#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012163.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012163_Fobs loop_ _publ_author_name 'Farrell, Dorcas M. M.' 'Ferguson, George' 'Lough, Alan J.' 'Glidewell, Christopher' _publ_section_title ; Hydrogen-bonded bilayers in piperazinium(2+) bis(mandelate) bis(methanol) solvate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 955 _journal_page_last 957 _journal_volume 57 _journal_year 2001 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.7360 _cell_length_b 10.2394 _cell_length_c 29.7822 _exptl_crystal_F_000 976.00 _reflns_d_resolution_high 0.8403 _[local]_cod_data_source_file sk1483Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 26 With A/B labels switched' _shelx_refln_list_code 4 _shelx_f_calc_maximum 234.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 55130.89 51149.05 1889.41 o 4 0 0 4267.34 4406.26 177.58 o 6 0 0 70.69 37.88 35.52 o 8 0 0 2.45 -28.41 85.24 o 2 1 0 11291.34 10936.33 331.48 o 4 1 0 3785.46 3729.10 116.02 o 6 1 0 30.62 61.56 28.41 o 8 1 0 13.01 0.00 82.87 o 0 2 0 20155.31 18754.41 852.37 o 2 2 0 9795.70 9705.13 442.76 o 4 2 0 356.54 404.87 30.78 o 6 2 0 1.51 7.10 35.52 o 8 2 0 0.06 99.44 104.18 o 2 3 0 9952.14 9686.19 329.11 o 4 3 0 915.90 961.28 49.72 o 6 3 0 890.23 968.38 63.93 o 8 3 0 397.57 407.24 106.55 o 0 4 0 0.56 0.00 11.84 o 2 4 0 3170.81 3170.33 116.02 o 4 4 0 269.56 250.97 26.04 o 6 4 0 743.12 719.78 63.93 o 8 4 0 70.96 -33.15 68.66 o 2 5 0 38.19 28.41 11.84 o 4 5 0 2321.91 2502.64 94.71 o 6 5 0 1336.48 1491.64 94.71 o 8 5 0 70.23 61.56 52.09 o 0 6 0 402.79 440.39 33.15 o 2 6 0 94.22 71.03 14.21 o 4 6 0 313.41 274.65 30.78 o 6 6 0 99.57 137.33 54.46 o 8 6 0 90.98 101.81 85.24 o 2 7 0 1183.51 1396.93 59.19 o 4 7 0 39.42 68.66 28.41 o 6 7 0 45.11 -28.41 40.25 o 0 8 0 9.45 9.47 18.94 o 2 8 0 441.11 390.67 30.78 o 4 8 0 678.40 724.51 52.09 o 6 8 0 32.65 33.15 54.46 o 2 9 0 604.26 719.78 59.19 o 4 9 0 10.11 49.72 42.62 o 6 9 0 1.80 97.07 59.19 o 0 10 0 77.68 7.10 52.09 o 2 10 0 352.29 430.92 49.72 o 4 10 0 452.28 322.00 61.56 o 2 11 0 1.98 61.56 33.15 o 0 12 0 52.59 -26.04 59.19 o 1 1 1 824.59 650.10 21.76 o 2 1 1 799.34 730.99 20.48 o 3 1 1 104.50 98.94 8.29 o 4 1 1 527.10 466.09 15.76 o 5 1 1 212.54 201.97 10.93 o 6 1 1 12.56 10.65 5.92 o 7 1 1 0.09 24.27 63.93 o 8 1 1 9.11 47.35 63.66 o 9 1 1 2.53 2.93 92.34 o 0 2 1 635.13 556.41 16.57 o 1 2 1 2287.43 2239.25 47.69 o 2 2 1 264.99 261.68 15.07 o 3 2 1 