#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/21/2012135.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012135_Fobs loop_ _publ_author_name 'Ardeshir, Khazaei' 'Banks, R. Eric' 'Besheesh, Mohammed K.' 'Brisdon, Alan K.' 'Pritchard, Robin G.' _publ_section_title ; 1,2-Bis(N-fluoro-p-toluenesulfonamido)ethane chloroform solvate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 970 _journal_page_last 972 _journal_volume 57 _journal_year 2001 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yac' _symmetry_space_group_name_H-M 'P 1 2/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.815 _cell_angle_gamma 90.000 _cell_length_a 10.9948 _cell_length_b 9.6922 _cell_length_c 21.3810 _exptl_crystal_F_000 1072.00 _reflns_d_resolution_high 0.8415 _[local]_cod_data_source_file gg1055Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' GG1055 N-F compound [JFG 04-04-01]' _shelx_refln_list_code 4 _shelx_f_calc_maximum 392.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 24381.19 22983.95 60.45 o 4 0 0 589.35 532.35 17.72 o 6 0 0 383.43 365.28 20.24 o 8 0 0 20856.52 20419.89 125.30 o 10 0 0 5348.60 5234.14 77.65 o 12 0 0 1.26 9.10 29.17 o 0 1 0 2518.37 2491.98 17.34 o 1 1 0 189.81 189.66 10.28 o 2 1 0 1563.01 1695.01 22.29 o 3 1 0 112.30 114.09 14.43 o 4 1 0 19.68 -0.97 15.99 o 5 1 0 502.45 500.17 19.86 o 6 1 0 0.80 21.42 15.68 o 7 1 0 180.48 182.61 18.86 o 8 1 0 720.39 749.63 29.21 o 9 1 0 157.18 163.12 28.79 o 10 1 0 54.51 45.12 27.37 o 11 1 0 0.13 10.17 26.92 o 12 1 0 0.03 53.81 29.00 o 0 2 0 38299.83 38192.88 82.29 o 1 2 0 4075.39 4048.50 31.49 o 2 2 0 4748.33 4572.58 36.13 o 3 2 0 1068.87 833.85 21.90 o 4 2 0 1121.58 1037.40 25.16 o 5 2 0 4942.20 5632.81 54.02 o 6 2 0 1231.77 1363.47 33.25 o 7 2 0 118.35 109.49 17.92 o 8 2 0 2224.86 2318.06 47.89 o 9 2 0 63.99 45.05 25.71 o 10 2 0 10.42 7.41 26.54 o 11 2 0 123.06 141.29 28.76 o 12 2 0 8.76 4.67 31.01 o 0 3 0 29858.87 28057.70 86.86 o 1 3 0 3593.74 3552.45 34.60 o 2 3 0 83.97 75.64 13.43 o 3 3 0 0.07 2.84 15.68 o 4 3 0 0.57 14.74 15.05 o 5 3 0 255.31 386.56 19.97 o 6 3 0 134.18 148.35 18.79 o 7 3 0 360.92 415.01 23.29 o 8 3 0 852.98 880.67 36.78 o 9 3 0 44.62 26.58 27.06 o 10 3 0 1.12 -19.24 27.65 o 11 3 0 147.25 223.58 31.46 o 12 3 0 9.92 26.44 31.11 o 0 4 0 599.54 639.21 19.27 o 1 4 0 21.19 8.69 14.57 o 2 