#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/10/2011058.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011058_Fobs loop_ _publ_author_name 'Figgis, Brian N.' 'Sobolev, Alexandre N.' 'Kucharski, Edward S.' 'Broughton, Vanessa' _publ_section_title ; Rinneite, K~3~Na[FeCl~6~], at 293, 84 and 9.5K ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e228 _journal_page_last e229 _journal_volume 56 _journal_year 2000 _space_group_IT_number 167 _symmetry_space_group_name_Hall '-R 3 2"c' _symmetry_space_group_name_H-M 'R -3 c :H' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 11.8930 _cell_length_b 11.8930 _cell_length_c 13.7350 _exptl_crystal_F_000 1176.00 _reflns_d_resolution_high 0.4629 _[local]_cod_data_source_file qb021010Ksup4.hkl _[local]_cod_data_source_block 10K #BEGIN Tags that were not found in dictionaries: _shelx_title ' rinn10K in R-3c at 9.5 K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 463.52 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'y, x, -z+1/2' 'x-y, -y, -z+1/2' '-x, -x+y, -z+1/2' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'y+2/3, x+1/3, -z+5/6' 'x-y+2/3, -y+1/3, -z+5/6' '-x+2/3, -x+y+1/3, -z+5/6' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' 'y+1/3, x+2/3, -z+7/6' 'x-y+1/3, -y+2/3, -z+7/6' '-x+1/3, -x+y+2/3, -z+7/6' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-y, -x, z-1/2' '-x+y, y, z-1/2' 'x, x-y, z-1/2' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-y+2/3, -x+1/3, z-1/6' '-x+y+2/3, y+1/3, z-1/6' 'x+2/3, x-y+1/3, z-1/6' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' '-y+1/3, -x+2/3, z+1/6' '-x+y+1/3, y+2/3, z+1/6' 'x+1/3, x-y+2/3, z+1/6' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -1 2 0 21644.12 23034.68 227.44 o 0 3 0 52641.14 47542.18 500.12 o -2 4 0 13635.64 14395.42 118.80 o -1 5 0 21449.91 21012.53 133.56 o -3 6 0 37382.93 36642.41 309.87 o 0 6 0 208145.17 190419.72 1489.09 o -2 7 0 44923.86 44801.96 314.13 o -4 8 0 1462.79 1474.38 11.52 o -1 8 0 10458.25 10544.48 50.68 o -3 9 0 1214.81 1320.00 12.03 o 0 9 0 2569.08 2606.38 49.47 o -5 10 0 29488.77 29689.89 384.57 o -2 10 0 9121.12 9162.98 50.60 o -4 11 0 10440.23 10352.87 73.59 o -1 11 0 8048.74 8185.03 47.28 o -6 12 0 15194.15 15330.42 187.02 o -3 12 0 10709.75 10876.89 65.84 o 0 12 0 6005.46 6079.67 35.43 o -5 13 0 43136.73 43977.11 372.93 o -2 13 0 32500.51 32886.96 133.94 o -7 14 0 1490.71 1088.78 15.84 o -4 14 0 179.61 258.94 12.13 o -1 14 0 876.94 920.82 7.28 o -6 15 0 4309.50 4282.64 31.11 o -3 15 0 982.78 1088.33 20.32 o 0 15 0 684.65 648.84 14.08 o -8 16 0 27614.80 28013.63 306.20 o -5 16 0 7326.31 7340.43 40.61 o -2 16 0 8351.39 8327.67 