733.51 676.61 25.91 o 4 2 1 238.75 216.11 18.42 o 5 2 1 228.35 215.52 22.19 o 6 2 1 0.79 -11.22 17.92 o 7 2 1 37.13 47.63 48.54 o 8 2 1 0.06 -46.27 53.27 o 9 2 1 1.38 37.88 82.87 o 1 3 1 4540.37 4332.24 94.49 o 2 3 1 488.12 511.59 16.74 o 3 3 1 595.10 655.95 25.59 o 4 3 1 66.40 58.03 13.39 o 5 3 1 113.58 111.64 20.09 o 6 3 1 0.01 14.01 19.27 o 7 3 1 385.91 411.55 79.32 o 8 3 1 30.31 66.47 68.66 o 0 4 1 506.05 532.73 21.31 o 1 4 1 2674.15 2728.12 62.63 o 2 4 1 2111.92 2239.57 59.19 o 3 4 1 447.04 476.33 20.88 o 4 4 1 80.85 79.18 6.53 o 5 4 1 29.03 18.19 15.84 o 6 4 1 415.70 410.52 49.72 o 7 4 1 144.39 178.76 56.82 o 8 4 1 9.95 -48.43 66.30 o 1 5 1 1609.52 1766.98 44.99 o 2 5 1 1323.43 1371.58 33.48 o 3 5 1 603.85 638.58 24.95 o 4 5 1 20.71 13.26 16.57 o 5 5 1 460.89 437.97 26.63 o 6 5 1 0.00 13.82 28.41 o 7 5 1 1.57 -10.34 30.64 o 8 5 1 1.34 -16.66 74.58 o 0 6 1 2689.58 3023.53 108.91 o 1 6 1 386.63 382.07 15.84 o 2 6 1 931.56 1020.49 28.46 o 3 6 1 95.90 98.72 29.60 o 4 6 1 23.80 58.26 16.74 o 5 6 1 705.18 788.61 21.57 o 6 6 1 102.24 34.33 31.81 o 7 6 1 6.02 -6.72 29.34 o 8 6 1 19.70 39.02 82.87 o 1 7 1 100.22 93.52 11.36 o 2 7 1 312.38 309.74 14.79 o 3 7 1 203.14 208.75 47.35 o 4 7 1 1.12 1.74 15.84 o 5 7 1 72.31 95.29 39.07 o 6 7 1 21.37 -26.04 35.52 o 7 7 1 11.03 57.04 34.59 o 0 8 1 15.44 35.52 18.94 o 1 8 1 111.43 90.14 14.16 o 2 8 1 24.68 28.54 15.84 o 3 8 1 133.50 101.15 18.77 o 4 8 1 1.73 -25.91 25.91 o 5 8 1 399.35 389.57 40.99 o 6 8 1 37.74 32.28 34.05 o 1 9 1 106.10 108.44 18.42 o 2 9 1 2.74 -3.40 18.77 o 3 9 1 8.71 56.08 53.27 o 4 9 1 48.04 61.20 35.52 o 5 9 1 11.14 27.64 34.33 o 6 9 1 38.15 -4.05 46.02 o 0 10 1 7.34 -26.04 26.04 o 1 10 1 72.99 63.93 28.46 o 2 10 1 57.56 27.89 29.58 o 3 10 1 132.37 128.14 34.29 o 4 10 1 168.63 136.42 39.32 o 5 10 1 0.20 12.10 29.58 o 1 11 1 217.74 172.50 36.98 o 2 11 1 79.95 112.46 38.51 o 3 11 1 14.30 4.86 29.75 o 0 12 1 4.59 -54.46 54.46 o 1 12 1 62.56 71.12 55.64 o 1 0 2 1072.64 1048.88 33.15 o 2 0 2 6489.15 5990.24 156.27 o 3 0 2 2519.56 2429.24 73.40 o 4 0 2 1327.38 1541.36 56.82 o 5 0 2 360.21 319.64 28.41 o 6 0 2 25.89 47.35 26.04 o 7 0 2 264.28 243.87 49.72 o 8 0 2 91.95 75.77 52.09 o 9 0 2 73.83 78.13 94.71 o 1 1 2 14419.13 13977.23 438.50 o 2 1 2 2500.11 2222.49 50.06 o 3 1 2 2032.30 2068.43 43.14 o 4 1 2 1.33 5.26 4.55 o 5 1 2 20.70 40.84 8.47 o 6 1 2 47.82 53.30 6.70 o 7 1 2 100.02 80.40 61.56 o 8 1 2 17.26 -63.93 66.30 o 9 1 2 12.46 41.91 68.74 o 0 2 2 