4 0 48.34 45.02 14.95 o 3 4 0 160.21 134.96 16.82 o 4 4 0 80.89 65.23 16.51 o 5 4 0 151.88 148.24 17.99 o 6 4 0 0.01 -20.45 20.45 o 7 4 0 32.59 51.35 20.62 o 8 4 0 49.90 72.84 25.12 o 9 4 0 0.01 -7.27 27.27 o 10 4 0 90.96 72.95 28.93 o 11 4 0 23.10 3.39 29.48 o 12 4 0 5.10 -1.25 31.52 o 0 5 0 13273.68 13644.83 81.28 o 1 5 0 4132.17 4293.74 48.41 o 2 5 0 136.57 191.15 17.68 o 3 5 0 5747.79 5734.76 58.27 o 4 5 0 935.77 1051.34 31.35 o 5 5 0 870.07 858.08 27.06 o 6 5 0 118.66 120.91 21.52 o 7 5 0 1231.22 1143.21 40.59 o 8 5 0 376.05 344.66 33.29 o 9 5 0 32.07 36.13 26.65 o 10 5 0 1.11 -15.02 29.07 o 11 5 0 691.43 631.14 44.78 o 0 6 0 55.73 70.83 16.26 o 1 6 0 30.62 35.61 15.88 o 2 6 0 53.58 72.63 16.92 o 3 6 0 1535.09 1530.09 37.93 o 4 6 0 51.26 48.48 19.00 o 5 6 0 2465.15 2443.25 50.14 o 6 6 0 228.27 221.71 28.65 o 7 6 0 132.29 93.85 27.75 o 8 6 0 8.53 15.19 25.23 o 9 6 0 4.09 -10.59 28.17 o 10 6 0 0.54 -30.24 30.24 o 11 6 0 39.40 112.67 32.35 o 0 7 0 228.27 270.29 21.84 o 1 7 0 8.63 6.02 20.97 o 2 7 0 0.63 -14.43 22.18 o 3 7 0 2731.79 2656.90 51.01 o 4 7 0 316.91 320.19 30.28 o 5 7 0 2477.27 2373.18 53.43 o 6 7 0 62.47 51.11 26.85 o 7 7 0 52.52 7.79 27.96 o 8 7 0 20.78 29.24 27.86 o 9 7 0 53.81 87.48 29.66 o 10 7 0 249.80 243.40 34.64 o 0 8 0 132.24 99.07 26.23 o 1 8 0 590.50 607.65 33.05 o 2 8 0 183.21 152.57 27.37 o 3 8 0 837.18 770.22 37.13 o 4 8 0 95.76 112.95 25.16 o 5 8 0 410.77 393.17 32.04 o 6 8 0 357.04 285.38 33.01 o 7 8 0 232.31 216.00 31.59 o 8 8 0 204.29 224.41 33.43 o 9 8 0 30.50 67.24 30.17 o 0 9 0 0.10 -0.90 24.53 o 1 9 0 0.70 36.23 23.98 o 2 9 0 0.05 -12.15 26.09 o 3 9 0 34.97 62.67 26.47 o 4 9 0 1.99 9.00 27.96 o 5 9 0 44.37 18.89 30.31 o 6 9 0 0.05 -4.46 29.28 o 7 9 0 0.63 -5.92 29.03 o 8 9 0 0.80 45.75 27.68 o 0 10 0 103.56 94.30 29.41 o 1 10 0 9.64 87.51 25.54 o 2 10 0 508.11 576.12 38.58 o 3 10 0 614.65 570.31 39.66 o 4 10 0 3.97 49.93 28.41 o 5 10 0 698.37 721.70 42.01 o 6 10 0 290.07 287.97 37.10 o 0 11 0 145.32 118.38 32.11 o 1 11 0 21.12 35.68 31.11 o 2 11 0 178.94 171.08 34.71 o 3 11 0 62.18 66.23 33.64 o -13 0 1 1.39 71.18 29.24 o -11 0 1 0.01 -8.06 28.06 o -9 0 1 12.57 -8.58 26.33 o -7 0 1 1.18 -20.45 20.45 o -5 0 1 0.16 -4.74 17.72 o -3 0 1 65.77 70.35 14.60 o -1 0 1 30.75 31.14 7.86 o 1 0 1 40.29 139.56 8.79 o 3 0 1 1.89 -11.00 15.71 o 5 0 1 11.87 