45.63 o -7 17 0 1602.37 1701.45 25.07 o -4 17 0 3794.76 3893.76 34.81 o -1 17 0 318.11 363.45 9.66 o -9 18 0 20245.34 20240.89 218.61 o -6 18 0 41.47 148.26 23.31 o -3 18 0 20375.80 20712.08 156.11 o 0 18 0 1752.60 1774.49 17.81 o -8 19 0 18202.62 18163.06 112.38 o -5 19 0 6687.20 6760.31 49.43 o -2 19 0 3324.45 3353.24 27.49 o -10 20 0 1457.31 1437.85 22.67 o -7 20 0 1011.51 1041.82 15.74 o -4 20 0 1313.60 1376.81 17.47 o -1 20 0 66.98 110.28 8.63 o -9 21 0 290.78 316.71 9.95 o -6 21 0 50.79 143.76 19.01 o -3 21 0 7354.07 7406.33 66.62 o 0 21 0 6096.25 6020.86 99.13 o -11 22 0 38.08 58.38 14.13 o -8 22 0 5675.11 5655.55 47.45 o -5 22 0 70.41 100.49 6.22 o -2 22 0 1263.16 1300.91 12.77 o -10 23 0 5125.95 5098.69 34.76 o -7 23 0 2318.64 2354.68 18.34 o -4 23 0 720.08 734.27 11.67 o -12 24 0 185.44 261.72 15.69 o -9 24 0 14378.01 14121.48 130.19 o -6 24 0 399.81 431.19 8.13 o -11 25 0 1612.63 1592.96 16.82 o -8 25 0 802.33 828.80 12.26 o -2 3 1 4157.35 4361.85 29.94 o -1 4 1 101224.83 97187.12 3052.03 o -3 5 1 12248.51 12282.42 90.31 o -5 6 1 37666.04 37123.79 256.81 o -2 6 1 1615.08 1646.85 11.26 o -4 7 1 5357.30 5143.79 44.71 o -1 7 1 48162.13 48079.20 235.01 o -6 8 1 14928.45 14671.76 98.97 o -3 8 1 498.10 537.94 4.84 o -8 9 1 1205.36 1240.24 10.19 o -5 9 1 11643.78 11577.89 98.29 o -2 9 1 5522.45 5557.96 32.04 o -7 10 1 36722.14 37065.68 251.21 o -4 10 1 4159.13 4210.43 32.94 o -1 10 1 25850.54 25737.01 114.13 o -9 11 1 2358.36 2394.98 16.77 o -6 11 1 6748.91 6698.48 57.37 o -3 11 1 290.91 351.22 11.28 o -11 12 1 3578.89 3622.01 20.91 o -8 12 1 15687.16 15517.18 106.66 o -5 12 1 24478.39 24573.08 172.31 o -2 12 1 39.30 247.40 39.40 o -10 13 1 11481.67 11527.77 64.62 o -7 13 1 1067.79 1234.52 42.69 o -4 13 1 16.13 37.56 3.64 o -1 13 1 5600.23 5581.91 15.53 o -12 14 1 34997.09 35708.06 126.66 o -9 14 1 1190.08 1252.70 12.51 o -6 14 1 5729.52 5706.34 39.63 o -3 14 1 3812.91 3832.45 22.25 o -14 15 1 6572.38 6528.67 34.20 o -11 15 1 5556.03 5609.92 44.44 o -8 15 1 290.80 340.26 8.51 o -5 15 1 22.46 83.48 6.69 o -2 15 1 3856.37 3939.10 16.09 o -13 16 1 8214.97 8219.02 46.18 o -10 16 1 107.40 185.19 7.30 o -7 16 1 1136.34 1165.13 11.32 o -4 16 1 383.54 420.32 5.26 o -1 16 1 1816.61 1837.83 12.44 o -15 17 1 4421.20 4460.79 24.64 o -12 17 1 2645.67 2685.40 22.14 o -9 17 1 79.34 152.09 17.14 o -6 17 1 9882.45 9822.62 54.38 o -3 17 1 239.01 271.03 9.67 o -17 18 1 2.77 111.74 24.07 o -14 18 1 12432.69 12374.99 69.50 o -11 18 1 1003.50 1113.44 29.44 o -8 18 1 2552.00 2548.36 21.72 o -5 18 1 1884.62 1915.69 23.45 o -2 18 1 650.40 691.03 12.42 o -16 19 1 3558.53 3563.52 21.90 o -13 19 1 1831.77 1848.00 17.70 o -10 19 1 