11256.73 9660.15 331.48 o 1 2 2 3431.70 3282.79 68.64 o 2 2 2 843.53 875.51 23.26 o 3 2 2 144.92 133.18 12.47 o 4 2 2 171.05 152.92 17.76 o 5 2 2 481.86 410.57 28.31 o 6 2 2 70.16 61.48 23.26 o 7 2 2 0.90 5.92 41.86 o 8 2 2 3.68 -71.03 71.03 o 9 2 2 0.97 -35.52 116.02 o 1 3 2 14.53 12.31 3.94 o 2 3 2 23.09 22.89 7.40 o 3 3 2 9.05 12.55 10.65 o 4 3 2 91.84 98.27 15.84 o 5 3 2 109.88 109.36 28.41 o 6 3 2 173.65 146.87 27.23 o 7 3 2 7.10 2.18 39.79 o 8 3 2 27.65 -12.64 62.74 o 0 4 2 3258.28 3257.93 87.60 o 1 4 2 209.18 202.44 8.37 o 2 4 2 642.12 651.68 22.56 o 3 4 2 320.64 312.82 15.07 o 4 4 2 561.69 580.09 15.07 o 5 4 2 14.23 -17.76 17.76 o 6 4 2 105.51 108.98 28.41 o 7 4 2 7.91 43.29 52.56 o 8 4 2 0.01 -3.76 48.47 o 1 5 2 115.57 121.73 9.09 o 2 5 2 3032.82 3229.02 72.47 o 3 5 2 964.13 936.54 33.48 o 4 5 2 1.33 4.88 13.08 o 5 5 2 24.88 35.18 17.76 o 6 5 2 1.26 -18.86 27.23 o 7 5 2 82.12 82.25 56.82 o 8 5 2 100.09 63.93 57.18 o 0 6 2 44.22 47.35 14.21 o 1 6 2 106.98 108.91 11.72 o 2 6 2 73.84 76.15 17.76 o 3 6 2 100.64 114.28 17.76 o 4 6 2 12.85 26.64 14.21 o 5 6 2 2.32 11.05 10.59 o 6 6 2 18.48 26.41 25.40 o 7 6 2 0.09 2.58 47.35 o 1 7 2 594.60 554.20 20.09 o 2 7 2 149.11 147.93 14.79 o 3 7 2 218.43 204.45 30.78 o 4 7 2 78.82 80.41 20.88 o 5 7 2 115.85 91.36 17.46 o 6 7 2 39.29 48.54 30.14 o 7 7 2 1.37 -25.92 31.68 o 0 8 2 0.02 0.00 18.94 o 1 8 2 29.57 19.26 13.02 o 2 8 2 48.41 27.23 13.39 o 3 8 2 105.17 104.75 31.96 o 4 8 2 185.75 247.46 35.73 o 5 8 2 94.31 121.15 41.43 o 6 8 2 70.34 14.02 31.85 o 1 9 2 5.53 14.62 18.77 o 2 9 2 618.41 598.77 38.05 o 3 9 2 49.47 49.00 27.59 o 4 9 2 6.00 1.82 39.07 o 5 9 2 59.03 66.30 27.97 o 6 9 2 55.10 53.04 31.52 o 0 10 2 94.60 125.49 42.62 o 1 10 2 143.21 140.14 28.98 o 2 10 2 28.04 11.84 34.33 o 3 10 2 46.03 85.24 32.98 o 4 10 2 43.03 61.37 29.34 o 5 10 2 7.60 -1.21 44.15 o 1 11 2 95.98 125.37 35.04 o 2 11 2 3.53 64.25 31.96 o 3 11 2 57.32 50.53 36.72 o 0 12 2 225.06 241.50 56.82 o 1 12 2 0.06 -40.38 40.38 o 1 1 3 6588.54 6015.34 176.61 o 2 1 3 6306.15 6414.21 132.23 o 3 1 3 5.11 5.21 3.94 o 4 1 3 559.60 542.20 20.08 o 5 1 3 174.77 165.42 18.94 o 6 1 3 316.03 300.71 13.39 o 7 1 3 0.23 5.09 47.35 o 8 1 3 76.14 32.53 57.60 o 9 1 3 8.11 55.71 82.87 o 0 2 3 5148.87 4775.62 142.06 o 1 2 3 421.66 389.31 10.79 o 2 2 3 0.49 2.37 4.24 o 3 2 3 513.00 529.51 19.20 o 4 2 3 1727.51 1908.09 95.89 o 5 2 3 201.24 184.95 21.76 o 6 2 3 82.90 57.55 21.57 o 7 2 3 235.29 261.90 59.28 o 8 2 3 