#------------------------------------------------------------------------------ #$Date: 2016-04-02 20:33:49 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180765 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/86/2008655.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008655_Fobs loop_ _publ_author_name 'Hempel, A.' 'Camerman, N.' 'Mastropaolo, D.' 'Camerman, A.' _publ_section_title ; Bis(2,2-dimethylaziridinyl)phosphinic amide ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1173 _journal_page_last 1175 _journal_volume 55 _journal_year 1999 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 96.440 _cell_angle_beta 84.110 _cell_angle_gamma 78.880 _cell_length_a 5.2750 _cell_length_b 9.7470 _cell_length_c 11.4510 _exptl_crystal_F_000 220.00 _reflns_d_resolution_high 0.8506 _cod_data_source_file bk1457sup2.hkl _cod_data_source_block azir #BEGIN Tags that were not found in dictionaries: _shelx_title ' Aziridinyl #3 C8H18N3OP P1 bar Z=2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 88.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4115.23 5459.39 244.20 o 2 0 0 15.10 19.30 0.68 o 3 0 0 166.17 159.98 1.48 o 4 0 0 297.93 315.54 10.32 o 5 0 0 158.14 165.91 5.48 o 6 0 0 10.72 11.47 0.49 o -5 1 0 140.90 108.50 3.55 o -4 1 0 282.13 285.87 13.22 o -3 1 0 51.46 46.81 2.24 o -2 1 0 0.48 1.62 0.23 o -1 1 0 674.67 750.72 33.66 o 0 1 0 3416.10 2643.16 118.24 o 1 1 0 7908.86 9529.59 426.25 o 2 1 0 80.43 81.48 3.79 o 3 1 0 334.50 328.73 15.15 o 4 1 0 496.03 525.34 24.21 o 5 1 0 141.67 141.09 6.62 o 6 1 0 17.19 15.67 0.89 o -5 2 0 78.95 84.82 4.02 o -4 2 0 224.21 235.53 10.92 o -3 2 0 24.64 25.97 1.31 o -2 2 0 72.43 70.40 3.29 o -1 2 0 1550.00 1776.53 79.54 o 0 2 0 56.18 53.76 2.51 o 1 2 0 349.88 346.83 15.93 o 2 2 0 225.09 215.35 9.93 o 3 2 0 326.10 331.28 15.27 o 4 2 0 597.26 624.03 28.74 o 5 2 0 112.34 117.56 5.55 o 6 2 0 4.61 5.36 0.46 o -5 3 0 63.14 74.45 3.54 o -4 3 0 134.78 147.35 6.89 o -3 3 0 80.07 84.26 3.97 o -2 3 0 17.42 13.87 0.74 o -1 3 0 1211.83 1313.07 58.87 o 0 3 0 2752.17 2908.10 130.13 o 1 3 0 1.62 4.31 0.35 o 2 3 0 12.29 11.20 0.65 o 3 3 0 464.03 498.83 22.96 o 4 3 0 765.06 827.60 