4636.28 4637.35 33.30 o -7 19 1 5213.43 5166.44 33.19 o -4 19 1 219.34 241.83 6.03 o -1 19 1 645.10 694.08 14.60 o -18 20 1 7080.56 7093.68 51.38 o -15 20 1 1831.10 1867.30 21.65 o -12 20 1 3755.23 3831.13 33.65 o -9 20 1 3981.10 3927.26 26.65 o -6 20 1 408.97 446.21 9.79 o -3 20 1 7618.22 7621.65 62.74 o -20 21 1 782.07 797.64 6.95 o -17 21 1 1006.00 1025.49 11.20 o -14 21 1 16.97 86.96 15.23 o -11 21 1 2457.02 2427.98 21.86 o -8 21 1 2568.56 2559.86 29.01 o -5 21 1 3267.79 3252.34 32.19 o -2 21 1 2591.72 2626.67 20.00 o -19 22 1 2532.38 2552.05 28.65 o -16 22 1 1449.11 1511.72 15.88 o -13 22 1 22.01 61.37 5.28 o -10 22 1 283.88 306.97 6.41 o -7 22 1 5826.23 5821.27 36.49 o -4 22 1 1231.99 1223.42 10.33 o -1 22 1 3581.81 3505.43 28.31 o -21 23 1 34.46 86.68 10.60 o -18 23 1 422.32 451.30 8.07 o -15 23 1 293.31 305.80 6.65 o -12 23 1 5631.23 5567.41 42.85 o -9 23 1 1193.78 1194.64 13.88 o -6 23 1 4509.36 4421.93 31.28 o -3 23 1 349.46 389.14 12.67 o -17 24 1 239.15 263.46 5.83 o -14 24 1 39.73 66.79 5.38 o -11 24 1 34.15 47.90 5.95 o -8 24 1 10.44 42.57 6.03 o -5 24 1 15.06 37.01 4.74 o -16 25 1 62.90 83.33 5.96 o -13 25 1 3539.12 3485.05 35.65 o -10 25 1 634.44 663.64 11.50 o 0 1 2 37929.46 38042.40 427.86 o -2 2 2 4300.00 4243.75 42.62 o -1 3 2 935.08 1293.79 34.61 o -3 4 2 58841.81 56419.25 408.85 o 0 4 2 231.36 236.58 5.17 o -5 5 2 1115.94 1111.21 8.30 o -2 5 2 8204.39 8274.27 71.48 o -4 6 2 13498.77 13630.09 136.08 o -1 6 2 17871.58 17279.27 89.66 o -6 7 2 18640.83 18377.53 101.12 o -3 7 2 26876.92 26896.10 223.65 o 0 7 2 3355.06 3320.08 41.98 o -8 8 2 1169.73 1237.31 20.86 o -5 8 2 49100.96 48686.93 432.03 o -2 8 2 10944.84 10798.39 73.32 o -7 9 2 4440.87 4477.76 31.21 o -4 9 2 27706.11 28181.13 242.70 o -1 9 2 5780.60 5624.57 31.10 o -9 10 2 50441.97 50586.65 148.51 o -6 10 2 618.55 618.53 6.21 o -3 10 2 20300.80 20617.97 121.15 o 0 10 2 25930.55 25222.09 189.94 o -11 11 2 1519.05 1515.81 12.27 o -8 11 2 11890.31 11890.08 74.89 o -5 11 2 1991.38 2118.37 33.09 o -2 11 2 2025.52 2230.51 37.71 o -10 12 2 1394.11 1417.51 6.96 o -7 12 2 7634.95 7591.90 63.98 o -4 12 2 15398.53 15425.85 106.22 o -1 12 2 23457.83 23379.51 72.78 o -12 13 2 229.19 299.78 9.53 o -9 13 2 12262.83 12294.96 86.76 o -6 13 2 57.36 164.58 13.09 o -3 13 2 1334.86 1383.46 11.06 o 0 13 2 3352.30 3328.08 23.09 o -14 14 2 9960.52 10069.44 49.83 o -11 14 2 4509.71 4620.59 45.03 o -8 14 2 11232.13 11353.16 88.71 o -5 14 2 5900.77 5840.74 36.70 o -2 14 2 19926.19 20074.05 92.51 o -13 15 2 590.40 660.51 11.91 o -10 15 2 8525.30 8579.82 53.64 o -7 15 2 1383.93 1435.43 13.40 o -4 15 2 6808.73 6975.46 78.24 o -1 15 2 998.37 1017.44 11.14 o -15 