9.38 16.16 o 7 0 1 101.39 92.60 18.55 o 9 0 1 12.26 42.60 26.71 o 11 0 1 17.15 40.66 26.44 o -12 1 1 124.87 150.60 32.22 o -11 1 1 0.11 24.33 27.30 o -10 1 1 202.95 238.25 30.76 o -9 1 1 278.90 298.81 29.83 o -8 1 1 1594.77 1745.88 42.84 o -7 1 1 1.85 26.78 16.58 o -6 1 1 966.41 864.65 24.74 o -5 1 1 4953.42 4921.98 48.86 o -4 1 1 800.60 700.35 19.03 o -3 1 1 126.08 89.87 13.95 o -2 1 1 33331.46 34388.72 79.35 o -1 1 1 0.66 34.47 9.76 o 0 1 1 6254.00 5898.47 251.33 o 1 1 1 6447.96 6425.00 30.42 o 2 1 1 2152.17 2487.06 26.06 o 3 1 1 136.43 83.60 14.29 o 4 1 1 1703.27 2065.17 30.73 o 5 1 1 1215.91 1268.07 29.62 o 6 1 1 972.30 999.50 29.79 o 7 1 1 14.41 28.96 17.65 o 8 1 1 4984.45 5096.00 66.30 o 9 1 1 114.59 112.29 28.48 o 10 1 1 299.66 261.81 30.69 o 11 1 1 13.24 19.45 28.06 o 12 1 1 213.01 209.74 35.85 o -12 2 1 234.73 273.10 35.23 o -11 2 1 3.63 78.66 26.06 o -10 2 1 1.58 -27.41 27.41 o -9 2 1 451.72 453.59 33.12 o -8 2 1 327.15 371.92 23.70 o -7 2 1 133.14 93.29 19.41 o -6 2 1 629.40 701.18 23.43 o -5 2 1 1000.24 950.57 28.31 o -4 2 1 6410.45 6467.98 51.32 o -3 2 1 1479.55 1466.49 25.78 o -2 2 1 8405.04 7998.52 45.82 o -1 2 1 276.51 340.40 14.85 o 0 2 1 13704.35 13614.97 457.26 o 1 2 1 6861.48 7039.09 39.97 o 2 2 1 455.99 459.27 15.85 o 3 2 1 346.06 222.92 14.85 o 4 2 1 884.31 1062.45 25.54 o 5 2 1 729.18 887.49 23.46 o 6 2 1 3552.97 3855.10 49.48 o 7 2 1 281.65 292.51 22.08 o 8 2 1 938.25 953.86 30.52 o 9 2 1 544.60 522.35 34.40 o 10 2 1 102.98 132.26 27.34 o 11 2 1 31.85 7.34 27.72 o 12 2 1 155.55 97.41 35.64 o -12 3 1 4.69 33.53 30.73 o -11 3 1 0.25 38.55 27.13 o -10 3 1 31.12 -9.59 27.41 o -9 3 1 466.57 450.10 33.67 o -8 3 1 393.52 368.15 29.90 o -7 3 1 545.73 584.19 25.09 o -6 3 1 673.49 727.97 24.22 o -5 3 1 95.78 67.30 16.54 o -4 3 1 82.02 90.04 16.19 o -3 3 1 3.00 3.53 15.99 o -2 3 1 87.64 84.50 13.08 o -1 3 1 2531.68 2520.77 30.24 o 0 3 1 11858.28 10924.59 285.21 o 1 3 1 6265.44 6547.64 45.33 o 2 3 1 496.92 517.19 16.75 o 3 3 1 196.50 222.05 16.06 o 4 3 1 110.95 62.43 15.26 o 5 3 1 4.52 7.92 18.89 o 6 3 1 47.02 25.68 17.20 o 7 3 1 4.13 4.01 21.39 o 8 3 1 11.39 22.56 24.29 o 9 3 1 844.13 778.73 38.13 o 10 3 1 298.56 278.87 32.60 o 11 3 1 126.84 129.80 30.66 o 12 3 1 26.51 42.32 29.59 o -12 4 1 36.97 33.67 32.25 o -11 4 1 22.66 35.88 29.34 o -10 4 1 195.50 165.55 29.31 