38.07 o 5 3 0 254.11 274.85 12.75 o 6 3 0 8.98 9.89 0.64 o -5 4 0 36.59 42.25 2.06 o -4 4 0 23.64 23.97 1.27 o -3 4 0 146.77 150.91 7.04 o -2 4 0 185.84 185.66 8.60 o -1 4 0 97.75 95.22 4.43 o 0 4 0 1303.65 1469.91 13.45 o 1 4 0 184.95 180.02 8.31 o 2 4 0 63.34 82.18 3.85 o 3 4 0 35.46 35.57 1.78 o 4 4 0 230.73 246.09 11.42 o 5 4 0 197.30 207.11 9.65 o 6 4 0 30.78 34.54 1.71 o -4 5 0 0.20 0.45 0.32 o -3 5 0 17.58 18.70 1.04 o -2 5 0 230.08 238.97 11.06 o -1 5 0 257.69 247.05 11.40 o 0 5 0 50.57 57.57 2.77 o 1 5 0 127.89 135.72 6.30 o 2 5 0 73.23 77.40 3.65 o 3 5 0 80.60 78.28 3.73 o 4 5 0 41.97 45.32 2.27 o 5 5 0 20.83 19.92 1.14 o -4 6 0 18.97 20.41 1.07 o -3 6 0 15.78 14.14 0.84 o -2 6 0 3.87 3.82 0.47 o -1 6 0 455.12 437.00 20.13 o 0 6 0 62.11 58.31 2.83 o 1 6 0 2.39 2.09 0.45 o 2 6 0 39.84 34.86 1.76 o 3 6 0 153.50 153.28 7.17 o 4 6 0 79.73 84.49 4.05 o 5 6 0 3.07 4.72 0.48 o -3 7 0 7.03 7.93 0.57 o -2 7 0 1.04 1.09 0.37 o -1 7 0 71.77 73.52 3.51 o 0 7 0 160.79 182.03 8.50 o 1 7 0 46.26 45.93 2.27 o 2 7 0 117.50 120.03 5.65 o 3 7 0 177.44 186.04 8.68 o 4 7 0 98.56 103.86 4.93 o 5 7 0 8.69 9.47 0.65 o -3 8 0 1.86 2.32 0.33 o -2 8 0 23.96 24.44 1.30 o -1 8 0 0.62 1.25 0.38 o 0 8 0 21.58 20.67 1.28 o 1 8 0 22.02 19.66 1.16 o 2 8 0 23.61 24.92 1.39 o 3 8 0 115.67 114.16 5.40 o 4 8 0 58.31 58.54 2.85 o 5 8 0 18.04 19.74 1.06 o -2 9 0 23.69 21.63 1.15 o -1 9 0 126.33 116.00 5.46 o 0 9 0 19.74 22.33 1.32 o 1 9 0 21.12 20.42 1.19 o 2 9 0 3.16 3.58 0.57 o 3 9 0 30.28 31.51 1.64 o 4 9 0 14.43 13.52 0.81 o -1 10 0 16.40 13.30 0.77 o 0 10 0 66.86 71.77 3.50 o 1 10 0 22.58 21.66 1.22 o 2 10 0 1.81 2.14 0.48 o 3 10 0 17.50 18.39 1.03 o 4 10 0 20.71 19.61 1.07 o 0 11 0 3.92 4.16 0.51 o 1 11 0 18.56 17.14 0.97 o 2 11 0 11.64 11.78 0.75 o -2 -11 1 3.31 3.31 0.43 o -1 -11 1 26.51 21.38 1.14 o 0 -11 1 7.64 9.15 0.67 o -4 -10 1 15.96 15.14 0.88 o -3 -10 1 12.52 10.95 0.76 o -2 -10 1 13.83 12.28 0.82 o -1 -10 1 97.86 82.95 3.97 o 0 -10 1 42.21 46.08 2.32 o 1 -10 1 1.25 0.57 0.31 o -4 -9 1 0.03 0.71 0.37 o -3 -9 1 1.54 1.46 0.48 o -2 -9 1 16.37 10.19 0.83 o -1 -9 1 54.10 44.90 2.26 o 0 -9 1 54.47 54.37 2.73 o 1 -9 1 9.64 9.93 0.67 