15 2 1 354.04 452.57 108.15 o 16 2 1 361.88 353.83 118.73 o 1 3 1 2191.89 1919.73 87.10 o 2 3 1 1318.70 1261.03 71.76 o 3 3 1 2454.89 2464.64 87.10 o 4 3 1 1221.75 1523.10 90.56 o 5 3 1 8414.08 8417.55 241.88 o 6 3 1 3210.06 3545.07 162.42 o 7 3 1 886.89 852.46 74.08 o 8 3 1 101.35 220.99 75.23 o 9 3 1 546.10 628.96 87.00 o 10 3 1 3672.23 3535.99 168.27 o 11 3 1 1000.10 886.51 92.88 o 12 3 1 1100.68 1009.97 104.64 o 13 3 1 209.24 86.99 104.62 o 14 3 1 346.90 298.58 125.78 o 15 3 1 110.96 -43.49 142.23 o 0 4 1 56259.80 55075.25 3146.30 o 1 4 1 23.45 -49.37 92.86 o 2 4 1 41416.84 40517.71 1499.55 o 3 4 1 102.49 83.46 64.65 o 4 4 1 31312.53 32062.86 902.51 o 5 4 1 183.67 202.19 68.18 o 6 4 1 23654.23 24168.73 616.46 o 7 4 1 552.52 451.44 78.77 o 8 4 1 10724.02 11120.65 435.20 o 9 4 1 2889.98 2861.07 118.82 o 10 4 1 3603.10 3840.41 160.02 o 11 4 1 1680.35 1603.98 145.82 o 12 4 1 2060.68 2185.04 174.05 o 13 4 1 520.75 474.93 109.33 o 14 4 1 1376.75 1506.18 157.55 o 15 4 1 453.11 359.71 159.87 o 1 5 1 825.31 614.94 78.78 o 2 5 1 19.72 -25.86 68.17 o 3 5 1 8.51 -11.75 76.40 o 4 5 1 112.24 332.66 75.23 o 5 5 1 1420.41 1307.69 82.32 o 6 5 1 1588.86 1599.38 104.67 o 7 5 1 2950.26 3067.06 141.18 o 8 5 1 0.90 -64.65 88.16 o 9 5 1 95.41 159.86 83.46 o 10 5 1 183.08 199.83 96.39 o 11 5 1 28.65 62.30 108.14 o 12 5 1 157.84 414.94 168.09 o 13 5 1 71.67 139.88 124.60 o 14 5 1 13.52 -5.88 142.23 o 0 6 1 10726.81 10965.12 431.72 o 1 6 1 287.78 238.63 76.41 o 2 6 1 8731.25 8640.05 301.75 o 3 6 1 2052.09 2068.90 109.38 o 4 6 1 14681.61 15189.78 549.03 o 5 6 1 112.86 36.44 79.93 o 6 6 1 8137.04 8390.78 300.43 o 7 6 1 2.87 65.82 85.81 o 8 6 1 2076.82 2329.77 130.54 o 9 6 1 414.06 425.55 104.62 o 10 6 1 1159.29 1124.01 132.86 o 11 6 1 294.60 181.03 95.22 o 12 6 1 1242.74 1120.48 151.67 o 13 6 1 380.96 302.11 159.87 o 1 7 1 5427.48 5673.08 204.84 o 2 7 1 7.30 -27.03 84.63 o 3 7 1 782.03 939.36 112.86 o 4 7 1 924.47 891.19 105.81 o 5 7 1 1684.16 1722.75 137.59 o 6 7 1 327.87 181.03 186.91 o 7 7 1 1969.21 1792.22 129.36 o 8 7 1 413.51 509.01 114.03 o 9 7 1 854.44 1094.53 136.38 o 10 7 1 755.18 801.77 123.44 o 11 7 1 558.64 478.45 116.38 o 0 8 1 111.97 -55.25 128.12 o 1 8 1 87.79 131.65 99.91 o 2 8 1 265.37 165.74 94.04 o 3 8 1 29.69 164.56 119.89 o 4 8 1 660.96 453.78 117.56 o 5 8 1 6.39 -35.26 109.31 o 6 8 1 362.61 238.63 155.17 o 7 8 1 22.47 253.89 136.35 o 8 8 1 52.08 -97.56 128.12 o 9 8 1 34.33 -3.53 132.82 o 1 9 1 1172.68 1065.21 114.05 o 2 9 1 5.16 -22.33 118.72 o 3 9 1 1054.44 1045.20 134.03 o 4 9 1 178.20 151.63 139.88 o 5 9 1 935.52 485.55 141.08 o 6 9 1 329.29 362.05 146.94 o 3 0 2 4365.42 2578.43 212.51 o 4 0 2 62998.66 64365.05 2952.28 o 5 0 2 3168.97 3381.36 138.98 o 6 0 2 13771.41 13829.98 536.34 