o -9 4 1 1665.96 1508.08 47.30 o -8 4 1 490.50 536.88 33.98 o -7 4 1 1848.17 1780.17 44.47 o -6 4 1 1409.47 1379.49 36.47 o -5 4 1 3128.79 3205.65 46.51 o -4 4 1 4139.26 3861.85 47.20 o -3 4 1 1544.19 1508.11 31.39 o -2 4 1 642.84 509.03 18.96 o -1 4 1 10817.39 11095.96 66.65 o 0 4 1 880.01 1116.76 18.47 o 1 4 1 14163.53 14192.61 74.50 o 2 4 1 169.92 175.96 16.58 o 3 4 1 1789.39 1590.89 32.29 o 4 4 1 1.88 -13.01 18.27 o 5 4 1 647.17 615.23 22.15 o 6 4 1 398.70 407.71 21.87 o 7 4 1 1001.89 999.64 30.28 o 8 4 1 198.37 186.20 29.00 o 9 4 1 3136.37 3182.22 63.05 o 10 4 1 293.48 263.99 33.15 o 11 4 1 743.31 715.16 42.60 o 12 4 1 5.41 71.70 30.28 o -11 5 1 2.53 55.68 30.14 o -10 5 1 0.81 5.33 28.41 o -9 5 1 34.86 0.00 28.51 o -8 5 1 2.01 -19.90 25.64 o -7 5 1 41.44 64.02 25.99 o -6 5 1 35.49 25.05 20.07 o -5 5 1 82.01 82.01 19.14 o -4 5 1 92.32 43.91 17.92 o -3 5 1 0.79 -10.35 18.48 o -2 5 1 68.45 78.34 16.33 o -1 5 1 41.81 32.35 16.61 o 0 5 1 2.26 24.51 20.23 o 1 5 1 299.06 280.29 18.65 o 2 5 1 21.45 1.45 18.62 o 3 5 1 1.79 -2.60 18.76 o 4 5 1 1.64 9.00 18.55 o 5 5 1 28.77 12.77 17.86 o 6 5 1 26.57 49.03 20.14 o 7 5 1 13.48 15.16 25.92 o 8 5 1 41.41 71.67 25.75 o 9 5 1 8.15 -16.71 29.48 o 10 5 1 16.79 11.94 27.20 o 11 5 1 4.39 29.90 30.17 o -11 6 1 1.61 -17.68 31.94 o -10 6 1 9.99 42.42 28.69 o -9 6 1 2.53 45.33 26.09 o -8 6 1 23.24 -11.35 25.81 o -7 6 1 2518.18 2583.37 55.95 o -6 6 1 1378.13 1431.71 42.91 o -5 6 1 7241.69 7028.43 77.41 o -4 6 1 63.92 29.66 19.48 o -3 6 1 28.19 -7.41 17.68 o -2 6 1 242.21 239.88 18.44 o -1 6 1 5.16 17.65 15.92 o 0 6 1 66.03 85.32 12.14 o 1 6 1 1570.08 1527.15 35.23 o 2 6 1 12.48 16.16 16.78 o 3 6 1 5078.62 4648.12 58.41 o 4 6 1 11.56 -11.28 21.87 o 5 6 1 2211.42 2196.46 47.51 o 6 6 1 222.63 215.96 29.14 o 7 6 1 247.35 282.30 30.66 o 8 6 1 38.00 10.52 27.48 o 9 6 1 225.72 270.05 33.50 o 10 6 1 115.18 121.43 31.11 o 11 6 1 387.30 473.42 40.28 o -10 7 1 130.25 139.94 32.35 o -9 7 1 10.83 -2.28 28.79 o -8 7 1 0.55 -1.04 27.20 o -7 7 1 650.05 646.68 37.34 o -6 7 1 852.34 889.29 40.00 o -5 7 1 1538.15 1555.38 45.82 o -4 7 1 3652.63 3727.41 61.01 o -3 7 1 21.16 15.71 20.69 o -2 7 1 36.60 65.99 18.65 o -1 7 1 130.49 98.73 20.21 o 0 7 1 8.95 5.55 22.67 o 1 7 1 91.04 92.91 18.86 o 2 7 1 111.88 142.26 19.90 o 3 7 1 2545.35 2518.73 50.14 o 4 7 1 772.34 742.33 