16 2 14513.26 14628.73 93.98 o -12 16 2 50.34 104.89 5.03 o -9 16 2 16962.35 17110.62 120.64 o -6 16 2 8888.64 8857.90 55.35 o -3 16 2 6.88 98.48 18.49 o 0 16 2 17280.92 17009.61 149.99 o -17 17 2 16.07 52.13 6.77 o -14 17 2 1453.72 1494.72 18.12 o -11 17 2 1189.45 1363.95 71.34 o -8 17 2 2535.67 2543.26 33.03 o -5 17 2 13410.85 13266.59 106.44 o -2 17 2 4043.84 4065.94 31.58 o -16 18 2 531.35 581.71 16.61 o -13 18 2 3893.78 3916.25 25.95 o -10 18 2 10.30 94.93 13.92 o -7 18 2 3140.79 3185.72 27.87 o -4 18 2 8653.18 8655.60 72.14 o -1 18 2 16175.52 16077.79 123.56 o -18 19 2 1410.14 1442.54 11.17 o -15 19 2 7806.95 7920.57 57.78 o -12 19 2 354.11 392.30 10.26 o -9 19 2 4546.09 4551.96 39.81 o -6 19 2 8.24 110.85 15.48 o -3 19 2 103.37 144.99 7.73 o 0 19 2 138.12 165.98 9.35 o -20 20 2 4868.90 4940.42 58.22 o -17 20 2 3801.72 3801.13 28.90 o -14 20 2 8748.18 8803.70 52.43 o -11 20 2 795.73 823.03 13.67 o -8 20 2 5719.63 5670.95 45.92 o -5 20 2 175.22 201.64 8.71 o -2 20 2 3152.89 3181.97 34.99 o -19 21 2 587.33 642.97 10.74 o -16 21 2 34.49 45.89 5.66 o -13 21 2 1797.83 1754.55 19.07 o -10 21 2 62.50 98.50 5.26 o -7 21 2 482.34 499.56 14.23 o -4 21 2 740.86 744.94 8.62 o -1 21 2 39.88 48.83 5.23 o -21 22 2 3701.03 3723.31 29.68 o -18 22 2 1367.40 1387.43 15.79 o -15 22 2 8322.01 8392.60 52.09 o -12 22 2 974.26 1016.98 9.44 o -9 22 2 1702.12 1728.59 13.39 o -6 22 2 155.87 197.40 8.35 o -3 22 2 13.51 79.82 15.15 o 0 22 2 39.05 42.59 6.83 o -20 23 2 3191.09 3184.26 32.91 o -17 23 2 102.12 145.83 9.16 o -14 23 2 5088.96 5107.14 36.49 o -11 23 2 1943.66 1976.71 12.42 o -8 23 2 1150.27 1171.89 11.85 o -5 23 2 2713.88 2694.14 23.68 o -2 23 2 42.90 78.79 5.98 o -19 24 2 3650.18 3614.52 38.55 o -16 24 2 912.47 949.10 14.22 o -13 24 2 837.19 847.99 15.12 o -10 24 2 724.00 723.82 10.38 o -7 24 2 4940.49 4886.23 54.20 o -15 25 2 3739.18 3700.70 42.74 o -12 25 2 1719.70 1675.06 18.87 o -9 25 2 1685.38 1646.27 18.34 o -1 2 3 10494.64 9763.09 66.65 o -2 4 3 214846.31 243393.00 1064.34 o -4 5 3 853.39 814.88 4.62 o -1 5 3 4075.27 4025.75 31.76 o -3 6 3 1351.71 1958.83 167.50 o -5 7 3 974.70 1072.17 19.49 o -2 7 3 14243.42 14054.61 107.53 o -7 8 3 2325.52 2291.67 13.42 o -4 8 3 21391.82 21239.03 169.97 o -1 8 3 54.06 83.93 3.95 o -6 9 3 3109.62 3051.85 18.54 o -3 9 3 2817.43 2833.13 26.67 o -8 10 3 6027.24 6018.00 29.48 o -5 10 3 2457.35 2481.71 21.65 o -2 10 3 10505.03 10564.78 63.19 o -10 11 3 6104.81 6033.26 18.98 o -7 11 3 6337.20 6330.38 48.39 o -4 11 3 49859.19 51079.75 342.35 o -1 11 3 55.44 138.78 10.15 o -9 12 3 4208.80 4241.32 21.87 o -6 12 3 9048.33 9082.00 73.58 o -3 12 3 4551.99 4565.80 31.51 o -11 13 3 670.84 