o 7 0 2 8876.22 8781.79 312.75 o 8 0 2 4404.75 4545.18 173.09 o 9 0 2 5689.94 5817.33 230.86 o 10 0 2 5847.13 5469.11 232.00 o 11 0 2 6245.00 6423.96 376.84 o 12 0 2 24.03 -173.96 178.66 o 13 0 2 3669.46 3597.86 247.07 o 14 0 2 294.34 597.15 159.87 o 15 0 2 2497.79 2106.39 296.38 o 16 0 2 125.61 382.02 183.37 o 3 1 2 2744.57 2925.72 113.12 o 4 1 2 1472.72 1559.08 72.95 o 5 1 2 7558.41 7472.85 226.70 o 6 1 2 1771.05 1737.66 118.82 o 7 1 2 12566.89 13369.53 373.51 o 8 1 2 491.58 399.72 74.07 o 9 1 2 2166.41 2038.57 105.87 o 10 1 2 542.12 590.16 101.10 o 11 1 2 1590.82 1729.86 112.89 o 12 1 2 51.34 82.28 83.46 o 13 1 2 538.00 564.28 104.63 o 14 1 2 101.69 74.05 109.32 o 15 1 2 104.46 148.11 112.84 o 16 1 2 0.41 -32.91 149.28 o 0 2 2 3555.58 4051.88 175.71 o 1 2 2 3461.47 3692.62 133.23 o 2 2 2 49232.55 50418.47 1385.42 o 3 2 2 62.26 45.84 49.37 o 4 2 2 5902.97 5841.44 175.76 o 5 2 2 3762.69 3888.94 155.46 o 6 2 2 307.62 204.55 62.31 o 7 2 2 5807.85 5762.84 182.63 o 8 2 2 2650.53 2616.72 101.19 o 9 2 2 2334.83 2175.08 111.75 o 10 2 2 1120.00 1151.14 82.31 o 11 2 2 872.49 893.54 98.76 o 12 2 2 2015.06 1954.61 128.19 o 13 2 2 2723.06 2691.21 138.79 o 14 2 2 14.90 -56.42 91.68 o 15 2 2 1208.43 1160.45 144.62 o 16 2 2 7.82 16.46 166.91 o 1 3 2 53651.89 51571.91 1565.65 o 2 3 2 487.80 502.05 77.60 o 3 3 2 32026.72 31772.23 1500.61 o 4 3 2 942.88 1025.44 63.50 o 5 3 2 36351.65 36669.03 941.36 o 6 3 2 1874.87 2256.19 132.92 o 7 3 2 23512.52 24777.24 578.67 o 8 3 2 165.72 295.05 79.93 o 9 3 2 13353.68 13921.94 332.88 o 10 3 2 1860.01 2004.02 114.08 o 11 3 2 6063.20 5725.65 273.15 o 12 3 2 73.49 297.39 121.07 o 13 3 2 1964.15 1955.66 152.88 o 14 3 2 106.23 83.46 121.07 o 15 3 2 1193.31 1039.34 144.61 o 0 4 2 137.07 219.82 76.41 o 1 4 2 282.83 302.12 61.13 o 2 4 2 994.24 909.01 77.61 o 3 4 2 684.87 741.91 104.64 o 4 4 2 715.03 846.55 90.53 o 5 4 2 334.85 382.06 82.29 o 6 4 2 3.70 -63.47 63.47 o 7 4 2 569.65 727.72 74.07 o 8 4 2 144.72 153.99 89.34 o 9 4 2 265.02 210.42 102.27 o 10 4 2 792.09 845.31 109.34 o 11 4 2 1.11 83.45 92.86 o 12 4 2 294.37 385.56 105.80 o 13 4 2 81.95 11.75 106.96 o 14 4 2 14.77 -79.93 134.00 o 15 4 2 43.43 148.10 142.23 o 1 5 2 28572.68 29579.87 849.62 o 2 5 2 20.30 8.23 67.00 o 3 5 2 26215.81 26483.77 812.86 o 4 5 2 24.64 59.95 75.23 o 5 5 2 12944.22 13593.75 404.92 o 6 5 2 84.52 38.79 88.16 o 7 5 2 12899.41 13645.68 628.95 o 8 5 2 2334.38 2238.32 107.03 o 9 5 2 11130.50 12002.09 420.90 o 10 5 2 324.67 363.23 85.81 o 11 5 2 3777.06 3998.97 188.24 o 12 5 2 407.73 486.67 132.83 o 13 5 2 1377.61 1604.94 122.28 o 14 5 2 140.60 219.81 142.23 o 0 6 2 1318.27 1212.38 156.40 o 1 6 2 131.53 95.21 96.39 o 2 6 2 17.92 -84.63 84.63 o 3 6 2 117.58 189.25 90.51 o 4 6 2 198.90 171.62 