o 2 -9 1 1.28 0.59 0.31 o -5 -8 1 6.36 7.93 0.57 o -4 -8 1 1.84 1.20 0.43 o -3 -8 1 13.61 15.55 0.97 o -2 -8 1 35.73 31.45 1.65 o -1 -8 1 90.40 81.71 3.91 o 0 -8 1 96.80 110.61 5.27 o 1 -8 1 33.97 28.53 1.49 o 2 -8 1 14.86 13.84 0.83 o 3 -8 1 1.30 1.45 0.31 o -5 -7 1 0.12 0.00 0.36 o -4 -7 1 0.85 1.83 0.48 o -3 -7 1 15.04 13.82 0.91 o -2 -7 1 4.03 1.87 0.55 o -1 -7 1 28.83 23.65 1.28 o 0 -7 1 4.44 5.86 0.68 o 1 -7 1 51.46 44.82 2.20 o 2 -7 1 114.84 97.68 4.63 o 3 -7 1 13.42 11.86 0.73 o 4 -7 1 6.12 5.84 0.45 o -5 -6 1 9.66 9.44 0.66 o -4 -6 1 83.81 85.32 4.08 o -3 -6 1 1.66 0.25 0.52 o -2 -6 1 55.86 56.60 2.73 o -1 -6 1 92.02 81.03 3.82 o 0 -6 1 69.31 87.86 4.16 o 1 -6 1 120.57 114.07 5.34 o 2 -6 1 80.28 76.54 3.64 o 3 -6 1 112.31 105.05 4.96 o 4 -6 1 7.47 6.65 0.49 o -5 -5 1 0.09 0.00 0.44 o -4 -5 1 270.31 277.16 12.86 o -3 -5 1 212.42 211.97 9.84 o -2 -5 1 4.07 4.35 0.46 o -1 -5 1 0.37 0.00 0.36 o 0 -5 1 104.05 120.61 5.63 o 1 -5 1 197.86 207.25 9.58 o 2 -5 1 4.35 3.64 0.42 o 3 -5 1 81.99 86.77 4.11 o 4 -5 1 25.56 24.86 1.30 o -6 -4 1 3.81 3.34 0.45 o -5 -4 1 9.00 7.85 0.68 o -4 -4 1 24.14 24.50 1.35 o -3 -4 1 75.16 74.45 3.54 o -2 -4 1 113.08 116.14 5.40 o -1 -4 1 14.70 18.07 0.93 o 0 -4 1 1332.73 1528.48 68.59 o 1 -4 1 190.15 203.56 9.39 o 2 -4 1 6.37 9.47 0.59 o 3 -4 1 0.07 0.57 0.37 o 4 -4 1 2.24 2.23 0.41 o 5 -4 1 0.49 1.05 0.30 o -6 -3 1 0.18 0.08 0.36 o -5 -3 1 15.09 15.92 0.98 o -4 -3 1 42.73 45.94 2.28 o -3 -3 1 16.58 17.39 0.96 o -2 -3 1 410.80 427.34 19.65 o -1 -3 1 1058.43 1249.30 56.04 o 0 -3 1 749.41 805.97 36.16 o 1 -3 1 215.08 243.64 11.21 o 2 -3 1 225.77 213.68 9.86 o 3 -3 1 37.51 41.34 2.02 o 4 -3 1 38.64 40.90 2.03 o 5 -3 1 38.09 41.07 2.02 o -6 -2 1 0.06 1.42 0.34 o -5 -2 1 21.39 21.75 1.22 o -4 -2 1 142.51 148.16 6.93 o -3 -2 1 36.93 35.11 1.73 o -2 -2 1 9.94 12.25 0.67 o -1 -2 1 26.08 28.55 1.36 o 0 -2 1 1006.85 934.07 41.84 o 1 -2 1 2173.79 2612.85 116.90 o 2 -2 1 6.66 7.79 0.46 o 3 -2 1 73.90 78.85 3.71 o 4 -2 1 2.67 2.78 0.42 o 5 -2 1 38.53 40.84 2.02 o -6 -1 1 4.39 5.04 0.47 o -5 -1 1 14.19 14.86 0.93 o -4 -1 1 134.62 135.47 6.35 o -3 -1 1 35.22 34.36 1.69 o -2 -1 1 171.28 181.42 8.37 o -1 -1 1 51.47 64.32 2.98 o 0 -1 1 5.23 5.03 0.29 o 1 -1 1 120.13 133.57 6.15 o 2 -1 1 1.57 2.35 0.25 o 3 -1 1 3.35 3.03 0.33 o 4 -1 1 33.77 39.06 1.93 o 5 -1 1 15.27 9.77 0.59 o -5 0 1 15.70 16.70 0.68 o -4 0 1 41.53 40.46 1.42 o -3 0 1 62.83 56.28 1.89 o -2 0 1 28.07 27.52 0.94 o -1 0 1 4.75 3.29 0.19 o 0 0 1 199.68 159.45 7.20 o 1 0 1 121.43 125.95 4.10 o 2 0 1 614.50 657.56 21.34 o 3 0 1 228.70 255.75 8.35 o 4 0 1 10.06 11.49 0.53 o 5 0 1 14.05 13.83 0.60 o 6 0 1 5.27 5.43 0.69 o -5 1 1 15.12 10.54 0.68 o -4 1 1 8.18 9.13 0.62 o -3 1 1 4.06 3.97 0.38 o -2 1 1 6.90 7.07 0.42 o -1 1 1 1.48 2.45 0.22 o 0 1 1 183.13 172.21 7.74 o 1 1 1 174.55 180.22 8.29 o 2 1 1 31.11 22.26 1.10 o 3 1 1 41.38 54.07 2.58 o 4 1 1 2.22 3.03 0.53 o 5 1 1 17.46 15.60 0.97 o 6 1 1 2.16 2.01 0.38 o -5 2 1 12.68 15.62 0.88 o -4 2 1 5.67 6.21 0.54 o -3 2 1 6.26 7.62 0.54 o -2 2 1 138.77 134.70 6.24 o -1 2 1 708.19 716.96 32.34 o 0 2 1 137.28 130.92 6.04 o 1 2 1 39.78 36.93 1.74 o 2 2 1 0.67 1.75 0.30 o 3 2 1 62.88 64.36 3.05 o 4 2 1 0.78 1.08 0.50 o 5 2 1 0.02 0.00 0.45 o 6 2 1 0.45 0.39 0.36 o -5 3 1 34.29 42.16 2.05 o -4 3 1 9.98 11.00 0.70 o -3 3 1 82.04 91.40 4.31 o -2 3 1 93.26 107.32 5.00 o -1 3 1 393.39 378.70 17.41 o 0 3 1 160.69 158.98 7.34 o 1 3 1 12.44 12.18 0.66 o 2 3 1 35.55 39.44 1.89 o 3 3 1 32.02 30.00 1.51 o 4 3 1 83.70 89.79 4.27 o 5 3 1 0.81 1.97 0.49 o 6 3 1 1.46 2.04 0.38 o -5 4 1 64.88 70.07 3.32 o -4 4 1 128.23 139.75 6.55 o -3 4 1 28.47 32.05 1.62 o -2 4 1 96.08 99.76 4.67 o -1 4 1 1.09 3.22 0.32 o 0 4 1 5.11 7.63 0.53 o 1 4 1 61.57 67.63 3.17 o 2 4 1 0.37 0.24 0.35 o 3 4 1 5.01 5.49 0.54 o 4 4 1 35.99 36.89 1.88 o 5 4 1 18.85 19.23 1.11 o 6 4 1 0.08 0.00 0.35 o -4 5 1 73.72 74.80 3.56 o -3 5 1 194.97 206.81 9.62 o -2 5 1 155.92 162.58 7.57 o -1 5 1 156.98 136.56 6.35 o 0 5 1 182.38 181.26 8.41 o 1 5 1 0.26 0.05 0.35 o 2 5 1 95.37 98.22 4.60 o 3 5 1 125.81 125.38 5.88 o 4 5 1 3.90 3.96 0.61 o 5 5 1 6.20 5.82 0.58 o -4 6 1 24.30 24.34 1.25 o -3 6 1 46.09 44.62 2.20 o -2 6 1 140.45 134.23 6.29 o -1 6 1 184.36 179.07 8.32 o 0 6 1 170.57 199.92 9.30 o 1 6 1 0.86 0.57 0.43 o 2 6 1 17.79 18.52 1.04 o 3 6 1 119.44 130.25 6.12 o 