#------------------------------------------------------------------------------ #$Date: 2016-04-02 20:34:04 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180767 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/88/2008882.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008882_Fobs loop_ _publ_author_name 'Cave, G. W. V.' 'Errington, W.' 'Rourke, J. P.' _publ_section_title ; (6-Chloropyridin-2-yl)iodobis(triphenylphosphine)palladium(II) ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1461 _journal_page_last 1463 _journal_volume 55 _journal_year 1999 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.451 _cell_angle_gamma 90.000 _cell_length_a 12.1621 _cell_length_b 14.7472 _cell_length_c 20.8082 _exptl_crystal_F_000 1728.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file cf1319sup2.hkl _cod_data_source_block jpr1 #BEGIN Tags that were not found in dictionaries: _shelx_title ' jpr1 in P2(1)/n (SADABS corrected data)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 418.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 10516.03 9244.00 442.89 o 6 0 0 18.81 56.69 185.19 o 8 0 0 842.44 515.56 146.66 o 10 0 0 8972.32 9852.50 671.31 o 12 0 0 117.23 442.55 445.27 o 14 0 0 122.49 567.14 567.14 o 1 1 0 1715.35 2412.53 80.39 o 2 1 0 1081.89 931.04 52.58 o 3 1 0 10698.37 12766.35 223.62 o 4 1 0 16066.10 15634.66 234.64 o 5 1 0 2517.64 2175.54 120.85 o 6 1 0 3029.31 4094.99 153.73 o 7 1 0 402.97 462.63 105.05 o 8 1 0 614.46 653.02 104.97 o 9 1 0 439.21 312.03 204.11 o 10 1 0 8524.57 9710.21 729.87 o 11 1 0 36.63 -77.30 207.40 o 12 1 0 14219.93 15795.71 894.29 o 13 1 0 0.04 145.12 328.33 o 14 1 0 2392.48 2901.05 493.31 o 0 2 0 172155.78 176643.13 2828.91 o 1 2 0 1345.27 1464.81 72.52 o 2 2 0 22055.39 18824.44 417.06 o 3 2 0 27543.29 30321.05 476.90 o 4 2 0 2362.41 3819.90 203.82 o 5 2 0 1996.27 1849.31 134.93 o 6 2 0 604.13 709.56 91.09 o 7 2 0 8717.66 9150.44 241.09 o 8 2 0 3324.97 3029.02 201.62 o 9 2 0 177.20 183.83 175.72 o 10 2 0 12501.51 13286.31 550.02 o 11 2 0 79.12 36.69 208.32 o 12 2 0 385.65 515.19 445.61 o 13 2 0 10.87 218.22 265.90 o 1 3 0 24956.12 22532.01 272.17 o 2 3 0 20094.75 20502.78 867.06 o 3 3 0 40000.44 40622.70 447.12 o 4 3 0 12213.31 12461.40 221.00 o 5 3 0 9857.74 8906.99 200.93 o 6 3 0 161.97 217.20 79.87 o 7 3 0 6995.75 6731.15 323.41 o 8 3 0 361.17 431.30 144.99 o 9 3 0 824.98 608.30 153.51 o 10 3 0 2187.47 2288.84 438.46 o 11 3 0 126.42 184.55 199.52 o 12 3 0 12024.47 12393.02 582.28 o 13 3 0 30.12 245.31 278.84 o 0 4 0 85498.59 82552.42 1508.07 o 1 4 0 422.58 475.17 131.18 o 2 4 0 9480.56 8484.31 147.33 o 3 4 0 633.69 397.66 73.07 o 4 4 0 262.23 494.90 121.44 o 5 4 0 5190.20 4634.92 162.00 o 6 4 0 81.15 155.99 118.22 o 7 4 0 9125.58 8915.91 234.29 o 8 4 0 2836.20 3314.87 404.42 o 9 4 0 