25.30 49.50 63.03 o 9 2 3 0.68 -44.99 108.91 o 1 3 3 474.50 412.47 11.36 o 2 3 3 105.13 88.31 22.49 o 3 3 3 2343.86 2485.84 89.97 o 4 3 3 767.55 768.70 31.68 o 5 3 3 1.95 11.46 15.84 o 6 3 3 222.80 194.96 26.63 o 7 3 3 21.87 9.55 52.72 o 8 3 3 0.46 -18.94 104.18 o 0 4 3 2055.05 2159.33 61.56 o 1 4 3 518.86 542.46 15.84 o 2 4 3 71.49 53.08 9.09 o 3 4 3 16.10 18.40 10.79 o 4 4 3 7.20 5.92 5.02 o 5 4 3 37.73 47.35 20.09 o 6 4 3 416.59 400.44 32.61 o 7 4 3 15.65 53.04 51.22 o 8 4 3 0.97 -11.30 130.22 o 1 5 3 85.78 123.17 10.05 o 2 5 3 440.17 451.78 15.84 o 3 5 3 1.74 -1.18 11.72 o 4 5 3 1700.99 1846.69 52.86 o 5 5 3 19.34 16.57 14.79 o 6 5 3 183.08 199.38 31.68 o 7 5 3 21.86 5.25 30.94 o 8 5 3 112.59 71.76 53.47 o 0 6 3 607.99 603.76 26.04 o 1 6 3 125.20 124.33 11.36 o 2 6 3 238.35 225.15 13.39 o 3 6 3 6.19 -2.84 12.47 o 4 6 3 82.02 58.01 18.42 o 5 6 3 53.55 43.14 10.78 o 6 6 3 0.03 -6.89 49.72 o 7 6 3 8.79 50.75 38.40 o 1 7 3 246.06 218.56 28.41 o 2 7 3 427.54 422.35 29.60 o 3 7 3 136.65 152.82 20.88 o 4 7 3 155.79 119.93 21.31 o 5 7 3 28.26 48.51 50.91 o 6 7 3 0.91 -6.34 30.94 o 7 7 3 1.71 -25.82 35.97 o 0 8 3 25.40 28.41 18.94 o 1 8 3 578.03 589.86 29.60 o 2 8 3 357.40 320.96 24.86 o 3 8 3 341.30 373.21 25.11 o 4 8 3 142.55 142.62 28.41 o 5 8 3 28.03 -10.08 25.59 o 6 8 3 33.99 47.63 35.73 o 1 9 3 96.48 106.12 30.78 o 2 9 3 27.74 28.05 21.57 o 3 9 3 55.39 48.50 27.23 o 4 9 3 27.41 18.94 26.79 o 5 9 3 21.32 8.42 29.58 o 6 9 3 14.45 -39.10 39.10 o 0 10 3 6.92 -37.88 37.88 o 1 10 3 22.29 28.21 29.26 o 2 10 3 6.86 5.14 22.22 o 3 10 3 5.82 -6.85 28.31 o 4 10 3 0.47 42.62 31.52 o 5 10 3 60.07 72.79 43.80 o 1 11 3 0.01 -16.15 40.25 o 2 11 3 57.42 53.49 31.10 o 3 11 3 8.82 -22.37 32.98 o 0 12 3 1.63 18.94 47.35 o 1 12 3 3.16 -8.09 39.07 o 0 0 4 3375.02 3165.59 120.75 o 1 0 4 888.68 707.94 23.68 o 2 0 4 10695.83 10446.22 300.70 o 3 0 4 3.66 0.00 9.47 o 4 0 4 2600.02 2673.11 92.34 o 5 0 4 466.26 459.33 37.88 o 6 0 4 91.64 87.60 16.57 o 7 0 4 454.20 456.96 42.62 o 8 0 4 96.36 163.37 63.93 o 9 0 4 7.50 -44.99 120.75 o 1 1 4 2.56 3.55 3.35 o 2 1 4 7697.56 7551.44 138.23 o 3 1 4 7259.55 7759.75 155.67 o 4 1 4 1.87 -6.35 6.35 o 5 1 4 537.40 584.53 21.46 o 6 1 4 61.60 61.56 9.09 o 7 1 4 53.94 62.56 30.21 o 8 1 4 2.07 34.22 51.64 o 9 1 4 96.37 28.97 56.82 o 0 2 4 11261.80 9941.90 310.17 o 1 2 4 1072.42 955.64 25.59 o 2 2 4 971.51 1053.62 28.31 o 3 2 4 44.13 42.89 6.09 o 4 2 4 1345.05 1407.45 42.47 o 5 2 4 139.43 135.53 19.20 o 