4 6 1 105.13 114.12 5.40 o 5 6 1 6.43 7.49 0.61 o -3 7 1 23.82 23.04 1.21 o -2 7 1 43.25 38.07 1.91 o -1 7 1 197.74 178.88 8.33 o 0 7 1 355.14 406.58 18.80 o 1 7 1 255.52 248.61 11.53 o 2 7 1 0.16 0.00 0.52 o 3 7 1 13.25 14.20 0.93 o 4 7 1 39.26 40.70 2.07 o 5 7 1 12.84 13.65 0.82 o -3 8 1 46.05 40.29 1.97 o -2 8 1 6.30 5.36 0.48 o -1 8 1 31.75 25.00 1.33 o 0 8 1 170.16 178.23 8.37 o 1 8 1 387.62 384.61 17.78 o 2 8 1 320.54 310.44 14.39 o 3 8 1 30.67 31.22 1.65 o 4 8 1 20.05 19.95 1.13 o 5 8 1 30.38 33.63 1.67 o -2 9 1 39.22 33.63 1.68 o -1 9 1 12.46 10.33 0.68 o 0 9 1 53.23 50.88 2.58 o 1 9 1 72.68 61.96 3.03 o 2 9 1 120.20 115.44 5.46 o 3 9 1 109.88 111.01 5.25 o 4 9 1 40.06 40.77 2.02 o -1 10 1 8.72 6.78 0.51 o 0 10 1 33.84 34.04 1.80 o 1 10 1 74.37 66.22 3.20 o 2 10 1 21.76 18.96 1.08 o 3 10 1 33.32 30.19 1.55 o 1 11 1 33.84 28.95 1.48 o 2 11 1 17.71 15.32 0.88 o -2 -11 2 8.13 6.95 0.55 o -1 -11 2 45.76 41.88 2.06 o 0 -11 2 44.93 46.77 2.31 o -3 -10 2 0.36 0.00 0.42 o -2 -10 2 2.66 3.21 0.49 o -1 -10 2 27.07 25.31 1.37 o 0 -10 2 33.05 37.60 1.94 o 1 -10 2 40.25 38.28 1.89 o -4 -9 2 16.85 16.68 0.94 o -3 -9 2 10.97 10.63 0.77 o -2 -9 2 20.28 19.64 1.17 o -1 -9 2 20.31 23.28 1.32 o 0 -9 2 0.40 0.49 0.57 o 1 -9 2 4.84 6.04 0.51 o 2 -9 2 73.28 70.56 3.36 o -5 -8 2 77.75 86.31 4.06 o -4 -8 2 44.83 48.24 2.37 o -3 -8 2 60.80 55.12 2.73 o -2 -8 2 212.22 192.51 8.98 o -1 -8 2 232.99 231.90 10.78 o 0 -8 2 17.68 24.39 1.40 o 1 -8 2 26.62 23.95 1.29 o 2 -8 2 7.82 7.70 0.58 o 3 -8 2 67.67 65.67 3.13 o -5 -7 2 42.43 43.14 2.12 o -4 -7 2 16.94 17.24 1.03 o -3 -7 2 12.39 13.98 0.92 o -2 -7 2 226.26 224.69 10.44 o -1 -7 2 394.10 385.48 17.80 o 0 -7 2 178.04 203.30 9.48 o 1 -7 2 22.34 29.34 1.51 o 2 -7 2 1.82 1.57 0.40 o 3 -7 2 52.75 54.74 2.66 o 4 -7 2 22.39 19.77 1.04 o -5 -6 2 59.17 61.29 2.96 o -4 -6 2 42.90 44.31 2.23 o -3 -6 2 16.02 16.23 0.99 o -2 -6 2 299.81 302.16 13.97 o -1 -6 2 556.95 581.84 26.77 o 0 -6 2 69.42 79.39 3.78 o 1 -6 2 44.08 49.70 2.40 o 2 -6 2 56.60 51.30 2.50 o 3 -6 2 32.28 31.06 1.59 o 4 -6 2 25.92 27.09 1.38 o -5 -5 2 88.65 97.10 4.60 o -4 -5 2 75.58 79.67 3.82 o -3 -5 2 36.69 37.51 1.89 o -2 -5 2 210.93 