1020.25 743.26 167.40 o 10 4 0 9380.48 9630.99 704.67 o 11 4 0 646.08 821.05 251.96 o 12 4 0 147.45 432.87 245.36 o 13 4 0 79.36 120.51 392.17 o 1 5 0 7292.94 5843.18 318.10 o 2 5 0 6535.02 6489.93 127.89 o 3 5 0 4636.65 3424.39 183.78 o 4 5 0 10651.81 10811.83 252.70 o 5 5 0 29291.21 30195.82 428.58 o 6 5 0 4723.46 4992.14 188.07 o 7 5 0 7801.03 7811.58 247.50 o 8 5 0 19.96 -79.21 128.65 o 9 5 0 416.83 443.97 259.64 o 10 5 0 503.16 714.04 257.83 o 11 5 0 34.04 -149.60 362.21 o 12 5 0 6237.70 5662.78 477.01 o 13 5 0 24.59 125.07 355.40 o 0 6 0 23631.05 26978.47 716.93 o 1 6 0 40.99 15.31 66.58 o 2 6 0 1043.77 832.49 92.38 o 3 6 0 1408.24 1868.19 136.67 o 4 6 0 10543.27 11764.71 284.07 o 5 6 0 12485.79 13517.36 329.00 o 6 6 0 4113.36 4124.16 179.96 o 7 6 0 7832.09 7846.80 295.76 o 8 6 0 1958.38 1792.26 194.59 o 9 6 0 1054.02 975.59 178.60 o 10 6 0 4631.80 4682.50 294.14 o 11 6 0 1234.58 1882.47 380.27 o 12 6 0 33.57 -267.18 268.23 o 13 6 0 16.01 121.52 612.76 o 1 7 0 1098.72 669.89 129.46 o 2 7 0 7734.42 7771.57 175.30 o 3 7 0 18918.64 18159.92 277.54 o 4 7 0 1234.97 1108.52 138.62 o 5 7 0 21079.61 21229.07 379.09 o 6 7 0 5563.99 5668.85 211.59 o 7 7 0 7573.41 6894.83 293.38 o 8 7 0 1946.58 1857.93 276.64 o 9 7 0 3.41 230.60 209.05 o 10 7 0 29.44 346.45 183.77 o 11 7 0 12.45 315.23 353.36 o 12 7 0 646.22 171.38 750.29 o 0 8 0 12496.63 13574.00 546.72 o 1 8 0 1617.77 1477.08 124.88 o 2 8 0 469.19 217.71 79.48 o 3 8 0 678.28 1011.91 163.64 o 4 8 0 6090.28 6093.44 247.55 o 5 8 0 4248.24 4173.43 191.54 o 6 8 0 3956.61 3919.89 233.13 o 7 8 0 13624.96 14168.39 502.79 o 8 8 0 46.36 -85.81 132.41 o 9 8 0 2851.59 3211.62 256.12 o 10 8 0 3780.75 3557.93 339.53 o 11 8 0 49.34 479.24 308.76 o 12 8 0 342.87 -59.20 299.33 o 1 9 0 89.47 -106.24 79.82 o 2 9 0 2634.38 3081.82 228.70 o 3 9 0 7711.59 7401.66 271.59 o 4 9 0 5667.00 5627.11 261.51 o 5 9 0 8318.09 8544.76 474.24 o 6 9 0 5876.53 6208.89 255.73 o 7 9 0 3061.43 3108.33 360.81 o 8 9 0 7791.27 8272.91 380.92 o 9 9 0 59.61 -88.41 175.03 o 10 9 0 188.53 656.03 214.81 o 11 9 0 0.12 175.15 246.33 o 12 9 0 14.05 -318.99 401.02 o 0 10 0 1.34 -82.38 188.59 o 1 10 0 2865.31 3274.35 242.67 o 2 10 0 4809.34 5546.21 288.28 o 3 10 0 450.27 478.46 168.86 o 4 10 0 4658.10 5106.21 330.42 o 5 10 0 1222.78 1162.75 340.02 o 6 10 0 4520.97 5107.70 338.89 o 7 10 0 4102.72 3731.05 284.68 o 8 10 0 111.03 -29.65 184.38 o 9 10 0 1479.97 1705.29 267.86 o 10 10 0 1274.50 1102.22 248.67 o 11 10 0 136.65 -35.65 223.06 o 1 11 0 53.14 -113.05 129.29 o 2 11 0 6450.90 6363.41 337.48 o 3 11 0 4311.90 4309.16 246.22 o 4 11 0 8.08 109.06 146.69 o 5 11 0 1803.33 2215.62 229.87 o 6 11 0 3667.28 3768.03 278.01 o 7 11 0 2239.91 2099.42 236.43 o 8 11 0 7391.82 8074.04 407.00 o 9 11 0 1423.47 1169.00 327.69 o 10 11 0 1350.49 1525.55 343.64 o 0 12 