6 2 4 165.38 180.52 24.45 o 7 2 4 9.72 -33.15 45.47 o 8 2 4 70.59 10.74 46.52 o 9 2 4 0.67 -9.47 120.75 o 1 3 4 5398.03 5289.53 110.50 o 2 3 4 5765.22 5883.80 136.44 o 3 3 4 14.90 19.05 15.39 o 4 3 4 1062.26 1099.15 43.43 o 5 3 4 1.56 6.69 14.16 o 6 3 4 16.04 26.27 20.13 o 7 3 4 0.35 1.76 35.27 o 8 3 4 12.05 45.60 73.61 o 0 4 4 24.91 47.35 9.47 o 1 4 4 207.12 201.28 10.05 o 2 4 4 5.05 10.65 8.37 o 3 4 4 480.29 540.61 20.88 o 4 4 4 0.06 -5.07 5.68 o 5 4 4 59.89 50.91 20.09 o 6 4 4 210.52 192.49 33.17 o 7 4 4 26.26 34.97 53.93 o 8 4 4 300.58 398.64 84.16 o 1 5 4 425.12 401.13 21.31 o 2 5 4 548.05 615.07 21.76 o 3 5 4 371.57 420.72 34.33 o 4 5 4 1162.79 1278.53 40.38 o 5 5 4 24.71 46.86 15.84 o 6 5 4 846.34 991.84 56.07 o 7 5 4 206.38 207.23 39.32 o 8 5 4 26.29 -54.46 54.46 o 0 6 4 67.97 63.93 11.84 o 1 6 4 29.66 22.49 8.37 o 2 6 4 13.00 14.21 10.05 o 3 6 4 285.03 320.24 18.19 o 4 6 4 38.20 22.49 16.74 o 5 6 4 111.15 117.22 11.84 o 6 6 4 254.72 304.78 43.14 o 7 6 4 3.48 -4.74 36.83 o 1 7 4 443.61 450.27 36.70 o 2 7 4 466.12 454.53 35.52 o 3 7 4 129.04 135.17 22.73 o 4 7 4 2.51 24.24 17.52 o 5 7 4 80.23 88.98 18.57 o 6 7 4 34.40 17.10 29.58 o 7 7 4 19.85 42.91 34.33 o 0 8 4 398.45 364.62 28.41 o 1 8 4 83.14 76.27 14.79 o 2 8 4 797.52 771.41 31.28 o 3 8 4 138.79 118.64 58.01 o 4 8 4 267.17 257.94 32.61 o 5 8 4 1.52 15.17 30.94 o 6 8 4 0.99 54.46 30.14 o 1 9 4 90.51 90.45 20.88 o 2 9 4 687.24 795.18 42.67 o 3 9 4 14.89 -8.94 22.56 o 4 9 4 456.21 406.48 45.20 o 5 9 4 232.18 220.69 40.25 o 6 9 4 0.54 70.05 46.42 o 0 10 4 669.14 674.79 63.93 o 1 10 4 182.27 187.49 31.85 o 2 10 4 302.99 315.81 40.08 o 3 10 4 98.36 79.05 30.00 o 4 10 4 10.23 -25.76 33.28 o 5 10 4 5.74 -5.59 41.75 o 1 11 4 201.06 129.55 43.80 o 2 11 4 53.45 -5.34 37.22 o 3 11 4 13.72 31.34 35.04 o 0 12 4 44.85 94.71 56.82 o 1 12 4 33.77 41.36 32.16 o 1 1 5 16158.07 15180.14 353.83 o 2 1 5 3034.60 3126.32 63.03 o 3 1 5 3846.66 4092.63 111.28 o 4 1 5 1274.47 1221.76 31.68 o 5 1 5 694.72 742.81 23.44 o 6 1 5 606.28 612.82 20.88 o 7 1 5 0.00 -13.40 13.40 o 8 1 5 109.90 165.74 68.66 o 9 1 5 5.15 -123.12 123.12 o 0 2 5 11988.78 11270.17 352.78 o 1 2 5 4508.33 4269.47 108.91 o 2 2 5 6948.19 6884.77 192.97 o 3 2 5 834.33 860.05 25.40 o 4 2 5 254.42 271.48 17.52 o 5 2 5 40.26 59.50 20.13 o 6 2 5 251.90 231.41 26.63 o 7 2 5 66.38 22.89 29.58 o 8 2 5 186.68 107.97 55.16 o 1 3 5 16.88 20.72 5.92 o 2 3 5 4160.52 4141.47 88.62 o 3 3 5 2299.63 2321.73 56.92 o 4 3 5 