216.28 10.01 o -1 -5 2 1649.34 1971.40 88.40 o 0 -5 2 911.16 1071.07 48.34 o 1 -5 2 167.00 174.86 8.10 o 2 -5 2 468.97 485.53 22.36 o 3 -5 2 208.47 211.40 9.82 o 4 -5 2 44.72 46.13 2.26 o -5 -4 2 127.42 136.37 6.40 o -4 -4 2 148.78 159.24 7.45 o -3 -4 2 175.51 178.24 8.29 o -2 -4 2 4.15 5.30 0.45 o -1 -4 2 22.40 20.73 1.06 o 0 -4 2 855.00 716.85 26.19 o 1 -4 2 173.47 157.02 7.26 o 2 -4 2 332.02 326.19 15.04 o 3 -4 2 570.38 598.94 27.57 o 4 -4 2 143.30 147.83 6.91 o 5 -4 2 40.70 48.36 2.33 o -6 -3 2 18.76 18.99 1.03 o -5 -3 2 62.59 65.94 3.19 o -4 -3 2 175.04 180.14 8.40 o -3 -3 2 454.28 490.56 22.59 o -2 -3 2 1222.26 1275.80 57.54 o -1 -3 2 34.03 32.93 1.58 o 0 -3 2 65.09 61.66 2.89 o 1 -3 2 363.25 342.34 15.74 o 2 -3 2 49.77 42.51 2.03 o 3 -3 2 331.37 342.98 15.82 o 4 -3 2 173.13 176.22 8.21 o 5 -3 2 38.13 37.85 1.89 o -5 -2 2 34.34 35.30 1.81 o -4 -2 2 159.97 162.91 7.61 o -3 -2 2 255.52 267.21 12.35 o -2 -2 2 1228.24 1273.69 57.44 o -1 -2 2 2428.82 2555.98 114.44 o 0 -2 2 261.95 238.68 10.98 o 1 -2 2 711.36 699.40 31.37 o 2 -2 2 287.88 247.05 11.38 o 3 -2 2 251.42 245.66 11.35 o 4 -2 2 301.63 318.43 14.72 o 5 -2 2 76.80 82.11 3.90 o -5 -1 2 26.38 25.91 1.38 o -4 -1 2 90.12 89.82 4.28 o -3 -1 2 350.12 351.11 16.19 o -2 -1 2 314.31 349.43 16.07 o -1 -1 2 2232.49 2317.13 103.74 o 0 -1 2 5012.92 3880.72 173.62 o 1 -1 2 914.66 871.16 39.08 o 2 -1 2 275.00 271.08 12.48 o 3 -1 2 43.20 37.90 1.83 o 4 -1 2 133.00 139.14 6.50 o 5 -1 2 134.10 107.73 4.26 o -5 0 2 15.24 15.35 0.64 o -4 0 2 2.79 2.16 0.32 o -3 0 2 106.74 101.38 3.36 o -2 0 2 145.68 122.88 4.03 o -1 0 2 289.15 270.66 8.79 o 0 0 2 2103.44 2042.03 62.38 o 1 0 2 3439.97 3502.28 154.51 o 2 0 2 947.93 978.61 31.20 o 3 0 2 185.81 188.22 6.16 o 4 0 2 25.69 22.22 1.34 o 5 0 2 65.31 64.64 2.69 o 6 0 2 35.17 35.63 1.35 o -5 1 2 24.53 27.84 1.42 o -4 1 2 12.10 14.80 0.86 o -3 1 2 3.56 5.03 0.42 o -2 1 2 501.89 522.28 24.00 o -1 1 2 0.92 0.73 0.20 o 0 1 2 543.04 487.66 21.88 o 1 1 2 537.12 477.26 21.53 o 2 1 2 537.31 562.09 25.82 o 3 1 2 611.69 634.75 29.18 o 4 1 2 153.92 154.95 7.24 o 5 1 2 38.46 39.92 2.01 o 6 1 2 26.82 25.29 1.31 o -5 2 2 10.34 11.51 0.69 o -4 2 2 