713.38 5.68 o -8 13 3 8591.89 8607.86 73.94 o -5 13 3 15.87 140.43 15.64 o -2 13 3 26820.37 26764.13 118.78 o -13 14 3 0.26 54.68 9.04 o -10 14 3 4983.42 5059.89 23.01 o -7 14 3 274.03 331.79 7.81 o -4 14 3 1345.48 1388.81 15.66 o -1 14 3 805.97 832.69 9.37 o -12 15 3 2228.70 2238.41 12.38 o -9 15 3 6917.80 6938.92 39.31 o -6 15 3 7271.96 7239.49 46.24 o -3 15 3 1849.49 1874.58 12.31 o -14 16 3 1160.13 1204.29 16.31 o -11 16 3 6430.52 6462.23 39.28 o -8 16 3 37.34 182.19 20.00 o -5 16 3 8765.45 8730.92 52.06 o -2 16 3 653.83 663.56 8.01 o -16 17 3 871.01 910.93 8.72 o -13 17 3 1854.93 1858.83 15.33 o -10 17 3 18589.03 18606.25 146.30 o -7 17 3 5695.17 5667.11 51.96 o -4 17 3 18660.26 18415.23 142.05 o -1 17 3 1984.32 2003.40 22.72 o -15 18 3 511.75 578.42 9.60 o -12 18 3 3295.04 3315.27 43.45 o -9 18 3 4540.17 4578.69 29.32 o -6 18 3 3356.67 3346.90 35.30 o -3 18 3 729.39 759.24 8.26 o -17 19 3 1036.31 1072.74 11.30 o -14 19 3 18.43 63.46 9.50 o -11 19 3 343.99 395.60 6.94 o -8 19 3 5712.11 5689.61 44.30 o -5 19 3 115.56 153.60 9.25 o -2 19 3 1174.34 1201.69 13.34 o -19 20 3 6108.27 6153.21 51.42 o -16 20 3 2393.62 2412.48 21.59 o -13 20 3 3396.03 3387.76 21.77 o -10 20 3 5018.95 5039.27 37.75 o -7 20 3 3552.76 3542.26 34.91 o -4 20 3 45.71 80.76 6.22 o -1 20 3 5064.29 5057.58 45.35 o -18 21 3 47.53 86.08 6.98 o -15 21 3 151.85 170.00 5.77 o -12 21 3 436.19 436.59 7.58 o -9 21 3 366.89 393.00 7.64 o -6 21 3 158.81 196.64 14.02 o -3 21 3 11.48 49.86 13.79 o -20 22 3 352.40 361.69 6.24 o -17 22 3 6676.71 6758.87 52.16 o -14 22 3 1794.81 1797.28 14.63 o -11 22 3 5333.48 5239.10 41.40 o -8 22 3 156.78 173.33 6.23 o -5 22 3 6769.88 6698.49 59.61 o -2 22 3 1589.45 1590.99 16.76 o -19 23 3 1385.58 1398.94 14.58 o -16 23 3 24.66 52.99 6.91 o -13 23 3 1096.93 1133.45 10.04 o -10 23 3 2494.98 2491.93 20.33 o -7 23 3 216.74 238.78 5.86 o -4 23 3 35.33 64.54 6.11 o -18 24 3 4.92 38.71 5.15 o -15 24 3 125.90 153.28 5.17 o -12 24 3 48.21 72.66 4.98 o -9 24 3 82.88 123.18 5.20 o -6 24 3 1.01 17.12 4.81 o -17 25 3 157.07 184.44 8.97 o -14 25 3 1985.69 1981.80 25.15 o -11 25 3 3011.70 2978.22 28.76 o -8 25 3 684.54 692.98 10.07 o -1 1 4 19609.88 19423.33 333.93 o 0 2 4 60139.86 58040.31 717.06 o -2 3 4 112038.76 103705.45 2510.15 o -4 4 4 22959.01 22527.77 254.00 o -1 4 4 24895.85 24414.38 159.44 o -3 5 4 120168.32 115732.41 1208.35 o 0 5 4 16611.59 16270.32 49.75 o -5 6 4 1862.54 1890.35 22.61 o -2 6 4 3029.38 3056.54 35.23 o -7 7 4 310.87 726.24 113.18 o -4 7 4 8549.69 8449.58 60.18 o -1 7 4 5401.37 5306.67 43.09 o -6 8 4 16406.72 16277.13 80.76 o -3 8 4 131375.59 134365.41 1070.15 o 0 8 4 61615.07 61747.82 319.49 o -8 9 4 