2399.80 2564.75 73.81 o 5 3 5 715.42 715.80 34.29 o 6 3 5 236.89 209.35 31.96 o 7 3 5 530.99 481.19 138.51 o 8 3 5 4.40 -46.91 46.91 o 0 4 5 164.77 179.94 11.84 o 1 4 5 530.80 563.29 20.13 o 2 4 5 12.49 8.29 8.29 o 3 4 5 917.76 972.85 26.63 o 4 4 5 104.15 90.97 9.47 o 5 4 5 15.20 21.99 16.13 o 6 4 5 393.48 433.00 39.10 o 7 4 5 23.92 15.99 44.10 o 8 4 5 11.13 -44.03 69.85 o 1 5 5 876.31 819.28 23.44 o 2 5 5 475.07 504.44 37.88 o 3 5 5 6.48 14.02 17.76 o 4 5 5 173.50 182.32 15.39 o 5 5 5 7.11 0.56 14.16 o 6 5 5 88.61 62.26 30.94 o 7 5 5 15.61 -33.36 33.36 o 8 5 5 16.47 -31.65 52.01 o 0 6 5 361.33 324.37 21.31 o 1 6 5 1287.13 1310.16 35.73 o 2 6 5 479.87 469.67 17.52 o 3 6 5 271.75 299.86 19.20 o 4 6 5 229.12 219.27 15.76 o 5 6 5 1620.93 1773.93 46.52 o 6 6 5 4.48 6.66 26.17 o 7 6 5 21.24 -27.16 27.16 o 1 7 5 197.94 165.45 16.57 o 2 7 5 471.11 467.10 20.88 o 3 7 5 142.84 148.43 17.76 o 4 7 5 71.35 83.43 19.20 o 5 7 5 0.03 10.19 29.60 o 6 7 5 106.16 107.73 35.16 o 7 7 5 34.90 52.28 41.75 o 0 8 5 23.09 23.68 18.94 o 1 8 5 239.03 238.33 21.31 o 2 8 5 0.00 -4.74 15.07 o 3 8 5 296.20 310.27 27.88 o 4 8 5 110.87 144.33 29.26 o 5 8 5 2.40 12.26 23.26 o 6 8 5 5.25 -2.89 37.88 o 1 9 5 0.06 -3.50 19.20 o 2 9 5 232.24 236.52 48.54 o 3 9 5 148.36 136.29 31.81 o 4 9 5 0.63 27.52 33.15 o 5 9 5 2.51 -8.29 46.17 o 6 9 5 4.36 22.02 82.87 o 0 10 5 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30.78 o 7 2 6 36.46 13.21 47.52 o 8 2 6 277.16 280.42 73.81 o 1 3 6 353.41 391.86 11.72 o 2 3 6 300.84 293.81 17.76 o 3 3 6 42.01 47.67 8.29 o 4 3 6 893.03 916.56 28.41 o 5 3 6 70.32 54.56 18.77 o 6 3 6 415.60 411.61 31.68 o 7 3 6 26.81 14.21 46.88 o 8 3 6 35.28 24.29 80.50 o 0 4 6 334.95 340.95 16.57 o 1 4 6 44.75 38.68 5.68 o 2 4 6 50.28 40.29 9.09 o 3 4 6 15.37 7.75 9.09 o 4 4 6 420.61 373.63 22.49 o 5 4 6 68.76 56.82 18.19 o 6 4 6 24.28 32.09 22.22 o 7 4 6 51.72 91.70 49.37 o 8 4 6 0.73 -43.71 94.71 o 1 5 6 939.94 1040.13 25.91 o 2 5 6 10.16 9.47 11.84 o 3 5 6 602.22 656.48 46.17 o 4 5 6 149.30 152.66 14.79 o 5 5 6 211.50 196.99 16.13 o 6 5 6 26.78 53.12 36.70 o 7 5 6 2.41 -44.92 46.17 o 8 5 6 162.15 118.90 38.40 o 0 6 6 2355.58 2568.94 82.87 o 1 6 6 51.95 64.66 9.09 o 2 6 6 658.66 722.34 23.44 o 3 6 6 467.32 478.62 41.43 o 4 6 6 49.60 40.84 13.08 o 5 6 6 464.38 449.68 21.31 o 6 6 6 28.88 32.10 30.00 o 7 6 6 113.29 126.65 59.19 o 1 7 6 26.30 24.04 10.79 o 2 7 6 29.09 12.93 10.79 o 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