35.71 o 5 7 1 592.24 549.10 34.26 o 6 7 1 623.61 638.65 36.13 o 7 7 1 135.72 108.73 29.72 o 8 7 1 15.19 -25.19 28.27 o 9 7 1 93.34 109.94 32.42 o 10 7 1 13.90 -11.25 31.11 o -9 8 1 65.28 43.95 34.92 o -8 8 1 5.11 -31.66 31.66 o -7 8 1 179.77 194.37 30.17 o -6 8 1 4.16 -1.00 26.30 o -5 8 1 44.79 36.06 26.33 o -4 8 1 14.55 59.48 24.57 o -3 8 1 0.33 -25.16 26.06 o -2 8 1 91.77 89.17 25.71 o -1 8 1 2.56 -25.88 25.88 o 0 8 1 18.84 5.01 17.75 o 1 8 1 522.78 484.98 32.49 o 2 8 1 29.99 45.12 25.30 o 3 8 1 257.99 293.62 28.65 o 4 8 1 58.01 72.95 25.75 o 5 8 1 4.85 46.47 25.26 o 6 8 1 102.47 91.56 27.82 o 7 8 1 27.65 21.39 28.72 o 8 8 1 41.74 32.39 31.35 o 9 8 1 117.23 78.79 35.40 o -8 9 1 15.39 49.45 31.14 o -7 9 1 430.69 519.27 38.79 o -6 9 1 9.88 58.90 29.31 o -5 9 1 886.42 799.53 40.24 o -4 9 1 1257.79 1245.75 46.75 o -3 9 1 50.00 9.65 27.79 o -2 9 1 88.99 143.16 28.03 o -1 9 1 0.15 -16.33 26.58 o 0 9 1 90.75 39.66 18.85 o 1 9 1 39.15 42.67 26.47 o 2 9 1 35.66 35.64 25.81 o 3 9 1 808.99 750.39 40.28 o 4 9 1 1183.67 1201.70 44.40 o 5 9 1 331.96 283.58 33.46 o 6 9 1 1078.91 1135.05 48.90 o 7 9 1 2.45 5.95 28.69 o 8 9 1 24.45 -11.49 32.42 o -6 10 1 1.70 29.90 31.84 o -5 10 1 14.30 4.74 31.18 o -4 10 1 74.72 69.21 31.84 o -3 10 1 8.97 13.22 27.51 o -2 10 1 35.01 21.45 29.79 o -1 10 1 1.39 -17.72 27.54 o 0 10 1 2.59 24.38 17.65 o 1 10 1 7.88 59.52 26.02 o 2 10 1 0.01 -18.27 29.48 o 3 10 1 33.03 -3.32 28.83 o 4 10 1 70.43 89.97 30.83 o 5 10 1 50.05 72.53 32.46 o 6 10 1 65.98 103.85 30.76 o -3 11 1 1.20 17.51 32.01 o -2 11 1 649.23 601.42 43.91 o -1 11 1 48.61 32.15 31.59 o 0 11 1 92.55 123.90 22.80 o 1 11 1 314.46 283.58 37.34 o 2 11 1 7.08 -17.13 33.22 o 3 11 1 149.99 181.64 33.50 o -12 0 2 174.62 181.29 33.74 o -10 0 2 232.09 216.55 31.21 o -8 0 2 3708.38 3730.18 56.72 o -6 0 2 8665.17 8498.45 68.10 o -4 0 2 90.28 71.73 14.26 o -2 0 2 1204.90 1085.94 19.38 o 0 0 2 102.83 113.99 5.66 o 2 0 2 82379.57 79319.05 120.08 o 4 0 2 1081.87 1375.13 27.09 o 6 0 2 2581.53 2799.78 42.11 o 8 0 2 1957.02 2064.48 45.92 o 10 0 2 10575.92 10442.99 108.41 o 12 0 2 434.77 436.95 37.79 o -13 1 2 7.20 75.30 31.39 o -12 1 2 10.26 3.43 30.00 o -11 1 2 12.74 9.10 27.44 o -10 1 2 62.16 67.41 26.09 o -9 1 2 25.49 30.11 26.06 o -8 1 2 27.08 7.68 20.21 o -7 1 2 8.79 11.45 17.06 o -6 1 2 566.74 578.93 22.18 o -5 1 