19.42 20.73 1.13 o -3 2 2 7.18 8.34 0.57 o -2 2 2 54.53 50.31 2.38 o -1 2 2 1559.75 1737.30 77.92 o 0 2 2 277.37 271.52 12.49 o 1 2 2 302.89 254.58 11.71 o 2 2 2 281.48 275.59 12.69 o 3 2 2 371.55 387.73 17.86 o 4 2 2 328.00 338.95 15.67 o 5 2 2 81.15 92.54 4.40 o 6 2 2 19.12 19.97 1.07 o -5 3 2 13.78 16.04 0.88 o -4 3 2 5.90 6.76 0.55 o -3 3 2 1.76 1.54 0.36 o -2 3 2 71.79 84.38 3.95 o -1 3 2 5.54 3.66 0.32 o 0 3 2 7.34 5.27 0.42 o 1 3 2 192.32 239.67 11.04 o 2 3 2 7.60 10.90 0.64 o 3 3 2 48.34 48.02 2.32 o 4 3 2 152.56 150.22 7.03 o 5 3 2 128.57 136.64 6.42 o 6 3 2 33.92 35.25 1.75 o -4 4 2 0.04 1.00 0.34 o -3 4 2 0.04 0.03 0.37 o -2 4 2 66.28 70.88 3.35 o -1 4 2 40.02 32.36 1.58 o 0 4 2 32.17 26.43 1.34 o 1 4 2 113.03 131.03 6.08 o 2 4 2 38.55 42.16 2.04 o 3 4 2 4.70 7.32 0.58 o 4 4 2 0.22 0.55 0.50 o 5 4 2 7.32 8.17 0.66 o 6 4 2 13.78 12.58 0.76 o -4 5 2 4.17 3.97 0.42 o -3 5 2 47.30 48.62 2.38 o -2 5 2 4.64 5.67 0.50 o -1 5 2 268.08 283.41 13.09 o 0 5 2 135.91 138.47 6.46 o 1 5 2 2.73 3.44 0.45 o 2 5 2 0.51 0.00 0.43 o 3 5 2 182.74 179.47 8.36 o 4 5 2 52.85 53.96 2.66 o 5 5 2 0.37 0.00 0.43 o -4 6 2 4.79 4.77 0.41 o -3 6 2 1.15 0.82 0.35 o -2 6 2 14.39 14.71 0.87 o -1 6 2 90.85 92.21 4.36 o 0 6 2 95.34 104.71 4.95 o 1 6 2 4.09 4.47 0.54 o 2 6 2 18.12 18.16 1.04 o 3 6 2 46.16 43.97 2.20 o 4 6 2 82.33 84.29 4.04 o 5 6 2 0.12 0.54 0.39 o -3 7 2 1.61 1.47 0.31 o -2 7 2 3.51 3.10 0.43 o -1 7 2 2.23 2.42 0.45 o 0 7 2 8.54 9.48 0.84 o 1 7 2 3.42 2.69 0.56 o 2 7 2 1.58 2.21 0.54 o 3 7 2 32.47 28.68 1.57 o 4 7 2 43.94 42.48 2.14 o 5 7 2 0.51 0.08 0.38 o -3 8 2 3.29 2.35 0.33 o -2 8 2 1.82 2.17 0.36 o -1 8 2 18.05 15.11 0.91 o 0 8 2 2.48 3.14 0.62 o 1 8 2 40.16 41.55 2.10 o 2 8 2 3.77 5.23 0.64 o 3 8 2 35.75 32.98 1.73 o 4 8 2 31.12 32.04 1.65 o 5 8 2 5.17 5.29 0.50 o -2 9 2 0.01 0.00 0.28 o -1 9 2 8.97 9.08 0.61 o 0 9 2 38.46 43.16 2.22 o 1 9 2 4.61 3.78 0.61 o 2 9 2 0.18 1.02 0.49 o 3 9 2 16.93 16.58 0.99 o 4 9 2 13.03 11.20 0.73 o -1 10 2 3.35 1.99 0.35 o 0 10 2 10.28 12.89 0.84 o 1 10 2 0.02 0.31 0.43 o 2 10 2 1.36 1.52 0.42 o 3 10 2 3.84 3.78 0.47 o 1 11 2 2.70 1.19 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