0 4737.13 4932.72 489.53 o 1 12 0 50.32 74.89 215.15 o 2 12 0 468.99 753.04 180.08 o 3 12 0 5453.61 5218.76 344.37 o 4 12 0 6659.50 7261.60 327.63 o 5 12 0 212.32 194.19 163.93 o 6 12 0 1089.80 936.28 437.27 o 7 12 0 2627.18 2418.55 334.32 o 8 12 0 4.19 7.74 195.11 o 9 12 0 259.79 154.06 260.39 o 10 12 0 913.47 744.07 320.50 o 1 13 0 2254.78 1889.04 279.76 o 2 13 0 92.69 186.90 154.85 o 3 13 0 1650.45 1334.73 250.64 o 4 13 0 1894.41 1390.94 218.33 o 5 13 0 1386.10 1138.49 208.90 o 6 13 0 1865.29 2202.07 257.34 o 7 13 0 4.98 -101.03 237.34 o 8 13 0 3332.72 3657.67 429.36 o 9 13 0 2149.19 1609.96 345.88 o 0 14 0 882.81 1350.12 378.55 o 1 14 0 274.21 388.47 230.76 o 2 14 0 990.61 1219.79 232.00 o 3 14 0 6598.02 6471.73 494.63 o 4 14 0 2059.96 1952.74 540.93 o 5 14 0 41.93 83.07 214.94 o 6 14 0 1715.89 1932.96 317.36 o 7 14 0 258.06 444.59 433.70 o 8 14 0 29.75 -234.79 242.81 o 1 15 0 1395.83 1802.11 299.36 o 2 15 0 574.78 631.96 257.28 o 3 15 0 96.86 144.30 262.37 o 4 15 0 12.11 -26.18 254.51 o 5 15 0 299.14 -257.36 305.02 o 6 15 0 82.25 -34.27 251.35 o 7 15 0 76.11 -64.07 263.13 o 0 16 0 445.96 725.78 393.53 o 1 16 0 11.65 -261.18 187.05 o 2 16 0 126.71 62.06 417.02 o 3 16 0 6732.49 7043.32 603.91 o 4 16 0 280.59 745.52 521.53 o 5 16 0 61.85 49.02 402.38 o 1 17 0 1457.87 2050.48 472.85 o 2 17 0 264.87 109.18 318.20 o 3 17 0 156.31 114.64 340.21 o -13 0 1 53.82 -98.04 405.78 o -11 0 1 4286.76 4735.96 582.80 o -9 0 1 187.62 483.40 249.19 o -7 0 1 204.40 214.35 219.23 o -5 0 1 35129.20 41368.09 1149.27 o -3 0 1 2829.54 1803.00 97.08 o -1 0 1 136316.63 130339.55 2164.41 o 1 0 1 26532.13 23390.60 329.48 o 3 0 1 78287.75 77445.03 2478.27 o 5 0 1 18.24 112.23 97.32 o 7 0 1 21638.74 23245.61 526.59 o 9 0 1 20027.89 21496.99 901.44 o 11 0 1 2315.17 1799.47 439.83 o 13 0 1 135.94 704.67 526.97 o -14 1 1 26.82 760.41 382.77 o -13 1 1 7213.04 8324.60 578.94 o -12 1 1 127.69 53.47 328.51 o -11 1 1 15436.05 16394.38 653.94 o -10 1 1 173.34 196.55 194.15 o -9 1 1 753.45 629.02 194.85 o -8 1 1 3493.20 3398.89 192.55 o -7 1 1 1330.69 1085.90 100.12 o -6 1 1 1789.76 1487.84 96.60 o -5 1 1 13791.26 12749.65 215.32 o -4 1 1 2895.16 3334.26 127.26 o -3 1 1 99601.13 101858.32 1800.73 o -2 1 1 141.39 23.35 31.64 o -1 1 1 17240.11 17425.71 179.06 o 0 1 1 100.57 52.06 20.21 o 1 1 1 25068.76 33131.93 362.69 o 2 1 1 46.84 29.54 35.44 o 3 1 1 6130.44 7051.78 185.85 o 4 1 1 1617.60 1488.95 97.10 o 5 1 1 1623.60 1801.10 102.24 o 6 1 1 723.34 774.89 94.12 o 7 1 1 472.31 407.56 99.02 o 8 1 1 432.68 310.02 151.24 o 9 1 1 28.80 8.92 193.23 o 10 1 1 5.20 13.08 185.14 o 11 1 1 16640.77 17280.60 653.02 o 12 1 1 29.58 159.55 499.74 o 13 1 1 5415.99 6744.39 549.04 o -14 2 1 78.61 -367.60 262.51 o -13 2 1 27.58 211.28 283.57 o -12 2 1 191.04 450.26 311.83 o -11 2 1 5475.73 4811.68 