81.11 o 5 6 2 3.73 17.63 114.02 o 6 6 2 1904.38 1911.09 104.67 o 7 6 2 401.96 359.72 104.62 o 8 6 2 398.76 383.23 88.17 o 9 6 2 1198.61 1132.27 111.70 o 10 6 2 31.20 -52.89 110.49 o 11 6 2 750.06 738.29 142.25 o 12 6 2 22.64 15.28 115.19 o 13 6 2 400.42 418.48 168.10 o 1 7 2 6036.32 6175.63 301.42 o 2 7 2 273.29 330.32 104.62 o 3 7 2 2139.26 2276.96 161.13 o 4 7 2 27.46 -52.89 94.03 o 5 7 2 859.89 1065.17 125.80 o 6 7 2 293.57 362.06 90.51 o 7 7 2 1865.81 1668.69 190.51 o 8 7 2 195.86 365.57 109.32 o 9 7 2 1097.94 997.01 128.15 o 10 7 2 0.23 -34.09 136.35 o 11 7 2 417.96 309.16 185.73 o 0 8 2 783.87 822.96 137.55 o 1 8 2 194.19 201.01 90.51 o 2 8 2 1450.40 1298.13 114.06 o 3 8 2 151.15 139.88 115.20 o 4 8 2 227.86 155.16 114.02 o 5 8 2 289.84 176.32 102.27 o 6 8 2 200.72 372.62 128.13 o 7 8 2 477.36 392.63 132.84 o 8 8 2 337.69 355.00 161.04 o 9 8 2 490.97 545.45 136.36 o 1 9 2 2.97 -4.70 101.09 o 2 9 2 18.05 71.70 117.54 o 3 9 2 209.63 193.95 138.71 o 4 9 2 16.98 123.42 125.77 o 5 9 2 127.61 126.95 141.05 o 6 9 2 14.03 119.89 130.47 o 2 1 3 3494.91 3959.40 142.76 o 3 1 3 64441.79 62751.48 1991.72 o 4 1 3 385.99 496.16 55.26 o 5 1 3 61593.41 59828.45 1810.03 o 6 1 3 758.67 718.45 65.85 o 7 1 3 41095.90 40515.84 1032.64 o 8 1 3 221.14 244.51 64.65 o 9 1 3 14327.20 14494.19 409.93 o 10 1 3 727.78 733.63 91.70 o 11 1 3 6949.63 6690.14 280.33 o 12 1 3 41.40 74.05 84.63 o 13 1 3 6605.39 6586.46 365.00 o 14 1 3 9.63 -84.63 111.66 o 15 1 3 1239.06 1251.00 172.84 o 16 1 3 207.62 125.78 157.51 o 0 2 3 12522.35 11207.47 798.50 o 1 2 3 13022.97 12785.92 376.69 o 2 2 3 4767.34 4789.66 153.36 o 3 2 3 52.71 -54.07 54.07 o 4 2 3 2008.37 1893.50 83.55 o 5 2 3 411.55 442.05 54.08 o 6 2 3 4.59 -19.98 65.82 o 7 2 3 2616.23 2625.18 96.49 o 8 2 3 483.39 558.42 69.36 o 9 2 3 1647.58 1731.18 85.85 o 10 2 3 445.72 574.86 98.75 o 11 2 3 3158.46 3455.34 144.71 o 12 2 3 442.59 490.21 96.40 o 13 2 3 1811.67 1615.76 116.42 o 14 2 3 26.10 338.52 103.44 o 15 2 3 1029.71 999.34 145.79 o 16 2 3 3.95 67.00 168.08 o 1 3 3 11621.93 11435.13 374.03 o 2 3 3 75.91 -101.09 101.09 o 3 3 3 5201.10 4983.47 166.19 o 4 3 3 324.14 311.53 81.12 o 5 3 3 16484.90 16819.73 459.42 o 6 3 3 2833.31 2924.29 110.62 o 7 3 3 3132.84 3120.86 102.38 o 8 3 3 1385.79 1506.43 95.25 o 9 3 3 1122.96 1254.62 96.42 o 10 3 3 182.25 -10.58 77.58 o 11 3 3 2671.02 2324.34 128.21 o 12 3 3 54.27 -35.26 128.12 o 13 3 3 583.94 573.69 108.15 o 14 3 3 29.39 82.28 153.98 o 15 3 3 450.76 345.61 146.94 o 0 4 3 3684.26 3472.33 182.51 o 1 4 3 401.12 569.01 84.65 o 2 4 3 4559.03 4648.97 155.48 o 3 4 3 4884.84 4643.31 147.24 o 4 4 3 2299.93 2162.45 107.06 o 5 4 3 2048.44 2171.53 89.40 o 6 4 3 1618.56 1579.50 88.21 o 7 4 3 1206.15 1093.58 87.02 o 8 4 3 175.03 204.53 