2 245.11 224.93 17.86 o -4 1 2 307.22 310.68 15.99 o -3 1 2 29.41 -7.65 15.92 o -2 1 2 2748.07 2940.17 27.75 o -1 1 2 0.34 1.70 10.55 o 0 1 2 92.92 101.39 7.19 o 1 1 2 381.59 392.76 12.73 o 2 1 2 84.88 48.83 13.77 o 3 1 2 789.66 734.47 20.97 o 4 1 2 151.26 161.84 15.40 o 5 1 2 0.06 0.31 15.33 o 6 1 2 74.39 72.36 17.03 o 7 1 2 22.94 48.41 17.72 o 8 1 2 125.87 142.05 22.39 o 9 1 2 201.77 189.87 29.34 o 10 1 2 196.48 226.93 32.46 o 11 1 2 158.62 139.59 30.24 o 12 1 2 63.36 55.78 31.84 o -12 2 2 99.84 146.27 32.91 o -11 2 2 45.64 6.19 29.66 o -10 2 2 10.02 28.55 24.64 o -9 2 2 739.36 708.17 38.00 o -8 2 2 1.17 38.24 19.03 o -7 2 2 330.79 369.71 22.60 o -6 2 2 6915.66 7484.82 66.79 o -5 2 2 427.88 607.13 21.94 o -4 2 2 6371.35 6357.49 50.76 o -3 2 2 3755.50 4036.67 38.27 o -2 2 2 4895.63 4712.14 36.92 o -1 2 2 1691.13 1852.91 24.81 o 0 2 2 3646.44 3675.70 104.04 o 1 2 2 4907.59 4926.89 35.64 o 2 2 2 15009.45 14311.41 61.66 o 3 2 2 7898.92 7404.72 51.11 o 4 2 2 1225.85 1504.38 28.96 o 5 2 2 8.40 -7.72 18.62 o 6 2 2 1640.98 1725.19 35.92 o 7 2 2 1101.38 1066.19 29.24 o 8 2 2 48.70 44.40 20.24 o 9 2 2 1178.15 1104.18 41.18 o 10 2 2 1618.72 1753.11 52.32 o 11 2 2 95.46 89.73 28.83 o 12 2 2 504.74 530.31 42.49 o -12 3 2 6.94 34.67 29.28 o -11 3 2 111.48 134.82 28.83 o -10 3 2 1.05 -26.82 26.99 o -9 3 2 1086.30 1019.82 40.73 o -8 3 2 27.26 30.52 24.26 o -7 3 2 1076.14 1039.33 30.04 o -6 3 2 4253.42 4182.77 53.12 o -5 3 2 3695.93 4010.02 48.90 o -4 3 2 195.62 205.17 17.20 o -3 3 2 110.04 86.13 14.33 o -2 3 2 34.00 31.28 12.87 o -1 3 2 16898.78 16917.96 71.28 o 0 3 2 10466.79 10129.67 308.50 o 1 3 2 9439.96 9202.71 53.88 o 2 3 2 2294.47 2213.86 31.04 o 3 3 2 548.07 591.04 18.89 o 4 3 2 635.52 432.59 20.04 o 5 3 2 307.63 433.73 20.00 o 6 3 2 285.19 342.86 19.86 o 7 3 2 1644.91 1674.59 40.94 o 8 3 2 22.38 39.59 23.63 o 9 3 2 1931.20 1891.91 49.93 o 10 3 2 463.58 451.72 35.61 o 11 3 2 8.28 15.29 28.34 o 12 3 2 140.34 145.06 34.81 o -12 4 2 0.57 -13.70 31.42 o -11 4 2 38.24 15.68 30.97 o -10 4 2 11.82 -4.05 26.78 o -9 4 2 133.54 106.10 28.31 o -8 4 2 51.36 53.50 24.43 o -7 4 2 13.57 -14.40 24.40 o -6 4 2 142.54 130.77 19.00 o -5 4 2 155.67 133.33 18.79 o -4 4 2 71.85 76.37 16.19 o -3 4 2 2.02 5.23 17.37 o -2 4 2 586.62 590.86 19.62 o -1 4 2 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