461.61 o -10 2 1 166.87 240.43 196.66 o -9 2 1 1502.79 1552.41 407.15 o -8 2 1 1156.95 1134.77 155.09 o -7 2 1 199.08 154.80 83.87 o -6 2 1 1663.68 1636.42 105.73 o -5 2 1 8412.89 10797.35 229.37 o -4 2 1 7223.11 7037.62 179.15 o -3 2 1 37106.26 37288.95 393.03 o -2 2 1 16187.20 16910.91 209.44 o -1 2 1 75834.88 77230.46 774.37 o 0 2 1 10098.70 10646.87 156.47 o 1 2 1 59353.03 53044.13 680.73 o 2 2 1 14947.16 17627.50 257.90 o 3 2 1 10042.93 8726.20 166.30 o 4 2 1 306.52 316.81 72.43 o 5 2 1 7217.68 9555.88 232.17 o 6 2 1 7258.78 7341.13 203.81 o 7 2 1 16963.07 17292.04 335.02 o 8 2 1 2573.55 2405.10 175.82 o 9 2 1 6937.54 7350.54 295.49 o 10 2 1 444.73 143.30 473.53 o 11 2 1 2921.46 3144.14 490.21 o 12 2 1 4.37 11.05 229.30 o 13 2 1 443.06 434.72 278.75 o -13 3 1 3655.51 3082.86 523.57 o -12 3 1 1078.48 992.75 436.42 o -11 3 1 5685.17 6275.01 870.46 o -10 3 1 318.71 297.04 196.42 o -9 3 1 778.59 680.20 150.06 o -8 3 1 1535.69 1565.86 163.78 o -7 3 1 444.71 655.04 105.82 o -6 3 1 2163.18 2128.30 177.48 o -5 3 1 4335.06 3718.06 132.66 o -4 3 1 15862.26 15807.18 248.82 o -3 3 1 82214.99 88224.84 816.79 o -2 3 1 1023.65 766.73 70.61 o -1 3 1 56103.87 58488.58 1196.69 o 1 3 1 41822.39 48116.27 454.03 o 2 3 1 22967.74 21943.39 260.02 o 3 3 1 3750.70 4639.41 128.00 o 4 3 1 4626.49 4124.97 178.46 o 5 3 1 4730.54 5304.77 164.98 o 6 3 1 15434.88 14964.82 282.87 o 7 3 1 2830.79 3099.65 158.73 o 8 3 1 3816.00 3393.74 216.19 o 9 3 1 198.76 105.49 125.24 o 10 3 1 691.09 555.39 485.44 o 11 3 1 10580.62 11418.98 548.26 o 12 3 1 594.65 486.12 247.31 o 13 3 1 2595.25 3519.60 399.83 o -13 4 1 185.63 90.01 258.42 o -12 4 1 2360.94 2548.34 337.89 o -11 4 1 2085.23 1830.92 296.53 o -10 4 1 43.13 81.75 204.81 o -9 4 1 6.59 -59.79 132.02 o -8 4 1 11270.88 10998.47 331.02 o -7 4 1 20.94 34.45 100.10 o -6 4 1 4278.01 4056.72 156.80 o -5 4 1 4144.16 4421.19 151.98 o -4 4 1 20338.32 20640.31 304.91 o -3 4 1 7109.23 7089.42 161.27 o -2 4 1 7369.85 6586.99 167.10 o -1 4 1 93699.06 93591.40 1481.78 o 0 4 1 14346.06 14076.73 429.27 o 1 4 1 12244.15 11159.68 158.00 o 2 4 1 7811.46 7927.17 155.59 o 3 4 1 209.58 420.42 78.60 o 4 4 1 2505.61 2863.22 132.73 o 5 4 1 1803.70 2535.70 131.39 o 6 4 1 6807.58 6788.90 205.30 o 7 4 1 3570.13 3386.76 167.04 o 8 4 1 4098.22 3728.10 224.33 o 9 4 1 16601.37 16787.70 456.43 o 10 4 1 322.28 -16.74 173.68 o 11 4 1 1305.74 1521.47 334.29 o 12 4 1 113.04 140.82 436.08 o 13 4 1 219.59 139.60 489.87 o -13 5 1 1634.14 1724.07 372.38 o -12 5 1 1230.28 1326.23 308.48 o -11 5 1 3195.97 3079.52 377.20 o -10 5 1 3806.29 3581.02 361.48 o -9 5 1 1673.10 1672.28 200.93 o -8 5 1 877.45 879.55 150.18 o -7 5 1 3508.40 3326.90 361.16 o -6 5 1 15295.22 15076.00 607.55 o -5 5 1 6764.30 6730.50 215.82 o -4 5 1 14201.33 14587.33 297.86 o -3 5 1 28956.91 32259.27 