97.56 o 9 4 3 2938.24 2991.67 134.11 o 10 4 3 310.77 224.52 101.09 o 11 4 3 3110.65 3243.26 149.40 o 12 4 3 890.58 900.57 128.15 o 13 4 3 3372.50 3457.29 171.75 o 14 4 3 54.96 -3.53 138.70 o 15 4 3 1379.96 1512.03 146.97 o 1 5 3 4179.16 3774.40 150.69 o 2 5 3 45.21 39.96 67.00 o 3 5 3 3614.43 3504.99 110.63 o 4 5 3 1312.55 1325.30 134.06 o 5 5 3 612.38 618.40 125.80 o 6 5 3 94.23 45.84 88.16 o 7 5 3 178.86 228.04 77.58 o 8 5 3 24.21 196.30 79.93 o 9 5 3 2341.55 2191.20 119.97 o 10 5 3 47.15 108.14 96.39 o 11 5 3 490.94 644.21 116.38 o 12 5 3 2.69 51.72 98.74 o 13 5 3 38.56 96.38 126.95 o 14 5 3 17.49 -131.65 131.65 o 0 6 3 432.49 277.44 102.28 o 1 6 3 173.27 166.92 86.99 o 2 6 3 700.12 847.67 108.16 o 3 6 3 431.20 430.26 92.87 o 4 6 3 884.72 672.52 83.48 o 5 6 3 657.61 585.47 105.81 o 6 6 3 603.61 624.25 90.52 o 7 6 3 498.99 464.35 92.87 o 8 6 3 251.84 343.24 104.62 o 9 6 3 1280.42 1100.54 115.23 o 10 6 3 529.49 484.33 109.33 o 11 6 3 1351.95 1470.91 124.63 o 12 6 3 20.83 -37.61 131.65 o 13 6 3 637.63 506.67 155.18 o 1 7 3 7334.48 7395.75 277.97 o 2 7 3 0.56 -84.63 84.63 o 3 7 3 7811.35 7752.09 285.06 o 4 7 3 51.07 -72.88 141.05 o 5 7 3 7587.94 7517.71 348.62 o 6 7 3 300.36 288.00 101.09 o 7 7 3 4499.39 4638.68 181.22 o 8 7 3 199.42 380.85 108.14 o 9 7 3 2192.34 2196.80 149.35 o 10 7 3 1.14 52.89 161.03 o 11 7 3 1307.35 1286.27 131.68 o 0 8 3 311.55 5.88 238.63 o 1 8 3 191.14 115.20 98.74 o 2 8 3 14.61 -104.61 105.79 o 3 8 3 188.21 136.35 104.62 o 4 8 3 241.36 335.01 110.50 o 5 8 3 17.25 57.60 146.93 o 6 8 3 1.84 30.56 114.02 o 7 8 3 8.68 21.16 110.49 o 8 8 3 4.83 55.24 165.73 o 9 8 3 1.87 -134.00 134.00 o 1 9 3 3834.33 3948.17 169.41 o 2 9 3 0.21 114.02 146.93 o 3 9 3 3016.41 3419.27 165.85 o 4 9 3 5.58 138.70 117.54 o 5 9 3 2498.54 2316.85 172.88 o 6 9 3 6.82 123.42 135.17 o 2 0 4 114327.78 121393.74 11052.24 o 3 0 4 288.32 543.18 70.54 o 4 0 4 85933.05 84672.49 3284.67 o 5 0 4 5348.33 5326.35 219.33 o 6 0 4 26564.26 25220.79 850.58 o 7 0 4 4112.52 3558.62 183.70 o 8 0 4 17845.20 17302.10 754.01 o 9 0 4 202.40 98.74 115.20 o 10 0 4 9877.63 9691.67 475.21 o 11 0 4 2568.46 2209.12 223.50 o 12 0 4 2816.90 2611.46 191.74 o 13 0 4 189.93 165.74 124.60 o 14 0 4 849.28 614.87 181.05 o 15 0 4 1262.77 1007.62 166.96 o 16 0 4 1328.97 1270.99 202.23 o 1 1 4 4786.35 5464.03 335.67 o 2 1 4 1063.34 1411.97 71.78 o 3 1 4 29786.76 28776.17 790.68 o 4 1 4 586.23 428.02 47.04 o 5 1 4 9.95 24.68 55.24 o 6 1 4 2.48 67.00 68.17 o 7 1 4 1989.27 2082.29 89.41 o 8 1 4 4316.61 4542.36 140.11 o 9 1 4 296.94 293.88 81.11 o 10 1 4 705.53 733.63 77.60 o 11 1 4 1668.78 1653.45 114.07 o 12 1 4 84.36 -84.63 125.77 o 13 1 4 316.00 550.14 99.92 o 14 1 4 188.17 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