48951.50 49197.60 211.99 o -5 9 4 11219.92 11337.78 92.72 o -2 9 4 13050.18 13039.79 107.48 o -10 10 4 64656.23 65524.50 242.80 o -7 10 4 7832.70 7889.15 41.48 o -4 10 4 14173.49 14151.05 141.54 o -1 10 4 2469.60 2546.68 23.53 o -9 11 4 5860.05 5883.57 23.44 o -6 11 4 5186.51 5248.27 36.29 o -3 11 4 34487.05 35113.25 259.08 o 0 11 4 20955.98 20829.34 87.50 o -11 12 4 1477.47 1474.65 9.53 o -8 12 4 1074.75 1359.98 75.82 o -5 12 4 419.90 467.34 8.00 o -2 12 4 203.67 307.40 14.67 o -13 13 4 28883.12 29026.42 143.24 o -10 13 4 4955.39 5011.10 28.05 o -7 13 4 5833.87 5895.30 43.39 o -4 13 4 26.11 250.75 28.47 o -1 13 4 1501.92 1568.11 8.33 o -12 14 4 102.01 149.94 5.06 o -9 14 4 22399.88 22744.24 157.93 o -6 14 4 10464.28 10470.24 78.80 o -3 14 4 15217.58 15251.32 96.21 o 0 14 4 10086.17 10127.66 58.83 o -14 15 4 10452.32 10628.89 48.69 o -11 15 4 2930.57 3023.98 18.91 o -8 15 4 21943.86 22039.17 176.40 o -5 15 4 11501.57 11644.91 80.82 o -2 15 4 6014.66 6038.56 37.64 o -16 16 4 45031.07 46421.21 429.21 o -13 16 4 8917.63 8980.58 55.82 o -10 16 4 31380.23 31799.55 181.50 o -7 16 4 797.16 874.36 16.17 o -4 16 4 3299.55 3282.14 30.62 o -1 16 4 1733.05 1810.03 23.06 o -15 17 4 329.99 416.55 29.22 o -12 17 4 142.26 203.07 11.25 o -9 17 4 881.75 882.11 8.95 o -6 17 4 4714.96 4693.62 35.15 o -3 17 4 135.14 161.87 8.58 o 0 17 4 6818.41 6738.57 75.40 o -17 18 4 18.20 116.25 24.83 o -14 18 4 1878.09 1921.62 13.12 o -11 18 4 1056.30 1077.77 10.15 o -8 18 4 260.72 297.68 6.58 o -5 18 4 12677.37 12508.11 105.46 o -2 18 4 2808.73 2852.67 29.52 o -19 19 4 11424.24 11504.60 107.08 o -16 19 4 2098.23 2205.20 23.22 o -13 19 4 12254.67 12424.06 67.38 o -10 19 4 1060.06 1083.13 11.45 o -7 19 4 3620.23 3612.46 28.81 o -4 19 4 1340.10 1339.09 12.13 o -1 19 4 7936.27 7813.91 82.33 o -18 20 4 350.93 420.57 13.00 o -15 20 4 3792.12 3863.34 27.01 o -12 20 4 1746.95 1802.75 14.56 o -9 20 4 1115.64 1158.97 9.93 o -6 20 4 1444.95 1474.46 16.75 o -3 20 4 25.75 63.35 7.04 o 0 20 4 988.65 1022.06 21.18 o -20 21 4 2194.88 2264.54 16.76 o -17 21 4 1350.43 1381.57 11.01 o -14 21 4 8942.47 8940.06 59.80 o -11 21 4 13831.48 13656.42 94.71 o -8 21 4 18700.24 18590.22 147.09 o -5 21 4 12206.28 11967.53 97.14 o -2 21 4 2576.88 2587.78 26.01 o -22 22 4 3167.82 3200.95 35.08 o -19 22 4 1919.78 1991.68 15.08 o -16 22 4 8083.26 8108.23 59.83 o -13 22 4 776.18 834.51 11.69 o -10 22 4 2856.51 2831.22 25.19 o -7 22 4 28.69 54.55 5.15 o -4 22 4 919.85 952.75 12.69 o -1 22 4 279.96 310.50 10.42 o -18 23 4 3078.08 3130.61 24.89 o -15 23 4 355.13 378.39 6.87 o -12 23 4 2169.71 2151.91 18.34 o -9 23 4 3015.29 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