469.57 o -2 5 1 5442.60 4497.66 102.16 o -1 5 1 10462.06 11076.75 233.95 o 0 5 1 9966.25 8352.60 345.19 o 1 5 1 11353.64 13069.32 203.89 o 2 5 1 932.46 358.47 65.44 o 3 5 1 7132.16 7515.13 210.03 o 4 5 1 33480.88 32610.41 439.56 o 5 5 1 3270.04 3313.51 175.92 o 6 5 1 11224.48 11523.39 273.22 o 7 5 1 3298.01 3214.64 179.11 o 8 5 1 6795.96 6342.73 683.47 o 9 5 1 356.13 207.03 288.85 o 10 5 1 626.13 751.52 199.45 o 11 5 1 3777.03 3598.09 380.38 o 12 5 1 80.88 -147.50 461.61 o 13 5 1 1170.25 1132.60 782.63 o -13 6 1 278.99 958.05 761.18 o -12 6 1 1222.81 1411.57 351.68 o -11 6 1 910.07 898.45 305.26 o -10 6 1 1510.43 1767.88 237.77 o -9 6 1 1538.82 1612.53 209.97 o -8 6 1 6543.32 6383.29 291.73 o -7 6 1 580.54 619.28 276.25 o -6 6 1 9188.78 9446.00 245.99 o -5 6 1 11209.78 11672.49 280.24 o -4 6 1 7098.67 6375.23 192.30 o -3 6 1 8401.45 8964.88 253.51 o -2 6 1 2527.92 2175.41 122.18 o -1 6 1 10020.75 10428.79 280.28 o 0 6 1 2785.06 2248.15 224.68 o 1 6 1 1460.94 1155.90 84.26 o 2 6 1 6011.40 6599.53 161.60 o 3 6 1 2116.05 1936.23 123.43 o 4 6 1 9708.21 10330.18 423.40 o 5 6 1 8738.79 9166.04 236.35 o 6 6 1 2356.68 2143.61 156.54 o 7 6 1 2511.64 2355.49 169.28 o 8 6 1 3060.24 3391.56 273.07 o 9 6 1 6079.74 6315.31 317.76 o 10 6 1 289.23 28.46 213.88 o 11 6 1 804.98 1281.28 377.39 o 12 6 1 2.26 31.59 300.62 o 13 6 1 715.58 188.24 336.28 o -13 7 1 937.55 843.51 569.19 o -12 7 1 1386.47 1146.61 333.94 o -11 7 1 59.38 -183.83 370.38 o -10 7 1 3014.05 2315.17 272.94 o -9 7 1 7290.76 7461.86 344.54 o -8 7 1 374.55 564.73 172.04 o -7 7 1 4213.65 4374.10 250.68 o -6 7 1 5768.42 5526.78 238.52 o -5 7 1 110.82 -12.44 92.19 o -4 7 1 18708.80 18138.92 450.33 o -3 7 1 3511.38 3588.93 149.19 o -2 7 1 179.10 21.57 70.50 o -1 7 1 10772.94 12379.26 357.35 o 0 7 1 9600.21 9311.55 304.67 o 1 7 1 30659.88 33348.62 481.79 o 2 7 1 5370.62 4691.56 134.58 o 3 7 1 625.98 735.39 97.21 o 4 7 1 23874.74 23230.54 446.90 o 5 7 1 57.92 131.47 94.16 o 6 7 1 14186.38 13525.22 311.07 o 7 7 1 2361.34 2300.60 223.87 o 8 7 1 1929.32 1932.07 201.63 o 9 7 1 1257.38 1010.54 181.50 o 10 7 1 826.54 1208.25 207.99 o 11 7 1 3000.17 2984.69 397.60 o 12 7 1 10.77 -228.20 268.87 o -12 8 1 429.78 353.87 303.44 o -11 8 1 3821.79 3395.89 382.44 o -10 8 1 726.75 924.29 217.54 o -9 8 1 295.00 303.18 183.27 o -8 8 1 12392.53 12398.91 668.70 o -7 8 1 242.67 305.18 271.66 o -6 8 1 2548.70 2790.43 189.18 o -5 8 1 11650.61 11470.89 284.14 o -4 8 1 2248.95 2017.52 161.60 o -3 8 1 483.60 425.42 108.03 o -2 8 1 1654.43 1424.49 191.17 o -1 8 1 1438.39 1564.58 218.55 o 0 8 1 1371.57 1094.69 278.81 o 1 8 1 1818.40 1692.96 122.20 o 2 8 1 14571.43 15550.73 272.43 o 3 8 1 3869.36 3499.87 249.30 o 4 8 1 848.16 652.98 125.60 o 5 8 1 14735.66 15335.58 380.98 o 6 8 1 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